PROJECT NAMEEPA Region 5 Records Ctr
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SAMPLE DESCRIPTION
SITE NAME/TDDf_
CASE NUMBER
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SAMPLE I/STATION LOCATION
SAMPLING DATE 7 A?3/85/
ORGANIC TRAFFIC NUMBER
INORGANIC TRAFFIC NUMBER
SAMPLING TIME
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SAMPLE DESCRIPTION
SITE NAME/TDD*
CASE NUMBER
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SAMPLE I/STATION LOCATION S3
SAMPLING DATE "7/33/85
ORGANIC TRAFFIC NUMBER
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SAMPLING TIME
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SAMPLE DESCRIPTION
SITE NAME/TDDf
CASE NUMBER Ji"73o
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SAMPLE ^/STATION LOCATION £3 /
SAMPLING DATE 7/33/85/
ORGANIC TRAFFIC NUMBER
INORGANIC TRAFFIC NUMBER
SAMPLING TIME 73-.
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BOTTLE ANALYSIS TAG NUMBERS LOT NUMBER
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1 1PHYSICAL DESCRIPTION AT TIME OF COLLECTION:
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CONDUCTIVITY
TEMPERATURE
SAMPLE DESCRIPTION
SITE NAME/TDM
CASE NUMBER
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SAMPLE I/STATION LOCATION
SAMPLING DATE
ORGANIC TRAFFIC NUMBER
INORGANIC TRAFFIC NJ1BER
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SAMPLE DESCRIPTION
SITE NAME/TOP* CWLIL. UE
CASE NUMBER
60 .
SAMPLE ^/STATION LOCATION S5/
SAMPLING DATE 7/33/85_ / "
ORGANIC TRAFFIC NUMBER
INORGANIC TRAFFIC NIMBER
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SAMPLING TIME
BOTTLE ANALYSIS TAG NUMBERS | LOT NUMBER
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PHYSICAL DESCRIPTION AT TIME OF COLLECTION - CM*
PHYSICAL CHANGES FROM TIME OF COLLECTION UNTIL SHIPMENT:
INSTRUMENT READINGS
pH
CONDUCTIVITY
TEMPERATURE
ctiloroMthane
trana-1 . 2. -dichloroethanechlofofom1.2-dichloroethane2-butanone1.1,1-trichloroethanacarbon tetrachloridevinyl acetate
1, 1,2,2-tetrachloroethane1 , 2-dlchloropropanetrane— 1 , 3-dichloropropene
dibroanchloronethane1.1.2-trichloroethanebenzenecia-1 , 3-dichloropropene
brow) for*2 -hex •none
tetrachloroethenetoluenechlorobenzeneethylbenzene•t^ranatotal xyleneaN iitroaodiMathylaninephenolanilinabia(2-chloroethyl lather2-chlorophenol1 . 3-dichlorobenzena1 ,4-dichlorobenzenebenzyl alcohol1 , 2-dichlorobanzene2-Mthylptwnolbi«< 2-chloroiaopropyl ) ether4-MthylptwnolN-nitroao-di-n-propylaninehex •chloroethanenitrobenzeneiaophron*2-nitrophwwl2.4-diMthylphanolbenzole acidbia( 2-chloroethoxy }aethane2,4-dichloroprienol1 *2.ft-trichlorobanzenanapthalane•4-chloroanilinehaxach lorobut adiene4-chloro-5-«thylDh«nol
2-wthylneptheIene
hexachlorocyc lopant adiene
2.4.6-trichloroohenol2,4,5-trichlorophenol
2 -chlor onepht halana
2-nitroanlline
diHthyl phthalata
acencpthylene
3-nitriMnilina
acmchthana
2,4-dinitrophanol4-nitrophenol
dibenzofurrwn
2,4-dinitrotoluana
2 , 6-dinl t rotoluene
dlathylphthalata
4-chlorophanyl-phenyletharflouran*
4-nitroeniline
4.a -dlnitro-2-a»thvlDhenol
M-nitrModiptwnvlaBine
4-brflBMihenvl-ohaoyletharhMachlorobenzera
oi
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STATE SIKCMrCK if6 t-VAtAflt mo PAGE 1 OF 2, SET f
COMPOUND |
pantachlorophanol
phananthrane
•nthracana
dl-n-butylphthalsta
riuoranthana
banzidina
pyranabutylbonzylphthalate
3.3' -dichlorobenzidina
bia(2-athylha»vl )phthlate
chryaanaJi-n-octyl phthlnta
b*nzo(bok ) f luorant hena
indano(1.2,3-cd)pyrene
ditwnzo(a,h)anthracene
banzo(a,h,i)parylan«
alpha -8HC
bota-8te
dalta-aHC
aaama-8tC(lind»ne)
aldrin
andoaulfan I
dialdrin4,4'-DDE
andoaulfan II4.4--DDD
andoaulfan aulfate
4, 4 '-DDT•athoxychlor
andrin katona
chlorodana
tovaphana
Aroclor-1016
Aroclor-1221Aroclor-1232
Aroclor-1242Aroclor-1248
Aroclor-12M
Aroclor-1240
ELEMENT
aluiinui
antiaony
araanic
bariia
barylliuB
cadBiui
calcim
cnnaliai
cobalt
iron
load•aonaaiin
•anganaoa
•arcurynickal
nntaaalia
aalaniua
ailvar
aodiuithalllM
tinvanadiuB
zinccrania* CHECK IF ANALYZED (</
TENTATIVELY IDENTIFIED ORGAN I CS
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A
INTRODUCTION TO DATA TABLES
A SUMMARY OF THE ANALYTICAL RESULTS FOR SAMPLES WHICH WERE TAKEN DURING FIELD ACTIVITIES CAN BE FOUND IN THEFOLOWING TABLES. ONLY DETECTABLE CONCENTRATIONS ARE REPORTED. HOWEVER, IF THE COMPOUND HAS A FOOTNOTEFOLLOWING THE VALUE, CONSULT THE DEFINITION OF THE FOOTNOTE PROVIDED BELOW. ADDITIONAL QA/QC INFORMATION ISPROVIDED IN THE ATTACHED DATA SHEETS.
I) REPORTING UNITSA) ORGANICS
1) Water Samples - ug/1 or ppb (parts per billion)2) Soils or Sediments - ug/kg or ppb (parts per billion)
B) METALS1) Water Samples - ug/1 or ppb2) Soils or sediments - mg/kg or ppm
II) DEFINITION OF FOOTNOTES TO ANALYTICAL DATAA) ORGANICS
Footnote Definition InterpretationUJ
UBUJB
JB
RC
QN
Detection Limit (D.L.) is estimated because of a QualityControl (QC) protocol. D.L. is possibly above or belowContract Required Detection Limit (CRDL).Compound found in laboratory blank. No Value above CRDL.Compound found in laboratory blank, but not detected insample. CRDL is estimated because of a QC protocol.Compound found in blank. Two interpretations arepossible:a) If sample value is equivalent to D.L. to 5x blank
concentrationb) If sample value is greater than 5x the blank
concentrationCompound found in blank, value is estimated because ofQC protocol.Do Not Use Value. Major Violation of QC ProtocolValue adjusted for blank (an unacceptable procedure)
Value is above CRDL and is an estimated value becauseof a QC protocolNo Analytical ResultPresumptive evidence for the presence of a compound asused for a Tentatively Identified Compound (TIC)
Compound was not detected
Compound was not detectedCompound was not detected
Compound value is semi-quantitative.Compound value is quantitative
Compound value is semi-quantitativeCompound value is not usable.Compound value is semi-quantitativeCompound value is semi-quantitativeCompound was not detectedCompound value is semi-quantitative
B) METALS
FOOTNOTE DEFINITION INTERPRETATION
8
R
[ 1
UJ
J
Estimated or not reported due to interference,laboratory narrative.
See
Analysis by Method of Standard Additions (Look for a "+"Footnote)Spike recoveries outside QC protocols which indicates apossible matrix problem. Data may be biased high or lowS/e spike results and laboratory narrative.Duplicate value outside QC protocols which indicates apossible matrix problemCorrelation coefficient for standard additions is lessthan 0.995. See review and laboratory narrative.Value is real, but is above instrument D.L. and belowCRDLD.L. is estimated because of a QC protocol. D.L. ispossibly above or below CRDL.Value is above CRDL and is an estimated value becauseof a QC protocol.
Compound or element was notdetected or value is semi-quantitativeValue is quantative
Value may be quantitative orsemiquantitative
Value is semiquantitative
Data value is biased
Value may be quantitative orsemiquantitativeCompound or element was notdetectedValue is semiquantitative
ecology and environment, inc.ni WEST JACKSON ilVD.. CMCAGO. HJJNOIS «NM. TEL. 312-6B3-M16
i bi tf» Emwormnf
Date Received for Review: /o-/r-f5' Date Review Completed:
To:
Froa: Cynthia Pugh
Subject: d*r±ef Le<.TiLff R^-S**iO'5^
Sample Description: Case I > - no f f ro
Project Data Status: fi'l Qu« ;•*• •
FIT Data Review Findings:
c /5sfcee-f:
Additional CoaKnts:
i*vfe. I"
Book No.Page Mo.
recycled papir
UNFTED STATES ENVIRONMENTAL WOllCtON ACENCVftEOION V
»»* • I'D III/ % S~~».<«. .f •*.. « Cir *U , / RECEIVED OCT 1 5 1985Received for Review en *
Data User:
Ve hive reviewed the tfala for the following case(s)
SITE £&>. SM3 Cise Mo.No. Of ~_lD.U./Act1v1tjr
Set MD.J^6r^yy^' Straplet; ^ Kuwbers
MO.SMO Trifflc HP. _ _ _
Hrs. RequiredCLF Laboratory: /?/<.&- for Review:
Following are our findings.
?03*eA*3X>«J*J ttXo *>* 7"* G*• i ^% M
ccc
HOtti tre accept able for me.Dtti are acceptable for use with qualifications noted above.Data are preUnlftary - pending verification by Contractor laboratory.Data are unacceptable
ec: Or. Alfred Haeberer/Joan Fisk/Gary Ifar*. EPA Support ServicesRoss K. Robeson» CKSL-Las VegasDon Trees , ClrVSample Management Off let
CSO/Centn) fteiional laboratory
TMCKHI6 - R*H IOCT t 5 1985
CW. Data Set *>- *^ ^^^f IRWS to
SMO Case to. <f746 Site »aa»: 1-g^, x^rg ^^ - r '^
•f laboratory:
•o. 0f $i 1«s 3~ Ptte Staples
1. Have diif»-of-CttSto4y records been received?2. lUve Traffic reports been received? TES ^101. If DO, ire Traffic report nuafcers vr-tten on the chain- - jstody record? TESJHIO4. If ao. W»<ch Traffic report aue&ers ire alsting?
5. Are basic data for« te? TES(. Ruc6er of samples claimed: ^^ Mmaber of uoples received:
7. Checkedt teteived by Contract Project Hanaoeaent Section^^ ^^^ •
t. teview started: <7-3O-?S _ Reviewer Si (mature:10. Total ti»e spent en review: yr~.<~* tote review enrol eted:
11. Copied (xeroxed) ly: _ I _ *tt
12. Mailed to Bata U««r by: /Y£f/Z/4*r6>sj jOviA^ ttlt«s
TO PAT A PSEtSt
fill i« tli* blanks aad return tbis form to:
Ckarlaa Illy. MO. l.flon V.^SSCU.•
»J«
^4*<jtr*4t^ /-^X/C—14. Q.A. *aviaw roeaivad
15. ft*c»i*ad by OIL - CFM Saction for f 11.
-r </£>(£* vi c- Dior;*/
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RECEIVED C^ 1 5 TO
ENVIRONMENTAL RESEARCH GROUP, INC
117 N. First Ann Arbor. Michigan 48104 (313)662-3104
;ait 19, 1985
Pr Ijrtis Ross_S" - Region V51 ~3uth Clark StreetCr . al Regional LaboratoryI'.'.- rloorC--:2go, IL 60605
De£- Vr. Ross:
T.-r -ollowing report contains the final results for the chemicalana /sis of the five soil samples contained in RAS Case 4730. Thesam'-'es arrived in the laboratory on July 24, 1985 and were analyzedfor complete organics according to the September 1984 revision of theStatement of Work. The work was performed according to Contract63-31-6869.
OA AC Summary - GC/MS Semi-Volatiles
Zero of forty-eight surrogates were outside of OC limits. Six oftwenty-four matrix spike recoveries and three of twelve matrix spikeRPO's were outside of QC limits. OFTPP tuning criteria were met forall DFTPP spectra.
OA/QC Summary - GC/EC Pesticides/PCB's
Two of eight surrogate recoveries fell outside the OC limits for di-butyl chlorendate. Six of twelve matrix spike recoveries and two ofsix matrix spike RPO's were outside of OjC limits. In the pesticidematrix spikes heptachlor was not recovered.
If you have any questions regarding this case, please do not hesitateto contact me.
Sincerely,
V-vzf
Joseph A. hkiatowRAS Program Kanager
cc Linda BoyntonUSEPA Contract Lab ProgramSample Management Office
JAH:kg
rjir; 01 ice:' .' • - — • . o
Data Audit Staff ^ -— - 'USEPA Environmental MonitoringSystems Laboratory (EMS/LV)
Am* Arbor Chicago Cleveland Sax Francisco Minneapolis-Si. Paul
r.o. BO.SIS. 703/U7-2490
Organic*Analysis OatSSfii&aVEO GCT(PageD
Sampler fltunuMr
7*7
Laboratory Name:
Lab Sample 10 No:
Sample Matrix: __
Case No:6.77 QC Report No:
Contract No: _
Data ReJeas* Authorize*! By: >ata- Sample Received:
Volatile Compounds
Concentration: (Low") Medium .(Circle One)
Date Extracted/Prepare*
Date Analyzed:
JV-
Cone/Oil Factor. .
Percent Moisture:
PH-.
Percent Moisture (Decanted):
CASnlUfftOOT
uQ/lof<xi/Xa>*jt_ CASNumber
ug/l
74^7-374^3-975-01-*75-00-375-09-167-64-175-15-a75-35-*.75-34-3156-60-567-66-3107-06-2'78-93-371-65-656-23-5108-05-475-2T-*
Chloromethanan ^aromofnetna neVlnyi ChlorideOiloraethane^
Acnon*-Carbon Oisulfkto1. 1 -OichloroMhcne, i -uicnioriMinflnv
i ran*- 1 . z-uicniOToeirwfMChloroform1 . 2-OicMoroetri8ne2-8utanone
L reon i fit •cnionoeVinyi Acetat*Drofnooicnim m i MU unv
/•} u/3 u/^ u/^ u79 TBA? UA? T*.T U&. 7 W6.7 U3.5 TB
.fr.7 U// T3.S TS5.7 U/5 w6*7 W
JJ
79-34-578-87-510061-02-679-01-6124-48-179-00-571-43-210061-01-511 0-75-875-25-2591-78-8108-10-1127-18-4108-88-3108-90-7100-41-4.100-42-5
1 . 1.2. 2-T«tracr)loroathane1 . 2-Oicf)loroprooan«Trans- 1. 3-Oichlorooropan*Tricntoroetnen*Dibfornochloromatriana1.1. 2-Trichloroathan*Benzenects-1. 3-Oichloroorooena2-ChlorovthvlvtnvietherBromoform2-Hexanone4-Methvl-2-P«ntanon»reiracnioroetnanaToluena-CnlorebenzeneEtnvlbanzeneStyreneTotal Xyianas
0.18 T4.7 U6.7 U
i.V Td.7 Ue.,7 uJ.i u6,.7 U/^ U
6.7 <J/3 u/3 ul.L T/.^ T
^.7 U<*7 U6.7 UL.H U
«o GFA. ttw faNavMngn*t§ or loacnaw* optemmq
MCA flag mim b* aeMit.
i or •qi»4 to ttw C Thw ll*q icplm to UHOCIIJI
anMynd for Out miKmil tar tM Mmpto «Mh
(Thw M not HMMMI itw i««runMnt) 11w taomow Mieuid rMd: U-
tar tout notlimn tar
tm bMn eerrfirnMd by GC/MS. Singta10 rtfl/ul in m» «n«l «anei
thauU te eanfirmvd by GC/MS.
•' TIM flag i»UMdw(«niM«wlvi»M found in owbtankM «MN M a •mal*. R intfeMM BonbM/praONMMar* contamination and worm ma data uaar to taka
•nd foomoiM ITW baTrvQima touaad. tnwnuai ba <iuiy
. 1OJ) Form I 4/84.
Hum*. LRG.
CascNo:
Of Analysis Data Sheet(Page 2)
S«mpl» Number
Semivoiatfl* Compounds
« (low) Medium . (Ode One)
OmEx
OmAnalyad:
Cone/Oil FactorI T
CAS
Laboratory Mini*-.•RECEIVED C CT 1 5 1SS5 I s-mp* NT
Organic* Analysis Data Sheet(Page 3) ;
Pasticide/PCSs
Concentration: ^ Low^) Medium (Circle One)
Data Extracted/Prepared: -Z!
Date Analyzed:
Cone/Oil Factor
CASNumber
Vj s Volume at txtracx injwad (ul)
Vs >VolunMofvi«Mrtxtracad(ml)
W, * Weight of sampto mraoad (g|
V. • Volume of total (ul)
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-87421-93-4.
1031-07-850-29-377-43-553494-70-557-74.98001-35-212874-11-211104-28-2'.11141-16-883469-11-912672-29-611097-69-1
Alona-BHC8eta-8HCOelta-8HCGamma-8HC (Lindane)HeotacniorAldnnHeotachlor EooxidaEndosulfan 1OieMrtn4. 4.--OOE 'EndrinEndosulfan U4. 4--000Endrin AMenvdeEndosulfan Sulfate4. 4---OOTMetnoxycntorEndrin Ketone-OilordaneToxaoheneArador-1016Arodor-1221Arador- 1232Arador-l24ZArodor-1248.Arador- 1254.
1 1096-82-5 1 Arador- 1 260
3«> U5."? Ua.> u5.? 0<?.! 0a.> u3."? U31."? u5.4 uS.M U5.H U5.«4 U^ U5> 05.4- u5.f U
£7 05.H 0
i"?- U5f Uil> U3T UIT U3i 03T? U64- USH U
1/85
Nem-C7 1 5 1985
Mac. 473Q
Organic* Analysts Data Sheet(Page 4)
Tentatively Identified Compounds-
CAS KT or ScanConowittmoo
(uo/loraa/hofj
VGA2..J-.
5.
UNKNOIWMIOT M CPAMM I ffRMOV BNASNA
BNA
S..
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1/85
• laianaria. Vfrgmta 22313 703/987-2490 1 5 1985
Organic* Analysis Data Sheet(Page!)
Laboratory Name:
Lab Sample ID No:
Sample Matrix: —
Case No: (-VaZTtfZAjr)
eoSO,
QC Report No:
Contract No: _
Data Release Authorized Q_ Sample Received: t *-*
Volatile Compounds
Concentration: ( UJwp Medium (Circle One)
Data Extracted/Prepared: 7^/2.7^/75
Date Analyzed: 7/7,7/?5
Cone/Oil Factor /
Percent Moisture: _
.pH.
Percent Moisture (Decanted):
CAS ug/1
79-34-578-87-5
10061-02-679-01-8124-48-179-00-571-43-210061-01-5
110-75-875-25-2591-78-6108-10-1127-18-4
108-88-3108-90-7100-41-4.
100-42-5
1 . 1.2. 2-Tatrachloroatriana1 . 2-Oichtoroorooane
TricnloroethaneDibromochloromathana1.1. 2-TriehloroatfianeBanzana
cis-1. 3-Oictitoroorooene2-OiloroetfiylvinyleT,herBrofnoTOfTTi
2-Haxanona
TolueneChlorobanzana
StyranaTotal Xylanas>
£ . 5 U
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oHuooft icoonv. (inM isHnMt.) TFW foovnoM iriould
for but not
C This (tog •«*•• 10 osttieids MramanrsidwnrfieatMn hM b««n corrfirm«o by GC/MS. SingMcommiiBin p»iticid«i210 ng/ul in tft« ftnai wona•nouM tw GOfKimwd by GC/MS.
Tito flag w uMdv*wntM«n*lvw «found in ttwbtan*as w l M • sampM. It indicaws pos»M>/pMank oornaminanon and nwrns m« data usar to tau
Othar soaoAe flags and foomoMs may oa nqwrad topraoarty daftna tna rsaulta. If uaad. may muai Oa fully
I ana auoti daaenpnon atiauiad to ma data
Form I 4/8*-
Name. RECEIVED G C T 1 5 19S5
Nee
Orgamcs Analysis Data Sheet(Page 2)
eo
r )
Oat*
Semivotetile Compounds
i. ( j Mwtium ; (Grd« On.)
/Pra
i 1 (uroau
Cone/Oil
CAS
1/85
laboratory N*m«RECEIVED CCT 1 5
Organic* Analysis Data Sheet(Page 3)
PMticida/PCBs
Concentration: Medium . (GrcJeOrw)
Date Extracted/Prepaid/
Date Analyzed:
Factor
CASNumber
319-84-6319-«5-7
319-86-8
58-39-976-44-8
309-00-21024-57-3
959-98-860-57-1
72-55-972-20-833213-65-972-5447421-93-4
1031-07-8
50-29-372-43-553494-7O-S
57-74-98001-35-2
12874-11-2
11141-16-5
Aloria-SHCBeta-BHC
Delta-BHCGamma-BHC (LJndane)HeptachlorAldrm
Heptacrtlor EpoxideEndosulfan I
Oieldrin
4. 4--OOE
Endrin
Endosulfan U
4. 4.--000Endrin Aldehyde
Endosulfan Sulfate4. 4--OOT
MethoxychlorEndrin Keton*
Chlordan«
Aroctor-1016
63469-21-912672-29-61 1097-69-1
Arodor-1232Arodor-1242
Aredor-1248Aroctor-1254
5.2.C.Z9.2
9. -Z
/o .
/o/o/o/o92xo52
100
5152
/oo ./oo
_UJU_U_UU
_uv/
(J
S«mp4«-Number
orW.
V; * Volume of extract injected (ut)
V$ * Volume of water extracted (ml)
W, * Weight of sample extracted (g)
V, » Volume of total extract (id)
23.
wr
/ Q
1/85
ERG, inc. RECEIVED OCT 1 5 1985Sample Number
Organics Analysis Data Sh««t(Page 4)
Tentatively Identified Compounds
CAS RT or Scan
, ~K-L1-4 VGA i&s HQ2..X.
10..
It.. V/7 3YOSNA tro
/YoBNA ft* 3.00BNABNA
UNKNOWN- NOT IN EPA/NM UBRAMY BNABNA
1S~
ao:.2T.,
UNKNOWN-HOT M EPA/NIH UBRAHY BNA /YZQ
(MKNONM-MOT M EPA/NM U8RAHY SNA***
UNKNOWN NOT TN EPAINIH UBRAITr BNA (HO
BNA /rt/
24., UBRARY BNABNA 169
UNKNOWN -NOT M EPAWW UBRARY BNAJNA IJVZ. / Joo
BNAUNKNOWN NOT M EPA/K1H LIBRARY dNA /loo
UNKNOWN • NCT "4 BNA
1, PeVT B 1/8S
* a Bo*tit. \flrgm«22313 7O3/M7-X480
Organics Analysis. Data* Sheet(Pagel)
EO
Laboratory Name:
Lab Sample 10 No:
Sample- Matrix: _
Case No:
QC Report No:
Contract No: _
Oat» Release-Authorized l >TS«t>Sample-Received:
Coo
Volatile) CompoundsX^N
ntrationr ( Low
Oat* Extracted/Prepared: —.—
Date Analyzed: 7/Z7/* F
Cone/Oil Factor. .
Percent Moisture:
Medium (CirdeOne)
7/2.7/9S(so
Percent Moisture (Decanted): /vACAS
Number74^7-374^3-975-01-4-75-00-375-09-267-64-175-15-0TSi.35-4.75-34-3-156-60-567-66-3107-08-278-93-371-55-656-23-5108=05-4,75-27-4-
i«niuf Oin«u imoBrornometnaneVinyl Chloric*cnioroetnsno*Metnylene- ChlorideAcetone-Carbon Oisuifkfe, i *oicnioroeVtntnei
i, T*uicniuiiMtranv'Trint-i . z-oicnJOf uvtnoi it •Chlorafui MI!• "T HLntil ertl1 • X UIOIIOIUwU IBIiV
2-8ut»none
Carbon- Tetrachtorioe'Vinyl Acetate
15 » al«7. U
if. ai«» . o?/ • RIT. (/
7.9 </7 .? f7.«?7.T
f/t;
9 .9 797.9 U
7.7 .=r - *> ^7.9 <J
15' U7-*7 </
T
•
:
*
79-34-578-87-510061-02-679-01-6124-48-T79-00-571-43-210061-01-5110-75-875-25-2591-78-6:108-10-1
127-18-4108-88-7108-90-T100-41-4-100-42-5-
1.1.2. 2-T«trachJoroetriine1 . 2-Oiehlofootupane
Tnchtorot7th«n«Dioromocnioromeinane, i . 2- < ncnraroetnirie
Benzenecis-1. 3-Oicritoraorooenel-Chloroetnylvinylether
2-H»wjnone*'Meinyi 2-PwitanotwlecracnioroetnerwToluene*
cthylbenzene •StyreneTotal Xytanct
7 . 5 '.i . <; (,-'7-9 (J7 .«T J\7.5 t/|7. 9 o'7 .9 J7.7 v
/9. «>7 -<T J
15 • \J15 -
/ -j? r7-9 i.'7-9 JT. T J7-9 J7 -*? f
u«» w 9Ai «• MtoMing i
<Mtiiiiiuii of MCA flag mu« M apiiat.
•»iirtiuiiun hat bMn uunlirmad by GC/MS. SinqMuummm* pMOadM210 ng/ul in tfw HnM wmei«tauU b* confcrm«d by GC/MS.
8 Tta«taoisuMd<i*wntiM»nMYttwfoundintn«M»m. (Thi*isnai(
i taror.) Tb»«oatna»««auW "«t U-ml LUM »iml\md tm hiit rrin -f-mr1 Tw"
i limit far
i md wamiitw 4m UMT to taka
mmiij mtini mi mnfn "iimi T-T~md Meh dnenpaon amthad to tn»<toa
Form I
Name:
CM* No:
Organics Analysts Data Sheet(Page 2)
G71
Conomn
Cbnc/WJ
CAS
No:
Organic* Analysts Data- Shear(Page 3)
Sample Number
BO 47?
Concentratioi
Date- Extracts
Oatec Analyze*
Cone/Oil Fac
CASNumber319-84^319-85-7319-86-858-39-97S-A4-3
309-00-21024-57-3959-98-860-57-171-55-972-20-833233-45-97Z-54-87421-93-4.
1031-07-8*50-29-3T2-43-5-53494-70-557-74-9-8001-35-212874.t1.2-11104-28-2"T1141-16-S53489- 11 -9>
12ff72--23-6tii^KC^-aaiiil I.SVM
Pesticide/ PC8s r
i: ( y Medium (GrdeOne)rt/0r^»rm<*- / ~O^ 7 ~§O
d" o F 25 Vij
1
AJorta-SHC
8eta-8HCOelta-8HCGamma-SHC (Lindane)H«otacftlorAJdnnH«otacnior ggoxideEndosulfan 1Oiefdrin4. 4--OOE 'EndnnEndosulfan U4. 4.'-OOa
EndhrrAldenvdeEndosutfan Sulfate4. 4---ODT
EndhnKetoneChlordaneToaohene'Arador-f016Arocior-1221Anjctor-l23ZArodorv124iArodor-tZ4ffArodor-1254.Arodor-1260
•3.0 u3.O 03-0 0S.O Ui.o u3.0 U3.0 U3.0 U10.0 0(o.O 0
(ff.O 0(*.o u4..0 o(a.O Ul*.o uU-0 0
5O U(o.O 0
30 o(.0 U30 u3o U3o O3o U3.0 OUKT U
<K) U
Vj * Volume of extract injected (ul)
Vs * Volume of weter extracted (ml)
W, 'Weight of sample extncted (a)
Vt 'Volume of total extract (ul)
„„ oW.^7<5L yffl^t^
DECEIVED OCT I 5 1385
1/85
[.-(Page A) 5 ' f3 i i.
^ n • •wontpouDECEIVED O C T 1 51385
ini4m
*/--• KTor
-V VITAr.X..A..
§..
9..
IT.. 397 J/o
BNA ill 300BNA /.too
SNAUNKNnwN-NOr IN EnUNiM (JBRAftr dNA tot?
BNA"BNA"
ffzf S/o6 TO
CLP S«npl»M«nig*nwni Oftter.J1 <-/ - J O I L- L f
•ai •» Vkginw.22313 703/967-2480
Organic* Analysis Data Sheet(Pagel)
Sample Number
60
Laboratory Name:
Lab Sample ID No:
6^6r.f*/C, Case No: 4-730
£ample> Matrix: -
Data- Release Authorized'
QC Report No:
Contract No: - £ 7- O/ -£&?
'XTcui Jatfr Sample Received: Ih
Volatile1 Compound?
rationr ow Medium- (Circle One)
Date Analyzed:
7/27/r^ RECEIVEb.GET 1 5 1855
Cone/Oil Factor ,
Percent Moisture:
7.?
CAS.Number
Percent Moisture (Decanted):
uO/lonbg/Kg.)
A/A
CASNumber
ug/lordg/Kg
74^7-374-83-975-OT-475-00-375-09-28T-84-175-1 oXT75-35-4.75-34-
156-60-56T-68-3>-10T-08-278-93-T71-55-8^Sff.23-5108-05-4-.71-.2T-4i
CMororrwman*OrOmOfirVinel ITff
Viny* Chtohda-iioreatnane1
Metnvten»Chterxie•Aeaton*Carbon Diauffide1. 1-Oietiloroathana-1. 1-OtchtoroaihanaTrana-1 . 2-Otehtoroatnen*Cntorotorm. 2-ulcnioreainane>
2-Sutanorw1, 1. r-rriehtoroetnene*Cartaorr TatrecntorideVlnv* Acetate
14.!*• .14 .
uJu
14 - W3L. 9\± . UL.\U .9
uu
i .9 (J(. -? u3 -5JBL .X U
2.T.3 .^£ -5
JM--
tipuu
t ,?r *;
0J
•
1 79-34-5 1 . 1 . 2. 2-T«traehlort»thaneT. Z-Oicftloroorooan*
ttv.icv'Ca Trans- 1 . 3-Oicrilorooroo«ne
124-48-179-00-571-43-210061-OV-S110-75-8.7S-25-2:591-78-81 08-10- V127-18-4108 88-3:108-90-7
100-42--?
Dibromocftloi umeihana*1.1. 2-TncnloreetnaneBanzan*-eis-1 . 3-Oich»oroorooana-
BramoformZ-Hexanona-4-Metnyl-2-Pantanon«-
•Toiuene-Chlorebanzana'EtnylbamarwSlvraneTotal Xylenas
L . 3 »-
<. .
.? Ul
vl
m-/, -T u
-r
X .? U
inwnr* ***n tfwrws IMWI confirmed by GC/MS. SingleMoadM£10 ng/ul in OM ftn«4 mna
Th» ftof it uMrt <«*i«n VM «n«lvw i* found in th» bUnfcwwoN Ma «mot«. It indicMMponAM/grodoM*Monk eontammmon «nd worn* in* <Ma UMT to taka
Oftir^^flcftoonndfiHftM iin ittttn If !•«! TTITT ~iai ni' I"TrcndMCfic
ito« 10J) Form I 4/84.
Name. EJU2*.
No:
Organic*. Analysis Data Shoot(Page 2)
SanWoiataa. Compounds.
Caneantrabon: <^w) Madiuny (GrdaOna)AT/^ & /9 ^^^^On§ £flu n_itrf/pftpgr^^ / /1 +~ * / *-*
Oata.Anaiyad:
Cone/Oil
CAS
1/85
laboratory Name.LRCL, Inc.
Qrganies Analysis Datasheet(Page 3)
Sampi* Number
Pesticide/PCSsConcentration: Medium
Data- Extracted/Prepared:
(Ord.On., CE|VED
-7-ys"~Cone/Oil Factor
CASNumber319-34-3319-35-T319-86-858-39-978-44-3309-00-21024-57-3959-98-380-57-172-55-972-20-8;33213-65-972V54-8
74Z1-93-*103.T-07-8;5O-29-372 41-r53494.70-587-74.98001 -3S-I128T4-!1- r11104-28-1TT141-16r«83489-ZT-912872-29-4-11097-49-111098-82-5
Alorti-3HCBeta-8HCO^W-SHCGamma-SHC (LJndane)HeptacftlorAldnnHeotacntor Eooxid*Endosulfan 1OwWnn4. 4.--OOE. '&iorinEnooauifan H4. 4. 00Endnn AldefivbeEndosuifan Sulfata4,4:4501MethoxyerilorErtdhir Katoo*OitordaneToMohene*Arodor-IOIffArocior-1221Arecter-1232Arador-1242,Arodor-1248Anxaor-125*Arodor-1260
^.> oa.f ua.> ui.> 03..T u?.T 03.? L>3.1 O5.f U5.«f 0S.f- U5.f 05.«t- 0S.v 05,f US.«f U
i> 05.** U
*•?- o54- 03> U^r U*7 UJL> Ua? o6H- US«f O
Vj * Volume of extract injected (ul)
Vf » Volume of water extracted (ml)
W_. *WeiQnt of sample extracted (o)
V, 'Volume of total extract (ul)
•W.
Puiin 1 1/85-
Organic* Analysis Data Shoot(Page 4) J *.'
ldantHfed Compounds. '.^tCElVEDCCT 1 5
KT or
VGA /2.0
3NA 373- 2,40
2 2 '- BNA
is.
^
tOftaiVb*nu223l3 7O3/H7-2490
Semp»e Numoer
EO 4.g/Organics Analysis Data Sheet
(Page 1)
Laboratory Name:
Lab Sample 10 No:
Case No:
Sample Matrix: .—
*5ata Refeas* Authorized By:
QC Report No:
Contract No: -
DatetSample Received:
Volatile CompoundsConcentration: (Csw} Medium , (Cirde One)
Oater Extracted/Prepared; J/7'7
Date Analyzed: 7/&7/?5RECEIVED G C T 1 51985
Cone/Oil Factor .
Percent Moisture:
Percent Moisture (Decanted): /VA
iULd
CAS ug/lor^g/Kg
•
JTu
79-34-578-87-5
1. 1.2. 2-tetracfiloroMhane1 . 2-Oichlorooropane
1 0061 -02-8 Trans- 1 , 3-Oicrttorooroo«ne
•>
I
•
-
*
*
4
*
*
*
f
f
79-01 -a124-48-179-00-S7T-43-210061-01-5110--75-8'75-25-159T-78-6108-10-112T-18^108-88-3108-90-T100 -1-4-100-42-5-
1.1. Z-TrietiloitMtfian*B«nan»cis-l. 3-Oichlorooropene2-Chkxo«fTvlvinvlether
2-H*unone4-M«tMv<-2-P«n«non«
TolucrwCMorotMnz«n«
StvrenaTotal Xvi«n«s-
9.^ Ul
?.6 vl
9.6 uiTr.H- T5 .6. C/5.6 y? .6 jy
• 9.6 y//. u? .6, (///. UII . U2..L, T!/-/ JlT -L UC .ir aT- 6 0< - e. \J
IMa flag aopliaa won has baan eontiimad by GC/MS. Singto
noda lO no/ul in torn final <
aiem. (Tn* « notHmt.) Tb* tooMMw «euid rawt U-
far Minai dMKHd. Tlwilli»Ml<i il «riii«i timct far
Mould b« cenfimwd by GC/MS.
B Thai flag muaad whan tna analwn found in ma blankaawaM a i aMnaM. «indteaiaa poea*ia/orobebleWank contamination and «amt ma data uaar w taka
Ottwr spaoiflc ftoaj'and feooiotaa may ba raajuifvd toproparty UaOiia Hia i amftj. If uaad. mar rnual b»1uit»
.1QJ) Form I 4/84-
411°Organic* Analyst* Data Shaat
(Page 2)
Cancm
DOT
Mwiium / (On3«Om)
Conc/DH „* *
CAS
1/85
ne:.
Organics- Analysis- Data Sheet(Page 3)
Pesticide/PCBs. i >
LovO Medium /(GrpleOne)Concentration:
D«tt>Extracted/Prepai
Date Analyzed:
" 7/iura
/»t/s15
Cone/Oil Factor.
CAS
319-84^319-«5-r319-86-858-89-976-44^309-00-21024-57-3959-98-860-57-172-S5-&72.20-833213-65-9-72-544
1031-07-8
Aloha-BHC8ata-8HCOa(ti-8HCGamma-SHC (UndanelHeptacftlorAldrinHeptactilof EpoxidaEndosulfan IOieWnn4, 4---OOEEndnnEndosulfan U4.4M)00
50-29-372-43.5153494-70-fr
8001 -35- r12674-11-2
Endoauifan Sulfatar4i4:-OOTMetnoxychlorEndnnCMofdana*ToupnanaAredoMOtfi
|11096-82-& | Aroctor-1260
•V ."5
V . 5.«;
. o
JS-i.
Vj *Vohmw of extract injected (ul|
Vf 'Volume of water extracted (ml)•
W, *We*Qht of sample extracted (9)
V, *Velunwof-tDta«4
U
o
.5 u
.s u
1 .0 V. O (J
1 . o U.0 \J.0 V
U*l .0 \J
U_i£U
JLV
(J
Sample Numberpie Number
£68)
n
v
l-
EstimatedConcafitnjjiQn'
(ug/t orijg/in
/do
J?0
tloo(7<*
.ZV0
179/?o/froSfO
V60
6YO
730
?/«/^ooloo6 -Jo6Jo/ Z O O
130
orW.
1/85
FUIIII 1 1/85
ecology and environment, inc.ZD WEST JACKSON •LVD.. CHICAGO. HUNOIS 80606. TEL. 312-663 HIS
Date Received for Review: % -'V/S'' Date Review Completed:
To: fi .K
From: Cynthia Bachunas /
Subject: '^/-/V' -*' , --' /,J ^ ~-- f~ s~i •_.<_ ^._c^^x.^ -
Sample Description: (*A_\f- jf 73<
Project Data Status: k/j/ ,'/ '.s - - - -<. *y> ^ _ '#/l *-*•
FIT Data Review Findings
Additional Comments:
UNITED STATES ENVIRONMENTAL FRDTECTON AGENCYREGION V
UCCT. Review ef Region V CLF DiUReceived for Review on
Curtis Ross, Director (SSCRL)Centrtl Regional laboratory
Data User:
Ve have reviewed the data for the following Cise(s).
*t£.&SITE
EPA Data Set No.
CRL No.
o oSampl es ;
SH3 Case No.D.U./Act1vity
Nunfcers
Traffic Mo.
CLP Laboratory:.Mrs. Requiredfor Review:
Following are our findings.
MEDM7
HData are acceptable for we.Data are acceptable for vse with qualifications noted above.Data are preliminary - pending verification by Contractor Laboratory.Data are unacceptable.
ee: Dr. Alfred Haeberer/Joan FUk/Gtry Ward. EPA Support ServicesRoss K. Robeson. EXSI-Ias VegasDon Trees. CLP/Sample Management Office
PA POM* UCM
ISO/Central Regional laboratory
DATA TMCKIK6 - FDHH I
ML Data Set to. T/ <?-?<S<T EKIUS to
PC Case to. */73t> Site toae: . f . ^
vt laboratory: / j & f - Data
to. *f Susies: -T Dite Sables »ecet»ed:
1. lUve dialfi-of-cttsto<y records been received? TES »0
t. Have Traffic reports been received? TES x^»3. If no. are Traffic report maters written en the chaln-of-custody record?
4. If no. %l)1ch Traffic report nuofrers are
$. Are basic data fortt In? IES6. Kutfcer of samples dated: ^ Iba6er of saaples received:
7.t. Received by Contract Project Management Section;». Review tt>rt>d; /- //I- ?? Itevletier Slonatiirg:
10. Total t1a» »pent en review: / 'ji 'Date rtvlew
11. Copied (xeroxed) *:_ __ *****
12. Mailed to Bat* W»«r by: _ _ »*t«:
TO PAT A PSEtSt
?!<••• fill !• t*« blanks ••< v*t«ra tfcl» form to:
Blly. MO. t.gion ?. 5SCIL
1J. Bat a vacaivai bys
14. Q.A. waviaw racaivaa1 byt
15. maeaivai by CM. - C?M faeti»« for ffil* bys
i^ j
DATA RE TEW SHEET
CASE Hf </7.5DATA SET t
LAB Q.C.HfDATE: /- 16, -
¥$ttMATRIX:CONC. :
REVIEW
WATER SAMPLE SPK.WATER SAMPLE DUP.SOIL SAMPLE SPK.SOIL SAMPLE DUP.
Matales
2. Antimony
3. Araenlc
4. Barium
5, Beryllium
6. Cadmium
7. Calcium
8. Chromium
9* Cobalt
10. Copper
11. Iron
12. Uad
13. Magnealum
14. Manganeae
15. Mercury
16. Nickel
17. Potasaium
18. Selenium
19. Silver
20. Sodium
21. Thallium
22. Vanadium
23. zinc
24. Cyanide
Others /^
CALIBRATIONTry crv ccv
,
•
ii
\
flwrS
>?^^»-
•>"*•
gi
rrv
'
BLANKSTfflrnffRRP PREP
'
ICP INTE1TNT E T N A
M. SPIKE DUPLICATEr u / A T F
••
SnTllWATE
/7 %
?&%
&1.
sniT.LC.S•STRP RnTT
•
,
•
Form I
U.S. EPA Contract Laboratory ProgramSaaple Management OfficeP.O. Box 818 - Alexandria. VA 223137C3/557-2490 FTS: 8-557-2490
EPA Sample No.MED543
J>/ - ' *!l L
Date S-14-S5
INORGANIC ANALYSIS DATA SHEET
LAB SAKE ROCKY MOUNTAIN ANALYTICAL CASE NO. 4730sov NO. 734LAB SAMPLE ID. NO.
Concentration :Matrix: Vater
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
ALUMIFJM
ANTIMONY
ARSEIIC
BARIUM
EERYLLIUX
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPE*
IRON
irn^Cvanlde *
Elements
Low XSoil
2110
[20]
40
6.8U
[0.3]
8.2
190000
307
[161
22
133000
37
1.2
Identified
X
mg/
P
p
\*
F
P
P
P
P
P
P
P
P
AS
QC
and Measured
HediuaSludge
kg dry
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
we i gnt
MAGNESIUM
MANGANESE
MESCUSY
IICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
Percent Solids O
REPORT NO. 55127
Other
[1390]
1100
0 . 057U
88
553U
28U
7.6
[1740]
5.7U
9.7U
[11]
23
i) 88
1
P
P
CV
P
P
F R
P
P *
F R
P R
P
P
Footnotes: For reporting results to EPA. standard result qualifiers areused as defined on Cover Page. Additional flags or footnotesexplaining results are encouraged. Deiinltion of such flagsmust be explicit and contained on Cover Page, however.
Coacaents:
RECEIVED AUB \ 9
Lab Manager
Form I
U.S. EPA Contract Laboratory ProgramSample Management OfficeP.O. Box 818 - Alexandria, VA 22313703/557-2490 FTS: 8-557-2490
EPA Sample No.MED544
Date 8-14-85
INORGANIC ANALYSIS DATA SHEET
LAB NAME ROCKY MOUNTAIN ANALYTICALSOW NO. 784LAB SAMPLE ID. NO.
CASE NO. 4730
QC REPORT NO. 5512^
Elements Identified and Measured
Concentration:Matrix-. Water-
Low Xr* _ j -iOUl 1 X
MediumSludge Other
msr/k.ar dry weight
1.
""2.
3.
4.
..-•5.
6.
7.
8.
9.
''10.
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
3820
19U
33
[61]
[0.32]
4
116000
197
[121
35
P
P
P
P
P
P
P
P
P
P
13. MAGNESIUM 6310
14.? MANGANESE 800
15. MERCURY 0.17 CV
16. //HICKEL
17. POTASSIUM
65
604U
18.^SELENIUM 18U F R
19. SILVER [4.51
20. SODIUM
V THALLIUM
[1060] P
21.l 6.1U F R
22. "'TIN 10U P R
11. IRON 87300 23. VANADIUM [17]
12. LEAD 137 24. ZINC 96
Cyanide 0.95 AS Percent Solids (%) 82
Footnotes: For reporting results to EPA, standard result qualifiers areused as defined on Cover Page. Additional flags or footnotesexplaining results are encouraged. Definition of such flagsmust be explicit and contained on Cover Page, however.
Comments:
T 3 7985
Lab Manager
Fora I
U.S. EPA Contract Laboratory FrotramSample Management OfiiceP.O. Bex 818 - Alexandria. VA 22213722/557-2493 FTS: 8-557-2493
ti~A Sample No.MED545
Date 8-14-S5
ISGR-3ASIC ANALYSIS DATA SHEET
LAB SAME ROCKY MOUNTAIN ANALYTICAL CASE HO. 4730sow SO. 7S4LAB SAMPLE ID. NO.
Concentration:Matrix: Water
1.
2.
3.
4.
5.
6.
7.
6.
10.
11.
12.
ALUM I SUM
AST I MO BY
ARSEIIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER-
IRON
LEAD
Cyanide
Elements
Low XSoil
[231
34
[10]
0.2U
5.7
171000
304
[15)
29
149000
27
1 . 2
Identified
X
ing /kg
P
P
P
P
P
P
P
P
P
P
P
P
AS
OC REPORT NO. 55127
and Measured
MediumSiudire Other ^
cry
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
weight
MAGNESIUM
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
Percent Solids (%>
[20501
919
0 . 067U
92
660U
33U
8.3
[12401
5.7U
11U
[161
36
75
P
CV
P
P
F R
P *_-•
P
F R
P R
P
P
Footnotes: For reporting results to EPA, standard result qualifiers areused as defined on Cover Page. Additional flags or footnotesexplaining results are encouracred. Definition of such flagsmust be explicit and contained on Cover Page, however.
Consents:
Lab Manaser
Form I
U.S. EPA Contract Laboratory ProgramSample Management OfficeP.O. Box 818 - Alexandria, VA 22313703/557-2490 FTS: 8-557-2490
!EFA Sample No.! MED546
Date 8-14-85
INORGANIC ANALYSIS DATA SHEET
LAB NAME ROCKY MOUNTAIN ANALYTICALSOW NO. 784LAB SAMPLE ID. NO.
CASE NO. 4730
QC REPORT NO. 55127
Elements Identified and Measured
Concentration: Low X MediumMatrix: Water
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
C ADM I UK
CALCIUM
CHROMIUM
COBALT
COPPER*
IRON
LEAD**
Cyanide
Soil
2370
19U
36
[123
[0.23
7
168000
319
[141
24
132000
25
0.95
X Sludge Other
rog/kg dry weight
P 13. MAGNESIUM
P
P
P
P
P
P
P
P
P
P
P
AS
14.
15.
16.
17.
IS.
19.
20.
21.
22.
23.
24.
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
Percent Solids <%)
[1790]
1030
0.061U
121
604U
30U
[5.8]
[1410]
6.1U
10U
[15]
26
82
P
P
CV
P
P
F R
P
P
F R
P R
P
P
Footnotes:
Comments:
For reporting results to EPA, standard result qualifiers areused as defined on Cover Page. Additional flags or footnotesexplaining results are encouraged. Definition of such flagsmust be explicit and contained on Cover Page, however.
DECEIVED AUB 1 9 1985
Lab Manager
U.S. EPA Contract Laboratory ProgramSample Management OfficeP.O". Box 61S - Alexandria, VA 22313"33/557-2490 FTS: 8-557-2490
EPA Sample So.'.-.,«.) MED547
Date 8-14-85
I50RGASIC ANALYSIS DATA SHEET
LAB EAXE ROCKY MOUNTAIN ANALYTICAL CASE NO. 4730SOV NO. 7S4LAB SAXPLE ID. SO.
Concentration:Matrix: Vater
2
3.
5.
6.
7.
8.
9.
10
11
12
.
ANTIMONY
ARSES 1C
BARIUM
BERYLLIUM
CADXrJX
CALCIUM
CHROMIUM
COBALT
. COPPER
. IROH
. LEAD
Cyanide
Eleaeiits
Low XSoil
i"T?
i i
[42]
C0.18]
2.2U
61000
33
[4.61
93
16700
70
0 . 56U
I dent 1:
X
P
F
F
P
P
p
P
P
P
P
P
F
AS
:ied
.„
dry
13
14
15
16
17
IS
19
20
21
22
23
24
0(
and Measured
Mediumlud^e
weight
. MAGNESIUM
. MANGANESE
. XERCURY
. NICKEL
. POT ASS I UX
. SELENIUM
. SILVER
. SODIUX
. THALLIUM
. TIN
. VANADIUM
. ZINC
Percent Solids <
: REPORT NO. 55127
Other
1-700
351
0.24
[16]
556U
2.SU
1.7U
[1070]
X!I 1.111
9.6U
[13]
89
:*> 89
>
P
P
CV
P
P
F P.
P *
P
F R
P R
P
P
Footnotes: For reporting results to EPA. standard result qualifiers areused as defined on Cover Page. Additional flags or footnotesexplaining results are encouraged. Definition of such flagsmust be explicit and contained on Cover Page, however.
Comments:
Lab Manager
Form 111
Q.C. Report No. 55127
BLANKS
LAB NAME ROCKYDATE
MOUNTAIN ANALYTICAL8-14-85
CASE NO. 4730UNITS ut
Matrix SOIL
! InitialPreparation ! Calibration. CoraDound 1 Blank ValueMetals: !
ii
1. ALUMINUM ! 25U2. ANTIMONY ! 31U3. ARSENIC i 21U4. BARIUM 1 12U5. BERYLLIUM: o.au6. CADMIUM ', 4U7. CALCIUM ! 280U8. CHROMIUM ; 4U9. COBALT ! 4U10. COPPER ! 3U11. IRON : 15U12. LEAD 1 15U13. MAGNESIUM: 250u14. MANGANESE: su15. MERCURY ! 0, 1 U16. NICKEL ! 5U17. POTASSIUM! 990U18. SELENIUM ! Jo,19. SILVER 1 3U20. SODIUM ! 590U21. THALLIUM ! 3 U22. TIN ! 17U23. VANADIUM ', 4U24. ZINC ! 2UOther: Afc&tlO 3*.
ffJ\-fyCyanide ! /O u
Continuing Calibration
1
25U31U21U12U0 . 3U4U280U4U4U3U[20]15U250U5U0.1 U5U990U33U590U3U17U4U2U3M,
10*
Blank Value2 3
3u
3U
<&
TM
4
PrtDarationBlank1 2
[73]31U21U12U0.3U4U280U4U4U3U[24]15U250U5Uo.iu5U990U
! 3t,: suI 590U: 3 U: 17U: 4U: [2.7]: 3u\! Inu
P
P
F
RECEIVED AU8HW5
rcrm V
Q.C. resort No. 5512?
DATE
XATSIX SOIL
EFA Ssaole No. HED543Lab Sinpis ID No.Units
Ccs-rouT-i
1. ALUM I SUM2. AS: i y. csv3. ARctSIC4. BARIUM5. BERYLLIUM6. CALCIUM7. CALCIUM8. CHROMIUM9. COBALT10. CCPrER11. ISO'S12. LEAD13. MAGICS i'JX14. MAKGASE.EE15. MERCUr.Y16. IICKEL17. POTASSIUM18. SELES !UM19. SILVER20. SODIUM21. THALLIUM22. Til23. VASADIUM24. ZISCOther:
Cvariide
•^c--Tr-l T i x < - . £sl>~d Samel er,?. ; ?. isx.lt <£££<
75-125 . 162075-125 : 2i575-125 ' 2"£7^-125 : 1C20"5-125 : 2475-125 : 2Z'5-125 . 16700075-125 : 35675-125 ; 252•~e;_ • - • '. «-5• j :. * • i. *»ii^5-125 I 11800075-125 : 26975-125 : [598175-125 : 122075-125 : 0.5175-125 : 31575-125 : 495U75-125 : 15U75-125 : 3475-125 : [1380]75-125 : 1875-125 : 13775-125 : 25875-125 : 270
;
75-125 : 5.5
O -T Itl Tj i. Ci
* k — - \i i. u *- w'iv f
I860[17]356U[0.26]7.2167000270[1432011700033[1670]9680.05U77495U25U6.7[154015U8.5U[9.4]21
1.1
SID iked.Added <SA)
SR25*25010002525NR
100250125N£
250S3
2500.5250
KR525
NR25250250250
5
/£*•."
879410295las
8S9598
94
101
10295
0
109
725599100
881 %R = USSR - E3;/SA] x"F"- out 01 controlCoameiits:
100
I S I8B3
Form VI
Q.C. Report No. 5512?
DUPLICATES
LAB NAME ROCKY MOUNTAIN ANALYTICAL CASE NO. 4730
DATE 8-14-85
Matrix SOIL
EPA Sample No. MED543DLab Sample ID No. ^_Units
CoinDoundMetals:1. ALUMINUM2. ANTIMONY3. ARSENIC4. BARIUM5. BERYLLIUM6. CADMIUM7. CALCIUM8. CHROMIUM9. COBALT10. COPPER11. IRON12. LEAD13. MAGNESIUM14. MANGANESE15. MERCURY16. NICKEL17. POTASSIUM13. SELENIUM19. SILVER20. SODIUM21. THALLIUM22. TIN23. VANADIUM24. ZINCOther :
Cyanide
Control Limit1 : SaiatjieCS)
! I860: [17]; 35; eui [0.261: 7.2
167000: 270: [143: 20! 117000: 33: [1670]I 968: 0.05U: 77! 495U! 25U! 6.7! [1540]! 5U! 8.5U: [9.4]: 21(i
t
; 1.1
Du^iicate^P'
1850[20]296U0.15U6.7166000265[13]1712000027[670]10200.05U78495U25U6.4[1250]5U8.5U[9.8]18
1.0
RFD2
0.54NC19NCNC7.20.61.9NC162.520NC5.2NC1.3NCNC4.6NCNCNCNC15
9.5
X Out of Control1 To be added at a later date. 2 RPD = [ !S-D! /< fS+D>/2>']'NC - Non calculable RFD due to value(s) less than CRDL
x
