Memorandum transmitting Sample Analysis Results for ASR ... · ASR Number: 6763 Project ID:...

United States Environmental Protection Agency Region 7

300 Minnesota Avenue Kansas City, KS 66101

APR 2 9 Transmittal of Sample Analysis Results for ASR #: 6763

Project ID: SFA72Q00

Project Description: PCE Former Dry Cleaner sampling

Margaret E.W. St. Germain, Chief Ff{ Laboratory Technology & Analysis Branchy Environmental Sciences & Technology Division

To: Susan Fisher SUPR/ERNB

Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) and Project. The Regional Laboratory has reviewed and verified the results in accordance with procedures described in our Quality Manual (QM). In addition to all of the analytical results, this transmittal contains pertinent information that may have influenced the reported results and documents any deviations from the established requirements of the QM.

Please contact us within 14 days of receipt of this package if you determine there is a need for any changes. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/Sample Release memo for this ASR as soon as possible. The process of disposing of the samples for this ASR will be initiated 30 days from the date of this transmittal unless an alternate release date is specified on the Data Disposition/Sample Release memo.

If you have any questions or concerns relating to this data package, contact our customer service line at 913-551-5295.

Enclosures

cc: Analytical Data File.

Date:

Subject:

From:

40492016 A°

Page 1 of 14 Superfund

£5 Oh - t00

ASR Number: 6763 Summary of Project Information 04/29/2015

Project Manager: Susan Fisher Org: SUPR/ERNB Phone: 913-551-7919

Project ID: SFA72Q00 QAPP Number: IN PROCESS

Project Desc: PCE Former Dry Cleaner sampling

Location: Atlantic State: Iowa Program: Superfund

Site Name: PCE FORMER DRY CLEANER - SITE Site ID: A72Q Site OU: 00 EVALUATION/DISPOSITION GPRA PRC: 303DC6

Purpose: Site Cleanup Support

Removal assessment support VOC indoor air sampling at PCE Former Dry Cleaner. Per THankins email dated 2/24/15: Site name used to be Atlantic Water Supply.

Explanation of Codes, Units and Qualifiers used on this report

Sample QC Codes: QC Codes identify the type of Units: Specific units in which results are sample for quality control purpose. reported.

= Field Sample ug/m3 = Micrograms per Cubic Meter

Data Qualifiers: Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.

(Blank)= Values have been reviewed and found acceptable for use. U = The analyte was not detected at or above the reporting limit.

UJ = The analyte was not detected at or above the reporting limit. The reporting limit is an estimate.

J = The identification of the analyte is acceptable; the reported value is an estimate.

Page 2 of 14

ASR Number: 6763


Sample Information Summary


04/29/2015

Sample QC External Start Start End End Receipt No Code Matrix Location Description Sample No Date Time Date Time Date

1 - _ Air 1013 East Third - Sub-slab 03/30/2015 16:30 03/31/2015 16:15 04/03/2015

2 - _ Air 1013 East Third - Indoor air 03/30/2015 16:40 03/31/2015 16:25 04/03/2015


4 - Air 1012 East Third - Indoor air 03/30/2015 17:05 03/31/2015 16:10 04/03/2015


6 - _ Air 1018 East Third - Indoor air 03/30/2015 . 18:00 03/31/2015 18:12 04/03/2015

7 - Air 1107 East Seventh - Indoor air 03/30/2015 14:50 03/31/2015 13:36 04/03/2015 (Office)

8 - _ Air 703 Plum Street - Sub-slab 03/31/2015 09:18 04/01/2015 09:04 04/03/2015

9 - _ Air 703 Plum Street - Indoor air 03/31/2015 09:20 04/01/2015 09:02 04/03/2015

10 - Air 315 Chestnut Street - Sub-slab 03/31/2015 13:18 04/01/2015 13:12 04/03/2015

11 - _ Air 315 Chestnut Street - Indoor air 03/31/2015 13:25 04/01/2015 13:15 04/03/2015

12 - Air 602 Mulberry Street - Sub-slab 03/31/2015 14:10 04/01/2015 13:36 04/03/2015

13 - _ Air 602 Mulberry Street - Indoor air 03/31/2015 14:18 04/01/2015 13:34 04/03/2015

14 - Air 319 Chestnut Street - Indoor air 03/31/2015 15:57 04/01/2015 13:22 04/03/2015

18 - Air 312 Chestnut Street - Sub-slab 03/31/2015 19:45 04/01/2015 19:34 04/03/2015

16 - Air 312 Chestnut Street - Indoor air 03/31/2015 19:18 04/01/2015 19:39 04/03/2015

17 - Air 1201 East Seventh - Indoor air 04/01/2015 10:10 04/02/2015 08:50 04/03/2015 (AS Inc.)

18 - Air 1201 East Seventh - Indoor air 04/01/2015 10:15 04/02/2015 08:56 04/03/2015 (Accounting)

Page 3 of 14

ASR Number: 6763 RLAB Approved Analysis Comments 04/29/2015

Project ID: SFA72Q00 Project Desc PCE Former Dry Cleaner sampling

Analysis Comments About Results For This Analysis

1 VOCs in Air at Ambient Levels by GC/MS

Lab: Region 7 EPA Laboratory - Kansas City, Ks.

Method: EPA Region 7 RLAB Method 3230.4G

Samples: 1- 2- 3- 4- 5- 6- 7-8- 9- 10- 11- 12- 13- 14-15- 16- 17- 18-

Comments: Reporting Limits: Sample 10 was analyzed at a 1/50,000 dilution to avoid damage to the instrumentation because of the excessively high concentration of Tetrachloroethene. The reporting limits were thus increased by a factor of 50,000 for sample 10.

2-Propanol was J-coded in sample 9. Tetrahydrofuran was J-coded in sample 7. Vinyl Acetate was J-coded in samples 3, 4, 6 and 7. Although the analytes in question have been positively identified in the samples, the quantitations are estimates (J-coded) due to the continuing calibration checks not meeting accuracy specifications. The actual concentrations for these analytes may be higher than the reported values.

Vinyl Acetate was UJ-coded in samples 1, 2, 5 and 8. Tetrahydrofuran was UJ-coded in samples 1-6 and 8. 1,2,4-Trichlorobenzene was UJ-coded in samples 1-18. These analytes were not found in the samples at or above the reporting limits, however, the reporting limits are estimates (UJ-coded) due to the continuing calibration checks not meeting accuracy specifications. The actual reporting limits for these analytes may be higher than the reported values.

2-Propanol was J-coded in samples 1, 3, 4, 6 and 7. Although the analyte in question has been positively identified in the samples, the quantitation is an estimate (J-coded) due to low recovery of this analyte in the laboratory control sample. The actual concentration for this analyte may be higher than the reported value.

Page 4 of 14

ASR Number: 6763


RLAB Approved Sample Analysis Results


04/29/2015

Analysis/ Analyte

1 VOCs in Air at Ambient Levels by GC/MS Acetone

Allyl Chloride

Benzene

Benzyl Chloride

Bromodichloromethane

Bromoform

Bromomethane

1,3-Butadiene

2-Butanone

Carbon Disulfide

Carbon Tetrachloride

Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane

Dibromochloromethane 1,2-Dibromoethane

1.2-Dichlorobenzene 1.3-Dichlorobenzene

1.4-Dichlorobenzene

Dichlorodifluoromethane

1.1-Dichloroethane 1.2-Dichloroethane

1.1-Dichloroethene

cis-l,2-Dichloroethene

trans-1,2-Dichloroethene

1.2-Dichloropropane

cis-l,3-Dichloropropene

trans-1,3-Dichloropropene

1,2-Dichlorotetrafluoroethane

1,4-Dioxane

Ethyl Acetate

Ethyl Benzene

4-Ethyltoluene

Heptane

Hexachlorobutadiene

Hexane

2-Hexanone

Methyl tert-butyl ether

Methylene Chloride

4-Methyl-2-Pentanone

2-Propanol

Propene

Styrene

Units 1- 2- 3- 4-

ug/m3 23 31 35 35

ug/m3 0.66 U 0.66 U 0.66 U 0.66 U

ug/m3 0.68 U 2.7 1.0 2.3

ug/m3 1.0 U 1.0 U 1.0 U i.O U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 2.2 U 2.2 U 2.2 U 2.2 U ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.45 U 0.45 U 0.45 U 0.45 U

ug/m3 3.2 2.2 1.8 1.8 ug/m3 1.5 0.64 U 0.64 U 0.64 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 0.99 U 0.99 U 0.99 U 0.99 U

ug/m3 0.57 U 0.57 U 0.57 U 0.57 U

ug/m3 1.2 1.0 1.0 U 1.0 U

ug/m3 2.5 1.8 2.5 2.9

ug/m3 0.74 U 2.4 0.74 U 9.1

ug/m3 1.8 U 1.8 U 1.8 U 1.8 U

ug/m3 1.7 U 1.7 U 1.7 U 1.7 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 2.4 2.0 2.2 2.1

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U ug/m3 0.85 U 0.85 U 0.97 1.5

ug/m3 0.80 U 0.80 U 0.80 U 0.80 U

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.83 U 0.83 U 0.83 U 0.83 U

ug/m3 0.98 U 0.98 U 0.98 U 0.98 U

ug/m3 0.96 U 0.96 U 0.96 U 0.96 U ug/m3 1.0 U 1.0 U 1.0 U 1.0 U

ug/m3 1.5 U 1.5 U 1.5 U 1.5 U ug/m3 0.71 U 0.71 U 0.71 U 0.71 U

ug/m3 1.1 U 30 5.9 11 ug/m3 2.7 1.0 '0.93 U 1.9

ug/m3 1.5 1.1 U 1.1 U 1.1 U ug/m3 0.89 U 4.2 1.1 3.0 ug/m3 2.1 U 2.1 U 2.1 U 2.1 U ug/m3 0.76 U 9.2 1.0 3.7

ug/m3 0.82 0.80 U 0.80 U 0.80 U ug/m3 0.77 U 0.77 U 0.77 U 0.77 U

ug/m3 0.71 U 0.71 U 0.71 U 0.71 U ug/m3 1.5 0.81 U 0.81 U 0.81 U ug/m3 0.66 J 0.45 UJ 22 J 19 J

ug/m3 0.57 3.5 0.59 1.3 ug/m3 0.91 U 0.91 U 0.91 U 0.91 U

Page 5 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte

1,1,2,2-Tetrachloroethane

Tetrachloroethene

Tetrahydrofuran

Toluene

1,2,4-Trichlorobenzene

1.1.1-Trichloroethane 1.1.2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,1,2-Trichlorotrifluoroethane

1.2.4-Tri methyl benzene

1.3.5-Trimethylbenzene

2,2,4-Trimethylpentane

Vinyl Acetate

Vinyl Bromide

Vinyl Chloride

m and/or p-Xylene

o-Xylene

Units 1- 2- 3- 4-

ug/m3 1.5 U 1.5 U 1.5 U 1.5 U

ug/m3 1.4 U 16 3.5 1.4 U

ug/m3 0.57 UJ 0.57 UJ 0.57 UJ 0.57 UJ

ug/m3 8.0 12 7.6 18

ug/m3 1.5 UJ 1.5 UJ 1.5 UJ 1.5 UJ ug/m3 1.1 U 1.1 U 1.1 U 1.1 U ug/m3 1.2 U 1.2 U 1.2 U 1.2 U ug/m3 1.1 U 1.1 U 1.1 U 1.1 U

ug/m3 1.4 1.3 1.4 1.4

ug/m3 1.5 U 1.5 U 1.5 U 1.5 U

ug/m3 6.7 1.5 1.2 2.0

ug/m3 1.5 1.0 U 1.0 U 1.0 U

ug/m3 1.0 u. 4.8 1.0 U 3.3

ug/m3 0.72 UJ 0.72 UJ 2.5 J 3.5 J

ug/m3 0.96 U 0.96 U 0.96 U 0.96 U

ug/m3 0.55 U 0.55 U 0.55 U 0.55 U

ug/m3 9.9 3.6 3.6 7.7

ug/m3 3.8 1.2 1.2 2.5

Page 6 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte


Allyl Chloride

Benzene

Benzyl Chloride


Bromoform Bromomethane

1,3-Butadiene

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane

Dibromochloromethane

1,2-Dibromoethane

1.2-Dichlorobenzene

1.3-Dichlorobenzene

1.4-Dichlorobenzene


1.1-Dichloroethane

1.2-Dichloroethane

1.1-Dichloroethene



1.2-Dichloropropane




1,4-Dioxane

Ethyl Acetate

Ethyl Benzene

4-Ethyltoluene •

Heptane

Hexachlorobutadiene

Hexane

2-Hexanone


Methylene Chloride


2-Propanol

Propene

Styrene

Units 5- 6- 7- 8-

ug/m3 38 56 60 21

ug/m3 0.66 U 0.66 U 0.66 U 0.66 U

ug/m3 0.68 U 2.5 2.2 0.90

ug/m3 1.0 U 1.0 U 1.0 U 1.0 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 2.2 U 2.2 U 2.2 U 2.2 U

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.45 U 0.45 U 0.45 U 0.45 U

ug/m3 1.6 4.2 7.2 4.0

ug/m3 0.64 U 0.64 U 0.64 U 1.2

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 0.99 U 0.99 U 0.99 U 0.99 U

ug/m3 0.57 U 0.57 U 0.57 U 0.57 U

ug/m3 1.0 U 2.0 1.0 U 1.0 U

ug/m3 0.44 U 1.6 1.7 0.44 U

ug/m3 0.74 U 1.8 1.3 0.74 U

ug/m3 1.8 U 1.8 U 1.8 U 1.8 U

ug/m3 1.7 U 1.7 U 1.7 U 1.7 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 1.3 U 1.3 1.3 U 1.3 U

ug/m3 2.5 2.2 2.2 11

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.85 U 3.2 0.85 U 0.85 U

ug/m3 0.80 U 0.80 U 0.80 U 0.80 U

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.83 U 0.83 U 0.83 U 0.83 U

ug/m3 0.98 U 0.98 U 0.98 U 0.98 U

ug/m3 0.96 U 0.96 U 0.96 U 0.96 U

ug/m3 1.0 U 1.0 U 1.0 U 1.0 U

ug/m3 1.5 U 1.5 U 1.5 U 1.5 U

ug/m3 0.71 U 0.71 U 0.71 U 0.71 U

ug/m3 1.1 U 41 1.2 1.1 U

ug/m3 2.9 2.3 6.1 3.9

ug/m3 2.1 1.4 1.2 1.8

ug/m3 0.89 U 6.8 2.9 0.89 U

ug/m3 2.1 U 2.1 U 2.1 U 2.1 U

ug/m3 0.76 U 2.6 6.4 0.76 U

ug/m3 0.80 U 0.82 0.80 U 0.91

ug/m3 0.77 U 0.77 U 0.77 U 0.77 U

ug/m3 0.71 U 0.71 U i.4 0.71 U

ug/m3 0.81 U 0.81 U 2.2 0.99

ug/m3 0.45 UJ 16 J 11 J 0.45 UJ

ug/m3 0.38 U 1.4 11 0.59

ug/m3 0.91 U 2.1 1.2 0.91 U

Page 7 of 14

ASR Number: 6763




04/29/2015

inalysis/ Analyte Units 5- 6- 7- 8-

1,1,2,2-Tetrachloroethane ug/m3 1.5 U 1.5 U 1.5 U 1.5 U Tetrachloroethene ug/m3 1.4 U 1.4 U 5.1 1.4 U Tetrahydrofuran ug/m3 0.57 UJ 0.57 UJ 1.8 J 0.57 UJ Toluene ug/m3 7.8 23 29 14 1,2,4-Trichlorobenzene ug/m3 1.5 UJ 1.5 UJ 1.5 UJ 1.5 UJ 1,1,1-Trichloroethane ug/m3 1.1 U 1.1 U 1.1 U 1.1 U 1,1,2-Trichloroethane ug/m3 1.2 U 1.2 U 1.2 U 1.2 U Trichloroethene ug/m3 1.1 U 1.1 U 1.1 U 1.1 U Trichlorofluoromethane ug/m3 1.4 1.4 2.5 1.5 1,1,2-Trichlorotrifluoroethane ug/m3 1.5 U 1.5 U 1.5 U 1.5 U 1,2,4-Trimethylbenzene ug/m3 9.4 6.0 3.9 7.0 1,3,5-Trimethylbenzene ug/m3 2.2 1.6 1.1 1.7 2,2,4-Trimethylpentane ug/m3 1.0 U 11 5.1 1.0 U Vinyl Acetate ug/m3 0.72 UJ 3.0 J 2.5 J 0.72 UJ Vinyl Bromide ug/m3 0.96 U 0.96 U 0.96 U 0.96 U Vinyl Chloride ug/m3 0.55 U 0.55 U 0.55 U 0.55 U m and/or p-Xylene ug/m3 11 7.9 18 13 o-Xylene ug/m3 4.4 3.1 5.8 5.0

Page 8 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte


Allyl Chloride

Benzene

Benzyl Chloride


Bromoform Bromomethane

1,3-Butadiene

2-Butanone Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane Cyclohexane


1.2-Dichlorobenzene

1.3-Dichlorobenzene

1.4-Dichlorobenzene


1.1-Dichloroethane

1.2-Dichloroethane

1.1-Dichloroethene


trans-l,2-Dichloroethene

1.2-Dichloropropane


trans-l,3-Dichloropropene


1,4-Dioxane Ethyl Acetate

Ethyl Benzene

4-Ethyltoluene

Heptane

Hexachlorobutadiene Hexane

2-Hexanone Methyl tert-butyl ether

Methylene Chloride


2-Propanol Propene

Styrene

Units 9- 10- 11- 12-

ug/m3 120 24000 U 65 99

ug/m3 0.66 U 33000 U 0.66 U 0.66 U

ug/m3 1.1 34000 U 3.1 0.84

ug/m3 1.0 U 50000 U 1.0 U 1.0 U

ug/m3 1.3 U 65000 U 1.3 U 1.3 U

ug/m3 2.2 U 110000 U 2.2 U 2.2 U

ug/m3 0.84 U 42000 U 0.84 U 0.84 U

ug/m3 0.45 U 22000 U 0.45 U 0.45 U

ug/m3 3.6 29000 U 30 6.1

ug/m3 0.64 U 32000 U 0.64 U 2.8

ug/m3 1.3 U 65000 U 1.3 U 1.3 U

ug/m3 0.99 U 50000 U 0.99 U 0.99 U

ug/m3 0.57 U 28000 U 0.57 U 0.57 U

ug/m3 1.0 U 50000 U 1.3 1.0 U

ug/m3 1.8 22000 U 1.3 0.44 U

ug/m3 0.74 U 37000 U 3.4 0.74 U

ug/m3 1.8 U 90000 U ' 1.8 U 1.8 U

ug/m3 1.7 U 85000 U 1.7 U 1.7 U

ug/m3 1.3 U 65000 U 1.3 U 1.3 U

ug/m3 1.3 U 65000 U 1.3 U 1.3 U

ug/m3 1.3 U 65000 U 1.3 U 1.3 U

ug/m3 2.3 55000 U 18 2.7

ug/m3 0.84 U 42000 U 0.84 U 0.84 U

ug/m3 32 42000 U 2.9 0.85 U

ug/m3 0.80 U 40000 U 0.80 U 0.80 U

ug/m3 0.84 U 42000 U 1.3 0.84 U

ug/m3 0.83 U 42000 U 0.83 0.83 U

ug/m3 0.98 U 49000 U 0.98 U 0.98 U

ug/m3 0.96 U 48000 U 0.96 U 0.96 U

ug/m3 1.0 U 50000 U 1.0 U 1.0 U

ug/m3 1.5 U 75000 U 1.5 U 1.5 U

ug/m3 0.71 U 36000 U 0.71 U 0.71 U

ug/m3 19 55000 U 17 1.1 U

ug/m3 0.93 U 46000 U 5.1 2.2

ug/m3 1.1 U 55000 U 1.4 3.4

ug/m3 1.1 44000 U 6.8 0.89 U

ug/m3 2.1 U 100000 U 2.1 U 2.1 U

ug/m3 1.1 38000 U 7.4 0.76 U

ug/m3 0.80 U 40000 U 1.5 0.80 U

ug/m3 0.77 U 38000 U 0.77 U 0.77 U

ug/m3 0.71 U 36000 U 20 2.4

ug/m3 0.81 U 40000 U 0.81 U 0.85

ug/m3 190 J 22000 U 0.45 U 0.52

ug/m3 1.8 19000 U 6.2 0.86

ug/m3 1.1 46000 U 0.92 0.91 U

Page 9 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte


Tetrachloroethene

Tetrahydrofuran

Toluene

1,2,4-Trichlorobenzene 1.1.1-Trichloroethane

1.1.2-Trichloroethane

Trichloroethene

Trichlorofluoromethane

1,1/2-Trichlorotrifluoroethane




Vinyl Acetate

Vinyl Bromide

Vinyl Chloride

m and/or p-Xylene

•o-Xylene

Units 9- 10- 11- 12-

ug/m3 1.5 U 75000 U 1.5 U 1.5 U ug/m3 1.4 U 2300000 550 40 ug/m3 0.57 U 28000 U 21 0.57 U ug/m3 5.0 40000 U 47 8.9 ug/m3 1.5 UJ 75000 UJ 1.5 UJ 1.5 UJ ug/m3 1.1 U 55000 U 1.1 U 1.1 U ug/m3 1.2 U 60000 U 1.2 U 1.2 U ug/m3 1.1 U 55000 U 1.1 U 1.1 U ug/m3 3.2 60000 U 3.7 1.4 ug/m3 1.5 U 75000 U 1.5 U 1.5 U ug/m3 1.1 U 55000 U 6.4 6.0 ug/m3 1.0 U 50000 U 1.6 1.4

ug/m3 1.5 50000 U 10 1.0 U

ug/m3 6.7 36000 U 7.0 0.72 U ug/m3 0.96 U 48000 U 0.96 U 0.96 U ug/m3 0.55 U 28000 U 0.55 U 0.55 U

ug/m3 1.9 U 95000 U 17 7.5 ug/m3 0.94 U 47000 U 6.0 3.0

Page 10 of 14

ASR Number: 6763 RLAB Approved Sample Analysis Results

Project ID: SFA72Q00 Project Desc: PCE Former Dry Cleaner sampling

04/29/2015

Analysis/ Analyte


Allyl Chloride

Benzene

Benzyl Chloride


Bromoform

Bromomethane

1,3-Butadiene

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Cyclohexane

Dibromochloromethane

1,2-Dibromoethane 1.2-Dichlorobenzene

1.3-Dichlorobenzene

1.4-Dichlorobenzene


1.1-Dichloroethane

1.2-Dichloroethane

1.1-Dichloroethene



1.2-Dichloropropane


trans-l,3-Dichloropropene


1,4-Dioxane

Ethyl Acetate

Ethyl Benzene

4-Ethyltoluene

Heptane

Hexachlorobutadiene

Hexane

2-Hexanone


Methylene Chloride


2-Propanol

Propene

Styrene

Units 13- 14- 15- 16-

ug/m3 29 16 26 25

ug/m3 0.66 U 0.66 U 0.66 U 0.66 U

ug/m3 0.68 U 39 1.3 1.3

ug/m3 1.0 U 1.0 U 1.0 U 1.0 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 2.2 U 2.2 U 2.2 U 2.2 U

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.45 U 0.45 U 0.45 U 0.45 U

ug/m3 5.5 16 3.6 2.1

ug/m3 0.64 U 0.64 U 2.9 0.64 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 0.99 U 0.99 U 0.99 U 0.99 U

ug/m3 0.57 U 0.82 0.57 U 0.57 U

ug/m3 1.0 U 1.0 U 1.0 U 1.0 U

ug/m3 1.0 1.2 0.44 U 1.4

ug/m3 0.74 U 30 0.97 1.5

ug/m3 1.8 U 1.8 U 1.8 U 1.8 U

ug/m3 1.7 U 1.7 U 1.7 U 1.7 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 1.3 U 1.3 U 1.3 U 1.3 U

ug/m3 2.2 2.5 2.8 2.6

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.85 U 0.85 U 0.85 U 0.85 U

ug/m3 0.80 U 0.80 U 0.80 U 0.80 U

ug/m3 0.84 U 0.84 U 0.84 U 0.84 U

ug/m3 0.83 U 0.83 U 0.83 U 0.83 U

ug/m3 0.98 U 0.98 U 0.98 U 0.98 U

ug/m3 0.96 U 0.96 U 0.96 U 0.96 U

ug/m3 1.0 U 1.0 U 1.0 U 1.0 U

ug/m3 1.5 U 1.5 U 1.5 U 1.5 U

ug/m3 0.71 U 0.71 U 0.71 U 0.71 U

ug/m3 1.1 U 1.1 U 1.1 U 1.1 U

ug/m3 0.93 U 40 2.5 2.0

ug/m3 1.1 U 43 3.3 1.1 U

ug/m3 0.89 U 49 0.89 U 0.95

ug/m3 2.1 U 2.1 U 2.1 U 2.1 U

ug/m3 0.76 U 67 1.2 1.6

ug/m3 0.80 U 12 0.93 0.80 U

ug/m3 0.77 U 0.77 U 0.77 U 0.77 U

ug/m3 0.71 U 0.71 U 2.5 3.7

ug/m3 0.81 U 0.81 U 0.81 U 0.81 U

ug/m3 0.70 3.5 0.50 0.85

ug/m3 0.61 5.1 1.1 0.77

ug/m3 0.95 0.91 U 0.91 U 0.91 U

Page 11 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte

1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene



1.1.2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,1,2-Trichlorotrifluoroethane

1.2.4-Trimethylbenzene 1.3.5-Trimethylbenzene


Vinyl Acetate

Vinyl Bromide

Vinyl Chloride

m and/or p-Xylene

o-Xylene

Units 13- 14- 15- 16-

ug/m3 1.5 U 1.5 U 1.5 U 1.5 U ug/m3 1.5 180 9200 2.5 ug/m3 7.3 0.57 U 0.57 U 0.57 U ug/m3 0.80 U 190 11 8.4 ug/m3 1.5 UJ 1.5 UJ 1.5 UJ 1.5 UJ ug/m3 1.1 U 1.1 U 1.1 U 1.1 U

ug/m3 1.2 U 1.2 U 1.2 U 1.2 U ug/m3 1.1 U 1.1 U 1.1 U 1.1 U

ug/m3 3.2 1.5 1.7 1.5 ug/m3 1.5 U 1.5 U 1.5 U 1.5 U ug/m3 2.2 60 5.6 2.0 ug/m3 1.0 U 18 1.4 1.0 U

ug/m3 1.0 U 150 1.8 2.3

ug/m3 0.72 U 48 0.72 U 0.72 U

ug/m3 0.96 U 0.96 U 0.96 U 0.96 U

ug/m3 0.55 U 0.55 U 0.55 U 0.55 U

ug/m3 1.9 U 140 8.2 6.1

ug/m3 0.94 U 56 3.2 1.9

Page 12 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte


Allyl Chloride

Benzene

Benzyl Chloride


Bromoform Bromomethane 1,3-Butadiene

2-Butanone

Carbon Disulfide


Chlorobenzene

Chloroethane Chloroform

Chloromethane

Cyclohexane


1.2-Dichlorobenzene

1.3-Dichlorobenzene

1.4-Dichlorobenzene


1.1-Dichloroethane

1.2-Dichloroethane

1.1-Dichloroethene cis-l,2-Dichloroethene trans-l,2-Dichloroethene

1.2-Dichloropropane




1,4-Dioxane Ethyl Acetate

Ethyl Benzene

4-Ethyltoluene

Heptane Hexachlorobutadiene

Hexane

2-Hexanone


Methylene Chloride


2-Propanol

Propene

Styrene

Units 17- 18-

ug/m3 69 82

ug/m3 0.66 U 0.66 U

ug/m3 0.92 0.68 U ug/m3 1.0 U 1.0 U

ug/m3 1.3 U 1.3 U ug/m3 2.2 U 2.2 U ug/m3 0.84 U 0.84 U ug/m3 0.45 U 0.45 U

ug/m3 10 5.0 ug/m3 0.64 U 0.64 U ug/m3 1.3 U 1.3 U

ug/m3 0.99 U 0.99 U

ug/m3 0.57 U 0.57 U ug/m3 1.0 U 1.0 U

ug/m3 2.5 1.3

ug/m3 0.74 U 0.74 U

ug/m3 1.8 U 1.8 U ug/m3 1.7 U 1.7 U

ug/m3 1.3 U 1.3 U ug/m3 1.3 U .1.3 U

ug/m3 1.3 U 1.3 U ug/m3 4.2 2.4 ug/m3 0.84 U 0.84 U ug/m3 0.95 0.85 U ug/m3 0.80 U 0.80 U ug/m3 0.84 U 0.84 U

ug/m3 0.83 U 0.83 U ug/m3 0.98 U 0.98 U

ug/m3 0.96 U 0.96 U

ug/m3 1.0 U 1.0 U ug/m3 1.5 U 1.5 U

ug/m3 0.71 U 0.71 U

ug/m3 3.1 2.0

ug/m3 0.93 U 0.93 U

ug/m3 1.1 U 1.1 U

ug/m3 0.89 U 0.89 U

ug/m3 2.1 U 2.1 U ug/m3 0.76 U 0.76 U ug/m3 0.80 U 0.82

ug/m3 0.77 U 0.77 U

ug/m3 0.71 U 0.71 U

ug/m3 0.81 U 0.81 U

ug/m3 20 13

ug/m3 0.71 0.53

ug/m3 0.91 U 0.91 U

Page 13 of 14

ASR Number: 6763




04/29/2015

Analysis/ Analyte


Tetrachloroethene

Tetrahydrofuran

Toluene



1.1.2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,1,2-Trichlorotrifluoroethane

1.2.4-Trimethy I benzene


2,2,4-Trimethylpentane .

Vinyl Acetate

Vinyl Bromide

Vinyl Chloride

m and/or p-Xylene

o-Xylene

Units 17- 18-

ug/m3 1.5 U 1.5 U

ug/m3 5.6 4.3

ug/m3 1.8 0.87

ug/m3 2.8 1.5

ug/m3 1.5 UJ 1.5 UJ

ug/m3 1.1 U 1.1 U

ug/m3 1.2 U 1.2 U

ug/m3 1.1 U 1.1 U

ug/m3 2.7 1.5 ug/m3 1.5 U 1.5 U

ug/m3 1.1 U 1.1 U

ug/m3 1.0 U 1.0 U

ug/m3 1.0 U 1.0 U

ug/m3 2.2 1.6

ug/m3 0.96 U 0.96 U

ug/m3 0.55 U 0.55 U

ug/m3 1.9 U 1.9 U

ug/m3 0.94 U 0.94 U

Page 14 of 14

CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION VII

ACTIVITY LEADER(Print) X* F'sbtlr

NAME OF SURVEY OR ACTIVITY At(as\-fic ts)cj-e.r £vpphf

DATE OF COLLECTION - P * '

MONTH YEAR 30-02 63-0*2015

DAY

TRET" Of

CONTENTS OF SHIPMENT

SAMPLE NUMBER

TYPE OF CONTAINERS

SwAFAfl-OUDITAIIItn- BOTTLE BOTTLE BOTTLE

VOA SET (2 VIALS EA]

NUMBERS OF CONTAINERS PER SAMPLE NUMBER

SAMPLED MEDIA other A

RECEIVING LABORATORY REMARKS-OTHER INFORMATION (condition of samples upon receipt, other sample numbers, etc }

(ol L>3 - I

- 2-

-4 -s

— (o

-7

- 8

-1

Ho - u

-12

-13

-I?

PERSONNEL CUSTODY RECORD FIEHNQUIS

"1 SEALED

(SAMPLER)

UNSEALED &

DATE

«/*/«

TIME RECEIVED BY

SEALED UNSEA

REASON FOR CHANGE OF CUSTODY

RELINQUISHED BY DATE TIME

I SEALED UNSEALED| RELINQUISHED BY DATE TIME

RECEIVED BY

|SEALED


R EC El V E D BY UNSEALED f


"1 SEALED UNSEALED) Q SEALED UNSEALEpf

7-EPA-9262 (Revised 5/85) •U.S. GPO- 2002-755-917/40053

Sample Collection Field Sheet US EPA Region 7 Kansas City, KS

ASR Number: 6763 Sample Number: 1 QC Code: Matrix: Air Tag ID: 6763-1-

Project ID: SFA72Q00 Project Manager: Susan Fisher Project Desc: PCE Former Dry Cleaner sampling

City: Atlantic State: Iowa Program: Superfund

Site Name: PCE FORMER DRY CLEANER - SITE Site ID: A72Q Site OU: 00 EVALUATION/DISPOSITION

Location Desc: / O / 3 ta.s( T- Sulo- £1

External Sample Number:

Expected Cone: (or Circle One: Low Medium High) Date Time(24 hr)

Latitude: Sample Collection: Start: 3/3o/tS Ho\3o

Longitude: End: 3/ 31/15 i t? ;i5

Laboratory Analyses: Container Preservative Holding Time Analysis

1 - 6 Liter Canister None 60 Days 1 VOCs in Air at Ambient Levels by GC/MS

Sample Comments:

(N/A) P^Ssore.! -afe.S* Hg

P*-essore » - */" Wcj

6v ^ 3oo I

Aol O (oOle>\- s

Sample Collected By: TT

1 of 1






Location Desc: 1013 6^-sf "Third- Indoor A,r


Expected Cone: (or Circle One: Low Medium High)

Latitude: Sample Collection: Start:

Longitude: End:

Date Time(24 hr)

3 /3o//5" I

J3Vj3!/I|5 MpjzS

Laboratory Analyses: Container Preservative

1 - 6 L i t e r C a n i s t e r N o n e Holding Time Analysis

60 Days 1 VOCs in Air at Ambient Levels by GC/MS

Sample Comments:

(N/A) Beg'>w.»CkVv^. Pressor. - 2^" Hg

Cwri sso«»

6ow.wj>- ^ 37-3 M -7Z7 2>OM(o


1 of 1


ASR Number: 6763 Sample Number: 3 QC Code: Matrix: Air Tag ID: 6763-3-_




Location Desc: j 01 2. Ea&l Third - Svlo- SlcJa

Expected Cone:

Latitude:

Longitude:

Date


(or Circle One: Low Medium High)

Sample Collection: Start: 3 /so/ jjj

End: 3V3y_\S

Time(24 hr)

n-.oo

jfe_: \3


1 - 6 Liter Canister None Holding Time Analysis


Sample Comments:

(N/A) Pis*orti-ZT Hg

£ k c J - O "

SOIWMJC *• M65T


1 of 1






Location Desc: /o/z Ea.sk Third — Indoor ft\r

Expected Cone:

Latitude:

Longitude:


(or Circle One: Low Medium High) Date

Sample Collection: Start: 3 l3ol 13

End: _3/3yiS

Time(24 hr)

j7:oS \(o :IO




Sample Comments: (N/A) fWssv-e: - 25"

£Vw-J P^ssur-^' "0"

Sukv\«v\^_"3C2S

<2_«xj * -7ZTT\to


1 of 1


ASR Number: 6763 Sample Number: 5 QC Code: Matrix: Air Tag ID: 6763-5-_



Site Name: PCE FORMER DRY CLEANER - SITE EVALUATION/DISPOSITION

Site ID: A72Q Site OU: 00

Location Desc: /o/8 ~Tb>rclSub — Slab

Expected Cone:

Latitude:

Longitude:


(or Circle One: Low Medium High) Date Time(24 hr)

Sample Collection: Start: 3 /3Q/I5

End: 3 /3i / >«5




Sample Comments:

(N/A) fVessorc'. - 3o" Kg

twd fv-essoct

fc- 302-fc


1 of 1






Location Desc: I O I S I r t d o p y



Latitude: Sample Collection: Start: 3 /3Q/ IS if} :oo

Longitude: End: 3 /3</is I8\l2.



Sample Comments: (N/A) P~s&or*. ( - 2g, 5"

Ei-iJ Pressure. ! — 3 "

SunAM-a 3013


1 of 1


ASR Number: 6763 Sample Number: 7 QC Code: _ Matrix: Air Tag ID: 6763-7-.





Location Desc:

Expected Cone:

Latitude:

Longitude:

/ I 0~7 5"e if/i - /nc/ooe fair - Oppic ct



Sample Collection: Start: 3/30/is

End:

Time(24 hr)

/V: 5o

13 ;3fe


1 - 6 L i t e r C a n i s t e r N o n e

Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS

Sample Comments:

(N/A) pressure ' - Z?" Hg

Pressure. : - O"

SuMIVA. ^ 3tSS

£*2 -ft-


1 of 1






Location Desc: 703 f 7 ! — 5vb- S\o.b

External SamDle Number:


Latitude: Sample Collection: Start: 3/31/15 05: j& Longitude: End: 4/ 1 / i5 Q^-qJL


1 - 6 L i t e r C a n i s t e r N o n e 6 0 D a y s 1 V O C s i n A i r a t A m b i e n t L e v e l s b y G C / M S

Sample Comments:

( N / A ) - Z 5 . S , l H 3

C. wJ fWssoce. •. - 3 " Wq

Sv 2118

* AOVOGO (oZ - 2 .


1 of 1






Location Desc: *7o3 "Plvtv* Indoor AV



Latitude: Sample Collection: Start: 3 /3I/I5 0*1: z-o

Longitude: End: H/ ) / 15 <9*? :oi



(Vci>so

Cvxti (Vessvjre- \ - 2" Ug

Sample Comments:

(N/A)


1 of 1







Location Desc: 315 CKeslmif Sub-Slo-b

Expected Cone:

Latitude:

Longitude:


(or Circle One: Low Medium High) Date Time(24 hr)

Sample Collection: Start: 3/3l/\S 13:

End: AJLJlS 13,'xtr




Sample Comments:

(N/A) fressuirt". "2"

(2-eg* 7-Z.7 3i<=>6

-Z7" He


1 of 1


ASR Number: 6763 Sample Number: 11 QC Code: Matrix: Air Tag ID: 6763-ll-_

Project ID: SFA72Q00 Project Desc: PCE Former Dry Cleaner sampling

City: Atlantic Program: Superfund


Project Manager: Susan Fisher

State: Iowa


Location Desc: 3l5 SV<*c.eA -* Indoor

Expected Cone:

Latitude:

Longitude:



Sample Collection: Start: _3/3J_/i5

End: _y_/ I /iQ

Time(24 hr)

13:^5

Laboratory Analyses: Container

1 - 6 Liter Canister Preservative None

Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS

Sample Comments:

(N/A)

t w J r * _ \ - 0 U

FC-21

l


1 of 1







Location Desc: (PQ2.



Latitude: Sample Collection: Start: 3 /31/ 15 14: io

Longitude: End: Hi I /13:3>(o



Sample Comments:

(N/A) e < W s s u r e - ' * " Z - 8 , S * H g

-7T--73I,:IS


1 of 1







Location Desc: LOT, awe* - i^doov



Latitude: Sample Collection: Start: 3 731/ >S H:ift

Longitude: End: H / \ /& 13: "31



Sample Comments:

(N/A) - 3o,v ^

P<-e.si»ar«A -q«. ^

Mzll i7n°nc><o


1 of 1


ASR Number: 6763 Sample Number: 14 QC Code: _ Matrix: Air Tag ID: 6763-14-_




Location Desc: 31^ CKtSVhvt — Ind 00/



Latitude: Sample Collection: Start: 3 / 3 l /i6 >9:S7

Longitude: End: H / I /1*5 \z \-vz.



Sample Comments: (N/A) " 28'6 " U3

ETrxJ - 3. 5"

(Leej ^ TzfeH33<o


1 of 1






Site ID: A72Q Site QU: 00

Location Desc: SiZ. S\reeA — SoW-S^olo



Latitude: Sample Collection: Start: 3 /3I /I f : M5

Longitude: End: M/ > / IS- \c); 3H



Sample Comments: (N/A) Pressor* : -z4.5"

Pressure - - o"

3020

Jt


1 of 1







Location Desc: .3IZ CU&sfru»4- - Irvdoov A»»"



Latitude: ; Sample Collection: Start: 3/31/15 H: IS

Longitude: End: H/ 1/1*5 11:3^



Sample Comments:

(N/A) S ure_'. - 2.^" Wg

Pr* 1 - O"

Aot 6ot>5g- z


1 of 1







Location Desc: / Z Q l E a . sf Sevenl-A — "Indoor Inc.



Latitude: Sample Collection: Start: H! I 7/5" /o : to

Longitude: End: H 1 2 - ! l 5 Q g \ S o


1 - 6 L i t e r C a n i s t e r ' N o n e 6 0 D a y s 1 V O C s i n A i r a t A m b i e n t L e v e l s b y G C / M S

Sample Comments: (N/A) Pre*S VCl - 2*?" Hg

Pressure - ~

S t/jwi A 3o3 o ft-*Ao/o 3


1 of 1







LOCation DeSC: I Z O l -~ I r \ c l o Q r - f y > r -


Expected Cone: (or Circle One: Low Medium High) Date

Latitude: Sample Collection: Start:

Longitude: End: Hj tj IS.

Time(24 hr)

/o_\rS




Sample Comments:

(N/A) I -30" He

Pressure. I - 5. S "

A* /V976

£.^*7277^/37


1 of 1

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