Page 1
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(I) ' ~v -o ~ SINCE 1984 • ~ ~-z- Cl)~ \'t. L ~ ~~~~
'l . ~~ 11-ollA1'11
Client Name: City of Rehoboth Contact: Bob Stenger
Address: P.O. Box 1163
Rehoboth, DE 19971
' 302-227-7801 Phone Cel Fax
emai
!
: 302-227-4649 I
Payment Rec. Cash Check# lnvoice~X-
Email Reports 0 Fax Reports 0
Lab I.D Sample Description/Location Sample Date Time I Matrix
01 \~'1'3 !Effluent Composite Start- .zq.fD o 61?~ I DIW I End- & . SO· tJ 0{1; I DIW
DIW D/W D/W DIW DIW DIW
Containers Received: (circle)
Type: Q M N/P Bacti Quant
Temperature Upon Receipt z ..0 a..
""" N CD
~ w
3.S oc lC)
N CD <( a.. w
""" c:i N
""" <( a.. w
I IXIXIXIXIX
Q=Quart (Unpreserved), M=Metals (HN03), N/P=Nutrients (H2S04), Bacti=P/A Colilert® (Sodium Thiosulfate)
Sampled by: ----"''-='b--.-::::..-· ~ .?:IJ-lo /Time l5os Received by. SJ,,.jJ,t'~ Date IP l~\•o !Time 15°
5
Reliniquished by: Date /Time __ _ Received by Date /Time __ _
Reliniquished by: Date /Time. __ _ Received by Date /Time __ _
©2007 Envirocorp Inc. Rev Feb 2007
Page 2
:-.1 "'..oi"'
/4oco..p· .. ~ 51 Clark St. Harrington, DE 19952 •> ..... -'0' > "');"' ''"' . ~ ------------------- ------------- PH: 302.398.4313 FX: 302.398.4312
S~. L. p.. '.:c fJ)/ ANALYTICAL SERVICES: NPDES, RCRA, GROUND WATER MONITORING '!r~,.l.,~·~"'·~
City of Rehoboth P.O. Box 1163 Rehoboth, DE 19971
Attention: Bob Stenger
Lab ID: 091893
Description:
Type: Composite
Metals
Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Mercury Metals Digestion for AA Nickel Selenium Silver Thallium Zinc
Miscellaneous/Other
SHIP
Printed: Jul12 2010 4:10PM
ANALYTICAL RESULTS
Matrix: Waste Water
Site: 001
mg/L <0.0010 mg/L 0.001 mg/L <0.0010 mg/L <0.00050 mg/L <0.0010 mg/L 0.0018 mg/L <0.0010 mg/L <0.00050
Completed mg/L 0.0034 mg/L 0.001 mg/L 0.00075 mg/L <0.0010 mg/L 0.0212
Completed
Page 1 of 1
7/2/1 0 19:08 7/2/1 0 19:08 7/2/1 0 19:08 7/2/10 19:08 7/2/10 19:08 7/2/10 19:08 7/2/10 19:08 7/8/10 12:22 7/1/10 14:10 7/2/10 19:08 7/2/10 19:08 7/2/10 19:08 7/2/10 19:08 7/2/10 19:08
7/12/10 15:00
Sample Start: 6/29/10 6:55
SampleEnd: 6/30/10 7:30
Date Received: 6/30/10 15:05
HJG3 HJG3 HJG3 HJG3 HJG3 HJG3 HJG3 ALSI HJG HJG3 HJG3 HJG3 HJG3 HJG3
ALSI
EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 245.1 EPA 200.2 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8
None
ND = Not Detected * = Above Specified Limit ** =Above Client Limit
Page 3
www.ana~lr:allab.r:om
NEUIP IICUIHilted PA 22•211S N.l PAflffl
SJIIJOflwood urne • Middletown, PA f7057 Phone: 7f7·1144·5S4f Fmc 7f7·1144·f4SO
Certificate of Analysis Project Name: NPDES PERMIT 001 • 1 Purchase Order:
Ms. Shelly Bloom Enviro Corporation Inc. 51 Clark Street Harrington, DE 19952
July 12, 201 0
Dear Ms. Bloom,
Workorder: 9853108
Workorder ID: Rehoboth, 91893
Enclosed are the analytical results for samples received by the laboratory on Friday, July 02, 2010
ALSI is a National Environmental Laboratory Accreditation Program (NELAP) accredited laboratory and as such, certifies that all applicable test results meet the requirements of NELAP.
If you have any questions regarding this certificate of analysis, please contact Denise Brooks (Project Coordinator) or Anna G Milliken (Laboratory Manager) at (717) 944-5541.
Please visit us at www.analyticallab.com for a listing of ALSI's NELAP accreditations and Scope of Work, as well as other links to Water Quality documentation on the internet.
This laboratory report may not be reproduced, except in full, without the written approval of ALSI.
NOTE: ALSI has changed the report generation tool and while we have tried to retain the existing format, you will notice some changes in the laboratory report. Please feel free to contact ALSI in case you have any questions.
Analytical Laboratory Services, Inc.
This page is included as part of the Analytical Report and
must be retained as a permanent record thereof.
ReportiD:9853108
cz___ ~ J,U__ Anna G Milliken
Laboratory Manager
Page 1 of 10
Page 4
ANALrrleAL LABDRIJFDRV SJSRIIIess, INe.
WWW.OIIII~Ir:GIIab.r:om
NELIIP Aurerlltetl PA :Z2•211S N.l PAtlfQ
u Dogwood l.llne • Middletown, IIA f70S'7 Phone: 7f7·fltll4·554f IFGJI: 7f7·SitiUI·f430
SAMPLE SUMMARY
Workorder: 9853108 Rehoboth, 91893 Discard Date: 07/26/2010
Lab ID Sample ID Matrix Date Collected Date Received Collected By
9853108001 91893-001 Composite WasteWater 6/30/10 07:30 7/2/10 10:25 Customer
Work order Comments:
Notes -- Samples collected by ALSI personnel are done so in accordance with the procedures set forth in the ALSI Field Sampling Plan (20 -
Field Services Sampling Plan). -- All Waste Water analyses comply with methodology requirements of 40 CFR Part 136. -- All Drinking Water analyses comply with methodology requirements of 40 CFR Part 141. -- Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis. -- The Chain of Custody document is included as part of this report.
Standard Acronyms/Flags J, B Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL) for the analyte U Indicates that the analyte was Not Detected (NO)
MDL Method Detection Limit PQL Practical Quantitation Limit RDL Reporting Detection Limit ND Not Detected - indicates that the analyte was Not Detected at the RDL Cntr Analysis was performed using this container
RegLmt Regulatory Limit LCS Laboratory Control Sample MS Matrix Spike
MSD Matrix Spike Duplicate DUP Sample Duplicate
%Rec Percent Recovery RPD Relative Percent Difference
Report ID: 9853108 Page 2 of 10
Page 5
ANALVT'ICAL I.ABIIRATIIRV SsRuless, INe.
~.ana~JeaUa&cvm
NELIIP Auredlted PA :Z:Z•:ZfiS N.l PADfO
U tJogwood "'ne · Mldii~Rown, PA f70S7 Phfllffl: 7'f7'·fl411•554f I=IIJl: 7f7'·flllll·f4SO
Workorder: 9853108 Rehoboth, 91893
Lab ID: 9853108001
Sample ID: 91893-001 Composite
Parameters Results Flag
VOLATILE ORGANICS
Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-Chloroethylvinyl ether Chloroform Chloromethane 1 , 1-Dichloroethane 1 ,2-Dichloroethane trans-1 ,2-Dichloroethene 1 ,2-Dichloropropane trans-1 ,3-Dichloropropene Ethylbenzene Methylene Chloride 1,1 ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1, 1-Trichloroethane 1,1 ,2-Trichloroethane Trichloroethene Vinyl Chloride
Surrogate Recoveries
1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Toluene-dB (S)
SEMIVOLATILES
Acenaphthene Acenaphthylene Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b )fluoranthene Benzo(g, h,i)perylene Benzo(k)fluoranthene 4-Bromophenyl-phenylether Butylbenzylphthalate
Report ID: 9853108
ND ND ND ND ND ND ND ND ND ND ND 1.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Results
82.5 85.4 90.6 101
ND ND ND ND ND ND ND ND ND ND ND
Flag
Units
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
Units
% % % %
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L
ANALYTICAL RESULTS
Date Collected: 6/30/2010 07:30
Date Received: 7/2/2010 10:25
Matrix: Waste Water
RDL
30.0 5.0 1.0 1.0 2.0 2.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0
Limits
72-142 73-119 74-132 75-133
1.4 1.4 1.4
18.9 1.4 1.4 1.4 1.4 1.4 2.8 2.8
Method
EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624
Method
EPA624 EPA624 EPA624 EPA624
EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625
Prepared By Analyzed By Cntr
718110 17:25 MES B 718110 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 7/8/10 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 7/8/10 17:25 MES B 718110 17:25 MES B 718110 17:25 MES B 718110 17:25 MES B
Prepared By Analyzed By Cntr
7/8/10 17:25 718110 17:25 718110 17:25 718110 17:25
MES B MES B MES B MES B
716110 RSS 7/7110 13:46 CGS D1 7/6/10 RSS 7/7110 13:46 CGS D1 716110 RSS 7/7110 13:46 CGS D1 716110 RSS 7/7110 13:46 CGS D1 7/6/10 RSS 717110 13:46 CGS D1 716110 RSS 7/7110 13:46 CGS D1 7/6/10 RSS 7/7110 13:46 CGS D1 716110 RSS 7/7110 13:46 CGS D1 716110 RSS 7/7110 13:46 CGS D1 716110 RSS 7/7110 13:46 CGS D1 7/6/10 RSS 7/7110 13:46 CGS D1
Page 3 of 10
Page 6
ANAI.VTICAI. I.IIBORATORV !!ll!lRIIICI!lS, INC.
www.ana~/callab.com
NEI.AIIIIcuedltetl Pll :Z2·2fiS Nl PIIDftl
u IIOfiWood l.flne • Middletown, PA f7057 Phone: 'n7·11114-5S4f t=IIX: 'n7·8411·14m
Workorder: 9853108 Rehoboth, 91893
Lab ID: 9853108001
Sample ID: 91893-001 Composite
Parameters
Bis(2-Chloroethoxy)methane Bis(2-Chloroethyl)ether bis(2-Chloroisopropyl)ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenyl-phenylether Chrysene mp-Cresol Di-n-Butylphthalate Di-n-Octylphthalate Dibenzo(a,h)anthracene 3,3-Dichlorobenzidine 2,4-Dichlorophenol 2,4-Dimethylphenol Dimethylphthalate 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 1 ,2-Diphenylhydrazine bis(2-Ethylhexyl}phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane lndeno(1 ,2,3-cd}pyrene lsophorone Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-Nitrosodimethylamine N-Nitroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 1 ,2,4-Trichlorobenzene 2,4,6-Trichlorophenol
Results
ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 8.0 ND ND NO ND ND ND ND ND ND ND ND ND ND ND ND ND NO ND ND ND ND
Flag
Surrogate Recoveries Results Flag
2,4,6-Tribromophenol (S) Phenol-d5 (S) Terphenyl-d14 (S) Nitrobenzene-d5 (S) 2-Fiuorobiphenyl (S)
Report ID: 9853108
60.1 21.8 69.2 80.6 66.7
··Units
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/i.. ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ugll ugll ug/L ug/L
Units
% % % % %
ANALYTICAL RESULTS
Date Collected: 6/30/2010 07:30
Date Received: 7/2/2010 10:25
Matrix: Waste Water
RDL Method Prepared By Analyzed By Cntr
2.8 2.8 2.8 2.8 7.5 2.8 1.4 7.5 2.8 7.5 1.4
15.1 7.5 7.5 7.5 15.1 2.8 2.8 2.8 2.8 1.4 1.4 2.8 2.8 7.5 2.8 1.4 2.8 1.4 2.8 7.5 7.5 2.8 2.8 2.8 15.1 1.4 7.5 1.4 2.8 7.5
Limits
38-134 11-53
33-125 37-124 37-113
EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625 EPA625
Method
EPA625 EPA625 EPA625 EPA625 EPA625
716/10 RSS 7/6/10 RSS 7/6/10 RSS 716110 RSS 7/6/10 RSS 716110 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS 7/6/10 RSS
7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS 01 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS 01 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS 01 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS 01 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1 7/7/10 13:46 CGS D1
Prepared By Analyzed By Cntr
7/6/10 RSS 7/7/10 13:46 CGS 01 7/6/10 RSS 7/7/10 13:46 CGS D1 7/6/10 RSS 7/7/10 13:46 CGS D1 7/6/10 RSS 7/7/10 13:46 CGS D1 7/6/10 RSS 7/7/10 13:46 CGS D1
Page 4 of 10
Page 7
ANIJI.VFICIJI. LABDIUI7DRV !!IJSRIIICISS, INC.
www.ana/Jftlt:allab.com NEUIP Aurerllted
PA :Z:Z·:ZIIS N.l PAfllfl
S4 Dogwood l.ane - Middletown, 1111 f7tl57 Ph011e: '71'7·11411·5541 FIIX: '71'7·11411·1/ISD
Workorder: 9853108 Rehoboth, 91893
Lab ID: 9853108001
Sample ID: 91893-001 Composite
Parameters Results Flag Units
2-Fiuorophenol (S) 33 %
WET CHEMISTRY
Phenolics 0.005 mg/L
METALS
Mercury, Total ND mg/L
Sample Comments:
Report ID: 9853108
ANALYTICAL RESULTS
Date Collected: 6/30/2010 07:30
Date Received: 7/2/2010 10:25
RDL Method Prepared
17-73 EPA625 7/6/10
0.005 EPA420.4 7/8/10
0.00050 EPA245.1 7/8/10
Matrix: Waste Water
By Analyzed By Cntr
RSS 7/7/10 13:46 CGS D1
KRK 7/9/10 04:43 KRK A
MNP 7/8/10 12:22 MNP F1
a____~ J.L2_ Anna G Milliken
Laboratory Manager
Page 5 of 10
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ANALV7'1CAL LABORATORV SISRIIICISS, INC.
FACIL.ITV' NAME AND PERMIT N\JM86R:
ACROLEIN
aa.u::NE
llROMOFORt/1
CAREiON Tl:TAA(:~ORICE
fiiETHYL CHI.ORIOE
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Report ID: 9853108
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ANAI.'ti'I'ICAI. I.ABOIUI'f'ORV !IIERIIICI!JS, INC.
www.ana~lt::allob.com
NEUP Accredited Pll :Z:Z•:ZIIS N.l Pllfl'lfl
M I.'IOgWOOII urne • MlddleflJWn, PA f7057 Phone: 7f7·D44·554f Pint: 7f7·SI44·f4SO
f'AC::ILffY NAME AND PIORMtT NUMBER:
. ~n ~ber! . . . (CampFe!& anoo for eildl outfall di.'ldl<lrplng oflluOnt to wM~Jr'li or tile Uniled Sta:e.s..)
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Report ID: 9853108
Page 11
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NEIJIP llccrerllted PA :Z:Z·:ZIIS N.l PAflfCI
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FACU.ITY N.ot.Me AND PERMIT ffUM8SR;
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IINALvrleAL I.ABDRATDRV SsR111ess, INe.
www.ana~l~allab.com
NELIIP Aeuerllted PA :Z:Z•:ZIIS N.l PAtlfQ
SJ1 Doflwood &ane • MiddletOWn, PA f705'7 Phone: '7f7·SI44·554f
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Page 10 of 10
Report ID: 9853108
Page 13
s1 o ~~~~
v'?-~~ 0 c 0 ~~().A (J ~ ~r 0
IL)~ ~-- -'() :-
0 ~ SINCE 1984 • ~ ~ ~ . "'.,::
Client Name: Contact: Address:
Phone Cell Fax
email
City of Rehoboth Bob Stenger
P.O. Box 1163
Rehoboth, DE 19971
302-227-7801
302-227-4649
Containers Received: (circle)
Type: Q
Quant: M NIP Bacti
Temperature Upon Receipt z_ c!! :J () ..: () -- c
4.~ °C 1.0 C'll <0
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q 2 2 '?>0 I Effluent Composite Start- DIW X X X X X
DIW
DIW
0/W
DIW
D/W
DIW
D/W Q=Quart (Unpreserved), M=Metals (HN03), N/P=Nutrients (H2S04), Bacti=P/A Colilert® (Sodium Thiosulfate)
Sampled by: t't.~ate Reliniquished by: ~= 3 Date
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Received by ~,l/t)~te 1·]./Drnme_f3_SV Received by U Date ffime __
©2007 Envirocorp Inc. Rev Feb 2007
Page 14
~f .........
.;··'$-OC 0~~\ 51 Clark St. Harrington, DE 19952 .. ~ sl~nc l~«l • ; ----------- -- --- - --- --- PH: 302.398.4313 FX: 302.398.4312 \ ~ A~} ANALYTICAL SERVICES: NPDES, RCRA, GROUND WATER MONITORING
"'·~ • L p.. v .;· >r~ 1 .J •'*'-'«wi·
City of Rehoboth P.O. Box 1163 Rehoboth, DE 19971
Attention: Bob Stenger
Lab 10: 092230
Description:
Type: Composite
Metals
Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Mercury Metals Digestion for AA Nickel Selenium Silver Thallium Zinc
Miscellaneous/Other
SHIP
Standards & Surrogates
Antimony (% Recovery) Arsenic (% Recovery) Beryllium (% Recovery) Cadmium (% Recovery) Chromium (% Recovery) Copper (% Recovery) Lead (% Recovery) Nickel (% Recovery) Selenium (% Recovery) Silver (% Recovery) Thallium (% Recovery) Zinc (% Recovery)
~ Printed: Aug 16 2010 4:48PM
ANALYTICAL RESULTS
Matrix: Waste Water
Site: 001
mg/L <0.0010 mg/L 0.0019 mg/L <0.0010 mg/L <0.00050 mg/L 0.003 mg/L 0.007 mg/L <0.0010 mg/L <0.00050
Completed mg/L 0.0062 mg/L <0.0010 mg/L 0.00068 mg/L <0.0010 mg/L 0.0467
Completed
% Rec. 116 % Rec. 104 % Rec. 111.2 % Rec. 92 % Rec. 103.5 % Rec. 117.92 % Rec. 100.6 % Rec. 108.7 mg/L 86.3 % Rec. 91.9 % Rec. 98.4 % Rec. 90
Page 1 of 1
8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/1 0 13:29 8/10/10 13:29 8/10/10 13:29 7/13110 9:23 7/14/10 11:00 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29
7/21/10 4:19
8/1 0/1 0 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/1 0 13:29 8/10/10 13:29 8/10/1 0 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29 8/10/10 13:29
Sample Start: 7/6/10 7:15
SampleEnd: 7/7/10 7:15
Date Received: 7/7/10 14:18
HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA 200.8 HJG3 EPA 200.8 HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA200.8 A LSI EPA245.1 HJG3 EPA200.2 HJG3 EPA200.8 HJG3 EPA 200.8 HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA200.8
ALSI None
HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA 200.8 HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA 200.8 HJG3 EPA 200.8 HJG3 EPA200.8 HJG3 EPA200.8 HJG3 EPA 200.8 HJG3 EPA 200.8
ND = Not Detected * = Above Specified Limit **=Above Client Limit I
---·--··-----1
Page 15
www.ana~lc6illab.cam
NEIJIP AUI'flllltfHI PA :ttl-:t!lii!S til PAtJID
S4 Dogwood ltlne • MtddletOtiln, PA f7GS7 Phone: 7f7·044·554f FIDC 7f7.fl44·f4SG
Certificate of Analysis
Ms. Shelly Bloom Enviro Corporation Inc. 51 Clark Street Harrington, DE 19952
July 22, 201 0
Dear Ms. Bloom,
Enclosed are the analytical results for samples received by the laboratory on Thursday, July 08, 2010
ALSI is a National Environmental Laboratory Accreditation Program (NELAP) accredited laporatory and as such, certifies that all applicable test results meet the requirements of NELAP.
If you have any questions regarding this certificate of analysis, please contact Denise Brooks (Project Coordinator) or Anna G Milliken (Laboratory Manager) at (717) 944-5541.
Please visit us at www.analyticallab.com for a listing of ALSI's NELAP accreditations and Scope of Work, as well as other links to Water Quality documentation on the internet.
This laboratory report may not be reproduced, except in full, without the written approval of ALSI.
NOTE: ALSI has changed the report generation tool and while we have tried to retain the existing format, you will notice some changes in the laboratory report. Please feel free to contactALSI in case you have any questions.
Analytical Laboratory Services, Inc.
This page is included as part of the Analytical Report ~nd
must be retained as a permanent record thereof.
ReportiD: 9853858
0--;;2 JL2__ Anna G Milliken Laboratory Manager
Page 1 of 6
Page 16
ANALVT'ICAL LABORAriJRV SsRIIItss, INe.
www.analytlcallab.com NELAP Atoedlteti
PA ~~;.:tf!IS N;l PA01D
SAMPLE SUMMARY
Workorder: 9853858 92230 Rehoboth Discard Date: 08/05/2010
$.ilf"\lpi~ID_
9853858001 92230-Effluent Waste Water 717/10 07:15 7/8/10 10:12 Customer
Workorder Comments:
Notes - Samples collected by ALSI personnel are done so in accordance with the procedures set forth in the ALSI Field Sampling Plan (20-
Field Services Sampling Plan). -- All Waste Water analyses comply with methodology requirements of 40 CFR Part 136. -- All Drinking Water analyses comply with methodology requirements of 40 CFR Part 141. -- Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis. - The Chain of Custody document Is included as part of this report.
Standard Acronyms/Flags J, B Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL) for the analyte U Indicates that the analyte was Not Detected (NO)
MDL Method Detection Limit PQL RDL NO Cntr
RegLmt LCS MS
MSD DUP %Rec RPD
Practical Quantitation Limit Reporting Detection Limit Not Detected - indicates that the analyte was Not Detected at the RDL Analysis was performed using this container Regulatory Limit Laboratory Control Sample Matrix Spike Matrix Spike Duplicate Sample Duplicate Percent Recovery Relative Percent Difference
Report 10: 9853858 Page 2 of6
Page 17
ANALVTICAL LABORATIJRV SsRtrltss, INe.
www.rtna~lcrtllob.com
NEI.AP Acuedlted PA :z:z.:z'IIS N.l PAOlO
S4 Dogwood J.llne • Middletown, Pll f"'OS7 Phlllfe: 7f"'·G411·5S4f FIIK: "'f"'-8411•14~0
Workorder: 9853858 92230 Rehoboth
Lab 10: 9853858001
Sample 10: 92230-Effluent
Pafamefets
VOLATILE ORGANICS
Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-Chloroethylvinyl ether Chloroform Chloromethane 1 ,2-Dichlorobenzene 1 ,3-Dichlorobenzene 1 A-Dichlorobenzene 1 , 1-Dichloroethane 1 ,2-Dichloroethane 1, 1-Dichloroethene trans-1 ,2-Dichloroethene 1 ,2-Dichloropropane cis-1 ,3-Dichloropropene trans-1 ,3-Dichloropropene 1 ,3-Dichloropropene, Total Ethylbenzene Methylene Chloride 1,1 ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1 , 1,1-Trichloroethane 1,1 ,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl Chloride
Surrogate Recoveries
1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 'roluene-d8 (S)
SEMIVOLATILES
Acenaphthene Acenaphthylene Anthracene Benzidine
Repor\10:9853858
NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO
Results Flag
108 81.3 1t1 114
NO NO NO NO
ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L. ug/L ug/L ug/L ugll ug/L ug/L ug/L ug/L ug/L
Units
% % % %
ug/L ug/L ug/L ug/L
ANALYTICAL RESULTS
Date Collected: 717/2010 07:15
Date Received: 7/8/2010 10:12
30.0 5.0 1.0 1.0 2.0 2.0 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0
EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 EPA624 t;;PA624
Matrix: Waste Water
7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 OJB B 7/21/10 04:19 DJB B 7/21/10 04:19 OJB B 7/21/10 04:19 DJB B 7/21/10 04:19 OJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 OJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 OJB B 7/21/10 04:19 OJB B 7/21/10 04:19 DJB B 7/21/1004:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 OJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B
Limits Method Prepared By Analyzed By Cntr
72-142 73-119 74-132 75-133
1.4 1.4 1.4 18.9
EPA624 EPA624 EPA624 EPA624
EPA625 EPA625 EPA625 EPA625
7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B 7/21/10 04:19 DJB B
7/14/10 GEC 7/14/10 19:57 CGS C1 7/14/10 GEC 7/14/10 19:57 CGS C1 7/14/10 GEC 7/14/10 19:57 CGS C1 7/14/10 GEC 7/14/10 19:57 CGS C1
Page 3 of6
Page 18
ANALVFICAL <(..~\\'\ Acc 011 {) ,..._ -?If,-
I.ABIJRATDRV www.analrtlr:allab.r:om ~C) (><'"' Qo: ~·
!!!lsRuless, INe. NELAP Acuedlted (.) ::. PA :Z:Z•:ZJIS N.IPA010 (.)
< :I:
S4 Dogwood Ulne • Middletown, PA f7GS7 Phone: 7f7·SI44·554f FIIK: 7f7·SI44•f4SO
ANALYTICAL RESULTS
Workorder: 9853858 92230 Rehoboth
Lab 10: 9853858001 Date Collected: 7nt201 0 07:15 Matrix: Waste Water
Sample 10: 92230-Effluent Date Received: 7/8/2010 10:12
., .. ······M~thod
,~ /'•'' ..
A.·n~l#~d '" · .· By ~.OL Prepared By cntr '·'· .. ··.·. :·:.·.'·
Benzo(a)anthracene ug/L 1,4 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
Benzo(a)pyrene ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
Benzo(b )fluoranthene ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
Benzo(g,h,i)perylene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
Benzo(k)fluoranthene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
4-Bromophenyl-phenylether NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
Butylbenzylphthalate NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
4-Chloro-3-methylphenol NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
Bis(2~Chloroethoxy)methane NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 ./ Bis(2-Chloroethyl)ether NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
bis(2-Chloroisopropyl)ether NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
2-Chloronaphthalene NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
2-Chlorophenol NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
4-Chlorophenyl-phenylether NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
Chrysene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 01-n-Butylphthalate NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 Di-n-Octylphthalate NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 Dibenzo(a,h}anthracene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 3,3-Dichlorobenzidine NO ug/L 15.1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 2,4-Dichlorophenol NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 Diethylphthalate NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
2,4-Dimethylphenol NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1 Dimethylphthalate NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 2,4-Dinitrophenol NO ug/L 15.1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 2,4-Dinitrotoluene NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 2,6-Dinitrotoluene NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 1 ,2-Diphenylhydrazine NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 bis(2-Ethylhexyl)phthalate NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 Fluoranthene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 Fluorene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1 Hexachlorobenzene NO ug/L 2.8 EPA625 7/14/10 GEC 7114110 19:57 CGS C1 Hexachlorobutadiene NO ugiL 2.8 EPA625 7114110 GEC 7114/10 19:57 CGS C1 ·Hexachlorocyclopentadiene NO ug/L 7.5 EPA625 7114/10 GEC 7114110 19:57 CGS C1 Hexachloroethane NO ugiL 2.8 EPA625 7114110 GEC 7114110 19:57 CGS C1 lndeno(1,2,3-cd)pyrene NO ug/L 1.4 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 lsophorone NO ugiL 2.8 EPA625 7/14110 GEC 7114/10 19:57 CGS C1 2-Methyl-4,6-dinitrophenol NO ugiL 7.5 EPA625 7/14110 GEC 7114/10 19:57 CGS C1 Naphthalene NO ugiL 1.4 EPA625 7114110 GEC 7/14/10 19:57 CGS C1 Nitrobenzene NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 2-Nitrophenol NO ug/L 7.5 EPA625 7114110 GEC 7114110 19:57 CGS C1 4-Nitrophenol NO ug/L 7.5 EPA625 7/14/10 GEC 7/14110 19:57 CGS C1 N-Nitrosodimethylamine NO ugiL 2.8 EPA625 7/14110 GEC 7/14/10 19:57 CGS C1 N-Nitroso-di-n-propylamine NO ug/L 2.8 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 N-Nitrosodiphenylamine NO ug/L 2.8 EPA625 7114110 GEC 7114/10 19:57 CGS C1 Pentachlorophenol NO ug/L 15.1 EPA625 7/14/10 GEC 7114/10 19:57 CGS C1 Phenanthrene NO ug/L 1.4 EPA625 7/14110 GEC 7114110 19:57 CGS C1 Phenol NO ug/L 7.5 EPA625 7/14/10 GEC 7/14/1019:57 CGS C1
Report ID: 9853858 Page 4 of6
Page 19
ANALVFICAL LABtJRA'I'tJRV SsRIIIt:ss, INc.
www.ana~lcallab.com
NELAP Acuerllted PA :Z:Z•:Z!l!l N.l PAOfO.
$4 DogwOOd l.llne • Middletown, PA f70S7 Ph01te: 717·1144·5541 Fax: '717-DU•f/ISO
Workorder: 9853858 92230 Rehoboth
Lab ID: 9853858001
Sample 10: 92230-Effluent
Parllmet~rs ·· ResUlts Fllig unlts Pyrene NO ug/L 1 ,2,4-Trichlorobenzene NO ug/L 2,4,6-Trichlorophenol NO ug/L
Surrogate Recoveries Results Flag Units
2,4,6-Tribromophenol (S) 80 % Phenol-d5 (S) 26 % Terphenyl-d14 (S) 77 % Nitrobenzene-d5 (S} 66.4 % 2-Fiuorobiphenyl (S} 68.5 % 2-Fiuorophenol (S) 43.1 %
WET CHEMISTRY
Phenolics NO mg/L
METALS
Mercury, Total NO mg/L
Sample Comments:
ReportiD:9853858
ANALYTICAL RESULTS
Date Collected:
Date Received:
RDL
1.4 2.8 7.5
Limits
38-134 11-53
33-125 37-124 37-113 17-73
0.01
0.00050
7/7/2010 07:15 Matrix: WasteWater
7/8/2010 10:12
Metho¢· Prepared By Analyzed By ·cntr
EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
Method Prepared By Analyzed By Cntr
EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1 EPA625 7/14/10 GEC 7/14/10 19:57 CGS C1
EPA420.4 7/12/10 KRK 7/13/10 02:04 KRK E
EPA245.1 7/13/10 MNP 7/13/10 09:23 MNP F1
a.,.__/) JL.L_ Anna G Milliken
Laboratory Manager
Page 5 of6
Page 20
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s1 o H,ql?
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v~d_ Q ~ &_.o" (()~ ~~ "'() .
o .::::. SINCE 1984 • ~ ~-z- Cl):
Client Name: Contact:
Address:
Phone Cell Fax
email
City of Rehoboth Bob Stenger
P.O. Box 1163
Rehoboth, DE 19971
302-227-7801
302-227-4649
ners Received: (circle)
Q M N/P Bacti
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o,7<S-~ • L 1\. ~ ~~(D ~So J-1\. 0
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Email Reports 0 Fax Reports 0
Lab 1.0 Sample Description/Location Sample Date Time Matrix
~ Effluent Composite Start- "+-~·-(6 1'/l> I 0/Wt I IXIXIXIXIX End- '1:-1<-(-ID I ·:z;:-;:s ':>-- I o/W
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nnreserved), M=Metals (HN03), N/P=Nutrients (H2S04), Bacti=P/A Colilert® (Sodium Thiosulfate)
· Sampled by: ~ )=:§. ' ..) Date == caw ?i{!6 /Time. ___ _ Received by. ~~~_o.ar!lt/j;o mme j'{.l5-
Reliniquished by: Date /Time. __ _ Received by Date /Time. __ _
Reliniquished by: Date /Time. __ _ Received by Date /Time __ _
©2007 Envirocorp Inc. Rev Feb 2007
Page 22
:>1 "-i"'
/q.oc 01;· .. ,. 51 Clark St. Harrington, DE 19952 <..... "'()' > <,JW'I; ~""' • : ~---------~·--~---~ PH: 302.398.4313 FX: 302.398.4312 ~~---·------~-~--------
·::~ "'" \ .... L Jl-~ /. ANALYTICAL SERVICES: NPDES, RCRA, GROUND WATER MONITORING )' 7? IJ ~ • 'I" i
City of Rehoboth P.O. Box 1163 Rehoboth, DE 19971
Attention: Bob Stenger
Lab ID: 092834
Description:
Type: Composite
. Metals
Antimony Arsenic Beryllium Cadmium Chromium Copper Lead Mercury Metals Digestion for AA Nickel Selenium Silver Thallium Zinc
Miscellaneous/Other
SHIP
Printed: Aug 6 2010 9:41AM
ANALYTICAL RESULTS
Matrix: Waste Water
Site: 001
mg/L <0.0010 mg/L <0.0010 mg/L <0.0010 mg/L <0.00050 mg/L 0.0026 mg/L 0.0046 mg/L <0.0010 mg/L <0.00050
Completed mg/L 0.0038 mg/L <0.0010 mg/L <0.00050 mg/L <0.0010 mg/L 0.0374
Completed
Page 1 of 1
8/4/1 0 11 :25 8/4/1 0 11 :25 8/4/10 11 :25 8/4/1 0 11 :25 8/4/1 0 11 :25 8/4/1 0 11 :25 8/4/1 0 11 :25 7/19/10 10:21 7/29/10 9:00 8/4/1 0 11 :25 8/4/10 11 :25 8/4/1 0 11 :25 8/4/1 0 11 :25 8/4/1 0 11 :25
7/23/10 1:10
Sample Start: 7/13/10 7:40
SampleEnd: 7/14/10 7:35
Date Received: 7/14/10 14:25
HJG3 HJG3 HJG3 HJG3 HJG3 HJG3 HJG3 A LSI HJG3 HJG3 HJG3 HJG3 HJG3 HJG3
A LSI
EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 245.1 EPA 200.2 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8 EPA 200.8
None
ND =Not Detected * = Above Specified Limit ** =Above Client Limit
Page 23
SIIIJfJgWOOII "'ne • lllllldletown, IIA f70S7 Phone: 7f'J'·f1411·554f I'IIX: 7f'J'·844-f4SG
Certificate of Analysis Project Name: Routine Sample Submission
Purchase Order:
Ms. Shelly Bloom Enviro Corporation Inc. 51 Clark Street Harrington, DE 19952
July 28, 201 0
Dear Ms. Bloom,
Workorder: 9855093 Workorder ID: 92834
Enclosed are the analytical results for samples received by the laboratory on Thursday, July 15, 2010
ALSI is a National Environmental Laboratory Accreditation Program (NELAP) accredited laboratory and as such, certifies that all applicable test results meet the requirements of NELAP.
If you have any questions regarding this certificate of analysis, please contact Denise Brooks (Project Coordinator) or Anna G Milliken (Laboratory Manager) at (717) 944-5541.
Please visit us at www.analyticallab.com for a listing of ALSI's NELAP accreditations and Scope of Work, as well as other links to Water Quality documentation on the internet.
This laboratory report may not be reproduced, except in full, without the written approval of ALSI.
NOTE: ALSI has changed the report generation tool and while we have tried to retain the existing format, you will notice some changes in the laboratory report. Please feel free to contact ALSI in case you have any questions.
Analytical Laboratory Services, Inc.
This page is included as part of the Analytical Report and
must be retained as a permanent record thereof.
ReportiD:9855093
0--~~ Anna G Milliken
Laboratory Manager
Page 1 of6
Page 24
ANALVTICAL I.A&ORAFORV IIIIERIIICES, INC.
WIVW.GnGIJitiCGIIGb.COnt
IIEIJUI ACCNHllted PA 22·2fiS N.l Pllllft:l
Sll Dogf/f/0011 ltllffl • lllllddleftlwn, PA f7IJ57 """"e: 7f7·fl44·554f PfiJt: 7f74144-f4~0
SAMPLE SUMMARY
Workorder: 9855093 92834 Discard Date: 08/10/2010
Lab ID Sample ID Matrix Date Collected Date Received Collected By
9855093001 92834-Effluent WasteWater 7/14/10 07:35 7/15/10 10:30 Customer
Workorder Comments:
Notes - Samples collected by ALSI personnel are done so in accordance with the procedures set forth in the ALSI Field Sampling Plan (20 -
Field Services Sampling Plan). - All Waste Water analyses comply with methodology requirements of 40 CFR Part 136. -- All Drinking Water analyses comply with methodology requirements of 40 CFR Part 141. -- Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis. - The Chain of Custody document is included as part of this report.
Standard Acronyms/Flags J, B Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Ouantitation Limit (POL} for the analyte
U Indicates that the analyte was Not Detected (ND) MDL Method Detection Limit POL RDL ND Cntr
RegLmt LCS MS
MSD DUP
%Rec RPD
Practical Ouantitation Limit Reporting Detection Limit Not Detected - indicates that the analyte was Not Detected at the RDL Analysis was performed using this container Regulatory Limit Laboratory Control Sample Matrix Spike Matrix Spike Duplicate Sample Duplicate Percent Recovery Relative Percent Difference
ReportiD:9855093 Page 2 of6
Page 25
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ANALYTICAL RESULTS
Workorder: 9855093 92834
Lab ID: 9855093001 Date Collected: 7/14/2010 07:35 Matrix: WasteWater
Sample ID: 92834-Effluent Date Received: 7/15/2010 10:30
Parameters Results Flag Units RDL Method Prepared By Analyzed By Cntr
VOLATILE ORGANICS
Acrolein ND ug/L 30.0 EPA624 7/23/10 01:10 TMP A
Acrylonitrile ND ug/L 5.0 EPA624 7/23/10 01:10 TMP A Benzene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Bromodichloromethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A
Bromoform ND ug/L 2.0 EPA624 7/23/10 01:10 TMP A Bromomethane ND ug/L 2.0 EPA624 7/23/10 01:10 TMP A Carbon Tetrachloride ND ugiL 1.0 EPA624 7/23/10 01:10 TMP A Chlorobenzene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Chlorodibromomethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Chloroethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 2-Chloroethylvinyl ether ND ug/L 2.0 EPA624 7/23/10 01:10 TMP A Chloroform ND ug/L 1.0 EPA624 7123/10 01:10 TMP A Chloromethane ND ugiL 1.0 EPA624 7/23/10 01:10 TMP A 1 ,2-Dichlorobenzene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1 ,3-Dichlorobenzene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1 A-Dichlorobenzene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1, 1-Dichloroethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1 ,2-Dichloroethane ND ugiL 1.0 EPA624 7/23/10 01:10 TMP A 1, 1-Dichloroethene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A trans-1 ,2-Dichloroethene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1 ,2-Dichloropropane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A cis-1 ,3-Dichloropropene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A trans-1 ,3-Dichloropropene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1 ,3-Dichloropropene, Total ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Ethyl benzene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Methylene Chloride ND ugiL 1.0 EPA624 7/23/10 01:10 TMP A 1,1 ,2,2-Tetrachloroethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Tetrachloroethene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Toluene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1,1, 1-Trichloroethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A 1,1 ,2-Trichloroethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Trichloroethene ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Trichlorofluoromethane ND ug/L 1.0 EPA624 7/23/10 01:10 TMP A Vinyl Chloride ND ug/L 2.0 EPA624 7/23/10 01:10 TMP A
Surrogate Recoveries Results Flag Units Limits Method Prepared By Analyzed By Cntr
1 ,2-Dichloroethane-<:14 (S) 112 % 72-142 EPA624 7/23/10 01:10 TMP A 4-Bromofluorobenzene (S) 87.2 % 73-119 EPA624 7/23/10 01:10 TMP A Dibromofluoromethane (S) 113 % 74-132 EPA624 7/23/10 01:10 TMP A Toluene-dB (S) 110 % 75-133 EPA624 7/23/10 01:10 TMP A
SEMIVOLATILES
Acenaphthene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Acenaphthylene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Anthracene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Benzidine ND ug/L 18.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1
ReportiD:9855093 Page 3 of6
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ANALYTICAL RESULTS
Workorder: 9855093 92834
Lab 10: 9855093001 Date Collected: 7/14/2010 07:35 Matrix: WasteWater
Sample ID: 92834-Effluent Date Received: 7/15/2010 10:30
Parameters Results Flag Units RDL Method Prepared By Analyzed By Cntr
Benzo(a)anthracene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/1 0 12:39 DRS C1 Benzo(a)pyrene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Benzo(b)fluoranthene NO ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Benzo(g,h,i)perylene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Benzo(k)fluoranthene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 4-Bromophenyl-phenylether ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Butylbenzylphthalate NO ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 4-Chloro-3-methylphenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Bis(2-Chloroethoxy)methane ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Bis(2-Chloroethyl)ether ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 bis(2-Chloroisopropyl)ether ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2-Chloronaphthalene NO ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2-Chlorophenol NO ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 4-Chlorophenyl-phenylether NO ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Chrysene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Di-n-Butylphthalate ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Di-n-Octylphthalate ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Dibenzo(a,h)anthracene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 3,3-Dichlorobenzidine ND ug/L 15.0 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2,4-Dichlorophenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/1 0 12:39 DRS C1 Diethylphthalate ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2,4-Dimethylphenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Dimethylphthalate NO ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2,4-Dinitrophenol ND ug/L 15.0 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2,4-Dinitrotoluene ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2,6-Dinitrotoluene ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 1 ,2-Diphenylhydrazine ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 bis(2-Ethylhexyl)phthalate ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Fluoranthene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Fluorene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Hexachlorobenzene ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Hexachlorobutadiene ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Hexachlorocyclopentadiene ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Hexachloroethane ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 lndeno(1 ,2,3-cd)pyrene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 lsophorone ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2-Methyl-4,6-dinitrophenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Naphthalene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Nitrobenzene ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 2-Nitrophenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 4-Nitrophenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 N-Nitrosodimethylamine ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 N-Nitroso-di-n-propylamine ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 N-Nitrosodiphenylamine ND ug/L 2.8 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Pentachlorophenol ND ug/L 15.0 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Phenanthrene ND ug/L 1.4 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1 Phenol ND ug/L 7.5 EPA625 7/21/10 CAC 7/24/10 12:39 DRS C1
ReportiD:9855093 Page4 of6
Page 27
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