This document is downloaded from DR‑NTU (https://dr.ntu.edu.sg)Nanyang Technological University, Singapore.
Performance characteristics of hot mix asphaltwith recycled materials
Lee, Zhen Hao.
2009
http://hdl.handle.net/10356/16328
Nanyang Technological University
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Performance Characteristics of Hot Mix Asphalt With
Recycled Materials
Lee Zhen Hao
School of Civil and Environmental Engineering
College of Engineering
Nanyang Technological University
2009
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Performance Characteristics of Hot Mix Asphalt
With Recycled Materials
Submitted by
Lee Zhen Hao
School of Civil and Environmental Engineering
College of Engineering
Nanyang Technological University
A Final Year Project Report presented to the
Nanyang Technological University
in partial fulfilment of the requirements for the
Degree of Bachelor of Engineering
2009
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Summary
In this study, Recycled Concrete Aggregate (RCA) was used as a partial replacement of
Indonesian granite aggregates in LTA’s W3B mix to evaluate it’s feasibility in hot mix asphalt
(HMA) application.
Nine Marshall specimens were fabricated with a binder range of 4.75% to 5.25%. The optimum
binder content of 5.3% was adopted from the results of the Marshall Test. An amount of 50% of
the top three sieve sizes (>6.3mm) was replaced by RCA in the research.
Large pavement slabs of the hybrid mix were fabricated to simulate field constructed conditions.
Specimens were cored from the slabs and tests were conducted to compare the performance
characteristics of the hybrid HMA mix with conventional W3B mix.
The results from the creep tests, on average, revealed higher creep stiffness but lower
accumulated strain than those obtained by past studies which involved the fabrication of
conventional W3B slab specimens. The findings suggest that the hybrid mix is stiffer and less
able to take as much strain as LTA’s W3B mix.
The rutting tests showed that the hybrid mix has lower track rate, exhibiting higher rutting
resistance than the conventional W3B. This can be due to the specimens being heavily
compacted during the fabrication, which keeps the aggregate highly interlocked and resistant to
rutting.
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Acknowledgements
The author would like to express his gratitude and appreciation to his project supervisor, Dr
Wong Yiik Diew, who has spent invaluable time suggesting ideas, guidance and insights
throughout this study.
The author would also like to thank Dr Lum Kit Meng for his assistance and allowing the author
and his partner to work in the Transport Lab after office hours.
Thanks are extended to the Transportation Lab technicians, Mr Choi Siew Pheng, Ms Ng-Ho
Choo Hiang and Mr Andrew Liew Kai Liang for providing technical assistance and supplying
equipment for the project throughout this study.
The author would like to thank Ph. D. candidate Ms Anggraini Zulkati in providing much help
and advice during the duration of the research.
Lastly, the author would also like to thank his project partner Mr Loy Pei Ping for providing the
valuable support, effort and time to work with the author throughout the year of work.
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TABLE OF CONTENTS
Page
Summary 2
Acknowledgements 3
Table of Contents 4
List of Tables 7
List of Figures 8
List of Standards ix
Chapter 1: Introduction
1.1 Background 1
1.2 Objectives 2
1.3 Scope of Work 2
1.4 Organisation of Report 3
Chapter 2: Literature Review
2.1 Recycled Concrete Aggregate (RCA)
2.1.1 Past and Present Developments of RCA 5
2.1.2 Physical Properties of RCA 5
2.1.3 Mechanical Properties of RCA 6
2.2 Creep and Rutting Characteristics of HMA Pavement
2.2.1 Creep performance 7
2.2.2 Rutting Performance 7
Chapter 3: Material Properties and Characteristics
3.1 Introduction 8
3.2 Bitumen 8
3.3 Indonesian Granite 8
3.3.1 Physical and Mechanical Properties 9
3.3.2 Specific Gravity and Water Absorption 10
3.4 Recycled Concrete Aggregates (RCA) 11
3.4.1 Selection of RCA Source 11
3.4.2 Physical and Mechanical Properties of RCA 11
3.4.3 Selection of Aggregate Sizes for Replacement with RCA 12
3.4.4 Specific Gravity and Water Absorption 12
Chapter 4: Marshall Mix Design
4.1 Introduction 13
4.1.1 Marshall Design Criteria and Important Design Parameters 13
4.1.2 Specifications 14
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4.1.3 Aggregate Gradation 16
4.2 Marshall Test Results 18
Chapter 5: Slab Fabrication
5.1 Introduction 21
5.2 Specimen Fabrication 21
5.3 Asphalt Content Tester 23
Chapter 6: Dynamic Creep Test
6.1 Test Objectives 25
6.2 Test Procedure 25
6.3 Test Results 26
Chapter 7: Rutting Test
7.1 Test Objectives 28
7.2 Track Rate and Relative Rut Depth 28
7.3 Test Procedure 29
7.4 Test Results 30
Chapter 8: Conclusion and Discussion
8.1 Review of Results 31
8.2 Recommendations 32
References 33
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APPENDICES
Appendix A Results for Change in Gradation of Recovered W3B-RCA Specimens
Appendix B Marshall Specimen Mass-Volume Relationship Table
Appendix C Measurements of Cored Specimens
Appendix D Results from Asphalt Content Tester
Appendix E Data Output from Dynamic Creep Test
Appendix F Time Schedule for Rutting Test
Appendix G Data Output from Rutting Test
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LIST OF TABLES
Page
Table 2.1 Typical Physical Properties of Processed 6
Reclaimed Concrete Material
Table 2.2 Typical Mechanical Properties of RCA 7
Table 3.1 LTA Requirements for Bitumen of Penetration 60/70 8
Table 3.2 Mechanical Properties and Requirements for Indonesian Granite 10
Table 3.3 Bulk Specific Gravity (OD) and Water Absorption of Indonesian 10
Granite (Cheong, 2007)
Table 3.4 Bulk Specific Gravity (OD) and Water Absorption of Indonesian 10
Granite (Ang, 2008)
Table 3.5 Mechanical Properties of RCA (Ang, 2008) 12
Table 3.6 Specific Gravity and Water Absorption for RCA (Ang, 2008) 12
Table 4.1 Important Design Parameters for Marshall Design Criteria 13
Table 4.2 Specification for Marshall Specimen Preparation 14
(ASTM D1559-89, 1994)
Table 4.3 LTA W3B Gradation Specifications 16
Table 4.4 Gradation of Hybrid Mix W3B-RCA27 18
Table 4.5 Summary of Marshall Specimen Test Results 18
Table 5.1 Gradation of W3B-RCA27 Slab Mix 21
Table 6.1 Dynamic Creep Test Conditions 26
Table 6.2 Dynamic Creep Test Results from Lee (2009) and Ho (2003) 27
Table 7.1 Rutting Test Results 30
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LIST OF FIGURES
Figure 1.1 Projects Flowchart 4
Figure 4.1 Graph of LTA’s W3B Gradation 16
Figure 4.2 Density, Flow, Stability (%), VTM (%), VFB (%), 19
VMA (%) vs Binder (%)
Figure 5.1 Wheel Roller Compactor (left), Machine Cutter (middle) 21
and Coring Machine (right)
Figure 5.2 Layout of Slab 23
Figure 5.3 Asphalt Content Tester 23
Figure 6.1 Universal Testing Machine (UTM) fitted with 25
Dynamic Creep Test Equipment
Figure 7.1 Wheel Tracking Machine 28
Figure 7.2 Cored Specimens S1-1 and S2-2 after Rutting Test 30
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LIST OF STANDARDS
AS 2891.12.1 – 1995 Determination of the Permanent Compressive Strain Characteristics
of Asphalt – Dynamic Creep Test
ASTM C127 – 04 Standard Test Method for Density, Relative Density (Specific
Gravity), and Absorption of Coarse Aggregate
ASTM D1559-89 Test Method for Resistance of Plastic Flow of Bituminous Mixtures
Using Marshall Apparatus
ASTM D2041 – 03a Standard Test Method for Theoretical Maximum Specific Gravity
and Density of Bituminous Paving Mixtures
ASTM D3549-03 Standard Test Method for Thickness or Height of Compacted
Bituminous Paving Mixture Specimens
ASTM D6926 – 04 Standard Practice For Preparation Of Bituminous Specimens Using
Marshall Apparatus
ASTM D6927 – 06 Standard Test Method for Marshall Stability and Flow of
Bituminous Mixtures
BS 598: PART 110: 1996 Method of Test for the Determination of Wheel-Tracking Rate
BS 812: PART 2: 1995 Methods of Determination of Density
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Chapter 1
INTRODUCTION
1.1 Background
Waste minimisation projects and research started many years ago. With an increasing waste
stream and global warming situation of our environment worsening over the past ten years, the
emphasis on waste minimisation has become even more crucial. Having effective ways to
minimise the amount of waste produced can contribute greatly towards protecting the
environment.
Several strategies are adopted by Singapore’s government to promote awareness of waste
minimisation. The aims are to formulate holistic waste minimisation policies and approaches,
undertake research and feasibility studies, encourage all sectors of the community to practise
waste minimisation and set up recycling programmes. Lastly, public education is to be given on
waste minimisation and recycling (NEA, 2002).
From a field trip by the author to Tuas Marine Transfer Station (TMTS) in September 2008, it
was found that out of the 350 hectares of landfill area, around 80 hectares of land has been
reclaimed up to the sea level. The Semakau landfill will be expected to meet Singapore’s need
for landfill space until 2045 (NEA, 2006).
In the year 2007, 778,300 tonnes of construction debris was produced in Singapore (NEA,
2008) and 98% of construction debris has been recycled. The remaining 2% consist of non-
recyclable or hazardous by-products that have to be disposed properly.
In Singapore, out of the total of $1.3 billion projected in the creation of Semakau Landfill, $610
million has been spent to date. Semakau Landfill is currently Singapore’s only landfill for waste
disposal. Due to Singapore’s lack of physical land area, recycling should play a major role in
reducing the landfill requirement. Use of recycled concrete aggregate (RCA) will also reduce
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our dependency on raw material.
1.2 Objectives
The main objective of this research was to assess the feasibility of substitution of coarse granite
aggregate (>3.35mm) with RCA, based on equivalent-volume replacement. To achieve this, the
author conducted experiments to measure the specific gravity of granite and RCA. Next, the
author decided on a replacement percentage of granite aggregate with RCA in terms of
equivalent volume.
After this, the author used the Marshall Mix Design method to determine the optimum binder
content of Pen 60/70 bitumen for design mix with RCA. Finally, the author and his partner
determine the creep characteristics and rutting performance of the design mix by fabricating
slabs and testing the cored samples.
1.3 Scope of Work
The research comprised of stages as illustrated in Figure 1.1.
The first stage of work was literature review of past research on hot mix asphalt with recycled
materials done in NTU, as well as from other sources. Time was also assigned to the
familiarisation of test equipment to be used throughout the experiment.
The second stage was the selection of the materials required for the research, as well as to
determine the replacement percentage by volume of granite aggregate with RCA. This was done
by obtaining the specific gravity of batches of granite aggregate and RCA through measurement
tests and doing a density conversion. Marshall specimens were fabricated and tested to
determine the optimum binder content of the hybrid mix.
In the third stage the author produced slab specimens according to the hybrid mix and cored
samples from the slabs. Tests were conducted on the cored samples to determine their resistance
to creep and rutting.
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The last stage involved the assessment of the test results and conclusions were made. This will
in turn allow for recommendation on further analysis of the feasibility of RCA.
1.4 Organisation of Report
The report is organised into 8 chapters, with the first chapter as the introduction.
Chapter 2 provides a literature review on the past and present developments of Recycled
Concrete Aggregate and past uses in pavement mixes.
Chapter 3 provides information on the physical and mechanical properties of the materials used
in the study.
Chapter 4 gives an in-depth review of the Marshall Mix Design Method. Trial hybrid Hot Mix
Asphalt (HMA) specimens are fabricated and tested. Important test parameters are discussed.
From various tests, the optimum binder content is obtained.
Chapter 5 involves the procedure for the fabrication of large slabs and the coring of sample
specimens to be tested. Physical parameters of the samples are measured and recorded.
Chapter 6 describes the Dynamic Creep test to obtain Creep Stiffness and Accumulated Strain.
Results are compared with previous studies.
Chapter 7 deals with the Rutting test conducted on large slab test samples and comparing the
results with past studies.
Chapter 8 summarises the findings of the study, reviewing the values obtained and giving
recommendations to improve the HMA mix design.
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Figure 1.1 Project Tasks Flowchart
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Identification of Objectives
Literature Review
Familiarisation of Test Equipment
Selection of Test EquipmentAggregate Material SelectionGraniteRecycled Concrete AggregateBinder Type
Mix Design and Specimen Preparation
Marshall Test (Destructive)
Determination of Optimum Binder Content
Preparation of Slab Specimens atOptimum Binder Content
Rutting Test Creep Test
Results and Discussions
Conclusions and Recommendations
Task 1
Task 2
Task 3
Task 4
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Chapter 2
LITERATURE REVIEW
2.1 Recycled Concrete Aggregate (RCA)
2.1.1 Past and Present Developments of RCA
Countries like America, United Kingdom, Japan and Germany have researched in construction
and demolition (C&D) waste aiming to find possible uses of recycled concrete aggregate (RCA)
as an alternative to natural granite aggregate for the construction sectors (Cheong, 2007).
In 2003, a Federal Highway Administration (FHWA) report has shown that recycled concrete
aggregate (RCA) used in the base and sub-base material has a beneficial performance (Focus,
April 2004). In the report, it is found that RCA application provides engineering, economic, and
environmental benefits. With regards to the environment, the need for construction debris to be
disposed of to landfills is also eliminated. The California Department of Transportation’s
(Caltrans) has also discovered that even though start up costs for collecting RCA is high,
hauling and overhead cost is reduced (FHWA 2003). This issue is of a lower importance in
Singapore due to its small land area. It can be seen that there can be further expansion in RCA
application in highway pavements.
In Singapore, RCA is obtained through the crushing of C&D waste into controlled sizes. To
obtain a clean batch of RCA, the sorting process is inclusive of the removal of steel and weaker
materials like wood.
2.1.2 Physical Properties of RCA
RCA is produced from construction debris and is angular in shape. RCA is coated with mortar,
which is due to hydrated cement that remains adhered to the aggregate after the batching
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process. This mortar may also contain cement paste that has not hydrated during the prior
construction phase. RCA has a surface texture which is rougher in comparison to virgin
Indonesian granite. It is also more porous, and has a lower specific gravity than Indonesian
granite.
Smaller RCA has a lower specific gravity compared to larger ones. This is because smaller RCA
has a proportionately larger surface area as compared to larger RCA. Smaller RCA tend to have
higher water absorption as well. Physical properties of RCA are given in Table 2.1.
Table 2.1 Typical Physical Properties of Processed Reclaimed Concrete Material (FHWA, 2006)
Property ValueSpecific Gravity, %
2.2 to 2.5
2.0 to 2.3
Coarse aggregate
Fine aggregate
Absorption, %
2 to 6
4 to 8
Coarse aggregate
Fine aggregate
2.1.3 Mechanical Properties of RCA
RCA that is larger than 4.75mm in size has been reported to have favourable mechanical
properties for aggregate use. RCA greater than 4.75mm in size has good abrasion resistance,
good bearing strength and good soundness characteristic. Magnesium sulfate soundness and
California Bearing Ratio (CBR) values are comparable to conventional granite aggregate. The
mechanical properties of RCA are given in Table 2.2.
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Table 2.2 Typical Mechanical Properties of RCA (FHWA, 2006)
Property ValueLos Angeles Abrasion Loss (ASTM C131), %
20 – 45Coarse Aggregate
Magnesium Sulfate Soundness Loss (ASTM C88), %
< 4
< 9
Coarse Aggregate
Fine Aggregate
California Bearing Ratio (CBR), % 94 to 148
2.2 Creep and Rutting Characteristics of HMA Pavement
2.2.1 Creep performance
Creep is defined as the permanent deformation tendency of a material under loading. The rate of
such a deformation is a function of its material properties, time of exposure to loading as well as
the amount of applied stress. In this case creep deformation is time-dependent and occurs upon
accumulation of strain over a certain period of loading time.
HMA pavements that are subjected to traffic loading over a long period of time will eventually
develop creep deformation. Subsequently, this will result in rutting failure of the pavement.
2.2.2 Rutting Performance
Rutting is defined as the accumulation of small amounts of unrecoverable strain as a result of
repeated loading applied to the HMA pavement. The author performed creep tests and rutting
performance tests, simulating in-situ conditions, to estimate creep and rutting potential of the
design mix.
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Chapter 3
MATERIAL PROPERTIES AND CHARACTERISTICS
3.1 Introduction
The HMA of this research consists of aggregate types comprising Indonesian granite and RCA,
as well as the binder bitumen. The properties of these materials shall be elaborated in this
chapter.
3.2 Bitumen
Bitumen is a black material which is a by-product of petroleum refining processes. It is highly
viscous at temperatures above 100 degrees Celsius and is solid at room temperature. At room
temperature it has excellent weathering properties, water resistance, flexibility and ductility.
Bitumen is widely used as binder of aggregate in flexible pavement construction. No tests were
done on the bitumen as tests have been performed by NTU students regularly in every semester
and consistent results that meet LTA’s requirements have been obtained. The required properties
are shown in Table 3.1.
Table 3.1 LTA Requirements for Bitumen of Penetration 60/70 (LTA. 2009)
Property RequirementsPenetration at 25oC, 100g, 5s (0.1mm) 60 - 70Softening point, ring and ball (oC) 47 – 56Flash point, Cleveland open cup (oC)
Thin film oven test, 3.2mm at 163 oC, 5hrs
(i) Loss in heating (% by weight)
(ii) Penetration of residue at 25 oC (% of original penetration)
(ii) Ductility of residue at 25 oC at 5cm/min (cm)
Min. 230
Max. 0.8
Min. 52
Min. 55Solubility in trichloroethylene (% by weight) Min. 99.5Specific gravity at 25 oC 1.0 – 1.11
3.3 Indonesian Granite
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This research uses granite aggregate originating from Indonesia. The batch of Indonesian
granite was the same as Ang’s (2008). Coarse aggregate (>3.35mm) offers the major support in
carrying load, whereas the fine aggregate (<3.35mm) provides filler accommodation for the
voids in the binder mix. Selection of aggregate is determined by the following characteristics:
• Toughness
• Porosity
• Surface Texture
• Soundness
• Polish Resistance
• Specific Gravity
• Absorption and Affinity for Binder
• Sensitivity to Chemical Additives
• Particle Size And Aggregate Gradation
• Cleanliness (Or Clay Content)
• Particle Shape
3.3.1 Physical and Mechanical Properties
Cheong (2007) and Phoon (1998) have performed Los Angeles abrasion test, aggregate crushing
value test and 10% fines test on the Indonesian granite according to ASTM and Singapore
Standards. It is found that the mechanical properties of the granite meet the minimum
specifications set out by LTA. The following are the requirements by LTA as well as the results
of Cheong (2007) and Phoon’s (1998) studies, as shown in Table 3.2.
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Table 3.2 Mechanical Properties and Requirements for Indonesian Granite (LTA 2009)
Property Measured Value Allowable Value Test MethodLos Angeles Abrasion Test 30.44% < 40.00% ASTM C131 – 06Aggregate Crushing Value Test 21.55% < 35.00% SS 73:197410% Fines Test 204.6kN > 130.000kN (NZ) SS 73:1974
The author has verified through consistent results in past reports that Indonesian granite is able
to meet the requirements as set out by LTA. Thus our batch of Indonesian granite is suitable for
use as an aggregate in HMA pavement construction.
3.3.2 Specific Gravity and Water Absorption
Specific gravity is defined as the ratio of the density of a given solid or liquid to the density of water
at a specific temperature and pressure. Aggregate with high voids will have a higher water
absorption compared to aggregate with low voids. More binder will be absorbed into aggregate with
high absorption, and this will cause a drop in the compactability of the mix.
Cheong (2007) has conducted specific gravity and water absorption tests according to BS 812:
Part 2. The figures are reported as in Tables 3.3.
Table 3.3: Bulk Specific Gravity (OD) and
Water Absorption of Indonesian Granite (Cheong, 2007)
Sizes (mm) Bulk Specific Gravity
(Oven Dry)
Water Absorption (%)
19.0 – 3.35 2.572 0.8243.35 – 1.18 2.590 0.634
1.18 – 0.3 2.586 0.929
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Tests conducted by Ang (2008) gave results similar to Cheong’s (2007) and are summarised in
Table 3.4.
Table 3.4: Bulk Specific Gravity (OD) and
Water Absorption of Indonesian Granite (Ang, 2008)
Sizes (mm) Bulk Specific Gravity
(Oven Dry)
Water Absorption (%)
19- 13.5 2.592 0.435
13.5- 6.30 2.596 0.4476.30- 3.35 2.599 0.6153.35- 1.18 2.601 0.3561.18- 0.30 2.594 0.4360.30- 0.075 2.525 1.4210.075- pan 2.560 1.035
3.4 Recycled Concrete Aggregates (RCA)
3.4.1 Selection of RCA Source
The RCA used in this research is taken from Samwoh Recycling Plant. The batch of RCA used
in this research was the same as Ang’s (2008). In the Construction Laboratory, the author
checked the composition of granite and RCA by quickly washing the aggregates under running
water. RCA is more powdery than granite. White patches can be visibly seen adhered to the
surface of RCA. The batch of RCA was then sieved to obtain aggregate sizes corresponding to
those of the first 3 sieve sizes of LTA’s W3B Gradation. Debris material like chips of brick and
broken metal wires were removed during the sieving of RCA.
3.4.2 Physical and Mechanical Properties of RCA
Ang (2008) has done LA abrasion test, aggregate crushing value test and 10% fines test on this
batch of RCA to ensure that the mechanical properties of the aggregate meet the specifications
set out by LTA. The results are shown in Table 3.5.
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Table 3.5 Mechanical Properties of RCA (Ang, 2008)
Property Measured Value LTA’s Allowable
Value
Test Method
Los Angeles abrasion test 32.30% < 40.00% ASTM C131 – 06Aggregate crushing value test 21.55% < 35.00% SS 73:197410% fines test 146.0kN > 130.000kN (NZ) SS 73:1974
3.4.3 Selection of Aggregate Sizes for Replacement with RCA
Ang’s (2008) report has shown that there is comparable strength and rutting performance in the
use of coarse RCA (>6.3mm) in HMA pavement. The author has conducted some visual
inspection and noticed how aggregate 3.35mm down consisted of mostly mortar which was
easily broken up into even smaller pieces. This is consistent with Ang’s (2008) inspection.
It is also reported from FHWA that the specific density of RCA decreases while water
absorption increases as the size of aggregate decreases. This is due to the higher mortar
proportion adhering to finer RCA (FHWA. 2006).
The performance of the hybrid mix will decrease in terms of flexural strength and deformation with
higher mortar content. Hence we will use coarse RCA and avoid the use of fine RCA in our
experiment.
3.4.4 Specific Gravity and Water Absorption
Ang (2008) has conducted specific gravity and water absorption tests for coarse RCA and they
found values consistent with those reported in the literature. RCA generally has a lower specific
gravity and higher water absorption than Indonesian Granite, as shown in Table 3.6.
Table 3.6 Specific Gravity and Water Absorption for RCA (Ang, 2008)
Sieve Size (mm) Bulk specific gravity (Oven Dry) Water Absorption (%)19.0 – 13.5 2.323 4.83913.5 – 9.5 2.328 4.9299.5 – 6.3 2.331 5.009
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Chapter 4
MARSHALL MIX DESIGN
4.1 Introduction
The specifications for Marshall Specimen preparation will be covered in this chapter, as well as
the Marshall Design Criteria. Specimens will be fabricated according to a speculated range of
binder contents and tests will be conducted to obtain important design parameters. The optimum
binder content will be found from the results that meet the Marshall Design Criteria and this
binder content will be used for fabrication of the slab.
4.1.1 Marshall Design Criteria and Important Design Parameters
The Marshall Design Criteria is based on three volumetric properties and two mechanical
properties (see Table 4.1). The volumetric properties are Voids in total mix (VTM), Voids in
Mineral Aggregate (VMA), and Voids filled with binder (VFB). The two mechanical properties
are stability and flow. Using the mass-volume relationship of a Marshall specimen, it was found
out that stability and flow values are not greatly affected by the type of aggregate and asphalt
used, while the volumetric properties (VTM, VMA and VFB) are dependent on the quality of
the aggregate used.
Table 4.1 Important Design Parameters for Marshall Design Criteria
Property Limits
Mechanical Stability >9.0kN
Flow 8 to 16 units OR 2 to 4mm
Volumetric Voids in Total Mix, VTM 3 to 5%
Voids Filled with binder, VFB 75% to 82%
Past studies have highlighted that it is difficult to reach the design criteria. Values are often
found at the opposite limits within the criteria. For example, a mix that meets the criteria for
VFB at the upper limit may have a flow that is too high. Nevertheless, a compromise can be
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made to choose an optimum binder content that will produce the best performance for the
hybrid mix.
4.1.2 Specifications
Table 4.2 shows the specifications for the production of a Marshall specimen.
Table 4.2 Specification for Marshall Specimen Preparation (ASTM D1559-89, 1994)
Aggregate Heating Temperature (2 hours) 105 - 110°CBitumen Heating Temperature (2 hours) 150°C (for PEN 60/70)
Compaction Temperature 135 - 150°C (for PEN 60/70)Tamper Foot Flat and circular with a diameter of 98.4 mm
corresponding to an area of 76 cm²Trowelling 15 times round the perimeter and 10 times in the
centre leaving a slightly rounded surface
Compaction Pressure 457.2 mm free fall drop distance of a hammer
assembly with a 4536 g sliding weightNumber of Blows 75 on each side ( for heavy traffic loading)
Mould Size 101.6 mm DiameterSpecimen Height 65 - 75mm
In our experiments, other than following the specifications in ASTM D1559-89, some
alterations were made due to lab constraints and to improve the quality of the specimen:
The aggregates and bitumen were put in the oven to be preheated at 120°C for 4 hours
instead of 2 hours and compaction was done at 100°C;
Pieces of round paper were cut and placed at the bottom and the top of the Marshall
specimen during the compaction to prevent the mixture from sticking to the metal collar;
The compacting mould, collar and base were oiled after the production of each specimen to
prevent the mixture from sticking to them.
In our preliminary, specimens were fabricated and broken up before compaction to test for
breakages of RCA by machine mixing. Tests were done with a total replacement of RCA with
the top three coarse grain sizes of granite aggregate for , with 2 W3B specimens for comparison.
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The results from the test are shown in Appendix A.
The graphs in Appendix A showed that the recovered gradations of all four specimens have
fallen out of LTA’s specifications in the fines area of 1mm down. W3B has suffered, on average,
10.4% breakages in its coarse aggregate while the hybrid specimen has suffered 15.9% in
breakages of its coarse aggregate. The author concluded that the increase in breakages is due to
the inclusion of RCA in the mix.
In terms of fines, W3B specimens have a loss of 11.4% while RCA hybrid specimen 1 has a loss
of 9.04%. This can be due to mortar in the RCA clumping up into larger particles during
recovery, and are not washed away. Granite fines are free of mortar and cleaner than RCA. Thus
granite fines do not clump up together as easily. To conclude, it is seen that the amount of
breakage from RCA during machine mixing is rather negligible and will produce specimens of
comparable strength in terms of rutting and creep resistance.
For preparation of the actual Marshall specimens, the following improvements were made to the
procedure:
For consistency, the duration for machine mixing of the aggregates and bitumen was
restricted to 4 minutes. If the aggregates are found not to be totally covered in bitumen, the
mixture is given another 30 seconds of machine mixing. In this way, we minimise the
possibility of variances in performance due to breakages from machine mixing.
A spatula was used to push the mixture carefully into the mould to prevent segregation of
the aggregates.
For additional steps in Marshall Specimen production, after taking the specimens out from
the extruder, the top filter paper is then removed and the specimen is labelled with a wax
pencil. Finally the specimen is left to cool to room temperature.
In Ang’s (2008) report, the hand-mixing method was used for Marshall specimen
production. To better simulate an in-situ condition, the author has used machine mixing and
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machine compaction in production of the Marshall mix specimens. During the process, care
was taken to guard against segregation of the aggregates when pouring the hot mix from
the machine-mix heating bowl into the Marshall mould.
4.1.3 Aggregate Gradation
In this research the LTA W3B gradation with nominal sieve size 13.2mm is adopted. Aggregates
were sieved and blended satisfying upper and lower limit requirements as shown in Figure 4.1
and Table 4.3. Aggregates of size 3.35mm and above are considered to be coarse aggregates and
those below are considered fines.
Table 4.3 LTA W3B Gradation Specifications
Sieve Size (mm) W3B Gradation Envelope Mid Value
Lower Higher
19 100 100 100 13.2 85 95 90 6.3 58 68 63
3.35 40 50 45
1.18 21 31 25
0.3 11 17 14
0.075 4 8 6
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Figure 4.1 Graph of LTA’s W3B Gradation
LTA W3B Gradation
0
10
20
30
40
50
60
70
80
90
100
0.01 0.1 1 10 100Aggregate Size
Vo
lum
e P
ass
ing
(%
)
Upper Limit
Lower Limit
W3B(cm^3)
It has been found that previous design mix samples that have partial replacement of RCA by
Ang (2008) and Cheong (2007) are of a greater thickness. In a previous study of substitution of
granite for glass (Thein Moe, 2005), glass hybrid Marshall specimens have been found to be
generally thicker than the standard W3B Marshall specimen. This increased thickness is due to
‘over’ replacement of the aggregate by equivalent mass. Hence we have adopted the
replacement of Indonesian granite for RCA by equivalent volume.
Table 4.4 shows the gradation of the finalised hybrid mix. As 27% of the aggregate has been
substituted with RCA, the hybrid specimen shall be named W3B-RCA27.
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Table 4.4 Gradation of Hybrid Mix W3B-RCA27
Sieve Size (mm) Weight (g)
W3B mix W3B-RCA27 mix
Granite Granite RCA
19 - 13.2 120 60 58.84
13.2 - 6.3 324 162 160.75
6.3 - 3.35 216 108 99.66
3.35 - 1.18 228 228 0
1.18 - 0.3 144 144 0
0.3 - 0.075 96 96 0
Pan 72 72 0
Total (g) 1200 1189.25
Total (cm^3) 463.32 463.32
Percent Aggregate (%) 100 73 27
Due to RCA’s lower density, the mass of RCA to be used in each sieve size is recalculated by
the following formula. Values of 2.59 and 2.43 were adopted from Cheong’s (2007) past results
in determining bulk specific gravity of Indonesian Granite and RCA respectively.
Weight of RCA to substitute = Weight of Granite Aggregate / Granite S.G. * RCA S.G
Whereby,
Specific Gravity of Indonesian Granite = 2.59
Specific Gravity of RCA = 2.43
4.2 Marshall Test Results
All specimens met the requirements for stability. All except Specimen 7 met LTA’s requirements
for flow, but only specimens 7, 8 and 9 met the requirements for VTM. None of the specimens
had met the requirements for VFB. The Mass-Volume Relationship calculation results are
included in Appendix B. The numeric results are summarised in Table 4.5.
Table 4.5 Summary of Marshall Specimen Test Results
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Specimen No.
% Binder Flow(mm)
Corrected Stability (kN)
Density (g/cm3)
VTM% VMA% VFB%
1 4.75 3.43 13.375 2.26 5.90 14.94 60.51
2 4.75 2.957 17.124 2.28 5.11 14.23 64.09
3 4.75 3.378 16.656 2.27 5.57 14.65 61.95
4 5.00 3.075 15.138 2.25 5.75 15.33 62.49
5 5.00 2.861 14.128 2.26 5.67 15.26 62.83
6 5.00 2.853 13.993 2.27 5.11 14.75 65.39
7 5.25 4.495 17.366 2.28 4.28 14.54 70.57
8 5.25 3.186 16.164 2.28 4.56 14.79 69.16
9 5.25 3.866 16.932 2.30 3.71 14.03 73.59
The following trends were seen within this range of binder content. As binder content increases
from 4.75%, Density, Flow, Stability and VFB decreases. The minimum value is reached at
4.9%. Towards the bitumen content of 5.25%, Density, Flow, Stability and VFB increase. VTM
peaks at 4.9% and decreases as bitumen content increases. VMA increases until it reaches a
peak at 5%, then decreases as bitumen content increases.
The author has decided to adopt the optimum binder content 5.3% for the slab mix. This was
chosen to have values which are closest to the range of values required of the Marshall Design
Criteria.
According to the graph of VFB (%) vs Binder (%) in Figure 4.2, it is predicted that the VFB of
the mix will increase to a value higher than 75%. The hybrid specimen will have increased
stability. Flow will have a small increment and VTM will have a small decrement but not go out
of the bands, and this will meet the Marshall Design Criteria. Plot of these values are shown in
Figure 4.2.
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Figure 4.2 Density, Flow, Stability (%), VTM (%), VFB (%), VMA (%) vs Binder (%)
Area of values which satisfies Marshall Design Criteria
20
VTM (%) vs Binder Content (%)
3.0
3.5
4.0
4.5
5.0
5.5
6.0
4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50
Binder Content (%)
VT
M (
%)
VMA (%) vs Binder Content (%)
13.5
14.0
14.5
15.0
15.5
4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50
Binder Content (%)
VM
A (
%)
VFB (%) vs Binder Content (%)
55
60
65
70
75
80
85
4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50
Binder Content (%)
VF
B (
%)
Stabili ty vs Binder Content (%)
5
7
9
11
13
15
17
19
4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50
Binder Content (%)
Sta
bil
ity
(k
N)
Flow vs Binder Content (%)
2
3
4
5
6
4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50
Binder Content (%)
Flo
w (
mm
)
Density vs Binder Content (%)
2.25
2.26
2.27
2.28
2.29
2.30
4.50 4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50
Binder Content (%)
De
nsit
y (g
/cm
^3)
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Chapter 5
SLAB FABRICATION
5.1 Introduction
This chapter covers the fabrication of two slabs with the hybrid mix followed by the coring of
specimens.
5.2 Specimen Fabrication
The author included the production of a first ‘dummy’ slab, with two objectives. This slab had
aggregate samples with roughly the same weight and gradation as the two test slabs. Firstly, the
mixture will coat the chamber with binder, effectively conditioning it for the next two slabs.
With this “buttering” process the chamber of the mixer will be fully coated with binder and
additional compensatory binder will not be required.
Thein Moe (2003) previously used 5% more bitumen to allow for the loss in binder that is left
coated in the mixing chamber walls when the mixture is discharged. Second, the author was
able to use this first slab to familiarise with the usage of the equipment (Wheel Roller
Compactor, machine cutter and coring machine as shown in Figure 5.1). The gradation and
amounts of aggregate for the slabs are shown in Table 5.1.
Figure 5.1 Wheel Roller Compactor (left), Machine Cutter (middle) and Coring Machine (right)
Table 5.1 Gradation of W3B-RCA27 Slab Mix
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Sieve Size (mm) Weight (g)
W3B-RCA27 mix
Granite RCA
19 - 13.2 2372.09 2326.3013.2 - 6.3 6404.65 6355.196.3 - 3.35 4269.76 3940.053.35 - 1.18 9013.95 -1.18 - 0.3 5693.02 -0.3 - 0.075 3795.35 -
Pan (<0.075) 2846.51 -
Total (g) 47016.86 Weight of Binder (g) 2631.36
The slabs were cast and left for 48 hours. The slabs were then marked for coring. In AASHTO
Designation PP3-94, it is stated in that no sample should be taken from within 50 mm of the
edge of the slab. Markings were made to maximise usage of the slab after incorporating the
discarded edges of the slab. Figure 5.2 shows the layout of the slab for coring purposes.
Figure 5.2 Layout of Slab
A coring machine with a 100mm bit and a 200mm bit were used to core the respective
specimens, while a machine saw cutter was used to cut out the beams.
A total of four 350x50 beams, five 100mm diameter specimens and two 200mm diameter
460
860
350
350
5050
50
Direction of Roll
Dimension of Specimen:860 x 460 x 50 (mm)
N denotes Slab Number100
SN-1SN-2
SN-3SN-4 SN-5
SN-1SN-2
SN-1 SN-2
SN-4SN-3
200
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specimens were cored from each slab. The specimens were weighed in air and in water to
determine their bulk density and percent compaction relative to the Marshall compaction of
98%. Measurement results are shown in Appendix C.
5.3 Asphalt Content Tester
After creep and rutting tests, some of the specimens were burnt in the Asphalt Content Tester
(also known as Thermolyne oven, as shown in Figure 5.3) as a post test study. It is an oven
equipped with an inbuilt balance which is used to determine binder content. Data such as mass
loss, percentage mass loss, test duration and cycle temperature are dynamically displayed.
Figure 5.3 Asphalt Content Tester
In Sim’s (2003) report, the recorded wet calibration factor used was 0.16%, and Chow (1998)
had used 0.20%. As past results showed that the average binder content using a wet calibration
method was practically the same as the actual binder content, the calibration factor of 0.16%
was adopted. The samples were preheated for an hour at 120 oC in a separate oven and broken
up before spreading them on the heating tray to increase the surface area. This enhances the
efficiency of the burning process. After the burning process, specimens were left to cool down
to room temperature.
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There were variations in the apparent bitumen content of the specimens. This is due to the non-
homogenous nature of the mixture, and the aggregate to bitumen ratio may be higher in some
samples. This increase in bitumen content is much more obvious with specimens that have
aggregates chipped off, with the encasing bitumen remaining on the specimen. The author
suggests that the surface of the specimens should be reasonably smooth before they are burnt.
This will minimise the error caused by an increase in the ratio bitumen to aggregate due to the
aggregates chipping off.
From the results that are included in Appendix D, the average recovered bitumen content for the
cored specimens was 5.05% and 5.38% for the beam specimens. The apparent bitumen content
of cored specimens burnt at 650 oC was higher than the results from specimens burnt at 450 oC
by 0.57%. This can be due to minerals being burnt off from the aggregates at 650 oC. It is also
coherent with the requirement of a calibration factor for temperature to reduce the apparent
bitumen content of the specimen.
A visual inspection showed that there was a thin black film of carbon covering the surface of the
specimens burnt at 450 oC. This black film is easily removed as it disintegrates into powder
when wiped. Specimens burnt at 650 oC were clean from this black film. The author suggests
that carbon residue can be due to the incomplete burning of bitumen, and further tests can be
made by burning control samples of bitumen and aggregate to work out the calibration factors
due to the temperature.
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Chapter 6
DYNAMIC CREEP TESTS
6.1 Test Objectives
Dynamic creep tests were carried out on 100mm diameter cored samples from the two test slabs
to assess the performance of the hybrid mix. The test objectives, method and results of the creep
test are provided followed by those of the rutting tests.
6.2 Test Procedures
The dynamic creep test was conducted to assess the creep response of the 100 diameter
specimens from each test slab. The IPC Universal Testing Machine as shown in Figure 6.1 was
used to determine the creep response of the specimens as specified in Australian Standard Method of
Sampling and Testing Asphalt (AS2891.12.1–1995).
Figure 6.1 Universal Testing Machine (UTM) Fitted with Dynamic Creep Test Equipment
The test was conducted in a controlled temperature and stress condition based on the Australian
standard method of sampling and testing asphalt (AS 2891.12.1-1995). LTA’s W3B was
designated as a reference mix to provide comparison benchmarks for the experiment. The
measured height values were input into the computer.
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The Australian Standard recommends a set of criteria which was used for the creep test. The
creep test criteria are summarised in Table 6.1.
Table 6.1 Dynamic Creep Test Conditions
Parameters Recommended valuesCompressive stress 200 ± 5kPa
Loading period 0.5 ± 0.05secPulse repetition period 2.0 ± 0.05sec
Test temperature 50 ± 0.5OCPre-conditioning time at 50 ± 0.5OC 2 hours
Test termination At 30 000 microstrain OR 40 000 pulse counts
A visual inspection of the integrity of the specimens was conducted. Specimens which had
pieces chipped off or seen to have clear fractures on the surface of the cored sample were not
used. As a result, 3 out of 5 cored specimens were selected per slab for the experiment.
From Ho’s (2003) study, it was found out that cored W3B samples have very low creep
resistance compared to Marshall Samples of the same gradation and bitumen content. This can
be due to the high disturbance brought about by coring the specimens with a coring machine.
This disturbance causes the creation of cracks and micro-fractures to form within the specimen.
6.3 Test Results
Ho’s results for LTA’s W3B were used as a reference mix to provide comparison benchmarks
with the W3B-RCA27 hybrid mix. The data output is listed in Appendix E. The summarised
results are shown in Table 6.2.
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Table 6.2 Dynamic Creep Test Results from This Study and Ho (2003)
Tester Mix Specimen Accum. Strain (microstrain,
fn)
Creep Stiffness (MPa)
Pulse Count @ 10000 fn
Pulse Count @ 30000 fn
This Study(Lee, 2009)
W3B RCA27
S1-1 30255 5.6 53 368S1-2 30275 5.5 37 274S1-5 30235 5.3 55 381S2-2 30122 5.5 51 530S2-3 30107 5.6 31 433S2-4 30077 5.5 44 541
Ho, 2003
W3B-PEN 60/70
S4-1 67628 2.58 29 198S4-2 76436 1.44 30 261S5-1 85646 2.19 40 193S5-2 78746 2.36 30 178S6-1 73579 2.54 35 379S6-2 67407 2.76 29 354
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CHAPTER 7
RUTTING TEST
7.1 Introduction
The rutting test was conducted on four cored 200mm diameter specimens to evaluate the rut
response of the W3B hybrid mix. All four 200mm specimens are in good quality and are thus
used for the Rutting tests. The experiment was conducted on a wheel tracking machine (see
Figure 7.1) based on the procedure described in BS598: Part 110: 1996 as well as improvements
made by past studies.
Figure 7.1 Wheel Tracking Machine
7.2 Track Rate and Relative Rut Depth
Track rate represents the rate at which the rut depth increases with time under repeated passes of
a loaded wheel (in mm/h). For each tested specimen, the track rate should be calculated using
the following formula:
15
900
TTR = (7.1)
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where,
TR = Track Rate (mm/h)
T15 = Time, in minute, for rut depth to reach 15 mm
When rut depth of 15 mm is not reached by 45 minutes, an alternative formula is used to relate
the track rate of the specimen to time:
60×=t
R T
RRDT (7.2)
where,
RRD = Relative Rut Depth (mm)
T1 = Test time (minute)
7.3 Test Procedure
A wooden block encases the specimen which is padded up with hard acrylic panels, as shown in
Figure 7.1. The temperature of the specimen is monitored via a sensor coated with heat transfer
silicon inserted into a 15mm hole bored into the specimen.
A thin layer of granite fines is spread on the length of rutting area to prevent bitumen from
damaging the wheel and affecting the experiment. Through a firm schedule shown in Appendix
F it was possible to complete testing four specimens in one day.
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7.4 Test Results
Figure 7.2 Cored Specimens S1-1 and S2-2 After Rutting Test
The tested specimens are shown in Figure 7.2. The summary of the results by the author as well
as those of previous rutting tests performed by Ang (2008), Ho (2003) and Ie (2000) are shown
in Table 7.1. The data output is shown in Appendix G.
Table 7.1 Rutting Test Results
Tester Slab Specimen Relative Rut Depth (mm)
Track Rate (mm/h)
Bulk density (kg/
m3)Lee, 2009 W3B RCA27 S1-1 2.60 3.47 2276.5
W3B RCA27 S1-2 1.92 2.56 2284.8
W3B RCA27 S2-1 2.71 3.61 2270.0
W3B RCA27 S2-2 2.71 3.61 2271.8
Average 2.49 3.31 2275.8Ang, 2008 W3B RCA37
(Average)2.47 3.29 2198.0
W3B RCA24 (Average)
1.38 1.84 2190.0
Ho, 2003 PEN 60/70 6.91 9.21 - PEN 60/70 6.01 8.01 - PEN 60/70 8.15 10.87 -
Ie, 2000 W3B (Average) 4.00 5.33 2285.0
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Chapter 8
CONCLUSIONS AND RECOMMENDATIONS
8.1 Review of Results
The objective of this study is to evaluate the performance of a hybrid mix of the Land Transport
Authority (LTA)’s W3B with partial substitution of Recycled Concrete Aggregate (RCA)
through creep performance and rutting tests.
The optimum binder content of the hybrid mix W3B-RCA27 was determined according to
LTA’s Marshall Design Criteria for W3B’s wearing course. A value of 5.3% binder content was
used for the hybrid mixes, and Ho’s (2003) W3B slab specimens were used as benchmark for
comparison in this research. Two slabs of this mix were fabricated. Samples were cored from
the slabs for performance testing. The individual performance values obtained would
correspond to the values to the fabricated slab on a whole.
The asphalt content tester results suggest that the bitumen content was higher than 5.3%. This
can be due to the burning off of minerals and fines in RCA. Further tests can be made to
determine the actual amount of RCA material burnt off in order to better assess the actual
bitumen content.
The results from the creep tests, on average, have higher creep stiffness but lower accumulated
strain than those obtained by Ho (2003). As the hybrid mix has higher pulse counts to failure
but a lower accumulated strain, the author suggests that the hybrid mix is not as stiff as Ho’s
(2003) W3B mix, but is more ductile and able to take more repetitions of pulse counts before
failure. The higher creep stiffness can be appropriated to the high density of the hybrid mix as
compared to Ho’s (2003). The hybrid mix is considerably weaker than Ho’s W3B-PEN 60/70
mix, and fails at a lower accumulated strain.
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The rutting tests showed that the hybrid mix has a lower track rate, exhibiting higher rutting
resistance compared to the results by Ho (2003) which consisted of pure granite aggregate. The
specimen (S1-2) with the highest bulk density gave the lowest track rate. This can be due to the
specimen being heavily compacted during the fabrication, which keeps the aggregate highly
interlocked and thus resistant to rutting. The graphs in Appendix G show that the rutting rate
decreases with time and forms a gentle slope near the end of the 45 minutes of testing. This
could be due to the initial shifting of the aggregate in the rutting specimen, causing the angular
aggregates to interlock even further near the end to form a stiffer structure.
8.2 Recommendations
The author would like to offer the following recommendations to reinforce the findings attained
in this research and to further verify the feasibility of RCA application in HMA.
The current rutting results suggest that the hybrid specimen has a better rutting performance
compared to conventional W3B, but shows a lower accumulated strain capability. Research can
be done to understand the durability of the wearing course in Singapore and whether the
pavements are first worn out by creep or rutting. There will be value-add in terms of designing a
hybrid that would make up for the weaker parameter and thus increases the longevity of the
wearing course of pavements.
The bulk density of the slab specimens implies that they have been over compacted. Better
knowledge of the newly acquired plate compactor will help to fabricate slabs with it and to
assess the differences in the Plate Compactor and Wheel Roller Compactor. Further research can
be done to increase the quality of the fabrication of large slabs in future studies.
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References
Ang, C. H. (2008). Performance Characteristics of Hot-Mix Asphaltic Concrete with Recycled
PCC Aggregate, Bachelor of Engineering Final Year Project Report, School of Civil and
Environmental Engineering, Nanyang Technological University, Singapore [Unpublished]
Cheong, C. M. (2007). Performance Evaluation of Recycled Concrete Aggregate in Hot-Mix
Asphalt, Bachelor of Engineering Final Year Project Report, School of Civil and Environmental
Engineering, Nanyang Technological University, Singapore [Unpublished]
Chow, C. G. (1998). Evaluation of the Asphalt Content Tester, Bachelor of Engineering Final
Year Project Report, School of Civil and Structural Engineering, Nanyang Technological
University, Singapore [Unpublished]
FHWA (2003). Summary of California Recycled Concrete Aggregate Review, Recycling,
Pavements, U.S. Department of Transportation, Federal Highway Administration (in
http://www.fhwa.dot.gov/pavement/recycling/rcaca.cfm; retrieved August 2008).
FHWA (2006). Reclaimed Concrete Material, US Department Of Transportation, Federal
Highway Administration (http://www.tfhrc.gov/hnr20/recycle/waste/index.htm; retrieved
August 2008).
Focus (April 2004). Recycled Concrete Study Identifies Current Uses, Best Practices, (in http://
www.tfhrc.gov/FOCUS/apr04/01.htm; retrieved August 2008).
Hidehito Ie (2000). Rutting Characteristics of Asphalt Concrete Mix, Bachelor of Engineering
Final Year Project, School of Civil and Structural Engineering, Nanyang Technological
University, Singapore [Unpublished]
Ho, S. S. (2003). Fatigue Characteristics of Hot-Mix Asphalt Concrete, Bachelor of Engineering
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Final Year Project, School of Civil and Environmental Engineering, Nanyang Technological
University, Singapore [Unpublished]
LTA (2009) Code of Practice for Works on Public Streets, March 2009 Edition Revision R1 (in
http://www.lta.gov.sg/dbc/doc/guideline/COP%20for%20Works%20on%20Public
%20Streets_Mar09Edrev1.pdf; retrieved March 2009)
NEA (2002). Waste Minimisation Section - Formation of Waste Minimisation Section (in http://
app.nea.gov.sg/cms/htdocs/article.asp?pid=1460 ; retrieved September 15, 2008).
NEA (2006). Semakau Landfill & Tuas Marine Transfer Station, (in
http://www.nea.gov.sg/cms/esd/brochure/TMTS.pdf ; retrieved September 15, 2008).
NEA (2008). Waste Statistics and Recycling Rate for 2007 (in http://app.nea.gov.sg/cms/htdocs/
article.asp?pid=2706; retrieved August 2008).
Phoon, Y. L. (1998). Resilient Modulus Characteristics of Stone Mastic Asphalt, Bachelor of
Engineering Final Year Project, School of Civil and Structural Engineering, Nanyang
Technological University, Singapore [Unpublished]
Sim, Y. M. (2003). Fatigue Characteristics of Hot-Mix Asphalt Concrete, Bachelor of
Engineering Final Year Project, School of Civil and Environmental Engineering, Nanyang
Technological University, Singapore [Unpublished]
Thein Moe (2005). Rutting Characteristics of Asphalt Concrete Mix, Master of Science
(Transportation Engineering) Dissertation, School of Civil and Environmental Engineering,
Nanyang Technological University, Singapore [Unpublished]
34
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APPENDIX A:
Results for Change in Gradation of Recovered W3B-RCA Specimens
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Tables of Recovered W3B Gradation
By Mass* (g)
Sieve Size (mm) W3B(g) W3B-1(g) W3B-2(g)
19 0 0 013.2 120 113.8 102.96.3 324 289.6 295.33.35 216 195.5 184.91.18 228 207.7 224.70.3 144 58.2 57.6
0.075 96 157.7 142.4
0 72 50.9 57.7
Total Weight 1200 1073.4 1065.5Total Coarse 660 598.9 583.1
19 - 13.2 Lost (%) - 5.17 14.2513.2 - 6.3 Lost (%) - 10.62 8.866.3 - 3.35 Lost (%) - 9.49 14.403.35 - 1.18 Lost (%) - 8.90 1.451.18 - 0.3 Lost (%) - 59.58 60.000.3 - 0.075 Lost (%) - -64.27 -48.33
Pan Lost (%) - 29.31 19.86Total Coarse Lost (%) - 9.26 11.65
Total Fines (g) 540 474.5 482.4Total Fines Lost (g) - 65.5 57.6
Total Fines Lost (%) - 12.13 10.67*negative values in Lost (%) mean there is a gain in mass
Volume Passing (%)
Sieve Size (mm) W3B(cm^3) W3B-1-2(cm^3) W3B-2-2(cm^3)
19 100.00 100.00 100.0013.2 90.00 89.40 90.346.3 63.00 62.42 62.63
3.35 45.00 44.21 45.271.18 26.00 24.86 24.190.3 14.00 19.43 18.78
0.075 6.00 4.74 5.42
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Recovered W3B Gradations In Comparison with Specifications
0
10
20
30
40
50
60
70
80
90
100
0.01 0.1 1 10 100Aggregate Size (mm)
Vol
ume
Pas
sing
(%)
Upper Limit
Lower Limit
W3B-1(cm^3)
W3B-2(cm^3)
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Tables of Recovered W3B-RCA53 Gradation
By Mass* (g)
Sieve Size (mm) W3B-RCA53 (g) W3B-RCA53-1 (g) W3B-RCA53-2 (g)19 0 0 0
13.2 112.59 96.50 147.10 6.3 303.98 266.90 218.20
3.35 202.66 156.00 157.00 1.18 228 225.80 241.20 0.3 144 66.30 59.40
0.075 96 140.30 224.60 0 72 58.80 19.40
Total Weight 1159.23 1010.60 1066.90 Total Coarse 619.23 519.40 522.30
19 - 13.2 Lost (%) - 14.29 -30.65 13.2 - 6.3 Lost (%) - 12.20 28.22 6.3 - 3.35 Lost (%) - 23.02 22.53
3.35 - 1.18 Lost (%) - 0.96 -5.79 1.18 - 0.3 Lost (%) - 53.96 58.75
0.3 - 0.075 Lost (%) - -46.15 -133.96 Pan Lost (%) - 18.33 73.06
Coarse Lost (%) - 16.12 15.65 Total Fines 540 491.20 544.60
Total Fines Lost (g) - 48.80 -4.60 Total Fines Lost (%) - 9.04 -0.85
*negative values in Lost (%) mean there is a gain in mass
Volume Passing (%)
Sieve Size (mm)
W3B-RCA53 (cm^3) W3B-RCA53-1 (cm^3) W3B-RCA53-2 (cm^3)
19 100.00 100.00 100.00 13.2 90.00 90.36 86.08 6.3 63.00 63.70 65.42
3.35 45.00 48.12 50.56 1.18 26.00 26.00 28.17 0.3 14.00 19.50 22.65
0.075 6.00 5.76 1.80
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Recovered W3BRCA53 Gradations In Comparison with Specifications
0
10
20
30
40
50
60
70
80
90
100
0.01 0.1 1 10 100Aggregate Size
Vol
ume
Pas
sing
(%)
Upper Limit
Lower Limit
W3B-RCA53-1(cm^3)
W3B-RCA53-2(cm^3)
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APPENDIX B:
Marshall Specimen Mass-Volume Relationship Table
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
Spe
cim
en N
o.1
23
45
67
89
Mas
s of
Spe
cim
en in
Air
, g12
45.1
1239
.812
39.2
1232
.012
38.7
1242
.012
39.5
1246
.112
47.5
Mas
s of
Spe
cim
en in
Wat
er, g
694.
069
5.6
692.
668
5.6
689.
869
4.9
696.
369
8.4
704.
1
Vol
ume,
cm
355
1.1
544.
254
6.6
546.
454
8.9
547.
154
3.2
547.
754
3.4
Ave
rage
Thi
ckne
ss, m
m70
.49
68.4
669
.13
68.2
469
.25
68.6
367
.57
68.7
868
.16
Bin
der
abso
rpti
on, %
0.7
0.7
0.7
0.7
0.7
0.7
0.7
0.7
0.7
Bin
der
cont
ent,
%4.
754.
754.
755.
005.
005.
005.
255.
255.
25
Den
sity
of
bind
er, g
/cm
31.
021.
021.
021.
021.
021.
021.
021.
021.
02
Mas
s of
bin
der,
g59
.158
.958
.961
.661
.962
.165
.165
.465
.5M
ass
of a
ggre
gate
, g11
86.0
1180
.911
80.3
1170
.411
76.8
1179
.911
74.4
1180
.711
82M
ass
of a
bsor
bed
bind
er, g
8.3
8.3
8.3
8.2
8.2
8.3
8.2
8.3
8.3
Mas
s of
eff
ecti
ve b
inde
r, g
50.8
50.6
50.6
53.4
53.7
53.8
56.8
57.1
57.2
Vol
ume
of b
inde
r, cm
358
.057
.757
.760
.460
.760
.963
.864
.164
.2
Vol
ume
of a
bsor
bed
bind
er, c
m3
8.1
8.1
8.1
8.0
8.1
8.1
8.1
8.1
8.1
Vol
ume
of e
ffec
tive
bin
der,
cm3
49.8
49.6
49.6
52.4
52.6
52.8
55.7
56.0
56.1
Bul
k de
nsit
y of
agg
rega
te, g
/cm
32.
532.
532.
532.
532.
532.
532.
532.
532.
53M
ass
of a
ggre
gate
, g11
86.0
1180
.911
80.3
1170
.411
76.8
1179
.911
74.4
1180
.711
82B
ulk
volu
me
of a
ggre
gate
, g/
cm3
468.
846
6.8
466.
546
2.6
465.
146
6.4
464.
246
6.7
467.
2E
ffec
tive
vol
. of
aggr
egat
e, g
/cm
346
0.6
458.
645
8.4
454.
645
745
8.2
456.
145
8.6
459.
1
Vol
ume
of a
ir, c
m3
32.5
27.8
30.5
31.4
31.1
27.9
23.2
25.0
20.1
Bul
k de
nsit
y, g
/cm
32.
262.
282.
272.
252.
262.
272.
282.
282.
30
Max
imum
theo
reti
cal d
ensi
ty, g
/cm
32.
402.
402.
402.
392.
392.
392.
382.
382.
38
Voi
ds in
tota
l mix
, VT
M, %
5.90
5.11
5.57
5.75
5.67
5.11
4.28
4.56
3.71
Voi
ds in
min
eral
agg
rega
te, V
MA
, %14
.914
.214
.615
.315
.314
.814
.514
.814
.0
Voi
ds f
ille
d w
ith
bind
er, V
FB
, %60
.564
.161
.962
.562
.865
.470
.669
.273
.6
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APPENDIX C:
Measurements of Cored Specimens
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100m
m D
iam
eter
Cor
ed S
ampl
e
Sla
b N
umbe
rN
o.W
eigh
t in
Air
(kg
)W
eigh
t in
Wat
er (
kg)
Vol
ume
Bul
k de
nsit
y (k
g/m
3 )
Per
cent
age
com
pact
ion
(%)
1st
read
ing
(mm
)
2nd
read
ing
(mm
)
3rd
read
ing
(mm
)
Ave
rage
th
ickn
ess
(mm
)(m
3 ) X
10-3
S1
10.
946
0.52
8 0.
417
2266
.298
.11
55.5
5 55
.71
56.1
9 55
.82
20.
922
0.51
9 0.
403
2285
.698
.94
54.4
5 54
.34
54.7
2 54
.50
30.
895
0.51
1 0.
384
2328
.310
0.79
53.6
6 53
.00
53.2
4 53
.30
40.
886
0.50
4 0.
381
2323
.510
0.59
53.7
6 53
.05
52.5
8 53
.13
50.
905
0.51
6 0.
389
2328
.110
0.78
53.1
2 53
.58
52.9
3 53
.21
S2
10.
857
0.48
6 0.
370
2313
.910
0.17
50.5
7 50
.23
50.2
5 50
.35
20.
867
0.48
7 0.
380
2282
.698
.81
51.7
2 51
.73
52.4
5 51
.97
30.
866
0.49
2 0.
374
2314
.110
0.18
50.5
3 49
.89
50.7
7 50
.40
40.
842
0.47
7 0.
365
2306
.899
.86
49.4
1 49
.65
50.0
3 49
.70
50.
868
0.49
1 0.
377
2301
.099
.61
52.6
7 51
.31
52.6
0 52
.19
200m
m D
iam
eter
Cor
ed S
ampl
e
Sla
b N
umbe
rN
o.W
eigh
t in
Air
(kg
)W
eigh
t in
Wat
er (
kg)
Vol
ume
Bul
k de
nsit
y (k
g/m
3 )
Per
cent
age
com
pact
ion
(%)
1st
read
ing
(mm
)
2nd
read
ing
(mm
)
3rd
read
ing
(mm
)
Ave
rage
th
ickn
ess
(mm
)(m
3 ) X
10-3
S1
14.
305
2.41
4 1.
891
2276
.598
.55
63.3
0 61
.95
62.1
2 62
.46
24.
096
2.30
3 1.
793
2284
.898
.91
61.7
6 60
.30
56.9
0 59
.65
S2
13.
463
1.93
7 1.
525
2270
.098
.27
49.8
8 50
.73
50.3
5 50
.32
23.
799
2.12
7 1.
672
2271
.898
.35
55.4
4 56
.10
54.6
6 55
.40
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APPENDIX D:
Results from Asphalt Content Tester
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Res
ults
fro
m A
spha
lt C
onte
nt T
este
r
Cor
e S
ampl
e N
o.D
urat
ion
(min
)S
ampl
e W
eigh
t (g)
Wei
ght
Los
s (g
)P
erce
nt L
oss
(%)
Bin
der
Con
tent
(%
)Te
mpe
ratu
re
(o C)
Cal
ibra
tion
Fac
tor
for
Tem
pera
ture
Est
imat
ed
Bin
der
Con
tent
(%
)S
1 C
OR
E 1
8291
551
.15.
58
5.26
450
0.33
5.1
S2
ED
GE
9319
7110
5.1
5.33
5.
1845
00.
155.
02S
1 C
OR
E 2
3193
157
.26.
14
5.82
650
0.32
5.66
S2
CO
RE
235
863
52.7
6.11
5.
7665
00.
355.
6A
vera
ge B
inde
r C
onte
nt =
(5.
26%
+ 5
.18%
+ 5
.82%
+ 5
.76%
) / 4
= 5
.505
%
Bea
m N
o.D
urat
ion
(min
)S
ampl
e W
eigh
t (g)
Wei
ght
Los
s (g
)P
erce
nt L
oss
(%)
Bin
der
Con
tent
(%
)Te
mpe
ratu
re
(o C)
Cal
ibra
tion
Fac
tor
for
Tem
pera
ture
Est
imat
ed
Bin
der
Con
tent
(%
)S
1-1
105
2577
137.
05.
32
5.20
450
0.12
5.04
S1-
312
629
3316
2.4
5.56
-*
450
-*-*
S1-
488
2375
133.
05.
60
5.47
450
0.13
5.31
S2-
188
2457
129.
05.
25
5.13
450
0.12
4.97
S2-
211
025
1713
9.4
5.54
5.
4545
00.
095.
29S
2-3
-*27
1915
6.6
5.76
5.
6545
00.
115.
49S
2-4
117
2638
144.
45.
47
5.39
450
0.09
5.23
*Val
ues
not o
btai
ned
due
to b
reak
dow
n in
asp
halt
con
tent
test
erA
vera
ge B
inde
r C
onte
nt =
5.3
8%
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APPENDIX E:
Data Output from Dynamic Creep Test
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ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
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ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
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APPENDIX F:
Time Schedule for Rutting Test
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56
78
910
11
12
13
14
15
16
17
18
Hours
Heatin
g u
p O
ven
with
Sam
ple
(15m
ins)
Heatin
g u
p o
f S
am
ple
in
Ove
n
Tra
nsfe
r S
am
ple
to M
/C,
Heat
for
1h
r
Ru
n T
est
Com
ple
te T
est
Heatin
g u
p o
f S
am
ple
in
Ove
n
Tra
nsfe
r S
am
ple
to M
/C,
Heat
for
1h
r
Ru
n T
est
Com
ple
te T
est
Heatin
g u
p o
f S
am
ple
in
Ove
n
Tra
nsfe
r S
am
ple
to M
/C,
Heat
for
1h
r
Ru
n T
est
Com
ple
te T
est
Heatin
g u
p o
f S
am
ple
in
Ove
n
Tra
nsfe
r S
am
ple
to M
/C,
Heat
for
1h
r
Ru
n T
est
Com
ple
te T
est
Sample 1 Sample 2 Sample 3 Sample 4P
roje
ct T
ime
Lin
e
Not
es:
T
ime
line
ass
umes
a s
tart
ing
time
of m
anua
l wor
k at
9.0
0am
,
Ove
ns a
re ti
med
to s
tart
at 7
.45a
m a
nd 8
.00a
m
Tim
e to
hea
t up
sam
ple
in o
ven
is 3
hrs,
tim
e fo
r ac
tual
test
is 4
5min
utes
A
n ex
tra
15m
inut
es is
take
n in
to c
onsi
dera
tion
E
stim
ated
tim
e of
com
plet
ion
is 5
.00p
m
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APPENDIX G:
Data Output from Rutting Test
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Tim
eR
utti
ng D
epth
(m
m)
Tim
eR
utti
ng D
epth
(m
m)
00.
00
232.
31
10.
89
242.
35
21.
31
252.
41
31.
51
262.
41
41.
60
272.
41
51.
75
282.
41
61.
81
292.
41
71.
91
302.
41
82.
00
312.
44
92.
01
322.
51
102.
01
332.
51
112.
07
342.
51
122.
10
352.
51
132.
10
362.
51
142.
11
372.
51
152.
21
382.
51
162.
21
392.
51
172.
21
402.
51
182.
22
412.
51
192.
31
422.
60
202.
31
432.
60
212.
31
442.
60
222.
31
452.
60
Sla
b S
am
ple
S1
-1
0
0.51
1.52
2.53
05
101
52
025
30
35
40
45
Tim
e (
min
)Rutting Depth (mm)
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Tim
eR
utti
ng D
epth
(m
m)
Tim
eR
utti
ng D
epth
(m
m)
00.
0023
1.51
10.
1824
1.61
20.
4125
1.61
30.
6126
1.61
40.
7227
1.64
50.
8328
1.71
60.
9029
1.71
71.
0130
1.71
81.
0131
1.71
91.
1132
1.73
101.
1233
1.81
111.
2134
1.81
121.
2535
1.81
131.
3136
1.81
141.
3137
1.81
151.
3138
1.81
161.
3539
1.83
171.
4040
1.90
181.
4041
1.90
191.
4142
1.90
201.
4743
1.90
211.
5144
1.90
221.
5145
1.92
Sla
b S
am
ple
S1
-2
0
0.51
1.52
2.53
05
10
15
20
25
30
35
40
45
Tim
e (
min
)
Rutting Depth (mm)
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Tim
eR
utti
ng D
epth
(m
m)
Tim
eR
utti
ng D
epth
(m
m)
00.
0023
2.30
10.
7924
2.31
21.
0125
2.41
31.
3726
2.41
41.
5127
2.41
51.
6128
2.41
61.
7129
2.41
71.
7430
2.46
81.
8931
2.51
91.
9132
2.51
101.
9633
2.51
112.
0134
2.51
122.
0135
2.53
132.
1136
2.61
142.
1137
2.61
152.
1138
2.61
162.
1339
2.61
172.
2140
2.61
182.
2141
2.62
192.
2142
2.71
202.
2743
2.71
212.
3044
2.71
222.
3045
2.71
Sla
b S
am
ple
S2
-1
0
0.51
1.52
2.53
05
10
15
20
25
30
35
40
45
Tim
e (
min
)
Rutting Depth (mm)
ATTENTION: The Singapore Copyright Act applies to the use of this document. Nanyang Technological University Library
Sla
b S
am
ple
S2
-2
0
0.51
1.52
2.53
05
10
15
20
25
30
35
40
45
Tim
e (
min
)
Rutting Depth (mm)
Tim
eR
utti
ng D
epth
(m
m)
Tim
eR
utti
ng D
epth
(m
m)
00.
00
232.
31
10.
76
242.
36
21.
13
252.
41
31.
33
262.
41
41.
52
272.
41
51.
60
282.
41
61.
71
292.
43
71.
81
302.
51
81.
83
312.
51
91.
91
322.
51
101.
93
332.
51
112.
01
342.
51
122.
01
352.
51
132.
10
362.
60
142.
10
372.
60
152.
10
382.
60
162.
21
392.
60
172.
21
402.
60
182.
21
412.
61
192.
21
422.
61
202.
31
432.
61
212.
31
442.
63
222.
31
452.
71
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