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Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1 , L. Abbene 1,2 , N. Auricchio 1 ,E. Caroli 1 , M. Quadrini 1 , J.B. Stephen 1 , A. Zappettini 3 , R.M. Curado Da Silva 4 , O. Limousin 5 , A. Meuris 5 and P. Ubertini 1 1 IASF-INAF, Italy 2 DiFTeR Università di Palermo, Palermo, Italy 3 IMEM-CNR, Parma, Italy 4 Departmento de Física, Universidade de Coimbra, Coimbra, Portugal The Extreme Sky " Sampling the Universe above 10 keV" 13 - 17 October 2009 Otranto
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Page 1: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for

Astrophysical Applications

S. Del Sordo1, L. Abbene1,2, N. Auricchio 1 ,E. Caroli1, M. Quadrini1, J.B. Stephen1 , A. Zappettini3, R.M. Curado Da Silva4,

O. Limousin5, A. Meuris5 and P. Ubertini1

1IASF-INAF, Italy2DiFTeR Università di Palermo, Palermo, Italy

3IMEM-CNR, Parma, Italy4Departmento de Física, Universidade de Coimbra, Coimbra, Portugal

5CEA – DSM - Irfu - Service d’Astrophysique, Saclay, France

The Extreme Sky

" Sampling the Universe above 10 keV"

  13 - 17 October 2009 Otranto

Page 2: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Outline

Scenario (projects and collaborations)

CdTe / CdZnTe X-ray and gamma ray detectors

Detector prototypes

Work in progress and future developments

Conclusions

Page 3: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Projects and Collaborations

Progetto ASI Alte Energie (Study for the Gamma Ray Imager mission)

Progetto PRIN INAF SGRIP (funded by INAF)Development of an high efficiency wide band 3D CZT detector prototype for Laue telescope focal plane

Progetto PRIN (funded by MIUR)Growth technologies and spectroscopic optimization for X and Gamma ray detectors based on CdTe/CdZnTe.

IASF-INAF (Milano Bologna Roma Palermo) IMEM-CNR di Parma (crystal growth) Università di Lecce (crystal growth and bonding) IMM-CNR di Lecce (bonding and electrical characterization) DIFTER Università di Palermo (medical applications)

The Italian collaboration

• ESRF Grenoble

• Leicester University

• DTU Space Copenaghen

• Coimbra University

• CEA Saclay Paris

• ICE-CSIC Barcelona

International collaborations

Page 4: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

CdTe and CdZnTe I

High Z semiconductors

(Zmax = 52)

Wide band gap semiconductors

Del Sordo S. et al., Sensors, Vol. 9, 3491-3526, 2009.

Page 5: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

CdTe and CdZnTe II

Critical Issues

Poor transport properties of the charge carriers:

hh ~ 10-5-10-6 cm2/ V

ee ~ 10-2-10-3 cm2/V)

Small electrical signals at the electrodes

Small crystal size: typically < 2 cm3

Development of single charge carrier sensing detectors (pixel, strip, Frisch grid, multiple electrodes) to overcome the poor transport properties of the holes is mandatory.

L. Abbene et al., NIM A 583 (2007) 324-331.

1 mm 1 mm

Page 6: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

CdTe and CdZnTe III

Suppliers of Spectrometer grade crystals

Italian group at IMEM-CNR (A. Zappettini): CdZnTe crystals grown by the boron oxide encapsulated vertical Bridgman technique

A. Zappettini et al., IEEE Nucl. Sci. Symp. Conf. Rec. 2008, 118-121.

2-inch CdZnTe crystal

1.1 mm

Page 7: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

CdZnTe detector prototypes

DETECTORS CHARACTERISTICS

Pixel detectors CZT (eV Products)

Geometric surface 10×10 mm2

Active area 8×8 mm2

Thickness 1 mm and 2 mm

Number of pixels 256

Pitch 0.5 mm

(0.45 mm anodes, 0.05 mm gap)

focal plane detector prototypes for Hard X-ray multilayer telescopes (10-

100 keV)

CZT pixel detectors

Page 8: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Energy (keV)

Energy resolution (%)

Peak to valley ratio (2 x FWHM)

59.5 5.80 ± 0.16 28.1 ± 1.1

88,1 3.9 ± 0.2 19.5 ± 1.1

CZT pixel detectors performance

L. Abbene et al., JAP, Vol. 105, 2009.

CdZnTe detector prototypes

Page 9: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

thickness 1 mm 2 mm

energy resolution (%) (59.5 keV)

5.80 ± 0.16 5.50 ± 0.10

energy resolution (%) (88.1 keV)

3.9 ± 0.2 3.50 ± 0.13

deviation of the FW.1M/FWHM ratio from the Gaussian

ratio (1.82) (59.5 keV)

8 % 5 %

deviation of the FW.1M/FWHM ratio from the Gaussian

ratio (1.82) (88.1 keV)

16 % 10 %

“Small pixel effect”

H. Barrett, J. Eskin, H. Barber, Phys. Rev. Lett. 75 (1995) 156

CdZnTe detector prototypes

CZT pixel detectors performance

2 mm thick detector vs 1 mm

Page 10: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

CdZnTe detector prototypes

CZT pixel detector for the POLCA II Experiment (POLarimetry with CdZnTe Arrays)

Detector CZT Imarad4x4 cm2, 5 mm thickHV = -600 V16x16 pix with 2.5 mm pitch11x11 + 7 pix used

Readout Electronics

8 eV products ASIC 16 channels/chip33/50/100/200 sel. Gain0.6/1.2/2.4/4 μs shaping time

The POLCA quick look S/W user interface (LABVIEW)

Page 11: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

CdZnTe detector prototypes

Polca experiment: Set-up at ESRF beam line ID15B and Results

P o la r ised B ea m E n erg y ra n g e: 1 0 0 k e V to ~ 1 M e V

C d Te P ix e l M a tr ix

E

E

1 0 m m

2 m m

2 m m

C d Te P ix e l D im en sio n s

yx

yx

NN

NNQ

Counts maps (scattered events)

pixel 186, Energy 200 keV, Angle 0, 45 degree

Page 12: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Basic sensitive CZT unit▶External Dimensions: 10×10×2.5 mm3

Anode side: 8 anodes strips 0.15 mm wide (pitch=2.5 mm)

correcting field strips 0.15 mm wide gap between strips=0.15 mm

Cathode side: 4 cathodes strips 2.4 mm wide gap between strips=0.10 mm

3D detector prototype packaging scheme: The detector assembly is built with 8 identical modules packed together (64 anodes and 32

cathodes).

I/O pads Alumina support

Front end electronics board

data handling and logic board

Small 3D CZT position sensitive spectrometer (SmallGRIPrototype)

Redout Electronics NOVARAD Rena3

CdZnTe detector prototypes

See Poster E. Caroli et al. SGRIP …

Page 13: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Future Developments The POLCaliste experiment

Low noise readout electronics r.m.s. 80 e-

Caliste Module

CdTe Schottky detector

Page 14: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Future Developments The POLCaliste experiment

Polarimetric measurements at ESRF with the PolCaliste prototype are foreseen in 2010. We foresee to use in a first run the 64 ch device and in a next step the new 256 ch device. The device thickness will be 0.5, 1, 2 mm

Energy resolution 1.5 % (FWHM) @ 59.5 keV

T = -15 °C

POLCaliste Experiment (POLarimetry with Caliste)

Caliste module performance

Page 15: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Conclusions (I)

Italian CZT detector development (crystal growth and detectors assembly) activities are in progress with quite good expectations.

Experimental activities devoted to characterize imaging spectrometer operative in the 10 -100 keV energy band are in progress.

The SGRIP experiment (considered as a pathfinder for GRI) is in an advanced realization phase. The study of the prototype performances, foreseen in the 2010, will allow the optimization of the main operative parameters for a detector operative up to 800 keV in stack configuration.

The polarimetric performances of the POLCAII experiment are under evaluation. Measurements with the improved POLCaliste experiment are foreseen in the 2010 at ESRF.

Page 16: Recent Trends in the Development of CdTe and CdZnTe Semiconductor Detectors for Astrophysical Applications S. Del Sordo 1, L. Abbene 1,2, N. Auricchio.

The Extreme Sky, Otranto16th October 2009

Very recently ASI funded a technological project named : “LAUE - A Gamma Ray Lens”. In this project our collaboration has the responsibility of the focal plane detector (4 x 4 cm2 , 0.5 mm spatial resolution, good energy resolution) for the test of the lens prototypes. In this framework one of the most appealing possibilities will be the use of an array of Calliste detectors in the new 256 channel version.

Conclusions (II)


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