RI/FS - PART 2 OF 2 - US Environmental Protection Agency - As, As EP, Pb, Se, Se EP, Tl Flame AA -...

J'StSXJMANAGERS \+^ DESIGNERS/CONSULTANTS

\VESTOlJ-GUl.FCl.A: ' . . :; :-ATORIEt:. NC

2417 Bond St.. University Park, Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-7533

August 23, 1989

Mr. Chris BadeAvendt Group, Inc.432 North Saginaw StreetFlint, MI 48502

Dear Mr. Bade:

Please find enclosed the metals portion of the reports for thesamples submitted to Weston/Gulf Coast Laboratories for analyses.They were identified with our batch numbers 8907G520, 8907G528,8907G580, 8907G611, 8907G645, 8907G660, 8907G709, 8907G724 and8907G753. If you have any questions, please contact Sheryl Johnsonor Lynn Gifford at our laboratories.

Sincerely,

WESTON/GULF COAST LABORATORIES

Donald Gipple Eric A.Project Director Metals Unit Leader

igEnclosures

MANAGERS DESIGNERS/CONSULTANTS

WEST . N - ' " " . - ' " . • . : / : . ' " PATORIES. -NC.

2417 Bond St.. University Park. Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-7533

INORGANIC QUALIFIERS

u - Indicates compound was analyzed for but not detectedX - Result is by calculationd - Result is on a dry weight basis.E - Severe matrix interference.M - Duplicate injection precision not met.N - Spike recovery not within control limit.S - Indicates value determined by Method of Standard Addition.A - Result is on an "as is basis" (wet weight)W - Post analytical spike is out of control limits.B - Reported value is less than the CRDL but greater than IDL.* - Duplicate not within control limits.+ - Correlation coefficient for MSA < 0.995.

ORGANIC QUALIFIERS

U - Indicates that the compound was analyzed for but not detected.

J - Indicates an estimated value for either a TIC or an analytethat meets the identification criteria but the result is lessthan the specified detection limit.

B - Indicates the compound was found in the blank and the sample.

E - Concentrations exceed calibration range of the instrument.

BS - Indicates matrix analyses were conducted on reagent grade water.

BSD - Indicates blank spike duplicate.

BDL - Below Detection Limit.

MS - Indicates matrix spike.

MSD - Indicates matrix spike duplicate.

D - Indicates that surrogate/matrix spike recoveries were notobtained because the extract had to be diluted for analysis.

DL - Indicates a secondary dilution.

NA - Not applicable.

DF - Dilution factor.

Revised 06/16/89


WESTON-GULF COAST LABORATORIES, INC.

2417 Bond St., University Park, Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-7533

CASE NARRATIVE - METALS

8907G520-001 - 8907G520-013

The samples were analyzed as follows:

ICP - Ag,Al,Ba,Be,Ca,Cd,Co,Cr,Cu,Fe,K,Mg,Mn,Na,Ni,Sb,V,ZnPb for 520-001,520-005

GFAA - As, As EP, Pb, Se, Se EP, TlFlame AA - Ag EP, Ba EP, Cd EP, Cr EP, Pb EPCold Vapor - Hg, Hg EP

Preparation Blank (PB)

All PB results were below the Contract Required DetectionLimits (CRDL) except:

Pb - The PB for 520-002, 520-011 contained approximately1.2 mg/kg. The result for 520-002 was <2.3 mg/kg and theresult for 520-011 was 12.9 mg/kg. The PB contaminationshould be considered when evaluating the concentrationin these samples since part of the concentration may bedue to contamination.

Laboratory Control Sample (LCS)

All LCS results met the required QC limits.

Duplicate

8907G520-001 As, Se, Tl8907G520-002 Hg8907G520-003 Hg EP8907G520-006 As EP, Se EP8907G520-012 Ag EP, Cd EP, Cr EP, Pb EP

All duplicate results met the required QC limits.


WESTON-GULF COAST LABORATORIES. INC.


Phones: (312) 534-5200 (219)885-7077 (815)723-7533

Spike

8907G520-001 As, Se, Tl

All spike results met the required QC limits except:

As - The spike recovery was 49.9%Se - The spike recovery was 28.8%.

These poor spike results indicate that the sample containedmatrix interferences for the As and Se analyses.

8907G520-002 Hg

All spike results met the required QC limits.

8907G520-006 As EP, Se EP


8907G520-012 Ag EP, Cd EP, Cr EP, Pb EP




2417 Bond St., University Park, Illinois 60466Phones: (312) 534-5200 (219)885-7077 (815)723-7533

A N A L Y T I C A L R E P O R T

To: Avendt Group, Inc.432 North Saginaw Street3rd FloorFlint, MI 48502

Attn: Mr. Chris Bade

Date: Friday August 25th, 1989

RE: A10 15-17Project * 5160-01-01-0001Lab ID: 8907G611-004Sample Date: 07/13/89Date Received: 07/14/89

Inorganic Client Data Report

Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium,. Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.5

5150

3.4

252

1.3

17700

1.3

12.6

10.7

19.9

9990

0.13

1260

6700

236

1260

27.5

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.5

50.4

2.6

50.4

1.3

1260

1.3

12.6

2.5

6.3

25.2 *

0.13

1260

1260

3.8

1260

10.1




Phones: (312) 534-5200 (219)885-7077 (815)723-7533

A N A L Y T I C A L REPORT

To: Avendt Group, Inc.432 North Saginaw Street3rd FloorFlint, HI 48502



RE: A10 15-17Project * 5160-01-01-0001Lab ID: 8907G611-004Sample Date: 07/13/89Date Received: 07/14/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

10.8

15.1

0.51

2.6

16.5

82.5

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

2

15

0

2

12

5

.6

.1

.51

.6

.6

.0

MANAGERS OESlGNERSmmTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A10 15-17 EPTOXProject I 5160-01-01-0001Lab ID: 8907G611-005Sample Date: 07/13/89Date Received: 07/14/89


Parameters

Silver, EP Leachate

Arsenic, EP Leachate

Barium, EP Leachate

Cadmium, EP Leachate

Chromium, EP Leachate

Mercury, EP Leachate

Lead, EP Leachate——————————————————— i ———————————Selenium, EP Leachate

Result

0.020 u

0.010 u

1.3

0.010 u

0.024

0.0010 u

0.11

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: AHA 8-13Project # 5160-01-01-0001Lab ID: 8907G724-001Sample Date: 07/19/89Date Received: 07/19/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total!

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.7

7380

13.0

240

1.3

3940

5.2

13.5

222

1130

13800

0.10

1870

2660

56.0

1350

303

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.7

53.9

0.53

53.9

1.3

1350

1.3

13.5

'2.7

6.7

26.91

0.10

1350

1350

4.0

1350

10.8

XYVMANAGERS OeSIGNERS/CONSULTANTS







RE: AHA 8-13Project # 5160-01-01-0001Lab ID: 8907G724-001Sample Date: 07/19/89Date Received: 07/19/89


Parameters Result UnitsReporting

Limit

Lead, Total 72.0 mg/kg 10.6

Antimony, Total 16.2 mg/kg 16.2

Selenium, Total 0.53 u mg/kg 0.53

Tha l l ium, Total 2.6 u mg/kg 2.6

Vanadium, Total

Zinc, Total

21.0

1410

mg/kg

mg/kg

13.5

5.4




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: AHA 8-13 EPTOXProject # 5160-01-01-0001Lab ID: 8907G724-002Sample Date: 07/19/89Date Received: 07/19/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate

Selenium, EP Leachate

Result

0.020 u

0.010 u

1.0 u

0.069

0.030

0.0010 u

0.069

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS OESGNEFIS/CONSUITANTS







RE: Allb 4-8Project # 5160-01-01-0001Lab ID: 89076709-001Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel , Total

Result

2.6

5870

4.7

212

1.3

20100

1.3

15.7

11.7

117

13800

0.11

1490

6690

440

1310

23.0

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.6

52.5

0.55

52.5

1.3

1310

1.3

13.1

2.6

6.6i

26.3

0.11

1310

1310

3.9

1310

10.5

MANAGERS DeSGNERS/CONSUlTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allb 4-8Project * 5160-01-01-0001Lab ID: 8907G709-001Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

12.9

15.8

1.3

2.7

19.4

68.5

Units

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kgmg/kg

ReportingLimit

2

15

0

2

13

5

.7

.8

.55

.7

.1

.3

4




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allb 4-8 EPTOXProject # 5160-01-01-0001Lab ID: 8907G709-002Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate


Result

0.020 u

0.010 u

1.8

0.010 u

0.020 u

0.0010 u

0.076

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050



2417 Bond SL, University Park, Illinois 60466

Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: Allc 2-6.5Project * 5160-01-01-0001Lab ID: 8907G709-005Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

8.0

5430

23.1

162

0.95

8090

4.9

15.3

27.2

3330

16700

3.1

1090

4130

197

946

301

Units

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

1.9

37.8

1.9

37.8

0.95

946

0.95

9.5

1.9

4.7

18.9

0.27

946

946

2.8

946

7.6




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allc 2-6.5Project * 5160-01-01-0001Lab ID: 89076709-005Sample Date: 07/18/89Date Received: 07/18/89



Limit

Lead, Total 276 mg/kg 9.5


Selenium, Total 1.0 mg/kg 0.37

Tha l l ium, Total 1.9 mg/kg 1.9

Vanadium, Total 17.0 mg/kg 9.5

Zinc, Total 1200 mg/kg 3.8




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allc 2-6.5 EPTOXProject # 5160-01-01-0001Lab ID: 8907G709-006Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate

,-•• Cadmium, EP Leachate•



Lead, EP Leachate

Selertium, EP Leachate

Result

0.024

0.010

1.2

0.047

0.020 u

0.0010 u

0.23

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS DESGNER&CONSUITANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Alld 8-10Project # 5160-01-01-0001Lab ID: 8907G709-009Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

CobaU, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.4

10300

4.4

2450

1.2

11700

1.2

38.9

94.2

2100

13100

3.3

1180

2500

160

4540

6940

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

ReportingLimit

2.4

47.2

0.48

47.2

1.2

1180

1.2

11.8

2.4

5.9

23.6•i

0.54

1180

1180

3.5

1180

94.4








RE: Alld 8-10Project # 5160-01-01-0001Lab ID: 8907G709-009Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

718

142

0.60

2.4

33.5

655

Units

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

11.8

142

0.48

2.4

11.8

4.7




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Alld 8-10 EPTOXProject # 5160-01-01-0001Lab ID: 8907G709-010Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate

Seleitium, EP Leachate

Result

0.037

0.010 u

2.6

0.018

0.030

0.0010 u

0.33

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Alld 18.5-23.5Project # 5160-01-01-0001Lab ID: 8907G709-011Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total ,

Result

2.0 u

2220

1.8

135

1.0 u

8090

1.0 u

10.1 u

16.6

95.3

5830

0.087 u

1010 u

3160

73.6

1010 u

109

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

ReportingLimit

2.0

40.3

0.39

40.3

1.0

1010

1.0

10.1

2.0

5.0

20.1 .,

0.087

1010

1010

3.0

1010

8.1




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Alld 18.5-23.5Project # 5160-01-01-0001Lab ID: 8907G709-011Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

31

12

0

1

10

51

.5

.1

.39

.9

.1

.8

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

1

12

0

1

10

4

.9

.1

.39

.9

.1

.0

c MANAGERS OESIGNERSÔNSULTANTS







RE: Alld 18.5-23.5 EPTOXProject # 5160-01-01-0001Lab ID: 8907G709-012Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate

Selertium, EP Leachate

Result

0.028

0.010 u

1.0

0.010 u

0.022

0.0010 u

0.092

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050



2417 Bond SI., University Park, Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12A 8-11Project # 5160-01-01-0001Lab ID: 8907G724-004Sample Date: 07/19/89Date Received: 07/19/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.7

6270

3.9

197

1.3

15900

1.3

13.3

12.6

103

12100

0.12

1420

7330

150

1330

133

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.7

53.1

0.51

53.1

1.3

1330

1.3

13.3

'2.7,

6.6

26.6

0.12

1330

1330

4.0

1330

10.6

MANAGERS D€SIGNERSAX>NSU.TANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12A 8-11 EPTOXProject # 5160-01-01-0001Lab ID: 8907G724-005Sample Date: 07/19/89Date Received: 07/19/89


Parameters

Silver, EP Leachate


Barium, EP Leachate



Mercury, EP Leachate4

Lead, EP Leachate


Result

0.020 u

0.010 u

1.4

0.010 u

0.025

0.0010 u

0.096

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12A 8-11Project # 5160-01-01-0001Lab ID: 8907G724-004Sample Date: 07/19/89Date Received: 07/19/89



Limit




Tha l l ium, Total 2.5 u mg/kg 2.5



DE9GNERS/CONSULTANTS







RE: A12b 3-7Project I 5160-01-01-0001Lab ID: 8907G611-010Sample Date: 07/13/89Date Received: 07/14/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

328

8050

15.2

516

44.1

7800

393

78.0

553

77700

312000

27.0

7800

7800

41.6

7800

1530

Units

mg/kg

nig/ kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

15.6

312

15.2

312

7.8

7800

7.8

78.0

15.6

39.0——————— ; —————————156

1.4

7800

7800

23.4

7800

62.4

MANAGERS DeSGNERS/CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533







Parameters

Lead, Total

Antimony, Total

Selenium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Result

32400

356

38.9

15.2

78.0

26800

Units

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

78.0

93.6

15.2

15.2

78.0

31.2

i

MANAGERS DESIO«S/CONSUUANTS





Attn: Hr. Chris Bade


RE: a!2b 3-7 EPTOXProject # 5160-01-01-0001Lab ID: 8907G611-011Sample Date: 07/13/89Date Received: 07/14/89


Parameters

Silver, EP Leachate


Barium, EP Leachate

Cadmium, EP Leachate!



Lead,4EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.057

0.020 u

0.0010 u

8.4

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

1.0

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12C 4-9Project # 5610-01-01-0001Lab ID: 8907G580-007Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

93.0

3780

194

500

1.9

5330

47.0

17.7

695

34800

68100

5.3

1770

1770

139

1770

959

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

3.5

70.6

13.7

70.6

1.8

1770

1.8

17.7

3.5

8.8

35.3 '

0.36

1770

1770

5.3

1770

14.1








RE: A12C 4-9Project # 5610-01-01-0001Lab ID: 8907G580-007Sample Date: 07/12/89Date Received: 07/13/89

Parameters


Result UnitsReporting

Limit

Lead, Total 2380 mg/kg 17.7



Thallium, Total 3.4 mg/kg 3.4






Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A12C 4-9 EPTOXProject # 5610-01-01-0001Lab ID: 8907G580-008Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate


Result

0.020 u

0.010 u

1.0

1.0

0.020 u

0.0010 u

0.62

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.10

0.020

0.0010

0.050

0.0050








RE: A12C 10-13 EPTOXProject * 5610-01-01-0001Lab ID: 8907G580-010Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Leadj EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.048

0.020 u

0.0010 u

0.050 u

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12C 14-16 EPTOXProject * 5610-01-01-0001Lab ID: 89076580-012Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead. EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.032

0.020 u

0.0010 u

0.050 u

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

\w WESTON-GULF COAST LABORATORIES, INC.






RE: A12d 17-20Project # 5160-01-01-0001Lab ID: 8907G709-014Sample Date: 07/18/89Date Received: 07/18/89

Inorganic

Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobaft, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total ,

Client Data

Result

1.9 u

3170

3.0

244

0.94 u

9130

0.94 u

9.4 u

10.0

298

7310

0.13 u

944 u

3840

101

944 u

47.7

Report

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

ReportingLimit

1.9

37.7

0.39

37.7

0.94

944

0.94

9.4

1.9

4.7

18.9

0.13

944

944

2.8

944

7.5

r MANAGERS DESIGNERS/CONSULTANTS


2417 Bond SI., University Park, Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12d 17-20Project # 5160-01-01-0001Lab ID: 89076709-014Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

29.7

11.3

0.39

1.9

12.9

172

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

7

11

0

1

9

3

.7

.3

.39

.9

.4

.8

MANAGERS OESK5N£RSAX)NSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12d 17-20 EPTOXProject # 5160-01-01-0001Lab ID: 89076709-015Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate


Result

0.020 u

0.010 u

2.0

0.010

0.020 u

0.0010 u

0.086

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050








RE: A13A 9-14 EPTOXProject # 5160-01-01-0001Lab ID: 8907G753-002Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.028

0.0010 u

0.083

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13b 4.5-6Project # 5160-01-01-0001Lab ID: 8907G528-001Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmitum, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

154

5460

78.0

1960

9.1

14600

529

29.9

561

42600

118000

17.7

2990

2990

379

2990

1420

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

6.0

120

11.1

120

3.0

2990

3.0

29.9

6.0

14.9\

59.8

1.1

2990

2990

9.0

2990

23.9

MANAGERS DES)GNERSrtX>NSUlTANTS







RE: A13b 4.5-6Project * 5160-01-01-0001Lab ID: 8907G528-001Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

15700

98.6

5.6

5.6

41.5

21300

Units

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

12.0

35.9

5.6

5.6

29.9

12.0

i

MANAGERS DESGNeRS/CONSULTANTC



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13b 4.5-6 EPTOXProject * 5160-01-01-0001Lab ID: 8907G528-002Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead4 EP Leachate


Result

0.020 u

0.010

1.0 u

2.6

0.020 u

0.0010 u

14.6

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

1.0

0.020

0.0010

2.0

0.0050



2417 Bond SI., University Park, Illinois 60466Phones: (312) 534-5200 (219)885-7077 (815)723-7533

A N A L Y T I C A l R E P O R T




RE: A13C 4-8.5Project # 5610-01-01-0001Lab ID: 8907G580-001Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium* Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

73.5

4350

145

2180

3.4

12600

226

31.4

452

25900

83100

2.3

2370

2370

305

2370

2230

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

4.7

94.9

18.2

94.9

2.4

2370

2.4

23.7

4.7

11.9

47.4 '

0.22

2370

2370

7.1

2370

19.0




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13C 4-8.5Project # 5610-01-01-0001Lab ID: 8907G580-001Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

4160

46.0

0.91

4.6

35.4

11500

Units

mg/kg

nig/ kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

23

28

0

4

23

9

.7

.5

.91

.6

.7

.5

DESIGNERS/CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13C 4-8.5 EPTOXProject # 5610-01-01-0001Lab ID: 89076580-002Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate


Result

0.020 u

0.010

1.0 u

4.0

0.020 u

0.0010 u

0.85

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.40

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13C 6-13 EPTOXProject # 5610-01-01-0001Lab ID: 8907G580-004Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate


Result

0.020 u

0.010 u

1.0 u

1.9

0.028

0.0010 u

0.050 u

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.20

0.020

0.0010

0.050

0.0050








RE: A13C 13-16 EPTOXProject * 5610-01-01-0001Lab ID: 8907G580-006Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate

,- Cadmium, EP Leachate\



Lead^ EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.020 u

0.0010 u

0.050 u

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS DeSIGNERS/CONSULTANTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A13D 18-23Project f 5160-01-01-0001Lab ID: 8907G724-007Sample Date: 07/19/89Date Received: 07/19/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.4

5930

4.6

219

1.2

15000

1.2

11.9

15.4

151

12100

0.10

1220

6400

249

1190

27.4

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.4

47.6

0.47

47.6

1.2

1190

1.2

11.9

2.4

6.0

23.8

0.10

1190

1190

3.6

1190

9.5








RE: A13D 18-23Project HI 5160-01-01-0001Lab ID: 89076724-007Sample Date: 07/19/89Date Received: 07/19/89

Parameters



Limit


Antimony, Total 14.3 u mg/kg 14.3


T h a l l i u m , Total 2.3 mg/kg 2.3



MANAGERS OeSIGNERS/CONSUlTANTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A13D 18-23 EPTOXProject # 5160-01-01-0001Lab ID: 89076724-008Sample Date: 07/19/89Date Received: 07/19/89


Parameters

Silver, EP Leachate


Barium, EP Leachate


- Chromium, EP Leachate


Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.017

0.025

0.0010 u

0.074

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS OeSKJNERS/CONSULTANTS







RE: A14A 4-9Project # 5160-01-01-0001Lab ID: 89076753-005Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.5

5450

2.9

201

1.2

15700

1.2

12.3

10.8

48.1

11800

0.12

1250

6580

173

1230

27.7

Units

u mg/kg

nig/ kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.5

49.0

0.49

49.0

1.2

1230

1.2

12.3

2.5

6.1 t

24.5

0.12

1230

1230

3.7

1230

9.8

nMANAGERS OeSGNERS^CONSULTANTS







RE: A14A 4-9Project # 5160-01-01-0001Lab ID: 89076753-005Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

13

14

0

2

17

69

.6

.7

.49

.4

.4

.6

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

0

14

0

2

12

4

.98

.7

.49

.4

.3

.9

n



2417 Bond St., University Park, Illinois 60466Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A14A 4-9 EPTOXProject * 5160-01-01-0001Lab ID: 8907G753-006Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.027

0.0010 u

0.096

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14B 4.0-8.5Project I 5160-01-01-0001Lab ID: 89076528-005Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmiiim, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

44.1

3740

99.5

5200

1.7

12600

49.7

23.0

329

15600

76100

28.7

1660

2710

265

1660

1220

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mq/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

3.3

66.4

12.9

66.4

1.7

1660

1.7

16.6

3.3

8.3t

33.2

1.7

1660

1660

5.0

1660

13.3








RE: A14B 4.0-8.5Project # 5160-01-01-0001Lab ID: 8907G528-005Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Lead, Total

Antimony, Total

Selenium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Result

1640

22.6

1.2

3.2

34.6

6080

Units

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

6.6

19.9

0.65

3.2

16.6

6.6

4




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14B 4.0-8.5 EPTOXProject # 5160-01-01-0001Lab ID: 89076528-006Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead,*EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.47

0.020 u

0.0010 u

0.31

0.0050 u

Units

mq/L

mg/L

mq/L

mg/L

mq/L

mq/L

mg/L

mq/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.020

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14c 4.0-8.5Project * 5160-01-01-0001Lab ID: 8907G528-008Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

_ Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

141

4970

122

1560

25.2

5260

316

43.0

402

41300

172000

12.8

4300

4300

163

4300

1240

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

8.6

172

15.8

172

4.3

4300

4.3

43.0

8.6

21.5

86.0

0.77

4300

4300

12.9

4300

34.4

MANAGERS DESIGNERS/CONSUUANTS







RE: A14c 4.0-8.5Project # 5160-01-01-0001Lab ID: 89076528-008Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

20800

175

7.9

7.9

43.0

15000

Units

mg/kg

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

17.2

51.6

7.9

7.9

43.0

17.2

i








RE: A14c 4.0-8.5 EPTOXProject * 5160-01-01-0001Lab ID: 89076528-009Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

1.2

0.020 u

0.0010 u

5.5

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.40

0.020

0.0010

0.40

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14c 8.5-10.5Project # 5160-01-01-0001Lab ID: 89076528-010Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

3.4

7200

7.6

250

1.7

22700

2.7

16.9

17.0

338

19800

0.16

1720

5980

671

1690

47.7

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

3.4

67.4

0.63

67.4

1.7

1690

1.7

16.9

3.4

8.4

33.7

0.15

1690

1690

5.1

1690

13.5




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14c 8.5-10.5Project * 5160-01-01-0001Lab ID: 89076528-010Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

88.5

20.2

0.63

3.2

25.0

167

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

6.7

20.2

0.63

3.2

16.9

6.7

4



2417 Bond St., University Park, Illinois 60466Phones: (31 2) 534-5200 (219)885-7077 (815)723-7533





RE: A14D 10-14Project I 5610-01-01-0001Lab ID: 89076580-013Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.0

4550

5.5

191

1.0

14500

1.0

10.1

9.8

41.4

11200

0.10

1010

5180

351

1010

14.2

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.0

40.4

0.41

40.4

1.0

1010

1.0

10.1

2.0

5.0

20.2 '

0.10

1010

1010

3.0

1010

8.1

DESKJNER&CONSUUANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14D 10-14Project # 5610-01-01-0001Lab ID: 89076580-013Sample Date: 07/12/89Date Received: 07/13/89

Parameters



Limit

Lead, Total 10.6 nig/kg 2.0

Antimony, Total 12.1 u mg/kg 12.1

Selenium, Total 0.41 u mg/kg 0.41

Thallium, Total 2.0 u mg/kg 2.0


Zinc, Total 47.9 mg/kg 4.0








RE: A14D 10-14 EPTOXProject # 5610-01-01-0001Lab ID: 8907G580-014Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate——————————————————— t ———————————Selenium, EP Leachate

Result

0.020 u

0.010 u

1.0 u

0.010 u

0.020 u

0.0010 u

0.13

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050








RE: A15A 9-14 EPTOXProject I 5160-01-01-0001Lab ID: 8907G753-010Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead,* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.020

0.0010 u

0.089

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS DESGNER&CONSULTANTS







RE: A15b 6-9Project * 5160-01-01-0001Lab ID: 8907G520-001Sample Date: 07/07/89Date Received: 07/11/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Totalt

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

3.1

7180

11.9

242

1.6

21900

7.3

15.5

22.9

722

21200

0.14

1630

5880

622

1550

73.4

Units

u mq/kq

mg/kq

mg/kg

nig/ kg

mq/kq

mq/kq

mq/kq

u mq/kq

mg/kg

mg/kg

mq/kq

u mg/kg

mq/kq

mq/kq

mq/kq

U mq/kq

mq/kq

ReportingLimit

3.1

62.0

0.63

62.0

1.5

1550

1.5

15.5

3.1

7.7

31.0

0.14

1550

1550

4.6

1550

12.4




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15b 6-9Project # 5160-01-01-0001Lab ID: 8907G520-001Sample Date: 07/07/89Date Received: 07/11/89


Parameters

Lead, Total

Antimony,

Selenium,

,- Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

4

Result

250

18.6

1.6

3.2

24.8

337

Units

nig/ kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

6.2

18.6

1.6

3.2

15.5

6.2




ANALYT ICAL REPORT




RE: A15b 6-9 EPTOXProject f 5160-01-01-0001Lab ID: 89076520-013Sample Date: 07/07/89Date Received: 07/11/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead.t EP Leachate


Result

0.020 u

0.010 u

1.4

0.018

0.027

0.0010 u

0.14

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15b 13-16Project # 5160-01-01-0001Lab ID: 89076520-002Sample Date: 07/07/89Date Received: 07/11/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.4

1520

2.4

57.9

1.2

6270

1.2

11.8

4.9

28.4

4240

0.12

1180

2100

116

1180

9.4

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kq

mq/kq

mq/kq

u mq/kg

u mg/kq

ReportingLimit

2.4

47.0

0.45

47.0

1.2

1180

1.2

11.8

2.4

5.9i

23.5

0.12

1180

1180

3.5

1180

9.4

MANAGERS DeSlGNERS/CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15b 13-16Project * 5160-01-01-0001Lab ID: 89076520-002Sample Date: 07/07/89Date Received: 07/11/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,iVanadium,

Total

Total

Total

Total

Zinc, Total

4

Result

22.

14.

1.

2.

11.

28.

3

1

1

2

8

1

Units

u mg/kg

u mg/kg

u mq/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

22

14

1

2

11

4

.3

.1

.1

.2

.8

.7

MANAGERS OKIGNERS/CONSUUANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15b 13-16 EPTOXProject # 5160-01-01-0001Lab ID: 8907G520-003Sample Date: 07/07/89Date Received: 07/11/89


Parameters

Silver, EP Leachate


Barium, EP Leachate


_ Chromium, EP Leachate


Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.020 u

0.0010 u

0.061

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS DE3Gh£RS/CONSUUANTS







RE: A15c 4.5-9Project I 5160-01-01-0001Lab ID: 8907G520-005Sample Date: 07/10/89Date Received: 07/11/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

63.8

4540

105

2180

27.8

7350

532

37.0

333

17800

254000

61.2

3700

3700

230

3700

1820

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kq

mg/kg

u mq/kq

u mq/kq

mq/kq

u mq/kq

mq/kq

ReportingLimit

7.4

148

7.1

148

3.7

3700

3.7

37.0

7.4

18.5

74.0

3.8

3700

3700

11.1

3700

29.6








RE* A15c 4.5-9Project # 5160-01-01-0001Lab ID: 89076520-005Sample Date: 07/10/89Date Received: 07/11/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

4

Result

5860

136

17.7

7.1

43.0

13700

Units

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

14.8

44.4

17.7

7.1

37.0

14.8



2417 Bond St., University Park, Illinois 60466Phones. (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15c 4.5-9 EPTOXProject I 5160-01-01-0001Lab ID: 8907G520-006Sample Date: 07/10/89Date Received: 07/11/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.74

0.020 u

0.0010 u

0.32

0.0050 u

Units

mq/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.10

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15D 4-9Project # 5610-01-01-0001Lab ID: 8907G580-017Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total——————————————————— * —————————Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.0

4980

6.4

170

1.0

13500

1.0

10.0

11.3

25.0

10600

0.11

1060

5350

379

1000

15.0

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.0

40.2

0.39

40.2

1.0

1000

1.0

10.0

2.0

5.0

20.1 '

0.11

1000

1000

3.0

1000

8.0




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15D 4-9Project * 5610-01-01-0001Lab ID: 8907G580-017Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

9

12

0

1

15

52

.5

.0

.39

.9

.2

.1

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

1

12

0

1

10

4

.9

.0

.39

.9

.0

.0

MANAGERS DESXJNEF&'CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15D 4-9 EPTOXProject * 5610-01-01-0001Lab ID: 8907G580-018Sample Date: 07/12/89Date Received: 07/13/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead. EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.038

0.0010 u

0.13

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050








RE: A16A 9-14 EPTOXProject # 5160-01-01-0001Lab ID: 89076753-014Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead? EP Leachate


Result

0.032

0.010 u

1.1

0.010 u

0.044

0.0010 u

0.15

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050








RE: A16E 13-18 EPTOXProject * 5160-01-01-0001Lab ID: 8907G753-021Sample Date: 07/20/89Date Received: 07/20/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead,* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.030

0.0010 u

0.085

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533







Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total\:

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total ,

Result

55.8

1980

10.8

712

3.1

9030

52.5

13.1

128

26000

52300

124

1310

1560

47.7

1310

705

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.6

52.5

0.99

52.5

1.3

1310

1.3

13.1

2.6

6.6

26.2 ,

17.0

1310

1310

3.9

1310

10.5

MANAGERS OeSGNER&CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533







Parameters

Lead, Total

Antimony,

Selenium,

Thallium,i

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

3760

117

10.9

2.5

13.1

2290

Units

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

13.1

15.8

0.99

2.5

13.1

5.2

MANAGERS DESIGNERS/CONSULTAMTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16b 9-12 EPTOXProject # 5160-01-01-0001Lab ID: 89076709-018Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate

Cadmium, EP Leachate— \



Lead, EP Leachate


Result

0.020 u

0.018

1.0 u

1.0

0.020 u

0.0010 u

4.2

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.20

0.020

0.0010

2.0

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16c 2-5Project * 5160-01-01-0001Lab ID: 8907G709-020Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Totali

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobaft, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total ,

Result

91.9

1400

7.5

473

2.5

7270

49.4

10.9

119

16600

69900

93.0

1090

1090

40.1

1090

716

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.2

43.5

0.44

43.5

1.1

1090

1.1

10.9

2.2

5.4

21.8 ,

8.3

1090

1090

3.3

1090

8.7




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16c 2-5Project I 5160-01-01-0001Lab ID: 8907G709-020Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

2910

114

5.3

2.2

10.9

2120

Units

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

10

13

0

2

10

4

.9

.1

.44

.2

.9

.4




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16c 2-5 EPTOXProject # 5160-01-01-0001Lab ID: 89076709-021Sample Date: 07/18/89Date Received: 07/18/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.64

0.020 u

0.0010 u

1.8

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.50

0.0050










Parameters

Silver, Total

Aluminum, Total

Arsenic, lotai

Barium, Total

beryllium, Total

calcium, lotal

Cadmium, Total

Cobalt, lotal

Chromium, Total

Copper, lotal

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, lotal .

Nickel, lotal

Result

132

2800

/.b

529

2.9

1/UUU

13b

12.2

434

zy400

4t>/00

8.2

1ZZO

1600

228

1221)

bb2

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kgmg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.4

Aluminum, Tdtal

0.98

4878

1 .2

1220

1.2

12.2

———— 2r4 ——————————

——— *n.24.4

0.49

1220

1ZZU

3./

1220

y.a










Parameters

Lead, Total

Antimony, Total

Selenium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Result

10000

51.8

8.8

2.4

12.2

9300

Units

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

12.2

14.6

4.9

2.4

12.2

4.9

4








RE: A21b 1-6 EPTOXProject * 5160-01-01-0001Lab ID: 8907G660-002Sample Date: 07/17/89Date Received: 07/17/89


Parameters

Silver, EP Leachate


Barium, EP Leachate

Cadmium, EP Leachate\



Lead, EP Leachate


Result

0.020 u

0.35

1.5

3.4

0.13

0.0010 u

35.4

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.20

1.0

0.20

0.020

0.0010

2.0

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533







Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Totali

Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

348

5120

25.3

1050

36.0

12100

470

39.8

397

91800

199000

16.3

3980

3980

235

3980

6410

Units

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

8.0

159

3.3

159

4.0

3980

4.0

39.8

8.0

19.9

79.7

0.86

3980

3980

12.0

3980

31.9

MANAGERS OESKJNERSÔNSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533







Parameters

Lead, Total

Antimony, Total

Selenium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Result

30400

305

41.6

8.3

39.8

26700

Units

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

ReportingLimit

39.8

47.8

16.7

8.3

39.8

15.9

MANAGERS DE9GNERS/CONSUUAKTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A21c 4-8 EPTOXProject Jf 0000-00-00-0000Lab ID: 8907G645-002Sample Date: 07/14/89Date Received: 07/15/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead, EP Leachate——————————————————— t ———————————Selenium, EP Leachate

Result

0.020 u

0.010 u

3.3

3.9

0.020 u

0.0010 u

15.6

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.20

0.020

0.0010

1.0

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A21d 14-19Project I 5160-01-01-0001Lab ID: 8907G520-011Sample Date: 07/10/89Date Received: 07/11/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

_ Beryllium, Total

Calcium, Total

Cadmkim, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium* Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.7

4550

0.57

148

1.4

12600

1.4

13.6

12.4

24.7

11300

0.14

1360

4320

167

1360

47.7

Units

u mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

mq/kg

u mg/kg

u mq/kq

mq/kq

mq/kq

u mg/kg

mq/kq

ReportingLimit

2.7

54.3

0.57

54.3

1.4

1360

1.4

13.6

2.7

6.8i

27.2

0.14

1360

1360

4.1

1360

10.9

MANAGERS DeSIGNERS/CONSULTANTS







RE: A21d 14-19Project # 5160-01-01-0001Lab ID: 8907G520-011Sample Date: 07/10/89Date Received: 07/11/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

-_. Vanadium,

Total

Total

Total

Total

Zinc, Total

i

Result

12.9

16.3

1.4

2.8

20.3

270

Units

mg/kg

u mg/kgu mg/kg

u mg/kg

mg/kgmg/kg

ReportingLimit

11.4

16.3

1.4

2.8

13.6

5.4








RE: A21d 14-19 EPTOXProject f 5160-01-01-0001Lab ID: 89076520-012Sample Date: 07/10/89Date Received: 07/11/89


Parameters

Silver, EP Leachate


Barium, EP Leachate


_ Chromium, EP Leachate


Lead,t EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.020 u

0.0010 u

0.061

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS DESIGNERS/CONSUUANTS


2417 Bond Si., University Park, Illinois 60466Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A22a 9-14 EPTOXProject # 5160-01-01-0001Lab ID: 8907G528-013Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead,* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.010 u

0.020 u

0.0010 u

0.16

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/Lmg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.020

0.0050










Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmjum, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

2.4

3110

6.9

241

0.95

12700

2.6

9.5

28.7

1160

10100

0.17

946

4220

194

946

95.2

Units

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

1.9

37.9

0.39

37.9

0.95

946

0.95

9.5

1.9

4.7

18.9 '

0.13

946

946

2.8

946

7.6










Parameters

Lead, Total

Antimony, Total

Selenium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Result

145

11.4

0.73

2.0

10.3

373

Units

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

9.5

11.4

0.39

2.0

9.5

3.8

4

f MANAGERS DESIGNERS/CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533

ANALYTICAL REPORT




RE: A22b 0-7 EPTOXProject * 5160-01-01-0001Lab ID: 8907G660-006Sample Date: 07/17/89Date Received: 07/17/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Leadj EP Leachate


Result

0.020 u

0.050 u

3.9

0.10

0.060

0.0010 u

0.68

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.050

1.0

0.010

0.020

0.0010

0.050

0.0050








RE: A22c 3-9Project * 5160-01-01-0001Lab ID: 8907G660-008Sample Date: 07/17/89Date Received: 07/17/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

,,-- Barium, Totalt , . .. , ———————————————Beryllium, Total

Calcium, Total

Cadmium, Total

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total

Result

11.9

2970

18.5

414

1.0

12000

29.2

10.1

62.0

3510

12600

0.11

1010

2740

133

1010

317

Units

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kgu mg/kg

u mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

ReportingLimit

2.0

40.2

2.0

40.2

1.0

1010

1.0

10.1

2.0

5.0

20.1 '

0.11

1010

1010

3.0

1010

8.0

MANAGERS OeSGNEBS/CONSULTANrS







RE: A22c 3-9Project f 5160-01-01-0001Lab ID: 8907G660-008Sample Date: 07/17/89Date Received: 07/17/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,1

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

749

12.1

2.0

2.0

11.9

1510

Units

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

10

12

0

2

10

4

.1

.1

.39

.0

.1

.0




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A22c 3-9 EPTOXProject # 5160-01-01-0001Lab ID: 8907G660-009Sample Date: 07/17/89Date Received: 07/17/89

Inorganic

Parameters

Silver, EP Leachate


Barium, EP Leachate




Leadt EP Leachate


Client Data

Result

0.020 u

0.010 u

1.7

0.011

0.020 u

0.0010 u

0.10

0.0050 u

Report

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A22d 4-9 EPTOXProject # 5160-01-01-0001Lab ID: 89076528-017Sample Date: 07/11/89Date Received: 07/12/89


Parameters

Silver, EP Leachate


Barium, EP Leachate




Lead* EP Leachate


Result

0.020 u

0.010 u

1.0 u

0.045

0.020 u

0.0010 u

0.12

0.0050 u

Units

mq/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.020

0.0050

MANAGERS DESGNERS/CONSULTANTS







RE: A23a 19-20Project # 0000-00-00-0000Lab ID: 8907G645-007Sample Date: 07/14/89Date Received: 07/15/89


Parameters

Silver, Total

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Calcium, Total

Cadmium, Total——————————————————————————————— 4 ——————————————

Cobalt, Total

Chromium, Total

Copper, Total

Iron, Total

Mercury, Total

Potassium, Total

Magnesium, Total

Manganese, Total

Sodium, Total

Nickel, Total '

Result

2.8

5590

5.6

198

1.4

26200

1.4

23.0

15.6

591

13500

0.14

1390

5160

318

1390

56.3

Units

u mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

mg/kg

u mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kgu mg/kg

mg/kg

ReportingLimit

2.8

55.7

0.59

55.7

1.4

1390

1.4

13.9

2.8

7.0

27.8 '

0.14

1390

1390

4.2

1390

11.1

MANAGERS DESGNER&CONSULTANTS







RE: A23a 19-20Project * 0000-00-00-0000Lab ID: 8907G645-007Sample Date: 07/14/89Date Received: 07/15/89


Parameters

Lead, Total

Antimony,

Selenium,

Thallium,

Vanadium,

Total

Total

Total

Total

Zinc, Total

Result

24

16

0

3

17

237

.0

.7

.59

.0

.4

Units

mg/kg

u mg/kg

u mg/kg

u mg/kg

mg/kg

mg/kg

ReportingLimit

5.

16.

0.

3,

13.

5.

9

7

59

0

9

6




Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A23a 19-20 EPTOXProject * 0000-00-00-0000Lab ID: 8907G645-008Sample Date: 07/14/89Date Received: 07/15/89


Parameters

Silver, EP Leachate


Barium, EP Leachate

Cadmium, EP Leachatei



Lead,4EP Leachate


Result

0.024

0.010 u

1.0 u

0.012

0.033

0.0010 u

0.17

0.0050 u

Units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0.020

0.010

1.0

0.010

0.020

0.0010

0.050

0.0050

MANAGERS

rDESIGNERS/CONSULTANTS

-,Vr.i>M . - - - i . . LABORATORIES. INC.

2417 Bond Si . ;J. . .1 - , -s i t y Park. Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-7533

August 23, 1989


Dear Mr. Bade:

Please find enclosed the BNA portion of the reports for the samplessubmitted to Weston/Gulf Coast Laboratories for analyses. They wereanalyzed by Lionville Analytics. They were identified with ourbatch numbers 8907G520, 8907G528, 8907G580, 8907G611, 8907G645,8907G660 and 8907G709. If you have any questions, please contactSheryl Johnson or Lynn Gifford at our laboratories.

Sincerely,


Donald GippleProject Director

igEnclosures

in Roy F. Weston, Inc. - Llonville Laboratory1

RFW Batch Number: 8907G520

Cust ID:

Sample RFWf:Information Matrix:

D.F.:Units:

Nitrobenzene-d5Surrogate 2-FluorobiphenylRecovery p-Terphenyl-d!4

Phenol-d52-Fluorophenol

2,4, 6-Tribromophenol

Phenolbis { 2-Chloroethyl ) ethur2-Chlorophenol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis (2-Chloroiflopropyl) ether4-MethylphenolN-Nitroso-Di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbis ( 2 -Chloroethoxy ) methane2 , 4-Dichlorophenol1,2, 4-Tr ichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene*= Outside of EPA CLP QC limits.

Semivolatiles by GC,Client: AVENDT GROUP ~~"

A15B 6-9

001SOIL1.00ug/Kg

83891028777107

42042042012011004201100420420420420420420420420420240420420490420420420420420420

UUUJ

U

UUUUUUUUUJUU

UUUU

U

A15B 6-9

001 MSSOIL1.00ug/Kg

828077807593

8042081560

225 *420280042042042075420420420420420550420420233 *42042042096420420

=fl==

U

U

UUU

UUUUUJUU

UUU

UU

Appendix IX List Report Date: 08/02/89 '05Work Order: 5610-01-01-0001 Paq, la

A15B 6-9 A15C 4.5-9 SBLK

001 MSD 005 89LE0626-MB1SOIL SOIL SOIL1.00 25.0 1.00

ug/Kg ug/Kg ug/Kg

979810310088113

9042090360171 *420340042042042087420420420420420210042042097420420420118 *420420

iU

J

U

UUU

UUUUUUUU

UUU

UU

DDDDDD

= aSSE = ZTSS£3

180001800018000490064000180007400018000180001800018000180001800018000180001800088000180001800046000180001800018000180001800018000

==fl==sUUU

N J

U

jUUUUUUUUUUUU

UUUUUU

9698135928894

3303303303303303303303303303303303303303303303301700330330330330330330330330330

UUUUUUUUUUUUUUUUUUUUUUUUUU

RFW Batch N"mbert 8907G520 Clientt AVENDT GROUPCust ID: A15B 6-9 A15B 6-9

RFWl: > 001 001 US

2,4, 6-Trichlorophenol2,4, 5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2 , 6-Dinitrotoluene3-NitroanilineAcenaphthene2 , 4-Dinitrophenol4-NitrophenolDibenzofuran2 , 4-OinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherPluorene4-Nitroaniline4 , 6-Dinitro-2-methylphenolN-NitroBodiphenylamine (1)4-Bromophenyl-phenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButylbenzylphthalate3,3' -DichlorobenzidlneBenzo ( a ) anthraceneChryeenebis (2-Ethylhexyl ) phthalateDl-n-Octyl phthalateBenzo ( b ) f luorantheneBenzo (k)f luorantheneBenzo ( a ) pyreneI ndeno (1,2, 3-cd ) pyreneD ibenzo ( a , h ) anthraceneBenzo ( g , h , 1 ) pery lene1,4-Dioxane*= Outside of EPA CLP OC limits.

4202100420

2100420420420

2100420

21002100420420420420420

210021004942059

f 8842042056420420160840420420240420420420420420420420420

0UUUUUUUUUUUUUUUUUJUJJ)/UUJUUJUUUJBUUUUUUUU

4202100420

2100420420420

210094

2100143 *42091 *420420420

2100210042042013010542042085420102200850420420790420420420420420420420420

UUUUUUUU%U%U%UUUUUUUJ%UUJU%JUUUBUUUUUUUU

A15B 6-9

001 MSD

4202100420

2100420420420

210099

2100176 *420100 *420420420

2100210010042057

120 *4204204442096150830420420300420420420420420420420420

Work Order: 5610-01-01-0001 Paqe: IbA15C 4.5-9 SBLK

005 89LE0626-MB1

UUUUUUUU%U%U%UUUUUJUJ%UUJU%JUUUJBUUUUUUUU

18000880001800088000180001800018000880001800088000880001800018000180001800018000880008800025001800043008800018001800018000180001800011000350001800018000110001800018000180001800018000180001800018000

UUUUUUUUUUUUUUUUUUJUJUJUUUUJUUUJBUUUUUUUU

3301700330

1700330330330

1700330

17001700330330330330330

17001700330330330

170033033033033033033067033033055330330330330330330330330

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUJUUUUUUUU

RFH Batch Number; 8907G520 Client: AVENDT GROUP Work Orderi 5610-01-01-0001Oust IDt A15B 6-9 A15B 6-9 A15B 6-9 A15C 4.5-9 SBLK

Pages Ic

RFWft 001 001 MS 001 MSD 005 89LE0626-MB1

Methyl methacrylate_Pyridlne_________N-NitroBOdimethylamine_Ethyl methacrylate___2-PicolineN-Nitroaomethylethylamine_Methyl methanesulfonate__N-NitroBodiethylamine___Ethyl -methanesulfonate___AnilinePentachloroethane_3-Methylphenol"N-Nitroeopyrrolidine_Acetophenone_______N-NitroBomorpholine_o-ToluidineN-Nitrosopiperidine______a,a-Dimethylphenethylamine2,6-Dichlorophenol______Hexachloropropene_______p-Phenylenediamine_______N-Nitro80-di-n-butylamine_Safrole1,2,4,5-TetrachlorobenzeneiBosafrole1,4-Naphthoquinone_1,3-DinitrobenzenePentachlorobenzene1-Naphthylamine__2-Naphthylamine__2,3,4,6-Tetrachlorophenol_1,3,5-Trinitrobenzene___Diallate___________.Phenacetin____________Diphenylamine__________5-Nitro-o-toluidine_____4-Aminobiphenyl________Pronantide2-Bec-Butyl-4,6-dinitrophenol_Pentachloronitrobenzene

420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 ,U420 U140 J420 U420 U

2100 U420 U420 U420 U420 U420 U420 U140 J420 U420 U420 U380 J420 U420 U420 U420 U420 U420 U42 J420 U420 U420 U

2100 U2100 U

420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U370 J420 U420 U

2100 U420 U420 U420 U420 U420 U420 U600420 U420 U420 U710420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U

2100 U2100 U

420 U420 U420 U420 U420 U420 U420 U420 U420 U420 0420 U420 U420 U320 J420 U420 U

2100 U420 U420 U420 U420 U420 U420 U190 J420 U420 U420 U420420 U420 U420 U420 U420 U420 U100 J420 U420 U420 U

2100 U2100 U

18000 U18000 U18000 U18000 U18000 U18000 U18000 U18000 U18000 U18000 U18000 U18000 U18000 U8100 J18000 U18000 U88000 U18000 U18000 U18000 U18000 U18000 U18000 U10000 J18000 U18000 U18000 U2800018000 U18000 U18000 U18000 U18000 U18000 U2500 J18000 U18000 018000 U88000 U88000 U

330 U330 0330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U

1700 U330 U330 U330 U330330 U330 U330 U330 U330330330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U

1700 U1700 U

U

UU

*= Outside of EPA CLP QC limits.

RFW Batch "-nber : 8907G520 ClientJ AVENDT GROUPCust ID: A15B 6-9

RFWl: > 001

4-Nitroquinoline-l-oxideMethapyrileneAramiteChlorobenzilatep-Dimethylaminoazobenzene3,3' -Dimethylbenzidine2-Acetylaminof luorene7, 12-Dimethylbenz( a) anthraceneHexachlorophene3-Methylcholanthrene

8404208404204204204204203800420

UUUUUUUUUU

A15B 6-9

001 MS

8504208504204204204204203800420

UUUUUUUUUU

Work Order: 5610-01-01-0001 Paqe: IdA15B 6-9 A15C 4.5-9 SBLK

001 MSD 005 89LE0626-MB1

8304208304204204204204203700420

UUUUUUUUUU

350001800035000180001800018000180001800016000018000

UUUUUUUUUU

6703306703303303303303303000330

UUUUUUUUUU

(1) - Cannot be separated from Diphenylamine. *= Outside of EPA CLP QC limits.

Roy F. Weston, IncSemivolatiles by

Client> AVBNDT GROUP

- Lionville Laboratory,/MS, Appendix IX List

Work Order;Report Date: 08/C j 15:42

5610-01-01-0001_______Page; las

) Cuat ID:

Sample RFWf :Information Matrix:

D.F. :Units:


Phenol-d52 -F luor opheno 1


Phenolbis ( 2-Chloroethyl ) ether2-Chlorophenol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis { 2-Chloroisopropy 1 ) ether4-MethylphenolN-NitroBO-Di-n-propylamineHexachloroethaneNitrobenzenelaophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbis{2-Chloroethoxy)methane2 , 4-Dichlorophenol1,2, 4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene* = Outside of BPA CLP QC limits.

A13B4.5-6

001SOIL5.00ug/Kg

DDDDDD

130044004400,.510039000440012000440044004400440044004400440044004400220004400440047000440044004400440044004400

JU

)'U

UUUUUUUUUUUU

UUUUUU

A14C8.5-10.5 SBLK

010 89LE0626-MB1SOIL SOIL1.00 1.00

ug/Kg ug/Kg

4870107655295

420420420420730420210420420420420420420420420420

2100420420420420420420420420420

= fl==:

UUUU

UJUUUUUUUUUUUUUUUUUUU

96 %98 %135 %92 %88 %94 %

330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U1700 U330 U330 U330 U330 U330 U330 U330 U330 U330 U

RFW Ba» Numbert B907G52Bf "^^ ••• "~— -- " '• • •• ———————

CD

Client: AVENDT GROUPCust IDi A13B4.5-6

RFWf: 001

A14CB.5-1_

010

Work Order; 5610-01-01-0001 IbSBLK

89LE0626-MB1

2,4,6-Trichlorophenol_2,4,5-Trichlorophenol_2-Chloronaphthalene__2-Nitroaniline______Dlmethylphthalate___Acenaphthylene______2,6-Dinitrotoluene3-Nitroaniline___~Acenaphthene_____2,4-Dinitrophenol_4-Nitrophenol___Dibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline__________4,6-Dinitro-2-methylphenolN-Nitro8odiphenylamine (1)4-Brornophenyl-phenylether_Hexachlorobenzene_______Pentachlorophenol________Phenanthrene___________AnthraceneDi-n-ButylphthalateFluoranthene______Pyrene___________Butylbenzylphthalate__3,3'-DichlorobenzidineBenzo(a)anthracene___Chrysene___________bis(2-Ethylhexyl)phthalate_Di-n-Octyl phthalate____~Benzo(b)fluoranthene_____Benzo(k)fluoranthene_____Benzo(a)pyrene__________Indeno(1,2,3-cd)pyrene_Dibenzo(a,h)anthraceneBenzo(g,h,i)perylene__1,4-Dioxane_____

Outside of EPA CLP QC limits.

4400 U22000 U4400 U22000 U4400 U4400 U4400 U22000 U4400 D22000 U22000 U4400 U4400 U4400 U4400 U800 J

22000 U22000 U4400 U4400 U4400 U22000 U1800 J4400 U4400 U1400150011008900 U4400 U4400 U6200 B4400 U4400 U4400 U4400 U4400 U4400 U4400 U4400 U

JJJ

420 U2100 U420 U

2100 U420 U420 U420 U

2100 U420 U

2100 U2100 U420 U420 U420 U420 U420 U

2100 U2100 U420 U420 U420 U

2100 U420 U420 U420 U420 U420 U420 U840 U420 U420 U190 JB420 U420 U420 U420 U420 U420 U420 U420 U

330 U1700 U330 U

1700 U330 U330 U330 U

1700 U330 U

1700 U1700 U330 U330 U330 U330 U330 U

1700 U1700 U330 U330 U330 U

1700 U330 U330 U330 U330 U330 U330 U670 U330 U330 U55 J330 U330 U330 U330 U330 U330 U330 U330 U

RFWBa*--1- Number; 8907G528 Clientt AVENDT GROUP

O

Oust IDs A13B4.5-6

RFWl: 001

A14C8.5-._

010

Work Order; 5610-01-01-0001 IcSBLK

89LE0626-MB1

Methyl methacrylate_Pyridine_________N-NitroaodimethylamineEthyl methacrylate___2-PicolineN-Nltrosomethylethylamine_Methyl methanesulfonate__N-NitroBodiethylamine___Ethyl roethaneaulfonate__AnilinePentachloroethane_3-MethylphenolN-Nitrosopyrrolidine_Acetophenone_______N-NitroBomorpholine_o-ToluidineN-Nitrosopiperidine______a, a-Dimethylphenethylamine_2,6-Dichlorophenol_______Hexachloropropene_______p-Phenylenediamine_______N-NitroBO-di-n-butylamine_Safrole1,2,4,5-TetrachlorobenzeneiBosafrole1,4-Naphthoquinone1,3-Dinitrobenzene_Pentachlorobenzene1-Naphthylamine___2-Naphthylamine___2,3,4,6-Tetrachlorophenol1,3,5-Trinitrobenzene___Diallate______________Phenacetin____________Diphenylamine__________5-Nitro-o-toluidine_____4-Aminobiphenyl________Pronamide2-Bec-Butyl-4,6-dinitrophenol_Pentachloronitrobenzene

440044004400440044004400440044004400440044004400440024000j

UUUUUUUUUUUUU

440022000440044004400440044004400280004400440044001900044004400440044004400440044004400440044002200022000

UUUUUUUUU

UUU

U0UUUUUUUUUU

420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U320 J420 U420 U2100 U420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U260 J420 U420 U420 U420 U420 U420 U420 U420 U420 U420 U2100 U2100 U

Outside of EPA CLP QC limitB.

330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U1700 U330 U330330330330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330 U330330330 U1700 U1700 U

UUU

UU

RFW Bat--1- Number? B907G528 Client: AVENDT GROUP Work Order: 5610-01-01-0001 Id- Cuat ID«

RFWfs

4-Nitroquinoline-l-oxideMethapyrileneAraraiteChlorobenzilatep-Dimethylaminoazobenzene3,3' -Dimethylbenzidine2-Acetylaminof luorene7 , 12-Dimethylbenz { a ) anthraceneHex ach 1 orophene3-Methylcholanthrene

A13B4.5-6 A14C8.5-. , SBLK

001 010 89LE0626-MB1

89004400890044004400440044004400400004400

UUUUUUUUUU

8404208404204204204204203800420

UUUUUUUUUU

6703306703303303303303303000330

UUUUUUUUUU

(1) - Cannot be separated from Diphenylamine. *« Outside of EPA CLP QC limits.

Roy F. Western, IncSemivolatilea by

Client; AVENDT GROUP

Lionville Laboratory, MS, Appendix IX List Report Date: 08/0-, • 17:34

Work Order; 5160-01-01-0001_______Page; la

Cust ID:


D.F.:Units:




Phenolbis ( 2-Chloroethyl ) ether2-Chlorophenol1 , 3-Dichlorobenzene1, 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis { 2-Chloroi8opropyl ) ether4-MethylphenolN-NitroBO-Di-n-propylamineHex ach 1 or oet haneNitrobenzeneIsophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbis ( 2-Chloroethoxy ) methane2 , 4-Dichlorophenol1,2, 4-TrichlorobenzeneNaphthalene4-Chloroanil ineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene*- Outside of EPA CLP QC limits.

A12C 4-9 SBLK

007 89LE0635-MB1SOIL SOIL27.8 1.11

ug/Kg ug/Kg

DDDDDD

33000330003300033000180003300033000330003300033000330003300033000330003300033000170000330003300031000330003300033000330003300033000

|

UUUUJUUUUUUUUUUUUUUJUUUUUU

9083126737369

3703703703703703703703703703703703703703703703701900370370370370370370370370370

UUUUUUUUUUUUUUUUUUUUUUUUUU

«

RFW Bat"w Number: 8907G5803 Cust ID:

RFWf :

2,4, 6-Tr ichlorophenol2,4, 5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2 , 6-Dinitrotoluene3-NitroanilineAcenaphthene2 , 4-Dinitrophenol4-NitrophenolDibenzofuran2 , 4-DinitrotolueneDiethylphthalate4 -Ch loropheny 1-pheny let herFluorene4-Nitroaniline4 , 6-Dinitro-2-methylphenolN-NltroBodiphenylamine (1)4-Bromopheny 1-pheny letherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButylbenzylphthalate3,3' -DichlorobenzidineBenzo ( a ) anthraceneChrysenebis ( 2-Ethylhexyl ) phthalateDi-n-Octyl phthalateBenzo(b) f luorantheneBenzo ( k ) f luorantheneBenzo ( a ) pyreneI ndeno (1,2,3 -cd ) pyreneDibenzo ( a , h ) anthraceneBenzo(g,h, i)perylene1,4-Dloxane*«= Outside of EPA CLP QC limits.

Client:A12C 4-9

007

330001700003300017000033000330003300017000033000170000170000330003300033000330003300017000017000033000330003300017000033000330003300044006700330006600033000330008600380033000330003300033000330003300033000

AVENDT GROUP Work Order: 5160-01-01-0001 P—e: IbSBLK

89LE0635-MB1

UUUUUUUUUUUUUUUUUUUUUUUUUJJUUUUJJUUUU0UU

3701900370190037037037019003701900190037037037037037019001900370370370190037037057370370370740370370370370370370370370370370370

UUUUUUUUUUUUUUUUUUUUUUUUJUUUUUUUUUUUUUUU

RFW Bate*- Number: 8907G580Cust ID:

RFWf :

Methyl methacrylatePyridineN-NitroBodimethylainineEthyl methacrylate2-PicolineN-Nitro8omethylethylamineMethyl methanesulfonateN-NitrosodiethylainineEthyl methanesulfonateAnilinePentachloroethane3-MethylphenolN-NitrosopyrrolidineAcetophenoneN-NitroBomorpholineo-ToluidineN-Nitroaopiperidinea, a-Diroethylphenethylamine2 , 6-DichlorophenolHexachloropropenep-PhenylenediamineN-Nitroao-di-n-butylamineSafrole1,2,4, 5-TetrachlorobenzeneleoBafrole1 , 4-Naphthoquinone1 , 3-DinitrobenzenePentachlorobenzene1-Naphthylamine2-Naphthylamine2,3,4, 6-Tetrachlorophenol1,3, 5-Tr initrobenzeneDiallatePhenacetinDiphenylamine5-Nitro-o-toluidine4-ArainobiphenylPronamide2-sec-Butyl-4 , 6-dinitrophenolPentachloronitrobenzene*- Outside of EPA CLP QC limits.

Client:A12C 4-9

007

3300033000330003300033000330003300033000330003300033000330003300033000330003300017000033000330003300033000330003300080003300033000330001800033000330003300033000330003300033000330003300033000170000170000

AVENDT GROUP Work Order: 5160-01-01-0001 Paae: IcSBLK

B9LE0635-MB1

UUUUUUUUUUUUUUUUUUUUUUUJUUUJUUUUUUUUUUUU

370370370370370370370370370370370370370370370370190037037037037037037037037037037037037037037037037037037037037037019001900

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU «

RFWBatr Number; 8907G580 Client; AVENDT GROUP Work Order; 5160-01-01-0001 P—e: IdCust ID: A12C 4-9

RFWI: 007

SBLK

89LE0635-MB1

4-Nitroquinoline-l-oxideMethapyrilene__________AramiteChlorobenzilate________p-Dimethylaminoazobenzene3,3' -Dimethy Ibenzidine__~_2-Acetylaminofluorene___7,12-Dimethylbenz(a)anthracene_Hexachlorophene____________3-Methylcholanthrene

660003300066000330003300033000330003300030000033000

UUUUUUUUUU

7403707403703703703703703400370

UUUUUUUUUU

(1) - Cannot be separated from Diphenylamine. *- Outside of EPA CLP QC limits.

Roy F. Weeton, Inc. - Lionville Laboratory


Cuet ID:

Sample RFWf;Information Matrix:

D.F.:Units:



2,4, 6-Tr ibromophenol

Phenolbis ( 2-Chloroethyl ) ether2-Chlorophenol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis ( 2-Chloroisopropyl ) ether4-MethylphenolN-Nitroso-Di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbis (2-Chloroethoxy) methane2 , 4-Dichlorophenol1,2, 4-Tr ichlorobenzeneNaphthalene4-chloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene

Semivolatiles byClient: AVENDT GROUP

'MS,

A10 15-17 A10 15-17

004 004 MSSOIL SOIL1.11 1.11

ug/Kg ug/Kg

738386766978

500500500500210500585005005005005005005005005002500500500500130140500500500500

1uuuuJuJuuuuuuuuuuuuuJJuuuu

698188746886

865007250047500505005005006950050050050050025005005006712013050078500500

=fl==

U

U

UJUUU

uuuuuuuu

JJu

uu

Appendix IX List Report Date: 08/09 " 13:45Work Order: 5160-01-01-0001 je: la

A10 15-17

004 MSDSOIL1.11

ug/Kg

637090696481

8049066490374902649049049062490490490490490250049049061667149077490490

-fl-

U

U

UJUUU

U-UUUUUUU

JJU

UU

A12B 3-7 SBLK

010 89LE0635-MB1SOIL SOIL27.8 1.11

ug/Kg ug/Kg

DDDDDD

190001900019000320058000

f 19000610019000190001900019000190001900019000190001900097000190001900012000190001300019000190001900019000

*

UuuJ

uJuuuuuuuuuuuuJuJuuuu

9083126737369

3703703703703703703703703703703703703703703703701900370370370370370370370370370

\

UUuuuuuuuuuuuuuuuuuuuuuuuu

*» Outside of EPA CLP QC limits.

^ RFWBat-' Number; 8907G611 Client; AVENDT GROUPCust ID: A10 15-17 AID 15-.

Work Order; 5160-01-01-0001A10 15-17 A12B 3-7 SBLK

P a q e t l b

RFWf! 004 .004 MS 004 MSD 010 89LE0635-MB1

2,4,6-Trichlorophenol2,4,5-Trichlorophenol2-Chloronaphthalene__2-NitroanilineDimethylphthalateAcenaphthylene__2,6-Dinitrotoluene3-Nitroaniline___~Acenaphthene_____2,4-Dinitrophenol4-Nitrophenol___Dibenrofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline__________4,6-Dlnitro-2-methylphenol_N-NitroBodiphenylamine (1)4-Bromophenyl-phenylether_Hexachlorobenzene_______Pentachlorophenol_______Phenanthrene___________AnthraceneDi-n-ButylphthalateFluoranthene______Pyrene___________Butylbenzylphthalate__3,3'-Dichlorobenzidine_Benzo(a)anthracene___Chrysene___________bis{2-Ethylhexyl)phthalateDl-n-Octyl phthalate_____~Benzo(b)fluoranthene_____Benzo(k)fluoranthene_____Benzo{a)pyrene__________Indeno(1,2,3-cd)pyrene_Dibenzo(a,h)anthraceneBenzo(g,h,ijperylene__1,4-Dioxane_________

500 U2500 U500 U2500 U500 U500 U500 U2500 U500 U2500 U2500 U500 U500 U500 U500 U500 U2500 U2500 U110 J500 U500 U80066500 U55 JB500 U500 U500 U1000 U500 U500 U75 J500 U500 U500 U500 U500 U500 U500 U500 U

JJ


500 U2500 U500 U2500 U500 U500 U500 U2500 U95 %2500 U107 %500 U78 %500 U500 U500 U2500 U2500 U190 J500 U500 U7272500 U120 JB500 U97 %500 U990 U500 U500 U310 J500 U500 U500 U500 U500 U500 U500 U500 U

%J

490250049025004904904902500862500108490794904904902500250012049049057514901404909949099049049070490490490490490490490490

U0UUUUUU

U%UUUUUJUU%JUJBU%0UUUJUUUUUUUU

19000 U97000 U19000 U97000 U19000 U19000 U19000 U97000 U19000 U97000 U97000 U19000 U19000 U19000 U19000 U19000 U97000 U97000 U19000 U19000 U19000 U97000 U3000 J19000 U19000 03900 J4700 J19000 U39000 U19000 U19000 U3400 J19000 U19000 U19000 U19000 U19000 019000 U19000 U19000 U

370 U1900 U370 U1900 U370 U370 U370 U1900 U370 U1900 U1900 U370 U370 U370 U370 U370 U1900 U1900 U370 U370 U370 U1900 U370 U370 U57 J370 U370 U370 U740 U370 U370 U370 U370 U370 U370 U370 U370 U370 U370 U370 U

'R W Bate* Number: 8907G611Gust ID:

RFWf :

Methyl methacrylatePyridineN-NitrosodimethylamineEthyl methacrylate2-PicolineN-NitroBomethylethylajnineMethyl methanesulfonateN-NitrosodiethylainineEthyl methanesulfonateAnilinePentachloroethane3-MethylphenolN-NitroaopyrrolidineAcetophenoneN-Nitrosomorpholineo-ToluidineN-Nitrosopiperidinea, a-Dimethylphenethylamine2 , 6-DichlorophenolHexachloropropenep-PhenylenediamineN-Nitroso-di-n-butylamineSafrole1,2,4, 5-Tetrachlorobenzenelaoaafrole1 , 4-Naphthoquinone1 , 3-DinitrobenzenePentachlorobenzene1-Naphthylamine2-Naphthylamine2,3,4, 6-Tetrachlorophenol1,3, 5-TrinitrobenzeneDiallatePhenacetinDiphenylamine5-Nitro-o-toluidine4-AminobiphenylPronamide2-sec-Butyl-4 , 6-dinitrophenolPentachloronitrobenzene*- Outside of EPA CLP QC limits.

Client: AVENDT GROUP Work Order: 5160-01-01-0001AID 15-17 AID 15-: A10 15-17

004 .004 MS 004 MSD

500500500500500500500500500500500500500130500500250050050050050050050050050050050050050050050050050050011050050050025002500

UUUUUUUUUUUUUJUUUUUUUUUUUUUUUUUUUUJUUUUU

50050050050050050050050050050050050050098500500250050050050050050050050050050050050050050050050050050019050050050025002500

UUUUUUUUUUUUUJUUUUUUUUUUUUUUUUUUUUJUUUUU

49049049049049049049049049049049049049080490490250049049049049049049049049049049049049049049049049049012049049049025002500

UUUUUUUUUUUUUJUUUUUUUUUUU-0UUUUUUUUJUUUUU

Pf>ne: IcA12B 3-7 SBLK

010 89LE0635-MB1

190001900019000190001900019000190001900019000190001900019000190001900019000190009700019000

f 1900019000190001900019000310019000190001900044001900019000190001900019000190001900019000190001900097000970dO

UUUUUUUUUUUUUUUUUUUUUUUJUUUJUUUUUUUUUUUU

370370370370370370370370370370370370370370370370190037037037037037037037037037037037037037037037037037037037037037019001900

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

RFW Bat Number: 8907G61103 Cust ID:

RFWI:

4-Nitroqu inol ine- 1-ox ideMethapyrileneAramiteChlorobenzilatep-Dimethylaminoazobenzene3,3' -Dimethylbenzidine2-Acetylaminof luorene7 , 12-Dimethy Ibenz ( a ) anthracene ___Hexachlorophene3-Methylcholanthrene

Client: AVENDT GROUP WorkAID 15-17 A10 15-1, _- A10 15-17

004 004 MS 004 MSD

100050010005005005005005004500500

UUUUUUU0UU

9905009905005005005005004500500

UUUUUUUUUU

9904909904904904904904904400490

UUUUUUUUUU

Order: 5160-01-01-0001 F -: IdA12B 3-7 SBLK

010 89LE0635-MB1

390001900039000190001900019000190001900017000019000

UUUUUUUUUU

7403707403703703703703703400370

UUUUUUUUUU

(1) - Cannot be separated from Diphenylamina. *= Outside of EPA CLP QC limits.

•J JRoy F. Weeton, IncSemivolatilee by

Lionville Laboratory.'MS, Appendix IX List Report Date: 08/0: ) 18:20

Work Order; 5160-01-01-0001_______Page; la^>

Cust ID: A21C 4-8 A23A 19-20

Sample RFWf: 001 007Information Matrix: SOIL SOIL

D.F.: 27.8 11.1Units: ug/Kg ug/Kg

Nitrobenzene-d5 DSurrogate 2-Fluorobiphenyl DRecovery p-Terphenyl-d!4 D

Phenol-d5 D2-Fluorophenol D

2, 4, 6-Tribromophenol D

Phenolbis ( 2-Chloroethy 1 ) ether2-Chlorophenol1 , 3-Dichlorobenzene1,4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis ( 2-Chloroiaopropyl ) ether4-MethylphenolN-NitroBo-Di-n-propylamineHexachloroethaneNitrobenzeneleophorone2-Nitrophenol2 , 4 -Dimethyl phenolBenzoic acidbis (2-Chloroethoxy) methane2 , 4-Dichlorophenol1,2, 4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyc lopent adiene*- Outside of EPA CLP OC limits.

3300033000330003300013000330003300033000330003300033000330003300033000330003300017000033000330006000330003300033000330003300033000

= fl==UUUUJUUUUUUUUUUUUUuJuuuuuu

DDDDDD

38000540054005400

, 29008200061006005400120005400540054005400540055000

5400540095001500730005400540054005400

=fl=

UUUJ

JU

UUUUU

EUU

J

uuuu

A23A 19-20

007 DLSOIL55.5

ug/Kg

D %D %D %D %D %D %

===========£ 1=

NANANANANANANANANANANANANANANANA

280000NANANANANANANANANA

SBLK

89LE0635-MB1SOIL1.11

ug/Kg

9083126737369

3703703703703703703703703703703703703703703703701900370370370370370370370370370

~fl ——————— fl== — = ———— ==flUUUUUUUUUUUUUUUuuuuuuuuuuu

RFH Bat'-'i Number: 8907G645 Client: AVENDT GROUP Work Order: 5160-01-01-0001 Page: IbGust ID: A21C 4-8 A23A 19- A23A 19-20

CD -RFWf: 001 007 007 DL

2,4, 6-Tr ichlorophenol2,4, 5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2 , 6-Dinitrotoluene3-NitroanilineAcenaphthene2 , 4-Dinltrophenol4-NitrophenolDibenzofuran2 , 4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline4, 6-Dinitro-2-methylphenolN-Nitroaodiphenylamine (1)4-Bromophenyl-phenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo ( a ) anthraceneChrysenebis ( 2-Ethylhexyl ) phthalateDl-n-Octyl phthalateBenzo(b) f luorantheneBenzo(k) f luorantheneBenzo ( a ) pyreneIndeno (1,2, 3-cd ) pyreneDibenzo ( a , h ) anthraceneBenzo (g,h, i)perylene1,4-Dioxane

3300017000033000170000330003300033000170000330001700001700003300033000330003300033000170000170000330003300033000170000490033000330008100830033000670003300048006700730033000330003300033000330003300033000

UUUUUUUUUUUUUUUUUUUUUUJUUJJUUUJJJ0UUUUUU

54002700054002700054005400540027000540027000270005400540054005400540027000,27000540054005400270007105400290054005400620

11000540010002000054005400540054005400540054005400

UUUUUUUUUUU0UUUUUUUUUUJUJBUUJUUJ

UUUUUUUU

NANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANANA

SBLK

89LE0635-MB1

3701900370190037037037019003701900190037037037037037019001900370370370190037037057370370370740370370370370370370370370370370370

UUUUUUUUUUUUUUUU00UUUUUUJUUUUUUUUUUUUUUU

*«= Outside of EPA CLP QC limits.

RFW Batr1- Number: 8907G645 Client: AVENDT GROUP Work Order: 5160-01-01-0001 r ne: Ic*"*• Cust ID: A21C 4-8 A23A 19-: A23A 19-20

RFWf: 001 . 007 007 DL

c ————————————————— - ———--flethyl methacrylatePyridineN-NitroeodimethylamineEthyl methacrylate2-PicolineN-NitrosomethylethylamineMethyl methanesulfonateN-Nitrosodiethy laminaEthyl methanesulfonateAnilinePentachloroethane3-MethylphenolN-NitrosopyrrolidineAcetophenoneN-Nitroaomorpholineo-ToluidineN-Nitroeopiperidinea , a-Dimethylphenethylamine2 , 6-DichlorophenolHexachloropropenep-PhenylenediamineN-Nitroso-di-n-butylamineSafrole1,2,4, 5-TetrachlorobenzeneIsoaafrole1 , 4-Naphthoquinone1 , 3-DinitrobenzenePentachlorobenzene1-Naphthylamine2-Naphthylamine2,3,4, 6-Tetrachlorophenol1,3, 5-TrinitrobenzeneDiallatePhenacetinDiphenylamine5-Nitro-o-toluidine4-AminobiphenylPronamide2-aec-Butyl-4 , 6-dinitrophenolPentachloronitrobenzene*« Out Bide of EPA CLP OC limits.

33000330003300033000330003300033000330003300033000330003300033000330003300033000170000330003300033000330003300033000330003300033000330003300033000330003300033000330003300033000330003300033000170000170000


5400540054005400540054005400540054003600540012000540029005400540027000; 5400540054005400540054005400540054005400540054005400540054005400540054005400540054002700027000

UUUUUUUUUJU

UJUUUUUUUUUUUUUUUUUUUUUUUUUU


SBLK

89LE0635-MB1

370370370370370370370370370370370370370370370370190037037037037037037037037037037037037037037037037037037037037037019001900


Batfh Number; 8907G645 Client: AVENDT GROUP Work Order: 5160-01-01-0001 Id*** Cust ID:

RFWl :r(4-Nitroquinoline-l-oxideMethapyrileneAramiteChlorobenzilatep-Dimethylaminoazobenzene3,3'-Dimethylbenzidine2-Acetylaminof luorene7 , 12-Dimethylbenz ( a ) anthraceneHexachlorophene3-Hethylcholanthrene

A21C 4-8 A23A 19-

001 007

670003300067000330003300033000330003300030000033000

UUUUUUUUUU

1100054001100054005400540054005400490005400

A23A 19-20

007 DL

UUUUUUUUUU

NANANANANANANANANANA

SBLK

89LE0635-MB1

7403707403703703703703703400370

UUUUUUUUUU

(1) - Cannot be separated from Diphenylamine. * = Outside of EPA CLP QC limits.

if* Roy F. Weston, IncSemivolatilea by

Client! AVENDT GROUP

Lionville Laboratory/MS, Appendix IX List Report Dates 08/1 9 15s50

Work Order; 5160-01-01-0001_______Pages la

Gust ID:

Sample RFWfs/Information Matrix :

D.F.i\Units » \

Ni t roben zene-d 5Surrogate 2-FluorobiphenylRecovery p-Terphenyl-d!4


2,4, 6-Tr ibromophenol

Phenolbie ( 2-Chloroethyl ) ether2-Chlorophenol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbia ( 2-Chloroiaopropyl ) ether4-MethylphenolN-NitroBo-Di-n-propylamineHexachloroethaneNitrobenzeneiBophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbia ( 2-Chloroethoxy } methane2 , 4-Dichlorophenol1,2, 4-TrichlorobenreneNaphthalene4-Chloroanil ineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene*- Out aide of EPA CLP QC limits.

A22B 0-7 SBLK

\

005 89LE0635-MB1SOIL / SOIL111 / 1.11

ug/Kg / ug/Kg/

DDDDD

73000730007300073000340007300073000730007300073000730007300073000730007300073000370000730007300073000730007300073000730007300073000

S

UUu

uuuuuuuuuuuuuu0uuuuuu

9083126737369

3703703703703703703703703703703703703703703703701900370370370370370370370370370

UUOUUUUUOUUUUUUUUUUUUUUUuu

CDRFW Batch Number: 8907G660

Cust ID:

RFHf :

2, 4, 6-Trichlorophenol2,4, 5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2 , 6-Dinitrotoluene3-NitroanilineAcenaphthene2 , 4-Dinitrophenol4-NitrophenolOibenzofuran2 , 4-DinitrotolueneDlethylphthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline4 , 6-Dinitro-2-methylphenolN-Nitrosodiphenylamine ( 1 )4-Bromophenyl-phenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluor anthenePyreneButylbenzylphthalate3,3' -DichlorobenzidineBenzo ( a ) anthraceneChrysenebis ( 2-Ethylhexy 1 ) phthalateDi-n-Octyl phthalateBenzo ( b ) f luorantheneBenzo ( k) f luorantheneBenzo { a ) pyreneIndeno (1,2, 3-cd ) pyreneDibenzo ( a , h ) anthraceneBenzo ( g , h , i ) pery lene1,4-Dioxane*- Outside of EPA CLP QC limits.

Client:/A22B 0-7

I 005\ /V73000370000730003700007300073000730003700007300037000037000073000730007300073000730003700003700007300073000730003700001400073000730007300010000730001500007300073000730007300073000730007300073000730007300073000

AVENDT GROUP Work Order: 5160-01-01-0001 -ae: IbSBLK

/ 89LE0635-MB1

UUUUUUUUUUUUUUUUUUUUUUJ 'UUUJ 'UUUUUUUUUUUUU

37019003701900370370370190037019001900370370370370370190019003703703701900

J 37037057

. 370P/01 370

370740370370370370370370370370370370370

U0UUa000UUUUU00UUUUUUUUUJUUUUUUUDUUUUDUD

RFH Batch Number: 8907G660Cust ID:

RFWfi

Methyl methacrylatePyridineN-NitroBodlmethylamineEthyl methacrylate2-PicoltneN-NitroBomethylethylamineMethyl methanesulfonateN-NitroBodiethylamineEthyl methanesulfonateAnilinePentachloroethane3-MethylphenolN-NitroaopyrrolidineAcetophenoneN-NitroBomorpholineo-ToluidineN-Nitrosopiperidinea, a-Dimethylphenethylamine2 , 6-DichlorophenolHexachloropropenep-PhenylenediamineN-NitroBO-di-n-butylamineSafrole1,2,4, 5-TetrachlorobenzeneiBosafrole1 , 4-Naphthoquinone1 , 3-DinitrobenzenePentachlorobenzene1 -Napht hy 1 amine2 -Napht hy 1 amine2,3,4, 6-Tetrachlorophenol1,3, 5-TrinitrobenzeneDiallatePhenacetinDiphenylamine5-Nitro-o-toluidine4-AminobiphenylPronamide2-Bec-Butyl-4 , 6-dinitrophenol ____Pentachloronitrobenzene*- Outside of EPA CLP QC limits.

Client:A22B 0-7

005

73000730007300073000730007300073000730007300073000730007300073000730007300073000370000730007300073000730007300073000730007300073000730007300073000730007300073000730007300073000730007300073000370000370000

AVENDT GROUP Work Order: 5160-01-01-0001 *>-*ae: IcSBLK

89LE0635-MB1

UUU0UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

370370370370370370370370370370370370370370370370190037037037037037037037037037037037037037037037037037037037037037019001900

UUUUUUUOUUUUUUUUUUUUOUUUUUUUUUUUUUUUUUUU

CORFW Batch Number: 8907G660

Gust ID:

RFWf :

4-Nitroquinoline-l-oxideMethapyrileneAramiteChlorobenzilatep-Dimethylaminoazobenzene3,3' -Dlmethy Ibenzidine2-Acetylaminof luorene7 , 12-Dimethy Ibenz ( a ) anthracene ___Hexachlorophene3-Methylcholanthrene

Client: AVENDT GROUPA22B 0-7

005

150000 U73000 U150000 U73000 073000 U73000 U73000 U73000 U660000 U73000 U

Work Order: 5160-01-01-0001 Page: IdSBLK

89LE0635-MB1

7403707403703703703703703400370

UUU0OUUUUU

(1) - Cannot be separated from Diphenylamine. *= Outside of EPA CLP QC limits.

CDRFW Batch Number; B907G709

Roy F. Western, Inc Lionville LaboratorySemivolatiles by_.-/MS, Appendix IX List Report Date: 08/1 ) 11:44

Client; AVENDT GROUP______________Work Order; 5160-01-01-0001________*»aqe; la

Cust ID:


D.F. :Units:




Phenolbis ( 2-Chloroethy 1 ) ether2 -Ch loropheno 11 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis ( 2-Chloroisopropyl ) ether4-MethylphenolN-Nitroso-Di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbis (2-Chloroethoxy) methane2 , 4-Dichlorophenol1,2, 4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene*- Out Bide of EPA CL.P OO lim<t-n.

All B4-8 All C2-6.5

001 005SOIL SOIL11.1 11.1

ug/Kg ug/Kg

7593116867$64

720570057005700570057005700570057005700570057005700570057001600280005700570057005700170005700570057005700

JBUUUUUUUUUUUUUUJUUUUU

UUUU

DDDDDD

4700470047004700

, 36004700840470047004700470047004700470047004700240004700470088008509400470047006004700

==fl==UUUUJBUJBUUUUUUUUU0UUBJ

UUJU

A16 B9-12

017SOIL111

ug/Kg

DDDDDD

610000990009900032000390000990006500009900099000990009900099000990009900099000990004900009900099000160000990009900099000990009900099000

==flBUUJ ,BUBUUUUUUUUUUUUBUUUUUU

A16 C2-5i

020 /SOIL27.8

ug/Kg

DDDDDD

2100026000260002300026000026000

26000260002600026000260002600026000260002600013000026000260001200056001400026000260002600026000

==fl===JBUUJBUEUUUUUUUUUUUUJBJJ v

UUUU

A16 C2-5 A16 C2-5

020 DL 020 MSSOIL SOIL55.5 55.5

ug/Kg ug/Kg

DDDDDD

NANANANANANA

360000NANANANANANANANANANANANANANANANANANANA

% D% D% D% D% D% D

==fl= —— —— ——D

56000D

23000D

56000B 560000

560005600056000D

56000560005600056000560002800005600056000D

56000720056000D

5600056000

==fl

U

J

UBUUU

UUUUUUUU

UJU

UU

RFW B- Number: 8907G709 Client: AVENDT GROUPGust ID: All B4-8 All C2-t^_

RFWl: 001 005

2,4, 6-Trichlorophenol2,4, 5-Tr ichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2 , 6-Dinitrotoluene3-NitroanilineAcenaphthene2 , 4-Dinitrophenol4-NitrophenolDibenzofuran2 , 4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline4, 6-Dinitro-2-methylphenolN-NitroBodiphenylamine (1)4-Bromophenyl-phenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButylbenzylphthalate3,3' -DichlorobenzidineBenzo ( a ) anthraceneChrysenebis ( 2-Ethylhexy 1 ) phthalateDi-n-Octyl phthalateBenzo ( b ) f luorantheneBenzo ( k ) f luorantheneBenzo ( a ) pyreneIndeno (1,2, 3-cd ) pyreneDibenzo ( a , h ) anthraceneBenzo ( g , h , i ) pery lene1,4-Dioxane

57002800057002800057005700570028000570028000280005700570057005700570028000280005700570057002800057005700110057QO570057001100057005700570057005700570057005700570057005700

UUUUUUUUUUUUUUUUUUUUUUUUJBUUUUUUUUUUUUUUU

47002400047002400047004700470024000470024000240004700470047004700470024000.2400047004700170024000670470011005405404700950047004700470047004700470047004700470047004700

UUUUUUUUUUUUUUUUUUUUJUJUJBJJUUUU0UUUUUUUU

WorkA16 B9-12

017

99000490000990004900009900099000990004900009900049000049000099000990009900099000990004900004900009900099000990004900009900099000990009900099000700002000009900099000260009900099000990009900099000990009900099000

UUUUUUUUUUUUUUUUUUUUUUUUUUUJBUUUJBUUUUUUU0

Order: 5160-01-01-0001A16 C2-5

020

2600013000026000130000260002600026000130000260001300001300002600026000260002600026000130000130000420026000260001300005400260002600036004200

10000051000260005700260001800026000260002600026000260002600026000

UUUUUUUUUUUUUUUUUUJUUUJUUJJBUUJUJBUUUUUUU

A16 C2-5

020 DL


qe: IbI C2-5

020 MS

5600028000056000280000560005600056000280000

D280000

D56000D

560005600056000280000280000560005600056000D5400560005600056000D

150000110000560006900560002600056000560005600056000560005600056000

UUUUUUUU%U%U%UUUUUUUU%JUUU%BUUJUJBUUUUUUU

*- Outside of EPA CLP QC limits.

00 RFW B?' Number: 8907G709 Client; AVENDT GROUP Work Order; 5160-01-01-0001 IcCust ID:

RFWf :

Methyl methacrylatePyridineN-Nitro8odimethylamineEthyl methacrylate2-PicolineN-NitroaomethylethylamineMethyl methanesulfonateN-NitroBodiethylamineEthyl methanesulf onateAnilinePentachloroethane3-MethylphenolN-NitroBopyrrolidineAcetophenoneN-NitroBomorpholineo-ToluidineN-Nitrosopiperidinea,a-Dimethylphenethylamine2 , 6-DichlorophenolHexachloropropenep-PhenylenediamineN-Nitroso-di-n-butylamineSafrole1,2,4, 5-TetrachlorobenzeneIsoeafrole1 , 4-Naphthoquinone1 , 3-DinitrobenzenePentachlorobenzene1-Naphthylamine2-Naphthylamine2,3,4, 6-Tetrachlorophenol1,3, 5-Tr initrobenzeneDiallatePhenacetinDiphenylamine5-Nitro-o-toluidine4-AminobiphenylPronamide2-aec-Butyl-4 , 6-dinitrophenol ___Pentachloronitrobenzene

: All B4-8 All C2-6 _

001 005

5700570057005700570057005700570057005700570057005700570057005700280005700570057005700570057005700570057005700570057005700570057005700570057005700570057002800028000

U0UUUUUUUUUU0U0UUUUUuuuuuuuuuuuuuuu0uuuu

470047004700470047004700470047004700470047004700470013004700470024000... 470047004700470047004700190004700470047001300047004700470047004700470047004700470047002400024000

UUUUUUUUUUUUUJBUUUUUUUUU

Uuu

uuuuuuuuuuuu

A16 B9-12

017

99000990009900099000990009900099000990009900099000990009900099000990009900099000490000990009900099000990009900099000190009900099000990003700099000990001000099000990009900099000990009900099000490000490000

UUUUUUUUUUUUUUUUUUuuuuuJuuuJuuJ'uuuuuuuuu

A16 C2-5

020

260002600026000260002600026000260002600026000260002600026000260004300260002600013000026000260002600026000260002600026000260002600026000260002600026000260002600026000260004200260002600026000130000130000

UUUUUUUuuuuuuJBUUUUuuuuuuuuuuuuuuuuJuuuuu

A16 C2-5

020 DL


A -2-5

020 MS

56000560005600056000560005600056000560005600056000560005600056000560005600056000280000560005600056000560005600056000560005600056000560005600056000560005600056000560005600056000560005600056000280000280000

UUUUUUUUUUuuuuuuuuuuuuuuuuuuuuuuuu0uuuuu


RFW Bai- ' Number: 8907G709 Client: AVENDT GROUPCust ID: All B4-8

RFW#: 001

4-Nitroquinoline-l-oxideMethapyrileneAramiteChlorobenzilatep-Dimethylaminoazobenzene3,3' -Dimethy Ibenzid tne2-Acetylaminof luorene7 , 12-Dimethy Ibenz ( a ) anthraceneHexachlorophene3-Methylcholanthrene(1) - Cannot be separated from

1100057001100057005700570057005700510005700

Diphenylamine.

Work Order: 5160-01All C2-6 A16 B9-12 A16 C2-5

005 017 020

U0UUUUUUUU

* =

95004700950047004700470047004700430004700

Outside

UUUUUUUUUU

of EPA

20000099000200000990009900099000990009900089000099000

CLP QC

UUUUUUUUUUlimits.

510002600051000260002600026000260002600023000026000

UUUUUUUUUU

-01-0001A16 C2-5

020 DL

NANANANANANANANANANA

~ -qe:A J2-5

- 020 MS

11000056000110000560005600056000560005600051000056000

Id

UUUUUUUUUU

Roy F. Western, Inc. - Lionville Laboratory

RFW Batcn Number: 8907G709

Gust ID:

Sample RFWf:Information Matrix:

D.F.:Units:




Phenolbis ( 2-Chloroethy 1 ) ether2-Chlorophenol1 , 3-Dichlorobenzene1 , 4-DichlorobenzeneBenzyl alcohol1 , 2-Dichlorobenzene2-Methylphenolbis ( 2-Chloroisopropyl ) ether4-MethylphenolN-NitroBO-Di-n-propylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2 , 4-DimethylphenolBenzoic acidbis ( 2-Chloroethoxy ) methane2 , 4-Dichlorophenol1,2, 4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-methylphenol2-MethylnaphthaleneHexachlorocyclopentadiene*» Outside of EPA CLP QC limits.

Semivolatiles byClient: AVENDT GROUP

'MS, Appendix IX Liet Report Date: 08/1 11:44— Work Order: 5160-01-01-0001 . »qe: 2a

A16 C2-5 SBLK

020 MSD 89LE0659-MB1SOIL SOIL55.5 1.11

ug/Kg ug/Kg

DDDDDD

D60000

D ,24000D

60000560000600006000060000D

60000600006000060000600003000006000060000D

600001200060000D

6000060000

U

J

UBUUU

UUUUUUUU

UJU

uu

444557393640

26037037037015003702700370370370370370370370370370420370370110370370370370370370

JUUU

U

UUUUUUUUUJUUJUUUUUU

RFW Bat' Number: 8907G709Cuat ID:

RFW#:

2,4, 6-Trichlorophenol2,4, 5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2 , 6-Dinitrotoluene3-NitroanilineAcenaphthene2 , 4-Dinitrophenol4-NitrophenolDibenzofuran2 , 4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-Nitroaniline4 , 6-Dinitro-2-methylphenolN-NitroBodiphenylamine (1)4-Bromophenyl-phenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButylbenzylphthalate3 , 3 '-DichlorobenzidineBenzo ( a ) anthraceneChryeenebie ( 2-Ethy Ihexyl ) phthalateDi-n-Octyl phthalateBenzo (b) f luorantheneBenzo ( k ) £ luorantheneBenzo(a)pyreneI ndeno ( 1 , 2 , 3 -cd ) pyreneDibenzo ( a , h ) anthraceneBenzo (g,h, i)perylene1,4-Dioxane*« Outside of EPA CLP OC limitn.

Client:A16 C2-5

020 HSD

6000030000060000300000600006000060000300000

D300000

D60000D

600006000060000300000300000600006000060000D5300600006000060000D

150000120000600005600230002700060000600006000060000600006000060000

AVENDT GROUP Work Order: 5160-01-01-0001 P=>qe: 2bSBLK

89LE0659-MB1

UUUUUUUU%U%U%UUUUUUUU%JUUU%BUUJJBJBUUUUUUU

370180037018003703703701800370180018003703703703703701800

, 1800

370370370180037037055370370740740370370320130370370370370370370370

UUUUUUUUUUUUUUUUUUUUUUUUJUU

UUUJJUUUUUUU

RFW Bat-' Number: 8907G709Cust ID:

RFWf :

Methyl methacrylatePyridineN-NitrosodimethylamineEthyl methacrylate2-PicolineN-NitrosomethylethylamineMethyl methanesulfonateN-NitroBodiethylamineEthyl methanesulfonateAnilinePentachloroethane3-MethylphenolN-NitrosopyrrolidineAcetophenoneN-N it rosomor pho 1 ineo-ToluidineN-Nitrosopiperidinea, a-Dimethylphenethylamine2 , 6-DichlorophenolHexachloropropenep-PhenylenediamineN-NitroBo-di-n-butylamineSaf role1,2,4, 5-TetrachlorobenzeneiBosaf role1 , 4-Naphthoquinone1 , 3-DinitrobenzenePentachlorobenzene1-Naphthylamine2-Naphthylamine2,3,4, 6-Tetrachlorophenol1,3, 5-Tr initrobenzeneDiallatePhenacetinD ipheny 1 amine5-Nitro-o-toluidine4-AminobiphenylPronamide2-sec-Butyl-4, 6-dinitrophenol ____Pentachloronitrobenzene*- Outside of EPA CLP QC limits.

Client:A16 C2-5

020 MSD

60000600006000060000600006000060000600006000060000600006000060000600006000060000300000600006000060000600006000060000600006000060000600006000060000600006000060000600006000060000600006000060000300000300000

AVENDT GROUP Work Order: 5160-01-Ui-UUUi i UM>- .SBLK

89LE0659-MB1


3703703703703703703703703703703703703702303703701800

, 37037037037037037037037037037037037037037037037037037037037037018001800

UUUUUU0UUUUU0JUUUUUUUUUUUUUUUUUUUUUUUUUU

RFW BP Number; 8907G709 Client: AVENDT GROUP Work Order; 5160-01-01-0001 2dGust ID: A16 C2-5

RFWf: 020 MSD

4-Nitroquinoline-l-oxideMethapyrlleneAramiteChlorobenzilatep-Oimethylaminoazobenzene3,3' -Dimethylbenzidine2-Acetylamtnof luorene7, 12-Dimethylbenz( a) anthraceneHexachlorophene3-Methylcholanthrene(1) - Cannot be separated from

12000060000120000600006000060000600006000054000060000

Diphenylamine .

SBLK ^

89LE0659-MB1

U0UUUUUUUU

* =

7403707403703703703703703300370

Outside

UUUUUUUUUUof EPA CLP QC limits.

V.-- _ _ ______ _ _____ ___ _WESTON-GULF CO/-bi LA3OP.AV(. i - ,L i i . iu(.

2417 Bond St., University Park. Illinois 60466

Phones: (312) 534-5200 (219)885-7077 (815)723-753:

August 23, 1989


Dear Mr. Bade:

Please find enclosed the VGA portion of the reports for the samplessubmitted to Weston/Gulf Coast Laboratories for analyses. They wereanalyzed by Lionville Analytics. They were identified with ourbatch numbers 8907G520, 8907G528, 8907G580, 8907G611, 8907G645,8907G660 and 8907G709. If you have any questions, please contactSheryl Johnson or Lynn Gifford at our laboratories.

Sincerely,



igEnclosures

RFW Batch Number; 8907G611

Roy F. Weeton, In - Lionville LaboratoryVolatiles by Gt/MS, Appendix IX List Report Date: 08/Oo/89 15:50

Client; AVENDT GROUP_____________Work Order; 5160-01-01-0001_______Page; la

Cust ID: 10 15-17 10 15-17 A12B 3-7 VBLK

SampleInformation

RFWl:Matrix:D.F. iUnite:Level:

004SOIL1.25

UG/KGMED

004SOIL1.25

UG/KGMEDREPREP

010 89LVY178-MB1SOIL SOIL12.5 1.25

UG/KG UG/KGMED MED

Toluene-d8Surrogate BromofluorobenzeneRecovery l,2-Dichloroethane-d4

Chloromethane________________Br omomet h a ne_________________Vinyl Chloride________________ChloroethaneMethylene ChlorideAcetoneCarbon Dieulfide_________1,1-Dichloroethene______1.1-Dichloroethane______1.2-Dichloroethene (total)Chloroform1,2-Dichloroethane_2-Butanone1,1,1-TrichloroethaneCarbon Tetrachloride_Vinyl Acetate_______Bromodichloromethane1,2-Dichloropropane_cia-1,3-Dichloropropene_TrichloroetheneDibromochloromethane_1,1,2-TrichloroethaneBenzeneTrans-1,3-Dichloropropene_Bromoform4-Methyl-2-pentanone_2-HexanoneTetrachloroethene___________1,1,2,2-Tetrachloroethane______*- Outside of EPA CLP QC limits.

130 * %117 %134 * %

========fl=1700 U1700 U1700 U1700 U1600 B1700 U840 U840 U840 U840 U840 U840 U1700 U840 U840 U1700 U840 U840 U840 U740 J840 U840 U840 U840 U840 U1700 U1700 U840 U840 U

123 * %115 %126 * %

=======fl=1700 U1700 U1700 U1700 U2400 B3300 B840 U840 U840 U840 U840 U840 U1700 U840 U840 U1700 U840 U840 U840 U730 J840 U840 U840 U840 U840 U1700 U1700 U840 U840 U

147 * %163 * %160 * %

=========fl===26000 U26000 U26000 U26000 U25000 B22000 JB13000 U13000 U13000 U13000 U13000 U13000 U26000 U13000 U13000 U26000 U13000 U13000 U13000 U13000 U13000 U13000 U13000 U13000 U13000 U26000 U26000 U13000 U13000 U

106 %102 %89 %

========fl=1200 U1200 U1200 U1200 U1400810 J620 U620 U620 U620 U620 U620 U1200 U620 U620 U1200 U620 U620 U620 D620 U620 U620 U620 U620 U620 U1200 U1200 U620 U620 U

=fl

RFW B h Number; 8907G611 Client! AVENDT GROU Work Order; 5160-01-01-0001 age; IbCust ID:

RFWf :Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneDichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneiBobutyl alcohol1,2-Dibromoethane1, 1, 1,2-Tetrachloroethane1,2, 3-Trichloropropanetrans-1 , 4-Dichloro-2-butenel,2-Dibromo-3-chloropropane2-Chloro-l, 3-Butadiene*- Outside of EPA CLP QC limits.

10 1.5-17

004MED

640650960840840

17001700840

17003400460840034003400170034003400170017008400340017000

UJ

UUUUUUUJUUUUUUUUUUU

10 IS-^,

004MEDREPREP840670

1100840440

170017008401700340040084003400340017003400

. 3400170017008400340017000

UJ

U

UUUUUJUUUUUUUUUUU

A12B 3-7 VBLK

010 89LVY178-MB1MED MED

130005200360013000130002600026000130002600052000260001300005200052000260005200052000260002600013000052000260000

UJJUUUUUUUUUUUUUUUUUUU

, 620620620620620

12001200150

120025001200620025002500120025002500120012006200250012000

UUUUUUUJUUUUUUUUUUUUUU

LO


Roy F. Weeton, Inr - Lionville LaboratoryVolatiles by C,_rfS, Appendix IX List Report Date: 08/L J9 14:29

Client; AVENDT GROUP __ _ Work Order; 5160-01-01-0001_______Page; la

Gust ID:


D.F. :Unite:Level:

Toluene-d8Surrogate Bromof luorobenzeneRecovery l,2-Dichloroethane-d4

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecia-1 , 3-DichloropropeneTrichloroetheneDibromochloromethane1,1, 2-TrichloroethaneBenzeneTrana-1 , 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane*- Outside of EPA CLP QC limits.

A12C 4-9 VBLK

007 89LVY175-MB1SOIL SOIL .1.25 1.25

UG/KG UG/KGMED MED

79 * % 103 %80 % 104 %87 % 107 %

4500 U 1200 U4500 U 1200 U4500 U 1200 U4500 U 1200 U5400 B 17004500 B 1100 J2200 U , 620 U2200 U 620 U2200 U . 620 U2200 U 620 U2200 U 620 U2200 U . 620 U4500 U 1200 U2200 U 620 U2200 U 620 U4500 U 1200 U2200 U 620 U2200 U 620 U2200 U 620 U2200 U 620 U2200 U 620 U2200 U 620 U2200 U 620 U2200 U 620 U2200 U 620 U4500 U 1200 U4500 U 1200 U2200 U 620 U2200 U 620 U

RFW B h Number; 8907G580 Client; AVENDT GROU' Work Order; 5160-01-01-0001 IbGust ID:

RFWt:Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneDichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromome thaneIsobutyl alcohol1 , 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Trichloropropanetrans-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l, 3-Butadiene*= Outside of EPA CLP QC limits.

A12C 4-9 VBLK —

007 89L.VY175-MB1MED MED

690460022002200220045004500220045008900170022000890089004500890089004500450022000890045000

J

UUUUUUUUJUUUUUUUUUUU

6206206206206201200120062012002500120062002500250012002500

i 2500120024062002500

, 12000

UU ;UUUUUUUUUUUUUUUUJUUU

10RFH Batch Number; 8907GS28

Roy F. Western, Inc.Volatiles by Gc

Client: AVENDT GROUP

Lionville LaboratoryJ, Appendix IX List Report Date: 08/K 10:26

Work Order; 5610-01-01-0001 _______ Page; la

Cuat ID: A13B4.5-6 A13B4.5-6 A14C8.5-10.5 A14C8.5-10.5 A14C8.5-10.5 VBLK

Sample RFWl : 001Information Matrix: SOIL

D.F.: 1.25Unite: UG/KGLevel: MED

Toluene-d8 73 * %Surrogate Bromof luorobenzene 80 %Recovery l,2-Dichloroethane-d4 83 %

Chloromethane 3400 UBromome thaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Dieulfide1 , 1-Dichloroethene1, 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethaneIf 2-DichloropropaneciB-1 , 3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzeneTrans-1 , 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroetheneIf 1,2,2-Tetrachloroethane

38034003400440024001700170017001700170017003400170017003400170017001700170017001700170017001700340034003801700

JUUBJBUUUUUUUUUUUUUUUUUUUUUJU

001SOIL1.25

UG/KGMEDREPREP93 %103 %116 %

3400 U3400 U3400 U3400 U6200 B3400 U

i. 1700 U1700 U1700 U1700 U1700 U1700 U3400 U1700 U1700 U3400 U1700 U1700 U1700 U1700 U1700 U1700 U23001700 U1700 U3400 U3400 U1700 U1700 U

010SOIL1.26

UG/KGMED

858887

1700170017001700250013008508508508508508501700850850170085085085085085085085085085017001700680850

010 MSSOIL1.25

UG/KGMED

% 108% 93% 108

==fl===========U 1700U 1700U 1700U 1700B 2400JB 2600U 840U 87U 840U 840U 840U 840U 1700U 840U 840U 1700U 840U 840U 840U 95U 840U 840U 90U 840U 840U 1700U 1700J 840U 840

:=fl= = :

UUUUBBU

UUUUUUUUUUU

UU

UUUUUU

010 MSD 89LVY175-MB1SOIL SOIL1.25 1.25

UG/KG UG/KGMED MED

95 %82 %102 %

==========fl==:1700 U1700 U1700 U1700 U1600 B1700 U840 U75 %840 U840 U840 U840 U1700 U840 U840 U1700 U840 U840 U840 U84 %840 U840 U73 %840 U840 U1700 U1700 U840 U840 U

103 %104 %107 %

==========fl1200 U1200 U1200 U1200 U17001100 J620 U620 U620 U620 U620 U620 U1200 U620 U620 U1200 U620 U620 U620 U620 U620 U620 U620 0620 U620 U1200 U1200 U620 U620 U

oo

RFW Bf Number: 8907G528Gust ID:

RFWf :Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAery lonit rileTrichlorof luoromethaneDichlorodif luoromethaneAcetonitr i lelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneleobutyl alcohol1,2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Tr ichloropropanetrans-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l , 3-Butadiene*- Outside of EPA CLP QC limits.

Client: AVENDT GROUPA13B4.5-6

001MED

170021001400170046034003400170069006800180017000680068003400680068003400340017000680034000

U

JUJUUU

UJUUUUUUUUUUU

Work Order: 5610-01-01-0001 ie: IbA13B4.5_ A14C8.5-10.5 A14C8.5-10.5 A14C8.5-10.5 V

001 010 010 MS 010 MSD 89LVY175-MB1MED MED MED MED MEDREPREP5703700270017001700340034001700340068003400170006800680034006800

. 680034003400170006800

. 34000

J

UUUUUUUUUUUUUUUUUUU

85057085085085017001700170170034001300850034003400170034003400170017008500340017000

UJUUUUUJUUJUUUUUUUUOUU

, 929484084084017001700200170034001700840034003400170034003400170017008400340017000

UUUUUJBUUUUUUUUUUUUUU

80838408408401700170084017003400690840034003400170034003400170017008400340017000


6206206206206201200120062012002500120062002500250012002500250012002406200250012000

UUUUUUUUUUUUUU0UUUJUUU

Roy F. Weston, IncVolatilen by

Lionville Laboratory, Appendix IX List Report Date: 08/1, i 10:26


Cust ID:

Sample RFW I :Information Matrix:

D.F. :Units:Level :


ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecis-1 , 3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1, 2-TrichloroethaneBenzeneTrane-1 , 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane*- Ouflde of EPA CLP QC limits.

Client: AVI

VBLK

89LVY177-MB1SOIL1.25

UG/KGMED

88 %88 %99 %

= = = = :==::==: = = = f]

1200 U1200 U1200 U1200 U17002300620 U620 U620 U620 U620 U620 U1200 U620 U620 U1200 U620 U620 U620 U620 U620 U620 U620 U620 U620 U1200 U1200 U620 U620 U

ENDT GROUP Work Order: 5610-01-01-0001 Paqe: 2a

VBLK


UG/KGMED

106 %102 %89 %

1200 U1200 U1200 U1200 U1400810 J

^ 620 U620 U620 U620 U620 U620 U1200 U620 U620 U1200 U620 U620 U620 U620 U620 U620 U620 U620 U620 U1200 U1200 U620 U620 U

RFW Be Number: 8907G528rjQ CuBt ID:

OO RFWt:

Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneOichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneleobutyl alcohol1 , 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Tr ichloropropanetrans-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l,3-Butadiene*= Outside of EPA CLP QC limits.

Client: AVENDT GROUPVBLK .

89LVY177-MB1MED

62062062062062012001200620

120025001200620025002500120025002500120012006200250012000

UUUUUUUUUUUUUUUUUUU0UU

Work Order: 5610-01-01-0001 P^qe: 2bVBLK _

89LVY178-MB1MED

620620620620620

12001200150

12002500120062002500250012002500

12500120012006200250012000


Roy F. Weston, Inc Lionville LaboratoryVolatiles by G._ S, Appendix IX List Report Date: OB/1 J 14:51

Work Order; 5610-01-01-0001_______Page;

Cuet ID: A15B 6-9

Sample RFWf: 001Information Matrix: SOIL

D.F.: 4.50Units: UG/KGLevel: LOW

Toluene-d8Surrogate BromofluorobenzeneRecovery 1 , 2-Dichloroethane-d4

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecie-1 , 3-DichloropropeneTrichloroetheneDibromochloromethane1,1, 2-TrichloroethaneBenzeneTrans-1 , 3-DichloropropeneBromoform4 -Methyl-2 -pent anone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane

122 * %100 %99 %

6868686848683434344634346834346834343434343414343468683434

UUUUBUUUU

UUUUUUUUUUUUJUUUUUU

A15B 6-9

001SOIL1.27

UG/KGMED

102106107

190019001900190023002300

•> 9609609609609609601900960960190096096096096096096096096096019001900960960

'-fi-llUUUBBUUUUUUUUUUUUUUUUUUUUUUU

A15B 6-9

001 MSSOIL4.33UG/KGLOW

A15B 6-9 A15C 4.5-9

001 MSD 005 DLSOIL SOIL4.26 4.83UG/KG UG/KGLOW LOW

111 % 117 %106 % 110 %106 % 107 %

66 U 64 U66 U 64 U66 U 64 U66 U 64 U87 B 73 B66 U 14 J33 U 32 U96 % 97 %33 U 8 J21 J 5733 U 32 U33 U 32 U66 U 64 U33 U 32 U33 U 32 U66 U 64 U33 U 32 U33 U 32 U33 U 32 U99 % 100 %33 U 32 U33 U 32 U

104 % 110 %33 U 32 U33 U 32 U66 U 64 U66 U 64 U7 J 32 U33 U 32 U

A15C 4.5-9

005SOIL1.20

UG/KGMED

106 % 107102 % 92103 % 106

NA 3200NA 3200220 3200

NA 3200NA 6300NA 12000NA 1600NA 16002200 1600NA 1600NA 1600NA 1600NA 3200NA 1600NA 1600NA 3200NA 1600NA 1600NA 16001100 1600NA 1600NA 1600480 1600

NA 1600NA 1600240 3200

NA 3200330 1600

NA 1600

• ftUUUUBBUUUUUUUUUUUUUUUUUUUUUUU


CO RFW E Number: 8907G520Cuet ID:

RFWI:Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneDichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneIsobutyl alcohol1 , 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Trichloropropanetrana-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l , 3-Butadiene*= Outside of EPA CLP QC limits.

Client: AVENDT GROUA15B 6-9

001LOW

11

5634246868346814068340140140681401406868340140680

JE

UJUUUUUUUUUUUUUUUUU

A15B 6^1

001MED

9604209609609601900190096019003900100096003900390019003900^3900190019009600390019000

UJUUUUUUUUJUUUUUUUUUUU

A15B 6-9

001 MSLOW

1080 *2433146666336613066

330130130661301306666330130660

Work Order: 5610-01-01-0001

JUJUUUUUUUUUUUUUUUUU

A15B 6-9

001 MSDLOW

122183 *7532366464326413064320130130641301306464320130640

A15C 4.5-9 fl

005 DLLOW

U

UUUUUUUUUUUUUUUUU

NA16001600

EE

NANANANANANANANANANANANANANANANANA

ae: Ibk!5 4.5-9

005MED

16006301600160016003200320045032006300230016000630063003200630063003200320016000630032000

UJUUUUUJUUJUUUUUUUUUUU


Roy F. Weston, Inc Lionville LaboratoryVolatilee by GtîS, Appendix IX List Report Date: 08/1^. 9 14:51

Client: AVENDT GROUP Work Order; 5610-01-01-0001________Page; 2a

r Cuet ID:

Sample RFWl :Information Matrix »

D.F. :Units:Level t


ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Dieulfide1 , 1-Dichloroethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1, 1,2-TrichloroethaneBenzeneTrane-1 , 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane*- Outside of EPA CLP QC limits.

A15C 4.5-9

005SOIL1.20

UG/KGMEDREPREP102103127

3200320032003200380063001600160016001600160016003200160016003200160016001600870

16001600440

1600160032003200330

1600

%%

* %==flUUUUBBUU

UUUUUUUUUUJUUJUUUUJU

VBLK VBLK VBLK

89LVW147-MB1 89LVY175-MB1 89LVY177-MB1SOIL SOIL SOIL1.00 1.25 1.25

UG/KG UG/KG UG/KGLOW MED MED

10096105

10101010610555555105510555555555101055

%%%

—— fl —————— ='

U

UUU

UUUUUUUUUUUUUUUUUUUUUUUU

103 %104 %107 %

1200 U1200 U1200 U1200 U17001100 J620 U620 U620 U620 U620 U620 U

1200 U620 U620 U

1200 U620 U620 U620 U620 U620 U620 U620 U620 U620 U

1200 U1200 U620 U620 U

88 %88 %99 %

= ————— fl —————————— fl —— = ——— ====fl1200 U1200 U1200 U1200 U17002300620 U620 U620 U620 U620 U620 U

1200 U620 U620 U

1200 U620 U620 U620 U620 U620 U620 U620 U620 U620 U

1200 U1200 U620 U620 U

RFW BaJ Number: 8907G520 Client: AVENDT GROUPGust ID: A15C 4.5-9

RFWf: 005Level: MED

REPREPTolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneDichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneiBobutyl alcohol1, 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Tr ichloropropanetrans-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l, 3-Butadiene* = Outside of EPA CLP QC limits.

1600110014001600520032003200160032006300320016000630063003200630063003200320016000630032000

UJJU

U0UUU00UUUUUUU0UU

Work Order: 5610-01-01-0001 ie: 2bVBLK •— • VBLK VBLK

89LVW147-MB1 89LVY175-MB1 89LVY177-MB1LOW MED MED

55555101051020105020201020

• 2010105020100

UUUUUUUUUUUU0UUUUUUUUU

620620620620620

12001200620

12002500120062002500250012002500250012002406200250012000

UUUUUUUUUUUUUUUUUUJUUU

, 620620620620620

12001200620

120025001200620025002500120025002500120012006200250012000

UUUUUUUUUUUUUUUUUUuUUU


Roy F. Weston, In - Lionville LaboratoryVolatiles by _ MS, Appendix IX List Report Date: 08/ 89 14:58


Cuet ID: ALL B4-8 ALLC 2-6.5 ALLC 2-6.5 A16B 9-12 A16B 9-12 A16C 2-5

Sample RFHf: 001Information Matrix: SOIL

D.F.: 1.25Units: UG/KGLevel : MED

Toluene-d8 107Surrogate Bromof luorobenzene 97Recovery l,2-Dichloroethane-d4 121

Chloromethane 1400BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecis-1 , 3-DichloropropeneTrichloroetheneD ibromoch loromethane1,1, 2-Tr ichloroethaneBenzeneTrans-1 , 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane

140014001400150010006906906906906906901400690690140069069069069069069069069069014001400690690

%%%

==f 1===UuUuBJBUUUUUUUUUUUUuuuuuuuuuuu

005SOIL1.25

UG/KGMED

005SOIL1.25UG/K6MEDREPREP

143 * % 112 %125 * % 96 *161 * % 111 %

=========£ !============£ 1=

1300 U 1300 U1300 U 1300 U1300 U 1300 U1300 U 1300 U1700 B 2100 B690 JB 1800 B660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U1300 U 1300 U660 U 660 U660 U 660 U1300 U 1300 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U660 U 660 U1300 U 1300 U1300 U 1300 U660 U 140 J660 U 660 U

017SOIL12.5

UG/KGMED

165 * %145 * %192 * %

15000 U15000 U15000 U15000 U20000 B16000 B7700 U7700 U7700 U

, 150007700 U7700 U15000 U7700 U7700 U15000 U7700 U7700 U7700 U

1000007700 U7700 U2600 J7700 U7700 U15000 U15000 U4600 J7700 U

017SOIL125

UG/KGMEDREPREP3 * %4 * %4 * %

150000 U150000 U150000 U150000 U120000 B260000 B77000 U77000 U77000 U77000 U77000 U77000 U150000 U77000 U77000 U150000 U77000 U77000 U77000 U10000077000 U77000 U77000 U77000 U77000 U150000 U150000 U22000 J77000 U

020SOIL25.0UG/KGMED

137 * %144 * %161 * %

:==========fl

31000 U31000 U31000 U31000 U30000 B23000 JB15000 U15000 U6400 J15000 U15000 U15000 U31000 U15000 U15000 U31000 U15000 U15000 U15000 U14000 J15000 U15000 U8800 J15000 U15000 U31000 U31000 U11000 J15000 U


RFW Ba* h Number: 8907G709j- Cuet ID:

RFWt:Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAery Ion it rileTrichlorof luoromethaneDichlorodifluoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide) ____3 -Ch lor opropeneMethacrylonitrileDibromomethaneIsobutyl alcohol1 , 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Trichloropropanetrans-1, 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l, 3-Butadiene*= OutBide of EPA CLP QC limits.

AVENDT GROUP WorkALL B4-8 ALLC 2-v ALLC 2-6.5

001 . 005 005MED MED MED

REPREP69024029006903601400140069014002700630690027002700140027002700140014006900270014000

UJ

U

UUUUUJUUUUUUUUUUU

1705301700660380013001300660130027001300660027002700130027002700130013006600270013000

JJ

U

UUUUUUUUUUUUUUUUU

1807502400660240013001300660130027001300660027002700130027002700130013006600270013000

J

'UiU00UUUUUUUUUUUUUU

Order: 5160-01-01-0001A16B 9-12

017MED

720031000800007700

5000001500015000770015000310001500077000310003100015000310003100015000150007700031000150000

J

U

UUUUUUUUUUUUUUUUU

A16B 9-12

017MEDREPREP

77000370008500077000570000150000150000770001500003100001500007700003100003100001500003100003100001500001500007700003100001500000

UJ

U

UUUUUUUUUUUUUUUUU

Paqe: Ib: 2-5

020MED

150002400050000150002400003100031000150003100062000310001500006200062000310006200062000310003100015000062000310000

U

U

UUUUUUUUUUUUUUUUU

Roy F. Weston, In - Lionville Laboratory

ORrW Batch Number: 8907G709Volatiles by

Client: AVENDT GROUP~

Cust ID: VBLK

Sample RFWfi 89LVY179-MB1Information Matrix: SOIL

D.F.: 1.25Units: UG/KGLevel: MED

Toluene-d8Surrogate Bromof luorobenzeneRecovery 1 , 2-Dichloroethane-d4

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecis-1 , 3-DichloropropeneTrichloroetheneD ibromoch lor omet hane1,1, 2-Tr ichloroethaneBenzeneTrane-1, 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane*- Outside of EPA CLP QC limits.

949590

120012001200120068011006206206206206206201200620620120062062062062062062062062062012001200620620

%%%

==flUuUu

Juuuuuuuuuuuuuuuuuuuuuuu

^MS, Appendix IX List Report Date: 08/ 89 14:58Work Order: 5160-01-01-0001 Paqe: 2a

VBLK


UG/KGMED

928993

1200120012001200120024006206206206206206201200620620120062062062062062062062062062012001200620620

%%%

— fl== ——— = ———— fi ———————— =-fl ——— - = fl ———————— =-flUUUu

uuuuuuuuuuuuuuuuuuuuuuu

RFWJB" Number; 8907G709 Client; AVENDT GROITGust ID: VBLK VBLK

Work Order; 5160-01-01-0001 'age; 2b

RFWf: 89LVY179-MB1Level: MED

89L.VY180-MB1MED

Toluene_____Chlorobenzene_Ethylbenzene_Styrene_____Xylene (total)AcroleinAcrylonitrlle________Trtchlorofluoromethane_DichlorodifluoromethaneAcetonitrile_________lodomethanePropionitrlle (Ethyl Cyanide)3-Chloropropene____________Methacrylonitrile__________Dibrotnome thane____________leobutyl alcohol__________1,2-Dibromoethane__________1,1,1,2-Tetrachloroethane___1,2,3-Trichloropropane______trans-1,4-Dichloro-2-butene1,2-Dibromo-3-chloropropane2-Chloro-l,3-Butadiene*:

620 U620 U620 U620 U620 U1200 U1200 U620 U1200 U2500 U1200 U6200 U2500 U2500 U1200 U2500 U2500 U1200 U1200 U6200 U2500 U12000 U

620 U620 U620 U620 U620 U1200 U1200 U620 U1200 U2500 U1200 U6200 U2500 U2500 U1200 U2500 U2500 U1200 U1200 U6200 U2500 U12000 U



Roy F. Weston, Inc. - Lionville LaboratoryVolatiles by GC/MS, Appendix IX List Report Date: 08/07/89 14:32


Cust ID: A22B 0-7 VBLK

SampleInformation

RFWI:Matrix:

D.F.tUnits:Levelt

005 89LVY175-MB1SOIL SOIL1.20 1.25

UG/KG UG/KGMED MED

Toluene-d8Surrogate BromofluorobenzeneRecovery 1,2-Dichloroethane-d4

Chloromethane_________________Bromomethane_________________Vinyl Chloride________________ChloroethaneMethylene Chloride_AcetoneCarbon Disulfide________1,1-Dichloroethene_______1.1-Dichloroethane_______1.2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon Tetrachloride_Vinyl Acetate______Bromodichloromethane_1,2-Dichloropropanecia-l,3-Dichloropropene_TrichloroetheneDibromochloromethane_l,l,2-Trichloroethane_BenzeneTrans-1,3-Dichloropropene_Bromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene____________1,1,2,2-Tetrachloroethane_____*« Oufde of EPA CLP QC limits.

85 %88 %94 %

========fl====2500 U2500 U2500 U2500 U3100 B2000 JB1300 U1300 U260 J

14001300 U1300 U2500 U1300 U1300 U2500 U1300 U1300 U1300 U690 J1300 U1300 U1300 U1300 U1300 U2500 U2500 U1300 U1300 U

UU

103 %104 %107 %

=======£!=1200 U1200 U1200 U1200 U17001100 J620 U620 U620 U620 U620620

1200 U620 U620 U

1200 U620 U620 U620 U620 U620 U620 U620 U620 U620 U1200 U1200 U620 U620 U

=fl= = fl

RFW Number; 8907G660 Client; AVENDT GROUP Work Order: 5160-01-01-0001 Page; IbCust ID:

RFW#iLevel :

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneDichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide) ____3-ChloropropeneMethacryloriitrileDibromomethaneIsobutyl alcohol1 , 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Tr ichloropropanetrane-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l, 3-Butadiene*« Outside of EPA CLP QC limits.

A22B 0-7 VBLK

005 89LVY175-MB1MED MED

13006205601300130025002500130025005000100013000500050002500500050002500250013000500025000

UJJUUUUUUUJUUUUUUUUUUU

620620620620620

1200120062012002500120062002500250012002500250012002406200250012000

UUUUUUUU00UUUUUUUUJUUU

Roy F. Weston, IncVolatiles by

Lionville Laboratory, Appendix IX List Report Date: 08/0.. 9 15:16

Work Order; 5160-01-01-0001 _______ Page; la

Cust ID:


D.F. tUnits:Level:


ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1, 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1,1, 2-Tr ichloroethaneBenzeneTrans-l,3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane*«• Outside of EPA CLP QC limits.

A21C 4-8

001SOIL1.25

UG/KGMED

79 * %79 %84 %

4300 U4300 U4300 U4300 U5800 B4100 JB2200 U2200 U2200 U2200 U2200 U2200 U1600 J2200 U2200 U4300 U2200 U2200 U2200 U2200 U2200 U2200 U2200 U2200 U2200 U4300 U4300 U2200 U2200 U

A21C 4-8 A23A 19-20 A23A 19-20 VBLK VBLK

001 007 007 89LVY175-MB1 89LVY177-MB1SOIL SOIL SOIL SOIL SOIL1.25 1.25 1.25 1.25 1.25

UG/KG UG/KG ' UG/KG UG/KG UG/KGMED MED MED MED MEDREPREP REPREP89 %84 %115 %

==========£!==:

4300 U4300 U4300 U4300 U5900 B15000 B2200 U2200 U2200 U2200 U2200 U2200 U4300 U2200 U2200 U4300 U2200 U2200 U2200 U2200 U2200 U2200 U2200 U2200 U2200 U4300 U4300 U2200 U2200 U

15 * %15 * %16 * %

= = = = = sr = = = sfls = :

1600 U1600 U1600 U1600 U2100 B2400 B780 U780 U780 U780 U780 U780 U1600 U780 U780 U1600 U780 U780 U780 U2100780 U780 U780 U780 U780 U1600 U1600 U780 U780 U

14 * %15 * %16 * %

==========fl==:1600 U1600 U1600 U1600 U1400 B2000 B780 U780 U780 U780 U780 U780 U220 J780 U780 U1600 U780 U780 U780 U2000780 U780 U170 J780 U780 U1600 U1600 U860780 U

103104107

12001200120012001700110062062062062062062012006206201200620620620620620620620620620

12001200620620

%%%

:=fl = = :

U

U

U

U

J

U

U

UUUUUUUUUUUUUUUUUUUUU

888899

1200120012001200170023006206206206206206201200620620120062062062062062062062062062012001200620620

%%%

= = fl

U

U

U

U

UUUUUUUUUUUUUUUUUUUUUUU

RFW Be' '• Number; 8907G645 Client: AVENDT GROUP Work Order; 5160-01-01-0001 IbCuet ID:

RFWI:Level:

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrlchlorof luoromethaneDichlorodif luoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneIsobutyl alcohol1 , 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Trichloropropanetrans-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l , 3-Butadiene*= Outside of EPA CLP QC limits.

A21C 4-8

001MED

2200150022002200220043004300220043008600300022000860086004300860086004300430022000860043000

UJUUUUUUUUJUUUUUUUUUUU

A21C 4_ A23A 19-20 A23A 19-20 VBLK \

001 007 007 89LVY175-MB1 89LVY177-MB1MED MED MED MED MEDREPREP REPREP2200610022002200220043004300220043008600280022000860086004300860086004300430022000860043000

U


570018000330780780

16001600780

160031001600780031003100160031003100160016007800310016000

JUU0UUUUUUUUUUUUUUUU

580018000200780780

16001600780

160031001600780031003100160031003100160016007800310016000

JUUUUUUUUUUUUUUUUUUU

620620620620620

12001200620

12002500120062002500250012002500250012002406200250012000

UUUUUUUUUUUUUUUUUUJUUU

620620620620620

12001200620

120025001200620025002500120025002500120012006200250012000

0UUUUUUUUUUUUUUUUUUUUU

Roy F. Weeton, Inc Lionville Laboratory


Cust ID:

Sample RFWi :Information Matrix:

D.F. :Units:Level:

Toluene-d8Surrogate Bromof luorobenzeneRecovery 1, 2-Dichloroethane-d4

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1, 1-Dichloroethene1 , 1-Dichloroethane1, 2-Dichloroethene (total)Chloroform1 , 2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane1 , 2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1,1, 2-Tr ichloroethaneBenzeneTrans-1, 3-DichloropropeneBromoform4-Methyl-2-pentanone2-HexanoneTetrachloroethene1,1,2, 2-Tetrachloroethane*= Outside of EPA CLP QC limits.

Volatiles by GClient: AVENDT GROUP

VBLK


UG/KGMED

10610289

120012001200120014008106206206206206206201200620620120062062062062062062062062062012001200620620

%%%

=flUUUU

JUUUUUUUUUUUUUUUUUUUUUUU

S, Appendix IX List Report Date: 08/0 15:16Work Order: 5160-01-01-0001 raqe: 2a

VBLK


UG/KGMED

949590

1200120012001200680110062062062062062062012006206201200620620620620620.62062062062012001200620620

%%%

UUUU

JUUUUUUUUUUUUUUUUUUUUUUU

Work Order; 5160-01-01-0001 2bGust ID:

RFWf:Level :

TolueneChlorobenzeneEthylbenzeneStyreneXylene (total)AcroleinAcrylonitrileTrichlorof luoromethaneDichlorodifluoromethaneAcetonitrilelodomethanePropionitrile (Ethyl Cyanide)3-ChloropropeneMethacrylonitrileDibromomethaneIsobutyl alcohol1, 2-Dibromoethane1,1,1, 2-Tetrachloroethane1,2, 3-Tr ichloropropanetrane-1 , 4-Dichloro-2-butene1 , 2-Dibromo-3-chloropropane2-Chloro-l, 3-Butadiene*= Outside of EPA CLP OC limits.

VBLK VBLK ,_

89LVY178-MB1 89LVY179-MB1MED MED

62062062062062012001200150120025001200620025002500120025002500120012006200250012000


62062062062062012001200620120025001200620025002500120025002500120012006200250012000

UUUUUUUUUUUUUUUUUUUUUU




Phones: (312) 534-5200 (219)885-7077 (815)723-7533

August 29, 1989


Dear Mr. Bade:

Please find enclosed the Pesticide/PGftaportion of the reports forthe samples submitted to Weston/Gulf Coast Laboratories foranalyses. They were identified with our batch numbers 8907G520,8907G528, 8907G580, 8907G611, 8907G645, 8907G660, 8907G709, 8907G724and 8907G753. If you have any questions, please contact SherylJohnson or Lynn Gifford at our laboratories.

Sincerely,


Linda S. M&kleyOrganics Unit Leader

igEnclosures

MANAGERS \t.^ DESIGNERS/CONSUITANTS



Phones: (312)534-5200 (219)885-7077 (815)723-7533



ORGANIC QUALIFIERS



B - Indicates the compound was found in the blank and the sample.


BS - Indicates matrix analyses were conducted on reagent grade water.









Revised 06/16/89

MANAGERS DESCNERSAXNSUUANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533




Date: Thursday August 24th, 1989

RE: A10 6-7Project # 5160-01-01-0001Lab ID: 8907G611-001Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

92

92

92

92

92

180

180

Flag

U

U

U

U

U

U

U

OESKJNER&CONSU.TANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A10 9-10Project # 5160-01-01-0001Lab ID: 8907G611-002Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclot-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

120

120

120

120

120

240

240

Flag

U

U

U

U

U

U

U


i WESTON-GULF COAST LABORATORIES, INC.






RE: A10 20-22Project * 5160-01-01-0001Lab ID: 8907G611-006Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 ,

Result

BDL

BDL

BDL

BDL

1 11 f\±.m VfJ

*kl\l~

Limit

110

110

110

K©

zoo

4*A

Flag

U

U

U

U

U

U

MANAGERS DESK3NERS£ONSULTAOTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A10 24-29Project * 5160-01-01-0001Lab ID: 8907G611-008Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

10000

BDL

BDL

BDL

4300

BDL

Limit

200

200

200

200

200

400

400

Flag

U

U

U

U

U





To: Avendt Group, Inc.432 North Saglnaw Street3rd FloorFlint, MI 48502



RE: AID 37-38Project * 5160-01-01-0001Lab ID: 8907G611-009Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 t

Result

BDL

3200

BDL

BDL

BDL

880

BDL

Limit

95

95

95

95

95

190

190

Flag

U

U

U

U

U








RE: AHA 8-13Project * 5160-01-01-0001Lab ID: 8907G724-001Sample Date: 07/19/89Date Received: 07/19/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

0.00

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: AHA 13-18Project * 5160-01-01-0001Lab ID: 89076724-003Sample Date: 07/19/89Date Received: 07/19/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

120

120

120

120

120

240

240

Flag

U

U

U

U

U

U

U

MANAGERS DES1GNER&CONSUI.TAWTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allb 8.1-10.6Project # 5160-01-01-0001Lab ID: 89076709-003Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

210

BDL

Limit

140

140

140

140

140

270

270

Flag

U

U

U

U

U

J

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allb 12-17Project * 5160-01-01-0001Lab ID: 8907G709-004Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 t

Result

BDL

BDL

BDL

BDL

BDL

920

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

MANAGERS DESlGNERaCONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allc 6.5-10.5Project * 5160-01-01-0001Lab ID: 89076709-007Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

_ Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

13000

BDL

Limit

2000

2000

2000

2000

2000

4100

4100

Flag

U

U

U

U

U

U

MANAGERS OESIGNERS/CONSUITANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Allc 12.5-16.5Project # 5160-01-01-0001Lab 10: 8907G709-008Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

_ Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

1300

BDL

Limit

94

94

94

94

94

190

190

Flag

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Alld 8-10Project # 5160-01-01-0001Lab ID: 8907G709-009Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

5200

5200

5200

5200

5200

10000

10000

Flag

U

U

U

U

U

U

U

MANAGERS DESGNERS/CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: Alld 18.5-23.5Project * 5160-01-01-0001Lab ID: 89076709-011Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

38000

Limit

4800

4800

4800

4800

4800

9600

9600

Flag

U

U

U

U

U

U








RE: A12A 8-11Project * 5160-01-01-0001Lab ID: 8907G724-004Sample Date: 07/19/89Date Received: 07/19/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12A 11-20.5Project I 5160-01-01-0001Lab ID: 8907G724-006Sample Date: 07/19/89Date Received: 07/19/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

67

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

J

U

MANAGERS DeSBNERS/CONSUTANTS







RE: A12b 9-12Project * 5160-01-01-0001Lab ID: 8907G611-012Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

13000

BDL

BDL

BDL

830

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U








RE: A12b 14-17Project I 5160-01-01-0001Lab ID: 8907G611-013Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

490

490

490

490

490

990

990

Flag

U

U

U

U

U

U

U

MANAGERS OE3GNER&CONSULTANTS







RE: A12b 17-19Project # 5160-01-01-0001Lab ID: 8907G611-014Sample Date: 07/13/89Date Received: 07/14/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

270

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

MANAGERS DESIGNERS/CONSUITANTS







RE: A12C 10-13Project * 5610-01-01-0001Lab ID: 8907G580-009Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

U








RE: A12C 14-16Project I 5610-01-01-0001Lab ID: 8907G580-011Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

94

94

94

94

94

190

190

Flag

U

U

U

U

U

U

U

MANAGERS DESIGNEflS/CONSUlTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12d 6-13Project f 5160-01-01-0001Lab ID: 89076709-013Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

530000

BDL

Limit

52000

52000

52000

52000

52000

100000

100000

Flag

U

U

U

U

U

U

MANAGERS DESIGNERS£ONSUITANTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A12d 17-20Project # 5160-01-01-0001Lab ID: 8907G709-014Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

29000

BDL

72000

Limit

11000

11000

11000

11000

11000

21000

21000

Flag

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12d 20-25Project * 5160-01-01-0001Lab ID: 8907G709-OI6Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

6700

BDL

9100

Limit

970

970

970

970

970

1900

1900

Flag

U

U

U

U

U

MANAGERS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13A 9-14Project # 5160-01-01-0001Lab ID: 8907G753-001Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13A 14-19Project I 5160-01-01-0001Lab ID: 8907G753-003Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242i

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U

MANAGERS DESKNEf&CONSUlTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13A 19-20.5Project * 5160-01-01-0001Lab ID: 8907G753-004Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

U

U







Date: Wednesday August 16th, 1989

RE: A13b 6-9.5Project # 5160-01-01-0001Lab ID: 8907G528-003Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

32000

BDL

BDL

18000

BDL

Limit

1000

1000

1000

1000

1000

2100

2100

Flag

U

U

U

U

U








RE: A13b 9.5-12Project * 5160-01-01-0001Lab ID: 8907G528-004Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242i

Aroclor-1248

Aroclor-1254

Aroclor-1260 ,

Result

BDL

1900

BDL

BDL

BDL

350

BDL

Limit

96

96

96

96

96

190

190

Flag

U

U

U

U

U








RE: A13C 4-8.5Project # 5610-01-01-0001Lab ID: 8907G580-001Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

--...:'.• Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

780000

BDL

BDL

BDL

130000

BDL

Limit

38000

38000

38000

38000

38000

76000

76000

Flag

U

U

U

U

U








RE: A13C 6-13Project # 5610-01-01-0001Lab ID: 8907G580-003Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

20000

BDL

BDL

BDL

5500

BDL

Limit

990

990

990

990

990

2000

2000

Flag

U

U

U

U

U

MANAGERS DESGNERS/CONSUUANTS







RE: A13C 13-16Project I 5610-01-01-0001Lab ID: 89076580-005Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

95

95

95

95

95

190

190

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A13D 18-23Project # 5160-01-01-0001Lab ID: 89076724-007Sample Date: 07/19/89Date Received: 07/19/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

670

630

Limit

99

99

99

99

99

200

200

Flag

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533


To: Avendt Group, Inc.432 North Saglnaw Street3rd FloorFlint, HI 48502

Attn: Nr. Chris Bade


RE: A14A 4-9Project I 5160-01-01-0001Lab 10: 8907G753-005Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

99

BDL

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

J

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14A 13.5-23.5Project # 5160-01-01-0001Lab ID: 89076753-007Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242i

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

62

BDL

Limit

110

110

110

110

110

210

210

Flag

U

U

U

U

U

J

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14A 23.5-28.5Project I 5160-01-01-0001Lab ID: 8907G753-008Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

98

98

98

98

98

200

200

Flag

U

U

U

U

U

U

U








RE: A14B 4.0-8.5Project # 5160-01-01-0001Lab ID: 89076528-005Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

„ Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

100000

BDL

BDL

BDL

14000

BDL

Limit

2600

2600

2600

2600

2600

5200

5200

Flag

U

U

U

U

U

MANAGERS DESIGNER&CONSU.TANTS







RE: A14B 8.5-13Project # 5160-01-01-0001Lab ID: 89076528-007Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242(

Aroclor-1248

Aroclor-1254

Aroclor-1260 .

Result

BDL

5200

BDL

BDL

BDL

1100

BDL

Limit

94

94

94

94

94

190

190

Flag

U

U

U

U

U








RE: A14c 4.0-8.5Project # 5160-01-01-0001Lab ID: 8907G528-008Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242/

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

190000

BDL

BDL

BDL

350000

BDL

Limit

68000

68000

68000

68000

68000

140000

140000

Flag

U

U

U

U

U








RE: A14c 13.5-16.5Project * 5160-01-01-0001Lab ID: 8907G528-011Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 t

Result

BDL

5200

BDL

BDL

BDL

1000

BDL

Limit

470

470

470

470

470

940

940

Flag

U

U

U

U

U




Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A14D 10-14Project * 5610-01-01-0001Lab ID: 8907G580-013Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

96

96

96

96

96

190

190

Flag

U

U

U

U

U

U

U








RE: A14D 15-19Project # 5610-01-01-0001Lab ID: 8907G580-015Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

U

U

MANAGERS DESCNERS/CONSUITANTS








PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

90

90

90

90

90

180

180

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15A 9-14Project # 5160-01-01-0001Lab ID: 89076753-009Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 A

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

U

U

MANAGERS DESIGNER&CONSUUVJTS


2417 Bond Si., University Park, Illinois 60466

Phones: (312)534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242i

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

U

MANAGERS DESIGNERS-CONSULTANTS







RE: A15b 13-16Project * 5160-01-01-0001Lab 10: 8907G520-002Sample Date: 07/07/89Date Received: 07/11/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 t

Result

BDL

BDL

7200

BDL

BDL

1800

BDL

Limit

940

940

940

940

940

1900

1900

Flag

U

U

U

U

JU





To: Avendt Group, Inc.432 North Saglnaw Street3rd FloorFlint, HI 48502



RE: A15b 16-19Project f 5160-01-01-0001Lab ID: 8907G520-004Sample Date: 07/07/89Date Received: 07/11/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 A

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

99

99

99

99

99

200

200

Flag

U

U

U

U

U

U

U

MANAGERS DESK3NERS/CONSULTANTS







RE: A15c 9.5-14.5Project # 5160-01-01-0001Lab ID: 8907G520-007Sample Date: 07/10/89Date Received: 07/11/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

1500

BDL

BDL

BDL

160

BDL

Limit

98

98

98

98

98

200

200

Flag

U

U

U

U

J

U

MANAGERS OeSGNERS/CONSULTANTS







RE: A15c 14.5-17.5Project I 5160-01-01-0001Lab ID: 8907G520-008Sample Date: 07/10/89Date Received: 07/11/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

15000

BDL

BDL

BDL

2300

BDL

Limit

960

960

960

960

960

1900

1900

Flag

U

U

U

U

U




Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

91

91

91

91

91

180

180

Flag

U

U

U

U

U

U

U









PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

90

90

90

90

90

180

180

Flag

U

U

U

U

U

U

U








RE: A15D 19-24Project # 5610-01-01-0001Lab ID: 89076580-020Sample Date: 07/12/89Date Received: 07/13/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

96

96

96

96

96

190

190

Flag

U

U

U

U

U

U

U

MANAGERS DESX3NERSrtXNSUUANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

210

210

Flag

U

U

U

U

U

U

U

MANAGERS DESIGNERSCONSUI.TANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533

ANALYT ICAL R E P O R T




RE: A16A 9-14Project * 5160-01-01-0001Lab ID: 8907G753-013Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

210

210

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

2100

860

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

MANAGERS DESIGNEfl&CONSUlTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16A 24-29Project # 5160-01-01-0001Lab ID: 89076753-016Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 .

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16b 14-19Project I 5160-01-01-0001Lab ID: 89076709-019Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

5400

BDL

BDL

BDL

Limit

530

530

530

530

530

1100

1100

Flag

U

U

U

U

U

U

MANAGERS OeSXjNERS/CONSUlTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16c 7-12Project * 5160-01-01-0001Lab ID: 8907G709-022Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

13000

BDL

BDL

BDL

Limit

570

570

570

570

570

1100

1100

Flag

U

U

U

U

U

U

MANAGERS OE9GNER&CONSU.TANTS







RE: A16c 12-17Project # 5160-01-01-0001Lab ID: 8907G709-023Sample Date: 07/18/89Date Received: 07/18/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

1100

BDL

450

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U








RE: A16D 13-18Project * 5160-01-01-0001Lab ID: 89076753-017Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 .

Result

BDL

BDL

BDL

BDL

BDL

90

BDL

Limit

94

94

94

94

94

190

190

Flag

U

U

U

U

U

JU

MANAGERS DESIGNERS/CONSULTAHTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A16E 13-18Project # 5160-01-01-0001Lab ID: 8907G753-020Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242f

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

520

290

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

MANAGERS DESGNERSfcONSUlTANTS







RE: A16E 18-23Project f 5160-01-01-0001Lab ID: 89076753-022Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

1300

690

BDL

Limit

99

99

99

99

99

200

200

Flag

U

U

U

U

U








RE: A16E 25.5-28Project # 5160-01-01-0001Lab ID: 8907G753-023Sample Date: 07/20/89Date Received: 07/20/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 A

Result

BDL

BDL

BDL

BDL

550

400

BDL

Limit

94

94

94

94

94

190

190

Flag

U

U

U

U

U

MANAGERS DeSGNER&CONSUlTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 ^

Result

BDL

BDL

BDL

BDL

BDL

BDL

27000

Limit

9600

9600

9600

9600

9600

19000

19000

Flag

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

200

BDL

Limit

140

140

140

140

140

290

290

Flag

U

U

U

U

U

J

U

MANAGERS DESKSNER&CONSULTANTS







RE: A21b 10-13Project * 5160-01-01-0001Lab ID: 8907G660-004Sample Date: 07/17/89Date Received: 07/17/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

98

98

98

98

98

200

200

Flag

U

U

U

U

U

U

U

MANAGERS DeaGNER&TONSUlTANTS








PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U



2417 Bond Si., University Park, Illinois 60466Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A21c 13-14.5Project I 0000-00-00-0000Lab ID: 8907G645-004Sample Date: 07/14/89Date Received: 07/15/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 «

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

91

91

91

91

91

180

180

Flag

U

U

U

U

U

U

U

MANAGERS DESIGNERS*»NSUl.TANTS








PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

90

BDL

Limit

94

94

94

94

94

190

190

Flag

U

U

U

U

U

J

U








RE: A21d 9-14Project * 5160-01-01-0001Lab ID: 89076520-010Sample Date: 07/10/89Date Received: 07/11/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260

Result

BDL

BDL

BDL

BDL

BDL

150

BDL

Limit

99

99

99

99

99

200

200

Flag

U

U

U

U

U

J

U

MANAGERS OESG«R&CONSULTAMIS








PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 .

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A22a 9-14Project # 5160-01-01-0001Lab ID: 8907G528-012Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 «

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

220

220

Flag

U

U

U

U

U

U

U








RE' A22a 19-22Project # 5160-01-01-0001Lab ID: 8907G528-014Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242- -i ———————————————————————Aroclor-1248

Aroclor-1254

Aroclor-1260 «

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

99

99

99

99

99

200

200

Flag

U

U

U

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A22a 24-28Project # 5160-01-01-0001Lab ID: 8907G528-015Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

U

MANAGERS OE3GNERSCONSULTAMTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533



Att" RaHo


RE: A22b 7-13Project HI 5160-01-01-0001Lab ID: 8907G660-007Sample Date: 07/17/89Date Received: 07/17/89Units: UG/KG

Detectiona Result

*„TJ BDL

BDL

BDL

BDL

Aroclor-1254 BDL

Aroclor-1260 4 BDL

Limit

100

100

100

100

100

210

210

Flag

U

U

U

U

U

U

U








RE: A22c 3-9Project f 5160-01-01-0001Lab ID: 8907G660-008Sample Date: 07/17/89Date Received: 07/17/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

19000

BDL

Limit

2200

2200

2200

2200

2200

4500

4500

Flag

U

U

U

U

U

U

MANAGERS OESIGNER&CONSULTANTS








PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

100

100

100

100

100

200

200

Flag

U

U

U

U

U

U

U









PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

12000

Limit

480

480

480

480

480

970

970

Flag

U

U

U

U

U

U








RE: A22d 9-14Project # 5160-01-01-0001Lab ID: 89076528-018Sample Date: 07/11/89Date Received: 07/12/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

110

110

110

110

110

210

210

Flag

U

U

U

U

U

U

U

MANAGERS DeSK5NER&tONSULTANTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533






PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

._ Aroclor-1248

Aroclor-1254

Aroclor-1260 *

Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit

93

93

93

93

93

190

190

Flag

U

U

U

U

U

U

U








RE: A23a 12-13Project * 0000-00-00-0000Lab ID: 8907G645-005Sample Date: 07/14/89Date Received: 07/15/89Units: UG/KG

PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

3300

BDL

690

Limit

88

88

88

88

88

180

180

Flag

U

U

U

U

U









PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

5700

BDL

1200

Limit

190

190

190

190

190

370

370

Flag

U

U

U

U

U









PCBs by GC

DetectionCompound

Aroclor-1016

Aroclor-1221

Aroclor-1232

Aroclor-1242

Aroclor-1248

Aroclor-1254

Aroclor-1260 4

Result

BDL

BDL

BDL

BDL

1600

BDL

BDL

Limit

110

110

110

110

110

210

210

Flag

U

U

U

U

U

U

MANAGERS DESK3NER&CONSUUANTS



Phones. (312) 534-5200 (219)885-7077 (815)723-7533

August 29, 1989> -


Dear Mr. Bade:

Please find enclosed the Pesticide/PCB portion of the reports forthe samples submitted to Weston/Gulf Coast Laboratories foranalyses. They were identified with our batch numbers 8907G520,8907G528, 8907G580, 8907G611, 8907G645, 8907G660, 8907G709, 8907G724and 8907G753. If you have any questions, please contact SherylJohnson or Lynn Gifford at our laboratories.

Sincerely,


Linda S. MackleyOrganics Unit Leader

igEnclosures






ORGANIC QUALIFIERS



B - Indicates the4compound was found in the blank and the sample.«


BS* - Indicates matrix analyses were conducted on reagent grade water.









Revised 06/16/89




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A10 15-17 EPTOXProject # 5160-01-01-0001Lab ID: 8907G611-005Sample Date: 07/13/89Date Received: 07/14/89Units: UG/L

PESTICIDES BY GC, EP LEACHATE

Compound ResultDetection

Limit Flag

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

BDL

BDL

BDL

BDL

0.29

0.57

2.9

5.7

U

U

U

U








RE: AHA 8-13 EPTOXProject # 5160-01-01-0001Lab ID: 8907G724-002Sample Date: 07/19/89Date Received: 07/19/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

0.054

BDL

BDL

Limit

0.054

0.11

0.54

1.1

Flag

U

J

U

U

MANAGERS OESGNER&roNSULTANTS







RE: Allb 4-8 EPTOXProject # 5160-01-01-0001Lab ID: 89076709-002Sample Date: 07/18/89Date Received: 07/18/89Units: UG/L



Limit Flag

gamma-BHC (Lindane) BDL 0.53 U

Endrin BDL 1.1Methoxychlor BDL 5.3 U

Toxaphene BDL 11








RE: Allc 2-6.5 EPTOXProject # 5160-01-01-0001Lab ID: 8907G709-006Sample Date: 07/18/89Date Received: 07/18/89Units: UG/L



Limit Flag


Endrin BDL 1.1

Methoxychlor BDL 5.7

Toxaphene BDL 11








RE: Alld 18.5-23.5 EPTOXProject * 5160-01-01-0001Lab ID: 89076709-012Sample Date: 07/18/89Date Received: 07/18/89Units: UG/L



Limit Flag

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

BDL

BDL

BDL

BDL

5.4

11

54

110

U

U

U

U

MANAGERS OKIGNERS/CONSUITANTS







RE: Alld 8-10 EPTOXProject * 5160-01-01-0001Lab ID: 89076709-010Sample Date: 07/18/89Date Received: 07/18/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

5.1

10

51

100

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A12A 8-11 EPTOXProject * 5160-01-01-0001Lab ID: 89076724-005Sample Date: 07/19/89Date Received: 07/19/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.054

0.11

0.54

1.1

Flag

U

U

U

U








RE: A12C 4-9 EPTOXProject * 5610-01-01-0001Lab ID: 8907G580-008Sample Date: 07/12/89Date Received: 07/13/89Units: UG/L



Limit Flag


Endrin BDL 0.63

Methoxychlor BDL 3.2Toxaphene BDL 6.3








RE: A12d 17-20 EPTOXProject # 5160-01-01-0001Lab ID: 89076709-015Sample Date: 07/18/89Date Received: 07/18/89Units: UG/L



Limit Flag


Endrin BDL 0.51


Toxaphene BDL 5.1








RE: A13A 9-14 EPTOXProject # 5160-01-01-0001Lab ID: 8907G753-002Sample Date: 07/20/89Date Received: 07/20/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.049

0.098

0.49

0.98

Flag

U

U

U

U

MANAGERS OESGNERS/CCNSUUANTS







RE: A13b 4.5-6 EPTOXProject # 5160-01-01-0001Lab ID: 8907G528-002Sample Date: 07/11/89Date Received: 07/12/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.27

0.55

2.7

5.5

Flag

U

U

U

U






Attn: Mr. Rod Miller

Date: Tuesday August 1st, 1989

RE: A13b 4.5-6 EPTOXProject # 5160-01-01-0001Lab ID: 8907G528-002Sample Date: 07/11/89Date Received: 07/12/89Units: UG/L



Limit Flag


Endrin BDL 0.55


Toxaphene BDL 5.5

MANAGERS DeSGNERS/CONSUUANTS







RE: A13C 4-8.5 EPTOXProject * 5610-01-01-0001Lab ID: 8907G580-002Sample Date: 07/12/89Date Received: 07/13/89Units: UG/L



Limit Flag


Endrin BDL 0.60









RE: A13C 4-8.5 EPTOXProject # 5610-01-01-0001Lab ID: 8907G580-002Sample Date: 07/12/89Date Received: 07/13/89Units: UG/L



Limit Flag

gamma-BHC (Lindane)

Endrin

Methoxychlor

BDL 0.30 U

BDL 0.60

BDL 3.0

Toxaphene BDL 6.0








RE: A13D 18-23 EPTOXProject # 5160-01-01-0001Lab ID: 8907G724-008Sample Date: 07/19/89Date Received: 07/19/89Units: UG/L



Limit Flag


Endrin 0.021 0.10


Toxaphene BDL 1.0




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14A 4-9 EPTOXProject * 5160-01-01-0001Lab ID: 89076753-006Sample Date: 07/20/89Date Received: 07/20/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.27

0.54

2.7

5.4

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14B 4.0-8.5 EPTOXProject # 5160-01-01-0001Lab ID: 8907G528-006Sample Date: 07/11/89Date Received: 07/12/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.30

0.60

3.0

6.0

Flag

U

U

U

U



2417 Bond SI., University Park, Illinois 60466Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533

A N A L Y T I C A L R E P O R ! '




RE: A14B 4.0-8.5 EPTOXProject I 5160-01-01-0001Lab ID: 8907G528-006Sample Date: 07/11/89Date Received: 07/12/89Units: UG/L



Limit Flag

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

BDL

BDL

BDL

BDL

0.30

0.60

3.0

6.0

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A14c 4.0-8.5 EPTOXProject # 5160-01-01-0001Lab ID: 89076528-009Sample Date: 07/11/89Date Received: 07/12/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.28

0.56

2.8

5.6

Flag

U

U

U

U








RE: A14c 4.0-8.5 EPTOXProject # 5160-01-01-0001Lab ID: 8907G528-009Sample Date: 07/11/89Date Received: 07/12/89Units: UG/L


Compound Result

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

DetectionLimit Flag

BDL

BDL

BDL

BDL

0.28

0.56

2.8

5.6

U

U

U








RE: A15A 9-14 EPTOXProject * 5160-01-01-0001Lab ID: 8907G753-010Sample Date: 07/20/89Date Received: 07/20/89Units: UG/L


DetectionCompound

gamma -BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.054

0.11

0.54

1.1

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15b 13-16 EPTOXProject * 5160-01-01-0001Lab ID: 8907G520-003Sample Date: 07/07/89Date Received: 07/11/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.056

0.11

0.56

1.1

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15b 13-16 EPTOXProject # 5160-01-01-0001Lab ID: 8907G520-003Sample Date: 07/07/89Date Received: 07/11/89Units: UG/L



Limit Flag


Endrin BDL 0.11


Toxaphene BDL 1.1

MANAGERS DESIGNERS ONSULTAMTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15c 4.5-9 EPTOXProject # 5160-01-01-0001Lab ID: 8907G520-006Sample Date: 07/10/89Date Received: 07/11/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.27

0.54

2.7

5.4

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A15c 4.5-9 EPTOXProject # 5160-01-01-0001Lab ID: 8907G520-006Sample Date: 07/10/89Date Received: 07/11/89Units: UG/L



Limit Flag


Endrin BDL 0.54


MANAGERS DE3GNERS/CONSULTANTS



Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533





RE: A16A 9-14 EPTOXProject # 5160-01-01-0001Lab ID: 8907G753-014Sample Date: 07/20/89Date Received: 07/20/89Units: UG/L



Limit Flag


Endrin BDL 0.098


Toxaphene BDL 0.98




Phones: (312) 534-5200 (219) 885-7077 (815) 723-7533








Limit Flag

gamma-BHC (Lindane) BDL 12 U

Endrin BDL 25

Methoxychlor BDL 120

Toxaphene BDL 250








RE: A16c 2-5 EPTOXProject * 5160-01-01-0001Lab ID: 8907G709-021Sample Date: 07/18/89Date Received: 07/18/89Units: UG/L


DetectionCompound

gamma -BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

5.0

10

50

100

Flag

U

U

U

U

MANAGERS DE3GNER&CONSULTANTS







RE: A16E 13-18 EPTOXProject # 5160-01-01-0001Lab ID: 89076753-021Sample Date: 07/20/89Date Received: 07/20/89Units: UG/L


DetectionCompound

gamma- BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.053

0.11

0.53

1.1

Flag

U

U

U

U








RE: A21b 1-6 EPTOXProject * 5160-01-01-0001Lab ID: 8907G660-002Sample Date: 07/17/89Date Received: 07/17/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.29

0.57

2.9

5.7

Flag

U

U

U

U










DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.099

0.20

0.99

2.0

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A21d 14-19 EPTOXProject # 5160-01-01-0001Lab ID: 8907G520-012Sample Date: 07/10/89Date Received: 07/11/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.25

0.50

2.5

5.0

Flag

U

U

U

U




Phones: (312) 534-5200 (219)885-7077 (815)723-7533





RE: A21d 14-19 EPTOXProject # 5160-01-01-0001Lab ID: 8907G520-012Sample Date: 07/10/89Date Received: 07/11/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.25

0.50

2.5

5.0

Flag

U

U

U

U










DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.28

0.57

2.8

5.7

Flag

U

U

U

U










DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

0.25

0.50

2.5

5.0

Flag

U

U

U

U








RE: A23a 19-20 EPTOXProject # 0000-00-00-0000Lab ID: 8907G645-008Sample Date: 07/14/89Date Received: 07/15/89Units: UG/L


DetectionCompound

gamma-BHC (Lindane)

Endrin

Methoxychlor

Toxaphene

Result

BDL

BDL

BDL

BDL

Limit

5.6

11

56

110

Flag

U

U

U

U

WtAGERS DESIGNERS CONSULTANTS

WESTON-GULF COAST LABORA-ORIES -nc2417 Bond St.. University Park, Illinois 50466

Phones: (312) 534-5200 ( 2 1 9 ) 8 8 5 - 7 0 7 7 ( 8 l 5 i ~ 2 3 -

September 11, 1989


Dear Mr. Bade:

Please find enclosed the Appendix IX Pesticide/ PCB reports for thesamples submitted to Weston/Gulf Coast Laboratories for analyses.The samples were analyzed at Weston/Lionville Analytics. They wereidentified with our batch numbers 8907G520, 8907G528, 8907G580,8907G611, 8907G645, 8907G660, 8907G709. If you have any questions,please contact Sheryl Johnson or Lynn Gifford at our laboratories.

Sincerely,



DG/lg

Enclosures

O

Peeticlde/PCBe hv GC, Appendix IX List Report Dates 08/21/89 16i38Work Ordert 5610-01-01-0001 e i 1 _

ooGust IDi A15B 6-9

Sample RFWf : 001Information Matrix i SOIL

D.F.J 5.00Unite i ug/Kg

Surrogate: Di-n-butylchlorendate 97 %

Alpha-BHCBeta-BHCDelta-BHCganma-BHC (Lindane)HeptachlorAldrinHeptachlor epoxideKndosulfan IDleldrin4, 4 '-DDKKndrinKndoeulfan II4, 4 '-ODDKndoBulfan sulfate4,4'-DDTMethoxychlorKndrin aldehydeKeponealpha-Chlordanegamna-Ch lordaneToxapheneAroclor-1016Aroc lor- 1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260Iiodrin

8585858585858585170170170170170170170850170170850850

17008508503700850850940

1700170

UUUUUUUUUUUUUUUUUUuuuuu

uuJuu

A15C 4.5-9 PBLK

005 89LE0659-MB2SOIL SOIL250 0.500

ug/Kg ug/Kg

D

25002500250025002500250025002500490049004900490049004900490025000490049002500025000490002500025000300000250002500068000490004900

UUUUUUU0UUUUUUUuuuuuu0u

uu

uu

51

.0

.0

.0

.0

.0

.0

.0

.08.08.08.08.08.08.08.0408.08.0404080404040404080808.0

UUUUUUU0UUUUUUUUUUUuuuuuuuuuu

A16 C2-5

709-020SOIL

50.0ug/Kg

D

110011001100110011001100110011002200220022002200220022002200

1100022002200

11000110002200011000110001100011000900022000220002200

UUUUUUUUUUUUUuuuuuuuuuuuuJuuu

A16 C2-5

709-020 MSSOIL

50.0ug/Kg

D

120012001200DDD

12001200D2400D240024002400D

120002400240012000120002400012000120001200012000990024000240002400

-fl —UUU

U0

U

UUU

OUUuuuuuuuJuuu

A16 C2-5

709-020 MSDSOIL

50.0ug/Kg

D

130013001300DDD

13001300D2600D260026002600D

1300026002600130001300026000130001300013000130001400026000260002600

-flUUU

UU

U

UUU

UUUUuuuuuu

uuu

1 . I I H I V I I 1 1 1 ] , ( l l " : | 1 1 1 t i lI l l i y I . l , 4 ' l l l I I I ) , t i l

Peeticide/PCB- ->y GC, Appendix IX ListClient! AVENDT GRO.

Report Date: 08/"'1/89 16i43Work Order; 5610-01-01-0001 __.._ age: 1

Cust ID i A13B4.5-6 A14C8.5-10.5 PBLK

Sample RFHf: 001 010 89LE0659-MB2Information Matrix: SOIL SOIL SOIL

D.F.i 100 2.50 0.500Unite t ug/Kg ug/Kg ug/Kg

Surrogate! Di-n-butylchlorendate D %

Alpha-BHCBeta-BHCDelta-BHCgamma-BHC (Lindane)HeptachlorAldrinHeptachlor epoxideEndoBulfan IDieldrin4, 4 '-DDEEndrinEndoBulfan II4, 4 '-ODDEndoBulfan sulfate4,4' -DOTMethoxychlorEndrin aldehydeKeponealpha-Chlordanegamna-ChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260iBodrin

22002200220022002200220022002200440,0440044004400440044004400220004400440022000220004400022000220003400002200022000100000440004400

uuuuuuuuuuuuuuuuuuuuuuu

uu

uu

83

2424242424242424474747474747472404747240240470240240170024024052047047

UU0UUUUUUUUUUUUUuuu0uuu

uu

uu

51

4.04.04.04.04.04.04.04.08.08.08.08.08.08.08.0408.08.0404080404040404080808.0

UUUUUUUUUUUUUUUUUUUUUuuuuuuuu

A16 C2-5

709-020SOIL50.0

ug/Kg

D

110011001100110011001100110011002200220022002200220022002200110002200220011000110002200011000110001100011000900022000220002200

— fi-llUUU0UUUUUUUUUUuuuuo0uuuuJuuu

A16 C2-5

709-020 MSSOIL50.0

ug/Kg

D

120012001200DDD12001200D2400D240024002400D

120002400240012000120002400012000120001200012000990024000240002400

%

UUu

0u

u

uuu

uuuuuuuuuuJuuu

A16 C2-5

709-020 MSDSOIL50.0

ug/Kg

D

130013001300DDD13001300D2600D260026002600D

1300026002600130001300026000130001300013000130001400026000260002600

*

UUU

UU

U

UUU

UUUUUUUUUu

uuu


Roy T. Weaton,! . - Lionville LaboratoryPeaticide/PCBs by GC, Appendix IX List

Client: AVENDT GROUP Work Order;Report Date: 09/06/89 15s10

5160-01-01-0001_______Page; 1

Cuet ID: A12C 4-9

SampleInformation

RFWf :Matrix:D.F.:Units:

007SOIL50.0

ug/Kg

PBLK

89LE0635-MB2SOIL1.00ug/Kg

AID 15-17

611-004 MSSOIL5. dO

ug/Kg

A10 15-17

611-004 MSSOIL0.625ug/KgREPREP

AlO 15-17

611-004 MSDSOIL5.00ug/Kg

A10 15-17

611-004 MSDSOIL0.420ug/KgREPREP

Surrogate: Di-n-butylchlorendate

Alpha-BHCBeta-BHCDelta-BHCgamma-BHC (Lindane)HeptachlorAldrinHeptachlor epoxideEndoBulfan IDieldrin4,4' -DDEEndrinEndosulfan II4, 4 '-ODDEndoBulfan sulfate4, 4 '-DOTMethoxychlorEndrin aldehydeKeponealpha-Chlordanegamma-ChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260iBodrin

92

1400140014001400140014001400140029002900290029002900290029001400029002900140001400029000140001400014000140001400023000290002900

=.£!===UUUUUUUUUUUUUU0UUUUUUUUUUUJUU

86

8.18.18.13636498.18.1120161601616162208116168181160818181818116016016

*

UUU

0U

U

UUU

UUUUUUUUUUoUUU

117

5454549085555454

125110

142 *110110110157 *540110110540540

1100540540540540540

11001100110

UUU%%%UU%U%UUU%UUUUUUUUUUUUUU

53

6.66.66.633 *49656.66.65513

94131313966613136666130666666666650013013

=fl«=UUU%%%UU%U%UUU%UUUUUUUUUUU

UU

109

5353538082625353

109110117110110110107530110110530530

1100530530530530530

11001100110

UUU%%%UU%U%UUU%UUUUUUUUUUUUUU

35

4.44.44.422 *33 *394.44.4I8.8638.88.88.864448.88.84444884444444444340888.8

%

UUU%%%UU%U%UUU%UUUUoUUUUUU

UU

Penticide/PCBu by GC, Appendix IX Lint Report Date: 08/21/89 16:31Work Orderi 5160-01-01-0001 Page: _1

Cust IDs

Sample RFWf iInformation Matrix i

D.F. sUnits i

Surrogate i Di-n-butylchlorendate

Alpha-BHCBeta-BHCDelta-BHCgamma-BHC (Lindane)HeptachlorAldrinHeptachlor epoxideKndoaulfan IDieldrin4,4'-DDEKndrinBndoaulfan II4,4'-DDDBndosulfan sulfate4,4'-DDTMethoxychlorKndrin aldehydeKeponealpha-Chlordanegamraa-ChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260Itodrin

All B4-8 All C2-6.5

001 005SOIL SOIL5.00 50.0

ug/Kg ug/Kg

I

6161616161616161120120120120120120120610120

: 120610610

1200610610610610610530

1200120

%•-fi-

llUUuuuuuuuuuuu0uuuuuuuuuuuJuu

0

510510510510510510510510

1000100010001000100010001000510010001000510051001000051005100450005100510010000100001000

%

Uuuuuuuuuuuuuuuuuuuuuuu

uu

uu

A16 B9-12

017SOIL1250

ug/Kg

D

2700027000270002700027000270002700027000530005300053000530005300053000530002700005300053000270000270000530000270000270000160000027000027000030000053000053000

%

Uouuuuuuuuuuuouuuuuuuuu

uuJuu

A16 C2-5

020SOIL50.0

ug/Kg

D

110011001100110011001100110011002200220022002200220022002200

1100022002200

11000110002200011000110001100011000900022000220002200

%

UuuuuuuuuuuuuuuuuuuuuuuDDJuuu

A16 C2-5

020 MSSOIL50.0

ug/Kg

D

120012001200DD0

12001200D2400D240024002400D

120002400240012000120002400012000120001200012000990024000240002400

%

UUu%%%uu%u%uuu%uuuuuuuuuuJuuu

A16 C2-5

020 USDSOIL50.0

ug/Kg

D

130013001300DDD

1300130002600D260026002600D

1300026002600130001300026000130001300013000130001400026000260002600

%

UUu%%%uu%u%uuu%uuuu0uuuuo

uuu

PeBticide/PCBB by GC, Appendix IX Lint Report UaLe: 09/06/09 JS:ir> RTW h Number: 8907G645O

CuBt IDi

Sample RFWf sInformation Matrix i

D.F. «UnitBt

Surrogates Di-n-butylchlorendate

Alpha-BHCBeta-BHCDelta-BHCgaona-BHC (Lindane)HeptachlorAldrinHeptachlor epoxideEndoBulfan IDieldrin4,4' -DDEBndrinEndoBulfan II4,4'-DDDEndoaulfan aulfate4, 4 '-DOTMethoxychlorEndrin aldehydeKeponealpha-Chlordaneganma-ChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260laodrin

Clients AVENDT GROf Work Order i 5160-01-01-0001 qe: 1

A21C 4-8 A23A 19-20 PBLK A10 15-17 AlO 15-17 A10 15-17

001 007 89LE0635-MB2 611-004 MS 611-004 MS 611-004 MSDSOIL SOIL SOIL SOIL SOIL SOIL50.0 200 1.00 5.00 0.625 5.00

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/KgRBPREP

D

1400140014001400140014001400140029002900290029002900290029001400029002900140001400029000140001400014000140001400029000300002900

'-fl—UUUUUUUUUUUUUUUUUUUUUUuuuuu

u

D

23002300230023002300230023002300470047004700470047004700470023000470047002300023000470002300023000230002300015000047000470004700

..£!»-•

UUUUUUUUUUUUUUUUuuuuuuuuu

uuu

86

8.18.18.13636498.18.1120161601616162208116168181160818181818116016016

— fl——UUU

UU

U

UUU

UUUUUUUUUUUUUu

117

5454549085555454

125110142 *110110110157 *540110110540540

1100540540540540540

11001100110

-fl——0UU

UU

U

UUO

0UUUUUuuuuuuuu

53

6.66.66.63349656.66.6551394131313966613136666130666666666650013013

==fl-«UUU

* %

UU

u

uuu

uuuuuuuuuuu

uu

109

5353538082625353

109110

117110110110107530110110530530

1100530530530530530

11001100110

%

UUu

Ou

u

uuu

uu0uuuuuuuuuuu

Pesticide/PCBe by GC, Appendix IX List Report Date: U9/06/By lb:U/CRFW h Humbert 8907O660•O

Gust IDtiSample RFHI iInformation Matrix t

D.r.iUnits:

Surrogate i Di-n-butylchlorendate

Alpha-BBCBeta-BBCDelta-BBCgaoata-BBC (Lindane)HeptachlorAldrinBeptachlor epoxideBndoaulfan IDieldrln4,4'-DDBBndrinBndoaulfan II4, 4 '-ODDBndoaulfan eulfate4,4'-DDTMethoxychlorBndrin aldehydeKeponealpha-Chlordaneganma-ChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260laodrin

Client: AVBNDT GROr Work Order t 5160-01-01-0001 •>qet 1

A22B 0-7 PBLR AlO 15-17 A10 15-17 A10 15-17 A10 15-17

005 89LB0635-MB2 611-004 MS 611-004 MS 611-004 MSD 611-004 MSDSOIL SOIL SOIL SOIL SOIL SOIL200 1.00 5.00 0.625 5.00 0.420

ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/KgRBPRBP REPRBP

D

32003200320032003200320032003200630063006300630063006300630032000630063003200032000630003200032000320003200012000063000630006300

UUU0UUUUUUUUUUUUuuuuuuuuu

uuu

86

8.18.18.13636498.18.1120161601616162208116168181160818181818116016016

UUU

UU

U

UUU

UUUUUUUDUUUUUU

117

5454549085555454

125110142 *110110110157 *540110110540540110054054054054054011001100110

«fl...,DU0

1UU

0

u0D

U0UUUUUuuuuuuu

53

6.66.66.633 *49656.66.6551394131313966613136666130666666666650013013

UUU

0U

U

UUU

0UU0UUDUD0O

UU

109

5353538082625353

1091101171101101101075301101105305301100530530530530530

11001100110

DUU

UU

U

UUU

UUUUUUUUUUuuu0

35

4.44.44.422 *33 *394.44.4I8.8638.88.88.864448.88.84444884444444444340888.8

-flU0U

uu

u

uuu

u0uuuuuuuuu

uu

RFW âtch Number; 8907G611

Roy F. Weeton, Inc. - Lionvillu LaboratoryPeaticide/PCf y GC, Appendix IX List Report Date: 09,' '89 11:57

Client; AVENDT GR(X._____________Work Order; 5160-01-01-0001_______**aqe; 1

Gust ID: A10 15-17 AID 15-17

Sample RFWl : 004 004Information Matrix: SOIL SOIL

D.F.: 5.00 0.625Units: ug/Kg ug/Kg

REPREPSurrogate: Di-n-butylchlorendate 100

Alpha-BHCBeta-BHCDelta-BHCgamma -BHC (Lindane)HeptachlorAldrinHeptachlor epoxideEndoeulfan IDieldrin4,4' -DDEEndrinEndoBulfan II4, 4 '-ODDEndoBulfan aulfate4,4' -DOTMethoxychlorEndrin aldehydeKeponealpha-Chlordanegamma-ChlordaneToxapheneAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260laodrin

5454545454545454110110110110110110110540110110540540110054054054054054011001100110

-fl— =0UUUUUUUUUUUUUUUUUUuuuuuuuuuu

54

6.66.66.66.66.66.66.66.6131313131313136613136666130666666666648013013

==fl=UUUUUUUUUUUUUUUUUUuuuuuuuu

uu

A10 15-17

004 MSSOIL5.00

ug/Kg

117

5454549085555454

125110142 *110110110157 *540110110540540110054054054054054011001100110

= fl—UUU

UU

U

UUU

UUUUUUUUUUuuuu

A10 15-17 A10 15-17 A10 15-17

004 MS 004 MSD 004 MSDSOIL SOIL SOIL0.625 5.00 0.420ug/Kg ug/Kg ug/KgREPREP REPREP53

6.66.66.633 *49656.66.65513

94131313966613136666130666666666650013013

=fl==:UUu%

uu

u

uuu

uuuuuuuuuuu

uu

109

5353538082625353

109110

117110110110107530110110530530110053053053053053011001100110

==fl===UU0

UU

U

uuu

uuuuuuuuuuuuuu

35

4.44.44.422 *33 *394.44.4I8.8638.88.88.864448.88.84444884444444444340888.8

-flUUU%%

UU

u

uuu

uuuuuuuuuuu

uu

RFW Batch Number; B907G611

Roy F. Weston, T««7. _ Lionville LaboratoryPestlcide/Pd )y GC, Appendix IX Hat Report Date: Of '89 11:57

Client: AVENDT GROUP______________Work Order; 5160-01-01-0001________Page; 2

Gust ID: A12B 3-7 A12B 3-7 PBLK PBLK

SampleInformation

RFWl:Matrix:D.F.:Units:

010SOIL500

ug/Kg

010SOIL100

ug/KgREPREP


ug/Kg

89LR0635-MB1SOIL0.500ug/Kg

Surrogate: Di-n-butylchlorendate

Alpha-BHCBet a - BHCDelta-BHCgamma-BHC (Lindane)HeptachlorAldrinHeptachlor epoxideEndoaulfan IDieldrin4,4' -DDEEndrinEndoaulfan II4, 4 '-ODDEndoaulfan sulfate4,4" -DOT________~Methoxychlor__Endrin aldehydeKepone________alpha-Chlordanegamma-ChlordaneTox aphene______Aroclor-1016___Aroclor-1221___Aroclor-1232___Aroclor-1242___Aroclor-1248___Aroclor-1254___Aroclor-1260___Isodrin

D %==========f1=

8300 U8300 U8300 U8300 U8300 U8300 U8300 U8300 U17000 U17000 U17000 U17000 U17000 U17000 U17000 U83000 U17000 U17000 U83000 U83000 U170000 U83000 U83000 U83000 U83000 U83000 U170000 U61000 J17000 U

D %=========fl-.

1600 U1600 U1600 U1600 U1600 U1600 U1600 U1600 U3200 U3200 U3200 U3200 U3200 U3200 U3200 U16000 U3200 U3200 U16000 U16000 U32000 U16000 U16000 U3200016000 U16000 U11000 J32000 U3200 U

86 %=======f1====8.1 U8.1 U8.1 U3636498.1 U8.1 U12016 U16016 U16 U16 U22081 U16 U16 U81 U81 U160 U81 U81 U81 U81 U81 U160 U160 U16 U

110= = = 2±r5J

4.04.04.04.04.04.04.04.08.08.08.08.08.08.08.0408.08.0404080404040404080808.0

<=fl=UUUUUUUUUUUUUUUUUUUUUUUUUUUUU

========fl============fl

\ V




Phones: (312)534-5200 (219)885-7077 (815)723-7533

September 18, 1989


Dear Mr. Bade:

Please find enclosed the OPP Pesticide portion of the reports forthe samples submitted to Weston/Gulf Coast Laboratories foranalyses. They were identified with our batch numbers 8907G520,8907G528, 8907G580, 8907G611, 8907G645, 8907G660, 8907G709. If youhave any questions, please contact Sheryl Johnson or Lynn Giffordat our laboratories.

Sincerely,



kl

Enclosures

WESTON ANALYTICSORGANOPHOSPHORUS PESTICIDES

APPENDIX IX

RFW Batch Number: 8907G520 Client: AVENDT GROUP

SampleInformation

Surrogate :

Analyte:

Ethyl Phosphorothioate*. . .Thionazin (zinophos) ......Phorate ...................Sulfotepp. ................

Dimethoate ................Methyl Parathion. .........Ethyl Parathion. ..........

Diazinon. .................

GustID:

RFW#:D.F. :

Matrix:Units:

Ethion:

A15b6-90011

Soilug/kg

78 %.Cl _

A15b6-9

001 MS1

Soilug/kg

75 %«i _= —————————————— : —— - ———— 5— — -=• ——— J. JL— — - —— s —— ~ ——— — X J--

43 U43 U8.6 U43 U8.6 U43 U8.6 U8.6 U86 UNA

43 U43 U8.6 U43 U8.6 U43 U101 %8.6 U86 U86 %

A15b6-9

001 MSD1

Soilug/kg

57 %f ~\——————————— I JL —

43 U43 U8.6 U43 U8.6 U43 U28 %8.6 U86 U62 %

A15C4.5-90051

Soilug/kg

57 %-_ — ^-. -F 1= ——— ——to. —

76 U76 U15 U76 U15 U76 U15 U15 UI

NA

A15C4.5-9005 RE

20Soilug/kg

57

NANANANANANANANA

3100NA

Page: 1

BLANK89LE0625

MB11

Soilug/kg

% 62 %-fi f i

33 U33 U7.0 U33 U7.0 U33 U7.0 U7.0 U

U 66 UNA

* o,o,o-Triethyl Ester Phosphorothioic Acid

U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested.%=F ~ent recovery. NS=Not spiked.

RFW Batch Number:

WESTOi ANALYTICSORGANOPHOSPHORUS PESTICIDES

APPENDIX IX

8907G528 Client: AVENDT GROUP Page: 1

SampleInformation

Surrogate:

Analyte:

Ethyl Phosphorothioate*Thionazin (zinophos) .......Phorate ....................Sulfotepp. .................Disulfoton. ................

Methyl Parathion. ..........Ethyl Parathion. ...........Famphur (famophos) .........Diazinon. ..................

Cust ID:RFW#:

Matrix:D.F. :Units:

Ethion:

A13b 4.5-6001

Soil1

ug/kg

38 %= —————— fl

33.0 U33.0 U7.0 U33.0 U7.0 U33.0 U7.0 U7.0 U66.0 UNA

A14C 8.5-10.010

Soil10

ug/kg

96 %

33.0 U33.0 U7.0 U33.0 U7.0 U33.0 U7.0 U7.0 U66.0 UNA

5 BLANK625-MB1Soil

1ug/kg

62 %——————— f 1 ———————— f 1 — - ————— f 1 — f 1

33.0 U33.0 U7.0 U33.0 U7.0 U33.0 U7.0 U7.0 U66.0 UNA


U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested.%=Percent recovery. NS=Not spiked.

WESTON ANALYTICSORGANOPHOSPHORUS PESTICIDES

APPENDIX IX

RFW Batch Number: 8907G580 Client:

SampleInformation

Gust A12C 4-9ID:

RFW#: 007D.F.: 1

Matrix: SoilUnits: ug/kg

AVENDT GROUP

8907G611

004 MS1

Soilug/kg

8907G611

004 MSD1

Soilug/kg

:===as====s=====ss================== ————

Page : 1

BLANK89LE0636

MB11

Soilug/kg

Surrogate:

Analyte:

Ethyl Phosphorothioate*.Thionazin (zinophos)....Phorate.................Sulfotepp...............Disulfoton..............Dimethoate..............Methyl Parathion........Ethyl Parathion.........Famphur (famophos)......Diazinon................

Ethion: 80 % 79 % 93 % 98 %==================fl=========fl=========fl=========fl=

% %=fl=========fl

120 U120 U24 U120 U24 U120 U24 U24 U240 UNA

45 U45 U9.0 U45 U9.0 U45 U57 %9.0 U90 U53 %

45 U45 U9.0 U45 U9.0 U45 U73 %9.0 U90 U66 %

33 U33 U7.0 U33 U7.0 U33 U7.0 U7.0 U66 UNA


U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested,%=F cent recovery. NS=Not spiked. NA=Not App^'âble.

LOWESTON ANALYTICS

ORGANOPHOSPHORUS PESTICIDESAPPENDIX IX


Gust A10 15-17 A10 15-17 A10 15-17 A12& 3-7SampleInformation

Surrogate:

Analyte:

Ethyl Phosphorothioate* . . .Thionazin (zinophos) ......Phorate ...................Sulfotepp. ................Disulfoton. ...............Dimethoate ................Methyl Parathion. .........Ethyl Parathion. ..........Famphur (famophos) ........Diazinon. .................

ID:RFW#: 004D.F.: 1

Matrix: SoilUnits: - ug/kg

Ethion: 113 %====================fl=

.......... 45 U

.......... 45 U

.......... 9.0 U

.......... 45 U

.......... 9.0 U......... 45 U......... 57 U.......... 9.0 U......... 90 U......... NA

004 MS1

Soilug/kg

79 %========fl=

45 U45 U9.0 U45 U9.0 U45 U57 %9.0 U90 U53 %

f004 MSD '

1Soilug/kg

93 %C T:_= ————————— f 1 =

45 U45 U9.0 U45 U9.0 U45 U73 %9.0 U90 U66 %

Page: 1

BLANKi|7 ':'- 89LE0636

0101

Soilug/kg

121 %f\= —————— i j. ——

69 U69 U14 U69 U14 U69 U14 U14 U140 UNA

MB11

Soilug/kg

98 % %•fi — fl

33 U33 U7.0 U33 U7.0 U33 U7.0 U7.0 U66 UNA


U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested.%=P--cent recovery. NS=Not spiked. NA=Not Applicable.

WESTOli .tfALYTICSORGANOPHOSPHORUS PESTICIDES

APPENDIX IX— ______ —— .__. —— . ————— _____ ————————— _ —————————————————— . ———————————— __ ————————————— .. ——————————————————————————— =B=ss==_== = _- =====-= = = = ==== = — = ————————————————————

RFW Batch Number: 8907G645 Client: AVENDT GROUP Page: 1

Cust ID: A21c 4-8 A23a 19-20Sample RFW#: 001 007Information Matrix: Soil Soil

D.F.: 1 10Units : ' ug/kg ug/kg

Surrogate: Ethion:

Analyte:

Ethyl Phosphorothioate* .............Thionazin (zinophos) ...............Phorate ............................Sul f otepp ..........................Disulfoton. ........................Dimethoate .........................Methyl Parathion. ..................Ethyl Parathion. ....................Famphur ( f amophos) .................Diazinon. ..........................

99 %——————— =1 ——— •£ _L ——

33.0 U33.0 U7.0 U

33.0 U7.0 U

33.0 U7.0 U7.0 U

66.0 UNA

33 %= ———— =— f 1-

330.0 U330.0 U70.0 U330.0 U70.0 U330.0 U550.070.0 U660.0 U

NA

BLANK793-MB1Water

1ug/1

98 %————— =-fl ———————— fl ———————— fi=========fl

33.0 U33.0 U7.0 U

33.0 U7.0 U33.0 U7.0 U7.0 U

66.0 UNA


U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested.%=Pei-cent recovery. NS=Not spiked.

WESTON . ALYTICSORGANOPHOSPHORUS PESTICIDES

APPENDIX IX

RFW Batch Number: 8907G660 Client: AVENDT GROUP Page: 1

SampleInformation

GustID:

RFW#: .D.F. :

Matrix:Units:

A22B0-70051

Soilug/kg

8907G611

004 S1

Soilug/kg

8907G611

004 T1

Soilug/kg

BLANK89LE0636

MB11

Soilug/kg

Surrogate:

Analyte:

Ethyl Phosphorothioate*Thionazin (zinophos)...Phorate................Sulfotepp..............Disulfoton..............Dimethoate..............Methyl Parathion........Ethyl Parathion.........Famphur (famophos)......Diazinon................

Ethion; 99 % 79 % 93 % 98 %=====fl=========fl=========fl=========fl

65 U65 U13 U65 U13 U65 U13 U13 U130 UNA

45 U45 U9.0 U45 U9.0 U45 U57 %9.0 U90 U53 %

45 U45 U9.0 U45 U9.0 U45 U73 %9.0 U90 U66 %

33 U33 U7.0 U33 U7.0 U33 U7.0 U7.0 U66 UNA


U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested.%=P 'cent recovery. NS=Not spiked. NA=Not App"1 -'cable.

WESTC .iNALYTICSORGANOPHOSPHORUS PESTICIDES

, APPENDIX IX


Cust ID: Allb 4-8 Allb 4-8Sample RFWf: 001 001 MSInformation Matrix: Soil Soil

D.F.: 1 1Units: ug/kg ug/kg

Surrogate: Ethion: 1

Analyte :

Ethyl Phosphorothioate* ............. 33Thionazin (zinophos) ..........Phorate .......................Sulfotepp. ....................Disulfoton. ...................Dimethoate ....................Methyl Parathion. .............Ethyl Parathion. ..............

Diazinon. .....................

. . ... 33

. . . . . 7

. . . . . 33

. . . . . 7

..... 33

. . . . . 7

...... 7

..... 66

15 %:===fl =

.0 U

.0 U

.0 U

.0 U

.0 U

.0 U

.0 U

.0 U

.0 UNA

Allb 4-8001 MSD

Soil1

ug/kg

Allc 2-6005Soil

1ug/kg

Page: 1

.5 A16b 9-12 A16c 2-5017 020

Soil Soil1 1

ug/kg ug/kg

95 % 92 % 99 % 121 %========fl=========fl=========fl=========fl==

33.0 U 33.0 U 33.0 U 33.0 U33.0 U 33.0 U 33.0 U 33.0 U7.0 U 7.0 U 7.0 U 7.0 U33.0 U 33.0 U 33.0 U 33.0 U7.0 U 7.0 U 7.0 U 7.0 U33.0 U 33.0 U 33.0 U 33.0 U121.0 % 118.0 % 7.0 U 7.0 U7.0 U 7.0 U 7.0 U 7.0 U66.0 U 66.0 U 66.0 U 66.0 U78.0 % 76.0 % NA NA

15 %======== fl

33.0 U33.0 U7.0 U33.0 U7.0 U33.0 U7.0 U7.0 U66.0 UNA


U=Analyzed,not detected. J=Present below detection limit. B=Present in blank. NR=Not requested.%=Percent recovery. NS=Not spiked.

cMANAGERS DESIGNERS/CONSULTANTS



Phones: (312) 534-5200 (219)885-7077 (815)723-7533

September 6, 1989


Dear Mr. Bade:

Please find enclosed the herbicide portion of the reports for thesamples submitted to Weston/Gulf Coast Laboratories for analyses.The samples were analyzed at Weston/Lionville Analytics. They.wereidentified with our batch numbers 8907Gr520, 8907G528, 8907G580,8907G611, 8907G645, 8907G660, 8907G709. If you have any questions,please contact Sheryl Johnson or Lynn Gifford at our laboratories.

Sincerely,



DG/lg

Enclosures


Roy F. Weston, In<j* Lionville LaboratoryHerb. Jes by GC Report Date: 08/0 16:05

Client; AVENDT GROUP______________Work Order; 5610-01-01-0001________Page; 1

Gust ID: A15B 6-9 6-9 A15B 6-9 A15C 4.5-9 PBLK

Sample RFWt :Information Matrix:

D.F.:Units:

2,4-D2,4,5-TP (Silvex)2,4,5-T

001 001 MS 001 MSD 005 89LE0624-MB1SOIL SOIL . SOIL SOIL SOIL10.0 10.0 10.0 50.0 50.0

UG/KG UG/KG UG/KG UG/KG UG/KG

==-= —— == —— fl ———— = ——— =-fl ———— = ————— fl —————————— f 1 ———————— = — f 1 — = —— ==-= — f 118 J 54 % 49 % 2300 U 1000 U130 U 73 % 71 % 1100 U 500 U130 U 68 % 100 % 1100 U 500 U

U= Analyzed, not detected. J= Present below detection limit. B= Present in blank. NR= Not requested. NS= Not spiked.%= Percent recovery. D= Diluted out. 1= Interference. NA= Not Applicable. *= Outside of EPA CLP QC


Roy F. Western, Inc. - Lionville LaboratoryHerR des by GC

Client; AVENDT GROUP______________Work Order;Report Date: 08/C' ' 15:15

5610-01-01-0001________age; 1

Cust ID: A13B4.5-6 A14C8.5-10.5 PBLK A15B 6-9 A15B 6-9

SampleInformation

RFWf:Matrix:

D.F.:Units:

001SOIL20.0UG/KG

010 89LE0624-MB1SOIL SOIL5.00 50.0

UG/KG UG/KG

520-001 MSSOIL10.0

UG/KG

520-001 MSDSOIL10.0

UG/KG

2,4-D___________2,4,5-TP (Silvex)2,4,5-T______

_______ 480 J_______ 580

580UU

======fl=21063 U63 U

==========f1=1000 U500 U500 U

547368

===fl=%%%

:===========f1

49 %71 %100 %

U= Analyzed, not detected. J= Present below detection limit. B= Present in blank. NR= Not requested. NS=%= Percent recovery. D= Diluted out. 1= Interference. NA= Not Applicable. *= Outside of EPA CLP QC

Not spiked.


Roy F. Weston, Inc.Herbil

Client; AVENDT GROUP

Lionville Laboratoryas by GC

_____Work Order:Report Date: 08/10, 13:36

5160-01-01-0001_______Page; 1

Cust ID: A12C 4-9 PBLK A10 15-17 AID 15-17

SampleInformation

RFWl:Matrix:D.F.:Units:

007 89LE0639-MB1SOIL SOIL20.0 10.0UG/KG UG/KG

611-004 MSSOIL10.0

UG/KG

611-004 MSDSOIL10.0

UG/KG

2,4-D___________2,4,5-TP (Silvex)2,4,5-T______

======fl====720 J720 U720 U

======fl====330 U170 U170 U

= fl134 %102 %92 %

99 %74 %96 %



Roy F. Western, Inc, Lionville LaboratoryHerbi Jes by GC Report Date: 08/lt 13:37

Client; AVENDT GROUP_____________Work Order; 5160-01-01-0001_______Page: 1

Cust ID: A10 15-17 AID' 15-17 AID 15-17 A12B 3-7 PBLK

SampleInformation

2,4-D2,4,5-TP (Silvex)2,4,5-T

RFWf: 004Matrix: SOILD.F.: 10.0Unite: UG/KG

__ __ ____ __ ___ __..__._.«_ —-.__ XT

270 U130 U130 U

004 MS 004 MSDSOIL10.0

UG/KG

============fl======134 %102 %92 %

SOIL10.0

UG/KG

======fl====99 %74 %96 %

010 89LE0639-MB1SOIL20.0UG/KG

_ ___ __.f 1 _ ___ __

550 J410 U410 U

SOIL10.0

UG/KG

======= f i============f l330 U170 U170 U

U= Analyzed, not detected. J= Present below detection limit. B= Present in blank. NR= Not requested. NS=%= Percent recovery. D= Diluted out. 1= Interference. NA= Not Applicable. *= Outside of EPA CLP QC

Not spiked.


Roy F. Weston, Inti • Lionville LaboratoryHerbicides by GC Report Date: 08/K 9 13:44

Client; AVENDT GROUP______________Work Order; 5160-01-01-0001________Page; 1

Cust ID: A21C 4-8 A23A 19-20 PBLK A10 15-17 A10 15-17

SampleInformation

RFW*:Matrix:

D.F.:Units:

001SOIL20.0UG/KG

007 89LE0639-MB1SOIL SOIL20.0 10.0UG/KG UG/KG

611-004 MSSOIL10.0

UG/KG

611-004 MSDSOIL10.0

UG/KG

2,4-D___________2,4,5-TP (Silvex)2,4,5-T

======f1=510 J730 U730 U

======fl====590 U290 U290 U

======fl===330 U170 U170 U

=====fl13410292

997496



Roy F. Weston, Inci Lionville LaboratoryHerbi _des by GC Report Date: 08/10. 13:41

Client; AVENDT GROUP_____________Work Order; 5160-01-01-0001_______Page; 1

Cust ID: A22B 0-7 PBLK A10 15-17 A10 15-17

SampleInformation

RFW#:Matrix:

D.F.:Units:

005 89LE0639-MB1SOIL SOIL50.0 10.0

UG/KG UG/KG

611-004 MSSOIL10.0

UG/KG

611-004 MSDSOIL10.0

UG/KG

2,4-D___________2,4,5-TP (Silvex)2,4,5-T________"

=======fi====3200 U1600 U1600 U

======fl====330 U170 U170 U

134 % 99 %102 % 74 %92 % 96 %


CORoy F. Weeton,

Hert- Lionville Laboratory.des by GC Report Date: 08/. 9 15:05

RFW Batch Number:

SampleInformation

8907G709

Cust ID:

RFWl:Matrix:

D.F. :Units:

Client: AVENDT GROUP

All B4-8

001SOIL10.0

UG/KGREPREP

All C2-6.5

005SOIL20.0

UG/KG

Work

All C2-6.5

005 MSSOIL20.0UG/KG

Order: 5160-01-01-0001

All C2-6.5 A16 B9-12

005 MSD 017SOIL SOIL20.0 200

UG/KG UG/KG

Paqe:

A16 C2-5

020SOIL

1

100UG/KG

===== = = = = === ==« = = = M== = = === === ======= = = :«= ===fl = = = = === =

2,4-D2,4,5-TP (Silvex)2,4,5-T

SampleInformation

2,4-D2,4,5-TP (Silvex)2,4,5-T

Cust ID:

RFWf:Matrix:

D.F.:Units:

330 U160 U160 U

PBLK

89LR0653-MB1SOIL10.0

UG/KG

============fl200 U100 U100 U

180 J280 U280 U

PBLK BS

89LR0653-MB1SOIL10.0

, UG/KG

.«*.„__.«..£]

I %

I %

I %I %109 %

PBLK


UG/KG

-.

200 U100 U100 U

I % 13000 UI % 6400 U10 % 6400 U

. j f 1

730037003700

UUU

£•,

U« Analyzed, not detect*!. J= Present below detection limit. B~ Present in blank. NR»= Not requested. NS«%- Percent recovery. .q«4Diluted out. I«= Interference. NA- Not Applicable. *- Outside of EPA CLP QC

Not spiked.

Date post:	26-May-2018
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