IIM

'tarE!PA Region 5 Records Ctr.

301389744 Hea Hand TrailP.O. Etc» 8923Madison Wl 53708-8923Phone: .608)831-4444FAX: (6013)831-33014

Wisconsin Department of Natural Resources

1125 N. Military Avenue

P.O. Box10448

Green Elay, Wl 54307-0448

LETTER OF TRANSMITTAL

DATE: 8 August 2003 JOB NO.: 3452.11

ATTENTION: Ms. Linda Vogen

RE: Lemberger Landfill Superfund Site

Whitelaw, Wisconsin

WE APE SENDING YOU S Attached D Under separate cover via. the following items:

D Cor tract Documents D Purchase OrderID Certificates of Insurance D Copy of letter

D Waiver of LienD Plans

D Laboratory Analysis Report

COPIES

2

2

DATE

8-8-03

8-8-03

NO.

-

-

DESCRIPTION

June 2003 Discharge Monitoring Report

Discharge Monitoring Report - Annual

THESE ARE TRANSMITTED as checked below:

D FOR APPROVAL

D APPROVED AS NOTED

D APPROVED AS SUBMITTED

D SIGN AND RETURN E FOR YOUR USE

D FOR REVIEW AND COMMENT D AS REQUESTED

D RETURNED FOR CORRECTIONS D

REMARKS:

Please contact me at 608-662-5228 if you have questions regarding the enclosed DMR.

TO Mr. Doug Clark - Foley & Lardner

Mr. Darryl Owens - USEPA

Mr. Mark Brooks - RMT/Site Operator SIGNED

Eric Gredell, P.E.Project Manager

Wastewater Discharge Monitoring Short Keport

Facility Name: LEMBERGER LANDFILL SUPERFUND SITEContact Adtliess: 744 Heartland Trail

Madison WI 53717-8923

Facility Contact- Eric Uredell , Senior Consulting EngineerPhone number:' (608)662-5228

Reporting Period: 01/01/2003 - 12/31/2003 Frequency: AnnualForm Due Date: 01/15/2004Permit Number: 0049573

F(ir DNR Use Only

Date Received:DOC: 101323FIN: 11188FID: 436016790Region: NortheastPermit Drafter: David J HantzReviewer: David A GerdmanOffice: Mishicot

SamplePoint

Number

001

1

!

Para-meterSlumber

604

624

368

633

64

181

167

304

393

169

16

51

Ir ssL

'

Parameter

2,4-DimethyIphenol

4-Nitrophenol

Pentachloro- phenol

Phenol

Bis(2-Ethylhexyl) phthalate

Dimethyl phthalate

Di-n-butyl phthalate

'N-Nitrosodiphenyl-amine

PAHs

Di-n-octyl phthalate

Aldrin

BHC beta

BHC gamma (Lindane)

DateSampleTaken

, .6.//3/03

<c/l 3/O3

toflS/o^

(cf i S/O5

(s/ 1 3JOS

1 3/03I f / I f O

• ,fc//T/03

/ // 3 /o<

to//3/03

C.//3/03

/ // 3 1 n~z

tf.ii 7 in ~z

i it ^io<

Sample Type

GRAB

CALCULATED

GRAB

GRAB

CALCULATED

GRAB

CALCULATED

GRAB

CALCULATED

GRAB

CALCULATED

GRAB ]

CALCULATED

GRAB

CALCULATED

GRAB

GRAB

GRAB

CALCULATE!

ORAB

CALCULATEL

GRAB

CALCULATE!

SampleResults

{O.OO12.

0

tO. OO3.O

CO.OOS3.

O

<i0.002(*

O*0.00</3_

O+ D.OO/8

O

^0.00?i<tO

ZO.OO3.O

0

<0t000032

*- 3.fct 0.0071

04.O.OOS4

) 0£.0.0055

1 oi

Units

mg/L

Ibs/day

mg/L

mg/L

Ibs/day

mg/L

Ibs/day

mg/L

Ibs/day

mg/L

Ibs/day

mg/L

Ibs/day

mg/L

Ibs/day

ffc^/day

ug/L

ug/L

ibs/day

ug/L

Ibs/day

ug/Lii lbs,'day

Limit

4.2.^

3/.4t.Sfc

0.1251

2,35

2. i fc«

25.6

22.1

4k3(.fcO

H2101.8121020

M.I

J .SS

0.00/S

k>+*c*

3 9 9.• a o

*****

D.00^1

K«»*3:

Limit Type

Da.i ly Mo.y

MonfhJy AvqDaily Mt^yDAilyM«.)^

MontWy^k'g.

bA.ly H^VMoo+h'yA</3.

Dai /y A-f«-X

Mon+f»ly^i / J .

Da/'y M<t«Mon^hlyAi/3.

Dai/y Ma/

^or>Hi'y4^3'Dai ly Ha.y

hlcnth'y A</*

H o n f f > / y A < / 9 <

Dai ly Max

Monthly Avg

i>ai ly M#-VijMo.rtfhly /Ivti.

LOD

0. 0022.

0.0O2O

Q.OOS2

O.OOK*

0,00^1

O.OO/8

0.0024

0. OO3.O

O.OI2

3, ipO.oo-?/

o-oosy

\O.QO6$

LOQ

0,0012.

O.OObS0.011

Q.00%6

a.ory;

0. 005*1

0.00 22^

O.OCXcb

O.040

12,o.ozt

0,018

o.o/S

QC;xce.

r

>-

• '• , •• . ' • •

LabCertification

Number

VOS/3-275C

t/oS 1 33 7 SO

i/OS 1 3 21 SO

40S(33->SO

ijOSl^ a>1 SO

yoS/ 5 17 SO

V05-/3J.7J-0

<^O SI 3 J.7 £-&

L/OS-/317SV

yO£t$?-T5<J

~IDZ/3l->*u

V^-5"/32.VSO

<JOS-/327SO

<JOf/32~JSC

LjO£'/3'Z-~)S&

t/OStil ISO

«OS,327*V

^SI31-ISC>

<Jo5t2Z-f50

HO f 13^.7 SO

i/OS'/52-75'C5

<J05 1 33-75-0

Fwn,it: 0019573

Wastewater Discharge Monitoring Short Report

SamplePoint

Nurnber

•J'J!

Para-meter

Nuniberji

5291

176

197

232

366

57

31

Parameteri

4,4'-DDT

Dtelrlrin

Endrin

Heptachlor

PCB Total

BUG delta

Antimony, Total Recoverable

DateSampleTaken ii

!1

Sample Typei

1sampleResults Units i

\1 tm;»

GRAB |^ ^m |ng/L \O.*<P

iI • •. T- 1L/II IUL t v l t r ;

bai ly M<x<CALCULATED! Q jibs/day | JGRAB

CALCULATED

GRAB

CALCULATED

GRAB

CALCULATED

GRAB

CALCULATED

GRAB

GRAB

CALCULATED

<O.O/a.

0<O.OO^O

otO.OObb

0

*-2(s,0o

CO. OO£(c

<o.oosz0

ug/L

Ibs/day

ug/L

Ibs/day

ug/L

Ibs/day

ng/L

Ibs/day

ug/L

mg/L

Ibs/day

2.(*>*

0.202

,OOH»6

0.-I12

.oc-032?i

0.001

t+^**

260. tie

1 <? .^ l

Dai ly Ma.*

bfti 'y H<xyMon+hlyA*4.

Da.i ly M<xx

Meanly Av5-

Moo^Jy^^.

Daily M<XJC

Menfhly A^.

t1i-,* iu

/v

O.OI3.

O'OOtO

D.OObb

ZteO

O.OOSk

O.OOSi

1

LOQ

YS-1

O.O^Z

0.03O

0,022

870

o.oiq0.017

1oc

Exce.

-

LabCt^rrifirfltion |

"Number

</05V3Z7b"»

if OS/ 31.7 SO

l/u£/3Z7fD

4vs~/ 33~t*°

</OSV3Z750

t/aSr/SZf^O

</05/'3Z7SO

VoSVJ27St>

</05V3Z73TD

</VS'/327$-D

V05VJ27SO

^VS"/3</03c

VV5"/3V<?3i?

General Remarks

Laboratory Quality Control Comments

Submittal of this form is required by section 283.55, Wis. Stats, and chapters NR 205 and 214, Wis. Adm. Code.

Personally identifiable information collected on this form may be used for purposes other than that for which it was originally collected. Under Wisconsin's open records laws,DNR is required to provide all non-confidential information to any person who requests it. Such information may be provided to the public in written or electronic form.Information reported may be made available to the public via a DNR web page.

1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure thatWastewater Discharge Monitoring FormFacility Name: LHMBERGER LANDFILL SUPERFUND SITEReporting Period: 01/01/2003 - 12/31/2003

Permit: 0049573DOC: 101323 Page 2 of 3

all attachments were prepared under my direction or supervision in accordance with a system designed to assure thatqualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directlyresnonsib!e for "atheriri0 the information the information submitted is to the best of mv know!cd°e and belief true accurate »nd c^rn^l^te I sm s\vare that there ar<5 c- innif ipenalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.

If you have any questions about this form, please call Linda Vogen at (920)492-5900.

Return Form To Authorized Representative Signature Date

Wl Department of Natural ResourcesLinda Vogen1125 N MilitaryGreen Bay, Wl 54307

Operator Signature Certificate Number Date

Make two copies of the completed form. Keep one copy and return the original and one copy to the DNR address provided.

Wastewatcr Discharge Monitoring formFacility Name: LEMBERGER LANDFILL SUPERFUND SITEReporting Period: 01/01/2003 -12/31/2003

Permit: 0049573DOC: 101323 Page 3 of 3

Wastewateir Discharge Monitoring Long Report For DNR Use Only

Facility Narie:Contact Address:

Facility Contact:Phone Number:Reporting Period:Form Due Date:Perm it Number:

LEMBERGER LANDFILL SUPERFUND SITE744 Heartland TrailMadison, Wl 53717-8923Eric Gredell, Senior Consulting Engineer(608)662-522806/01'2003-06/30/200307/15/20030049573

Date Received:DOC:FIN:FID:Region:Permit Drafter:Reviewer:Office:

10590411188436016790NortheastDavid HantzDavid GerdmanMishicot

Sample Results

Sample Point 701Description Influent

Parameter 561Description 1,1,1-Trichloro-

ethaneUnits ug/L

Sample Type GrabFrequency MonthlyFootnotes 2

Day 12345

6

* 7

* 8

Jc 9

101112

•'3 20# l4

* 15* 16

17181920

.* 21* 22* 23

24252627

* 28* 29* 30

31

Total 2 0

701Influent

117Chloroethane

ug/LGrab

Monthly2

<O.<?7

to.97

701Influent

5561,1-Dichloroetha

ug/LGrab

Monthly2

f.o

$.0

701Influent

5701,2-Dichloroetha

ug/LGrab

Monthly2

<L0.3(#

001 001I

Prior to BranchCr211

i Flow Rate

MGDContinuous

Daily1,2

O-ZltSVO. 283470,307/S0. 30873O.ZlOb^0. 3/38^o . mqi0.3/2-12-0.51212-O, 30/710.3IO<J80.297040.322/3O.30W70.30157o.zoWl0. 3/34 7O. 3083/O. 2^7990.2>22~7'?O. -2.13.0kO. 3/20(00, T>/20(cOtiy/^s

' Prior to BranchCr377

pH Field

suGrabDaUjT ^

j*.2g?.28 \

I 2 .2%8.28 j£.28?.2S

[ 8 .2%I 2.2?1 S.2?

3.2%S/2S1 1

!8.2$ ,$.28§.2?S.2??,2g

1

S.28 J0. 2 S8S2 g, 2 g0.320VS- 8.28O. 310^0 8.280. 308780,308720.3087$ 8.28

<o.3(* 9./So4(p

Wastewater Diii;harge Monitoring FormFacility Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003-06/30/2003 DOC: 105904 Page 1 of 29

[•

1SummaryValues

Limit(s) InEffect

QA/QCInformation

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week" 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg_ J22-28) _Monthly Avg

Daily Max

Daily Min

WeeTcly"Average

UOD

LOQ

QCExceedence

La5~Certification

No.

701Influent

5611,1,1-Trichloro-

etbaneUg/L

xxxxxxx

20xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

701Influent

117Chloroethane

ug/LXXXXXXX

^0,17XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

1

o.io

701 j 701Influent

5561,1-Dichloroetha

ug^XXXXXXX

%.oxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

Influent

5701,2-Dichloroetha

ug/LXXXXXXX

<O.3<cxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

[

001 001Prior to Branch

Cr211

i Flow Rate

MOD

O. 3&(pO2.

Prior to BranchCr377

PH Field

suXXXXXXX

0.32313 8,28

0.2.^/^8XXXXXXX

xxxxxxx

?.2fXXXXXXX 1XXXXXXX i

1

xxxxxxx xxxxxxxI

xxxxxxx xxxxxxx

1

0.31 0,75 : 0.3(e

9 o6 o

2.3 3,1 2.4 I.I

yoS/337^0 */OS/337SD i/O5'/337SO ^O^/3Q^^O

Wastewaicr Discharge Monitoring FormFacility Maine LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reportin|;Peri3d: 06/01/2003-06/30/2003 DOC: 105904 Page 2 of29

Sample PointDescription

iParameterDescription

UnitsSample Type

Frequency

FootnotesSample Results E>ay 1

34

5678910111213

001Prior to Branch

Cr457

Suspended Solids,Total

mg/L

Grab

Weekly

+ 3.0

+ 3.0

001Prior to Branch

Cr66

BODS, Total

mg/L

Grab

Monthly

+ 2. O

001Prior to Branch

Cr487

Temperature

degF

Grab

Monthly

SI. 2

S/.$

001Prior to Branch

Cr388

Phosphorus,Totalmg/L

GrabMonthly

<O./2.

001Prior to Branch

Cr789

Nitrogen, Ammonia(NH3-N) Total

mg/L

Grab

Monthly

O.l^

001Prior to Branch

Cr231

Hardness, Total asCaCO3

mg/LGrab

Monthly

. J

37O

15

17

~I3"19"20" SI. 821"2T23

~24

"25

"26 Sl.%11

2829

!

30"3T

Total £2.0 O.ll 370

Wastewziter Discharge Monitoring FormFacility Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 - 06/30/2003 DOC: 105904 Page 3 of 29

SummaryValues

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

001Prior to Branch

Cr457

Suspended Solids,Total

mg/L

0

+ 2.0

<3,0XXXXXXX

xxxxxxx

001Prior to Branch

Cr66

BODS, Total

mg/LXXXXXXX

+ 2,0xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

001Prior to Branch

Cr487

Temperature

degFXXXXXXX

6-J.8xxxxxxx

xxxxxxx

001 001Prior to Branch

Cr388

Phosphorus,Totalmg/L

XXXXXXX

£0. 11xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

Prior to BranchCr789

Nitrogen, Ammonia(NH3-N) Total

mg/LXXXXXXX

o.rtxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx xxxxxxx

xxxxxxx xxxxxxx xxxxxxx xxxxxxx xxxxxxxLimiit(s) In Monthly AvgEffect

QAu'QCInformation

Daily Max

Daily Min

WeeklyAverage

LOD

LOQ

QCExceedence

LabCertification Uyg/3<jD^

No. i

1

^0

001Prior to Branch

Cr231

Hardness, Total asCaC03

mg/LXXXXXXX

380xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

i i

1O.ll

0.3$

!

V^/3^0 WS,3**30 W,3V**>VW3S<XO.

Wastcwaier Discharge Monitoring FormFacility Maine LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003-06/30/2003 DOC: 105904 Page 4 of 29

Sample Poinl1 Descriptioni

Parameter;

Description

UnitsSample Type

I Frequency1 Footnotes

Sample Results Day 1

j_ 2L 3

4

5

r 678910111213141516171819202122232425262728293031

Total

001Prior to Branch

Cr40

Benzene

mg/LGrab

Monthly2

^OeOOO*//

<LO. ooom

001Prior to Branch

Cr40

Benzene

Ibs/dayCalculatedMonthly

<o.ooi too

\

tiD.OOIlOO

001 001 001 001Prior to Branch Prior to Branch Prior to Branch Prior to Branch

Cr Cr Cr Cr80 80 93 93

Bromoform Bromoform Carbon Carbontetrachloride tetrachloride

mg/L Ibs/day mg/L Ibs/dayGrab Calculated Grab Calculated

Monthly Monthly Monthly Monthly

: ,

i

JLO.OOO^y <LO.OOa.S£l t.OeOOoyCj t.O.OOI3!<-/

tiOvOOQl^ £O,OO3.S3I ^-O-OOOyy SO.OOISl*/\

Wastewater I) schargt Monitoring FormFacility Name LEMBKRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting F'eriod: 06/01/2003 - 06/30/2003 DOC: 105904 Page 5 of29

Sample Point{ 001Description

1Parameteri iDescription

UnitsSummary Monthly AvgValues

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Prior to BranchCr40

Benzene

mg/LXXXXXXX

001Prior to Branch

Cr40

Benzene

Ibs/day

O

<o.ooo4l <o.oonooxxxxxxx

xxxxxxx

xxxxxxx

Week 3 Avg ; XXXXXXX(15-21) i

XXXXXXX

xxxxxxx

001Prior to Branc

Cr80

Bromoform

mg/LXXXXXXX

^O.ooomxxxxxxx

xxxxxxx

xxxxxxx , xxxxxxx

xxxxxxx xxxxxxx

Week 4 Avg XXXXXXX XXXXXXX XXXXXXX(22-28)

Limit(s) In Monthly AvgEffect

Daily Max 10.6

Daily Min

WeeklyAverage

0.393 0

o | 58-6 ,

QA/QC LODInformation O.OOO4I

LOQ

001h Prior to Branc

Cr80

Bromoform

Ibs/day

0

<o.ooiS3>: XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.141 c

2

001h Prior to Branch

Cr93

Carbontetrachloride

mg/LXXXXXXX

40.00041XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

001Prior to Branch

Cr

*I_~^_\Carbon

tetrachlorideIbs/day

0

<O.OOI3I4XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

)

70.4

0.165 o

o

0,000^4 o. 00049

ExceedenceLab

Certification yo^/337Sl>No. <«*•/«'*>

O. 0030 O. OOl(0

«>«*„*> </05-/337» *«,„,«, VOSVM7SO

Wasti;watei Discharge Monitoring FormFacility Na-ne LEMBHRGER LANDFILL SUPERFUND SITE Permit: 0049573Reportini;I'erod:06/01/2D03-06/30/2003 DOC: 105904 Page 6 of29

Sample Results

Sample PointDescription

ParameterDescription

Units

Sample TypeFrequency

Footnotes

» Day 1

234

56

78910111213141516171819202122232425262728293031

Total

001Prior to Branch

Cr118

Chloroform

mg/LGrab

Monthly

£O. 00037

< O.OOO 37

001Prior to Branch

Cr118

Chloroform

Ibs/dayCalculated

Monthly

to.oooWz

£O.OOO<?q2

001 001 001 001Prior to Branch Prior to Branch Prior to Branch Prior to Branch

Cr Cr Cr Cr174 174 570 570

Dichlorobromo-methBkhlorobromo-methi,2-Dichloroethad,2-Dichloroetha[bromo-dichlorometl(bromo-dichloromet>!

ug/L Ibs/day mg/L Ibs/day

Grab Calculated Grab CalculatedMonthly Monthly Monthly Monthly

1

I

i

<LO.S(0 ^.D.OOISOI. £O,OO03(0 -tO.OOOybb

• \

i

<:£>,£"& ^O.ODISOl. <O.OOO3b {.O.OOOlbb

Wastewatet D scharge Monitoring FormFacility Name LEMBKRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2303 -06/3(1/2003 DOC: 105904 Page 7 of29

r

SummaryValues

Limit(s) InEffect

QA/Q<rInform alien

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Min

V/eeklyAverage

LOD

001 001Prior to Branch Prior to Branch

Cr Cr118

Chloroform

mg/LXXXXXXX

<0.0003~7XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

57.80

o.ooo^n

118Chloroform

Ibs/day

0

*O.OOOW2XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.115

L°Q 0.0012

o

001Prior to Branch

Cr174

Dichlorobromo-mtth(bromo-dichlorometl

ug/LXXXXXXX

^0.6(oXXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

O. 5" 6

! /. 8

001Prior to Branch

Cr174

Bichlorobromo-mcth[bromo-dichlorometl

Ibs/day

0

<o,ooisozXXXXXXX

001Prior to Branch

Cr570

1,2-Dichloroetha

mg/LXXXXXXX

<D.0003(0

xxxxxxx

xxxxxxx xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.141 o

xxxxxxx

xxxxxxx

xxxxxxx

j 236

O.OOD3

O.OOII

o

fc

001Prior to Branch

Cr570

f^DTchlorbeTiia

Ibs/day

O

<O.OOO^tXXXXXX

xxxxxx

X

x~xxxxxxx

xxxxxxx

xxxxxxx

0.290

ExceedenceLaS

CenificationNo.

5O

Wastcwatei Dscharge Mc^iloring FormFacility Name LEMBHRGER LANDFILL SUPERFUND SITE Permit: 0049573Reportinj; T'ericd: 06/01/2003 -06/30/2003 DOC: 105904 Page 8 of29

Sariample Results

iSample PointDescription

i ParameterDescription

iUnits

[Sample TypeFrequencyFootnotes

Day 12

3

, " 4

56

189

1112

001 | 001Prior to Branch

Cr570

1,2-Dichloroetha

% RemovalCalculatedMonthly

Prior to BranchCr558

1,1-Dichloroethy

mg/LGrab

Monthly

i

001Prior to Branch

Cr558

1,1-Dichloroethy

Ibs/dayCalculatedMonthly

001Prior to Branch

Cr576

1,2-transDichloroethylene

mg/LGrab

Monthly

001Prior to Branch

Cr576

1,2-transDichloroethylene

Ibs/dayCalculatedMonthly

001Prior to Branch

Cr567

1,2-cisDichloroethenr

mgTL

GrabMonthly

i!

I

13 IOO1415

^.O.OOOSl \^.O.OOfS2^

16

.._ . _ .j

^O,OOO%^ <£0'O02.3'8~!*.C>'OOO$3

1718192021

"2T~""23—"24"25~""26"27"28293031

Total / D O ^0,002387

Waste water Discharge Monitoring FormFacility Maine LEMBIiRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003-06/30/2003 DOC: 105904 Page 9 of29

SummaryValues

Limit(s) InEffect

QA/QCInformation

Sample Point 001Description Prior to Branch

Parameter 570Description 1,2-Dichloroetha

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

% RemovalXXXXXXX

/OO

XXXXXXX

XXXXXXX

Week 2 Avg XXXXXXX('8- 14) i

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Min

WeeklyAverage

LOD

LOQ

QCExceedence

001Prior to Branch

Cr558

1,1-Dichloroethy

mg/LXXXXXXX

<LO.COOS1XXXXXXX

001Prior to Branch

Cr558

1,1-Dichloroethy

Ibs/day

O

< 0 > O O I < > 2 1XXXXXXX

XXXXXXX XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX

XXXXXXX XXXXXXX

60.544

i

LabCertification tjo<5/33~?£o

No. '

o

O.OOOS7

o.oo/g

fOS7«7»

XXXXXXX

XXXXXXX

001Prior to Bran

Cr576

1,2-transDichloroethylen

mg/LXXXXXXX

001ch Prior to Branch

Cr

001Prior to Bra

Crnch

576 5671,2-trans

e DichloroethyleneIbs/day

O£0.00081 £0.002387

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX

0.1650

270(

yO f}S~\/~) Q CCs * Ls Cx(— ' O

0.002%

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

2U 0

?1

1,2-cisDichloroetheni:

mg/LXXXXXXX

£O.OOO&xxxxxx

"locxxxx

>3X

X

XXXXXXX

XXXXXXX

XXXXXXX

270

1 O. ooo S

0

' _̂>

0,0026

W5M2WO W.7SO WS/M7*> V«r/327*>

Waste water Discharge: Monitoring FormFacility Maine LEMBEIRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 - 06/30/2003 DOC: 105904 Page 10 of 29

Sample Results

)le Pointcription

ameteri:ription

Jnitspie Typequencyitnotes)ay 1

2

345

6

789101112131415

001Prior to Branch

Cr567

1,2-cisDichloroethene

Ibs/dayCalculatedMonthly

^0.002226

001Prior to Branch

Cr200

Ethylbenzene

mg/L

GrabMonthly

<O.OOOS4

001Prior to Branch

Cr200

Ethylbenzene

Ibs/dayCalculatedMonthly

£0.00)4^$

001Prior to Branch

Cr285

Methylenechloride

mg/L

GrabMonthly

<£O,O0043

001Prior to Branch

Cr285

MethylenechlorideIbs/day

CalculatedMonthly

<O.OOll63

001Prior to Branch

Cr490

Tetrachloro-ethylene

mg/L

GrabMonthly

<O*OOOVS

"T6"T7

~T8~T9^20"21"22

24"25"26"27"28~""29"3031

Ol<ll ^ ^*^o.oo/^^S <z.o.ooo</3 ^0. 0011 S3 ^0.

Wastcwater Discharge Monitoring FormFacility Maine LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Peri 3d: 06/01/2003 -06/30/2003 DOC: 105904 Page 11 of 29

SummaryValues

Limit(s) IrEffect

QA7QC"Information

Sample Point] 001 001Description

ParameterDescription

UnitsMonthly Avg

Da.ily Max

Daily Min

Week 1 Avg(1-7)

Prior to BranchCr567

1,2-cisDichloroethene

Ibs/day

0

±0,D0222bXXXXXXX

Prior to BranchCr200

Ethylbenzene

mg/LXXXXXXX

<O.OOOS4XXXXXXX

XXXXXXX XXXXXXX

Week 2 Avg XXXXXXX(8-14)

Week 3 Avg XXXXXXX(15-21)

Week 4 Avg XXXXXXX(22-28)

Monthly Avg 21.1 oDaily Max

Da.ily Min

WeeklyAverage

LOD

LOQ

QCExceedence

LabCertification t/Q5/327fO

No.

XXXXXXX

XXXXXXX

XXXXXXX

90.630

O.ooost

O.OOH

001 | 001Prior to Branch

Cr200

Ethylbenzene

Ibs/day

0

<o.ooM8XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

110 o

001Prior to Branch Prior to Branch

Cr Cr285

Methylenechloride

mg/LXXXXXXX

285MethylenechlorideIbs/day

O<aoooV3 <o.oons3

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

448

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

3.680

o

001Prior to Branch

Cr490

Tetrachloro-ethylene

mg/L"XXXXXXX"

^.O, ODORS'XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

125'8 \o

O.OOO43

o.ooiy0.000 IS

O.OOUt

xMxnso fos.3^0 <,w3rw6 vor/^fixtor/s^*,

Wastewater Discharge Monitoring FormFacility Name: LEMBEiRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003-06/30/2003 DOC: 105904 Page 12 of 29

Sample R» suit?I

Sample Point 001Description

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Day 123456789

Prior to BranchCr490

Tetrachloro-ethyleneIbs/day

CalculatedMonthly

001Prior to Branch

Cr500

Toluene

mg/LGrab

Monthly

101112

001Prior to Branch

Cr500

Toluene

Ibs/dayCalculatedMonthly

001 | 001 j 001Prior to Branch

Cr561

1,1,1-Trichloro-ethanemg/LGrab

Monthly

Prior to BranchCr561

1,1,1-Trichloro-ethane

% RemovalCalculatedMonthly

Prior to BranchCr561

1,1,1-Trichloro-ethane

Ibs/dayCalculatedMonthly

131415161718

<:<?. 00/207 £O.OOOL>7 ^o.oonli ^D.OOOqo /OO £O.OO3<-J

2021

22232425262728293031

Total < 0. OO 1 J O~7 40.000(.1

\

*0.£>0rt<n\<0.00090 /DO <0.0024l<t

WasU;watcr Discharge Mcnitoring FormFacility Name LEMBHRGER LANDFILL SUPERFUND SITE Permit: 0049573Reportini; Period: 06/01/2003 -06/30/2003 DOC: 105904 Page 13 of29

SummaryValues;

Jmiit(s) InEffect

QA7QC~Information

—

Sample Pointj 001Description

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avgd-7) j

FWeek 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Prior to BranchCr490

Tetrachloro-ethyleneIbs/day

0

+ 0.00/10-1xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

Monthly Avg 0.361

Daily Max

001 \ 001

Prior to BranchCr500

Toluene

mg/LXXXXXXX

<O.OOO(o~lxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

34.918

Daily Min

WeeklyAverage

LOD

Prior to BranchCr500

Toluene

Ibs/day

O

<O.OOI7C?7XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

001Prior to Branch

Cr561

1,1,1-Trichloro-ethanemg/L

XXXXXXX

+o.oc>oc?0

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

596 o

o 139.4 o

001Prior to Branch

Cr561

1,1,1-Trichloro-ethane

% RemovalXXXXXXX

/DOXXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

<?. 00067 o.oocnoL°Q 0.0021 0.0021QC

ExceedenceLab

Certification ^0^/32 7SONo.

yos,^SD vOW3a7«, W«3U7« v««»wo

001Prior to Branch

Cr561 - "

ethaneIbs/day

0

<0.0014Hxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

15.6 \J O

\

W&SO

Wastewatei D'schargc Monitoring FormFacility Name LE MBKRGER LANDFILL SUPERFUND SITE Permit: 0049573Reportinj; Period: 06/01/2003 - 06/30/2003 DOC: 105904 Page 14 of29

Sample Results

Sample Point; 001Description

ParameterDescription

Units

Sample Type

Frequency

FootnotesDay 1

2

4

Prior to BranchCr508

Trichloroethylen

mg/L

GrabMonthly

56 i7

8 ;

001Prior to Branch

Cr508

Frichloroethylen

Ibs/day

CalculatedMonthly

001Prior to Branch

Cr517

t Vinyl chloride

ug/LGrab

Monthly

j

9 :

10

11

12

001Prior to Branch

Cr517

Vinyl chloride

Ibs/day

CalculatedMonthly

001Prior to Branch

Cr229

Halomethanes,Totalug/L

Grab

Monthly

13 tO.OOOyg <0.00/J.8g ^.O.lS <O.000483 ^O.I'J1415

001Prior to Branch

Cr229

Halomethanes,Total

Ibs/dayCalculated

Monthly

<0. OO2.S3I

1617

~T81920

rh

21

~~22

"23

""24

"25

"27

"28"29

"~30

~"3T

Total '-40.00252

Wastewater Discharge Monitoring FormFacility Name LEMBEiRGER LANDFILL SUPERFUND SITE Permit: 0049573Reportinj'Pericd: 06/01/2003-06/30/2003 DOC: 105904 Page 15 of 29

7 "

SummaryValues;

Limit(s) InEffect

QA/QCInformation

Sample PoinlDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

001Prior to Branch

Cr508

Trichloroethylen

mg/LXXXXXXX

4.0.00048XXXXXXX

XXXXXXX

Week 2 Avg XXXXXXX(8-14)

001Prior to Branch

Cr508

Trichloroethylen

Ibs/day

0

^0.00(28$XXXXXXX

XXXXXXX

XXXXXXX

Week 3 Avg XXXXXXX XXXXXXX(15-21)

Week 4 Avg ' XXXXXXX XXXXXXX(22-28)

Monthly Avg

Daily Max 81.4

0.392 0

001Prior to Branc

Cr517

E Vinyl chloride

ug/LXXXXXXX

4.0.18XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

Daiily Min

V/eeklyAverage

O.OOO^SLOO

V.OOIS

< O. iS

QCExceedence

LabCertification t^o 5- / 3J) TfTD yo S / 3 ̂ "?.TO

No.

O.57

001ti Prior to Branch

Cr517

Vinyl chloride

Ibs/day

O

< 0.000483XXXXXXX

XXXXXXX

XXXXXXX

001Prior to Branch

Cr229

Halomethanes,Totalug/L

XXXXXXX

4.0.94XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX

XXXXXXX XXXXXXX

001Prior to Branch

Cr229

Halomethanes,Total

Ibs/day

O

+ O.002.S3IXXXXXXX

XXXXXXX

XXXXXXX

xxxxx>:x

XXXXXXX

0.0117 0.141

0.94

3.0

Wr/azTffoW/^sov^/s^so**/*:^

Wastcwater Discharge Monitoring FormFacility Maine LEMBF.RGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 -06/30/2003 DOC: 105904 Page 16 of29

: I ruui.iiui.c9

'Sample Results] Day 1

Sample Point

Description

Parameter

Description

Units

Sample Type

Frequency

Footnotes

Day 1

34567891011121314151617181920

- -21 -222324252627282930

001Prior to~Branch

Cr117

Chloroethane

ug/L

Grab

Monthly

^0.17

001Prior to Branch

Cr117

Chloroethane

% Removal

Calculated

Monthly

/OO

\\1

j

001Prior to Branch

Cr556

1,1-Dichloroetha

ug/L

Grab

Monthly

4-o.is

001 j 001

Prior to BranchCr556

1,1-Dichloroetha

% Removal

Calculated

Monthly

100

1

i

\ Prior to BranchCr35

\ Arsenic, TotalRecoverable

ug/L

Grab

Monthly

O.t,

:̂ i

001Prior to Branch

CrT5 ~"~

Arsenic, TotalRecoverable

Ibs/day

Calculated

Monthly

1

,

i

i

< D.OQbQltj- '

i I iI I : :

ii i

31 ! ;

l. Total loo /oo

Waste water Discharge Monitoring FormFacility Name: LEMB1ERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting I'enod: 06/01/2003 -06/30/2003 DOC: 105904 Page 17 of 29

Summary(Values;

i

Limit(s) InEffect

QA/QCInformation

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

001Prior to Branch

Cr117

Chloroethane

ug/LXXXXXXX

^o.nXXXXXXX

XXXXXXX

001Prior to Branch

Cr117

Chloroethane

% RemovalXXXXXXX

IOOXXXXXXX

XXXXXXX

XXXXXXX XXXXXXX

Week 3 Avg XXXXXXX(15-21)

Week 4 Avg XXXXXXX(22-28)

Monthly Avg;

Daily Max

Daily Min

WeeklyAverage

LOD

L.OQZ. I

QCExceedence

LabCertification

No.

XXXXXXX

001Prior to Branch

Cr556

1,1-Dichloroetha

ug/LXXXXXXX

^o.-i^XXXXXXX

XXXXXXX

XXXXXXX

001 001Prior to Branch

Cr556

1,1-Dichloroetha

% RemovalXXXXXXX

100XXXXXXX

XXXXXXX

XXXXXXX

Prior to BranchCr35

1 Arsenic, TotalRecoverable

ug/LXXXXXXX

^2,<oXXXXXXX

OXXXXXXX XXXXXXX

1XXXXXXX XXXXXXX XXXXXXX ;

0.15

2,4

001Prior to Branch

Cr35

Arsenic, TotalRecoverable

Ibs/day

O

<O.OO(o9 7VXXXXXXX

xxxxxx

xxxxxx

X

x~

XXXXXXX

xxxxxx

3.88

727.6 0

X

O

51 o .

2.(*

2-7'.

WWSB ̂ s,W£0 **•/»,*, v«r/3«rt Wr«y«o Wwojo

Wastewaler Discharge Monitoring FormFacility Maine LEMBLRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 - 06/30/2003 DOC: 105904 Page 18 of 29

Sample PointDescription

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Sample Results Day 1

234

5678910111213141516

" "17181920

212223 ;2425262728293031

Total !

001Prior to Branch

Cr50

Beryllium, TotalRecoverable

ug/L

GrabMonthly

< O .2 I

^D.2.1

001Prior to Branch

Cr50

Beryllium, TotalRecoverable

Ibs/dayCalculatedMonthly

^D.OOO5(f3

^O.OOOSio3

001 001 001 001Prior to Branch Prior to Branch Prior to Branch Prior to Branch

Cr Cr Cr Cr87 87 126 126

Cadmium, Total Cadmium, Total Chromium +3 Chromium +3Recoverable Recoverable

ug/L Ibs/day mg/L Ibs/dayGrab Calculated Grab Calculated

Monthly Monthly Monthly Monthly

1

!• : :

I

:

^O,l5 <0*OOO4o2. 40.OOI7 tiO.OoygJeO

I !

i

+ D.IS < 0.000^02.- 4.0.0017 ±D.004£<eQ

Wastewater Discharge Monitoring FormFacil ity Name: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting I'erod: 06/01/2003 -06/30/2003 DOC: 105904 Page 19 of 29

l

SummaryValue:;

i1I

Limit(s) InEffect

QA/QCInformation

Sample Point 001Description

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

Monthly Avg

Daily Max

Daily Min!

WeeklyAverage

LOD

LOQ

QCExceedence

LabCertification

No.

\ 001Prior to Branch

Cr50

Beryllium, TotalRecoverable

ug/LXXXXXXX

40.21xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

4660

0. 2/

0.70

</ys73</0

Prior to BranchCr50

Beryllium, TotalRecoverable

Ibs/day

0

+ D.OOOS£3XXXXXXX

xxxxxxx

xxxxxxx

001Prior to Branc

Cr87

Cadmium, TotalRecoverable

ug/LXXXXXXX

001h Prior to Branch

Cr87

Cadmium, TotalRecoverable

Ibs/day

O

001Prior to Bran

Cr126

Chromium +

mg/LXXXXXXX

^O.iS 1^.0.000^02. <D,OOI~Ixxxxxxx

Oxxxxxxx

xxxxxxx

0.00258

O

O

27.08

' °'573 O

5o

0. 16

O.SD

XXXXXXX XXXXXXX

xxxxxxx

xxxxxxx o

xxxxxxx

xxxxxxx

0.775

)

09.2 c

0.046 ,

o.ocn0.0057

001 "ch Prior to Branch

Cr126

3 Chromium +3

Ibs/day

O

<co.ooys(i,oxxxxxxx

xxxxxxx

xxxxxxx:

xxxxxxx

xxxxxxx

109700 1

) 1

mw«o -w«^«o vW3^5OjHKW*

Wastewater Discharge Mcinitoring FormFacility Name: LEMB1SRGER LANDFILL SUPERFUND SITE Permit: 0049573Reportin.? Per od: 06/01/2003 - 06/30/2003 DOC: 105904 Page 20 of 29

Sample PointDescription

Sample Results

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Day 1

001rior to Branch

Cr147

Copper, TotalRecoverable

"ugTL"

GrabMonthly

001Prior to Branch

Cr155

Cyanide, Total

ug/LGrab

Monthly

001Prior to Branch

Cr155

Cyanide, Total

Ibs/day

Calculated

001 001Prior to Branch

Cr264

L"d, TotalRecoverable

mg/L

MonthlyGrab

Monthly

Prior to BranchCr264

Lead, TotalRecoverable

Ibs/day

CalculatedMonthly

001Prior to Branch

Cr280"

Mercury, TotalRecoverable

ngftr

"Grab"Monthly

8""9"TO"~T\~T2

"T4

"T5

^0.53

161718

~T9"20"21

/. 5

22"23"24"25"26

"28

"29~""30~"

j

Total + O.O007S

Wastcwai.er Discharge: Monitoring FormFacility Mams: LEMBF.RGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Periad: 06/01/2003 - 06/30/2003 DOC: 105904 Page 21 of 29

SummaryValues;

Limit(s) InEffect

Sample PointDescription

ParameterDescription

UnitsMonthly Avg

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

001 j 001Prior to Branch

Cr147

Copper, TotalRecoverable

ug/LXXXXXXX

<O.S3XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

Week 4 Avg XXXXXXX(22-28)

Monthly Avg

Daily Max 93.34

Da.ily Min

WeeklyAverage

Prior to BranchCr155

Cyanide, Total

ug/LXXXXXXX

*I.SXXXXXXX

001Prior to Branch

Cr155

Cyanide, Total

Ibs/day

O

<O. 004024

XXXXXXX

XXXXXXX XXXXXXX

XXXXXXX XXXXXXX

XXXXXXX XXXXXXX

001Prior to Bran<

Cr264

Lead, TotalRecoverable

mg/LXXXXXXX

001 001:h Prior to Branch

Cr264

Lead, TotalRecoverable

Ibs/day

O

<O.OOO~fS <O.OO2Ol3.xxxxxxx

0

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX XXXXXXX ;

o

QA/QC LOD - -,Information C/»oo

44.8 o

/.-s

47O

1.37(

0.0145

O.OOO1S

XXXXXXX

3.86 o

*2

Prior to BranchCr280

Mercury, ToRecoverabl

ngTL

a

+ S(e

tale

XXXXXXX

XXXXXXX

XXXXXXX

XXXXXXX

xxxxxxX

o

S6LOQ

"QC~ .Exceedence A

TJ5BCertification

No.

s.o O.OO2S

X X 11

Wastcwaier Discharge Monitoring FormFacility Maine: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Perisd: 06/01/2003-06/30/2003 DOC: 105904 Page 22 of 29

Sample Results

Sample Poinf' Description

ParameterDescription

UnitsSample Type

FrequencyFootnotes

Day 12

34

567

r :8 -9

L 10 .r "12

001Prior to Branch

Cr280

Mercury, TotalRecoverable

Ibs/dayCalculatedMonthly

001Prior to Branch

Cr315

Nickel, TotalRecoverable

mg/L

GrabMonthly

001Prior to Branch

Cr315

Nickel, TotalRecoverable

Ibs/day

CalculatedMonthly

001Prior to Branch

Cr423

Selenium, TotalRecoverable

ug/L

GrabMonthly

001Prior to Branch

Cr423

Selenium, TotalRecoverable

Ibs/dayCalculatedMonthly

001Prior to Branch

Cr430

Silver, TotalRecoverable

ug/LGrab

Monthly

£0,003151

15"16'Yt"18"19

21"22

"232425zo2728

~"29""30""31

Total :O.OO2$

Wastewaier Discharge Monitoring FormFacility Maine LEMBE:RGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 -06/30/2003 DOC: 105904 Page 23 of 29

\

SummaryValues

iLimiit(s) InAffect

bx/QcInformation

Sample Point! 001Description

Ta rameterDescription

UnitsMonthly Avg

Daily Max

Dziily Min

Week 1 Avg(1-7)

Week 2 Avgi (8-14)Week 3 Avg

(15-21)Week 4 Avg

(22-28)

001Prior to Branch

Cr280

Mercury, TotalRecoverable

Ibs/day

O

^o.oooiSoXXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

Monthly Avg 0.0062

Daily Max

Da.ily Min

WeeklyAverage

L.OD

LOQ

QCExceedence

LabCertification iJij^/St/o

No.

Prior to BranchCr315

Nickel, TotalRecoverable

mg/LXXXXXXX

^0,OO3SXXXXXXX

O

O5.06

0.052

O < OO3

o.ootis

3oWsV3</0«

001Prior to Branch

Cr315

Nickel, TotalRecoverable

Ibs/day

O

*o.oo(.™<oxxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

001 001 001Prior to Branch Prior to Branch Prior to Branch

Cr Cr Cr423

Selenium, TotalRecoverable

ug/LXXXXXXX

*/./xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx xxxxxxx

13.1

O

0

> !

50

O\ 116

423 430Selenium, Total Silver, Total

Recoverable RecoverableIbs/day

0<0. 00 J. 75 /

ug/LXXXXXXX

^>.vs-XXXXXXX XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

xxxxxxx

0.785

)

I . I3.7

O12.16

O

2.03 Q

O,4S

1.6

^S,3^30 WMVMOWM^SO WSM030

Wastewater Discharge Monitoring FormFacility Name: LEMBIiRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Per od: 06/01/2003 - 06/30/2003 DOC: 105904 Page 24 of 29

Sample Results

Sample Point

Description

Parameter

Description

Units

Sample Type

Frequency

Footnotes

Day 1

234

5

7891011121314

1516171819202122232425262728293031

Total

001

Prior to BranchCr430

Silver, TotalRecoverable

Ibs/day

Calculated

Monthly

£0.00/30-7

\

1

^0. OO/307

001Prior to Branch

Cr553

Zinc, TotalRecoverable

ug/L

Grab

Monthly

<0.%0

<D.%0 \

\ 0011 Prior to Branch

Cr553

Zinc, TotalRecoverable

Ibs/day

Calculated

Monthly

+ O.OO2/^Lf

,

t-0.b03.i4b

001 001Prior to Branch Prior to Branch

Cr Cr251 27

Iron, Total Aluminum, TotalRecoverable Recoverable

mg/L mg/L

Grab Grab

Monthly Monthly

^O'O/g ^O.OO-?7

^0.0/8 +0,0077

DO!"" ]Prior to Branch

Cr"105" "

Chloride

mg/L

Grab

Monthly

/£

13

Wastewatei ]>!,chargi: Monitoring FormFacility Name LEMBHRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2D03 - 06/30/2003 DOC: 105904 Page 25 of 29

1 Sample PointDescription

|i ParameteriDescription

iUnits

Summary Monthly AvgValues

Daily Max

Daily Min

Week 1 Avg(1-7)

Week 2 Avg(8-14)

Week 3 Avg(15-21)

Week 4 Avg(22-28)

jLimit(s) In Monthly AvgEffect

001Prior to Branch

Cr430

Silver, TotalRecoverable

Ibs/day

O

±0.00/307XXXXXXX

xxxxxxx

xxxxxxx

xxxxxxx

001Prior to Branch

Cr553

Zinc, TotalRecoverable

ug/LXXXXXXX

*o.8t>xxxxxxx

o

001Prior to Branch

Cr553

Zinc, TotalRecoverable

Ibs/day

O

* -0.00314(0XXXXXXX

001Prior to Branch

Cr251

Iron, TotalRecoverable

mg/LXXXXXXX

<0.0/8xxxxxxx

xxxxxxx

xxxxxxx oxxxxxxx

xxxxxxx

0.458

Daily Max j

' Daily Min

WeeklyAverage

QA/QC LODInformation

LOQ

QCExceedence

LabCertification i/t/^ /3^o3

No.

o572

43.7

0.80

xxxxxxx ;

0

0

<3.7

X

0 MSJ3401\

391 o

333

0.0/2

O.D(j>O

001 001Prior to Branch Prior to Branch

Cr Cr27 105

Aluminum, Total ChlorideRecoverable

mg/L mg/L,XXXXXXX XXXXXXX

^0.00-7-7 ISxxxxxxx xxxxxxx

xxxxxxx

XXXXXXX . g.

xxxxxxx

xxxxxxx

2.2

o0. OO1

0 "*~ o

133 o1

7

D.OZl*

X

>O VVS'/SC/OSD YVSVJtfOSO y</S'/34O30 ^573^030

Wastewatei Discharge Monitoring FormFacility Name LEMBHRGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2D03- 06/30/2003 DOC: 105904 Page 26 of 29

[Sample Point 001Description

Parameter"Description

UnitsSample Type

Prior to BranchCr

L

Sample Results Day 1

FrequencyFootnotes

7~~8""5

531Additive Water

Treatment - SpecifyIbs/day

Record ofAddition

Daily

1112

"T4~""T5~""T6~

17

"T9~"

"21'22•2T""24"25"26"2728

"29"3031

Total

Wastewater O:schargc Monitoring FormFacility Maine LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 - 06/30/2003 DOC: 105904 Page 27 of 29

Sample Pointj 001Inscription ! Prior to Branch

: CrParameter

SummaryValues

531Description Additive Water

UEIfcTreatment - Specify

Ibs/dayMonthly Avg

""DailyMax"

Dailv M&~

Week 1 Avg(1-7)

xxxxxxx

"Week 2 Avg XXXXXXX

"Week 3 Avg] XXXXXXX"(15-21)

pniit(s)lrEffect

4 Avg"__C22-28)_

"TMonthiy Avg

XXXXXXX

f Dally Max

Deiily Mm

SJS/QC[Information

V/eeklyAverage

LOD

LOQ

"QCExceedence

~1̂ BCertification

No.

Wastcwal:er Discharge Monitoring FormFacility Name: LEMBE:RGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting Period: 06/01/2003 -06/30/2003 DOC: 105904 Page 28 of 29

Footnotes

1. Results of annual priority pollutant and RCRA Appendix 9 must be attached to DMR.2.Only VOCs detected in influent or effluent must be on DMR. Attach all VOC results.3. Altach monthly record of water treatment additive use.

General Remarks

7~.hese PlowJ values are averages oP a total //ou/ taken on a.^j

The Monday value vJOuld be a total -for 3the

Laboratory Quality Control Comments

x = j^ ,aM val ida t ion r u / e < > resu/ t as nondetect due to

se detect/on in the associated blank.

Submiital of this form is required by section 283.55, Wis. Stats, and chapters NR 205 and 214, Wis. Adm. Code.

Personally identifiable information collected on this form may be used for purposes other than that for which it was originally collected.Under Wisconsin's open records laws, DNR is required to provide all non-confidential information to any person who requests it. Suchinformation may be provided to the public in written or electronic form. Information reported may be made available to the public via aDNR web page.

I certify under penally of law that this document and all attachments were prepared under my direction or supervision in accordance with asystem designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of theperson or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is,to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false•information, including the possibility of fine and imprisonment for knowing violations.

If you have any questions about this form, please call Linda Vogen at (920)492-5900.

Return Form To Authorized Representative Signature Date

WI Department of Natural Resources

Linda Vogen pnBoy~1044a112:5 N Military PU BUA limo

Green Bay, Wl 54307

LSRGrOperator Signature Certificate Number Date

Mzike two copies of the completed form. Keep one copy and return the original and one copy to the DNR address provided.

Wastcwaler Discharge Monitoring FormFacility Maine: LEMBERGER LANDFILL SUPERFUND SITE Permit: 0049573Reporting; Period: 06/01/2003-06/30/2003 DOC: 105904 Page 29 of 29

En Chem Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-<.69-8827

Analytical Report Number: 835514

Client: RMT - MADISON

Project Name : LEMBERGER LANDFILL

Project Number: 3452.11

Field II) : ANNUAL INFLUENT

Matrix Type : WATER

Collection Date : 06/13/03

Report Date : 07/29/03

Lab Sample Number : 835514-001

INORG'ANICS

Test

Antimony

Arsenic

Beryl iuin

Cadrriiu.riChromium

Coppsr

LeadMercuryNic<el

SeleniumSilver

ThalliumZinc

VOLATILES- SPECIAL

Ana lyte

1,1,1-Trii:hloroe thane1 , 1 , 2 ,2-T etra chl Droe thane

1,1, 2-Trii:hloroe thane1,1-Di:hl:roeth£ine

I.l-Dichbroethane

1,2-Diohloroethsme

1.2-[)ii:hloroethene, Total

1,2-Dichloropropane2-Chlc roi j :hylvinylether

Acrolein

Acryloiitii e

BenzeneBrorncdicJiloromethEirie

BrorncformBrornomolhane

Carbon TetrachlorideChlorobeazene

Chic rodibromom ethane

ChloroethcineChlorofom

Chlorome thanecis-1 ,3-Dichloropropene

Ethylbon;:(:ne

F'luorolnctiloromathaneMethyl3m;Chlorde

Result

< 5.2

< 2.6

< 0.21

< 0.15

< 1.7

1.7

< 0.75

< 0.056< 4.2

1.4

< 0.45

< 5.6

< 2.1

LIST

Result

20

< 0.20

< 0.42

8.0

1.5

< 0.36

5.0

< 0.46

< 0.95

< 10

< 1.3< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.41

< 0.81

< 0.97

< 0.37< 0.24

< 0.19

< 0.54

< 0.79

< 0.43

LOD

5.2

2.6

0.21

0.15

1.7

0.53

0.75

0.0564.2

1.1

0.45

5.6

2.1

LOD

0.90

0.20

0.42

0.75

0.57

0.361.4

0.46

0.95

10

1.30.41

0.56

0.94

0.91

0.49

0.41

0.81

0.97

0.370.24

0.19

0.54

0.79

0.43

LOQ

17

8.7

0.70

0.50

5.7

1.8

2.5

0.1914

3.7

1.5

19

7.0

LOQ

3.0

0.67

1.4

2.5

1.91.2

4.7

1.5

3.2

33

4.3

1.4

1.9

3.1

3.0

1.6

1.4

2.7

3.2

1.20.80

0.63

1.8

2.6

1.4

EQL Dil. Units

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

EQL Dil. Units

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

Analysis Prep AnalysisCode Date Method Method

06/20/03 SW8463005A SW846 6010B

06/20/03 SW8463010A SW846 6010B

A 06/20/03 SW8463010A SW8466010B

06/24/03 SW8463020A SW846 713106/20/03 SW8463010A SW8466010B

QA 06/20/03 SW8463010A SW846 6010B

06/27/03 SW8463020A SW846 7421

06/19/03 SW8467470 SW846 7470A06/20/03 SW8463010A SW8466010B

Q 06/25/03 SW8467740 SW846 774006/24/03 SW8463020A SW846 776106/20/03 SW8463010A SW846 6010B

06/20/03 SW8463010A SW8466010B

Prep Date: 06/19/03

Analysis Prep Method AnalysisCode Date Method

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B06/19/03 SW8465030B SW846 8260B

Q 06/19/03 SW8465030B SW846 8260B

06/19/03 SW846 5030B SW846 8260B06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SWB46 8260B06/19/03 SW8465030B 8W846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B06/19/03 SW8465030B SW846 8260B06/19/03 SWS465030B SW846 8260B

En Chemi Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-469-8827

Analytical Report Number: 835514

Client: RMT- MADISON

Project Mame : LEMBERGER LANDFILL

Proj act Number: 3452.11

Field II): ANNUAL INFLUENT

Matrix Type: WATER

Collection Date : 06/13/03

Report Date : 07/29/03

Lab Sample Number : 835514-001

VOLATILES • SPECIAL LIST

Analyte

Tetra^hbroethesne

Toluene

trans- 1 ,:i-Dichforop -opene

TrichlorC'Othene

Vinyl Chloride

Result

< 0.45

< 0.67

< 0.19

2.7

< 0.18

LOD

0.45

0.67

0.19

0.48

0.18

LOQ

1.5

2.2

0.63

1.60.60

EQL Oil. Units

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

SEMIVOLATILES - SPECIAL LIST

Amilyte

1 ,2,4-Tn -hlorobenzisne

1,2-Dichiorobenzene

1 ,2-Diphenylhyclrazine

1 ,3-Dich orobenzenij

1,4-Dichcirobenzeni3

2,2'-oxyti:3(1-Chlorapropane)

2,4,5-Tridilorophenol

2,4-Dishlcrophenol

2,4-DiTietnylphejnol

2,4-Dhitiophenol

2,4-Dhitiotoluerie

2,6-Dinitiotoluene

2-Chloroiiaphthalene

2-Chloro|)-ienol

2-NitropNinol

3,3- Dichlorobenzidir e

4,6Oinitrc-2-methylphenol

4-Brono|nenyl =henyl Ether

4-Chlcro-o-rretriylprienol

4-Chlcro|>henyl Phenyl Ether

4-Nilrcphenol

Acenaph:hene

Acenaptrhylene

Anthracene

Benzidnc!

Ben::o(a)anthracene

Eien;:o(£):DyreneBen::o;t)iljoran1hens

Ben::o;grTiperyleneE!en;io(k)'lijoranthene

bis(2:-Chliroethoxy)methane

bis(2-CHiroethyl)etrer

bis(2:-Ethylhexyl)phthalate

Result

< 1.5

< 4.2

< 2.3

< 3.7

< 4.1

< 2.0

< 1.5

< 1.8< 2.2

< 1.7

< 1.4

< 1.2

< 1.7

< 4.9

< 1.4

< 2.9

< 3.6

< 1.6

< 1.5

< 1.6< 2.0

< 2.2

< 1.8

< 1.9

< 13< 2.4

< 2.8

< 3.0

< 3.5< 2.4

< 1.8

< 5.0

< 4.2

LOD

1.5

4.2

2.3

3.7

4.1

2.0

1.5

1.8

2.2

1.7

1.4

1.2

1.7

4.9

1.4

2.9

3.6

1.6

1.5

1.6

2.0

2.2

1.8

1.9

13

2.4

2.8

3.0

3.52.4

1.8

5.0

4.2

LOQ

4.9

14

7.8

12

14

6.5

5.1

5.9

7.2

5.5

4.7

4.1

5.7

16

4.8

9.7

12

5.4

5.0

5.4

6.5

7.4

6.1

6.3

44

7.8

9.3

1012

8.1

6.117

14

EQL DM. Units

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

Prep Date: 06/19/03

Analysis Prep Method AnalysisCode Date Method

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 B260B

06/19/03 SW846 5030B SW846 8260B

06/19/03 SW8465030B SWB46 8260B

06/19/03 SW846 5030B SW846 8260B

Prep Date: 06/20/03

Analysis Prep Method AnalysisCode Date Method

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW846 3510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

& 06/24/03 SW846 3510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW846 3510C SW846 8270C

06/24/03 SWB463510C SW846 8270C

06/24/03 SW846 3510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 B270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW846 3510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

06/24/03 SW8463510C SW846 8270C

En Chemi Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-469-8827

Analytical Report Number: 835514

Client: RMT - MADISON

Project Name : LEMB=RGER LANDFILL

Project Number: 3452.11

Field 1C): TRIP BLANK

Matrix Type: WATER

Collection Date : 06/13/03

Report Date: 07/29/03

Lab Sample Number : 835514-002

VOLATILES • SPECIAL LIST

Analyte Result LOD

1,1,1-TrchloroEithane

1.1 ,2,2-"etrachloroothane

1,1,2-Trichloroeithane

1,1-Dichloroethane

1,1-D'Chloroethsne

1,2-Dchloroethane

1,2-Dchloroethene, Total

1,2--Dchic)ropropan<5

2-Chlorcethylvinylether

Acrolein

Acrylonilrle

Benzene

Bromodi ̂ loramethaneBroiTiofo.in

Bromom ethane

Carbon TfjtrachlorideChlorobenzene

Chlorodiliromomethane

Chlorcie thane

Chloroform

Chloromtithane

ds-'l ,0-Dichloropropene

Ethylben .rane

Flucrotrichloromethcine

Methyiene Chloiide

Tetrachlcroethene

Toluene

tranis-i ,3 -DichloropropeneTrichloros:hene

Vinyl Chi ride

< 0.90

< 0.20

< 0.42

< 0.75

< 0.57

< 0.36

< 1.4

< 0.46

< 0.95

< 10

< 1.3< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.41

< 0.81

< 0.97

< 0.37

< 0.24

< 0.19

< 0.54

< 0.79

0.55

< 0.45

< 0.67

< 0.19

< 0.48

< 0.18

0.90

0.20

0.42

0.75

0.57

0.36

1.4

0.46

0.95

10

1.30.41

0.56

0.94

0.91

0.49

0.41

0.81

0.97

0.37

0.24

0.19

0.54

0.79

0.43

0.45

0.67

0.19

0.48

0.18

LOQ EQL DM.

3.0

0.67

1.4

2.5

1.9

1.2

4.7

1.5

3.2

33

4.3

1.4

1.9

3.1

3.0

1.6

1.4

2.7

3.2

1.2

0.80

0.63

1.8

2.6

1.4

1.5

2.2

0.63

1.6

0.60

11

1

1

1

11

1

1

1

11

11

1

11

1

1

1

1

1

1

11

1

1

1

1

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

AnalysisCode Date

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

Q 06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

Prep Date: 06/19/03

Prep Method AnalysisMethod

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SWB46 8260B

SW846 8260B

SW846 8260B

SW846 B260B

SW846 8260B

SW846 8260B

SW846 8260 B

SW846 8260B

SW846 8260B

SW646 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

3W846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

3W846 8260B

En Chem Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-469-6827

Analytical Report Number: 835514

Client: RMT - MADISON

PrcjecJ Kama : LEMBERGER LANDFILL

Project Number: 3452.11

Field ID: STORAGE BLANK

Matrix Type: WATER

Collection Date : 06/13/03

Report Date: 07/29/03

Lab Sample Number : 835514-003

VOLATILES » SPECIAL LIST

Analyte Result LOD

1 , 1 , 1 -Tr chloroethane

1,1 ,2,2-"etrachloroi3thane1,1,2-Trichloroethane

1,1-D'Chloro ethane

1,1-D'Chloroethene1,2-Dichoroethane

1,2-Dichioroethene, Total1 ,2-Dichioropropane2-Cfiloroethylvinylether

Acrolein

Acrylonitrile

BenzeneBromodiciloronriethane

Bromofo'inBromomsthane

Carbon Tetrachlorids

Chlorobenzene

Chlorodiliromom ethaneChloroethane

ChlorofoirnChloromoihane

cis-1 ,3-DichloropropeneEthylben'aneFlucrotrichloromethane

Methyene Chloride~retrachloroethene

Toluenetrams-" ,3 -Dichloropropene

TrichloroistheneVinyl Chloride

< 0.90

< 0.20

< 0.42

< 0.75

< 0.57

< 0.36

< 1.4

< 0.46< 0.95

< 10

< 1.3

< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.41

< 0.81

< 0.97

< 0.37

< 0.24

< 0.19

< 0.54

< 0.79

0.68

< 0.45< 0.67

< 0.19

< 0.48

< 0.18

0.90

0.20

0.42

0.75

0.57

0.36

1.4

0.46

0.95

10

1.3

0.41

0.56

0.94

0.91

0.49

0.41

0.81

0.97

0.37

0.24

0.19

0.54

0.79

0.43

0.45

0.67

0.19

0.48

0.18

LOQ EQL DM. Units

3.0

0.67

1.4

2.5

1.9

1.2

4.7

1.53.2

33

4.3

1.4

1.9

3.1

3.0

1.6

1.42.7

3.2

1.2

0.80

0.63

1.8

2.6

1.4

1.52.2

0.63

1.6

0.60

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

AnalysisCode Date

06/19/03

06/19/0306/19/03

06/19/03

06/19/0306/19/03

06/19/03

06/19/0306/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/0306/19/03

06/19/03

06/19/0306/19/03

06/19/03

06/19/0306/19/03

06/19/03

06/19/03

06/19/03

Q 06/19/03

06/19/03

06/19/0306/19/03

06/19/0306/19/03

Prep Date: 06/19/03

Prep Method AnalysisMethod

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 8260B

SW846 8260B

SW846 8260BSW846 8260B

SW846 8260B

SW846 8260B

SW846 8260BSW846 8260BSW846 8260BSW846 8260B

SW846 8260B

SW846 8260B

SW846 8260BSW846 8260B

SW846 8260B

SW846 8260B

SW846 8260BSW846 8260B

SW846 8260B

SWB46 8260BSW846 8260B

SW846 8260B

SW846 8260BSW846 8260B

SW846 8260B

SW846 8260B

SW846 8260 BSW846 8260B

SW846 8260B

SW846 8260B

En Chem Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-469-8827

Analytical Report Number: 835518

Client: RMT-MADISON

Project Name : LEMBERGER LANDFILL

Project Number: 3452.11

Field ID: TRIP BLANK

Matrix Type: WATER

Collection Date : 06/13/03

Report Date : 07/29/03

Lab Sample Number : 835513-003

VOLATILES - SF>ECIAL LIST

Analyte Result LOD

1,1,1-Trichloroethaie

1 , 1 ,2,2- retracriloroethane

1,1,2-Tri<:hloroi3thane

1,1-Cichloroethane

1,1-CicHaroethene

1,1-DicMoropropen3

1,2-Dic.Moroethane

1 ,2-Dicr loroethene, Total

1,2-DicHoropropani32,3-Dichloropropeni3

2-C hi DroesthylvinylelherAcrolein

Acryloniirile

Benz«:ne

BromodichloromethaneBromoform

Bromomethane

Carbon ~3trachloride

Chlorobenzene

Chlorodibromomethane

Chloroet'iane

Chlorofo in

Chlororvi thane

cis- 1 ,?.-Dichloroethene

cis-1,3-Dii:hloropropeneDichloroclifluoromethane

Ethylben.:ene

l-luorotricihloromethcine

Methyiene Chloride

Tetrachloroethene

Toluene

trans-1 ,2 -IDichloroethene

tran 3-1 ,3 -Dichloropropene

Tricnloro'jtheneVinyl Chi Dride

< 0.90

< 0.20

< 0.42

< 0.75

< 0.57

< 0.75

< 0.36

< 1.4

< 0.46

< 0.84

< 0.95< 10

< 1.3

< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.41

< 0.81

< 0.97

< 0.37

0.46

< 0.83

< 0.19

< 0.99

< 0.54

< 0.79

0.50

< 0.45

< 0.67

< 0.89

< 0.19

< 0.48

< 0.18

0.90

0.20

0.42

0.75

0.57

0.75

0.36

1.4

0.46

0.84

0.95

10

1.3

0.41

0.56

0.94

0.91

0.49

0.41

0.810.97

0.37

0.24

0.83

0.19

0.99

0.54

0.79

0.43

0.45

0.67

0.89

0.19

0.480.18

LOQ EQL Dil. Units

3.0

0.67

1.4

2.5

1.9

2.5

1.2

4.7

1.5

2.8

3.2

33

4.3

1.4

1.9

3.1

3.0

1.6

1.4

2.7

3.2

1.2

0.80

2.8

0.63

3.3

1.8

2.6

1.4

1.5

2.2

3.0

0.63

1.6

0.60

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 UB/L

1 ug/L

1 ug/L

1 ug/L

AnalysisCode Date

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

Q 06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

Q 06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

Prep Date: 06/19/03

Prep Method AnalysisMethod

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW646 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260$

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SWB46 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

3W846 8260B

SW846 8260B

SW846 8260B

3W846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

En Chem Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-469-8827

Analytical

Client : RMT - MADISON

Project Name : LEMBERGER LANDFILL

Project Number : 3452.1 1

Field ID: STORAGE BLANK

Report Number: 835518

Matrix Type: WATER

Collection Date : 06/13/03

Report Date : 07/29/03

Lab Sample Number : 835513-004

VOLATILES - SPECIAL LIST

Analyte

1,1,1-Trichloroethane

1 , 1 ,2 ,2-Tetrachloroethane1 ,1 ,2-Tr ohloroethane

1,1-DicMoroethane

1,1-Dicrloroethene1,1 -Dirt loroprc pen e

1,2-DicMoroettiane

1,2 -Diet loroethene Total

1,2-DicHoroprcpane

2,3--D:chloropropene

2-Chlorc «thylvinylether

Acroloin

Acryloni'rile

Benzene

Bro-nodichloromethane

Bro.TioformBromome:thane

Canon Tetrachloride

Chlorobenzene

ChlorodiforomomethaneChloroetnane

Chlorcifo-in

Chloromethane

cis- 1 ,2-C i :hloroethene

cis-1 ,o-CichloroDropene

Dicnloroclifluoromethane

EEthylbenzene

Flucrotrichloromethcme

Methyene Chloride

Tetrachlciroetheie

Toluene

trans- 1 ,2-Dichloroethene

tran:s-'l ,3-Dichloropropene

Trichlc>r33thene

Vinyl Chloride

Result

< 0.90

< 0.20

< 0.42

< 0.75

< 0.57

< 0.75

< 0.36

< 1.4

< 0.46

< 0.84

< 0.95

< 10

< 1.3< 0.41

< 0.56

< 0.94

< 0.91

< 0.49

< 0.41

< 0.81

< 0.97

< 0.37

< 0.24

< 0.83

< 0.19

< 0.99< 0.54

< 0.79

0.50

< 0.45

< 0.67

< 0.89

< 0.19

< 0.48

< 0.18

LOD

0.90

0.20

0.42

0.75

0.57

0.75

0.36

1.4

0.46

0.84

0.95

10

1.3

0.41

0.56

0.94

0.91

0.49

0.41

0.81

0.97

0.37

0.24

0.83

0.19

0.990.54

0.79

0.43

0.45

0.67

0.89

0.19

0.48

0.18

LOQ

3.0

0.67

1.4

2.5

1.9

2.5

1.2

4.7

1.5

2.8

3.2

33

4.3

1.4

1.9

3.1

3.0

1.6

1.4

2.7

3.2

1.2

0.80

2.8

0.63

3.3

1.8

2.6

1.4

1.5

2.2

3.0

0.63

1.6

0.60

EQL Oil. Units

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

1 ug/L

Prep Date: 06/19/03

Analysis Prep Method AnalysisCode Date Method

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SWB46 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 82606

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 B260B

06/19/03 SW846 5030B SW846 8260B

Q 06/19/03 SW8465030B 3W846 8260B

06/19/03 SW846 5030B SW846 8260B

06/19/03 SW8465030B 3W846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B SW846 8260B

06/19/03 SW8465030B 8W846 B260B

En Chem Inc.1241 Bellevue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-<.69-8827

Analytical Report Number: 835518

Client: RMT- MADISON

Project Names: LEMBERGER LANDFILL

Project Number: 3452.11

Field 1C): ANNUAL EFFLUENT

Matrix Type: WATER

Collection Date : 06/13/03

Report Date : 07/29/03

Lab Sample Number : 835518-001

INORGANICS

Test

Aluminum

Aluminum - RecoverableAntimon/

Arsenic

Beryll uni

Cadmium

Caclmiun - Recoverable

Chromiuii

Chromiu.ii - Recoverable

Chromium, Hexavalent

Copper

Copper - (Recoverable

Hardness

iron

Lead

Lead - R'3;overable

Mercury

Nickel

Michel - Recoverable

Selemiurri

Silver

Silver - Recoverable

Thallium

Zinc

Zinc - Recoverable

BOD

Chloride

Cyanide, Amenable

Cyanide, TotalNitrogen, Ammonia

Phoisp-ioms

Total Suspended Solids

VOLATILES- SPECIAL

Analyte

1,1,'l-TncNoroethani;

1 , 1 ,2,2-To:rachloroe:hane

1,1,2-TncHoroethane

1,1-Dichloroethane

1.1-Dichloroethene

1,1-Dichlorapropene

Result

23

25

< 5.2

< 2.6

< 0.21

< 0.15

< 0.15

< 1.7

1.4

< 2.6

1.2

< 0.82

370

< 18

< 0.75

< 0.75

< 0.056

< 4.2

< 2.5

< 1.1

< 0.45

< 0.45

< 5.6

< 2.1

1.1

< 2.0

15

0.0027

0.0027

0.19

< 0.12

< 2.0

LIST

Result

< 0.90< 0.20

< 0.42

< 0.75< 0.57

< 0.75

LOD

19

7.7

5.2

2.6

0.21

0.15

0.15

1.7

0.52

2.6

0.53

0.82

0.081

18

0.75

0.75

0.056

4.2

2.5

1.1

0.45

0.45

5.6

2.1

0.80

0.27

0.0015

0.00150.11

0.12

LOD

0.900.20

0.42

0.75

0.57

0.75

LOQ EQL

63

26

17

8.7

0.70

0.50

0.50

5.7

1.7

8.7

1.82.7

0.27

60

2.5

2.5

0.1914

8.3

3.7

1.5

1.5

19

7.0

2.7

2.0

0.90

0.0050

0.00500.37

0.40

2.0

LOQ EQL

3.0

0.67

1.4

2.5

1.9

2.5

DM.

11

1

1

1

11

11

11

1

1

1

1

1

11

1

1

1

1

11

1

1

1

1

111

1

Dil.

11

1

1

1

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

mg/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Analysis Prep AnalysisCode Date Method Method

QA 06/20/03 SW8463010A SW846 6010B

QA 06/20/03 SW8463005A SW846 6010B

06/20/03 SW8463005A SW846 6010B

06/20/03 SW8463010A SW846 6010B

A 06/20/03 SW8463010A SW8466010B

06/24/03 SW8463020A SW846 7131

06/24/03 SW846 M3020 SW8467131

06/20/03 SW8463010A SW846 6010B

Q 06/20/03 SW8463005A SW846 6010B

06/13/03 SW8467196A SW846 7 196 A

QA 06/20/03 SW8463010A SW8466010B

06/20/03 SW8463005A SW846 6010B

06/20/03 SW8463010A 6010B/2340B

06/20/03 SW8463010A SW846 6010B

06/27/03 SW8463020A SW846 7421

A 06/27/03 SW846 M3020 SW846 7421

06/19/03 SW846 7470 SW846 7470A

06/20/03 SW8463010A SW846 6010B

06/20/03 SW8463005A SW846 6010B

06/25/03 SW846 7740 SW846 7740

06/24/03 SW8463020A SW846 7761

06/24/03 SW846 M3020 SW846 7761

06/20/03 SW8463010A SW6466010B

06/20/03 SW8463010A SWB46 6010B

Q 06/20/03 SW8463005A SW646 6010B

06/13/03 SM5210B SM 5210B

N 06/19/03 EPA 300.0 EPA 300.0

Q 06/27/03 EPA 335.4 EPA 335.4

Q 06/20/03 EPA 335.4 EPA 335.4

Q 06/23/03 EPA 350.1 EPA 350.1

A 06/23/03 EPA 365.4 EPA 365.4

06/18/03 EPA 160.2 EPA 160.2

Prep Date: 06 '19/03

Analysis Prep Method AnalysisCode Date Method

06/19/03 SW8465030B 5W846 8260E3

06/19/03 SW846 5030B 5W846 8260B

06/19/03 SW8465030B 3W846 8260B

06/19/03 SW846 5030B 5W846 8260B

06/19/03 SW8465030B 5W846 8260B

06/19/03 SW8465030B 5W846 8260B

En Chem Inc.1241 Bellewue StreetGreen Bay, Wl 54302920-469-2436800-7-ENCHEMFax: 920-469-8827

Analytical Report Number: 835518

Client: RMT - MADISON

Project Namo : LEMBERGER LANDFILL

Project Number: 3452.11

Field ID : ANNUAL EFFLUENT

Matrix Type: WATER

Collection Date : 06/13/03

Report Date : 07/29/03

Lab Sample Number : 835518-001

VOLATILES - SPECIAL LIST

Analyte

1,2-DicHoroethane1,2-Dictloroethene, Total1 ,2-Dichloropropane

2,3--Dichloropropen<5

2-ChlorcethylvinyletherAcrolejin

AcrylonilrileBenzene

BroTiodichloromethaneBrornofomn

BromomethaneCarbon "jtrachloride

Chlorobc-nzeneChlorodib'omometh.aneChloroehane

Chlorofo-in

Chloromethane

cis-1,2-Cichloroethenecis-1 ,;i-Dii:hloropropene

Dichlorodifluoromethane

EthylbenzeneFJuorotrichloromethcine

Methy ene: Cnloride

Tetrachk'roetheneToluene

trans-'! ,2 -Dichloi'oethenetran!5-1,3-Dichloropropene

TrichlorOfjthene

Vinyl Chloride

SEMIVOLATILES - SPECIAL

Analyle

AnthraceneE5enzo(a)3nthraceneEienzo(a)DyreneEien::o;b)fluoranthena

E!en;:o;gM)peryleneElen;:o [k ) 1 joranthene

ChryseneDibenzo(;i.h)anthraci5ne

Fluoranthene

Result

< 0.36

< 1.4

< 0.46

< 0.84

< 0.95

< 10

< 1.3

< 0.41

< 0.56

< 0.94

< 0.91< 0.49

< 0.41

< 0.81

< 0.97

< 0.37

< 0.24

< 0.83

< 0.19

< 0.99

< 0.54

< 0.79

0.49

< 0.45

0.72

< 0.89

< 0.19

< 0.48

< 0.18

LIST - SIM

Result

< 0.012

< 0.010

< 0.0085< 0.010< 0.0094

< 0.0091

< 0.0076< 0.0095

< 0.012

LOD

0.36

1.4

0.46

0.84

0.95

101.3

0.41

0.56

0.94

0.91

0.49

0.41

0.810.97

0.37

0.24

0.83

0.19

0.99

0.54

0.79

0.43

0.45

0.67

0.89

0.19

0.48

0.18

LOQ

1.2

4.7

1.5

2.8

3.2

33

4.3

1.4

1.9

3.1

3.0

1.61.4

2.7

3.2

1.2

0.80

2.8

0.63

3.3

1.8

2.6

1.4

1.52.2

3.0

0.63

1.6

0.60

EQL Dll.

11

1

1

1

11

1

1

1

1

11

1

11

1

1

1

1

1

1

1

11

1

11

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

AnalysisCode Date

06/19/0306/19/03

06/19/0306/19/03

06/19/0306/19/03

06/19/03

06/19/03

06/19/0306/19/03

06/19/0306/19/03

06/19/0306/19/03

06/19/03

06/19/0306/19/03

06/19/03

06/19/03

06/19/03

06/19/03

06/19/03

Q 06/19/03

06/19/03Q 06/19/03

06/19/03

06/19/0306/19/03

06/19/03

Prep Date: 06/19/03

Prep Method

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030BSWB46 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

SW846 5030BSW846 5030BSW846 5030B

SW846 5030B

SW846 5030B

SW846 5030B

AnalysisMethod

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260BSW846 82608SW846 8260B

SW846 8260B

SW846 8260BSW846 8260B

SW846 8260BSW846 8260BSW846 8260BSW846 8260BSW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260B

SW846 8260BSW846 8260B

SW646 8260B

SW846 8260B

SW846 8260BSW846 8260BSW846 B260B

SW846 8260B

SW846 8260B

SW846 8260B

Prep Date: 06/20/03

LOD

0.012

0.010

0.00850.0100.0094

0.0091

0.00760.0095

0.012

LOQ

0.041

0.034

0.0280.0350.031

0.030

0.0250.032

0.039

EQL Dil.

11

11

11

1

1

1

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

AnalysisCode Date

& 06/23/0306/23/03

&* 06/23/0306/23/0306/23/0306/23/03

06/23/03

06/23/03

06/23/03

Prep Method

SW8463510CSW8463510CSW8463510C

SW8463510CSW8463510CSW8463510C

SW8463510CSW8463510C

SW8463510C

AnalysisMethod

8270C-SIM8270C-SIM8270C-SIM6I270C-SIM

8270C-SIMEI270C-SIM

8270C-SIM8270C-SIM

8270C-SIM