Scheme of Instruction and Examination and 7th Sem. and 8th ... · 2 Process Modelling, Simulation...

Approved by BOS (Technology)( Circulation) June 2019,UCT,OU,HYD.7

Scheme of Instruction and Examination

and

Syllabi of (CBCS)

7th Sem. and 8th Sem.

of

B.Tech.

(Chemical Engineering)

(Effective from Academic Year- 2019-20)

University College of Techology (A)

Osmania University, Hyderabad,TS


SCHEME OF INSTRUCTION AND EXAMINATION (CBCS)

B.TECH (CHEM. ENGG) SEVENTH SEMESTER

(Effective from Academic Year 2019-2020)

R-Report P - Presentation/Viva-Voce, * - 50 % Project work is completed

ELECTIVE – III : 1 Fertilizer Technology, 2. Ind. Entrepreneurship & Management

3. Process Intensification, 4.Sugar Technology, 5.Mineral Processing Technology,

Elective-IV (Open )

1.Pollution Control in Process Industries (Chem. Eng.) 2.Patents & Intellectual Property

Rights (FT) 3.Operations Research for Engineers, (TT)

S.No.

Course

No.

Course Title

SCHEME OF

INSTRUCTION HOURS PER WEEK

SCHEME OF EXAMINATION Credit

s

L

T

P Durat

ion, Hour

s

CIE SEE

1

PC

701

MTO

Mass

Transfer

Operations -

II

3 1 - 3 25 75 4

2

PC

702

PMS

Process

Modeling &

Simulation

3 1 - 3 25 75 4

3

PC

703

TP

Transport

Phenomena

3 1 - 3 25 75 4

4

PE

704

EIII

Elective –

III

4 - 3 25 75 4

5

PE

705 E-

V

Elective-IV

(Open )

4 - 3 25 75 4

Practicals

6

PC

751

MTO

Mass

Transfer

Operations

Lab

- 3 4 25 50 2

7

PC

752

PMS

Process

Modeling &

Simulation

Lab

- 3 4 25 50 2

8 SEC

753

PRO

Project

Seminar*

- 50

Internal

25 - R

25-P

100

External

50-R

50-P

4

Total

20 6 250 475 26


SCHEME OF INSTRUCTION AND EXAMINATION (CBCS)

B.TECH (CHEM. ENGG) EIGTH SEMESTER (Effective from Academic Year 2019-2020)

S.No.

Course

No.

Course Title

SCHEME OF

INSTRUCTION HOURS PER WEEK

SCHEME OF

EXAMINATION

Credits

L T P Duration,

Hours CIE SEE

1. PC 801

PDE

Plant

Design &

Econ.

3 1 - 3 25 75 4

2. PC 802

PED

Process

Equipment

Design

3 1 - 3 25 75 4

3. PE 803

EL-V

Elective-

V (Open

Elective)

4 - 3 25 75 4

4. PE 804

EL-VI

Elective-

VI 4 - 3 25 75 4

Practicals

5

PC 851

PDD

Process

Equipment

Design

and

Drawing

Lab

- 3 4 25 50 2

6

SEC

852

PRW

Project

Work - 12 - 75

Internal

50-R

25-P

150

External

R-50

P-100

6

Total

16 15 200 500 24

R-Report P - Presentation/Viva-Voce,

Elective-V (Open)

1 Biochemical Engineering (Chem. Eng.) 2. Supply Chain Management (FT) 3.Six Sigma Lean Manufacture (TT)

Elective-VI

1. Principles of Management and Industry Psychology, 2. Fibre, Pulp and paper Industry, 3.

Corrosion & Corrosion Control, 4.Membrane Separation processes, 5.Electrochemical

Engineering, 6. Simulation and computer aided Design,


PC 701 MTO-II

MASS TRANSFER OPERATIONS – II

Instruction per week : 4 Hours CIE: 25 Marks

Duration of SEE : 3 Hours SEE : 75 Marks

Credits : 4

Course Objectives

Students will learn to

1. Interpret Vapor Liquid Equilibrium Data and know the applications

of simple, steam distillation operations

2. Design, calculate and evaluate the optimum operating conditions of

continuous distillation operations

3. Interpret Liquid-Liquid & Solid-Liquid Equilibrium Data, calculate

and evaluate the optimum operating conditions for batch &

continuous Extraction & Leaching operations

4. Adsorption principles to various adsorption operations, calculate

operating conditions for batch & fixed bed adsorption

5. Classify membrane separation operations and apply for various

industrial cases.

6. Design of the related mass transfer equipment

UNIT-I

Distillation: Batch Type

Introduction to Distillation, Vapor-liquid Equilibrium for Binary Mixtures: VLE Phase

diagrams, Tie lines and mixture Rule, VLE at constant Pressure and at constant temperature,

Minimum and maximum boiling Azeotropes; Methods of distillation for binary mixtures:

Flash Vaporization/ Equilibrium Distillation, Differential distillation and Steam Distillation;

Batch Distillation with Reflux: Brief discussion and calculations.

UNIT-II

Distillation: Continuous Type

Continuous Rectification/ Fractionation of Binary Mixtures, Calculations of number of ideal

stages in multistage countercurrent rectification; Concepts with Brief Discussion of McCabe

Thiele Method, Ponchon-Savarit Method and Lewis-Sorel Method; Optimum Reflux Ratio, ,

Use of total and Partial Condensers, Use of Open Steam, Principles of Azeotropic

Distillation; Extractive Distillation; Reactive Distillation.

UNIT-III

Liquid-Liquid Extraction:

Introduction to Liquid-Liquid Extraction, Choice of Solvent for Liquid-Liquid Extraction,

Triangular coordinate system; Ternary Equilibrium; Brief Discussion and Calculations for

Single Stage Operation, Multistage Cross Current Operation, Multistage Counter Current

Operation without reflux; Equipment for liquid-liquid extraction; Leaching: Type of

Leaching methods; Solid Preparation for Leaching; Leaching Equilibrium, Brief discussion


and Calculations for Single stage leaching, Multistage Cross Current Leaching, Multistage

Counter Current Leaching; Equipment for Leaching.

UNIT-IV

Adsorption and Ion Exchange:

Introduction to Adsorption; Principles of Adsorption and Their Applications, Types of

Adsorbents, Adsorption Isotherms, Brief Discussion and Calculations for Single Stage

Adsorption, Multistage Cross Current Adsorption, Multistage Counter Current Adsorption;

Packed Bed Adsorption; Adsorption Wave and Breakthrough curve; Equipment for

Adsorption Operation; Ion Exchange Equilibrium, Ion Exchange Equipment.

UNIT-V

Membrane Separation Techniques:

Need of membrane separation and its advantages; classification of membrane separation

process; various membrane configurations; Brief discussion and Calculations of Membrane

Configuration models, various membrane and their applications; Brief Discussion of Ultra

filtration; Nano filtration; Reverse osmosis; dialysis, electro dialysis, Pervaporation;

Membrane distillation, Liquid Membrane and their applications in chemical and its allied

industries.

EXAMINATION: Part – A for 25 marks (with 10 questions: two question from each unit -

Compulsory) and Part – B for 50 marks ( 5 questions to be answered out of 7 of equal

weightage selecting at least one from each Unit).

TEXT BOOK

1. Treybal R.E., Mass transfer operation, 3rd ed., McGraw Hill New York, 1980.

2. Geankoplis C.J., Transport processed and unit operations, Prentice Hall, New Delhi

1997.

REFFERENCE BOOKS

1. McCabe W.L. and Smith J.C., Unit operation in chemical engineering, 5th ed.,

McGraw Hill New York 1993.

2. Seader J D and Henley, E.J., Separation Process Principles, Wiley India, 2010

3. Dutta B.K., Principles of Mass Transfer and Separation Processes, Prentice Hall, New

Delhi, 2005

4. Coulson J.M., Richardson J.F., Backhurst J.R. and Harker J.H. , Coulson and

Richardson chemical engineering, vol 1, Butterworth Heinman, New Delhi, 2000.

5. Coulson J.M. Richardson J.F. Backhurst J.R.and Harker J.H. Coulson and Richardosn

chemical engineering, vol 2, Asian book pvt ltd, New Delhi, 2000.

6. R.K.Sinnot (Ed) Coulson and Richardson chemical engineering, vol 6, Butterworth

Heinman, New Delhi, 2000.

Course Outcomes

Students will be able to


1. Interpret Vapour Liquid Equilibrium Data and know the applications

of simple, steam distillation operations

2. Design, calculate and evaluate the optimum operating conditions of

continuous distillation operations

3. Interpret Liquid-Liquid & Solid-Liquid Equilibrium Data, calculate

and evaluate the optimum operating conditions for batch &

continuous Extraction & Leaching operations

4. Apply the Adsorption principles to various adsorption operations,

calculate operating conditions for batch & fixed bed adsorption

5. Classify membrane separation operations and apply for various

industrial cases.

6. Design of the related mass transfer equipment

*****


PC 702 PMS

PROCESS MODELLING AND SIMULATION



Credits : 4

Course Objectives

Students to learn

1. the classification, uses and need for development of process

models to initiate real problems

2. basic knowledge of mathematics, science and engineering to

formulate mathematical models

3. to identify, formulate and solve chemical engineering

problems.

4. Numerical techniques, skills and modern engineering tools

necessary for engineering practice.

5. Various simulation approaches

6. Process design problems, based on economic analysis

using mathematical models of chemical processes and simulation

tools

Note: The Programs are to be written in "C" / MATLAB

UNIT - I

Computers and Software: Computing environments, The software development processes,

Algorithm design, Program composition, Quality Control, Documentation, Storage and

Maintenance, Software strategy.

Process Models: Uses, Distributed & Lumped parameter models, Linear and Nonlinear

models, Steady state and Dynamic models, continuous and Discrete models, Empirical

models.

Formulation of Process Models: Momentum, mass and energy balances, constitutive rate

equations, transport rate equations, chemical kinetic rate expressions, thermodynamic

relations.

Review on "C" Language and MATLAB Fundamentals.

UNIT - II


Formulation Process Models leading to set of ordinary differential equations and solution

procedures by Eulers, Modified Eulers and Runge Kutta, multi step, finite difference,

shooting and collocation methods.

UNIT - III

Formulation of Process Models leading to set of linear simultaneous equations and solution

procedures by Method of determinants, Gauss Elimination, Gauss Jordan, Jacobi and Gauss

Seidel methods.

Formulation Process Models leading to differential algebraic equations (DAE’s) and solution

procedures by backward differentiation and Runge Kutta methods

UNIT - IV

Formulation of Process Models leading to transcendental and polynomial equations and

solution procedures by Bi-section, Reguli-falsi, Newton Raphson, Richmond, Muller`s and

Bairstow methods.

Function Approximations by linear and nonlinear least square analysis, Approximations by

orthogonal functions, chebyshev polynomials.

UNIT - V

Chemical Process simulators

Introduction to process Simulators: Flow sheet Presentation, Process Simulation Programs -

Model solving approaches-Sequential modular, Simultaneous modular and equation solving

approach.

Steps of Process simulation: Flow sheet, Component Property Models, Streams, Simulation

of Unit Operations, Flow sheets with Recycle - tearing algorithms, Flow sheet Optimization

Commercial Simulators: Steady state simulators, Dynamic simulators, Online Optimizers,

Specialized simulators for flare networks, pipe networks, HAZOP etc.

EXAMINATION : Part-A for 25 Marks (with 10 Questions: two questions from each unit -

Compulsory ) & Part -B for 50 Marks (5 Questions to be answered out of 7 of equal

weightage selecting atleast one from each Unit)

TEXT BOOK

Process Modelling Analysis and Simulation by B.Wayne Bequette, Prentice Hall

International Series, 1998.

Numerical methods for Engineers by Steven C.Chapra and Raymond P Canale, 2nd edition,

McGraw Hill International edition, 1988.

SK Gupta, Numerical methods for Engineers, ,New Age International Edition:3rd , 2015

Process flow sheeting Westerberg, Hutchison, Motard & Winter, Cambridge University

Press.

REFFERENCE BOOKS

1 Digital Computations for chemical engineers by Leon Lapidus, McGraw Hill Book

Company, 1962

2 Process Modelling, Simulation and Control for Chemical Engineers, by William L

Luyben, 2nd edition, McGraw Hill Publishing Company, 1990.

3 Chemical Engineering Design, Sinnott & Towler, Elsevier BH

4 Integrated Design and Simulation of Chemical Processes, Volume 13 (Computer

Aided Chemical Engineering) A C Dimian


5 Chemical Process design - Computer aided case studies by A C Dimian, C S Bildea,

Wiley VCH

6 B V Babu, Process Plant Simulation, Oxford University Press

Course Outcomes

Student will be able to

1. Understand of the classification, uses and need for development of

process models to initiate real problems

2. Apply basic knowledge of mathematics, science and engineering

to formulate mathematical models

3. Identify, formulate and solve chemical engineering

problems.

4. Use the Numerical techniques, skills and modern engineering

tools necessary for engineering practice.

5. Use various simulation approaches

6. Solve process design problems, based on economic

analysis usingmathematical models of chemicalprocesses and

simulation tools

*****


PC 703 TP

T R A N S P O R T P H E N O M E N A



Credits : 4

Course Objectives

Students to learn

1. Knowledge on processes involving simultaneous momentum, energy

& mass transfer and analyze analogies by modeling.

2. Energy distribution and develop equations for heat conduction

different heat sources and compare.

3. the mass transfer in solids & fluids; derive concentration profiles for

systems with & without reactions.

4. to Compare and contrast all equations of change, apply and

formulate systems with simultaneous transports.

5. to Classify empirical equations for systems with turbulence; design

equations for unsteady state transport of momentum, energy & mass.

6. to Identify the mechanism of transport, Develop model for processes

with multi-, multi dimension- transport with turbulent flow under

unsteady state conditions.

UNIT – I

Introduction – Mechanism of molecular transport of momentum, heat and Mass Transfer.

Flux equations – Newton’s, Fouriers’ and Fick’s laws. Similarities and differences, Non-

Newtonian fluids, transport properties – estimation, temperature and pressure dependence,

estimation of transport properties of binary gaseous mixtures.

Velocity distributions in laminar flow – shell momentum balances – Flow of falling film –

flow of fluids through circular tubes. Annulus and Immiscible fluids between parallel

plates. Creeping flow around sphere – Drag calculations.

UNIT - II

Temperature distributions in solids and in laminar flow – shell balances - Heat

conduction with electrical, Nuclear, viscous and chemical heat source. Heat conduction

through composite walls, and cooling fin. Forced convection and free convection.

UNIT - III

Concentration distributions in solids and in laminar flow - shell mass balances, diffusion

through a stagnant gas film, Diffusion with homogenous chemical reaction and

heterogeneous chemical reaction. Diffusion into a falling liquid film-chemical reaction inside

a porous catalyst.

UNIT – IV


Equations of change for isothermal systems – Equation of continuity, Equation of Motion,

Equations of change in curvilinear coordinates, use of equations of change to set up steady

flow problems.

Equations of change for non-isothermal systems – Equation of energy – use of equations of

change to set up steady state flow problems.

Equation of change for a binary mixture – Equation of continuity of a component in

curvilinear coordinates.

Dimensionless equations of change and principle of similitude.

UNIT - V

Unsteady state problems in momentum, energy and Mass Transfer operations.

Turbulence - Time smoothing of equations of change of momentum, energy and Mass

Transfer. Eddy properties - Intensity of turbulence Reynolds stresses. Semi empirical

expressions for turbulent – Momentum – energy and mass fluxes.




TEXT BOOK :

1. R.B.Bird; W.E.Stewart and E,N,Lightfoot, Transport phenomena, John Wiley &

Sons. Inc. 1960 and recent edition 2002

REFERECE BOOK:

1. R.S.Broadkay Introduction to Transport Phenomena, , McGraw Hill Publications,

1980.

Course Outcomes


*****

7. Understand the processes involving simultaneous momentum,

energy & mass transfer and analyze analogies by modeling.

8. Interpret energy distribution and develop equations for heat

conduction different heat sources and compare.

9. Understand the mass transfer in solids & fluids; derive concentration

profiles for systems with & without reactions.

10. Compare and contrast all equations of change, apply and formulate

systems with simultaneous transports.

11. Classify empirical equations for systems with turbulence; design

equations for unsteady state transport of momentum, energy & mass.

12. Identify the mechanism of transport, Develop model for processes

with multi-, multi dimension- transport with turbulent flow under

unsteady state conditions.


PE 704 E-III (1)

FERTILIZER TECHNOLOGY

PROGRAM ELECTIVE - III (1)



Credits : 4

Course Objectives

Students to learn

1. the fundamental principles of chemistry and chemical technology

and on contemporary applications

2. the different processes of manufacturing of ammonia and nitric

acid.

3. the production of urea & other nitrogen based fertilizers

4. the Classification of phosphoric fertilizers and the production of

ammonium phosphate, nitro phosphates & phosphoric acid

5. Classification of fertilizers based on physical state and the

production of potassium fertilizers, economics of production in

India & to use fertilizer application techniques for different soil.

6. to solve major engineering problems in fertilizer industry.

UNIT - I

Sources of Nitrogen and Hydrogen Steam reformation of Hydrocarbons. Coal classification

processes. Partial oxidation of fuel oils. Gas purification – High & Low temperature shift

conversion, CO2 removal processes Methanation.

UNIT - II

Manufacture of Ammonia. Ammonia synthesis by various processes. By-product Ammonia

recovery by direct and indirect methods. Manufacture of nitric acid.

UNIT - III

Production of Urea – Urea processes, manufacture of other nitrogenous fertilizers such as

ammonium sulphate, calcium ammonium nitrate, ammonium chloride etc.

UNIT - IV

Phosphoric fertilizers – single & triple super phosphate manufacture. Production of

ammonium phosphates & nitro phosphates, Manufacture of phosphoric acid.

UNIT - V


Potassium Fertilizers, Mixed & compound fertilizers, liquid fertilizers. Indian Fertilizer

industry – production Economics and future plans. Fertilizer application techniques for

different soil Controlled release fertilizers.




TEXT BOOKS RECOMMENDED :

1. V. Sauchelli, “Chemistry and Technology of Fertilizers”, Reinhold 1960.

2. Slack A.V “Ammonia” -.Marcel Dekker – 1973.

3. F.T.Nielsson “Manual of fertilizer processing”, Marcel Dekker, 1987

Course Outcomes


1. Apply the knowledge on fundamental principles of chemistry and

chemical technology and on contemporary applications

2. Demonstrate knowledge on different processes of manufacturing of

ammonia and nitric acid.

3. Apply knowledge on production of urea & other nitrogen based

fertilizers

4. Classify phosphoric fertilizers and apply knowledge for production

of ammonium phosphate, nitro phosphates & phosphoric acid

5. Classify fertilizers based on physical state and apply knowledge for

production of potassium fertilizers, analyze economics of

production in India & to use fertilizer application techniques for

different soil.

6. Undertake to solve major engineering problems in fertilizer

industry.

*****


PE 704 E-III (2)

INDUSTRIAL ENTREPRENEURSHIP AND MANAGEMENT

PROGRAM ELECTIVE - III ( 2 )



Credits : 4

Course Objectives

Students to learn

1. to Evaluate the effectiveness of different entrepreneurship strategies

2. to Understood principles &functions management , process of

decision making , modern trends in management process

3. to Prepare own business plan

4. to Understanding the role and importance of entrepreneurship for

economic development.

5. to Understand and acquaint with legislations realting to industrial

and labour welfare ACTs

6. to Analyse the business environment in order to identify business

UNIT - I

Entrepreneurship: Concept, need, its existence in India and abroad Traits of an Entrepreneur,

Development of entrepreneurial talents – Motivation, Achievement, Risk taking, Goal

setting, Creativity. Obligation, pitfalls and steps for successful Entrepreneurship.

UNIT - II

Enterpreneurship education and role of Institutions. Entrepreneurship development through

promotional organization. Concept and growth of such organizations specially with respect

to state procedure for starting small scale industry, incentives for their promotions.

UNIT - III

Product development and Research preparation of project report, Decision making, Forms

of Ownership: Organization structure, production planning and control, Marketing.

UNIT - IV

Working capital management, operation and control through budget, inventory control,

motion and time study job Evaluation.

UNIT – V

Industrial psychology, Industrial safety, Labour Disputes, Labour welfare and Morale,

Leadership – Development and training of Managers.





TEXT BOOK :

1. Vasant Desai Management of Small Scale Industry, Third Edition, 1986, published by

Himalaya Publishing House, Bombay.

2. O.P.Khanna Industrial Engineering & Management, , Reprint Ed. 1988.

3. S.A.Sherlekar Industrial Organisation and Management, First Edition, July, 1979.

REFERENCE BOOKS :

1. Kootz & O.Donnell Essential of Management , TMH Ed. 1975.

2 Grant & Grant.Hand Book of Industrial Engg. And Management .

3. Charles A. Myers Personnel Administration, , 8th Ed., 1977.

Course Outcomes


1. Evaluate the effectiveness of different entrepreneurship strategies

2. Understood principles &functions management , process of decision

making , modern trends in management process

3. Prepare own business plan

4. Understand the role and importance of entrepreneurship for

economic development.

5. Understand and acquaint with legislations realting to industrial and

labour welfare ACTs

6. Analyse the business environment in order to identify business

*****


PE 704 E-III (3)

PROCESS INTENSIFICATION

PROGRAM ELECTIVE III - ( 3 )



Credits : 4

Course Outcomes

Students to learn

1.

the approaches and methods involved in Process Intensification

(PI) in Chemical Process Industries

2. to interpret four PI approaches for various industrial cases

3.

PI Techniques to improve heat transfer & Mass Transfer in

Reactors and design HiGee equipment

4.

processing methods and the intensification strategy for separation

and mixing operations

5.

to Develop and design PI equipment in Petrochemical and Fine

chemical Process Industries

6. to Design and develop PI equipment in Nuclear Industry

UNIT –I

Introduction to Process Intensification(PI): sustainability-related issues in process industry,

definitions of Process Intensification, fundamental principles and techniques of PI, the original ICI PI

strategy, benefits of PI and obstacles to PI

Issues in designing of a sustainable, inherently safer processing plant

UNIt-II

PI Approaches: STRUCTURE - PI approach in spatial domain, ENERGY - PI approach in

thermodynamic domain, SYNERGY - PI approach in functional domain and TIME - PI approach in

temporal domain

Mechanisms involved in PI : Mechanisms of intensified heat transfer, mass transfer, electrically

enhanced processes, microfluidics

UNIT –III

Application of PI techniques to heat transfer : Compact & micro heat exchangers

Application of Pi techniques to reactors: Spinning disc reactors, oscillatory baffled reactors (OBR),

Rotating reactors, Micro reactors, membrane reactors, micro reactors, Reactive separation/ super

critical operation and other intensified reactor types.


UNIT-IV

Intensification of Separation Processes: Distillation, Centrifuges, membranes, drying, precipitation

and crystallization

Intensified Mixing : Inline mixers, mixing on spinning disk, induction heated mixer

UNIT –V

Application areas of PI :

Petrochemicals and Fine Chemicals : Refineries, Bulk Chemicals, Fine Chemicals, Fine Chemicals

and Pharmaceuticals, bio processing

Offshore Processing, Nuclear Industries, Food and drink water sector, Textiles, Aerospace,

biotechnology



weightage selecting at least one from each Unit). TEXT BOOK

1.David Reay, Colin Ramshaw, Adam Harvey, Process Intensification- Reengineering for

efficiency, sustainability and flexibility, Butterworth Heinemann, (Elsevier) Edition: 2nd ,

2013

REFERENCE BOOKS

1, Stankiewicz, A. and Moulijn, (Eds.), Reengineering the Chemical Process Plants, Process

Intensification, marcel dekker 2003

2 KameliaBoodhooo, Adam Harvey (Editors) Process Intensification Technologies for Green

Chemistry : Engineering Solution to Sustainable Chemical Processing, Wiley 2013

3. K. V. Raghavan and B M Reddy (Editor) Industrial Catalysis and Separations : Innovations

for Process Intensification, Apple Academic Press, CRC Press, 2015


Course Outcomes


*****

1. Apply knowledge on approaches and methods involved in

Process Intensification (PI) in Chemical Process Industries

2. Apply and interpret four PI approaches for various ndustrial

cases

3. Apply PI Techniques to improve heat transfer & Mass Transfer

in Reactors and design HiGee equipment

4. Analyze the processing methods and implement the intensification

strategy for separation and mixing operations

5. Develop and design PI equipment in Petrochemical and Fine

chemical Process Industries

6. Design and develop PI equipment in Nuclear Industry


PE 704 E-III (4)

SUGAR TECHNOLOGY

PROGRAM ELECTIVE - III (4)



Credits : 4

Course Objectives

i To learn fundamental principles of chemistry and chemical

technology and on contemporary applications;

ii To learn to design and conduct experiments, as well as critically analyze

and interpret experiment results;

iii To learn to identify, formulate and to solve problems in chemical

technology and related fields;

iv To learn to specify, modify and design a component, process or system to

meet the needs of trade;

UNIT - I

Importance of Sugar Industry. Different raw materials for sugar manufacturing,

Composition of raw materials. Manufacturing processes, Raw sugar, Crystalline white sugar,

Reducing sugars.

UNIT - II

Conveying of raw materials. Extraction of cane juice by milling operation. Maceration and

Imbibition principles of cane juice clarification methods. Defecation procedures.

Sulphitation and carbonation.

UNIT - III

Juice heaters - construction and juice circulation. Filters - plate and Frame filter presses.

Continuous Rotary vacuum filters. Washing of filter cake. Evaporation multiple effect

evaporators - construction and operation. Steam economy and capacity.


UNIT - IV

Vacuum pan boiling - coil and calandria vacuum pans. Crystallization Nucleation and crystal

growth, Equipment for crystallization. Centrifuges , Batch and continuous. Separation of

Molasses. Sugar drying, packing of sugar.

UNIT - V

Introductory treatment of chemical control - Boiling house control - Recovery formulae (Noel

Deer`s, SJM & Gundu Rao) Sugar by-products : oagasse - production of bio-gas, Fibre board,

Furfurol Filter mud - Extraction of cane wax, Manuxe, Molasses - Manufacture of Industrial

alcohol and rectified spirit. Sugar scales and normal weight. India`s position in world sugar

market.




.

TEXT BOOK

1. Spencer and Meade.Indian Sugar Hand Book,

2. H.T.P. Horiot and Baet The Manufacture of Sugar from Cane.

3. Geelige.Plantation White Sugar Manufacture

4. H.G.Goorlige.Cane Sugar and its Manufacture

5. G.H.Jenkions Introduction to cane sugar Technology. (Elsevier Publishing Company)

6. Petrace Sugar by-products , Elsevier publishing company.

REFERENCE BOOKS:

1.Indian Sugar Journal

2.Publications of the Indian Sugar Technologists Association.

3 F.Henig.Principles of Sugar Technology.

4.Hugot E. Jonkins G.H. Hand Book of Cane Sugar Engineering.

5. Noel Derr Cane Sugar.

6. W.Jones and L.Scord The Manufacture of Cane Sugar.

7. L.A.Tromp. Machinery and Equipment of the Cane Sugar Factory


Course Outcomes

i Be able to demonstrate knowledge and understanding on fundamental principles of chemistry and chemical technology and

on contemporary

applications; ii Be able to design and conduct experiments, as well as critically analyze

and interpret experiment results;

iii Be able to identify, formulate and solve problems in chemical technology

and related fields;

iv Be able to specify, modify and design a component, process or system to

meet the needs of trade;

*****


PE 704 E-III (5)

MINERAL PROCESSING TECHNOLOGY

ELECTIVE - III (5)



Credits : 4

Course Objectives

1. To learn Mineral Processing methods to solve practical problems.

2. To learn minerals identification , analysis and estimation

3. To learn the Mineral processing (testing), analysis and estimation

of content of mineral in the earth clusters

4. To learn the analysis of ores and purification methods

UNIT - I

Properties and Types of Minerals - Pretreatment of ores: removal of harmful materials -

sampling of ores: moisture sampling, assay sampling, sampling systems, sample division

methods, online analysis.

UNIT - II

Mineral Liberations, concentration, measures of assessing metallurgical performance viz.,

recovery, ration of concentration, grade, enrichment ratio - Laboratory sizing; particle size

and shape, sieve analysis, sub sieve techniques, centrifugal methods (warman cyclosizer),

microscopic sizing, online particle size analysis - industrial screening; objectives,

performance of screens, screen types - Magnetic and Electrical Separation ; magnetic

separation principles, design and types of magnetic separators, principles of electric

separation, separation equipment.

UNIT - III

Movement of solids in Fluids and classification : principles, types of classifiers Gravity

concentration ; principles, concentration in vertical surren (Jigging), Jigs, types of Jigs Viz,

Harz Jig, circular and radial jigs, coal jigs (Baumb and Batac jigs) - Gravity concentration in

streaming currents : pinched sluice, cones, spirals, shaking tables.

UNIT - IV


Slurry Transport of Materials ; pulp density, composition of slurry, online instrumentation for

mass flow measurement, pumping equipment and piping for slurry transport - Heavy medical

separation ; principles, liquids and suspension for heavy media separation, separation vessels

; gravitational vessels, Wemco separator, drum separator; centrifugal separators; DMS

cyclone, Vorsyl separator, LSRCODEMS. Dyna whirlpool separator; DMS circuits.

UNIT - V

Flotation - History and theory: contact angle, work of adhesion; Floatation Reagents:

collectors, frothers, regulators; and their action - Floatation practice ; ore and pulp

preparation, reagents and conditioning - Machines: pneumatic (Davera cell, flotation column,

Jameson cell, froth separators) and mechanical (Denver cell, Wemco cell) - electro flotation,

skin flotation and table flotation.




TEXT BOOKS

1. S.K.Jain "Ore Processing" Oxford and TBHY Publishing Co. (P) Ltd., India (1986)

2..B A Wills and T J Napier-Munn "Wills Mineral Processing Technology" Butterworth-

Heinemann, 7th Edition, 2011

Course Outcomes

1. The students able with an appreciation of knowledge in various Mineral Processing methods to solve practical problems.

2. Ability to apply knowledge in minerals identification , analysis and

estimation

3. Able to apply knowledge in Mineral processing (testing), analysis

and estimation of content of mineral in the earth clusters

4. Ability to apply knowledge in analysis of ores and purification methods

*****


PE 705 E- IV (1)

POLLUTION CONTROL IN PROCESS INDUSTRIES (Chem. Eng.)

OPEN ELECTIVE



Credits : 4

Course Objectives

Students to learn

1. Global environmental problems, industry emissions and

categorize pollutants

2. Pollution levels, monitoring of pollutants and estimation of

pollutants

3. the methods of control, Design equipment

4. to Measure BOD,COD,TOC levels, treatment of IWW

5. to Examine bacterial phenomena , determine efficiencies

6. to Chose the required level of treatment and various P-C-

methods

UNIT - I

Introduction to Industrial pollution and types of pollution from chemical industries. Effects

of pollution as environment and ecosystems - global warning - green house effect.

Environmental legislatures - standards and guide lines.

UNIT – II

Air pollution - Meteorological aspects of pollution dispersion - adiabatio lapse Rate -

Environmental lapse rate - Turbulence and stability of atmosphere Richardson Number -

Plume raise - plume behaviour and characteristics effective stack height. Major Air

pollutants and their sources and measurement of air pollutants. Indoor air pollution - smoke

and hydrocarbons.

UNIT - III

General methods of control of air pollutants removal of sulphur dioxide - oxides of nitrogen

and organic vapors from gaseous effluents. Removal of particulate matter - principle and

working of settling chambers cyclone separators solid traps, fabric and fibre filters - elector

static precipitators. Treatment of gaseous.

UNIT - IV

Introduction to water pollution - water pollutants classification - characteristics of liquid

effluents from fertilizer, pulp & paper and petroleum Industries Estimation of oxygen

demands - DO, BOD, COD, TOD - BOD curves oxygen sag curve - modeling of BOD

curves.

Biological treatment of waste waters - aerobic and anaerobic methods - suspended and

attached growth processes - bacteria - Reproduction in bacterial - Bacterial growth crushes


conventional activated sludge process - Trickling filters Aerated lagoons - stabilization ponds

- fluidized bed contractors.

UNIT - V

Physical Trt methods principle and working of screening - sedimentation - flotation -

filtration - flocculation. Tertrary Trt methods - carbon adsorption - Ion Exchange - Resserse

Osmon`s Boralin chlorinating - ultrafiltration. Sludge treatment and disposal removal of

chromium and phenol from liquid effluents.




TEXT BOOK

1. C.S. Rao Environmental Pollution Control Engineering, New Age International

Publishing

Ltd, 2006.

REFERENCE BOOKS

S.P.Mahajan Pollution control in process industries,. Mc.Graw Hill Publishing

M.Narayanna Rao & A.K.Datta Waste Water Treatment, Oxford and IBH. Publishing --

Co. Pvt.Ltd., New Delhi.

P.Pratap Mouli & N.Venkata subbayya Divya Jyothi Prakasham Air pollution control ,

Jodhpur.

R.S.Ramaiho Introduction to Waste Water Treatment , Academic Press, new york.

Stem Fundamentals of Air Pollution Control , Academic press

Course Outcomes


1. Analyze global environmental problems, industry emissions and

categorize pollutants

2. Evaluate Pollution levels, monitoring of pollutants and

estimation of pollutants

3. Justify the methods of control, Design equipment

4. Measure BOD,COD,TOC levels, treatment of IWW

5. Examine bacterial phenomena , determine efficiencies

6. Chose the required level of treatment and illustrate various P-C-

methods

*****


Patents and Intellectual Property Rights (FT)

(Open Elective)


Statistical Analysis and Design of Experiments (TT)

(Open Elective)


PC 751 MTO

MASS TRANSFER OPERATION LABORATORY



Credits : 2

Course Objectives :

1. To learn to obtain experimental data relevant to different types of

distillations.

2. To learn to determine experimental data relevant for liquid-liquid

extraction. 3. To learn to identify solvents for leaching.

4. To learn to evaluate single versus multi stage operations.

5. To learn to design experiments to obtain mass transfer coefficients like diffusion coefficient in liquids and gases.

6. To learn to troubleshoot problems in liquid - liquid extraction

perforated towers or spray towers.

7. To learn to calculate drying rates of wet solids and volatile chemical spills.

8. To learn to design gas – liquid absorption columns.

( Minimum of 8 experiments to be performed)

1. Determination of concentration profile for the given system

2. Estimation of differivity coefficient for the gaseous system (Acetone - Air)

3. Estimation of differivity coefficient for the liquid system (H2SO4 - water)

4. Determination of vapor - liquid equilibrium data for the given system.

5. Estimation of vaporization efficiency and prediction of steam distillation temperature.

6. Verification of the Rayleigh`s equation for the system of methanol and water.

7. Determination of the capacity coefficient of the packed column under total reflux

conditions and calculation of height equivalent to theoretical plate.

8. Development of the solubility curve for the given system

9. Prediction of Liquid - Liquid equilibrium data for the given system and determination

of the plait point.

10. Estimation of the solid - liquid equilibrium data for the given system.

11. Estimation of the mass - transfer coefficient and plotting the variation of standard.

Number with Reynold`s member.

12. Developing the drying curve by using tray drier and estimation and composition of

time required for drying the given solid.

Course Outcomes


1. Able to obtain experimentally the data relevant to different types

of distillation.

2. Able to determine experimentally the data relevant for liquid-liquid

extraction. 3. Able to identify solvents for leaching.

4. Able to evaluate single versus multi stage operations.

5. Able to design experiments to obtain mass transfer coefficients like

diffusion coefficient in liquids and gases.

6. Able to troubleshoot problems in liquid - liquid extraction

perforated towers or spray towers.

7. Able to calculate drying rates of wet solids and volatile

chemical spills.

8. Able to design gas – liquid absorbtion columns.

*****


PC 752 PMS

PROCESS MODELLING AND SIMULATION LABORATORY



Credits : 2

Course Objectives

Student to learn

1. to Analyze the Chemical Engineering problems with computed

knowledge

2. to Develop the computer programs for the real chemical

engineering problems

3. to Estimate and validate a model based on input and output data

4. to Numerically simulate chemical process systems

5. to Solve chemical engineering problems by applying the

numerical methods using C language and MATLAB

6. to Use range of commercial simulators such as Aspen Plus to

solve chemical engineering problems

Note: The Programs are to be written in 'C" and MATLAB

PART - A

Application of following Numerical Methods for Process Calculations:

i) Solution of differential equations : Euler`s, Modified Euler`s, Runge-Kutta

methods

ii) Solution of set of simultaneous equations by Gauss elimination, Gauss Jordan and

Gauss Seidel methods.

iii) Solution of transcendental equations by bisection, Reguli Falsi, Newton Raphson

and Richmond iterations.

iv) Linear and Nonlinear Least square analysis.

PART - B

Open loop and Closed loop simulations of the following Process systems:

( A minimum of 5 process systems to be simulated)

i) Series of isothermal, constant holdup CSTRs

ii) CSTR with variable holdups

iii) Two heated Tanks

iv) Gas Phase Pressurized CSTR

v) Non-Isothermal CSTR

vi) Single Component Vaporizer

vii) Batch Reactor

viii) Reactor with Mass Transfer

ix) Ideal Binary distillation with holdups


x) Batch distillation with holdups

xi) Vapour Liquid Equilibrium : Bubble Point and Dew Point Calculations

PART – C

Demonstration of Software Packages

Suggested Books:

1.Process Modelling, Simulation and Control for Chemical Engineers, by William L

Luyben, 2nd

edition, Mc Graw Hill Publishing Company, 1990.

2.Process Modelling Analysis and Simulation by B.wayne Bequette, Prentice Hall

International

Series, 1998.

3.Numerical methods for Engineers by Steven C.Chapra and Raymond P Canale, 2nd

edition,

McGraw Hill International edition, 1988.

Course Outcomes


1. Analyze the Chemical Engineering problems with computed

knowledge

2. Develop the computer programs for the real chemical engineering

problems

3. Estimate and validate a model based on input and output data

4. Numerically simulate chemical process systems

5. Solve chemical engineering problems by applying the numerical

methods using C language and MATLAB

6. Use range of commercial simulators such as Aspen Plus to solve

chemical engineering problems

*****


PROJECT SEMINAR

Instruction per week : 4 CIE: 25 Marks

Credits : 2

Course Objectives :

Each student has to work on any one of the following projects allotted by the department and

submit a comprehensive typed and bound report ( 2 copies) at the end of the second semester

Process Based Project : Manufacture of a product

The report shall consist of collection of literature, study of the various processes available,

selection of the process, calculation of material and energy balances, process design of

important equipment, cost estimation, plant location and lay out, safety aspects, summary and

conclusions, Bibliography

Equipment Based Project: Detailed design of the equipment for a given capacity

The report shall consist of collection of literature, selection of the process & process

equipment indicating all design considerations, detailed process design and mechanical

design of equipment, drawings of the equipment with design data, material of construction of

each part of the equipment, summary and conclusions, bibliography

Experiment Based Project : Experimental investigation of basic applied research problem

The report shall consist of objectives of proposed study, collection of literature, detailed

design of experimental set-up, materials and methods, design of experiments, experimental

observations, results & discussion, conclusion, bibliography.

Each student is expected to complete about one third quantum of work involved during this

semester.

- In case of process based project, up to calculation of mass and energy balances

- In case of equipment based project, up to process & mechanical design of equipment

- In case of experimental based project, up to materials and methods

The candidate has to give seminar presentation regarding his progress of project work.

Evaluation is done by internal evaluation committee as given below

- Marks for report : 15 max.

- Marks for Seminar talk : 10 max.

The balance of the work will be continued as per MEB course, final report to be submitted as

per MEB for external evaluation.

1. To learn to collect information on own regarding a chemical

product or process.

2. To learn to perform basic and detailed engineering for a given

process. 3. To learn to carry out economic feasibility of a given product

production. 4. To learn to present coherent data and analysis about a given

process.


Course Outcomes

*****

Course Outcomes

1. Ability to collect information on own regarding a chemical

product or process.

2. Ability to perform basic and detailed engineering for a given

process. 3. Ability to carry out economic feasibility of a given product production. 4. Ability to present coherent data and analysis about a given

process.


PC 801 PDE

PLANT DESIGN & ECONOMICS



Credits : 4

Course Objectives

Students to learn

1. to Rephrase steps involved in evaluation of new project viability,

design from basic stage of selection of MOC of process equipments to

development of processes with HAZOP study.

2. to Summarize principles of plant layouts and design P&ID for

processes

3. to Identify, analyze and interpret various concepts and functions of

finance of an industry.

4. to Interpret sources of capital, Evaluate total capital investment,

recommend balance sheet and propose economic production chart for

plant

5. to Evaluate and select between alternates using Present worth-, Annual

cost-, Capitalized cost-, ROI, Payback period Methods. Justify

replacement and optimum operation of plant.

6. to Get the knowledge of design of entire plant w.r.t SHE; design a

sustainable process for a manufacturing plant.

UNIT – I

Evolution of process, process design including material and energy balance flow sheets and

engineering flow diagrams selection procedure for process equipment such as selection of

size reduction equipment, material handling equipment, size separation equipment,

evaporators, heat exchanger, filtration units and dryers, Material of construction for

equipment, Safety Considerations.

UNIT – II

Principles of plant layout, plot plans, piping engineering, sizing, selection, materials for

piping (ferrous and non-ferrous and plastics); layout, stress design and installation

(excluding drainage/under ground piping).

UNIT – III

Process industries – Capital and interests, economics and process engineering, value of

money, equations for economic studies, equivalence. The bond, capital recovery,

depreciation, interest in depreciation capital.

UNIT - IV


Cost indices, equipment cost, the William’s six-tenths factor, service facilities, capital

requirements for complete plants, total and process investment, the balance sheet, sources of

capital, Variable cost, fixed cost, use of cost data, profits and earnings economic

production charts.

UNIT - V

Annual cost method, present worth method, equivalent alternatives, rate of return method,

pay out lime method, effect of source of capital, replacement of existing facilities.




TEXT BOOKS :

1. Chemical Engineering Plant Design by C.Vilbrandt and Dryden C.E. 4th Edition, Mc

Graw Hill Book Co., 1959.

2. Process Engineering Economics, by H.E. Schweyer, Mc Graw Hill Co.,

New York,Kogakusha Co., Ltd., Tokyo. 1955.

Course Outcomes


1. Rephrase steps involved in evaluation of new project viability, design

from basic stage of selection of MOC of process equipments to

development of processes with HAZOP study.

2. Summarize principles of plant layouts and design P&ID for processes

3. Identify, analyze and interpret various concepts and functions of

finance of an industry.

4. Interpret sources of capital, Evaluate total capital investment,

recommend balance sheet and propose economic production chart for

plant

5. Evaluate and select between alternates using Present worth-, Annual

cost-, Capitalized cost-, ROI, Payback period Methods. Justify

replacement and optimum operation of plant.

6. Get the knowledge of design of entire plant w.r.t SHE; design a

sustainable process for a manufacturing plant.

*****


PC 802 PED

PROCESS EQUIPMENT DESIGN



Credits : 4

Course Objectives :

Students to learn

1. to chemical process equipment design procedures, design codes

and standards.

2. to design storage vessels under internal & external pressure

3. to Analyze and design heat transfer equipment

4. to Analyze and design mass transfer equipment

5. to Intensify and integrate the processes

6. to Waste minimization, pollution & abatement and safety & health

considerations

UNIT-I

INTRODUCTION

Introduction to Chemical Engineering Design, Process design, Mechanical aspects of process

equipment design, General design procedure, Equipment classifications, Design codes and

standards (IS, ASTM and BS)

DESIGN OF PRESSURE VESSELS

Design of pressure vessels under internal pressure, Construction features, Pressure vessel

code, Design of shell, various types of heads, nozzles, flanges for pressure vessel, Design and

construction features of thick-walled pressure vessels, Various types of jackets and coils for

reactors, Auxiliary process vessels

UNIT-II

SUPPORTS FOR VESSELS

Design consideration for supports for process equipment, Design of brackets support, leg

support skirt, support, saddle support.

DESIGN OF STORAGE VESSEL

Storage of nonvolatile and volatile liquids and gases, Codes for storage vessel design,

Bottom, Roof and Shell designs.

DESIGN OF VESSELS UNDER EXTERNAL PRESSURE

Design criteria for external design pressure, vessels operated under vacuum, Use of stiffeners,

Design of covers, pipes and tubes

UNIT-III

DESIGN OF HEAT EXCHANGERS

Types of heat exchangers, Selection criteria, Shell and Tube Exchanger’s Construction

details, TEMA standards and general design considerations, Kern’s Method of Process design

of Heat Exchangers, Mechanical design of shell, tube, baffles, closures, channels, tube sheets


etc. Design of Shell and Tube Condensers (excluding multi- component condensers) and

Design of 1-2 shell and Tube Exchangers in Series

UNIT-IV

DESIGN OF DISTILLATION AND ABSORPTION COLUMNS

Continuous stage wise distillation Column (for Binary Mixtures), design variables, McCabe-

Thiele Method for Low Product concentration, Smoker equations, prediction of plate

efficiency, column sizing, distillation with multi feed and side streams, Choice of Plate verses

Packed towers, Basic features of tall vertical equipment/ towers, Towers/Column Internal,

Design of tower shell and internals, supports etc.

UNIT-V

PROCESS INTENSIFICATION EQUIPMENT

Introduction, Definition and Concept, Fundamentals, Mixing (Macro, Meso and

Micromixing), Intensification in Heat and Mass Transfer, Intensification Techniques:

Enhanced force fields like Centrifugal fields, alternative force fields, HiGee equipment,

Rotating Packed Bed, Enhanced Surface Configurations like micro/ milli channel reactors,

monolithic structures, static mixers; Integrating Process Steps, Merits of PI Technologies,

Challenges to Implementation PI.

EXAMINATION: Part – A for 25 marks (with 10 questions : two question from each unit -



Text Books

For UNITs I and II

1. Joshi M.V., Mahajani V.V., “Process Equipment Design”, 3rd Ed., MacMillan, Delhi,

1996.

2. Code for unfired Pressure Vessels - IS Code: 2825 (1969).

For UNIT III

3. Kern D.Q., “Process Heat Transfer”, McGraw-Hill, New York, 1965.

For UNIT-IV

4. Coulson J.M, Richardson J.F. and Simmott R.K. Chemical Engineering, Vol. 6, 4th

Ed., Elesevier, New Delhi, 2006.

For UNIT-V

5. Boodhoo Kamelia and Adam P Harvey, Process Intensification for Green Chemistry:

Engineering Solutions for Sustainable Chemical Processing, 1st Edition, pp.1-27,

John Wiley & Sons, Ltd., Chichester, 2013

Reference Books

6. Bhattacharyya B.C., “Introduction to Chemical Equipment Design: Mechanical

Aspects”, 5th Ed., CBS Publishers, New Delhi, 2008.

7. Suresh C Maidargi, Chemical Process Equipment Design and Drawing, Vol-1, PHI,

2012

8. Coupes, James R, Fair James R and Pearny W Roy, Chemical Process Equipment:

Selection & Design. 3rd Edition, Butterworth- Heinemann, UK, 2012

9. Shrikant D Dawande, Process Equipment Design, Vol-1, 7th Edition, 2013

Branan C.R., “Rules of Thumb for Chemical Engineers”, 4th Ed., Elsevier, Oxford,

2005.


Course Outcomes


1. Apply the knowledge of chemical process equipment, design

procedures, design codes and standards.

2. Effectively design storage vessels under internal & external

pressure

3. Analyze and design heat transfer equipment

4. Analyze and design mass transfer equipment

5. Intensify and integrate the processes

6. Waste minimization, pollution & abatement and safety & health

considerations

*****


PE 803 ELE-V (OPEN)

BIO-CHEMICAL ENGINEERING (Chem. Eng.)

OPEN ELECTIVE



Credits : 4

Course Objectives

Students to learn

1. to molecular biology and metabolism

2. to important role of microbiology

3. to Engineer the enzyme technology

4. concepts of bioreactors and down stream techniques

5. concepts of bioprocess technology

6. the biochemical engineering applications

UNIT - I: Introduction to Biochemical Engineering & Molecular Biology

Biochemical Engineering Principles, Biophysics and cell doctrine: Atomic Theory and Cell

Theory, Important cell types, structure and functions of a typical cell and their components,

Transport across cell membranes: Passive and facilitated diffusion, Active transport;

Structure and functions of Bio Molecules: Carbohydrates, lipids, Nucleotides to Nucleic

Acids - R N A and DNA, Amino acids to Proteins - the building blocks of biochemical life.;

Biosynthesis and Metabolic Pathways: Biosynthesis of Small and Macro Molecules

Introduction of metabolic pathways and end products of glucose metabolism.

UNIT - II: Introductory Microbiology

Introduction to Microbiology: Classification and Industrial uses of Microorganisms; Growth

and Reproduction of Microbes: Growth cycle phases for batch cultivation. Monod’s growth

kinetics – Growth Rate dependant classification of Microorganisms; Microbial Genetics:

Recombinant DNA technology and mutant populations; Multiple Interacting Microbial

populations: Neutralism, Mutualism, Commensalism, Amenalism, Predatism and Parasitism

UNIT - III: Enzyme Technology

Enzymology: Enzymes as Biocatalysts - The enzyme substrate complex and enzyme action

and Classification of Enzymes based on Functions; Kinetics of Enzyme Catalyzed Reactions:

Simple enzyme kinetics with one and two substrates; determination of rate constants,

substrate activation and inhibition, modulation and regulation of enzyme activity / effect of

pH and temp on enzyme activity. Immobilized Enzyme Technology: Types of Enzyme

immobilization, Immobilized enzymes in industrial processes, Cofactors, Apo-enzymes and

Coenzymes utilization and regeneration

UNIT - IV: Bioreactors and Down Stream Techniques - Introduction


Design and Analysis of Biological Reactors: Batch and CSTR reactors, Enzyme reactors;

Ideal Reactors for kinetic measurements: The ideal batch reactor / The ideal continuous flow

stirred thank reactor - Alternate bio-reactor configurations; Separation Processes: Filtration,

Centrifugation, Adsorption, Reverse osmosis, Dialysis, Electrophoresis, Sedimentation and

Extraction; Purification Processes: Precipitation, Crystallization, and Chromatography

UNIT - V: Bioprocess Technology

Fermentation Technology: Types of Fermentation - Anaerobic and Aerobic Fermentation

process. Surface and Submerged Fermentation process, Medium formulation and Culture

Propagation: Media composition and Sterilization, Inoculum’s culture development under

aseptic conditions of transfer. Environmental biotechnology: Effluent treatment. Industrial

Biotechnology: Commercial enzymes, Antibiotics and single cell protein




TEXT BOOK :

1. Biochemical Engineering Fundamentals, by James, E.Bailey and David F Ollis, II

Edition, 1986. McGraw-Hill Internal Edition.

Course Outcomes :


1. Provides information about molecular biology and metabolism

2. Explain how microbiology playing important role

3. Engineer the enzyme technology

4. Apply concepts of bioreactors and down stream techniques

5. Apply concepts of bioprocess technology

6. Engineer the biochemical engineering applications

*****


Supply Chain Management (FT)

(Open Elective)


Six Sigma and Lean Management Technology (TT)

(Open Elective)


PE 804 ELE-VI (1)

PRINCIPLES OF MANAGEMENT AND INDUSTRIAL PSYCHOLOGY

PROGRAM ELECTIVE - VI(1)



Credits : 4

Course Objectives

Students to learn

1. Contemporary issues in General and Industrial Management 2. the concepts and principles of Management and Industrial

psychology 3. to develop and integrate for recognition of the need and to engage

in perpetual learning in management and industrial psychology 4. to Analyze and Select various concepts of Industrial relations,

Marketing, HR and Productions systems to enable the student to

meet the needs of industry 5. to Asses and compare the concepts of Management and industrial

psychology 6. the basic concepts and principles of Management and Industrial

psychology

(Basic concepts of management (A brief study of some the topics) and application in areas

like Purchase, , HRD, Production, Marketing, Industrial Psychology and Relations with

reference to Chemical, Food and Textile Industries)

UNIT - I

Management definition, Administration Vs Management, Principles and Functions of

Management, Levels of management - System and Contingency approach to management –

Planning: defination, process - Forecasting methods - Decision making proces- Organization:

Definition, Line, staff, functional and matrix type organization, span of control (Graicuna's

Formulae), Centralization Vs Decentralization,Coordination Vs Cooperation.

UNIT - II

Supervision : Roles and function of supervisor, Tasks and Process of supervision -

Communication: process, grapevine, networks and barriers of communication – Leadership :

definition, styles of leadership, Managerial grid, Theory of X, Y and Z, – Control: meaning,

definition and control process - Introduction to Personnel Management: Need, Scope,

Functions, staffing process, Methods of remuneration , performance Appraisal and Training

UNIT – III

Industrial Relations: Human relation Vs Industrial relations, Trade Unionism, Industrial

Unrest, Wage and Incentive concepts -

Introduction to Purchase & Material management Purchasing objects and principles, types of

purchasing, Vendor selection, rating, evaluation & Development - Inventory control, ABC

analysis, stores organization - concept of Warehousing.

UNIT - IV

Production & Marketing Management: Types of Production, Quality control (Tools used),

PPC, Maintenance management - Marketing management; Definition and concept of

marketing, functions of marketing, market research, Types of markets, Sales Forecasting,


Pricing , Advertising Strategy, Distribution Channels ,Packaging and Product Promotion.

UNIT - V ,

Industrial Psychology: definition, meaning and scope – Engineering Psychology : Tailors

Scientific Management as a base of Engg. Psychology,work culture and Ergonomics,

Industrial Fatigue

Motivation : Meaning, Types of Motives, Maslow’s and Herzberg theory of Motivation.

Morale : Meaning, Measurement , relation with motivation, Tips for Morale improvement

Attitudes and Job Satisfaction : Meaning of Attitudes and methods to find employee attitude.

Meaning of Job satisfaction, its relation to productivity, Interpersonal factors relating to job

satisfaction and Job dis-satisfaction.

EXAMINATION: Part – A for 25 marks (with 10 questions : two question from each unit -



Text Books:

1. Principles and Practice of Management - T.N.Chhabra, Dhanpat Rai & Sons, New

Delhi, 2008

2. Principles and Practice Management - LM.Prasad, Sultan chand Publications, New

Delhi 2008

3. Industrial Psychology – P.K.Ghosh and M.B.Ghorpade, Himayala Publishing House,

Delhi 2006

Reference Books

1. Personal Management – C.B.Memoria- Himayala Publishing House, Delhi, 2006

2. Industrial Engg. And Management – O.P. Khanna, Dhanpatrai & Sons, New Delhi

2007

Course Outcome


1. Discuss and explain to gain insight on contemporary issues in

General and Industrial Management 2. Apply and illustrate the concepts and principles of Management

and Industrial psychology 3. Develop and integrate for recognition of the need and to engage in

perpetual learning in management and industrial psychology 4. Analyze and Select various concepts of Industrial relations,

Marketing, HR and Productions systems to enable the student to

meet the needs of industry 5. Asses and compare the concepts of Management and industrial

psychology 6. Remember and recall the use of these basic concepts and

principles of Management and Industrial psychology

*****


PE 804 E-VI(2)

FIBRE, PULP AND PAPER TECHNOLOGY

PROGRAM ELECTIVE - VI (2)



Credits : 4

Course Objectives

1. To learn the fundamental principles of chemistry and

chemical

technology and contemporary applications;

2. To learn design and conduct experiments, as well as critically

analyze and interpret experiment results;

3. To learn to identify, formulate and solve problems in chemical


4. To learn to specify, modify and design a component, process or

system to meet the needs of trade;

UNIT - I

Brief history of Indian Paper Industry - Importance of paper industry. Different types and

uses of paper. Different raw materials for paper manufacture. Classification of hard and soft

woods their behavior in manufacture.

UNIT - II

Outline of the manufacturing process of pulp : Conveying and preparation of the raw

materials ; pulping and different pulping processes, washing and bleaching refining and

beating of the pulp. Analysis and testing of pulp.

UNIT - III

Outline of the manufacturing process of paper, Testing of the different properties of paper.

Paper as a medium for chromatography, characteristics needed for chromatographic paper

UNIT - IV

Effluents from pulp and paper industry: Recovery of chemicals in the digestion and pulping

process and their treatment before discharge for preventing pollution of the surroundings.

TEXT BOOK :


1. Kenneth W.Brill.Hand Book of pulp and paper Technology,

2. A.J.Stemon Wood and Cellulose Science, , The Ronald Press Co., New York.

3. SIRI, 4/43 Paper, pulp and specialty papers, Roopnagar, Delhi–007.

4. K.A Chowdhury and S.S.Gosh Indian woods , Vol . I, II& III, Survey of India

Publications.

5. V.Poddar, Paper Industry in India Weighcost Oxford and HBH Co., New Delhi.

6. Paper Industry in India –Instt. Of Economic and Market Research, 16, Dekshneswr,

10, Hailay Road, New Delhi – 110 001.

7. Jire Gesparie.Paper and Thin Layer Chromatography,

Course Outcomes

i Be able to demonstrate knowledge and understanding

on fundamental principles of chemistry and chemical

technology and on contemporary applications;

ii Be able to design and conduct experiments, as well as critically

analyze and interpret experiment results;

iii Be able to identify, formulate and solve problems in chemical


iv Be able to specify, modify and design a component, process or

system to meet the needs of trade;

*****


PE 804 ELE-VI (3)

CORROSION AND CORROSION CONTROL

PROGRAM ELECTIVE - III ( 3 )



Credits : 4

Course Objectives

1. To learn various corrosion types, methods of corrosion and to solve

practical corrosion problems.

2. To learn prevention methods of corrosion, analysis and estimation

3. To learn the corrosion testing, analysis and methods of prevention

4. To learn the analysis of metals and alloys in preventing corrosion

UNIT - I

Introduction . Cost of corrosion; corrosion engineering; Definition corrosion;

environments; corrosion damage; appearance maintenance and operating costs; plant shut

downs, contamination of product, loss of valuable products, effects on safety and reliability;

Classification of corrosion.

CORROSION PRINCIPLES :

Introduction; Corrosion rate expressions; Electro-Chemical Reactions; polarization

passivity; Environmental effects : effect of oxygen and oxidizers – effect of velocity; effect

of temperature; effect of corrosive concentration; effect of galvanic coupling. Metallurgical

aspects; Metallic properties; Ring work corrosion.

UNIT - II

THE EIGHT FORMS OF CORROSION :

Uniform attack :- Galvanic Corrosion : EMF and galvanic series; Environmental effects;

Distance Effect: Area effect prevention; Catholic protection. Crevice Corrosion : Environmental

factors : Combating crevice Corrosion, fill form corrosion; Environmental factors; prevention.

Pitting : Solution composition; Velocity; Metallurgical variables; Evaluation of pitting damage;

prevention.Intergrannular Corrosion : Austenitic stainless steels; Control for Austenitic stainless

steels; Knife line attack. Selective Leaching : Dezincification; Mechanism, prevention,

graphitization.Erosion Corrosion : Surface films; Velocity; Turbulence; Impingement;

Galvanic effect nature of metal or alloys; Combating Erosion Corrosion; Civilization damage;

Fretting corrosion.Stress Corrosion :Clack morphology; stress effects; Time of cracking;

environmental factors; Metallurgical factors; Methods of prevention; Corrosion fatigue.

Hydrogen damage: Characteristics; Environmental factors, Hydrogen blistering;

prevention.

UNIT - III

CORROSION TESTING


Introduction; Classification- Purposes; Materials and specimens surface preparation;

Measuring and weighing; Exposure Techniques; Duration; Planned interval tests; Aeration;

Cleaning specimens after exposure; Temperature Standard expression for corrosion rate;

Huey test for stainless steels; Stretcher test for a stainless steels; warren test for low carbon

steel.

UNIT - IV

Materials: Mechanical properties; other properties; Metals and alloys; cast irons; Stainless

steels.Non-metallic : Natural and synthetic rubbers – plastics.Thermoplastics

:Thermometers : Other non-metallic : Carbon and graphite, wood. CORROSION

PREVENTION : Materials selection; Metals and alloys; Metal purification non-metallic;

Alteration of environment;Changing mediums; Inhibitors.Catholic and Anodic Protection :

Catholic protection; Anodic protection; Comparison of anodic and catholic protection.

Coatings : Metallic and other Inorganic cosigns; Electro deposition; Flame spraying;

cladding; Hot dipping; Vapor deposition; Diffusion; Chemical conversion.

UNIT - V

MODERN THEORY – PRINCIPLES

Introduction; Thermodynamics : Free energy; Cell potentials and EMF Series;

Applications of thermodynamics to corrosion; Electrode Kinetics; Exchange current density;

Activation; Polarisation; Concentration polarization; Combined polarization mixed

potential theory; Mixed electrodes; passivity.

MODERN THEORY – APPLICATIONS

Introduction; Predicting corrosion behavior; Corrosion prevention; Corrosion rate

measurements.




TEXT BOOK :

M.G.Fontana and N.D.Greene, Corrosion Engineering, McGraw Hill Book Company

(1978) A, 2nd Edition.

Course Outcomes

1. The students should be able to use knowledge in various corrosion

types, methods of corrosion and to solve practical corrosion

problems.

2. Able to apply prevention methods of corrosion, analysis and

estimation

3. Able to apply corrosion testing, analysis and methods of prevention

4. Able to provide knowledge in analysis of metals and alloys in

preventing corrosion

*****


PE 804 E-VI (4)

MEMBRANE SEPARATION PROCESSES

PROGRAM ELECTIVE - VI(4)



Credits : 4

UNIT - I

Introduction to Membrane Separation processes :

Classification of separation processes – Separating agents – principles of gas permeation,

reverse osmosis, ultra-filtration, perparation dialysis, Electro-dialysis.

UNIT - II

Applications of membrane separation processes :

Applications of membranes for the separation of hydrogen or acid gases from O2 – N2

separation from air – stability of membrane processes for waste water treatment, applications

in pulp and paper, electroplating and Electro-coating industries – Applications in food

industry – denaturing of liquid foods, cheese making and whey processing.

UNIT - III

Ideal separation on capabilities of membrane processes : Separation factor, rejection factor,

expressions for ideal separation factors in various membrane processes.

Secondary Phenomena in Membrane processes : Secondary physical and transport

phenomena in membrane processes, concentration polarization in membrane processes.

UNIT - IV

Equipment for membrane processes: Flat sheet, tubular, spiral wound and hollow fibber

membrane modular designs for various membrane processes, single entry and double entry

separating elements, separation stage. Flow configuration in membrane systems.

Course Objectives

1. To learn membrane technology and characteristics of the species to be

separated.

2. To learn to select the right material and membrane structure according

to the properties of the involved compounds.

3. To learn to Evaluate the flux of water and solute through a

membrane, under fixed operating conditions, from transport

equations or supplier information

4. To learn to Identify the membrane technology applications for energy

efficient and environmental friendly operations.


UNIT - V

Design of membrane systems: Design equations for perfect mixing and cross flow

configuration, separation stages for gas permeation, reverse osmosis and ultra filtration.

Design equations for perfect mixing and parallel flow dialyze. Simple design equations for

Electro-dialytic stacks.




TEXT BOOKS :

“Membranes in Separation” - S.T. Hwang and K.Mammermeyer, Wiley – Inter

Science, New York, (1975).

“Membrane Technology” notices of Winter School conducted at College of

Technology, O.U. – December – 1987.

*

*

*

*

*

Course Outcomes

1. Able to apply the membrane technology according to the characteristics

of the species to be separated.

2. Able to select the right material and membrane structure according to

the properties of the involved compounds.

3. Able to Evaluate the flux of water and solute through a membrane,

under fixed operating conditions, from transport equations or

supplier information

4. Able to Identify and understand the membrane technology

applications for energy efficient and environmental friendly

operations.


PE 804 E-VI (5)

ELECTROCHEMICAL ENGINEERING

PROGRAM ELECTIVE - VI (5 )



Credits : 4

Course Outcomes

1. Students to learn balanced electrochemical reactions; analyze the

open-circuit potentials of electrochemical cells, including liquid-

junction

potentials

structure of the electric double

layer, based partly on surface-

tension data.

2. Students to learn reaction mechanisms and kinetics to obtain

electrode over potentials and mass-transfer phenomena,

including the estimation of

limiting currents. 3. Students to learn the principles and work in conditions of the

different types of primary and secondary batteries.

4. Students to learn the use of electrodes used in various

electrochemical; industries like metal finishing, electroplating

and electro polishing, etc.

UNIT – I

Introduction of Electrochemical Engineering: The scope of Electro Chemistry, the five “E”

Electrochemistry, Engineering, Energy, Environment and Economics, Examples from the

Electro Chemical Industry.

The Electrolytic solution – Conduction in aqueous solution – Debye – Huckel Theory. The

concept of Electrical potential, conduction in non-aqueous solutions and fused salts. Primary

current distribution in various geometrical cells.

UNIT - II

Thermodynamics of Galvanic Cells : The electromotive force, standard potentials and the

Nernst Equations, Application of Electrochemical cells: Measurements of Gibbs free

Energy. Entropy Enthalpy Activated Coefficients, Standard potentials and Sign Convention,

Reference Electrodes.

UNIT - III

Electro-chemicals Kinetics: The Electrical Double Layer. The Theory of Rate Processes

Applied to Electrochemistry. The Tafel Equation. Charge Transfer Over-potential.


UNIT - IV

Mass Transfer in Electro Chemical system: Diffusion controlled Electro-Chemical reaction.

The importance of convention and the concept of limiting current. Mass Transfer

Overpotential or concentration polarization. Secondary current Distribution. The Rotating

Disk Electrode.

UNIT - V

Synthesis of the principles and applications. Evaluation of cell potential and Oven potential.

The combined effect of standard potential. Chemical Resistance, Charge Transfer and Mass

Transfer over-potential. Industrial Examples: Batteries, Chlor-Alkali in plating, Electro-

winning, Corrosion. Modeling and Optimization of Electrochemical systems. Electro-

chemical machining - Design problem. The Chlor-Alkali Industry – Economic

Environmental Evaluation, New process Design.




TEXT BOOKS :

1.“Industrial Electrochemical Process”, T.A.Elsevier publishing Company (1971).

2.“Symposium on Electrochemical Engineering”, by J.D.Thrston, The Institution of

Chemical Engineering, London, 1973.

3.“Advances in Electrochemistry and Electrochemical Engineering:, by Charles W. Tohias

and Paul Delahay, Inter Science Publishers (1966).

Course Outcomes

1. i Students will be able to apply balanced electrochemical reactions;

analyze the open-circuit potentials of electrochemical cells,

including liquid-junction

potentials and understand the

structure of the electric double

layer, based partly on surface-

tension data.

2. i

i

Students will be able to understand the reaction mechanisms

and kinetics to obtain electrode over potentials and mass-transfer

phenomena,

including the estimation of

limiting currents.

3. i

i

i

Students will be able to explain the principles and work in conditions of the different types of primary and secondary batteries.

4. i

v

Students will be able to understand the uses of electrodes in used in

various electrochemical; industries like metal finishing, electroplating

and electro polishing, etc.

*****


PE 804 E-VI (6)

SIMULATION AND COMPUTER AIDED DESIGN

PROGRAM ELECTIVE III - ( 6 )



Credits : 4

UNIT - I

Modular approaches to process simulation- Analysis vs. design mode, The equations solving

approach, Decomposition of networks- tearing algorithms, based on the signal flow graph,

list processing algorithms

UNIT- II

Convergence promotion- Newton’s method, direct substitution, Wegstins method. Physical

and thermodynamic properties- sources, data banks and Routing. Professional simulation

packages- HYSIS, CHEMSHARE, ASPENPLUS and their Architecture.

UNIT - III

Fundamentals of CAD : Introduction, Definitions. The Design process - the

application of computers for Design. The Design work station - Graphics terminal, Input

and output devices.

UNIT - IV

Graphics packages & their functions. The data base structure & content, wire frame

modeling, Solids modeling.

UNIT - V

Computer Control. Introduction, Model of process. Process control strategies. Distributed

and Centralized control. Direct Digital control and Supervisory control.




TEXT BOOKS :

1.‘Process Plant Simulation’ by B. V. Babu, Oxford University Press, 2004

2. Chemical plant Simulation : Crowe, Hamielec, Hoffmon, Johnson, Shannou & Woods,

McMaster University Publication. 1965

3. CAD/CAM :Mickell P.Groover & E.N.Zummers Jr. Prentice Hall India Pvt. Ltd., N.D.

1989.

Course Objectives

1. To learn to prepare process flow sheets for design showing reactors, distillation columns and other process equipment.

2. To learn mathematics, science and engineering.

3. To learn to design a system, component, or process to meet desired

needs.

4. To learn the techniques, skills and modern engineering computer



Course Outcomes

i An ability to prepare process flow sheets for design showing reactors,

distillation columns and other process equipment.

ii An ability to apply knowledge of mathematics, science and engineering.

iii An ability to design a system, component, or process to meet desired

needs.

iv An ability to use the techniques, skills and modern engineering computer



PC 851 PEDD

PROCESS EQUIPMENT DESIGN AND DRAWING LAB



Credits : 2

Course Objectives

1. To learn to synthesize and analyze process flow sheets, draw flow

charts, layout and specification of equipment

2. To learn to effectively lead chemical engineering projects in industry

3. To learn to perform process selection

4. To learn to analyze and design mass and heat transfer equipment

Drawings of symbols in flow sheets, piping, instrumentation on and other flow sheets.

Flow sheet development work and drawings of few flow sheets.

Mechanical designs and drawings of vessels under external and internal pressures, reactor

kettles, heat exchangers, evaporators, plate and packed column.

Typical layout and elevation drawing, simple piping pipe work design and drawings.

BOOKS RECOMMENDED :

1. Vilbrandt, C.T. and Dryden, C.E., Chemical Engineering plant design, International

Student Edition, Fourth Edition, Kogakusha.

2. Joshi, M.V. “Process Equipment Design”, 2nd Edition, McMillan Co. of India

Limited, Madras, 1932.

3. Bachurst, J.R. and Harker, J.A. “Process Plant Design”, Heiman

Education Books, London, 1973.

4. Evans, F.L., Equipment Design Hand Book for refineries and Chemical Plants,

Vol .I, 1979, Vol. II, 1980, Gulf Publishing Co., Houston, Texas.

Course Outcomes

i To synthesize and analyze process flow sheets, draw flow charts, layout

and specification of equipment

ii To effectively lead chemical engineering projects in industry

iii To know how to perform process selection

iv To analyze and design mass and heat transfer equipment

*****


PC 851 PROJECT

PROJECT WORK


Duration of SEE : SEE : 150 Marks

Credits : 6

Course Objectives

i To learn to analyze and improve a chemical process or a chemical plant.

ii To provide alternative methods to reduce energy requirements and raw

material

requirement. iii To design a virtual chemical plant using computer software.

iv To create a comprehensive technical report

and present it.

The final Project report will be submitted in the form bounded book (2 copies). The Report

will be evaluated by external examiner in the form Viva voce exam.

Course Outcomes

i Able to analyze and improve a chemical process or a chemical plant.

ii Able to provide alternative methods to reduce energy requirements and raw

material

requirement. iii Able to design a virtual chemical plant using computer software.

iv Able to create a comprehensive technical report

and present it.

*****

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