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SDMS Document __WHITMAN_ anies. INC.' 98438 _ ompanie 300782 PROGRESS REPORT #38 NOVEMBER 1998 ACTIVITIES FOR ROCKAWAY BOROUGH WELL FIELD SITE OPERABLE UNIT #3 FOR PROPERTY OF KLOCKNER & KLOCKNER ROCKAWAY BOROUGH, NEW JERSEY SUBMITTED TO: USEPA-REGION II EMERGENCY & REMEDIAL RESPONSE DIVISION NEW YORK, NEW YORK SUBMITTED BY: THE WHITMAN COMPANIES, INC. EAST BRUNSWICK, NEW JERSEY ON BEHALF OF KLOCKNER & KLOCKNER IN ACCORDANCE WITH: ADMINISTRATIVE ORDER ON CONSENT INDEX NO. H-CERCLA-95-0104 DECEMBER 1998 /ML (G: Michael N. Metlitz Project Manager Ira L. Whitman, Ph.D., P.E. Principal Consultant 44 West Ferris Street, East Brunswick, New Jersey 08816
Transcript
Page 1: SDMS Document WHITMAN anies . ompanie

SDMS Document __WHITMAN_anies.

INC.'

98438

_ompanie

300782

PROGRESS REPORT #38

NOVEMBER 1998 ACTIVITIES

FOR

ROCKAWAY BOROUGH WELL FIELD SITEOPERABLE UNIT #3FOR PROPERTY OF

KLOCKNER & KLOCKNERROCKAWAY BOROUGH, NEW JERSEY

SUBMITTED TO:

USEPA-REGION IIEMERGENCY & REMEDIAL RESPONSE DIVISION

NEW YORK, NEW YORK

SUBMITTED BY:

THE WHITMAN COMPANIES, INC.EAST BRUNSWICK, NEW JERSEY

ON BEHALF OF KLOCKNER & KLOCKNER

IN ACCORDANCE WITH:

ADMINISTRATIVE ORDER ON CONSENTINDEX NO. H-CERCLA-95-0104

DECEMBER 1998

/ML(G:

Michael N. MetlitzProject Manager

Ira L. Whitman, Ph.D., P.E.Principal Consultant

44 West Ferris Street, East Brunswick, New Jersey 08816

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I THE

WHITMAN-Companies,

www.whitmanco.com 44 West Ferris StreetEast Brunswick, N.J. 08816Tel.: (732) 390-5858Fax: (732) 390-9496

December 11,1998

Nancy Eberhardt, EsquireRiker, Danzig, Scherer, Hyland & PerrettiHeadquarters PlazaOne Speedwell AvenueMorristown,NJ 07962-1981

RE: Klockner&KlocknerRockaway Borough Wellfield Superfund Site - OU3Whitman Project #95-03-02

Dear Ms. Eberhardt:

Enclosed are an original and three (3) copies of the Progress Report for the month ofNovember 1998 for the'above-referencedproperty for your submittalto EPA.

\

If you have any questions concerning this submittal, please feel free to contactIra L. Whitman, Ph.D., P.E. or me at (732) 390-5858.

Very truly yours,

MichaerN. MProject Manager

MNM/sm

Enclosures

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PROGRESS REPORT #38NOVEMBER 1998 ACTIVITIES

ROCKAWAY BOROUGH WELL FIELD SITEOPERABLE UNIT #3

FOR PROPERTY OF KLOCKNER & KLOCKNERROCKAWAY BOROUGH, NEW JERSEY

1.0 INTRODUCTION

The following is a Progress Report for the month of November 1998 for the Klockner &Klockner portion of the Rockaway Borough Wellfield Superfund Site OU3 (Klockner Property). Thisreport is submitted pursuant to Paragraph 58 of the September 27, 1995 Administrative Order onConsent (AOC) between Klockner & Klockner (Klockner) and the United States EnvironmentalProtection Agency (EPA). Two (2) copies of this report are being submitted pursuant to Paragraph 61of the AOC.

2.0 ACTIONS TAKEN TOWARD ACHIEVING COMPLIANCE WITH AOCNOVEMBER 1998

The status of work and progress for the month of November 1998 is reported below. Progressfor work conducted prior to November 1998 is reported in the progress reports submitted for previousmonths.

Analytical data packages for the October 1998 soil sampling activities were received during themonth of November 1998. Review of the data and preparation of the Characterization Reportcommenced.

3.0 PERCENT OF WORK COMPLETED AND THE STATUS OF THE SCHEDULE

At this time, the percentage of work completed is approximately sixty percent (60%). Theactivities conducted to comply with the AOC are on schedule. The next scheduled activity byKlockner is to review the results of the approvedrrevised RI/FS WorksBlan soil sampling activities,identify any data deficiencies and prepare the Site Characterization Report. A schedule of activities ispresented in Table 1.

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4.0 DIFFICULTIES ENCOUNTERED AND CORRECTIVE ACTIONS TO BE TAKEN

No difficulties were encountered during the reporting period

5.0 SUMMARY OF RESULTS

A summary of the sample results received during November 1998 is provided below. Asummary of the sample results received during October 1998 was provided in the previous ProgressReport. Soil sample locations are indicated on the three (3) figures provided in Attachment 1. Draftanalytical data sheets for the sample results received during November 1998 are included inAttachment 2.

5.1 Building 12 - Underground Gasoline Tank

Two soil samples, SSGT-1 and SSGT-2, were collected at the former underground gasoline tanklocation for TCL Volatile Organic Compounds + 10 (VO+10) and Lead laboratory analysis. SampleSSGT-3 was collected as a duplicate of SSGT-1 for VO+10 analysis. The samples were collected tosatisfy the New Jersey Department of Environmental Protection's (NJDEP's) outstanding comments

on the investigation of this area. The VO results were none detected and the Lead concentrationswere well below the most stringent New Jersey Soil Cleanup Criteria (NJSCG) currently in effect.

5.2 Building 12 - Waste Oil Tank

Two delineation soil samples, SSWT-1 and SSWT-2, were collected at the former location ofthe underground waste oil tank for Purgeable Halocarbons (PHAL) analysis. Sample SSWT-1 alsoincluded analysis for TAL Metals. The analytical results indicated no contaminants were presentabove the most stringent NJSCC currently in effect.

5.3 Building 12 - Catch Basin/Storm Sewer

Soil sample SSCB-1 was collected at former sample location SS-8 to determine if furtherremediation is warranted pursuant to N.J.A.C. 7:26E due to the presence of Petroleum Hydrocarbons(PHCs). The sample was analyzed for TGL Base/Neutral Ex&aetable Organic Compounds + 15

(BN+15) and TAL Metals. The analytical results indicated no contaminants were present above themost stringent NJSCC currently in effect. '

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5.4 Building 12 - Leaching Pit

Soil sample SSLP-1 was collected from previous sample location SS-25 to determine if TALMetals were present. The analytical results indicated the presence of TAL Metals at concentrationsbelow the most stringent NJSCC currently in effect.

5.5 Building 12 - Degreaser Pit

Soil sample SSDP-1 was collected for PHAL analysis from between previous soil gassurvey samples VD-13 and VD-14 at the degreaserpit. The sample included analysis for TAL Metals.The analytical results indicated the presence of Tetrachloroethene (PCE) at 1.1 mg/kg which is just

above its current New Jersey Impact to Ground Water Soil Cleanup Criteria (NJIGWSCC) of 1 mg/kg.Trichloroethene (TCE) and TAL Metals were detected at concentrations below their respective moststringent NJSCC currently in effect.

5.6 Building 12 - Alleyway

This area included the alleyway, adjacent quonset hut, area between the alleyway and degreaserpit inside the building and western area of the building adjacent to the alleyway. Previous sampleresults indicated the presence of PHAL contamination in these areas. Twenty eight (28) soil gassamples had been proposed for the alleyway area for PHAL analysis. The soil gas survey indicated thepresence of PHAL throughout the area. TCE was detected in all of the soil gas samples collected. Theother PHAL detected in a significant number of the samples were cis-l,2-Dichloroethene(c-DCE) andPCE. The results of the soil gas survey were summarized in the previous Progress Report. Based onthe results of the approved soil gas samples, an additional fourteen (14) locations were sampled. Theadditional samples were collected from beneath the building area located west of the Alleyway.

Based on the soil gas survey results, nine (9) soil borings (SSAW-1 through SSAW-9) weresampled at two (2) depths for PHAL analysis. Sample SSAW-10 was collected as a duplicate ofsample SSAW-9 for PHAL analysis. The sample depths were based on field observations andscreening with a photoionization detector (PID). The analytical results indicated the presence of TCEabove or at its current New Jersey Residential Direct Contact Soil Cleanup Criteria (NJRDCSCC) of23 mg/kg in five (5) of the nine (9) shallow (<5 feet) sample locations and above its currentNJIGWSCC of 1 mg/kg in one (1) additioriafehallow sample location. PCE was detected above itscurrent NJRDCSCC of 4 mg/kg and NJIGWSCC of 1 mg/kg in the two shallow sample locationsbeneath the quonset hut. c-DCE was detected in two (2) of the shallow sample locations above itscurrent NJIGWSCC of 1 mg/kg. Samples collected at depth (>5 feet) were below the current NJSCC

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except at one (1) location, SSAW-1. TCE was detected in sample location SSAW-1 just above its

current NJIGWSCC.

5.7 Building 12 - Scale Room

The scale room is located inside the building at the southwest corner of the alleyway. This areawas included in the alleyway soil gas survey. TCE was detected in the soil gas samples collected inthis area. Soil samples SSSR-lthrough SSSR-3 were collected for PHAL. Sample SSSR-4 wascollected as a duplicate of SSSR-1 for PHAL analysis. Sample SSSR-1 was collected at a depth of 4

to 4.5 feet to vertically delineate the PHAL previously detected in this location. TCE was detectedbelow its current most stringent NJSCC in sample SSSR-1. The two (2) other sample locations werecollected from the 6 inch interval below the floor. TCE was detected in these two (2) sample locationsat concentrations exceeding the current NJRDCSCC and NJIGWSCC.

5.8 Building 12 - Drum Storage Shed

Soil sample SSFS-1 A and B were collected from the former location of a drum storage shed.

This area is located just northeast of the alleyway. Sample SSFS-1 A was analyzed for PHC, BN+15and TAL Metals. Samples SSFS-2 was collected as a duplicate of SSFS-1 A for the same parameters.Sample SSFS-1B was analyzed for VO+10. The analytical results indicated the presence of TCE and

c-DCE just above their respective current NJIGWSCC and Lead just above its current NJRDCSCC of400mg/kg.

5.9 Building 12 - Drum Storage in Alleyway

Soil sample SSDSA-1 was collected from the soil below the reported location of a spill of

cyanide containing solution and lead tin solution resulting from historical drum storage in thealleyway. The sample was analyzed for TAL Metals and total Cyanides. Sample SSDA-2 wascollected as a duplicate of SSDA-1 for the same parameters. Based on the elevated soil gas sampleresults in the area, the location was additionally sampled for PHAL at a field determined depth of 1.5-2feet. TCE was detected at this location above its NJIGWSCC. No other contaminants, including TALMetals or total cyanides, were detected above the most stringent NJSCC currently in effect.

S.lOBuilding 12 - North Drum Storage Area

Trichloroethene (TCE) was detected in four (4) of the twelve (12) soil gas samples collected

from this area. The samples where the TCE was detected are located north of the alleyway and justnorth of Building 12. As approved in the revised RI/FS Work Plan, soil at the two samples exhibiting

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the highest soil gas concentrations (SGN-33, SGN-43) were sampled for VO+10, BN+15, PHC andTAL Metals laboratory analyses. The analytical results indicated the presence of TCE above thecurrent NJRDCSCC and NJIGWSCC in sample SSNDS-1A and above the current NJIGWSCC inSSNDS-2A. No other contaminants were detected above the most stringent NJSCC currently ineffect.

5.11 Building 12-Sump

Soil sample SSSP-1 was collected from below the invert of the sump located in the building areajust west of the alleyway. The sample was analyzed for VO+10, PHC and TAL Metals. Contingentanalysis for BN+15 was not done as PHCs were detected below 100 mg/kg. The analytical resultsindicated the presence of TCE above its current NJRDCSCC and NJIGWSCC and PCE above itscurrent NJIGWSCC. Arsenic was detected at a concentration just above its current NJSCC of 20mg/kg.

5.12Building 13 - Soil Gas Survey

Thirty eight (38) soil gas samples had been proposed for the Building 13 property for PHALanalysis. The presence of PHAL was detected at eight (8) sample locations. The predominant PHALsdetected were PCE and" TCE. Based on the results of the approved soil gas samples and fieldobservations, eighteen (18) additional samples were collected. The additional samples collectedincluded those used to delineate the vertical and horizontal extent of contamination at soil gas samplelocations SG-22A (Concrete Pad Area) and SS-33 (Fence Area). A summary of the soil gas surveyresults was provided in the previous Progress Report.

Based on the results of the soil gas survey, additional soil samples for PHAL laboratory analysiswere collected from the Dumpster Pad, Former Dry Well, Hydropress Floor Drain, Concrete Pad andFence Areas. A summary of the results for each of these areas is presented below under each area'sheading.

5.13Building 13 - Former Dry Well

The soil gas survey indicated a relatively low concentration of PCE in this area. Higher PCEconcentrations were "detected in the soil gas samples in the fence area immediately to the south.Based on the soil gas results, soil sample SSDW-1 was collected adjacent to the former dry well forPHAL analysis. The analytical results indicated the presence of PCE at the current NJIGWSCC.

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5.14Building 13 - Oil Storage Shed

A soil gas sample collected as part of the site-wide soil gas survey was collected in front of thedischarge point of the pipe from the oil storage shed. The soil gas results indicated a relatively lowconcentration of 1,1,1-Trichloroethane. Soil sample SSOSS-1 was collected for PHAL laboratoryanalysis. The analytical results indicated the presence of 1,1,1-Trichloroethane below its currentNJIGWSCC of 50 mg/kg and NJRDCSCC of 210 mg/kg.

S.lSBuilding 13 - Storm Drain

A soil gas sample for PHAL was collected at the location of the storm drain catch basin as partof the site-wide soil gas survey. The results of the soil gas sample were none detected. As approvedin the revised RI/FS Work Plan, soil sample SSSD-1 was collected beneath the catch basin invert forPHAL laboratory analysis. The analytical results were none detected.

5.16Building 13 - Pipe

A soil gas sample for PHAL was collected near the pipe exiting the eastside of the building andthe recently discovered underground storage tank as part of the site-wide soil gas survey. The resultsof the soil gas sample were none detected. As discussed with the EPA case manager, CourtneyMcEnery, soil sample SSPP-1 was collected beneath the tank invert for PHAL laboratory analysis. Asample, UST-1 of the product in the tank was also collected for PHAL laboratory analysis. Theanalytical results were none detected.

S.lTBuilding 13 - Floor Drains

Floor drains are located in the vibratory cleaner area, basement bathroom and hydropressareas. Soil gas samples were collected for PHAL in the vicinity of the floor drains as part of thesite-wide soil gas survey. The results of the soil gas samples were none detected with theexception of Methylene Chloride detected at a relatively low concentration in the hydropress floordrain location (SG-22C).

As approved in the revised RI/FS Work Plan, soil sample SSFD-1 was collected beneath thebasement floor drain invert for PHAL laboratory analysis. The analytical results were none detected.

Based on the soil gas survey results, soil sample SSFD-2 was collected from the vicinity ofthe hydropress area for PHAL. The results indicated the presence of PCE in concentrations belowits most stringent NJSCC currently in effect.

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5.18Building 13 - Dumpster Pad

1 A soil gas sample was collected for PHAL at the corner of the concrete dumpster pad as part ofthe site-wide soil gas survey. A relatively low concentration of PCE was detected in the soil gassample. Soil sample SSDA-1 was collected on the down-slope side of the dumpster pad for PHALlaboratory analysis. The results indicated the presence of PCE in concentrations below its moststringent NJSCC currently in effect.

5.19Building 13 - Concrete Pad

The results of the site-wide soil gas survey indicated the presence of PHAL at the concrete padlocated south of Building 13. Additional soil gas samples were collected to further investigate thisarea during the soil gas survey. The results of the soil gas survey were summarized in the previousProgress Report. Soil samples were collected from borings SSCP-1 through SSCP-4 for PHALlaboratory analysis. Boring SSCP-1 was located at soil gas sample location SG-2A. Soil sampleswere collected from two depths at SSCP-1 and one depth at the other three (3) borings. The analysisof the two (2) samples collected at boring SSCP-1 was rushed by the laboratory to determine if thethree (3) horizontal delineation samples should be analyzed. The analytical results for the shallow anddeep sample depths at SSCP-1 were none detected. Based on a field instrument reading being higherin contingent sample SSCP-4, the laboratory was directed to analyze this sample. The analyticalresults for sample SSCP-4 were none detected.

5.20Building 13 - Fence Area

The results of the site-wide soil gas survey indicated the presence of PHAL at the fence arealocated southeast of Building 13. Additional soil gas samples were collected to further investigate thisarea during the soil gas survey. The results of the soil gas survey were summarized in the previousProgress Report. Soil samples were collected from borings SSFA-1 through SSFA-5 for PHALlaboratory analysis. Boring SSFA-1 was located at soil gas sample location SG-33. Soil samples werecollected from two depths at SSFA-1 and one depth at the other four (4) borings. The analysis of thetwo samples collected at boring SSFA-1 was rushed by the laboratory to determine if the four (4)horizontal delineation samples should be analyzed. The analytical results for the shallow sample depth

"at SSFA-1 indicated the presence of PCE just above the current NJIGWSCC. Based on this result, thelaboratory was directed to analyze the other four (4) samples. PCE was detected in sample SSFA-4just above its current NJRDCSCC and NJIGWSCC and in sample SSFA-3 just above its current

NJIGWSCC.

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5.21 Other

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Four (4) geological characterization samples were collected from each of the properties.

Samples SSGC-1 through SSGC-4 were collected at the Building 12 Property and samples SSGC-1A

through SSGC-4A were collected from the Building 13 Property. The samples were collected from

the different soil types encountered at each of the properties. The samples were analyzed for grain size

and total organic carbon (TOC). The TOC and grain size analysis indicated the presence of the

following soil conditions:

Sample Location

Alleyway SSAW-3

Alleyway SSAW-9

Alleyway SSAW-2

Alleyway SSAW-4

Concrete Pad SSCP-4

Fence Area SSFA-5

Fence Area SSFA-1

Former Dry Well SSDW-1

Sample ID

SSGC-1

SSGC-2

SSGC-3

SSGC-4

SSGC-1 A

SSGC-2A

SSGC-3A

SSGC-4A

Depth

4'-6'

l'-3'

r-4-

4'-7'

1.5'-4'

3 '-4'

4.5'-5'

2'-4'

TOC

(mg/kg)

8,720

14,900

6,660

390

16,200

1,960

429

10,400

Description

Fine to medium sand, some finegravel, some clayey si l t

Fine to medium sand and clayeysilt, little fine gravel

Clayey silt, some fine to coarse

sand, trace fine gravel

Fine to course sand and fine tocourse gravel, trace silt

Fine to medium sand and clayeysilt, some fine to coarse gravel

Fine to coarse sand and gravel,some silt

Fine to coarse sand, little fine

gravel, trace silt

Silt and fine to coarse sand, littlefine gravel

Note:Waiting on hard copy of SSGC-2Ato 4A grain size results.

The results of the disposal samples from the waste generated from the scale room pit clean-out

(DSSR-1) and sampling decon water (DSRW-1) are included in Attachment 2.

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Iii 6.0 ACTIVITIES PLANNED FOR NEXT REPORTING PERIOD

During the next reporting period the following activities will be conducted:

I«i 1. Continue the review of the analytical data packages.

IB 2. Preparation of the draft CharacterizationReport to be completed in January 1999.

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TABLE 1

KLOCKNER PROPERTY

PROJECTED RI/FS SCHEDULE

Jan Feb March AprilNov Dec

9.0 TASK 9 - FS REPORT

9.1 Detailed Analysis of Remedial Alternatives

9.2 Draft FS Report

9.3 Agency Review

1.0 TASK 1 - PROJECT PLANNING

1.1 Draft Plans (May 1996)

1.2 Agency Review (May 1996 to March 1997)

1.3 Draft Final Plans (June 1997}

1.4 Agency Review (June 1997 to July 1997)

2.0 TASK 2 - COMMUNITY RELATIONS (EPA)

3.0 TASK 3 - SITE CHARACTERIZATION

3.1 Field Investigation

3.1.1 Procure Subcontractors

3.1.2 Soil Gas Surveys

3.1 3 Soil Sampling

3.2 Data Analysis

3.3 Data Management

3.3.1 Sample Analysis

3.3.2 Validation

3.4 Monthly Progress Reports

3.5 Characterization Summary Report

4.0 TASK 4 - IDENTIFICATION OF CANDIDATE

TECHNOLOGIES FOR TREATABILITY STUDIES

(May 1996)

5.0 TASK 5 - TREATABILITY STUDIES

6.0 TASK 6 - RISK ASSESSMENT (EPA)

7.0 TASK 7 - R l REPORT

7.1 Draft Rl Report

7.2 Agency Review

7 3 Final Rl Report

8.0 TASK 8 - DEVELOPMENT OF REMEDIAL ACTION

OBJECTIVES AND SCREENING OF REMEDIAL

ALTERNATIVES

8.1 Identification

8.2 Initial Screening

8.3 Technical Memo

- Projected period for agency review of documents and preparation of Risk Assessment

* If task is necessary, schedule will be revised

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ATTACHMENT 1

DRAFT SOIL

SAMPLE LOCATION FIGURES

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SCALE 1" = 10'

I 1I SSCT-1 SSGT-211 • • 'I I

ELM STREET

- PROPERTY BOUNDARY

- STORM SEWER

- SANITARY SEWER

- SOIL SAMPLE LOCATION

THE

WHITMANCompanies,

INC.

ORIGINAL BY:

ccCHECKED 8Y:

CC

KLOCKNER & KLOCKNER PROPERTYROCKAWAY BOROUGHMORRIS COUNTY, NJ

SOIL SAMPLE LOCATIONS

BUILDING 12

DRAWN BY:A J

DATE:NOV 1998

DRAWING NO:

950302A41

FIGURE NO:

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FENCE

N

\

NORTH DRUM STORAGE AREA

PROPERTYBOUNDARY

• SSFS-1

SSNDS-1

SSAW-8SSDSA

SSNOS-2

SSCB-1

SSAW-7

SSAW-5

QUONSET HUT

•SSAW-6

ALLEYWAYSSAW-1

SSWT-1•

. SSAW-3

SSWT-2

SSSR-1

SSSP-1 SCALE ROOM

• •SSSR-2 SSSR-3

SSAW-9

BUILDING

12

SSAW-4

SSAW-2

STORAGE

STORAGE

SHIPPINGROOM

LOADINGBAY

300796

LEGEND

• - SOIL SAMPLE LOCATION

SCALE

20'

wTHE

WHITMANCompanies,

ORIG. BY: CC

DWG.#: 950302A2

KLOCKNER & KLOCKNER PROPERTY

ROCKAWAY BOROUGH

MORRIS COUNTY. NJ

NORTH DRUM STORAGE AREA AND

ALLEYWAY SOIL SAMPLE LOCATIONS

BUILDING 12

DWG.

DATE: NOV 1998

CHK. BY: CC

FIGURE: 2

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5

2 3ELM STREET

4 5

UJUJtr

CD

g LEGEND

SS*Q 1 SOIL SAMPLE LOCATION

300797

wTHE

WHITMANCompanies,

ORIG. BY:

DWG.#: 950302X4

KLOCKNER «c KLOCKNER PROPERTYROCKAWAY BOROUGH

MORRIS COUNTY. NJ

SOIL SAMPLE LOCATIONS

DWG- BY: A 3

DATE: NOV 1998

CHK- 8Y: CC

HGURE: 3

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II ATTACHMENT 2

II DRAFT SOIL SAMPLE DATA SHEETS

II

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ENVIROTECH RESEARCH, INC.

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777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.comII

II Novembers, 1998

The Whitman Companies, Inc.|B 44 West Ferris Street|| East Brunswick, NJ 08816W

U Attention: Mr. Michael Metlitz

Re: Job No. 1053 - Klockner & Klockner

Dear Mr. Metlitz:

» Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 09,1998:

flj Lab No. Client ID Analysis Required

89308 SSAW-5J.5-2 Purgeable HalocarbonsII 89309 SSAW-5_11-11.5 Purgeable Halocarbons' 89310 SSDP-l_2.5-3 Purgeable Halocarbons, TAL Metals

II If you have any questions please contact your Project Manager, Robert McGrady,at (732) 549-3900.

Very truly yoi

:" )

^Michael J. UrlLaboratory M

1)^ nUUan

JJJ II W E

i^OV §1996 !

]

ifffeg&r'hitman Companies. Inc.

300799

Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

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0(III Client ID: SSAW-5_1.5-2Site: Klockner & Klockner

B Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/22/98GC Column: DB624

B Instrument ID: VOAGC1.iLab File ID: geld9628.d

Lab Sample No: 89308Lab Job No: 1053

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 100.0% Moisture: 18.8

Parameter

g- Dichlorodifluoromethane]• ChloromethaneIP Vinyl Chloride

Bromomethane« ChioroethaneTrichlorofluoromethane1,l-DichloroetheneMethylene Chloridetrans-l,2-Dichloroethene1,l-Dichloroethanecis-1,2-Dichloroethene« Chloroform1,1,1-TrichloroethaneCarbon Tetrachloride

m 1,2-Dichloroethanefll Trichloroethene™ 1,2-Dichloropropane

Bromodichloromethane« 2-Chloroethyl Vinyl Ethercis-1,3-Di chloropropenetrans -1,3 -Dichloropropene1,1,2-Trichloroethane

B TetrachloroetheneDibromochloromethaneChlorobenzene« Bromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene

II) 1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDND

406

10600

5850

NDNDNDND

NDNDNDNDNDND

NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

302302302302302302302302302302302302302302302302302302302302302302302302302302302302302302

300800

Page 20: SDMS Document WHITMAN anies . ompanie

(III

Client ID: SSAW-5_11-11.5Site: Klockner & Klockner

m Date Sampled: 10/08/98II Date Received: 10/09/98II Date Analyzed: 10/21/98

GC Column: DB624» Instrument ID: VOAGC1.iLab File ID: geld9611.d

Lab Sample No: 89309Lab Job No: 1053

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 5.8

25 .0 ml50 .0

1

II

II

0

IIII

II1IIIIII1

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChioroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,1-Dichloroethane . ..cis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

123123123123123123123123123123123123123123123123123123123123123123123123123123123123123123

300801

Page 21: SDMS Document WHITMAN anies . ompanie

III0

Client ID: SSDP-l_2.5-3Site: Klockner & Klockner

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/21/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9612.d

I00IIiIIII1IIH0flH

Lab Sample No: 89310Lab Job No: 1053

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 10.2

25.0 ml50.0

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChioroethaneTrichlorofluoromethane1,l-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethane . ..cis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2 -Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/'kg(Dry Weight)

KDXDXDKDKDKDKDKDKDKDXDKDKDXDXT)

656

1100

XDXT)KDKDKDKD

KDXT)XT)XT)XT)XT)

QuantitationLimit

Units: ug/kg

139139139139139139139139139139139139139139139139139139139139139139139139139139139139139139

300802

Page 22: SDMS Document WHITMAN anies . ompanie

IIII1II0II

Client ID: SSDP-1 2.5-3Site: Klockner & Klockner

Date Sampled:Date Received:

10/08/9810/09/98

Lab Sample No: 89310Lab Job No: 1053

Matrix: SOLIDLevel: LOW% Moisture: 10.2

METALS ANALYSIS

II

II

0

0

II

Analvte

AnalyticalResult

Units: mg/kg(Dry Weight)

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

9080ND10.154.50.520.36

537012.07.8

28.129600

1732480446

0.1415.0912NDNDNDND25.597.6

InstrumentDetection

Limit Qual M

13 .01.0 N0.850.31. 0 .0450.089 B9.40 . 2 2 *0 . 2 7 B0.789.20 .569 .00.24 *0.0190.47

66.9 B1.10.31

94.91.10 .421.0 *

PPPPPPPPPPPPPPcvPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300803

Page 23: SDMS Document WHITMAN anies . ompanie

K*tk+tr A

fROJKCTNOt M-OJ-OJ

LABORATORY: Envlrotech Rtsctrch, Inc.

SITE ADDRESS: SllcUt Avt»« & Elm Strut, R<yck«w»y Boronth, NJ

SAMPLE DATE: I °( t^'^

SAMPLER(S): Cheryl L. CofTte L .

AMPLE,TIME

.: SAMPLELOCATION

X:SAMPLE

DM .SAMPLE; DEPTH

SAMPLEMATRIX

'<,'• ANALYSISREQUESTED

PRESER-'VATIVE

NO. OK

CONT.^ SPECIAL. . ^

" X< INSTRUCTIONS ^*-V

2-

TOTAL NO. CONTAINERS

RELINQUISHED BY:

RELINQUISHED BV:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PHC PETROLEUM HYDROCARBONS

VOC VOLATILE OROANICS BY GOMS WITH LIBRARY SEARCH

PAH POLYCYCLIC AROMATIC HYOROCARBOSS IN BASE NEUTRAL SCAN WITH LIBRARY SEARCH

BN BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTABLES WITH LIBRARY SEARCHPPM PRIORITY POLLUTANT METALSPP'JO PRJORtTY POLLUTANT PLUS FORTY PEAKS

CT • CEILING TILE

FT- FLOOR TILE

TSI - THERMAL SYSTEM IVSL'LATION

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300804

Page 24: SDMS Document WHITMAN anies . ompanie

0III

ENVIROTECH RESEARCH, INC.

777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.com

Novembers, 1998

I

fl

ll

II

0fl•I

niiftiiII

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Mr. Michael Metlitz

-.

1998 !L:;;

Tho Whitrnan Companies, Inc.j

Re: Job No. 105 1 - Klockner & Klockner

Dear Mr. Metlitz:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 09, 1998:

Lab No.

89298

Client ID

UST-1

Analysis Reuired

Purgeable Halocarbons

If you have any questions please contact your Project Manager, Robert McGrady,at (732) 549-3900.

Michael J. UrbanLaboratory Manager

300805

Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

Page 25: SDMS Document WHITMAN anies . ompanie

III10II

Client ID: UST-1Site: Klockner & Klockner

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/22/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9631.d

Lab Sample No: 89298Lab Job No: 1051

Matrix: SOILLevel: HIGHSample Weight: 1 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 0.0

10.0 ml2500.0

00HII

IIfl1IIfl1no

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

236002360023600236002360023600236002360023600236002360023600236002360023600236002360023600236002360023600236002360023600236002360023600236002360023600

300806

Page 26: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klockner & Klockner

PROJECTNO: 95-03-02 £ f\vi'"ofeth

LABORATORY: Envirotech Research, Inc.

?"0<iOO2>SITE ADDRESS: Stickle Aveine & Elm Street, Rockr»*y Borough, NJ

SAMPLE DATE: I of 8

PAGE 1 OF |

SAMPLER(S): Cheryl L. Coffee I i, -

SAMPLE.TIME

(3^o

.,, . -SAMPLELOCATION

USrf&upG-is)

SAMPLE jtut '..'

•jusT-r

„ /'/

SAMPLEDEPTH

T->/»/

SAMPLEMATRIX

;

to

_,, - ANALYSIS .• , REQUESTED . ;

*

Pil/\u

• -- .4 ^*1

PRESER^VATIVE

I f^ / fid

NO. OF

CONT.:.

//^

SPECIAL""•'INSTRUCTIONS'1^

rJ>?-5»-*

RELINQUISHED BY

RELINQWSHED BY:

ANALYTICAL PARAMETEKIDENTIFICATION KEY:PHC PETROLEUM HYDROCARBONS

VOC VOLATILE ORGANICS BY GOMS WITH LIBRARY SEARCH

PAH POLYCVCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SEARCH

BN BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTABLES WITH LIBRARY SEARCHPPM PRIORITY POLLUTANT METALSPPMO PRJORtTY POLLUTANT PLUS FORTY PEAKS

CT • CEILING TILK

FT- FLOOKTIU

TSI • THERMAL SYSTEM INSL'LATION

TOTAL NO. CONTAINERS,

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300807

Page 27: SDMS Document WHITMAN anies . ompanie

IIn ENVIROTECH RESEARCH, INC.

777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.com

00noonoogii

Novembers, 1998

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Dr. Ira Whitman

Re: Job No. H950 - Klockner & Klockner

Dear Dr. Whitman:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 07,1998:

oo0n

Lab No.

88662886638866488665886668866788668886698867088671886728867388674886758867788678886798868088681

Client ID

Trip_BlankFB-2

SSAW-7_5-5.5SSAW-7J2-12.5

SSSP-l_4-4.5SSAW-9_1-1.5

SSAW-KM-1.5SSAW-9J 1.5-12

SSGC-2J-3SSAW-2J.5-2SSAW-2_7.5-8SSGC-3_l-4

SSSR-2_>0.5SSSR-3_0-0.5SSFS-2_0-0.5

SSAW-4_4-4.5SSAW-4_9.5-10

SSGC-4_4-7SSSR-1 4-4.5

Analysis Required

TCLVOA-t-10TCLVOA+10

Purgeable HalocarbonsPurgeable Halocarbons

TCL VOA+10, TAL Metals, PHCPurgeable HalocarbonsPurgeable HalocarbonsPurgeable Halocarbons

TOCPurgeable HalocarbonsPurgeable Halocarbons

TOCPurgeable HalocarbonsPurgeable Halocarbons

TCL BN+10, TAL Metals, PHCPurgeable HalocarbonsPurgeable Halocarbons

TOCPurgeable Halocarbons

300808

Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

Page 28: SDMS Document WHITMAN anies . ompanie

Lab No.

8868288683886848868588686

Client ID

SSSR-4 4-4.5SSLP-1 12-12.5SSGT-2 7-7.5SSGT-1 7-7.5SSGT-3 7-7.5

Analysis Required

Purgeable HalocarbonsTAL Metals

TCLVOA+10,PbTCLVOA+10,Pb

TCLVOA+10

Michael J. Urban

1I! ENVIROTECH RESEARCH, INC.

niiiiH An invoice for our services is also enclosed. If you have any questions please

contact your Project Manager, Robert McGrady, at (732) 549-3900.

Very truly ^ours,

I11 Laboratory Manager

II

0001IInnio

300809

Page 29: SDMS Document WHITMAN anies . ompanie

1IIIIIIII1II0II0

Client ID: Trip_BlankSite: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMSS.iLab File ID: e4657.d

Lab Sample No: 88662Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight:Methanol Ext.Ext. Dilution% Moisture: 0

10.0 gVolume: 25.0 mlFactor: 50.0

II

1

II

II

00

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1,3 -DichloropropeneBromoform4-Methyl-2 -Pentanone2 -HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

620620620620380620620250620620620620250620620250120120620120620380120620500620620120120620620500620620

300810

Page 30: SDMS Document WHITMAN anies . ompanie

II

IIniioaoD

Client ID: Trip_BlankSite: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMS5.iLab File ID: e4657.d

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 826OB

Lab Sample No: 88662Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10.0 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 0.0

• GC/MSCOMPOUNDS

2550

ml

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT EST . CONC .ug/kg

Q

0IIIn

nnno

TOTAL ESTIMATED CONCENTRATION 0.0

300811

Page 31: SDMS Document WHITMAN anies . ompanie

IIIIIIIIII0000100

Client ID: FB-2Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAMS3.iLab File ID: c2236.d

Lab Sample No: 88663Lab Job No: H950

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 1.0

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 8260

Analytical ResultUnits: uq/1

II00II

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,l-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans -1,3-DichloropropeneBromoform4-Methyl-2 -Pentanone2 -HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/1

5.05.05.05.03.05.05.02.05.05.05.05.02.05.05.02.0115153154551155455

.0

.0

. 0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

300812

Page 32: SDMS Document WHITMAN anies . ompanie

IIniinnnninnioinninn

Client ID: FB-2Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAMS3.iLab File ID: c2236.d

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 826OB

Lab Sample No: 88663Lab Job No: H950

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 1.0

• GC/MSCOMPOUNDS

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT EST. CONC.ug/1

Q

TOTAL ESTIMATED CONCENTRATION 0.0

300813

Page 33: SDMS Document WHITMAN anies . ompanie

Client ID: SSSP-l_4-4.5Site: Klockner & Klockner

Lab Sample No: 88666Lab Job No: H950

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAMSl.iLab File ID: a6484.d

Matrix: SOILLevel: HIGHSample Weight: 10.8 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 250.0% Moisture: 10

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg(Dry Weight)

00IID

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,l-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichlpropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans -1,3-DichloropropeneBromoform4-Methyl- 2 -Pentanone2 -HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

NDNDNDNDNDNDNDNDNDND

790 JNDNDNDNDNDNDNDND

37000NDNDNDNDNDNDND

2100NDNDNDNDNDND

QuantitationLimit

Units: ug/kg

3200320032003200190032003200130032003200320032001300320032001300640640320064032001900640

320026003200320064064032003200260032003200

300814

Page 34: SDMS Document WHITMAN anies . ompanie

IIniinin

Client ID: SSSP-l_4-4.5Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAMSl.iLab File ID: a6484.d

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 826OB

Lab Sample No: 88666Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10.8 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 250.0% Moisture: 10.0

- GC/MSCOMPOUNDS

IIflnioiiinniii

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.

-29.30.

RT

TOTAL ESTIMATED CONCENTRATION

30081

EST. CONC.ug/kg

0.0

5

Q

Page 35: SDMS Document WHITMAN anies . ompanie

IIIIIII0I0uDIIIII01II1111

Client ID: SSFS-2_0-0.5Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/21/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8328.d

Lab Sample No: 88677Lab Job No: H950

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 5.0 mlDilution Factor: 1.0% Moisture: 4

Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 8270C

Analytical ResultsUnits: ug/kg(Dry Weight)

bis(2-Chloroethyl)ether1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzenebis(2-chloroisopropyl)etherN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophoronebis(2-Chloroethoxy)methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene2-MethylnaphthaleneHexachlorocyclopentadiene2 -Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphtheneDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-NitroanilineN-Nitrosodiphenylamine4 -Bromophenyl-phenyletherHexachlorobenzenePhenanthreneAnthracene

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

78 JND

QuantitationLimit

Units: ug/kg

878708708708708787878708708787087017087087087017008708701701700870870170870870870170087087087870870

300816

Page 36: SDMS Document WHITMAN anies . ompanie

II11Client ID: SSFS-2_0-0.5Site: Klockner & Klockner

II

II

II

II

Date Sampled: 10/07/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/21/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8328.d

Lab Sample No: 88677Lab Job No: H950

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 5.0 mlDilution Factor: 1.0% Moisture: 4

Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 8270C

Analytical ResultsUnits: ug/kg(Dry Weight)

II

P

HII

CarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)anthraceneChrysenebis(2 -Ethylhexyl)phthalateDi-n-octylphthalateBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(a)pyreneIndeno(1,2,3-cd)pyreneDibenz(a,h)anthraceneBenzo(g,h,i)perylene

NDND

120 J130 J

NDND

55 J120 J

13000ND

ioo39 J81 J36 JND

46 J

QuantitationLimit

Units: ug/kg

8708708708708701700878708708708787878787870

PI11

300817

Page 37: SDMS Document WHITMAN anies . ompanie

II1II1II

Client ID: SSFS-2_0-0.5Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/21/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8328.d

Lab Sample No: 88677Lab Job No: H950

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 5.0 mlDilution Factor: 1.0% Moisture: 4.5

SEMI-VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 827OC

COMPOUND NAME

1 . Unknown Alkane2 . Unknown Alkane3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

27.0329.20

'

EST. CONG,ug/kg

12003900

Q

TOTAL ESTIMATED CONCENTRATION 5100

300818

Page 38: SDMS Document WHITMAN anies . ompanie

0DIIIII

Client ID: SSGT-2_7-7.5Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMS5.iLab File ID: e4658.d

Lab Sample No: 88684Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10.7 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 7

25.0 ml50.0

II

1

II

If

I

II

nipnniii

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg(Dry Weight)

ChioromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,l-Dichloroethanetrans -1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1,3-DichloropropeneBromoform4-Methyl- 2 -Pentanone2 -HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

620620620620380620620250620620620620250620620250120120620

- 120620380120620500620620120120620620500620620

300819

Page 39: SDMS Document WHITMAN anies . ompanie

nii

Client ID: SSGT-2_7-7.5Site: Klockner & Klockner

1

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMS5.iLab File ID: e4658.d

Lab Sample No: 88684Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10.7 gMethanol Ext. Volume :Ext. Dilution Factor:% Moisture: 6.6

25.0 ml50.0

VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 826OB

11_

n"

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT EST. CONG,ug/kg

Q

IIi

TOTAL ESTIMATED CONCENTRATION 0.0

300820

Page 40: SDMS Document WHITMAN anies . ompanie

Client ID: SSGT-l_7-7.5,Site: Klockner & Klockner

Lab Sample No: 88685Lab Job No: H950

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMSS.iLab File ID: e4659.d

Matrix: SOILLevel: HIGHSample Weight: 10.0 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 8

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg(Dry Weight)

Chloromethane« Bromome thaneVinyl ChlorideChloroethaneMethylene Chloride

\]| Acetone|§ Carbon Disulf ide1,1-Dichloroethene

10 1, l-Dichloroethane11 trans-1,2-Dichloroethene'" cis-1,2-DichloroetheneChloroform

fl, 2 -Dichloroethane2-Butanone1,1,1-Trichloroethane

jg Carbon Tetrachloride!• Bromodichloromethane™ 1,2-Dichloropropane

cis-1,3-Dichloropropene

B TrichloroetheneDibromochloromethane1,1,2-Trichloroethane

§ Benzenetrans-1,3-DichloropropeneBromoform4-Methyl- 2 -Pentanone

H 2-HexanoneTetrachloroethene1,1,2,2-Tetrachloroethane

» TolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

1

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

680680680680410680680270680680680680270680680270140140680140680410140680540680680140140680680540680680

300821

Page 41: SDMS Document WHITMAN anies . ompanie

IClient ID: SSGT-l_7-7.5Site: Klockner & Klockner

Lab Sample No: 88685Lab Job No: H950

II

Date Sampled: 10/07/98ate Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMS5.iLab File ID: e4659.d

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 826OB

Matrix: SOILLevel: HIGHSample Weight: 10.0 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 7.8

- GC/MSCOMPOUNDS

25.0 ml50.0

II COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.2?.23.24.25.26.27.28.29.30.

RT EST. CONG,ug/kg

Q

II

i

liiii

i

TOTAL ESTIMATED CONCENTRATION

300822

0.0

Page 42: SDMS Document WHITMAN anies . ompanie

I1Client ID: SSGT-3_7-7.5Site: Klockner & Klockner

Date Sampled: 10/07/98"Date Received: 10/07/98jiDate Analyzed: 10/15/98GC Column: DB624

IInstrument ID: VOAMSS.iLab File ID: e4660.d

Lab Sample No: 88686Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10.2 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 9

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 8260B

Analytical ResultsUnits: ug/kg(Dry Weight)

Chloromethane

H BromomethaneVinyl ChlorideChloroethaneMethylene Chloride

II Acetone|i Carbon Disulf ide

1,1-Dichloroethene

H I, 1-Dichloroe thane'trans-1,2-Dichloroethenecis-l,2-DichloroetheneChloroform

II 1,2-DichloroethaneII 2-Butanone

1,1,1-Trichloroethane« Carbon Tetrachloride:Bromodichloromethane1,2-Dichloropropane

_ cis-l,3-Dichloropropene|| TrichloroetheneJ| Dibromochloromethane

1,1,2 -Trichloroethane

I Benzenetrans-1,3-DichloropropeneBromoform4-Methyl-2 -Pentanone

B 2-HexanoneTetrachloroethene1,1,2,2-Tetrachloroethane

m Toluenel| Chlorobenzene™ Ethylbenzene

StyreneJ| Xylene (Total)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

II

II

QuantitationLimit

Units: ug/kg

670670670670400670670270670670670670270670670270130130670

. 130670400130670540670670130130670670540670670

300823

Page 43: SDMS Document WHITMAN anies . ompanie

II0IIII11

Client ID: SSGT-3_7-7.5Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMS5.iLab File ID: e4660.d

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 826OB

Lab Sample No: 88686Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10.2 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 8.9

- GC/MSCOMPOUNDS

2550

ml

11IIIP

1111

n~

41IIII

'•£ITIE

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19 .20.21.22.23.24.25.26.27.28.

. 29.30.

RT EST. CONG,ug/kg

Q

IIII0

TOTAL ESTIMATED CONCENTRATION 0.0

300824

Page 44: SDMS Document WHITMAN anies . ompanie

IIII0IIn

Client ID: SSAW-7_5-5.5Site: Klockner & Klockner

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9565.d

Lab Sample No: 88664Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 13.9

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

283NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

140140140140140140140140140140140140140140140140140140140140140140140140140140140140140140

300825

Page 45: SDMS Document WHITMAN anies . ompanie

1Client ID: SSAW-7_12-12 . 5Site: Klockner & Klockner

II

nii11

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGCl.iLab File ID: geld9566-.d

Lab Sample No: 88665Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 5.5

1

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

648NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

128128128128128128128128128128128128128128128128128128128128128128128128128128128128128128

300826

Page 46: SDMS Document WHITMAN anies . ompanie

IIIClient ID: SSAW-9_1-1.5Site: Klockner & Klockner

Lab Sample No: 88667Lab Job No: H950

Date Sampled: 10/07/98pDate Received: 10/07/98bate Analyzed: 10/21/98GC Column: DB624Instrument ID: VOAGC1.i[Lab File ID: geld9602.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 17.0

25 .0 ml5 0 0 . 0

1

II

\\

1

Parameter

DichlorodifluoromethaneChioromethane'Vinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,l-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

23300NDNDNDNDNDNDNDNDNDNDNDNDNDND

II

ni

QuantitationLimit

Units: ug/kg

1460146014601460146014601460146014601460146014601460146014601460146014601460

. 14601460146014601460146014601460146014601460

300827

Page 47: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-10_1-1. 5.Site: Klockner & Klockner

Lab Sample No: 88668Lab Job No: H950

Date Sampled: 10/07/98pate Received: 10/07/98Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGCl.i[Lab File ID: geld9568.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 17.2

25.0 ml500.0

H Parameter

Dichlorodifluoromethane.. Chi or ome thaneII Vinyl Chloride"• Bromomethane

Chloroethane

V Trichlorof luorome thane1,1-DichloroetheneMethylene Chloride

I trans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform

I- 1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene

|| 1,2-Dichloropropane•I Bromodichloromethane

2-Chloroethyl Vinyl Ethern cis-1, 3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-Trichloroethane

, TetrachloroetheneII Dibromochloromethane11 Chlorobenzene

Bromoform

H I, 1, 2 , 2 -Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene

„ 1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

21200NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

151015101510151015101510151015101510151015101510151015101510151015101510151015101510151015101510151015101510151015101510

300828

Page 48: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-9_11.5-12.Site: Klockner & Klockner

Lab Sample No: 88669Lab Job No: H950

Date Sampled: 10/07/98[Date Received: 10/07/98[Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9569.d

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 3.8

25.0 ml50.0

II Parameter

Dichlorodifluoromethane

H Chloromethane'Vinyl ChlorideBromomethaneChloroethane

V Trichlorof luorome thane1,1-DichloroetheneMethylene Chloride

B trans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform« 1,1,1-TrichloroethaneCarbon Tetrachloride1,2-Dichloroethane

B Trichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethern cis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-Trichloroethane

.- TetrachloroetheneII Dibromochloromethane™ Chlorobenzene

Bromoform

B l, 1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

41

1

II

QuantitationLimit

Units: ug/kg

120120120120120120120120120120120120120120120120120120120

• 120120120120120120120120120120120

300829

Page 49: SDMS Document WHITMAN anies . ompanie

11Client ID: SSAW-2_1.5-2Site: Klockner & Klockner

Date Sampled: 10/07/98pate Received: 10/07/98Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGC1.i(Lab File ID: geld9570.d

Lab Sample No: 88671Lab Job No: H950

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 21.6

25.0 ml1000.0

ft

II

ft

I

I

Parameter

Dichlorodifluoromethane

I ChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethane'cis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

23100NDNDNDNDNDNDNDNDNDNDNDNDNDND

II

II

0

QuantitationLimit

Units: uQ/kg

307030703070307030703070307030703070307030703070307030703070307030703070307030703070307030703070307030703070307030703070

300830

Page 50: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-2_7.5-8nSite: Klockner & Klockner

Lab Sample No: 88672Lab Job No: H950

Date Sampled: 10/07/98|Date Received: 10/07/98foate Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGC1.i|Lab File ID: geld9564.d

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 4.6

25.0 ml50.0

Parameter

DichlorodifluoromethaneiChloromethaneVinyl Chloride'BromomethaneChloroethaneITrichlorofluoromethane,1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene11,1-Dichloroethane' cis-l,2-DichloroetheneChloroform

i l, 1,l-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-Dichloropropane

1Bromodichloromethane2-Chloroethyl Vinyl Ether

X cis-l,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

144NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

118118118118118118118118118118118118118118118118118118118

. 118118118118118118118118118118118

300831

Page 51: SDMS Document WHITMAN anies . ompanie

Client ID: SSSR-2_0-0.5Site: Klockner & Klockner

Lab Sample No: 88674Lab Job No: H950

Date Sampled: 10/07/98Date Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9593.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 7.5

25.0 ml1000.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideB romome t haneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,l-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDND

" NDNDNDNDND

43900NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

262026202620262026202620262026202620262026202620262026202620262026202620262026202620262026202620262026202620262026202620

II

II

II

300832

Page 52: SDMS Document WHITMAN anies . ompanie

Client ID: SSSR-3_0-0.5.Site: Klockner & Klockner

Lab Sample No: 88675Lab Job No: H950

Date Sampled: 10/07/98[Date Received: 10/07/98(Date Analyzed: 10/19/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9572.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 7.5

25 .0 ml1000.0

II

II

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDND

" NDNDNDNDND

19700NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

2620262026202620262026202620262026202620262026202620262026202620262026202620

. 26202620262026202620262026202620262026202620

300833

Page 53: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-4_4-4.5Site: Klockner & Klockner

Lab Sample No: 88678Lab Job No: H950

Date Sampled: 10/07/98

I Date Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.i[Lab File ID: geld9594.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 1000.0% Moisture: 21.8

II

II

II

II

I

II

ft

II

01no

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-Trichloroethane

1 Carbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

23200NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

307030703070307030703070307030703070307030703070307030703070307030703070307030703070307030703070307030703070307030703070

300834

Page 54: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-4_9 . 5-10Site: Klockner & Klockner

Lab Sample No: 88679Lab Job No: H950

Date Sampled: 10/07/98

IDate Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9595.d

II

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 4.0

25.0 ml100.0

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,l-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-l,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

260260260260260260260260260260260260260260260260260260260

. 260260260260260260260260260260260

300835

Page 55: SDMS Document WHITMAN anies . ompanie

Client ID: SSSR-l_4-4.5.Site: Klockner & Klockner

Lab Sample No: 88681Lab Job No: H950

Date Sampled: 10/07/98

I Date Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.i[Lab File ID: geld9579.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 11.5

25.0 ml50.0

B Parameter

Dichlorodifluoromethane._ Chloromethane11 Vinyl Chloride*" Bromomethane

Chloroethane

O Trichl or of luorome thane1,1-DichloroetheneMethylene Chloride

._ trans-1,2-DichloroetheneII1,1-Dichloroethane•* cis-l,2-DichloroetheneChloroform» 1,1,1 - TrichloroethaneCarbon Tetrachloride1,2-Dichloroethane

g TrichloroetheneJl1,2-Dichloropropane•I Bromodichloromethane

2-Chloroethyl Vinyl Ether

B cis-1, 3 -Dichloropropenetrans-1,3 -Dichloropropene1,1,2-TrichloroethaneTetrachloroethene

•I Dibromochloromethane11 Chlorobenzene

Bromoform

D l, 1, 2 , 2 - Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

1

159NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

138138138138138138138138138138138138138138138138138138138138138138138138138138138138138138

300836

1

Page 56: SDMS Document WHITMAN anies . ompanie

Client ID: SSSR-4_4-4.5Site: Klockner & Klockner

Lab Sample No: 88682Lab Job NO: H950

Date Sampled: 10/07/98[Date Received: 10/07/98[Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9586.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 12.1

25.0 ml50.0

II Parameter

Dichlorodifluoromethane

U Chlorome thaneVinyl Chloride

• BromomethaneChloroethane« Trichl or of luorome thane1,1-DichloroetheneMethylene Chloride

II trans-1,2-DichloroetheneII 1,1-Dichloroethane•• cis-1,2-Dichloroethene

Chloroform

0 1,1,1-TrichloroethaneCarbon Tetrachloride1,2-Dichloroethane

__ Trichloroethene11 1,2-Dichloropropane•• Bromodichloromethane

2-Chloroethyl Vinyl Ether

B cis-1, 3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroethene

•I Dibromochloromethane™ Chlorobenzene

Bromoform

B~~ 1,1,2, 2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

1

712NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

138138138138138138138138138138138138138138138138138138138

- 138138138138138138138138138138138

300837

I

Page 57: SDMS Document WHITMAN anies . ompanie

IIgH Client ID: SSSP-1 4-4.5

Site: Klockner & KlocknerLab Sample No: 88666Lab Job No: H950

I

Date Sampled:Date Received:

10/07/9810/07/98

Matrix: SOLIDLevel: LOW% Moisture: 10.0

METALS ANALYSIS

0no8Hniiiiiiii

Analvte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

AnalyticalResult

Units: mg/kg(Dry Weight)

8480ND21.12020.520.80

1140014.64.950.4

144003152200251

1.910.1818NDND257ND21.4294

InstrumentDetection

Limit Qual M

12100009000909000

6610

94101

.9

.0 N

.84

.31

.044

.089 ' B

.4

.22 *

.27 B

.78

.2

.56

.0

.24 *

.037

.47

.7 B

.1

.31

.7 B

.1

.42

.0 *

PPPPPPPPPPPPPPCVPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300838

Page 58: SDMS Document WHITMAN anies . ompanie

IIII111

Client ID: SSFS-2 0-0.5Site: Klockner & Klockner

Date Sampled:Date Received:

10/07/9810/07/98

Lab Sample No: 88677Lab Job No: H950

Matrix: SOLIDLevel: LOW% Moisture: 4.5

METALS ANALYSIS

fl

II

0II00IIIIII0I1

Analyte

AnalyticalResult

Units: mg/kg(Dry Weight)

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

5550ND2 .71.0.1.

423040.15.63.

2500070.

3420217

0.27.

1660NDNDNDND53.

334

74390

366

2

051

0

InstrumentDetection

Limit Qual M

12000008000808000

6210

89100

.2

.96 N

.80

.29

.042 B

.084 ' B

.8

.21 *

.25

.73

.7

.52

.4

.23 *

.017

.44

.9

.0

.29

.2

.0

.40

.94 *

PPPPPPPPPPPPPP

• cvPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300839

Page 59: SDMS Document WHITMAN anies . ompanie

0II1IiIIIIII

Client ID: SSLP-1 12-12.5Site: Klockner & Klockner

Date Sampled:Date Received:

10/07/9810/07/98

Lab Sample No: 88683Lab Job No: H950

Matrix: SOLIDLevel: LOW% Moisture: 4.1

II

011

II0I0

METALS ANALYSIS

Analyte

AnalyticalResult

Units: mg/kg(Dry Weight)

InstrumentDetection

Limit

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

3040ND4.15.0.

ND102000

6.5.12.

142006.

58000276ND9.

876NDND138ND9.38.

5752

130

6

7

92

Qual M

1200000

4400080

42000

6210

88100

.1

.96 N

.79

.29 B

.042

.083

.0

.21 *

.25 B

.73

.7

.52

.0

.23 *

.017

.44

.6 B

.0

.29

.8 B

.0

.40 B

.94 *

PPPPPPPPPPPPPPCVPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300840

Page 60: SDMS Document WHITMAN anies . ompanie

IIIII Client ID: SSGT-2 7-7.5

Site: Klockner & KlocknerLab Sample No: 88684Lab Job No: H950

II

Date Sampled:Date Received:

10/07/9810/07/98

METALS ANALYSIS

Matrix: SOLIDLevel: LOW% Moisture: 6.6

II

II

II

1

Analyte

Lead

AnalyticalResult

Units: mg/kg(Dry Weight)

2.6

InstrumentDetection

Limit

0.54

Qual M

P

II

II

1

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

I

300841

Page 61: SDMS Document WHITMAN anies . ompanie

II0

I10

Client ID: SSGT-1 7-7.5Site: Klockner & Klockner

Date Sampled:Date Received:

10/07/9810/07/98

METALS ANALYSIS

Lab Sample No: 88685Lab Job No: H950

Matrix: SOLIDLevel: LOW% Moisture: 7.

II

II

Analyte

Lead

AnalyticalResult

Units: mg/kg(Dry Weight)

4 .7

InstrumentDetection

Limit

0.54

Qual M

P

II

0

II1

IIII0

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300842

Page 62: SDMS Document WHITMAN anies . ompanie

1II11III

Site: Klockner & Klockner

Date Sampled: 10/7/98Date Received: 10/7/98Matrix: SOIL

Lab Job No: H950

Date Analyzed: 10/14/98QA Batch: 1402

EnvirotechSample #

88670

88673

88680

Client ID

SSGC-2_l-3

SSGC-3_l-4

SSGC-4 4-7

TOTAL ORGANIC CARBON

DilutionMoisture Factor

Analytical Resultmg/kg (Dry Wt.

17.4

18.5

3.7

4

4

2

.0

.0

.0

14900

6660

390

giioi

Quantitation Limit for Total Organic Carbon is 100 mg/kg for anundiluted sample.

II

01IIII

300843

Page 63: SDMS Document WHITMAN anies . ompanie

1

1IIII

Site: Klockner & Klockner

Date Sampled: 10/7/98Date Received: 10/7/98Matrix: SOIL

Lab Job No: H950

Date Extracted: 10/12/98Date Analyzed: 10/12/98QA Batch: 4638

EnvirotechSample #

88666

88677

TOTAL PETROLEUM HYDROCARBONS (418.1;

Client ID

SSSP-l_4-4.5

SSFS-2 0-0.5

Dilution Analytical Result% Moisture Factor mg/kg (Dry Wt.)

10.0

4.5

1.0

5.0

89.0

1490

I

II

II

D0

Quantitation Limit for Total Petroleum Hydrocarbons (418.1) is 25.0mg/kg for an undiluted sample.

II11

300844

Page 64: SDMS Document WHITMAN anies . ompanie

PHOJKCT NAfilKr K/orAnrr .« K/o

rtlOJECTNO: 95-OJ-02 <£V

MnOKATOKV: Ki iv / rn fe rh Kesrarrh, Inc.

C '] DO i4

SI I !•'. AI)l)Ul:SS: S l l cUIr A v r n l l f * Kim Slrf rl, H o c W u w «)' Uorouth, N.I

SAMPI .K DA IT.: fC l~1 / 'i 8

.SAMPI.KIl(S): Cheryl I,. Coffee / u. MJC=:•;f&.>^r

[SAMPLE'I TIME

RELINQUISHED

RELINQUISHED BY:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PIIC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS BY OC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH UIJRARY SEARCH

BN: DASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID l-.XTRACTAnl.l:.S WITH LIBRARY SEARCHTPM: PRIORITY POLLUTANT METALSPP«40 PRIORITY POLLUTANT PLUS TORTY PEAKS

K I C C E I V E I ) UV:

CT-Clill.lNtiTII.F.

1 T HM.OOUTIU:

LSI =7lli;HMALSYSTrM INSULATION

PRESER-VATIVE

NO. OFCONT.

2-z.

Z

Z-

SPECIALINSTRUCTIONS

7/

~73

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300845

Page 65: SDMS Document WHITMAN anies . ompanie

ws

K: Klotbnrr A Kr«Itatr

: 95-03-02 E/IV,<-C/«

I.ABORATOKV: Envlroltch Hcsrurch, Inf.

SI II . ADDKC.SS: Sllrl-lc A v r n u r A Clni S l t r r l , Untk lvoy Hotow th, NJ

.SAMI'I.K DAM'.:

SAMI'I.I-:H(.S): ci,rr,i i,.

SAMPLETIME

J.1 ,̂

: SAMPLE

i.sn c >

SAMPLE SAMPLKDEPTH

o- .£

tV-.<T

lo'

SAMPLE"MATKIX

Sel l

c vrn

lf(Q

i,. Cnrr^ I ̂

ANALYSISREQUESTED

Menus

RELINQUISHED UY: DATE:

n tit 'I IECEIVEO I1V:V

TIME: HECKIVEI) HV:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PHC: PCTKOLnUM HYDROCARBONS

VOC: VOLATILE OROANICS DY CC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARDONS IN DASK NEUTRAL SCAN WITH LIIIRAKY StAKCII

DN: BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID nXTRACTADI.l-S WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPPMO: PRIORITY POLLUTANT PLUS PORTY PEAKS

TT-CEILING TIL):

rr-ri.ooKTii.ii

T S I - T l m R M A I . SYSTEM INSULATION

PUESEil-VATIVE

t

\te

NO. OFCONT.

2.

^2-

z

2-

SPECIALINSTRUCTIONS

77-

9-8-6

r.3

DATE: \ (^ ' TIME I

DATE: TIME

TOTAL NO. CONTAINEHS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08316

300846 lir

Page 66: SDMS Document WHITMAN anies . ompanie

LABORSTOHVl C»lr*4r*h Krwirth. Inc

Mil MH'MISV «M

«• \Mri.K

[ T I M E LOCATION

SAMPLE

1D#SAMIM.E

DEI'TII

SAMI'LK

M A I U I X

.SAMI'I .KK(S): ( h r r y l l - C i ) f f r c

ANALYSIS

KKQUKSTKIJ

WCD

.RELINQUISHED BY:

RELINQUISHED BY:

DATE:

DATE:

ANALYTICAL PARAMETER IDENTIFICATION KEY:P1IC PETROLEUM HYDROCARBONS

VOC VOLATILE ORGANICS BY GC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARUONS IN BASE NEUTRAL SCAN WITH LIBRARY SI-ARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTAoLESVVmI LIBRARY SEARCHPPM PRIORITY POLLUTANT METALSPP*40: PRIORITY POLLUTANT PLUS PORTY PEAKS

K K C K I V K I , IIV:

RECEIVE!) I1Y:

C T - C E I L I N G TII.K

IT'-n.OORTII.r .

TSI - T H U R M A L S Y S r l l M INSULATION

DATE: TIME

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC

44 WEST FERRIS STREET

EAST BRUNSWICK, NJ 08816

300847

Page 67: SDMS Document WHITMAN anies . ompanie

1

ENVIROTECH RESEARCH, INC.

777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-iab.com

\LJ \

itman Companies, Inc.

October 29, 1998

II

II

II

II

II

00yiiiiniiiii

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Dr. Ira Whitman

Re: SDG No. H9411 - Klockner & Klockner (Inorganics)

Dear Dr. Whitman:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 07, 1998:

Lab No.

885488856488676

Client ID

FB-1SSDSA-1_0-0.5SSDSA-2 0-0.5

Analysis Required

CLPCNCLPCNCLPCN

An invoice for our services is also enclosed. If you have any questions pleasecontact your Project Manager, Robert McGrady, at (732) 549-3900.

Very trul>( yours,

Michael J. UrbanLaboratory Manager

300848

Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Is/and (132)

Page 68: SDMS Document WHITMAN anies . ompanie

11II

U.S. EPA - CLP

INORGANIC ANALYSES DATA SHEETEPA SAMPLE NO.

lab Name: ENVIROTECH_RESEARCH_INC.

Lab Code: 12543_ Case No.: _

jpatrix (soil/water): SOIL_

.ievel (low/med): LOW

•I Solids: 92.4

Contract:A-l 0-0.i5

SAS No.: SDG No.: H9411

Lab Sample ID: 88564

Date Received: 10/07/98

Concentration Units (ug/L or mg/kg dry weight): MG/KG

IIfl1IIIIII

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-659^5-70-0

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

0.54

C

U

Q M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRC

II1HII

olor Before:

Color After:

Clarity Before:

Clarity After:

Texture:

Artifacts

•Comments :SSDSA-1 0-0 .5

FORM I - IN ILM04.0300849

Page 69: SDMS Document WHITMAN anies . ompanie

U.S. EPA - CLP

INORGANIC ANALYSES DATA SHEETEPA SAMPLE NO.

llab Name: ENVIROTECH_RESEARCH_INC._

Lab Code: 12543_ Case No.: _

IJlatrix (soil/water) : SOIL_

ii.evel (low/med) : LOW

Contract:A-2 0-0.5

SAS No.: SDG NO.: H9411

Lab Sample ID: 88676

Date Received: 10/07/98

Solids: 85.2

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89^67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-65955-70-0

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concent rat ion

0.59

C

U

Q M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRC

[Color Before:

.Color After:

Clarity Before:

Clarity After:

'Comments:SSDSA-2 0-0.5

Texture:

Artifacts:

FORM I - IN ILM04.0300850

Page 70: SDMS Document WHITMAN anies . ompanie

0II

U.S. EPA - CLP

1INORGANIC ANALYSES DATA SHEET

ab Name: ENVIROTECH RESEARCH INC. Contract:

EPA SAMPLE NO.

FB-1

Lab Code: 12543_ Case No.:

Beatrix (soil/water) : WATER

Level (low/med): LOW

SAS No.: SDG No.: H9411

Lab Sample ID: 88548

Date Received: 10/07/98

Solids 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L_

D1IIII0

IIII10

olor Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-65955-70-0

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

10.0

C

U

Q M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRC

Clarity Before:

Clarity After:

Texture:

Artifacts

FORM I - IN300851

ILM04.0

Page 71: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klockncr & Klockner

rnojECTNO: 95-03-02LABORATORY: Envlrolech Research, Inc.

-tLSlli; ADDRESS: Stickle Avenue & Klin Street, Rockawny IlorouRb, NJ

SAMPLE DATE: (ftfb/Qfi

SAMPI.KR(S): Cheryl L. Coffee fi-

PAGE / OF

RELINQUISHEDBY:

ANALYTICAL PARAMETERJPENTIFICATION KEY:PHC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS BY GC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH UURARY SLARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCII

AE. ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLLTTA.ST METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT-CEILING TILC

FT- FLOOR TILE

TSI - Tl IURMAL SYSTEM INSULATION

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300852

Page 72: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klockntr & Klochncr

PROJECT NO: 95-03-02 ^nv^o-kc

LABORATORY: Envirolech Research, Inc.

SITE ADDRESS: Slicklc.Avcnuc & Elm Slrtcl, Rocknwny Borough, NJ

SAMPLE DATE: / 6> /6 / /£>I '

SAMPLKU(S): Cheryl L. Coffct / (, . IfJl^ST Cffff

PACE

ANALYTICAL PARAMETERJDENTIFICATION.KEY:PHC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS DY OC/MS WITH I.IDRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARHONS IN BASE NEUTRAL SCAN WITII LIBRARY SEARCII

BN: BASE NEUTRALS WITI I LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT-CEILIN(i Tll.l-

IT - I:LOOR TILE

TSI -THERMAI.SYSTEM INSULATION

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300853

Page 73: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klockner & Klockntr

PROJECTNO: 95-03-02 EvWi'tofcCh **•

LABORATORY: Envirolech Research, Inc.

SITE: ADDRESS: Slickk Avenue & Klin Street , llocltaway Borough, NJ

SAMPLE DATE:

PACE OF

SAMI'I.ER(S): Cheryl I. Coffee h

0)

ANALYTIQALPARAMETEFLIDENTIFI5ATIONKEY;.PHC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS DY COM3 WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SEARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT - CEILING TILK

FT - FLOOR TILIi

TSI - THERMAL SYSTEM INSULATION

TOTAL NO. CONTAINERS_

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300854

Page 74: SDMS Document WHITMAN anies . ompanie

I

ENVIROTECH RESEARCH, INC.

777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.com

Q

1rhe— ..—

PfF~]MMV/~?r~ — '

1 11998

lVhiJmflnCompn:-«:.>,

(!)i

November 3, 1998

i

tt

II

iu

oiuun

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Dr. Ira Whitman

Re: Job No. H941 - Klockner & Klockner

Dear Dr. Whitman:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 07, 1998:

Lab No.

88548

8854988550885518855288553885548855588556885578855888559885608856188562

88563

88564

Client ID

FB-1

SSGC-1J-4TB-1

SSAW-8_5.5-6SSAW-3_1-1.5

SSAW-3J 1.5-12SSWT-l_7-7.5SSAW-l_2.5-3

SSAW-1J3-13.5SSNDS-2J.5-2SSAN-8J1-11.5SSNDS-1AJ-1.5

SSFS-1_.5-1SSWT-2_7-7.5

SSNDS-1A_0-0.5

SSNDS-2A_0-0.5

SSDSA-1 0-0.5

Analysis Required

TCLBN+10,TAL Metals, PHC

TOCTCLVOA+10

Purgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable Halocarbons

TCLVOA+10Purgeable Halocarbons

TCLVOA+10TCLVOA+10

Purgeable HalocarbonsTCLBN+10,

TAL Metals, PHCTCLBN+10,

TAL Metals, PHCTAL Metals

300855

Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

Page 75: SDMS Document WHITMAN anies . ompanie

ENVIROTECH RESEARCH, INC.

1

I

1

il

II

i

ft

II

9

yiii

Lab No. Client ID Analysis Required

88565 SSFS-1_0-0.5 TCLBN+10,TAL Metals, PHC

88566 SSCB-l_2-2.5 TCL BN+10, TAL Metals88567 SSWT-l_7-7.5 TAJL Metals88568 SSDSA-l_1.5-2 Purgeable Halocarbons88569 SSAW-6_2-2.5 Purgeable Halocarbons88570 SSAW-6_9-9.5 Purgeable Halocarbons

An invoice for our services is also enclosed. If you have any questions pleasecontact your Project Manager, Robert McGrady, at (732) 549-3900.

Very truly yours,

Michael J. UrbanLaboratory Manager

300856

Page 76: SDMS Document WHITMAN anies . ompanie

Client ID: FB-1|J3ite: Klockner & Klockner

Lab Sample No: 88548Lab Job No: H941

-Date Sampled: 10/06/98[bate Received: 10/07/98^Date Extracted: 10/09/98Date Analyzed: 10/15/98JGC Column: DB-5|Instrument ID: BNAMS5.iLab File ID: q7549.d

Matrix: WATERLevel: LOWSample Volume: 930 mlExtract Final Volume: 2.0 mlDilution Factor: 1.0

I

1

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 827OC

Parameter

»bis(2-Chloroethyl)ether1,3-Dichlorobenzene1,4-Dichlorobenzene

I1,2-Dichlorobenzenebis(2 -chloroisopropyl)etherN-Nitroso-di-n-propylamineHexachloroethane

BNitrobenzeneIsophorone - -bis(2-Chloroethoxy)methane

Bl, 2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene

12-MethylnaphthaleneHexachlorocyclopentadiene2 -Chloronaphthalene

H2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene»3-NitroanilineAcenaphtheneDibenzofuran

__ 2,4-Dini trotolueneIIDiethylphthalate!• 4 -Chlorophenyl-phenyletherFluorene

H 4-NitroanilineN-Nitrosodiphenylamine4 -Bromophenyl-phenylether

nHexachlorobenzene•IPhenanthrene"• Anthracene

Analytical ResultUnits: ug/1

NDNDNDNDNDNDNDND

- NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

II

II

QuantitationLimit

Units: ug/1

1.1111111111.11.11.111111.111112.21111112211112.22211112.21111112211111.11111

300857

Page 77: SDMS Document WHITMAN anies . ompanie

1'Client ID: FB-1Site: Klockner & Klockner

Date Sampled: 10/06/98iDate Received: 10/07/98pate Extracted: 10/09/98'Date Analyzed: 10/15/98GC Column: DB-5•instrument ID: BNAMSS.i[Lab File ID: q7549.d

Lab Sample No: 88548Lab Job No: H941

Matrix: WATERLevel: LOWSample Volume: 930 mlExtract Final Volume: 2 . 0 mlDilution Factor: 1.0

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 827OC

| Parameter

B CarbazoleI Di-n-butylphthalate1 FluoranthenePyrene

I Butylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)anthraceneChrysene| bis(2 -Ethylhexyl)phthalateI Di-n-octylphthalateBenzo(b)fluoranthene

a Benzo(k)fluorantheneh Benzo(a)pyrene' Indeno(1,2,3 -cd)pyreneDibenz(a,h)anthracene|Benzo(g,h,i)perylene

Analytical ResultUnits: ug/1

NDNDNDNDNDNDNDNDND

• NDNDNDNDNDNDND

QuantitationLimit

Units: ug/1

1111111111221.11111111.11.11.11.11.111

II

II

1

ii

300858

Page 78: SDMS Document WHITMAN anies . ompanie

Client 3D: FB-1[site: Klockner & Klockner

Lab Sample No: 88548Lab Job No: H941

i

Date Sampled: 10/06/98Date Received: 10/07/98Date Extracted: 10/09/98Date Analyzed: 10/15/98GC Column: DB-5Instrument ID: BNAMS5.iLab File ID: q7549.d

Matrix: WATERLevel: LOWSample Volume: 930 mlExtract Final Volume: 2.0 mlDilution Factor: 1.0

1

SEMI-VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 827OC

1..

COMPOUND NAME

1. NO SEMI -VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26..27.28.29.30.

RT

1

EST. CONG.ug/1

Q

II1

TOTAL ESTIMATED CONCENTRATION

300859

0.0

Page 79: SDMS Document WHITMAN anies . ompanie

Client ID: TB-1jlfeite: Klockner & Klockner

.•Date Sampled: 10/06/98•bate Received: 10/07/98'•bate Analyzed: 10/18/98GC Column: DB624

tnstrument ID: VOAMS2 . iab File ID: b8532.d

Lab Sample No: 88550Lab Job No: H941

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 1.0

1VOLATILE ORGANICS - GC/MS

METHOD 8260

^Parameter

(ChloromethaneIBromomethaneInyl ChlorideChioroethane

HMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene

Bl,l-Dichloroethanetrans -1,2-Dichloroethenecis-1,2-Dichloroethene

BChloroform1,2 -Dichloroethane2-Butanone1,1,1-Trichloroethane«Carbon TetrachlorideBromodichloromethane1,2-Dichloropropane

0cis-1,3 -DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane

R Benzenetrans-1,3-DichloropropeneBromoform

B- 4 -Methyl - 2 - Pentanone2-HexanoneTetrachloroethene1,1,2,2-Tetrachloroethane

H TolueneChlorobenzeneEthylbenzene

nStyrenellXylene (Total)II

Analytical ResultUnits: ug/1

NDNDNDNDNDNDNDNDND

- NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

II

I

QuantitationLimit

Units: ug/1

5555355255552552115153154551155455

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

300860

Page 80: SDMS Document WHITMAN anies . ompanie

IClient ID: TB-1

fiSite: Klockner & KlocknerLab Sample No: 88550Lab Job No: H941

I

1

ate Sampled: 10/06/98Date Received: 10/07/98'Date Analyzed: 10/18/98GC Column: DB624Instrument ID: VOAMS2.i•Lab File ID: b8532.d

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 1.0

VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 826OB

11I111

1iiii

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

TOTAL ESTIMATED CONCENTRATION

EST. CONC.ug/1

0.0

Q

300861

I

Page 81: SDMS Document WHITMAN anies . ompanie

Client ID: SSNDS-2_1.5-2[Site: Klockner & Klockner

.Date Sampled: 10/06/98pate Received: 10/07/98'Date Analyzed: 10/15/98GC Column: DB624

[Instrument ID: VOAMS5.iLab File ID: e4656.d

Lab Sample No: 88557Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 11.0 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 8

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg(Dry Weight)

ChioromethaneII Bromomethane»Vinyl ChlorideChioroethane

B Methylene ChlorideAcetone

- Carbon Bisulfide1,1-Dichloroethene« 1,1-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-Dichloroethene

I" Chloroform1,2 -Dichloroethane2-Butanone1,1,1-Trichloroethane« Carbon TetrachlorideBromodichloromethane1,2-Dichloropropane

H cis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane

Benzenetrans-1,3-DichloropropeneBromoform

._ 4-Methyl-2-PentanoneII 2-Hexanone"̂ Tetrachloroethene

1,1,2,2-Tetrachloroethane

TolueneChlorobenzeneEthylbenzene

_- StyreneII Xylene (Total)

NDNDNDNDNDNDNDNDND

• ND93 JNDNDNDNDNDNDNDND

6200NDNDNDNDNDNDND

130NDNDNDNDNDND

QuantitationLimit

Units: ug/kg

620620620620370620620250620620620620250620620250120120620120620370120620490620620120120620620490620620

300862

Page 82: SDMS Document WHITMAN anies . ompanie

1iI1II1

Client ID: SSNDS-2_1.5-2Site: Klockner & Klockner

Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/15/98GC Column: DB624Instrument ID: VOAMS5.iLab File ID: e4656.d

Lab Sample No: 88557Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 11.0 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 7.7

VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 826OB

II111IIIIIIuIIII1II0n

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3 .4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

TOTAL ESTIMATED CONCENTRATION

30C

EST. CONC.ug/kg

0.0

863

Q

Page 83: SDMS Document WHITMAN anies . ompanie

Client ID: SSNDS-1A_1-1.5[site: Klockner & Klockner

Lab Sample No: 88559Lab Job No: H941

I Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/20/98GC Column: DB624

I Instrument ID: VOAMSl.iI Lab File ID: a6473.d

Matrix: SOILLevel: HIGHSample Weight: 11.2 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 500.0% Moisture: 15

]p Parameter

._ ChloromethaneII Bromomethane«• Vinyl ChlorideChloroethane

O Methylene ChlorideAcetone

"' Carbon Disulfide1,1-Dichloroethene

Jl 1,1-Dichloroethane

II

0

II

0IIu0II

trans -1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1,3-DichloropropeneBromoform4-Methyl- 2 -Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

" ND1300 J

NDNDNDNDNDNDNDND

90000NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

6500650065006500390065006500260065006500650065002600650065002600130013006500130065003900130065005200650065001300130065006500520065006500

300864

Page 84: SDMS Document WHITMAN anies . ompanie

Client ID: SSNDS-1A_1-1.5Ifeite: Klockner & Klockner

Lab Sample No: 88559Lab Job No: H941

(jpate Sampled: 10/06/98•bate Received: 10/07/98|Bbate Analyzed: 10/20/98GC Column: DB624

tnst rumen t ID: VOAMSl.iab File ID: a6473.d

Matrix: SOILLevel: HIGHSample Weight: 11.2 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 500.0% Moisture: 14.6

IVOLATILE ORGANICS - GC/MS

TENTATIVELY IDENTIFIED COMPOUNDSMETHOD 826OB

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16 .17.18.19.20.21.22.23.24.25.26.27.2 8 .29.30.

RT EST. CONC.ug/kg

Q

.— — - .

I

1I

I

I TOTAL ESTIMATED CONCENTRATION

300865

0.0

Page 85: SDMS Document WHITMAN anies . ompanie

Client ID: SSFS-1_.5-1Isite: Klockner & Klockner

Lab Sample No: 88560Lab Job No: H941

(Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/16/98GC Column: DB624

I Instrument ID: VOAMS5.iLab File ID: e4675.d

Matrix: SOILLevel: HIGHSample Weight: 10.7 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 100.0% Moisture: 8

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 826OB

Analytical ResultsUnits: ug/kg(Dry Weight)

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,l-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1,3-DichloropropeneBromoform4-Methyl-2 -Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

NDNDNDNDNDNDNDNDND

•• ND1200 J

NDNDNDNDNDNDNDND

23000NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

13001300130013007601300130051013001300130013005101300130051025025013002501300760250130010001300130025025013001300100013001300

300866

Page 86: SDMS Document WHITMAN anies . ompanie

1I1Client ID: SSFS-1_.5-1Site: Klockner & Klockner

iDate Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/16/98GC Column: DB624(instrument ID: VOAMS5.1(Lab File ID: e4675.d

Lab Sample No: 88560Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 10.7 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 100.0% Moisture: 8.1

IVOLATILE ORGANICS - GC/MS

TENTATIVELY IDENTIFIED COMPOUNDSMETHOD 826OB

ill111

in

COMPOUND NAME

1. Unknown Siloxane2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

15.87

EST. CONC.ug/kg

2400

Q

TOTAL ESTIMATED CONCENTRATION

300867

2400

I

Page 87: SDMS Document WHITMAN anies . ompanie

Client ID: SSNDS-1A_0-0 . 5iSite: Klockner & Klockner

Lab Sample No: 88562Lab Job No: H941

(Date Sampled: 10/06/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/20/98JGC Column: DB-5[Instrument ID: BNAMS2.iLab File ID: s8301.d

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11

Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 827OC

Analytical ResultsUnits: ug/kg(Dry Weight)

I bis(2-Chloroethyl)ether1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzenebis(2-chloroisopropyl)etherN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophoronebis(2-Chloroethoxy)methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene2-MethylnaphthaleneHexachlorocyclopentadiene2 -Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphtheneDibenzofuran2,4-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyletherFluorene4-NitroanilineN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzenePhenanthreneAnthracene

NDNDNDNDNDNDNDND

" NDNDNDNDNDNDNDNDNDNDND

23 JNDNDNDNDNDNDNDNDNDNDNDND

130 J18 J

QuantitationLimit

Units: uq/kg

373703703703703737373703703737037075

370370370750370370757503703707537037037075037037037370370

300868

Page 88: SDMS Document WHITMAN anies . ompanie

«I1'Client ID: SSNDS-1A_0-0 . 5Site: Klockner & Klockner

II

Date Sampled: 10/06/98pate Received: 10/07/98bate Extracted: 10/15/98bate Analyzed: 10/20/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8301.d

Lab Sample No: 88562Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11

[Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 8270C

Analytical ResultsUnits: ug/kg(Dry Weight)

Carbazole|oi-n-butylphthalateJFluoranthenePyrene

IButylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)anthraceneChrysene

Ibis(2-Ethylhexyl)phthalateDi-n-octylphthalateBenzo(b)fluoranthene

IBenzo(k)fluorantheneBenzo(a)pyreneIndeno(1,2,3-cd)pyreneDibenz(a,h)anthracene| Benzo(g,h,i)perylene

11 JND

220 J240 J

NDND

97150 J

ND" ND180921104614 J36 J

QuantitationLimit

Units: ug/kg

370370370370370750373703703703737373737370

1

II

I

a300869

Page 89: SDMS Document WHITMAN anies . ompanie

I1Client ID: SSNDS- 1A_0- 0 . 5ISite: Klockner & Klockner

Date Sampled: 10/06/98ate Received: 10/07/98ate Extracted: 10/15/98Date Analyzed: 10/20/98GC Column: DB-5[Instrument ID: BNAMS2 . iLab File ID: s8301.d

Lab Sample No: 88562Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11.1

i SEMI-VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 827OC

COMPOUND NAME

1. NO SEMI -VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT EST. CONC.ug/kg

Q

""

1II0II

IIIIIIII00 TOTAL ESTIMATED CONCENTRATION

300870

0.0

Page 90: SDMS Document WHITMAN anies . ompanie

Ii

I

I

I

Client ID: SSNDS-2A_0-0.5Site: Klockner & Klockner

iDate Sampled: 10/06/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/20/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8302.d

Lab Sample No: 88563Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11

1Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 827OC

Analytical ResultsUnits: ug/kg(Dry Weight)

0111II

bis(2-Chloroethyl)ether1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzenebis(2-chloroisopropyl)etherN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophoronebis(2 -Chloroethoxy)methane1,2,4-TrichlorobenzeneNaphthalene4 -ChloroanilineHexachlorobutadiene2-MethylnaphthaleneHexachlorocyclopentadiene2 -Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthy1ene2,6-Dinitrotoluene3-NitroanilineAcenaphtheneDibenzofuran2,4-DinitrotolueneDiethylphthalate4 -Chlorophenyl-phenyletherFluorene4-NitroanilineN-Nitrosodiphenylamine4-Bromophenyl-phenyletherHexachlorobenzenePhenanthreneAnthracene

NDNDNDNDNDNDNDND

• NDNDNDNDNDNDNDNDNDNDND

18 JNDNDNDNDNDNDNDNDNDNDNDND

43 J16 J

QuantitationLimit

Units: ug/kg

38380380380380383838

38038038

38038075

3803803807503803807575038038075

38038038075038038038

380380

300871

II

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"Client ID: SSNDS-2A_0-0.5Site: Klockner & Klockner

Date Sampled: 10/06/98(•Date Received: 10/07/98•pate Extracted: 10/15/98'"Date Analyzed: 10/20/98GC Column: DB-5

(•instrument ID: BNAMS2 . iliLab File ID: s8302.d

Lab Sample No: 88563Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11

[[Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 8270C

Analytical ResultsUnits: ug/kg(Dry Weight)

1

1

H1

CarbazoleJDi - n - butylphthalat eFluoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)anthraceneChrysenebis(2-Ethylhexyl)phthalate:Di-n-octylphthalateBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(a)pyreneIndeno(1,2,3-cd)pyreneDibenz(a,h)anthraceneBenzo(g,h,i)perylene

NDND

140 J170 J

NDND

100110 J23 J

" ND1606694341127

JJJ

QuantitationLimit

Units: ug/kg

38038038038038075038

3803803803838383838380

1IIIIi

300872

Page 92: SDMS Document WHITMAN anies . ompanie

1

IClient ID: SSNDS-2A_0-0 . 5Site: Klockner & Klockner

1

I

I

Date Sampled: 10/06/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/20/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8302.d

Lab Sample No: 88563Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11.2

SEMI-VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 8270C

COMPOUND NAME

1 . Unknown2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

9.64

EST. CONC.ug/kg

6800

Q

0

II

0000IIII

TOTAL ESTIMATED CONCENTRATION

300873

6800

Page 93: SDMS Document WHITMAN anies . ompanie

Client ID: SSFS-1_0-0.5Isite: Klockner & Klockner

Lab Sample No: 88565Lab Job No: H941

ijDate Sampled: 10/06/98pate Received: 10/07/98"Date Extracted: 10/15/98Date Analyzed: 10/21/98

SGC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8315.d

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11

Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 8270C

Analytical ResultsUnits: ug/kg(Dry Weight)

I

1

1

I

1

bis(2-Chloroethyl)ether1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzenebis(2 -chloroisopropyl)etherN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophoronebis(2-Chloroethoxy)methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene2-MethylnaphthaleneHexachlorocyclopentadiene2 -Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphtheneDibenzofuran2,4-DinitrotolueneDiethylphthalate4 -Chlorophenyl-phenyletherFluorene4-NitroanilineN-Ni t ros odiphenylamine4-Bromophenyl-phenyletherHexachlorobenzenePhenanthreneAnthracene

NDNDNDNDNDNDNDND

" NDNDNDNDNDNDNDNDNDNDND

48 JNDND8.1JNDNDNDND

14 JNDNDNDND

130 J47 J

QuantitationLimit

Units: ug/kg

373703703703703737373703703737037075370370370750370370757503703707537037037075037037037370370

300874

Page 94: SDMS Document WHITMAN anies . ompanie

II11IIIIIIIII0IIIIIaiiiiiiiiin

Client ID: SSFS-1_0-0.5Site: Klockner & Klockner

Date Sampled: 10/06/98Date Received: 10/07/98Date Extracted: 10/15/98Date Analyzed: 10/21/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s8315.d

Lab Sample No: 88565Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 11

Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 827OC

Analytical ResultsUnits: ug/kg(Dry Weight)

CarbazoleDi-n-butylphthalateFluoranthenePyreneButylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)anthraceneChrysenebis(2 -Ethylhexyl)phthalateDi-n-octylphthalateBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(a)pyreneIndeno(1,2,3 -cd)pyreneDibenz(a,h)anthraceneBenzo(g,h,i)perylene

12 JND

290 J360 J1000

ND170220 J260 J- ND2701201807425 J59 J

QuantitationLimit

Units: ug/kg

370370370370370750373703703703737373737370

300875

Page 95: SDMS Document WHITMAN anies . ompanie

IIClient ID: SSFS-1_0-0.5Ifeite: Klockner & Klockner

Lab Sample No: 88565Lab Job No: H941

•Date Sampled: 10/06/98[bate Received: 10/07/98TDate Extracted: 10/15/98Date Analyzed: 10/21/98IteC Column: DB-5[(instrument ID: BNAMS2 . iLab File ID: s83l5.d

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 10.8

SEMI-VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 827OCIIIIII1

1II

II11

COMPOUND NAME

1.2.3.4.5.6.7.8.9.10.11.

Tricresylphosphate isomerTricresylphosphate isomerUnknownUnknownC20H12 PAH/UnknownUnknownUnknownUnknownUnknownUnknown

12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

25.3225.5325.5825.8027.4627.6728'. 1229.0429.5530.68

EST. CONC.ug/kg

320620300540630560110052023001800

Q

II1

TOTAL ESTIMATED CONCENTRATION

300876

8690

Page 96: SDMS Document WHITMAN anies . ompanie

Client ID: SSCB-l_2-2.5BSite: Klockner & Klockner

Lab Sample No: 88566Lab Job No: H941

Date Sampled: 10/06/98pate Received: 10/07/98•Date Extracted: 10/14/98Date Analyzed: 10/21/98IGC Column: DB-5[Instrument ID: BNAMS2.iLab File ID: s8316.d

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 12

Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 8270C

Analytical ResultsUnits: ug/kg(Dry Weight)

II

1

II

II

II

DI0II

bis(2-Chloroethyl)ether1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzenebis(2-chloroisopropyl)etherN-Nitroso-di-n-propylamineHexachloroethaneNitrobenzeneIsophoronebis(2-Chloroethoxy)methane1,2,4-TrichlorobenzeneNaphthalene4-ChloroanilineHexachlorobutadiene2-MethylnaphthaleneHexachlorocyclopentadiene2 -Chloronaphthalene2-NitroanilineDimethylphthalateAcenaphthylene2,6-Dinitrotoluene3-NitroanilineAcenaphtheneDibenzofuran2,4-DinitrotolueneDiethylphthalate4 -Chlorophenyl-phenyletherFluorene4-NitroanilineN-Nitrosodiphenylamine4 -Bromophenyl-phenyletherHexachlorobenzenePhenanthreneAnthracene

NDNDNDNDNDNDNDNDNDNDND9.3JNDND

12 JNDNDNDND

24 JNDNDND9.6JNDNDNDNDNDNDNDND

86 J15 J

QuantitationLimit

Units: ug/kg

3838038038038038383838038038380380763803803807603803807676038038076

38038038076038038038380380

300877

Page 97: SDMS Document WHITMAN anies . ompanie

"Client ID: SSCB-l_2-2.5Site: Klockner & Klockner

Lab Sample No: 88566Lab Job No: H941

Date Sampled: 10/06/98

VDate Received: 10/07/98Date Extracted: 10/14/98Date Analyzed: 10/21/98GC Column: DB-5

1Instrument ID: BNAMS2.iLab File ID: s8316.d

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 12

[Parameter

SEMI-VOLATILE ORGANICS - GC/MSMETHOD 827OC

Analytical ResultsUnits: ug/kg(Dry Weight)

CarbazolejDi-n-butylphthalateiFluoranthenePyrene

I Butylbenzylphthalate3,3'-DichlorobenzidineBenzo(a)anthraceneChryseneIbis(2-Ethylhexyl)phthalatemi-n-octylphthalateBenzo(b)fluoranthene

I Benzo(k)fluorantheneBenzo(a)pyreneIndeno(1,2,3 -cd)pyreneDibenz(a,h)anthraceneIBenzo(g,h,i)perylene

9.0JND

130 J140 J80 JND

5583 J85 J

- ND110507140ND

39 J

QuantitationLimit

Units: ug/kg

380380380380380760383803803803838383838380

II

HIIIIIII0

300878

Page 98: SDMS Document WHITMAN anies . ompanie

111Client ID: SSCB-l_2-2.5Site: Klockner & Klockner

1

Date Sampled: 10/06/98Date Received: 10/07/98Date Extracted: 10/14/98Date Analyzed: 10/21/98GC Column: DB-5Instrument ID: BNAMS2.iLab File ID: s83l6.d

Lab Sample No: 88566Lab Job No: H941

Matrix: SOILLevel: LOWSample Weight: 30.0 gExtract Final Volume: 2.0 mlDilution Factor: 1.0% Moisture: 12.1

SEMI-VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 8270C

COMPOUND NAME

1 . Unknown2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT

30.63

EST. CONG,ug/kg

310

Q1II

I1

1TOTAL ESTIMATED CONCENTRATION

300879

310

Page 99: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-8_5.5-6HSite: Klockner & Klockner

Lab Sample No: 88551Lab Job No: H941

[Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/16/98GC Column: DB624finstrument ID: VOAGC1.iI Lab File ID: geld9515.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 10.1

[Parameter

inDichlorodifluoromethane•ChloromethaneVinyl ChlorideBromomethane

IChloroethaneTrichlorofluoromethane1,1-Dichloroethene

,-jMethylene ChlorideIII trans-1, 2-Dichloroethene•I 1,1-Dichloroethanecis-1,2-Dichloroethene

IChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-Dichloroethane

II TrichloroetheneB1,2-DichloropropaneBromodiChloromethane

H 2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzene

D Bromof orm1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene

II 1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

1 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

II

QuantitationLimit

Units: ug/kg

139139139139139139139139139139139139139139139139139139139139139139139139139139139139139139

300880

0

Page 100: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-3_1-1.5ISite: Klockner & Klockner

Lab Sample No: 88552Lab Job No: H941

Date Sampled: 10/06/98Date Received: 10/07/98bate Analyzed: 10/16/98GC Column: DB624

[Instrument ID: VOAGC1.iLab File ID: geld9516.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 16.6

25.0 ml1000.0

I Parameter

Dichlorodifluoromethane

I ChioromethaneVinyl ChlorideB r omome thane

I ChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloride

I trans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-Trichloroethane'Carbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2 -DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

> ND10800

32300

NDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

294029402940294029402940294029402940294029402940294029402940294029402940294029402940294029402940294029402940294029402940

300881

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I

1

Client ID: SSAW-3_11.5-12Site: Klockner & Klockner

Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/16/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9517.d

Lab Sample No: 88553Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 3.0

25.0 ml50.0

1Parameter

Dichlorodifluoromethane

IChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloride

Itrans -1,2-Dichloroethene1,1-Dichloroethanecis-1,2-Dichloroethene

. Chloroform•1,1,1-TrichloroethaneIII Carbon Tetrachloride1,2-Dichloroethane

|H TrichloroethenelU 1, 2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ether

HI cis-1,3-Dichloropropene111 trans-1, 3-Dichloropropene1,1,2-Trichloroethane

ITetrachloroetheneDibromochloromethaneChlorobenzeneBromoform

1 1,1,2,2- Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

131131131131131131131131131131131131131131131131131131131131131131131131131131131131131131

300882

Page 102: SDMS Document WHITMAN anies . ompanie

Client ID: SSWT-l_7-7 . 5Site: Klockner & Klockner

Lab Sample No: 88554Lab Job No: H941

Date Sampled: 10/06/98[Date Received: 10/07/98(Date Analyzed: 10/17/98GC Column: DB624

I Instrument ID: VOAGCl.iI Lab File ID: geld9518.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 10.1

25.0 ml50.0

I Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloride

t trans -1,2-DichloroetheneI 1,1-Dichloroethanecis-l,2-DichloroetheneChloroform

1 1,1,1-TrichloroethaneCarbon Tetrachloride1,2-Dichloroethane

!

Trichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ether

!cis-l,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-Trichloroethane

I TetrachloroetheneDibromochloromethaneChlorobenzeneBromoform

1 1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

, NDNDNDNDNDND

237NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: uQ/kg

134134134134134134134134134134134134134134134134134134134134134134134134134134134134134134

nii

300883

Page 103: SDMS Document WHITMAN anies . ompanie

1

IIIIII11IIIIIIIIIIIIIIIIIIIIII

Client ID: SSAW-l_2.5-3Site: Klockner & Klockner

Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/17/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9519.d

Lab Sample No: 88555Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 4.0

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

- ND351

2470

NDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

130130130130130130130130130130130130130130130130130130130130130130130130130130130130130130

300884

Page 104: SDMS Document WHITMAN anies . ompanie

I

I

Client ID: SSAW-1_13-13.5Site: Klockner & Klockner

Date Sampled: 10/06/98Date Received: 10/07/98Date Analyzed: 10/17/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9520.d

Lab Sample No: 88556Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 6.5

25.0 ml50.0

II

I

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethane . ..cis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDND

143

1330

NDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

130130130130130130130130130130130130130130130130130130130130130130130130130130130130130130

1

I

300885

Page 105: SDMS Document WHITMAN anies . ompanie

I

1Client ID: SSAN-8_11-11.5Site: Klockner & Klockner

•Date Sampled: 10/06/98pate Received: 10/07/98'Date Analyzed: 10/17/98GC Column: DB624[Instrument ID: VOAGC1.iLab File ID: geld9521.d

Lab Sample No: 88558Lab Job No: H941

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 13.8

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethane

I Vinyl ChlorideBromomethaneiChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloride'trans-1,2-Dichloroethene'1,1-Dichloroethanecis-1,2-Dichloroethene

i Chloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodi chlorome thane2-Chloroethyl Vinyl Ethercis-l,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

136136136136136136136136136136136136136136136136136136136136136136136136136136136136136136

0II

300886

Page 106: SDMS Document WHITMAN anies . ompanie

Client ID: SSWT-2_7-7.5ISite: Klockner & Klockner

Lab Sample No: 88561Lab Job No: H941

Date Sampled: 10/06/98bate Received: 10/07/98bate Analyzed: 10/17/98GC Column: DB624|Instrument ID: VOAGC1.iLab File ID: geld9522.d

1 Parameter

Dichlorodifluoromethane1ChloromethaneIVinyl ChlorideBromomethane

I ChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloride

I trans-1,2-Dichloroethene\ 1,1-Dichloroethanecis-1,2-Dichloroethene

I Chloroform1,1,1-Trichloroethane'Carbon Tetrachloride1,2-DichloroethaneITrichloroethene[1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropene'trans-1,3-Dichloropropene1,1,2-Trichloroethane

'. Tetrachloroethene|DibromochloromethaneChlorobenzeneBromoforml,1,2,2-Tetrachloroethane'1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 5.0

25.0 ml50.0

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

• NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

132132132132132132132132132132132132132132132132132132132132132132132132132132132132132132

300887

Page 107: SDMS Document WHITMAN anies . ompanie

Client ID: SSDSA-1_1.5-2ItSite: Klockner & Klockner

Lab Sample No: 88568Lab Job No: H941

_Date Sampled: 10/06/98pate Received: 10/07/98Ifeate Analyzed: 10/17/98GC Column: DB624

[Instrument ID: VOAGC1.iLab File ID: geld9523.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 6.9

25.0 ml50.0

•Parameter

Dichlorodifluoromethane

IGhloromethaneVinyl ChlorideBromomethane

VChioroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloride

Itrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-Dichloroethene

Chloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-Dichloroethane

III Trichloroethene|H 1,2-DichloropropaneBromodichloromethane

,g,2-Chloroethyl Vinyl EtherHI cis-1,3-Dichloropropene™trans-1,3-Dichloropropene1,1,2-Trichloroethane

H TetrachloroetheneDibromochloromethaneChlorobenzene

mBromoform•1,1,2,2-Tetrachloroethane™l,3-Dichlorobenzene1,4-Dichlorobenzene

in 1, 2 -Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDND

-• NDNDNDNDNDND

4560NDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

132132132132132132132132132132132132132132132132132132132132132132132132132132132132132132

300888

Page 108: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-6_2-2.5[Site: Klockner & Klockner

Lab Sample No: 88569Lab Job No: H941

Date Sampled: 10/06/98[Date Received: 10/07/98(Date Analyzed: 10/17/98GC Column: DB624[Instrument ID: VOAGCl.iLab File ID: geld9524.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 17.3

25 .0 ml2 5 0 0 . 0

I

1

1

1

II

II

1

II

II

II

II

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTr ichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDND

16400

65900

23700

NDNDNDND

NDNDNDNDNDND

NDNDNDNDNDNDND

300889

QuantitationLimit

Units: ug/kg

734073407340734073407340734073407340734073407340734073407340734073407340734073407340734073407340734073407340734073407340

Page 109: SDMS Document WHITMAN anies . ompanie

Client ID: SSAW-6_9-9.5iSite: Klockner & Klockner

Lab Sample No: 88570Lab Job No: H941

Date Sampled: 10/06/98|Date Received: 10/07/98bate Analyzed: 10/19/98GC Column: DB624

[Instrument ID: VOAGC1.iLab File ID: geld9561.d

jl ParameterIV

Dichlorodifluoromethane

B ChioromethaneVinyl ChlorideBromomethane

._ Chloroethanejl Trichlorofluoromethane'• 1,1-DichloroetheneMethylene Chloride

Itrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-Dichloroethene

._ Chloroform•1,1,1-TrichloroethaneI" Carbon Tetrachloride1,2-Dichloroethane

BTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1, 3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-Trichloroethane

ITetrachloroetheneDibromochloromethaneChlorobenzeneBromoform

111 1,1,2,2- TetrachloroethaneIP 1,3-Dichlorobenzene

1,4-Dichlorobenzene1,2-Dichlorobenzene

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 17.4

25.0 ml50.0

1

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

147147147147147147147147147147147147147147147147147147147147147147147147147147147147147147

300890

Page 110: SDMS Document WHITMAN anies . ompanie

1II11I1111

Client ID: FB-1Site: Klockner & Klockner

Date Sampled: 10/06/98Date Received: 10/07/98

Lab Sample No: 88548Lab Job No: H941

Matrix: WATERLevel: LOW

1

1

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

METALS ANALYSIS

AnalyticalResult

Units: ug/1

NDNDNDNDNDND2811.8

NDNDNDNDND3.0

NDND328NDNDNDNDND17.4

InstrumentDetection

Limit Qual

58.24.6 N3 .81.40.200.40

42.2 B1.0 BN1.23 .5

41.52.5 *

40.31.1 BN0.102.1

300 B4.81.4

4264.81.94.5 B

M

PPPPPPPPPPPPPPCVPPPPPPPP

I

I

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300891

Page 111: SDMS Document WHITMAN anies . ompanie

I

Client ID: SSNDS-1A 0-0.5Site: Klockner & Klockner

Lab Sample No: 88562Lab Job No: H941

Date Sampled:Date Received:

1

1

1

1

I

1

10/06/9810/07/98

Matrix: SOLIDLevel: LOW% Moisture: 11.1

1111IIII

Analvte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

METALS ANALYSIS

AnalyticalResult

Units: mg/kg(Dry Weight)

11200ND7.2

1520.63

ND525022.97.569.9

3130034319503970.6515.3719NDNDNDND35.2

273

InstrumentDetection

Limit Qual

13100009000909000

6710

95101

.1

.0

.85

.31

.045

.090

.5

.22

.27

.79

.3

.56

. 1

.25

.019

.47

.6

.1

.31

.8

.1

.43

.0

N

.

NB

*

N

B

M

PPPPPPPPPPPPPPCVPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300892

II

Page 112: SDMS Document WHITMAN anies . ompanie

IIII111

Client ID: SSNDS-2A 0-0.5Site: Klockner & Klockner

Date Sampled:Date Received:

10/06/9810/07/98

Lab Sample No: 88563Lab Job No: H941

Matrix: SOLIDLevel: LOW% Moisture: 11.2

METALS ANALYSIS

II

1

II

II

1

1

1

II

Analyte

AnalyticalResult

Units: mg/kg(Dry Weight)

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

83701.03.480.60.430.15

118014.07.1

25.518200

75.717002160.1011.1

399NDNDNDND24.3195

InstrumentDetection

Limit Qual M

13100009000909000

6710

95101

.1

.0

.86

.32

.045

.090

.5

.23

.27

.79

.3

.56

. 1

.25

.019

.47

.6

.1

.32

.9

.1

.43

.0

BN

• BB

NB

*

N

B

PPPPPPPPPPPPPPCVPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

1

1

300893

Page 113: SDMS Document WHITMAN anies . ompanie

IIIII Client ID: SSDSA-1 0-0.5

Site: Klockner & KlocknerLab Sample No: 88564Lab Job No: H941

Date Sampled:Date Received:

10/06/9810/07/98

1

Matrix: SOLIDLevel: LOW% Moisture: 7.6

METALS ANALYSIS

I

II

0II

0II

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

AnalyticalResult

Units: mg/kg(Dry Weight)

106001.45.0

2220.560.76

358045.69.8

1052160034424404190.3934.8

1070ND0.40

NDND35.2408

InstrumentDetection

Limit Qual

121000,09000908000

6510

92100

.6

.00

.82

.30

.043

.087

.1

.22

.26

.76

.0

.54

.7

.24

.018

.45

.0

.0

.30

.2

.0

.41

.97

BN

B

NB

*

N

B

B

M

PPPPPPPPPP.PPPPCVPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

0 300894

Page 114: SDMS Document WHITMAN anies . ompanie

IIII1

Client ID: SSFS-1 0-0.5Site: Klockner & Klockner

Date Sampled:Date Received:

10/06/9810/07/98

Lab Sample No: 88565Lab Job No: H941

Matrix: SOLIDLevel: LOW% Moisture: 10.8

1 METALS ANALYSIS

1

1

1

I

1

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

AnalyticalResult

Units: mg/kg(Dry Weight)

7590ND3.7

2520.430.78

966032.18.2

215195004712610298

0.3518.8979ND0.72

NDND32.4371

InstrumentDetectionLimit Qual

13.01.00.850.310 . 0 4 50 . 0 9 09.50 . 2 20 . 2 70 .789.30.569 .00 .250.0190 .47

67.31.10.31

95.51.10.431.0

N

,BB

NB

*

N

B

B

M

PPPPPPPPPPPPPPCVPPPPPPPP

1

1

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300895

Page 115: SDMS Document WHITMAN anies . ompanie

IIIIIIIIIIIIII0II

Client ID: SSCB-1 2-2.5Site: Klockner & Klockner

Date Sampled:Date Received:

10/06/9810/07/98

Lab Sample No: 88566Lab Job No: H941

Matrix: SOLIDLevel: LOW% Moisture: 12.1

IIIID

100

Analyte

AluminumAnt imonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

METALS ANALYSIS

AnalyticalResult

Units: mg/kg(Dry Weight)

8660ND2.673.90.630.33

332026.48.3

36.919200104

3150259

0.0514.9

1110NDND147ND53 .8131

InstrumentDetectionLimit Qual

13100009000909000

6810

96101

.2

.0

.86

.32

. 046

.091

.6

.23

.27

.80

.4

.57

.2

.25

.019

.48

.3

.1

.32

.9

.1

.43

.0

N

B

NB

*

N

B

B

M

PPPPPPPPPPPPPPCVPPPPPPPP

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report)M Column - Method Code (See Section 2 of Report)

300896

Page 116: SDMS Document WHITMAN anies . ompanie

Client ID: SSWT-1 7-7.5Site: Klockner & Klockner

Lab Sample No: 88567Lab Job No: H941

1 Date Sampled:Date Received:

10/06/9810/07/98

Matrix: SOLIDLevel: LOW% Moisture: 3.9

METALS ANALYSIS

I

1

P

Analyte

AnalyticalResult

Units: mg/kg(Dry Weight)

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

4910ND3.20.0.

ND622

8.4.13.

1650010.

162084 .0.8.

326NDNDNDND14.63.

2046

718

1

5086

76

InstrumentDetection

Limit Qual M

12000008000808000

6210

88100

.1

.96

.79

.29

. 042

.083

.8

.21

.25

.73

.6

.52

.4

.23

.017

.44

.5

.00

.29

.7

.00

.40

.94

N

B

BNB

*

N

B

PPPPPPPPPPPPPPCVPPPPPPPP

1

I

Qual Column - Data Reporting Qualifiers (See Sec 2 of Report!M Column - Method Code (See Section 2 of Report)

300897

Page 117: SDMS Document WHITMAN anies . ompanie

1I-, Site: Klockner & Klockner Lab Job No: H941

™ Date Sampled: 10/6/98Date Received: 10/7/98 Date Analyzed: 10/14/98

|| Matrix: SOIL QA Batch: 1402

I

II

I

II

II

II

II

II

0II

TOTAL ORGANIC CARBON

1._ Envirotech Dilution Analytical Result]l Sample tt Client ID % Moisture Factor mg/kg (Dry Wt.)

88549 SSGC-1 1-4 8.3 2.0 8720

Quantitation Limit for Total Organic Carbon is 100 mg/kg for anundiluted sample.

II

300898

Page 118: SDMS Document WHITMAN anies . ompanie

I1

Site: Klockner & Klockner

Date Sampled: 10/6/98Date Received: 10/7/98Matrix: WATER

Lab Job No: H941

Date Extracted: 10/12/98Date Analyzed: 10/12/98QA Batch: 4639

II

II

0

TOTAL PETROLEUM HYDROCARBONS (418.1)

I

II

EnvirotechSample #

88548

Client ID

FB-1

Dilution Analytical ResultFactor Units: mg/1

1.0 ND

Quantitation Limit for Total Petroleum Hydrocarbons (418.1) is 1.0 mg/1for an undiluted sample.

0IIIIII

300899

Page 119: SDMS Document WHITMAN anies . ompanie

1

I Site: Klockner & Klockner

Date Sampled: 10/6/98Date Received: 10/7/98Matrix: SOIL

Lab Job No: H941

Date Extracted: 10/12/98Date Analyzed: 10/12/98QA Batch: 4645

1

I

II

I

II

II

II

EnvirotechSample #

TOTAL PETROLEUM HYDROCARBONS (418.1;

Dilution Analytical ResultClient ID % Moisture Factor mg/kg (Dry Wt.)

88562 SSNDS-1A 0-0.5

88563 SSNDS-2A 0-0.5

88565 SSFS-1 0-0.5

11.1

11.2

10.8

1.0

1.0

1.0

374

225

823

Quantitation Limit for Total Petroleum Hydrocarbons (418.1) is 25.0mg/kg for an undiluted sample.

II

II

II

1

300900

Page 120: SDMS Document WHITMAN anies . ompanie

Ul

I-ROJKCTNO, 90-01-01

/-/iBOfMTOKV: Envlrolrrh Hcscnrch, /nr.

-fcL f O 9 ^>f •» "

MI r.,

SAMIM.K DATE:

SAMPI.r.H(S): Cheryl I,. Coffee

ANALYTICAL PARAMETER IDENTIFICATION KEY:PHC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS BY OC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SEARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPPMO: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT - CEILING TILE

FT" FLOOR TILE

TSI -THERMAL SYSTEM INSULATION

No. OKCONT.

•4

1.

;u•vi-^

SI'MC'IAL

i INSTRUCTIONS

S6550

6&SS3

_ ....... DATE:

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300901

Page 121: SDMS Document WHITMAN anies . ompanie

.CT HAMK: Ktorknrr A Kforltnrr Nil K ADDKKSS: Mlrhlt.Avtnlit A Klin Strtrt, Hotk«««y HnrouRh, N.I

LADOKATORV: Envlrolrch Research, Inc.

SAMPI.K DATE: /f6?/L> / / £ >

SAMI'I.KK(S): Cheryl L. Coffee /

DAT

ANALYTICAL PARAMETER IDENTIFICATIOHKEY:PHC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS DY OC/MS W1TII LIBRARY SEARCII

PAH: POLYCYCLIC AROMATIC HYDROCARDONS IN BASE NEUTRAL SCAN WITH LIBRARY SEARCH

BN: DASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCH

PPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS PORTY PEAKS

TE: ^///f 5 TIME: 6T^ UECKIVEI) »V:

PA™.:.(9/7/96 JJME/)A£D

IT-l:LOOIl III.I;

TSI -TIIEUMAI. SYSTEM INSULATION

TOTAL NO. CONTAINERS_

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300902

Jj-

Page 122: SDMS Document WHITMAN anies . ompanie

ENVIROTECH RESEARCH, INC.

Ill New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.com

1

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Mr. Michael Metlitz

November 2, 1998

\The

E ( 8 - E 0 W E

r'; I T I998 1Whitman Companies. Inc.

Re: Job No. 1052 - Klockner & Klockner

1

6

Dear Mr. Metlitz:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 09, 1998:

Lab No.

89299893008930189302893038930489305

Client ID

TB-3SSOSS-1J-1.5SSCP-1_3.5_4

SSGC-1AJ.5-4SSCP-1J1-11.5SSFD-l_1.5-2SSCP-4 1-1.5

Analysis Required

Purgeable HalocarbonsPurgeable HalocarbonsPurgeable Halocarbons

TOCPurgeable HalocarbonsPurgeable HalocarbonsPurgeable Halocarbons

If you have any questions please contact your Project Manager, Robert McGrady,at (732) 549-3900.

DII

1II

Very trulyxyours,

Michael J. UrbanLaboratory Manager

300903

Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

Page 123: SDMS Document WHITMAN anies . ompanie

Client ID: TB-3Site: Klockner & Klockner

Lab Sample No: 89299Lab Job No: 1052

1

1

1

1

I

V

1ii

iiiiii

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9587.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 0.0

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1.2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

125125125125125125125125125125125125125125125125125125125125125125125125125125125125125125

300904

Page 124: SDMS Document WHITMAN anies . ompanie

IllClient ID: SSOSS-1_1-1.5Site: Klockner & Klockner

Lab Sample No: 89300Lab Job No: 1052

1

1

1

I

II

HIIIIII0HIIflIIII

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/21/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9609.d

Matrix: SOILLevel: HIGHSample Weight: 9 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 8.7

25.0 ml100.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDND

7250NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

294294294294294294294294294294294294294294294294294294294294294294294294294294294294294294

300905

Page 125: SDMS Document WHITMAN anies . ompanie

Client ID: SSCP-1_3.5_4Site: Klockner & Klockner

Lab Sample No: 89301Lab Job No: 1052

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/16/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9508.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 4.3

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideB romome t haneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1, l-Dichloroethane . ..cis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGAN1CS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

133133133133133133133133133133133133133133133133133133133133133133133133133133133133133133

I

1

II

300906

Page 126: SDMS Document WHITMAN anies . ompanie

Client ID: SSCP-1JL1-11.5Site: Klockner & Klockner

Lab Sample No: 89303Lab Job No: 1052

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/16/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9509.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume: 25.0 mlExt. Dilution Factor: 50.0% Moisture: 7.1

1

9

II

II

II

II

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChioroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,l-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenet rans-1,3 -Di chloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

142142142142142142142142142142142142142142142142142142142142142142142142142142142142142142

300907

HII

Page 127: SDMS Document WHITMAN anies . ompanie

1Client ID: SSFD-l_1.5-2Site: Klockner & Klockner

Lab Sample No: 89304Lab Job No: 1052

Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/20/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9589.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 6.2

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChioroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

137137137137137137137137137137137137137137137137137137137137137137137137137137137137137137

300908

I

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IIIClient ID: SSCP-4_1-1.5

Site: Klockner & Klockner

I- Date Sampled: 10/08/98Date Received: 10/09/98Date Analyzed: 10/20/98GC Column: DB624

Instrument ID: VOAGC1.iLab File ID: geld9590.d

Lab Sample No: 89305Lab Job No: 1052

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 3.7

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

130130130130130130130130130130130130130130130130130130130130130130130130130130130130130130

300909

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II0•g Site: Klockner & Klockner Lab Job No: 1052

'• Date Sampled: 10/8/98Date Received: 10/9/98 Date Analyzed: 10/14/98Matrix: SOIL QA Batch: 1402

1

1

I!II

TOTAL ORGANIC CARBON

I

1_ Envirotech Dilution Analytical ResultII Sample # Client ID % Moisture Factor mg/kg (Dry Wt. )

89302 SSGC-lA_1.5-4 13.7 4.0 16200

I

1* Quantitation Limit for Total Organic Carbon is 100 mg/kg for anundiluted sample.

ft

300910

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PROJECT NAME!: Kloekner & Kloekntr

PROJECTNO: 95-03-02 r?i\vinjfec

LABORATORY: Envlrolech Rest»rch, Inc.

AMPU^

SITE ADDRESS: Stick!* Avtsut & Elm Strut, RcxW.w.y Borough, NJ

SAMPLE DATE: (o/$|42>

SAMPLER(S): Cheryl L. Coffee / L -

PAGE

^SAMPLE . SAMPLEDEPTH

SAMPLEMATRIX

~n>a>1

• ANALYSIS k

REQUESTED

PRESER-VATIVE

NO.:OFcocnv.

\

s , SPECIAL.. t "/or"1 1NSTRUCTIONS '• '' r<

ssoss-.r •l-l.-S" Prt/ ,

C-I/V

SScP- \ \ 2-

SSf-D-

-l.-S'

( SSCP-I 1' Sc.'l

I3ao SSCP-3 15-3'

Nr

RELINQUISHED

RELINQIVISHED BY: DATF/e - R E C E I V E D BY:

TIMF

ANALYTICAL PARAMETER IDENTIFICATION KEY:PHC PETROLEUM HYDROCARBONS

VOC VOLATILE ORGANICS BY GC.MS WITH LIBRARY SEARCH

PAH POLYCYCLIC AROMATIC HYDROCARBOsS IN BASE NEUTRAL SCAN WITH LIBR *RY SEARCH

BN BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTABLES WITH LIBRARY SEARCHPPM PRIORITY POLLUTANT METALS

-W PRIORITY POLLUTANT PLUS FORTY PEAKS

DATE: .fc/2/2! TIME J^\O_

ftCT • CEILING TILK

FT • FLOOR TILE

TSI • THERMAL SYSTEM INSL'LATION

TOTAL NO. CONTAINERS,

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300911

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1

I

ENVIROTECH RESEARCH, INC.

777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.com

November 06, 1998

1

II

inii

nnii

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Mr. Michael Metlitz

H\ fS fi°nL^ ^UJfi\Uu Nnv

E

i

The Whitman

0

T

^7

(998

E QM - ! 'i ' ;! '

I1'"'Companies, l.'v.-

Re: Job No. 1279 - Klockner & Klockner

Dear Mr. Metlitz:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 16, 1998:

Lab No.

908219082290823908249082590826908279082890829908309083190832908339083490835

Client ID

SSFA-1J.5-2SSFA-6AJ.5-2SSFA-1J0.5-11SSFA-2_0.5-1SSFA-3_0.5-1SSFA-4_0.5-1SSFA-5_3-3.5SSPP-l_6.5-7SSFD-2_3-4

SSDW-l_1.5-2SSSD-l_5-5.5SSDA-l_1.5-2Trip_Blank-4Field_Blank-3SSGC-4 2-4

Analysis Required

Purgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable HalocarbonsPurgeable Halocarbons

TOC

II

II

300912

Laboratory'Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

Page 132: SDMS Document WHITMAN anies . ompanie

II„ ENVIROTECH RESEARCH, INC.

II

ilIIII0

IB Lab No. Client ID Analysis Required

90836 SSGC-3_4.5-5 TOCII 90837 SSGC-2J-4 TOC

If you have any questions please contact your Project Manager, Robert McGrady,|| at (732) 549-3900.

|l Very trulyx yours,

™ Michael J. Urban- Laboratory Manager

I

II

300913

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1i1

1II

11II

Client ID: SSFA-l_1.5-2Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/22/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9629.d

Lab Sample No: 90821Lab Job No: 1279

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 9.9

25.0 ml50.0

Parameter

DichlorodifluoromethaneChio rome t haneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,l-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

1510NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

128128128128128128128128128128128128128128128128128128128128128128128128128128128128128128

300914

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IIfl Client ID: SSFA-6A_1.5-2

Site: Klockner & KlocknerLab Sample No: 90822Lab Job No: 1279

1

II

1

II

1

1

fl

n

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/22/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9634.d

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,l-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 8.6

25.0 ml50.0

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

3720NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

134134134134134134134134134134134134134134134134134134134134134134134134134134134134134134

ni0

300915

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11

I1

II

11

I1

Client ID: SSFA-1_10.5-11Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/22/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9635.d

Lab Sample No: 90823Lab Job No: 1279

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 5.0

25.0 ml50.0

II

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideBromomethaneChioroe thaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-l,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3 -Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: uq/kq

123123123123123123123123123123123123123123123123123123123123123123123123123123123123123123

I

1

300916

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III Client ID: SSFA-2_0.5-1

Site: Klockner & KlocknerLab Sample No: 90824Lab Job No: 1279

1

I

I

I

I

I

nii

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/22/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9636.d

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 8.3

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

161NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

124124124124124124124124124124124124124124124124124124124124124124124124124124124124124124

300917

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1II1II

II

IIDIIII!

IIeii

Client ID: SSFA-3_0.5-1Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9646.d

Lab Sample No: 90825Lab Job No: 1279

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 4.1

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideB romome t haneChloroethaneTrichlorofluoromethane1,l-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,l-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichicroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-l,3-Dichloropropenetrans -1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoforml,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

1100NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

137137137137137137137137137137137137137137137137137137137137137137137137137137137137137137

300918

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IIII

Client ID: SSFA-4_0.5-1Site: Klockner & Klockner

Lab Sample No: 90826Lab Job No: 1279

I

1

I

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGCl.iLab File ID: geld9647.d

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 3.2

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

4280NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

129129129129129129129129129129129129129129129129129129129129129129129129129129129129129129

II

0 300919

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IIII

Client ID: SSFA-5_3-3.5Site: Klockner & Klockner

Lab Sample No: 90827Lab Job No: 1279

II

0I

11giiD1IIII1i1

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9648.d

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 13.9

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,l-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-l,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 8021B

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: uq/kq

127127127127127127127127127127127127127127127127127127127127127127127127127127127127127127

300920

I!

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Client ID: SSPP-l_6.5-7Site: Klockner & Klockner

Lab Sample No: 90828Lab Job No: 1279

I

1

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGCl.iLab File ID: geld9649.d

I

1

1

II

I

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 11.2

25.0 ml50.0

DII

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,l-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

123123123123123123123123123123123123123123123123123123123123123123123123123123123123123123

0c

300921

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IClient ID: SSFD-2_3-4Site: Klockner & Klockner

Lab Sample No: 90829Lab Job No: 1279

I

1

1

niiinoB

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9650.d

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,l-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,l-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,, 1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 14.6

25.0 ml50.0

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

266NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

139139139139139139139139139139139139139139139139139139139139139139139139139139139139139139

300922

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HII

Client ID: SSDW-1_1.5-2Site: Klockner & Klockner

Lab Sample No: 90830Lab Job No: 1279

1

1

II

1

II

II

Deo

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGCl.iLab File ID: geld9651.d

Parameter

DichlorodifluoromethaneChi ororne thaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,l-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1.2-Dichlorobenzene

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 12.5

25.0 ml50.0

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

1040NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

128128128128128128128128128128128128128128128128128128128128128128128128128128128128128128

300923

H

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1

1

II

1

II

II

0

IIIIIII

Client ID: SSSD-l_5-5.5Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9652.d

Lab Sample No: 90831Lab Job No: 1279

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 4.7

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans -1,2-Dichloroethene1,1-Dichloroethanecis-l,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-l,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

125125125125125125125125125125125125125125125125125125125125125125125125125125125125125125

IIII

300924

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III1

I1

«1

1

1

Client ID: SSDA-l_1.5-2Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/23/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9653.d

Lab Sample No: 90832Lab Job No: 1279

Matrix: SOILLevel: HIGHSample Weight: 11 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 15.5

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropenel,.l, 2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1 ,.1, 2 , 2 -Tetrachloroethane1 ,,3 - Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

154NDNDNDNDNDNDND

QuantitationLimit

Units: ug/kq

132132132132132132132132132132132132132132132132132132132132132132132132132132132132132132

1300925

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1

I

1

Client ID: Trip_Blank-4Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/24/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9661.d

1

1

1

1

1

I

I

Lab Sample No: 90833Lab Job No: 1279

Matrix: SOILLevel: HIGHSample Weight: 10 gMethanol Ext. Volume:Ext. Dilution Factor:% Moisture: 0.0

25.0 ml50.0

Parameter

DichlorodifluoromethaneChioromethaneVinyl ChlorideBromome thaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultsUnits: ug/kg(Dry Weight)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/kg

125125125125125125125125125125125125125125125125125125125125125125125125125125125125125125

300926

1

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IIClient ID: Field_Blank-3Site: Klockner & Klockner

Lab Sample No: 90834Lab Job No: 1279

II

II

II

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/24/98GC Column: DB624Instrument ID: VOAGC1.iLab File ID: geld9662.d

0

IIIIII

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlFinal Volume: 0.0 mLDilution Factor: 1.0

Parameter

DichlorodifluoromethaneChloromethaneVinyl ChlorideB romomethaneChloroethaneTrichlorofluoromethane1,1-DichloroetheneMethylene Chloridetrans-1,2-Dichloroethene1,1-Dichloroethanecis-1,2-DichloroetheneChloroform1,1,1-TrichloroethaneCarbon Tetrachloride1,2-DichloroethaneTrichloroethene1,2-DichloropropaneBromodichloromethane2-Chloroethyl Vinyl Ethercis-1,3-Dichloropropenetrans-1,3-Dichloropropene1,1,2-TrichloroethaneTetrachloroetheneDibromochloromethaneChlorobenzeneBromoform1,1,2,2-Tetrachloroethane1,3-Dichlorobenzene1,4-Dichlorobenzene1,2-Dichlorobenzene

VOLATILE ORGANICS - GC/ELCDMETHOD 802IB

Analytical ResultUnits: ug/1

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

QuantitationLimit

Units: ug/'l

111111111111111111111111111111

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

.0

IIIIII

300927

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11

II0ggiiiiii

iio

iio

Site: Klockner & Klockner Lab Job No: 1279

Date Sampled: 10/16/98Date Received: 10/16/98 Date Analyzed: 10/20/98Matrix: SOIL QA Batch: 1404

TOTAL ORGANIC CARBON

Envirotech Dilution Analytical ResultSample # Client ID % Moisture Factor mg/kg (Dry Wt. )

90835 SSGC-4A 2-4

90836 SSGC-3A_4 .5-5.5

90837 SSGC-2A 3-4

9.5

7.1

14 .6

1.0

1.0

2.5

10400

429

1960

Quantitation Limit for Total Organic Carbon is 100 mg/kg for anundiluted sample.

300928

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PROJECT NAME: Klurknrr A Klockncr

PROJECT NO: 95-03-02

LABORATORY: Envirotccli Project #809002

SITE ADDRESS: Slkkle Avrnur & Klin Slrccl, Kui-knwiiy Hiiruugh, N.I

SAMPLE DATE: / 0//£> /£ S^

SAMPLKU(S): Cheryl L. Coffi-c

ANALYSISREQUESTED

RELINQUISHED BY:i

RELINQUISHED BY:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PIIC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS BY GC/MS WITH LIBRARY SEARCH

PAH POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SI-ARCH

UN: BASE NEUTRALS WITH LIBRARY SEARCH

AE. ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

SO 82.\

^052-7

IME: \V ' -> '~> RECEIVED »Y:

r iME: R E C E I V E D BY:

CT-ClilUNGTII.i;

IT-= I-'I.OORTILE

I SI "THERMAL SYSTEM INSULATION

PRESER-VATIVE

NO. OFCONT.

M&t+\ 2.ti\ 2-

-2-.(to.

I'MiK. \ OV

SPECIAL

INSTRUCTIONS

DATE:' / ~

DATE: TIME

TOTAL NO. CONTAINERS

E /75":5

WHITMAN COMPANIES INC44 WESTFERRIS STREETEAST BRUNSWICK, NJ 08816

300929

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Ni

PROJECT NAME: Klorknrr & Klockner

PROJECT NO: 95-03-02

LABORATORY: Envirolcch Project #809002

SITE ADDUKSS: SlieUle A v e n u e & Klin Street , Uocknwi iy Hoi-ouch, N.I

SAMPLE DATE: /b///*/^*?

SAMI'LER(S): Cheryl L. Coffee

\»AGK.

| SAMPLE

TIME

SAMPLE SAMPLE

DEPTH

SAMPLE

MATRIX

ANALYSIS

REQUESTED

1/

i R E L I N Q U I S I I E D B Y :i

[ R E L I N Q U I S H E D BY:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PMC: PETROLEUM MYDROCARHONS

VOC: VOLATILE ORGANICS BY OC/MS WITH LIBRARY SI-ARCH

PAH: POLYCYCLIC AROMATIC HYDROCARHONS IN HASI: NliUTRAI. SCAN WITH LIIIKAKY SI-IARfll

DM: DASE NEUTRALS WITH LIBRARY SEARCH

TIME:

R E C E I V E D BY:

R E C E I V E D BY:

CT - CT.U.tNCi Tll.l-

IT" I LOOK TIL I-

AE:PPM:

ACID KXTRACTABLES WITH LIBRARY SEARCHPRIORITY POLLUTANT METALS

P+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

I P R E S E R -

! VATIVE

NO. OF

CONT.

SPECIAL

INSTRUCTIONS

DATE: T I M E

TOTAL NO. C. 'ONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300930

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IIII

1

ENVIROTECH RESEARCH, INC.

777 New Durham RoadEdison, New Jersey 08817Tel: (732) 549-3900Fax: (732) 549-3679www.enviro-lab.com

November 2, 1998

1

1

1

II

ninniDDiB

The Whitman Companies, Inc.44 West Ferris StreetEast Brunswick, NJ 08816

Attention: Mr. Michael Metlitz

Re: Job No. 1280 - Klockner & Klockner

Dear Mr. Metlitz:

Enclosed are the results you requested for the following sample(s) received at ourlaboratory on October 16, 1998:

Lab No.

90838

90839

90840

Client ID

DSSR-1

DSRW-1

Trip_Blank

Analysis Required

TCLVOA+10,PCBs,TAL Metals, Ignitability, Reactivity,

CorrosivityTCLVOA+10, PCBs,

TAL Metals, Ignitability, Reactivity,Corrosivity

TCLVOA+10

If you have any questions please contact your Project Manager, Robert McGrady,at (732) 549-3900.

Very trulyi yours,

Michael J. Urban-Laboratory Manager

IF n w i? nlr

JLJi

P i300931

Laboratory Certifications: New Jersey (12543) New York (11452) PeThe Whitman Companies, Inc.

icut (PH-0200) Rhode Island (132)

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0

H

II

nn

i

ioHnn

Analytical Methodology Summary

Volatile Organics:

n Unless otherwise specified, water samples are analyzed for volatile•I organics by purge and trap GC/MS as specified in EPA Method 624. Drinking

water samples are analyzed by EPA Method 524.2. Solid samples are analyzedfor volatile organics as specified in the EPA publication "Test Methods forEvaluating Solid Waste" (SW-846, 3rd Edition) Method 8260B. Water samples areanalyzed for volatile organics by purge and trap GC/PID and GC/ELCD asspecified in EPA Methods 601 and 602. Solid samples are analyzed by GC/PID andGC/ELCD in accordance with SW-846, 3rd Edition Method 8021B.

Acid and Base/Neutral Extractable Organics:

Unless otherwise specified, water samples are analyzed for acid and/orbase/neutral extractable organics by GC/MS in accordance with EPA Method 625.Solids are analyzed for acid and/or base/neutral extractable organics asspecified in the EPA publication "Test Methods for Evaluating Solid Waste"(SW-846, 3rd Edition) Method 8270C.

GC/MS Nontarget Compound Analysis:

Analysis for nontarget compounds is conducted, upon request, inconjunction with GC/MS analyses by EPA Methods 624, 625, 8260B and 8270C.Nontarget compound analysis is conducted using a forward library search of theEPA/NIH/NBS mass spectral library of compounds at the greatest apparentconcentration (10% or greater of the nearest internal standard) in eachorganic fraction (15 for volatile, 15 for base/neutrals and 10 for acidextractables). '

Organochlorine Pesticides and PCBs:

Unless otherwise specified, water samples are analyzed fororganochlorine pesticides and PCBs by dual column gas chromatography withelectron capture detectors as specified in EPA Method 608. Solid samples areanalyzed as specified in the EPA publication "Test Methods for EvaluatingSolid Waste" (SW-846, 3rd Edition) Method 8081A for organochlorine pesticidesand Method 8082 for PCBs.

Total Petroleum Hydrocarbons:

Water samples are analyzed for petroleum hydrocarbons by I.R. using EPAMethod 418.1. Solid samples are prepared for analysis by soxhlet extractionconsistent with the March 1990 N.J. DEP "Remedial Investigation Guide"Appendix A, page 52, and analyzed by U.S. EPA Method 418.1

300932

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Metals Analysis:

1

II

II

0IIII1II10II

IIII

Metals analyses are performed by any of four techniques specified by aMethod Code provided on each data report page, as follows:

P - Inductively Coupled Plasma Atomic EmissionSpectroscopy (ICP)

A - Flame Atomic Absorption

F - Furnace Atomic Absorption

CV - Manual Cold Vapor (Mercury)

Water samples are digested and analyzed using EPA methods provided in "Methodsfor Chemical Analysis of Water and Wastewater" (EPA 600/4-79-020). Solidsamples are analyzed as specified in the EPA publication "Test Methods forEvaluating Solid Waste" (SW-846, 3rd Edition); samples are digested accordingto Method 3050B "Acid Digestion of Soil, Sediments and Sludges."

Specific method references for ICP analyses are water Method 200.7 andsolid Method 6010B. Mercury analyses are conducted by the manual cold vaportechnique specified by water Method 245.1 and solid Method 7471A. Otherspecific Atomic Absorption method references are as follows:

ElementAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium, TotalChromium, (+6)CobaltCopperIronLeadMagnesiumManganeseNickelPotassiumSeleniumSilverSodiumTinThalliumVanadiumZinc

Cyanide:

Water samples are analyzed for cyanide using EPA Method 335.3. Cyanideis determined in solid samples as specified in the EPA Contract LaboratoryProgram IFB dated July 1988, revised February 1989.

300933

WaterFlame202.1204.1

--208.1210.1213.1215.1218.1218.4219.1220.1236.1239.1242.1243.1249.1258.1

—272.1273.1283.1279.1286.1289.1

Test MethodFurnace202 .22 0 4 . 2206 .2

—210.2213.2

—218.2218.5219.2220.2236.2239.2

—2 4 3 . 22 4 9 . 2

--270.2272 .2

—283.2279.2286 .2289 .2

SolidFlame70207040

--70807090713071407190719772007210738074207450746075207610--

776077707870784079107950

Test MethodFurnace--

70417060—70917131—719171957201--—

7421—

——--7740------78417911--

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1

IIIIit

iiifI!

II0

Phenols:

Water samples are analyzed for total phenols using EPA Method 420.2.Total phenols are determined in solid samples by preparing the sample asoutlined in the EPA Contract Laboratory Program IFB for cyanide, followed by aphenols determination using EPA Method 420.1.

Cleanup of Semivolatile Extracts:

Upon request Method 3611B Alumina Column Cleanup and/or Method 3650BAcid-Base Partition Cleanup are performed to improve detection limits by theremoval of saturated hydrocarbon interferences.

Hazardous Waste Characteristics:

Samples for hazardous waste characteristics are analyzed as specified inthe U.S. EPA publication "Test Methods for Evaluating Solid Waste" (SW-846,3rd Edition). Specific method references are as follows:

Ignitability - Method 1020A

Corrosivity - Water pH Method 9040BSoil pH Method 9045C

Reactivity - Chapter 7, Section 7.3.3 and 7.3.4respectively for hydrogen cyanide andhydrogen sulfide release

Toxicity - TCLP Method 1311

Miscellaneous Parameters:

Additional analyses performed on both aqueous and solid samples are inaccordance with methods published in the following references:

- Test Methods for Evaluating Solid Wastes, SW-846 3rd Edition,November 1986.

- Standard Methods for the Examination of Water and Wastewater,17th Edition.

- Methods for Chemical Analysis of Water and Wastes,EPA-600/4-79-020, 1979.

300934

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Ifi1

viiiI

1Ili

ORGANIC DATA REPORTING QUALIFIERSND - The compound was not detected at the indicated

concentration.

J - Mass spectral data indicates the presence of a compoundthat meets the identification criteria. The result is lessthan the specified quantitation limit but greater than zero.The concentration given is an approximate value.

B - The analyte was found in the laboratory blank as well as thesample. This indicates possible laboratory contamination ofthe environmental sample.

P - For dual column analysis, the percent differencebetween the quantitated concentrations on the twocolumns is greater than 40%.

* - For dual column analysis, the lowest quantitatedconcentration is being reported due to coelutinginterference.INORGANIC DATA REPORTING QUALIFIERS (SW-846 METHODS ONLY)

ND - The compound was not detected at the indicatedconcentration.

B - Reported value is less than the Method Detection Limit butgreater than or equal to the Instrument Detection Limit.

E - The reported value is estimated because of the presence ofinterference. See explanatory note in the NonconformanceSummary if the problem applies to all of the samples or onthe individual Inorganic Analysis Data Sheet if the problemis isolated.

M - Duplicate injection precision not met on the Furnace AtomicAbsorption analysis.

N - The spiked sample recovery is not within control limits.

S - The reported value was determined by the Method of StandardAdditions (MSA).

* - Duplicate Analysis is not within control limits.

W - Post digestion spike for Furnace Atomic Absorption analysisis out of control.

+ - Correlation coefficient for MSA is less than 0.995.

M Column - Method Qualifiers

P - Inductively Coupled Plasma Atomic Emission Spectroscopy

(ICP).

A - Flame Atomic Absorption Spectroscopy (FAA).

F - Graphite Furnace Atomic Absorption Spectroscopy (GFAA).

CV - Cold Vapor Atomic Absorption Spectroscopy. 300935

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Client ID: DSSR-1Site: Klockner & Klockner

Lab Sample No: 90838Lab Job No: 1280

Date Sampled: 10/16/98i Date Received: 10/16/98I Date Analyzed: 10/27/98VGC Column: DB624Instrument ID: VOAMSV.i

I Lab File ID: v5872.d

Matrix: WATERLevel: LOWPurge Volume: 5.Dilution Factor:

0 ml5.0

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 624

Analytical ResultUnits: ug/1

Chioromethane

n BromomethaneVinyl ChlorideChloroethaneMethylene Chloride

fjj AcetoneII Carbon Disulf ide

l, l-Dichloroethene

8 1,1-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-DichloroetheneChloroform

V I,2-Dichloroethane•2-Butanone' 1,1,l-Trichloroethane- Carbon Tetrachloride

]fj BromodichloromethaneI" 1,2-Dichloropropane

cis-1,3-Dichloropropene

H TrichloroetheneDibromochloromethane1,1,2-Trichloroethane

\̂ BenzeneII trans-1,3-Dichloropropene•I Bromof orm

4-Methyl-2 -Pentanone

H 2-HexanoneTetrachloroethene

- 1,1,2,2-TetrachloroethaneToluene

II Chlorobenzene11 Ethylbenzene

StyreneXylene (Total)

II

II

46

NDNDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

Method DetectionLimit

Units: ug/1

4.61.42.05.25.2

255.02.81.61.55.01.01.1

251.00.80.92.31.62.01.22.21.21.61.5

25250.51.60.90.71.25.05.0

300936

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II1II1III111

Client ID: DSSR-1Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/27/98GC Column: DB624Instrument ID: VOAMSV.iLab File ID: v5872.d

Lab Sample No: 90838Lab Job No: 1280

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 624

Matrix: WATERLevel: LOWPurge Volume: 5.Dilution Factor:

• GC/MSCOMPOUNDS

0 ml5.0

COMPOUND NAME

1 . NO VOLATILE ORGANIC COMPOUNDS FOUND2 .3 .4 .5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT EST. CONC.ug/1

Q

II

IIIIII

TOTAL ESTIMATED CONCENTRATION

300937

0.0

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IIVii

Client ID: DSRW-1Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98(Date Analyzed: 10/24/98GC Column: DB624Instrument ID: VOAMSV.iLab File ID: v5769.d

Lab Sample No: 90839Lab Job No: 1280

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 10.0

iVOLATILE ORGANICS - GC/MS

METHOD 624

Parameter

ChioromethaneBromomethaneVinyl ChlorideChioroethaneMethylene ChlorideAcetoneCarbon Disulfidel,1-Dichloroethene1,l-Dichloroethanetrans-1,2-Dichloroethenecis-1,2-DichloroetheneChloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenetrans-1,3-DichloropropeneBromoform4-Methyl- 2 -Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyreneXylene (Total)

Analytical ResultUnits: ug/1

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

Method DetectionLimit

Units: uq/1

923

10105010

533

1022

5021143424233

505013112

1010

.3

.7

.9

.5

.1

.0

.0

.2

.0

.6

.9

.6

. 3

.1

.3

.3

.4

.1

.0

.0

.3

.8

.4

.4

300938

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III

Client ID: DSRW-1Site: Klockner & Klockner

Lab Sample No: 90839Lab Job No: 1280

II

anHIIi

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/24/98GC Column: DB624Instrument ID: VOAMSV.iLab File ID: v5769.d

Matrix: WATERLevel: LOWPurge Volume: 5.Dilution Factor:

0 ml10.0

VOLATILE ORGANICS - GC/MSTENTATIVELY IDENTIFIED COMPOUNDS

METHOD 624

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

RT EST. CONG.ug/1

Q

31IIIIIIIIiitii

TOTAL ESTIMATED CONCENTRATION

300939

0.0

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i1I

Client ID: Trip_BlankSite: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/24/98GC Column: DB624Instrument ID: VOAMS7.iLab File ID: v5770.d

Lab Sample No: 90840Lab Job No: 1280

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 1.0

Parameter

VOLATILE ORGANICS - GC/MSMETHOD 624

Analytical ResultUnits: uq/1

Chloromethane« Bromome thaneVinyl Chloride

- Chloroethane_.N Methylene ChlorideM Acetonejp Carbon Disulfide

1,1-Dichloroethene

§ 1,1-Dichloroethanetrans-1,2-Dichloroethenecis-l,2-Dichloroethene.Chloroformi1,2-Dichloroethane2-Butanone1,1,l-Trichloroethane«• Carbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane

_ BenzeneII trans-1,3-Dichloropropene™ Bromoform

4-Methyl- 2 -Pentanone

1 2-HexanoneTetrachloroethene1,1,2,2-Tetrachloroethane

8TolueneChlorobenzeneEthylbenzeneStyrene

|j Xylene (Total)

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

0

A

Method DetectionLimit

Units: ug/1

000115100AVJ

100500000000000550000011

.9

.3

.4

.0

.0

.0

.0

.6

.3

.3

.0

.2

.2

.0

.2

.2

.2

.5

.3

.4

.2

.4

.2

.3

.3

.0

.0

.1

.3

.2

.1

.2

.0

.0

300940

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0IfII

IIIIIIa

Client ID: Trip_BlankSite: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Analyzed: 10/24/98GC Column: DB624Instrument ID: VOAMS7.iLab File ID: v5770.d

VOLATILE ORGANICSTENTATIVELY IDENTIFIED

METHOD 624

Lab Sample No: 90840Lab Job No: 1280

Matrix: WATERLevel: LOWPurge Volume: 5.0 mlDilution Factor: 1.0

• GC/MSCOMPOUNDS

COMPOUND NAME

1. NO VOLATILE ORGANIC COMPOUNDS FOUND2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22 .23.24.25.26.27.28.29.30.

RT EST. CONC.ug/1

Q

IIlliiiii

TOTAL ESTIMATED CONCENTRATION

300941

0.0

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II1

Client ID: DSSR-1Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Date Extract-.ed: 10/21/98Date Analyzed: 10/27/98GC Column: DB-608Instrument ID: PESTGC6.i

Lab Sample ID: 90838Lab Job No: 1280

Matrix: WATERSample Volume: 990 mlExtract Final Volume:Dilution Factor: 1.0Lab File ID: nr004375.d

5.0 ml

ORGANOCHLORINE PCBs - GC/ECDMETHOD 608

1

I

I

1

f

Parameter

Aroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260Aroclor-1262Aroclor-1268

Analytical ResultsUnits: ug/1

NDNDNDNDNDNDNDNDND

Method DetectionLimit

Units: ug/1

0.300.300.400.200.300.400.200.200.20

II

II

II

300942

Page 162: SDMS Document WHITMAN anies . ompanie

IIIIII1I1irii

Client ID: DSRW-1Site: Klockner & Klockner

Date Sampled: 10/16/98'•Date Received: 10/16/98Date Extracted: 10/21/98Date Analyzed: 10/27/98GC Column: DB-608Instrument ID: PESTGC6.i

Lab Sample ID: 90839Lab Job No: 1280

Matrix: WATERSample Volume: 920 mlExtract Final Volume:Dilution Factor: 1.0Lab File ID: nr004398.d

5.0 ml

Parameter

Aroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260Aroclor-1262Aroclor-1268

ORGANOCHLORINE PCBs - GC/ECDMETHOD 608

Analytical ResultsUnits: ug/1

NDNDNDNDNDNDNDNDND

Method DetectionLimit

Units: ug/1

0 .300 . 3 00 .400.200 .300 .400.200.200.20

II

1

ft

I

1

II

II 300943

Page 163: SDMS Document WHITMAN anies . ompanie

IIIIIIIIuIIIT

0(In11iiiiiii

Client ID: DSSR-1Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98

Lab Sample No: 90838Lab Job No: 1280

Matrix: WATERLevel: LOW

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

METALS ANALYSIS

AnalyticalResult

Units: ug/1

10200ND6.0

6064.517.5

9410036525.3231

153000304

4150079414.8123

106000NDND

246000ND21.2

5730

InstrumentDetection

Limit

M Column - Method Code (See Section 2 of Report)

M

58.24 . 63.81.40 . 2 00 . 4 0

4 2 . 21.01.23 .5

41.52 .5

4 0 . 31.10.502.1

6014 . 81.4

2634 . 81.99.0

PPPPPPPPPPPPPPCVPPPPPPPP

300944

I!

Page 164: SDMS Document WHITMAN anies . ompanie

9DIIHII0II1I

Client ID: DSRW-1Site: Klockner & Klockner

Date Sampled:Date Received:

10/16/9810/16/98

Lab Sample No: 90839Lab Job No: 1280

Matrix: WATERLevel: LOW

Ii

Analyte

METALS ANALYSIS

AnalyticalResult

Units: uq/1

InstrumentDetection

Limit

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

30100ND10.

2091.1.

15900015511.

26337500

92.117006960.

85.11400

NDND

319000ND64.684

6

40

5

5

152

2

5843100

4211341240102

30041

263414

.2

.6

.8

.4

.20

.40,

.2

.0

.2

.5

.5

.5

.3

. 1

.10

.1

.8

.4

.8

.9

.5

PPPPPPPPPPPPPPCVPPPPPPPP

M Column - Method Code (See Section 2 of Report)

DD

300945

Page 165: SDMS Document WHITMAN anies . ompanie

1I

1

II

II1IIII

III!IIII

II

Site: Klockner & Klockner Lab Job No: 1280

Date Sampled: 10/16/98Date Received: 10/16/98 Date Analyzed: 10/19/98Matrix: WATER QA Batch: 1681

ICORROSIVITY (pH)

Envirotech Analytical ResultSample # Client ID Units: std unit

90838 DSSR-1 7.63

90839 DSRW-1 10.31

300946

Page 166: SDMS Document WHITMAN anies . ompanie

ISite: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Matrix: WATER

Lab Job No: 1280

Date Analyzed: 10/19/98QA Batch: 1376

IIGNITABILITY

0IInii

nni

EnvirotechSample #

90838

90839

Client ID

DSSR-1

DSRW-1

FlashpointUnits: deg F

>160

>160

n300947

Page 167: SDMS Document WHITMAN anies . ompanie

Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Matrix: WATER

Lab Job No: 1280

Date Extracted: 10/19/98Date Analyzed: 10/19/98QA Batch: 1364

II11

EnvirotechSample #

90838

90839

REACTIVE

Client ID

DSSR-1

DSRW-1

CYANIDE

DilutionFactor

2.0

2.0

I

V1II

Analytical ResultUnits: mg/1

ND

ND

Quantitation Limit for Reactive Cyanide is 25.0 mg/1

IIIIIIIIII 300948

II

Page 168: SDMS Document WHITMAN anies . ompanie

Site: Klockner & Klockner

Date Sampled: 10/16/98Date Received: 10/16/98Matrix: WATER

Lab Job No: 1280

Date Extracted: 10/19/98Date Analyzed: 10/19/98QA Batch: 1364

IIJII

EnvirotechSample #

90838

90839

REACTIVE

Client ID

DSSR-1

DSRW-1

SULFIDE

DilutionFactor

2.0

2.0

Analytical ResultUnits: mg/1

ND

ND

IIni§iiitiii

Quantitation Limit for Reactive Sulfide is 20.0 mg/1

300949

Page 169: SDMS Document WHITMAN anies . ompanie

I'KOJKCTNA.MK: Klorkner J& Klocknrr

PROJECT NO: 95-03-02

LABORATORY: Envlrolcch Project #809002

f SAMPLE

! TIME

•HSAMPLE

LOCATION

6UJA/IC.

RELINQUISHED BY:

l:RELINQUISI IEDBY:

SI'I K ADDKKSS: Stickle A v e n u e £ l . l i n Street, I t i i ckuwu) Iliirough. NJ

SAMPLE DATE: / O// 10/tf ^

SAMPLER(S): Cheryl \.. Coffee

SAMPI.F SAMPLEDEPTH

SAMPLEMATRIX

ANALYTICAL PARAMETER IDENTIFICATION KEY:PMC: PETROLEUM HYDROCARBONS

VOC: VOLATILE ORGANICS BY OC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SI-ARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCIIPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

ANALYSISREQUESTED

TIME:

RECEIVED BY;

R E C E I V E D BY:

ri - n:n.ING TILE

TSI = THERMAL SYSTEM INSULATION

"1 PRESEK-

I VAT1VENo. orCONT.

2 !

SPECIALINSTRUCTIONS

DATE: K)f/C-/#) TIME /O7Z--

DATE: TIME

TOTAL NO. CONTAINERS __

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300950

Page 170: SDMS Document WHITMAN anies . ompanie

ft« ENVIROTECH RESEARCH, INC.11

777 New Durham RoadEdison, New Jersey 08817

•I Tel: (732) 549-3900II Fax: (732) 549-3679

www.enviro-lab.com

II

|| The Whitman Companies, Inc.44 West Ferris Street

I* East Brunswick, NJ 088 16

Attention: Dr. Ira Whitman

Re: Job No. H941GS

II Dear Dr. Whitman:

November 17, 1998

JP^CT|T^

c^^j'f- Klockner & Klockner •——•''

Enclosed are the results you requested for the following sample(s) received at our laboratory on|| October 7 and 9, 1998:

Lab No. Client ID

11H941-88549 SSGC-1

II H950-88670 SSGC-2|| H950-88673 SSGC-3

H950-88680 SSGC-4l| 1052-89302 SSGC-1A

Analysis Required

Grain SizeGrain SizeGrain SizeGrain SizeGrain Size

An invoice for our services is also enclosed. If you have any questions please contact your|| Project Manager, Robert McGrady, at (732) 549-3900.

1

II

ai

Very truly yours,

/ ^ J f \Michael J. Urban ^Laboratory Manager

300951

11 Laboratory Certifications: New Jersey (12543) New York (11452) Pennsylvania (68-522) Connecticut (PH-0200) Rhode Island (132)

Page 171: SDMS Document WHITMAN anies . ompanie

300952

COBBLES &BOULDERS

STANDARD SIEVE SIZE

GRAIN SIZE IN MILLIMETERS

fp^^KsiS^sS^

Page 172: SDMS Document WHITMAN anies . ompanie

I 300953

UNIFIED SOIL CLASSIFICATION

COBBLES &BOULDERS

ct

Ic<cIILCcLc

100

90

80

70

3 60y

nn

*!l 50rDJ

jL 40

30

20

10

0

CT-

GRAVELCOARSE FINE

e s e e

*v

\

\\

\

\

SANDCOARSE | MEDIUM FINE

SILI ORCLAY

STANDARD SIEVE SIZEo o o

o o o o o.̂ T- •& T- c\i c:

^^

\

\

\

\

^

\

\

\

\

\

"^

^^

s.\

X

\\\\

<

XN

\

\\\\

>

k

^ ^

I I I | 1 1 I 1 1 i I 1 1 I 1 1 1 1 I 1 1 1 1 1 1 1

3 0 0 *- t o ° i a , _ m . ^ o

GRAIN SIZE IN MILLIMETERS

EXPLORATION/IDENTIFICATION: C

H950-88673 ELINE SYMBOL:

EPTWSOURCE:

:NVIROTECH ;r-4'MOISTURE CONTENT (%):

19.4LIQUID LIMIT (%): PLASTIC LIMIT (%): USCS SYMBOL:

MLUSCS CLASSIFICATION:

CLAYEY SILT.SOME FINE TO COARSE SAND.TRACE FINE GRAVEL

H950-88680 ELINE SYMBOL:<>- •©

NVIROTECH ;4'-7'MOISTURE CONTENT (%):

2.9LIQUID LIMIT (%|: PLASTIC LIMIT <%l: USCS SYMBOL:

SP/SMUSCS CLASSIFICATION:

FINE TO COARSE SAND.AND FINE TO COARSE GRAVEL.TRACE SILT

GRADATION CURVES

MEL1CK - TULLY AND ASSOCIATES, P,C, PLATE 18

Page 173: SDMS Document WHITMAN anies . ompanie

UNIFIED SOIL CLASSIFICATION

COBBLES &BOULDERS

<

cc4

(

|t

L(CLC

TOO

90

80

70

3 602nn<

50£uJE1JL 40

30

OA

10

n

GRAVELCOARSE FINE

c c e c

X,

\\

SANDCOARSE MEDIUM FINE

STANDARD SIEVE SIZE0 0

•* «- ««•

\

\*\

N

SILT ORCLAY

o o oo o o•- OJ TO

\

\

" i i i I | i I I | i 1 1 1 1 1 1 1 1 1 1 1 1 1

O0 o o ._• - i n •- in ,- ";

GRAIN SIZE IN MILLIMETERS

EXPLORATION/IDENTIFICATION: C

I052-89302 ELINE SYMBOL:

EPTH/SOUHCE:

NVIROTECH :MOISTURE CONTENT (%l:

15.3

5-.4,LIQUID LIMIT (%}• PLASTIC LIMIT (%|:

X>

i | i i i |

USCS SYMBOL:

SMUSCS CLASSIFICATION:

FINE TO MEDIUM SAND.AND CLAYEY SILT.SOME FINE TO COARSE GRAVEL

GRADATION CURVE

MEUCK -TULLY AND ASSOCIATES. P.C.

300954

PLATE 1C

Page 174: SDMS Document WHITMAN anies . ompanie

SAMfl.K OATKl /£ A, / <?£

SAMPI.KK(S): Chtryl L. Coffee /(!-LXDO/tATOKVr Envfrofrrd Nnrcrrb, Inc.

ANALYSISREQUESTED

DATE: lO

DATE:

RELINQyiSllED BY:

RELINQUSHED__BY:

RECEIVED IIY

RECEIVED IIY

TOTAL NO. CONTA1NERS

v\

ANALYTICAL PARAMETER IDENTIFICATION KEY:PMC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS DY GC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SEARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPPHO: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT-CEILING TILH

FT" FLOOR TII.E

TSI=TIIERMALSYSTl:M INSULATION

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300955

_

Page 175: SDMS Document WHITMAN anies . ompanie

01

PROJECT NO: 9S-OJ-OJ £ nt»Vo4« ^

LABORATORY: Envlrolech Resenrth, Inc.

("SAMPLETIME

i Mt<U«.A>«lMM A

: /O I L I 7^>SAMPI.K DATK:

SAMI>I.KU(S): Cheryl I. Cofftc {, . Sf

SPECIAL"INS1 RUCTIONS

> KECEIVED

KKCEIVEI)

TOTAL NO. CONTAINERSANALYTICAL PARAMETER IDENTIFICATION KEY:PUC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS DY GC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC IIYDROCARIIONS IN BASE NEUTRAL SCAN WITII LIBRARY SEARCH

BN: BASE NEUTRALS WITI I LIBRARY SEARCII

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT-CEILING TILE

IT-FLOOR Tll.li

TSI -TIIILRMAI.SYSTEM INSULATION

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300956

Page 176: SDMS Document WHITMAN anies . ompanie

rHOJI.L'1 N . t A f K j Mcxk.rr A

rWOJfCTNO; 9S-03-01

LAfiOHATOHY: Knvlrnfcch Research, Inc.

Ml H ADKHKVS; Sllcklr A»r«nt A Kim Slrnl. HcKkin «j tlofMfk, NJ

SAMI'I.K DATE: fO ~7 / I Q

SAMI'I.ER(.S): Chtryl I. Coffee / (,. w^^^ H955;

w01

SAMPLETIME

1-21 0

: SAMPLELOCATION

RELINQUISHED BY:

RELINQUISHED BY:

•SAMi'LE;-.:

IDSSAMPLEDEPTH

SAMPLEMATRIX

F & - 2

)0

SSC^C-1

UM

:[ ANALYSIS •

REQUESTED

Tc'L

£o£lreduce

/

DATE:///^ilME: p ^RECEIVED

DATE: TIME: R E C E I V E D 11V:

ANALYTICAL PARAMEJER IDENTIFICATION KEY:PMC; Pr-TROUnUM MVDROCARDONS

VOC: VOLATILE OROANICS DV OC/MS WITH LIBRARY SRARCII

PAH: POLYCYCLIC AROMATIC HYDROCARUONS IN BASE NEU1RAL SCAN WITH I.IURARY SI-AKCII

BN: BASE NEUTRALS WITII LIBRARY SEARCII

AE: ACID nXTRACTABI.KS WITH LIBRARY SEARCH

PPM: PRIORITY POLLUTANT METALSPP^O: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT-CKII.IN(iTII.F.

IT" n.OOKTII.I:

TSI •= TllliUMAI. SYSTEM INSULATION

PRESER-VATIVE

INO.OFCONT.

I

2-2.

3

2-

z

2-Z

i ' .^; : : -- . - : S'p'ECiAL : : - i ; . . .;i^v INSTHUCTIONS...........

ttt 71

DATE: Y J r i n s T J M E

DATE: TIME

TOTAL NO. CONTAINERS .

E \1 ̂

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300957

Page 177: SDMS Document WHITMAN anies . ompanie

»»««« A »:im Mtftl. l<«*U«««r !»•»••««•. NJMff

.SAMI'I.K I>AIK: ~)

SAMPI.KHIS): f:iirryll.fi.ffr«

HKUSCTHO, M4MU

TOftVt tonimtt* Rrtnrrk. I ft.

ANALYTICAL PARAMETER IDENTIFICATION KEY;CMC: PLTROLHUM HYDROCARBONS

VOC: VOLATILE ORGANICS OYGC/MS WITH LIORARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIURARY StAKCII

DN: BASE NEUTRALS WITH LIBRARY SEARCH

AE. ACID EXTRACTAnLES WITH LIBRARY SEARCHPPM PRIORITY POLLUTANT METALSPPHO: PRIORITY POLLUTANT PLUS FORTY PEAKS

rr-cEii.iNOTii.i;IT- I-I .OORTII.I :

TSI • THERMAL SYSTEM INSULATION

DATE: \ ( ̂ TIME I

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300958

Page 178: SDMS Document WHITMAN anies . ompanie

w

PKOJKCT N.\*IKt Kforkufr Jl

PHOJtCTNO: 95-OJ-02

LAUOKATOKY: Envlrolech Ktstarch, Inc.

»: AODHI-VSi HlllkW Av««»t

KAMI' I .KDATK: I «/ "7

SAMPI.ER(S): Cheryl I. Coffee / t . <A->

SAMPLE

TIME

SAMPLE

LOCATION

SAMPLE SAMPLE

DEPTH

SAMPLE

MATRIX

ANALYSISREQUESTED

(RELINQUISHED BY:

'RELINQUISHED BY:

DATE:,

DATE: TIME:

R E C E I V E D BY:

R E C E I V E D IIY:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PMC PETROLEUM HYDROCARBONS

VOC: VOLATILE ORGANICS BY OC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH I.IIIRAKY SKARCH

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

CT • Cim.ING TII.I-:

IT- rLOOKTIl.l:

TSI --TIIKKMAI. SYSTliM INSULATION

PRESER-

VATIVENO. OF 1CONT.

1

SPECIALINSTRUCTIONS

1-

DATE: I / 7 * TIME

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300959

Page 179: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klockncr & Klockncr

PROJECT NO: 95-03-02 ^AUi

LABORATORY: Envlrolcch Research, Inc.

"tL gG^ OC>3

101

SITE ADDRESS: Slicldc Avenue & Elm Street, Rockaivny Uorough, NJ

SAMPLE DATE: fofl,lQ$

SAMI'I.EU(S): Cheryl U Coffee /I,

PAGE OF

ANALYTICAL PARAMETER IDENTIFICATION KEY:PIIC: PETROLEUM IIYDROCARDONS

VOC: VOLATILE ORGANICS DY OC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC IIYDROCARDONS IN DASE NEUTRAL SCAN WITH LIBRARY SEARCH

DN: DASE NEUTRALS WITH I.IDRARY SEARCH

AE: ACID HXTRACTADLHS WITH LIDRARY SEARCHPPM: PRIORITY POLLUTANT METALSPPUO PRIORITY POLLUTANT PLUS FORTY PEAKS

CT-CEILING TILl;

PT •• M.OOR Tll.l:

TSI "1 HURMAL SYSTEM INSULATION

DATE:

TOTAL NO. CONTAINERS.

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300960

Page 180: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klockntr & Klockncr

PROJECT NO: 95-03-02 fjivi^o-fci t-

LABORATORY: Enviroftch Rtsearck, Inc.

SITE ADDRESS: SlIckle.Avcnuc & Elm Strecl, Kockawny Borough, NJ

SAMPLE DATE: /6?/6/^&

SAMI'LEK(S): Cheryl I. Coffee / (, . M?XT CofT*'

PAGE

ANALYTICAL PARAMETER IDENTIFICATION.KEY:PIIC: PETROLEUM HYDROCARBONS

voc: VOLATILE ORGANICS BY GC/MS WITH LIBRARY SEARCHPAH. POLYCYCLIC AROMATIC IIYDROCARIIONS IN BASE NEUTRAL SCAN WITH LIDRARY SEARCII

BN: BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTABLES WITH LIDRARY SEARCHPPM: PRIORITY POLLUTANT METALSPPMO: PRIORITY POLLUTANT PLUS FORTY PEAKS

rr-c'Lii.iNd MM:IT - I LOOK lll.l;

1SI - Tlir.KMAI.SYSTEM INSULATION

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300961

Page 181: SDMS Document WHITMAN anies . ompanie

««/ A

: 9X-OJ-01

: Envlroftch Kestiirrh. Inc.

SAMPLETIME

SAMPLELOCATION

SSFS-2-

ION

SAMI'LE(Off

Mil' AI HIM I AM Ml. kl« V.«-.. A Mm Mm I. l»«Mk«.««r

SAMI'I.K t)A I II: £!/-7 I /'8

.SAMH.KU(.S): Chcr)ll.. Toffee A

SAMI'LEDEI'TII.

o-.r

SAMI'LEMATRIX

Soi l

RELINQUISIlEp BY:

IRELINQUISHEDBY: DATE:

ANALYSISHEQUESTEn

^

ftfAL-

f IME: \ T'5 RECEIVED I1Y:1

TIME: HECKIVEI1HY:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PHC. PETROLEUM HYDROCARBONS

VOC. VOLATILE OROANICS DV GCVMS WITII LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN DASI: NEUTRAL SCAN WITI I LIDRAR Y SliARCI I

DN. BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTAdLES WITH LIBRARY SEARCHPPM PRIORITY POLLUTANT METALSHPUO: PRIORITY POLLUTANT PLUS FORTY PEAKS

rr-cim.iNOTii.i;IT- FLOOR TILE

TSI -TlinRMAI. SYSTEM INSULATION

rilliSEH-VATIVE

U

NO. OFCONT.

2"

"2

2.

SPECIALINSTRUCTIONS

76 !

79

9-8-6 {TV

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300962 lir

\7

Page 182: SDMS Document WHITMAN anies . ompanie

Ai

PROJECT NAME: Klockntr & Klockner

PRO.IECTNO: 95-03-02

LAIiORATORY: Envlrolcch Rcsturch, Inc.

SITE ADDRESS: Slk-ktt Avenue & Elm Slrccl, UnckHway I)orouBh, NJ

SAMI'I.E DATE: / «?/ 7 |^2?

SAMPI.ER(S): Cheryl I.. Coffee //, • i

; SAMPLEi TIME

|(̂

SAMPLELOCATION

GiA<i 'TAroy—

. . _ . .

,

SAMPLEIDS

S5(yr-3

SAMPLEDEPTH

1-̂

SAMPLEMATRIX

ANALYSISREQUESTED

-TV1, i r\ ^L \jcx_x

PRESER-VATIVE

^iHfeM

NO. OKCONT.

2-

SPECIALINSTRUCTIONS

W0>

RELINQUISHED BY:

RELINQUISHED BY:

DATE

DATE:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PIIC: PETROLEUM HYDROCARBONS

VOC: VOLATILE ORGANICS DY GC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH I.IIIRAKY SEARCH

DN: BASE NEUTRALS WITH LIBRARY SEARCH

AE ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

TIME:

RECEIVED HY:

RECEIVED HY:

(T -CI-ILINOTII.I-:

IT- i LOOK rn.i;

TSI •= THERMAL SYSTEM INSULATION

DATE: | / "' ' TIME

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300963 iHr

Page 183: SDMS Document WHITMAN anies . ompanie

FHtVKCT /v.t.MK: Mwliirr «

PKOJKCT NO.' 9S.OJ-02 ef r\

M 11; ,\WHO

SAMt'l.H MATH: f

JSABil'LE

j TIME LOCATION

SAMPLE

ID/I

SAMPLE

PEPTIC

SAMPLE

MATRIX

S.V.Mrl.KK(S): ( lirryl I.. I'allec / L . l»j£'>rto f>

VA'I'IVF, COM',

SI'KCIAL

INSTRUCTIONS

wCO

M:\.KtQUK\mtn\: I ^Zt^fj/Ug* ^-^T}/( ^~ I'ATK:

RELINQUISHED BY: ' / DATK:

ANALYTICAL PARAMETER IDENTIFICATION KEY:IMIC rETROtKUM HYDROCARBONS

VOC VOI.ATH.I: OROANICS HVCCAIS WITH LinlMRY SEARCH

PAII POI.YCVn.IC AROMATIC IIVDROCARnONS IN DASE NLUTRAI, M'AN WITH UPHAKV SI.ARn

0N DASE NEUTRALS WITH LIBRARY SEARCH

AE ACIO tXTRACTAIll-ES WITH LmRARY SEARCHFFM PRIORITY POLLUTANT METALSfp'40 f'RIORirY POLLUTANT PI.US FORTY PKAKS

T.IVI.I) IIY:

TIMK: UKCKIVKI) IIY:

rr ~ i t . i \ iv(; in.iIT - n.()f>H m.i:

TIMK

DATE: TIMK

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC

44 WEST FERRIS STREET

EAST BRUNSWICK. NJ 08816

Page 184: SDMS Document WHITMAN anies . ompanie

PROJKCTN/IAIE: Klockner A Klorkncr

PROJECT NO: 95-03-02

LABORATORY: Envirolfch Project #809002

Mil-: ADDKKSS: Sllcklr Avrmir & Klin Slrccl, U«cknwny Horoueh, NJ

SAMIM.K1MTK: IO//(,/<i$/

1'A.GK OF

SAMPLER(S): C.'lirryl I.. Coffee

ANALYSIS

REQUESTED

RELINQUISHED BY:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PMC: PETROLEUM HYDROCARBONS

VOC: VOLATILE OROANICS DY OC/MS WITH LIBRARY SEARCH

PAH POL YCYCLIC AROMATIC HYDROCARBONS IN BASE NEUTRAL SCAN WITH LIBRARY SKARCII

t)N: BASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM: PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS FORTY PEAKS

: ' IME: |T ' J^> RECEIVED BY: {:

TIME: RECEIVED 11\':

PI - FLOOR Til. I:

TSI «TIII :KMAI.SY.STI: 'M INSULATION

PRESER-

VATIVE

NO. OFCONT.

SPECIAL

INSTRUCTIONS

DATE:

DATE: TIME

TOTAL NO. CONTAINERS

/75~i

THE WHITMAN COMPANIES INC44 WEST FERRIS STREETEAST BRUNSWICK, NJ 08816

300965

Page 185: SDMS Document WHITMAN anies . ompanie

PROJECT NAME: Klorknet- & Klockntr

PROJECT NO: 95-03-02

LABORATORY: Envfrotcch Project #809002

SAMPLE

• TIME

SAMPLE

LOCATION

RELINQUISHED BY:

(RELINQUISHED BY:

SAMPLE

t

SAMPLE'

DEPTH

SAMPLE

MATRIX

rAd^r

SITE ADDRESS: Slit-Mr Avenue & Klin Slrcel, Hockuwny Uorough, NJ

SAMPLE DATE: / &//£/'£• *?

SAMPI.EU(S): Cheryl L. Coffee

ANALYSIS

REQUESTED

PAGE

\5XC.'W->

DATE:

ANALYTICAL PARAMETER IDENTIFICATION KEY:PIIC: PETROLEUM HYDROCARBONS

VOC: VOLATILE ORGANICS BY GC/MS WITH LIBRARY SEARCH

PAH: POLYCYCLIC AROMATIC ttYDROCAROONS IN BASE NEUTRAL SCAN WlTl I I.IHRARY SI:ARCII

ON: DASE NEUTRALS WITH LIBRARY SEARCH

AE: ACID EXTRACTABLES WITH LIBRARY SEARCHPPM PRIORITY POLLUTANT METALSPP+40: PRIORITY POLLUTANT PLUS PORTY PEAKS

TIME:

RECEIVED HY:

RECEIVED HY:

<T =-- ri-n.iNO TII.I;

I-T « FLOOR TII.I:

TSI -THERMAL SYSTEM INSULATION

2,

W. OF~?

PRESER-

VATIVE:.: :

NO. OF:CONT.

SPECIAL

INSTRUCTIONS

DATE:

DATE: TIME

TOTAL NO. CONTAINERS

THE WHITMAN COMPANIES INC44 WEST FERRIS STREET

EAST BRUNSWICK, NJ 08816

300966


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