SDMS US EPA REGION V -1 · 2020. 11. 29. · 2. ie-1 nd 18/86/88 gub-81 mh b nd nd nd nd 213 i.ie-3...

SDMS US EPA REGION V -1

SOME IMAGES WITHIN THISDOCUMENT MAY BE ILLEGIBLE

DUE TO BAD SOURCEDOCUMENTS.

ft 0 0 0 0 1 0 7

JACOBS

IV

JACOBS ENGINEERING GROUP INC.ENVIRONMENTAL SYSTEMS DIVISION

IN ASSOCIATION WITH:TETRA TECH

METCALF & EDDYICAIR LIFE SYSTEMS

KELLOGG CORPORATIONGEO/RESOURCE CONSULTANTS

BATTELLE PACIFIC NORTHWEST LABORATORIESDEVELOPMENT PLANNING AND RESEARCH ASSOCIATES

U.S. ENVIRONMENTAL PROTECTION AGENCYTECHNICAL ENFORCEMENT SUPPORT

ATHAZARDOUS WASTE SITES

TES IVCONTRACT NO, 68-01-7351

WORK ASSIGNMENT NO. C05030

GROUNDWATER ANALYTICAL RESULTS SUMMARY7

PHASE I OF THE REMEDIAL INVESTIGATION f

WHEELER PITLaPRAIRIE TOWNSHIP, WISCONSIN

RI/FS OVERSIGHTEPA REGION V

JACOBS ENGINEERING GROUP INC.PROJECT NUMBER: 05-B918-00

FEBRUARY 191*

til JACOBS ENGINEERING GROUP INC.ENVIRONMENTAL SYSTEMS DIVISION222 S. RIVERSIDE PLAZA - SUITE 1870 CHICAGO, ILLINOIS 60606 (312) 648-0002 FAX (312) 648-0551

February 17, 1989

Mr. Michael ValentineTES IV Primary ContactU.S. Environmental Protection AgencyRegion V230 South Dearborn StreetChicago, IL 60604

Re: Contract No. 68-01-7351Project No. 05-B918-00Work Assignment No. C05030Wheeler PitLaPrairie TownshipRI/FS OversightCERCLA, Region V

Dear Mr. Valentine:

Please find submitted herewith four (4) copies of the spreadsheets which presentCLP and PRP groundwater sampling results from Phase I RI sampling at theWheeler Pit site in LaPrairie Township, Wisconsin. Please note that only 2 copiescontain both spreadsheets, one with the full results and one with only thechemicals detected in Phase I of the RI; also note that only one copy (intendeu foryour files) contains the CLP analytical data packages.

If you have any questions or require additional information, please feel free tocontact Michael Strimbu or me at (312) 648-0002.

Sincerely,

Dean GeersRegional Manager

Enclosures

cc: E. Howard

TABLE 1

CHEMICALS DETECTED DURINGPHASE I RI GROUNDWATER SAMPLING


TABLE 1

CHEMICALS DETECTED DURINGPHASE I RI GROUNDWATER SAMPLING


111PIw

K111111*•

ILLLI"

"Wi Of COMPOUNDS DETECTED IN ?

SCORCH P&8T<SAMPLING LOCATION

USEPA CASE NUMBER 11515DATE SAMPLED'ACRGAN1C TRAFFIC REPOP.TIORGANIC TRAFFIC REPCRTICBL SAMPLE NUMBER I89JGIHNAR7.VN SAMPLE NUMBER INP-ISAMPLING LOCATIONCHEMICAL

INORGANICS licj/ll

AntnonyArsenicSariulBerylliuiCaieiul

ChroiuiCocultIronHitMaqnesiui

HanqaneseNickelPotass iuiSeleniulSilier

SodiuiVanadiuilineCyanide

P"Specific conductanceTelperaturePercent solids 111

h«E I 81 GKOiINC yATER SSMPLU

USEPAMN IlB

II/I5/B8KE1911E1471SI!

MN IlBNOTES

• ND• NDt 4.79E-2 IBI• NDt 91.8

• ND» ND• 1. TOE-3 III

NDt 42.1

* 5.4E-3 IBIi ND* 1.92 IBI> ND• ND

« 4.11• Nl» 1.79> Nl

5, NHEEUR PI

papIN IlB

'.J/15/88

.,

GNMNIIB-I1NN IlB

NDNDNDND96.1

I.IE-3 IBINDNDND51.3

NDND

1.45 IBINDND

5.54M1.75I.K-2

7.32775B.5

, LbPRAIRlE 10)

.SEP*Mil i!A

11/85/68NEI912EI472S12

nN HA

ND2.6E-3 IBI4.B9E-2 IIII.IE-3 II)

91. b

NDNDNDND11.7

1.54E-2ND

1.24 IIII.7E-3 IBJNI

ND

4.14ND2.52

1.IE-2 IBI

fitnu HA

I1/I5/B8

MN IIA

NDNONONO94.2

I.IE-3 IIINDNOND52.5

NDND

1.35 IBINONO

5.43ND2.45

B. IE-3 III

7.397459.1

JSEPAnil A

11/15/88MEI9I3EIb73SI3

KN A

ND2.5E-3 III4.94E-2 IBII.IE-3 IBI

91.8

NDND

1.4IE-2 IBINO41.9

NDI.45E-2 !BI

NDNDNO

7.12ND

I.HE-IND

m':* A

IB/15/8B

..

GnA-llKN A

NDNDNDNO94.2


NOND

5.5E-1 IBINONO

4.2ND

I.41E-IND

7.2981111. 1

USEPA% J;B

13'15/BBNEI9KEI&74SI4

nit |?B

NDND

4.BE-2 IBII.IE-3 IBI

9!. 2

NDNDNDND

41.3

5.3E-3 181NO

1.3V IIINDND

4.14ND

7.47E-2Nl

PRPN. I2B

11/15/38--

GNMNI2B-I1MN I2B

NDNDNOND94

I.IE-3 IBINONO

3.4E-3 Ifljl45.7

NDND

1.55 IBINDND

5.33ND

7.2E-2 (BJIM

7.19BI5il.l

USE'SKN D

(Mf OF KH I2B

1I/I5/B8HE19I5EI475SI5

nN D

NDND

5.I5E-2 IBII.IE-3 IBI

92. B

NONONDXD

42.1

5.2E-3 IBIND

1.4 IBINDND

4.34NO

4.47E-2ND

uSEPAIW I2A

ins ( nsoi

ll/lk/88KEI9I4ET748Sit

MN I2A

ND3.5E-3 IBl

5.14E-2 IBII.IE-3 IBI

94.2

NO' ND

NDW

4J.4

4.9E-3 IBIM

4.8BE-1 (811.8E-3 IBJI3.3E-3 IBJI

14.3ND

4.2IE-2NO

PRPMN B2A

11/14/88--

GUSNI2MIMN B2A

NONDNDNO112

I.7E-3 IBIND

5. IE-2 IBI(.3

54.7

NDND

B.9E-1 IBINDND

13ND

7. IE-2 IBJI4.IE-3 IBI

7.288658.1

L

Lr

LG.:

DLecL

SUMNAdr OF COMPOUNDS DETECTED IN FMSE I RI GRSUND KATER SAMPLING, NHEELER PIT, ^PRAIRIE TCWISHIP, dlSCWSIN

SOURCE PARTV USEPA PRP PRP USEPA PRPSAMPLING LOCATION N* B MB MN B Mil 23B Hti I3B

IDUP).JSEPA CASE NUMBER 18535BATE SAMPLEDINORGANIC TRAFFIC REPORTIORGANIC TRAFFIC REPORTIcat SAMPLE NUMBER iB9jsn-)Mil* SAMPLE NUMBER IMP-1SAMPLING LOCATIONCHEMICAL

INORGANICS 114/1)

AntiunyArsenicBariuiBerylliuiCilciui

ChronuiCoDll tIronLe»dKjgnesiui

ManganeseNickelPotastiuiSeleniutSilver

SodiuiVanadiui2incCyanide

pHSpecific conductanceTeiperaturePercent solids HI

NEI9I7

SI7

MM B

NDND

2.I9E-1ND147

NDND

1.47E-2 IB)NO37

1.32E-IND

4.99 IIIND

9.8E-3 IBJI

92.4ND

2. IE-1ND

18/86/88

GUB-81MH B

NDNDNDND213


B.1BE-IND

4.24 IIINDND

94.4ND

2.25E-II.4E-2

4.851411II.)

18/14/88

GklB-91nU o

4.4E-3 IB)ND

2.3MND191

1.1E-3 IBINONDND37.4

8.I7E-1ND

4.1 IB)NOND

91.1ND

2.3K-II.4E-2

18/36/881EI918

SIS

MM B3B

ND2.7E-3 [iJn;4.S1E-2 IB)7.IE-4 IB)

B8.3

NONDNDNC41.2

2.7E-3 IBIND

1.25 IB)NDND

6.27ND

9.BIE-2ND

GUM83B-I!Mil I3B

NDND

ND117

7.3E-4 IB)ND

1.7E-I IBJIND51.2

NDND

1.17 IB)NDND

5.11NO

1.I6E-1NO

7.3174511.1

PRP

iDUP)

Til,"

NDN9

ND184

9. IE-4 IB)NC

4. IE-2 IBJIND<5.6

NDND

1.38 IB)NOND

5.54ND

9.9E-25.1E-3

USEPAIlk I3A

13/46/88MEI9I9EV77158?

f,'. 83A

I.48E-2 IB)3.64E-2

3.53E-2 IBIND179

ND5.8E-3 (61

9.14M61.7

I.I5E-1I.29E-2 IB)

7.24l.BE-3 IBJN)5.8E-3 (BJ)

51.2ND

I.45E-IND

PRPIU 33A

GUNVB3A-3IM 834

ND2.9E-2

fcDND239

1.4E-3 IB)NO9.12liD72.1

9.3E-2ND7.22NDND

52.9ND

I.74E-11.2E-2

6.95154112.1

-

I

11.f

11

||

11f»

''333

i

SuKMRY OF COMPOUNDS DETECTED IN PHASE ! RI GROUND WATER SAMPLING, WHEELER 'IT, LaPRAIRIE Tu.NSni?,

SOURCE PARTYSAILING ^CATION

USEPA CASE NUMBER 1Z5Z5DATE SAMPLEDINORGANIC TRAFFIC SEPCRT»ORGANIC TRAFFIC REPORT!CRL SAMPLE W.X3E9 i89JGBl-iWARZYN SAMPLE NiiMBER (WP-)SAMPLING LOCATIONCHESICAi.

INORGANICS !«q/l)

ArtiionyArsenicBariuiBeryl liuiCalciut

ChroniuiCobaltIronLeadMagnesia*

ManganeseNickelPotassiunSeieniu*Silver

SodiutVanadiuilineCyanide

PHSpecific conductanceTemperaturePercent solids (7.)

JSEPflFIELD BLANK

18/86/88yr yQTflnt*T£B

EY772329--

FIELD BLANK

NONDNDNDND

NDND

1.74E-2 (3)NDND

NDNDNDNDND

3.7BE-1 (B)NDNDND

USEPATRIP BLANK(VOA ONLY)

119/196/88

EY773R18--

TRIP BLANK

NANANANANA

NANANANANA

NANANANANA

NANANANA

NANANANA

PRPFIELD BLANK 1

119/06/88

----

FBB1-81FIELD BLANK 1

NDNDNDNDND

3.8E-4 (B)ND

5.BE-2 (BlNDND

NDNDNDNDND

NDNDtin111/

ND

7.52<1813. B

PR'r - *•• -. n> /MIL/ ">rid-U DLHIlK L

119/26/83

----

FB82-81FIELD BLANK 2

NDNDNDNDND

3.BE-4ND

1.10E-1 (BN)?xDND

NDmItU

1.8E-1 !BN;NDND

NDND

1.8E-2 (B!ND

7.72(1813.8

PRPTRIP BLANK 1

/ "in* nin u \I vuh uiiu ' J

12/85/83

----

TBZl-Z!T2 T C n' 'fc- 'i ft I r OLrtiif, i

NANANANANA

NANANANANA

NANANANANA

NANAr.n\\r\

NA

NANANANA

itfTRIP BLANK 2iVCA ONLY)

18/86/88~~----

TBB2-Z1"RIP BLANK 2

NANANANANA

NANANANANA :

NANANANANA

NANANANA

NANANANA

(I) spun* »»»3J»j

sri sri ii'i zrt•«gt*3

uri

5-31't

tin nn

itrt

net

nri nu

I'S l'5

n

t'.ci itri

I'S

KM

(9IOI !"a1oi ^Ja^-Jaûo^ A»Q-|i Ato-i

6»-jt

swi

nu

SISI'I

nail (a»ai

intu«|is

•""»«3'"«J»

lt/*»l S3HM9WKI

T\)31«3H3WI1OT01

(-H9f48i mm 3t<»ws "»"I180d38 31JJ081 3IIW98!!

H«Od3B 31JJOB1 3IHD980KI031dtl« 31«

Jlia«d 3301(15

1

NISN80SIS 'dlHSNBOl 3I819Md'T 'lid H3133HKB319K 18 ! 3SKHd Hi 03133135 SlWOOdUOO 40 AWtWHS

IIIrr

tIIIIIIIIIIDII

SUMARV OF CQNPOUNDS DEtECIEB 111 PhASl 1 01 BROW HATER SftWLlNG, rfHEElER P',T, LjPRft lRlE KKHSrtlP, HISCOHSIH

SOURCE PftRHSAWUH6 lOCftUOH

US£P» USE UMBER 11515OftU SMIPIEDlliORGAHIC UAFF1C REPOR1IOR6M1C IRAfFlC REPOR1ICH. SftHPtE KUHB» IB9J6I1-IHARM SMPLE NURBER IKP-1SftnPUHG IDCftllON

VOt.ftTli.ES

Htthylm ctiloridf IdichloroMUunt)ftcttoatl,2-4ichlarottlttn» lus <nl tuns I

cii-l,2-aUnUf<uu«uiitrins-l,2-cicMorcetli«i\e

CMorolori ttrichloroittMftt 12-buUnofll Uiltnyl ttliyl Utontl,(NEK)]

1,1,1-trictiloroelhintIncKlorMthene ITCEIBtniMtt«tr«chiori»thcn( iPCEl

(toUli

TICs (I)

tru%-l ,2-diMthylcyclotaiMiCK-I ,l-diMthylcyclolwiiii(

l-lthtnyl-2-uttiylbtnitniLi2-dichlQrobcniefltm-ocUMropentjlenf

itSEPAIW I1B

11/15/88AEI9I1EU)1Sll—

UN lieNOTES

• HD> 8 Ul* HD

*• HD

TPJ HD

• HIPut HD» HOTPJ U* ND II)

>/TP l.t U)»/TP HI>/TP ND

• HO« HI> Ntt HI> HO

• ND• HD• HD

PUPIW lit

11/15/88

•-

GNIWI1B-IIIW 118

HBIDHB

HDHD

HBHDHDNOND

NOHIHt

NDHIHIHIHD

NDHDNl

USEPAm HA

18/15/88nEl«l2EU12SI?--

IW lift

HBHDHO

HBHB

NDUHBHONO

HOHDH

NDHDHOHOHD

HDNDHD

fUtn» lift

11/15/88------

GHIWIIft-llIW lift

NDHIHI

HIM -

HtHBHBHONO

HDHDU

NOHIHDHDND

HDNDHD

USEPAnil A

11/15/88HEI9I3£ii?3SI3

IW ft

HDHIHD

HDHO

NDMNDHDHD

HOHIHt

HOHDHINtND

NDHDHD

mn< A

11/15/88----

GHA-llm A

HDHDU

HDHO

HDHDHtHIHI

HDHDHD

HDHDHDHDNO

HDNDNO

USEPARH I2B

11/15/88HE1W£U7<Sit--

NH 121

HBHOHB

NDHD

HBNDHCHOHD

HDHDND

NOHDHIHIHt

HDNO-HB

PftPIW 121

11/13/88

---.

UIWI2B-IIM IJ8

HBHDHD

NDHO

HBHDHBHDHD

HOHDNO

HDNDNtHtM

NDNDND

uSEPftNH D

(BUP Of IW I2B

11/15/88ntlllSEU75515--

IW D

HDk UlHD

NBND

HBHDMHD

. HD

NDNDHB

HDNDNDHDND

NDHDHB

USEPAM 12ft

ins i nSDi

11/16/88NE11I4E(7iBSit-.

IW 12ft

HDNOHO

NDHD

HBHBNDHOHD

HDHDHD

HDHDHOHDND

HDHDHB

PRPKH 12ft

ll/U/88

-.-.

G*!Ui;s-!lnn I2ft

HD3 .0)

1 UlHD

NOND

1.8 UlKDNO

1.) U)NDND

HDHONDHOND

NDNDHB

SUMMARY OF COMPOUNDS DETECTED IN "HOSE I Rl GROUND HATER SAMPLING, WEEPER PIT, LaPRfilRlE IBblliSHIP, SiSCQNSIN

SOURCE PAST/SUPPLING LOCATIuN

USERS CASE NUMBER U5B5DATE SAMPLEDINORGANIC TRAFFIC REPORTSStifiMC TRAFFIC REPORT*CRL SAMPLE NUMBER ,69J51|-iJAaiYN SAMPLE NLT.BER ( i f f - }SAMPLING LOCATIONCHtNICAL

IW B Pin B

£1769SI!

MN B ntl B

?RP USEPA% B flS 4aB

"-I918EW71588

GKB-91M 3 Mil D3B

PRP ?RP bSEPA =RPnit 23B MH 13B R«l 33A ',. 23A

(Su?l

389

P* 83B lii Kt n« 3:A nH 93A

VOLATlLES luij/1)

Nethylene chloride iaicnloroMthine)Acetone1,2-dicMoroethene (cis and trjns)

cis-l,2-dichloraetnenetrans-1 ,2-CichlorGetêne

Chlorotor» Uricr.loroieth.ne)2-butanor,e litettiyl ethyl ketone), IRtM )

l,l,l-trichloroetti«neTnchioroethene (TCEiBenieneTetrachloroethene IPCEi1,1,2,2-tetrichloroethjne

TolueneEthylbenzenelylenes (total)

TlCs (I)l,l-di*ethylcyclohexanetrins-l,2-diiethylcyclohexanecis-l,3-dnetnykyclohexineci5-l,2-diiethylcyclohe«ine

l-ethenyl-2-«ethylbenzene1,2-dicnlorobenzene

NDNDND

NOND

NDNDNDNCND

NDNDND

NDNDNDNDNO

NDNDND

NDND1,2

MNC

NCNDNDNDND

NDNDND

NDNDNDNDND

NDNDNO

NONCNO

L ' J 1

ND

NDNC

1 Ul\cND

1 U)I.B U)

ND

NDNDNDNDND

NDNCND

NCNCND

NDND

NDNCNDtiDND

NDNDND

NDNDNDNDND

NCNDND

N3NCVD

2 , ,.ND

NDND

1 UlNENC

1 Ula. a u)

NO

NDNDNDNDNO

NCNDHU

NDNDND

NSNC

NDND'•DNCND

NDNDND

NDNDNDNDND

NCNCND

NDNOND

NDND

ND\u

ND11 rj

NC

NOND

8.5 Ul

518 UlU (J)9 U)b Ul

U UlNCNC

NDNCNO

1 UlND

NDNSNDNDND

1 (JlND

b Ui

39 U)22 UlND

11 U)

»"36 U)6 Ul

SUGARY GF COMPOUNDS DETECTED IN PriASE ; RI GRCuND HiATER SAMPLING, iWEELER PIT, LaPRAIRIE TOWNSHIP, WISC3NS1N

SAMPLING LOCATION

usEPA CASE NUMBER lasasDATE SAMPLEDINORGANIC TRAFFIC REPORT*ORGANIC TRAFFIC REPORT*Cat SAMPLE NUMBER I89JGZ1-!SftRZYN SAMPLE NUMBER (HP-1SAMPLING LOCATIONCHEMICAL

VOIAT1LES tuq/1)

Methylene chloride (dichloronetlmneiAcetone1,2-dicnloroethene (cis and trans)

cis-l,2-dichloroetnenetran5-l,2-dicrilaroethene

Chlaratoris Itrichlarotetnane)2-butanone [Isetnyl ethyl ketane) , ;"£K1

1,1 , 1-tricnloroethaneTricnlorost-er.e (TCE;BenzeneTetracnlarjetr.ene iPCE)1,1,2,2-tetrachloroethane

TolueneEthylbenzeneXylenes (total)

TICs (I)1,1-dmetivylcyclohexanetrans-l,2-diiethylcyclohexaneci5-l,3-di§ethylcyclohexanecis-l,2-dii»ethylcyclohexafie

l-ethenyl-2-setnyi benzene1,2-dichlorobenzenecis-oc tahydropentdlene

r T r- r. n, AVLr 1CV-U DLHilK

12/26/33ME192UEY772R89--

FIELD BLANK

ND18ND

ND] ND

NDNDNDNDND

NDNDND

NDNDNDNDND

NDNDND

-^Tp n, t,\.yi

(VOA GNLY!

18/86/88

EV773R18--

TRIP BLANK

NDNDND

NDND

NDNDNDNDND

NDNDND

NDNDNDNDND

NDNDND

T i I.U di-Hi^K

18/86/88

----

FflBt-81FIELD BLANK

NDNDND

1 !J>ND

»v n

NDa. 7 (ji

NDND

8.7 U)NDND

NDNDNDNDND

NDNDND

1 FIELD BLANK 2

18/26/88

----

F822-811 FIELD BLANK 2

1 *i1 L

NDND

NDND

ND\jNDNDNO

NDNDND

NDNDNDNDND

NDNDND

T;;F SLAV: :iv'OA GNuVi

18/85/88

----

TB81-21TRIP BLANK 1

NDNDNC

nu

ND

NDNDND "NDND

NDNDND

NDNDNDNDND

NS\8ND

"RIP SLAMs, 2IVGft QV.v}

18/26/S8~ "

----

1 32i ~v 1TRIP BLANK 2

3 !JiND:Sir

'•IDit J

NDV T

NDNDNS

NDNDND

NnUrn

NDNDND

NDNDND

SUMMARY OF COMPOUNDS DETECTED IN PHASE 1 ftl GflOUND DATED SAMPLING, NHEELER PIT, LlPRAIfllE TBMiSHlP, UISCONSIN

SOURCE PARTYSAMPLING LOCATION

USEPA CASE NUNBEfl 11515DATE SAMPLEDINORGANIC TRAFFIC REPORTIORGANIC TRAFFIC REPCRTICRL SAMPLE NUMBER 189JG11-)UARZYN SAMPLE NUMBER Itf-l hiinuiSAWLINfi LOCATIONCHEHICAL Level INCH========================= ============

VOLATILES lug/11

Itethylene chloride ldichloro*ethine)Acetone1,2-dichloroethene Ins and trans)

cis-l ,2-dichloroetlienetrin5-l,2-duhloroethene

Chlorofori (tnchlomiethinel2-buUnone [luthyl ethyl ketone:,!MEKM

1,1,1-trichloroethane 211Trichloroetflene (TCEI 5Benzene 5Tetrichloroethene IPCE' S IP)1,1,2,2-tetrachloroethane

Toluene 2,811 IP)Ethylbenzene 7M IP)lylenes ItoUl) 11,111 IP)

DRINKING UA;ERCR:TE^;A

He.ltTi Adv isor ies

1-Day=;==:===r==;=

11, til

--

--

4,1112,721

--Bl.Ilt

111,111--

2112,111

--

21,111U,lll41, 111

i*-«j Cm id

11-Day;====!======

2,111----

1,8881,318

B, HI

41, lie--

2M2,811

—

3,1111,11141,111

Longer-tert============

—--—------

3,111

41,111---

1,111--

3,111i.eea41,111

Longer-ten============

—----

3,5113,511

--7,381

118,118----

5,211--

11,1113,11111,111

78-<q Adu l t

1.1E-6

DUEL Liletue Level ( C A G )============ =====:;;==== ============

2,111 - 5---

35J352

6m 211

1,881 211388 -- 3.1

1.8588 - 1.7--

11,911 2,1113, tea 7ii63,™ 11,881

TICs (I)l,l-diMthylcyclolie«anetrans-l,2-diiethylcyclohe<inecis-l,3-diuthy!cycloheianecis-l ,2-diiethylcyclohexne

l-ethenyl-2-«etr,yltien;enel,2-duh)orotien:eriecis-octahydropenti lene

L-1: 18' "'••'. "%1

.*Sg$P-:;?: ,

1

11111

..11»

* •1& -1 ,ri- .*•• ',

1V '•;.;•~-f .- •.'•-••"• -.

1 S -

1

•

J| ' SUMtMV Of COtfOUNOS DETECTED IN PHASE

B SOUKE PUTVH' SAKPllHi LOCAIUM

USEPA USE HMKI 11515DATE SMN.EIIHORGAMIC TRAFFIC REPORTIORGANIC TRAFFIC REPORIIC8L SAHPLE NUHIER (B9JGII-IMR1IN SAKPIE IUIUER INP-ISANPLING LOCATIONCHEMICAL

SEKWOIATILES lu|/ll

l.J-dichlofobtoitnt li-dicMorobcnzentl1,4-dkhlorobtRifnc (p-dichlorotenifoelNjpHulwi2-MthyliuptUltotActnipthtflt

DibMiOfurwFlourHiPlwiMtkrntAnthrictntDi-n-bbtylpntluliti

FluorwthmtPyrtntButyl btniyl ptiUiUtlBtmolilintliriCMibit(2-itbylh*iyll»»tlu)iti

CkryMMli-n-octyl plillMliUImiolklllwrMtttMtaiioUlpyrtw

TICs III5-MUyl-2-h<iiflM*1 , t ,2,2-tttrKblorwtliMitUunol, 2-cblorg-, pnoiputt1-tttbyltthyllMiim

l,],S-triwtkylbMUM2,2' -uobii-2-Mtbyl-pr«fMMitriltl-ttkMyl-2-MtbylbMimtI,4-diMthyloctw<2,2,3,4-UtriMtkylpwUnt

•. ij3-ittltyl-5-pri>fyl«w«i<1 -winy 1 - 1 -propmylbmimf2,4,5-tUMthyiBinioic it id4-(l,l-diutliyl)-lwnioic iciotlplM, tlphi beniene«thinol

propinou icid, 2-wthyl-3-hydroiy-

• I eMMO HATER SANPLIW, NHEELER PIT

NOTES

ttTPIP

TPJ

TPJTPJ

TPTPJ

t /TPJ

Piit/IPTPJ«/TPIPJ

P»t/*/TP

TPJPiSt/TPj

TPJTPJ

t*««

•

tttt•

•>t,t

t

USEPAIN Hi

11/15/88I4EI9I1EU7!Sll--

HM us

NDNDNDNOND

IDIDNDMOMD

NDNONDNOH

UUMU

2II IJAIII IJII

NDID

NDIDNOWMD

NONDKll'.!MD

MD

PRPIW III

II/IVB8------

GWINI IB-81N IIB

NONO10NO10

MOIDNDNDNl

MDMDNDMDND

NOID10M

inItNDNOND

NDIINDNDMO

NONDKuWMO

ND

LiPRAlRIE TOMMSHIP, MISCONSIM

USEPAIW IIA

11/15/88HEHI2

£1672SI2

NM IIA

MDMDMDMDND

NONlNDNDMD

NDWNDU

4 U)

NOIDMlNO

2It IJAI

ND13 IJI

M

MDNONOWNO

UDMDNONDMD

ND

PRPW IIA

II/I5/B8--

--GWWIIA-II

W IIA

NDNDNDNDU

ItWNlND

3 IJI

11•NONOID

NDmNDNO

MMNO

IS IJIM

IDIDIDNDND

MDNDMDNDND

NO

USEPAUN A

11/15/88KEI9I3

£1675SI3

IW A

NDNOWNDII

MHM•ma

. M•WH

NiUWNl

114 IJAI

MNtM

MNlUNDNO

MDMDNDMlND

MD

PRPHM A

11/85/88

--

GMA-llNM A

MDMOIDNDID

MDID

•fc*-. M .•. .- •' wNO

NDMHIDla

UHH10

nHMWU

IDNDItUnNOKDMDKDND

ND

USEPAIN 121

II/I5/B8KEHI4EH7(SI4--

MM 121

MDMMDNDND

MDMDNDNOND

HNDIINlH

IINlIDni

II UA)NtNONl

IDIIIIMDID

NDNDMOMDND

ND

PUPW 121

II/I5/B8--

-.6MNMI2I-II

M I2B

NDNDNDND10

NlIIIDNDND

MDMDMD10

2 IBJ)

HUnID

NDWIDIDND

NDNOIDMID

NtNDMDKDMD

MD

USEPAIW D

IOUP Of m I2B

11/15/88HE19IJtunSI5

flN D

NDNDNDMD10

UIDNDNDND

NONDID•DND

NDNDIDIt

1II IJAI

NDNDID

10NDNDNONO

NOMDNOND

1 ND

NO ' '

USEPANN I2A

ins i NSOI

11/14/88HEI911E»)46514

m I2A

NDMDNDMDND

MD10MDNDMB

NDND14ND

• ND

NDNDNDND

113 IJAI

MDIDND

MONDNDKDMD

MOWMDKDMD

' MD

PRPm I2A

11/16/88—

_

GVIWI2A-IIUN I2A

MNDNDMDMD

MDNDNDHO

1 IJI

MOII

19 (JlND

1 IJI

NOIDNOND

MDNONONOU

NONDNDNDMD

M3MDMMCC

ND,i " 2,4,4-lriittliylpwty-l-«stefi-vffltkk

tropMOK ail, 2-««tl\yl-2,2-diMtti»l-l-42-Mruy-l-Mtkyll PI)

iv* '••'•-•iSLiiiii'WjW ys* .t

»

ND

•-

NO

--

ND"

ND

.. .._rL»_*

NO ND

«.». •**..•

ND

....t%..._;

NO

ti S .,

II

.^•^0,,. -

MD

r-

ND

-•

SURRARY OF COMPOUNDS DETECTED IN PHASE I RI GROUND HATER SAMPLING, WHEELER PIT, LaPRAlRIE TONNSHIP, WISCONSIN

SOURCE PARTY USEPA PRP PRP USEPA PRP PBP USEPA PRPSAKPLING LOCATION Ilk i UK B UK B M* 838 Nti )3B RH 838 IM 83A PIH Z3A

USEFA CASE NUMBER 18515DATE SARPLED 18/86/88 1I/Z6/SS 13/86/88 18/26/83 18/36/88 U/86/88 11/86/88 It/16/88INORGANIC TRAFFIC REPORT* flllll - -- RE<918 -- -- NEI9I9ORGANIC TRAFFIC REPORTI EY769 -- -- EY778 -- -- F.V77ICRL SAHPLE NUMBER (89JGII-) SJ7 -- -- S»8 -- -- 589MR2VK SAhPLE HuNBEB (KP-iSAMPLING LOCATION IK B Nil B RU B % 33B IK 838 M 83B R* 83A RK I3ACHEMICAL

SEMIUQiATlLES iu i j / i>

1.3-dichloroDerijerie ;»-;,cniOfOberi ier,e) ND ND ND ND ND ><D 33 241.4-d ich lorotenzene Ip-d icMorobenzenei ND NO ND ND ND ND 34 22Naptnalene ND ND ND ND ND ND ND ND2-iethylnaptha!ene ND ND ND ND ND ND ND NDAcenapthene ND ND ND ND ND ND ND NS

Dlbenzoturan ND ND ND ND ND ND ND NDFlourene NO ND ND ND ND ND ND NDPnenantnrene ND ND ND ND ND KB ND NDAnthracene ND ND ND ND ND ND ND NDDi-n-butylphtnalate ND ND 8.7 IJ) ND 8.8 ;Ji It.9 IJ) ND 8.3 IJ)

Fluorantnene NO ND ND ND ND ND ND NDPyrene ND ND NO ND ND ND ND NDButyl benzyl phthaUte ND i IJ) 1.7 (Ji i.D I IJ) 2 IJ) '.D NDBenzolaianthracen? ND ND ND ND 'JO ND '<D NDDis(2-ethylhexyi lphthalate ND 3 IJI 2 IJ) ND I IJ) 1 IJ) '.5 I iJ)

Cnrysene ND NO NO ND ND ND ND NDDi -n -oc ty l phthaUte ND ND ND ND ND ND ND NDBenzolblfluaranthene ND ND ND ND ND ND NO NDBeniGlalpyrene ND ND ND ND ND ND ND ND

TICs II) 18 6 5 1 1 ND 19 145-Mthyl-2-tiexanone 11 UAI NO NO 15 UAI ND ND 18 UAI NO1,1,2,2-tetrachloroethane ND ND NO ND ND ND ND NDethanol, 2-chloro-, phosphate ND ND NO NO ND ND ND NDl-KthyUthylbtnznu ND NO NO ND NO NO 11 IJI ND

1,3,5-tritethylbenzene ND NO ND ND NO NO II (.1) ND2,2' -azoms-2-iethyl-propanenitrile ND ND ND NO ND NO 25 IJ) 36 (J)l-ethenyl-2-iethylbenzene ND ND ND ND ND ND 15 U) ND3,6-dnethylGctane NO 9 (J) 9 (Ji ND ND ND ND ND2,2,3,4-tctr»etnylpentar.e ND 13 IJ) 12 U) ND ND ND ND ND

3-wthyl-5-propylnor<ane ND ND 9 IJ) ND ND ND ND NDl-«thyl-l-propenylbenier,e ND ND ND ND ND ND 12 Ui dD2,4 ,5- t r i ie thy lbenzo ic acid ND ND ND ND ND NO ND ii U)4-( l , t -d i iethy>)- i>er>iOU acid ND ND ',', ND ND ND I<D I/ U)aloha, alpha benzeneiethanol ND ND ND ND ND ND ID 32 IJI

propanoic acid, 2 - ie thy l -3 -hydro«y- ND 16 IJ) 17 U) ND . 13 Ui ND ND 12 IJI2,4,4-truethylpenty-l-ester

propanoic acid, 2-iethyl-2,2-dnethyl - ND ND ND ND ND ND NO II IJII-(2-hydroiy- l- iethyl) PR

other unidentified TICs 8-43 (Jl 11-23 IJI 17 IJ) - -- - 9 - ;|g ;ji 9-7«| (j|

SUMMARY OF COMPOUNDS DETECTED IN PHASE 1 RI GROUND siATER SAMPLING, WHEELER PIT, LaPRAIRIE TOWNSHIP, WISCONSIN


USEFA CASE NUMBER 125Z5DATE SAMPLEDINORGANIC TRAFFIC REPORT!ORGANIC TRAFFIC REPORTICRL SAMPLE NUMBER (89JG81-)SiARZYN SAMPLE NUMBER (KP-!SAMPLING LOCATIONCHEMICAL

1 ,3-dichlorobenzene (•-dicnlorocenzene)1,4-dichlorobenzene ip-dicr.lorcoenzene)Napthalene2-nethylnapnaleneAcenapthene

DibenzofuranFlourenePhenanthreneAntnraceneOi-n-butyiphthalate

Fluoranthene"VsneButyl benzyl phthalateBenzo'a)anthracer<ebis(2-ethylhexyl!phtna!ate

ChryseneDi-n-octyl phthalateBenzoib! f luorantheneBenzolalpyrefie

TICs (I)5-«etnyl-2-hexafione1 , 1 ,2,2-tetrachloroethaneethanol, 2-chloro-, phosphatel-»ethylethylbenzene

1,3,5-tri ietnylbenzene2,2 ' -azobis-2-iethyl-propanenitnlel-ethenyl-2-iethyl benzene3,6-di»ethyloctane2 ,2 ,3 ,4 - te t rane thy lpen tane

3-«ethyl-5-propyinonanel-»ethyl-l-propeny Ibenzene2,4,5-tr i iethylbenzoic acid4-(l,l-dUethyl)-benzoic acidalpha, alpha benzeneaethanol

propanoic acid, 2-«ethyl-3-r i ydroxy-2,4,4-tr i»ethylpenty- i-ester

propanoic acid, 2-iethyl-2,2-di«thyl-l-(2-hydroxy-l-*ethyl) PR

-n-_, ,.„,•,(,>„*; tioii TITc

USEPAFIELD BLANK

12/26/86MEX92BEY772R39--

FIE^D SLANK

NDnn<tu

NDNDND

NDNDNDNDND

NDNDNDNDND

NDNDNDND

I28 <JA>

NDNDND

NDNDNDNDND

NDND*DNDND

ND

ND

USEPATRIP BLANK!VQA ONLY)

l!J/2i/33

EY773RIB--

TRIP BLANK

NftNANA\Ati A!1rt

NANANANANA

NANANA» A11M

NA

NANANANA

NANANANANA

NANANANANA

NANANANANA

NA

NA

PRPFIELD BLANK

12/26/38------

Faai-uirrri n n, A».yr i CLU Oi.H'i!',

NDNQND>-n:U

<*'J

NDI'A(1U

NDNDND

NDtil<W

NDSDND

ND»m«U

NDND

1NDNDNDND

NDNDNDNDNS

NDND'»U

NDND

!8 (J)

ND

PRP1 FIELD BLANK 2

119/26/88------

F322-Z11 FIELD BLANK 2

NDNDNDt>n,<u

ND

NDNDNDND

Z i. ' "* . O \ J /

N3«>n•1U

4 / I ti \ a /

NDND

NDNDNDND

2NDNDNDND

NDNDNDNDND

NDNDV n(wNDND

ND

ND

PSFTRIP BLANK 1(VGA ONLY)

1U/U5/88------

T38:-21TRIP BLANK 1

NANANANANA

NANANANANA

NANA\- AI1H

NANA

NANANANA

NANANANANA

NANANANANA

NANANANANA

NA

NA

PR?TRIP BLANK 2(VGA CN;J)

12/26/88------

• :-z:TRIP BLANK 2

V. ft"ih

NANANANA

NANANANA-NA

HA•ir-« t'*«

NA\.f\"tr<

NA

NAI. <SI"!

NANA

NANANANANA

. NANANANDv •-."IU

NDNA

NANA

NA

NA

IB-16 (J)

5UMAR4 OF COhPSJKOS DETECTED IN PHASE I Rl GROUND UATER SARPLING, UHEELER PIT, LaPRAIRlE TOUNSH1P, UlSCONSIN


DRINKING NATERCRUERIAUSEPA CASE MJHBER 11515 _____________________________DATE SAMPLED Health AdvisoriesINORGANIC TRAFFIC REPOR7I —..—.......-. — .—.—— — .————— — — ...—-. — — .-.......__._._.._._.._._.ORGANIC TRAFFIC REPORTI It-kq Child It-it) AoultCRL SAHPLE NUHBER (89J6H-) ........................................ —— — .............................................NARZVN SAKPIE NUHBER IMP-) Nj«l«u« I.IE-6SAKPL1N5 LOCATIONCHEniCAL Level IHCLi I-Day il-Day Longer-ten Lonqer-tert UtL nietue Level ICAG)

:,3-oichlorGDen:ene It-dicMa-obenienpi tie IP) 9,ita 9,188 9, lit 38, lit1,4-dichlorober.zer.e (p-dichloro:enier.ei /'5 :3,JJJ IZ.2JS ll,3ii i2,iZ!Naptnilenf2-MthylnapthileneAcenapthene

DibeniolurinFlourenePhenanthreneAnthraceneDi-n-butylphthalate

FluoranthenePyreneButyl benzyl phthalateBenzQlalanthractnebis(2-ethylheiyl>phthalate

ChryseneDi-n-octyl phthaUteBenzolbKluorantneneBenzolalpyrene

1,1,2,2-tetrachlaroethaneethanol, 2-chloro-, phosphate1-Mthylethylbenzene

1,3,5-triuthylbenzene2,2' -azol>is-2-iethyl-propaneiutrilel-ethenyl-2-uthy I benzene3,6-diMthyloctane2,2,3,4-Utratethylper.tane

3-tethyl-5-prop(lnor.ane1-tethyl-l-propenylbeniene2,4,5-triiethylt)en20ic acid4-l l , l-di«ethyl]-6enzoic icidalpha, alpha benzeneiethanol

proparioic acid, 2-«eLnyl -S-hydro«y-2,4,4-trnethylpenty-l-ester

propanoic acid, 2-iethyl-2,2-dnethyl-l - !2-hydro>y- l - tethyl) PR

other unmentided UCs

auRlKS ?HASE 1 Rl GROWS MATtK SAMPLING, FEELER Pii, LaPRAlRlt IG«NSHlP, WISCONSIN

r.t>:Note that all USEPA volatile sample tractions exceeded the required maximum holding tine of 7 days cy IB da»s; therefore all positive results are esunated !J1,

(A) Indicates that a TIC is a suspected aldol-condensation product.(B) Indicates aetcctea in alank and in the satple; possible/pro&ajle blank contamnaiion.(J) Indicates an estimated value.(M Fcr PRP results, irioicates inorganic spue sanple recovery is not «itnin control limts.(R) Indicates data is unusaule.IS) For PRP results, indicates value deterained by Method ot Standard Addition.ty> Indicates interference.NA Indicates not analyzed.ND Indicates not detected; see data sheet (or specific detection hut.TIC Tentatively identified cnesicallsi.TP Indicates deleted in test pit satple!s).TPJ Indicates detected in test pit sanplefsl at estiaated levels.* Indicates detected in groundHater satplels).!2) At the source.(P) Proposed.Lonqer-terii: approximately 7 /ears, or 12). of an individual s liletiee.Li(eti»e: apprcuiriately 78 years.

TABLE 2

ANALYTICAL RESULTS FORPHASE I RI GROUNDWATER SAMPLING


TABLE 2

ANALYTICAL RESULTS FORPHASE I RI GROUNDWATER SAMPLING


I;

L HOWD MTEI SMPLES SUMMV, MCELED I'll, LjPWURlE TOMISHIP, II5COIS1N

1rL

•*

111111

e

I1I11

SOURCE PARTYSAWL1W LOCATION

USEPA CASE IUIKR 11515DATE SAMPLEDIMRMIIC TRAFFIC REPORTIQRCM1C TRAFFIC REPORTIC*L SAMPLE MMEft (B9J6II-)IMHI SMVLE UKKI 1*-)

OCNICAL

1MRMIICS I*/ II

AliuinwtatiionyATM* icbrineItrylliw

CilciuCkrMiuCofelt

InnIt*l>H»iii«RMfWtMRflfCMTV

licit 1PotMfiMItlMiMSilwrSodiiu

TMlliuVM«4i«line

P"Specific cwducUnctIfiptrjturtPtrcnt in lids 111

USEPAW III

11/15/88If 1911EI47ISll-

IIIIID

4.79E-2 (IIM

ID91.8IIItH

I.9K-3 II)M

42.15.41-3 III

H

W1.12 III

NW

4.19

aw

1.79m

PRPIW III

11/15/88--

--BMMI8-II

IDIDIDIDII

l.K-4 IBJ)94.1

I.K-3 III

5 .3

ID1.45 III

HID

5.54

ItM

1.73I.K-2

7.32775B.5

USEPAIW lift

11/15/88KI9I2EI472SI2

—

IDII

2.4E-! Ill4.B9E-2 (III.IE-3 II)

II91.4H•U

NM

41.71.54E-2

U

•1.24 III

I.7E-1 IUIIID

4.14

IDIt

2.52I.K-2 III

PRPM IIA

11/15/88—

--WIWIIA-II

IDIDUMn

2.K-4 INIM.2

I.K-! IllW '•

MIt

52.5IDM

It1.33 (II

MU

5.41

IDID

2.458.K-1 II)

7.391459.1

USEPAIW A

11/15/88IE19I3

E1473Sll--

IDID

2.5E-1 III4.94E-2 IIII.IE-3 III

.-. W91.1

• •U

• M

I.4IE-2 III•

41.9IDID

1.45E-2 IIIMMH

7.12

IDID

I.39E-I

"

PRPB» A

11/15/88--——

SW-II

IDIDMWID

ID94.2

i.K-1 IIIW

*

IIID

44.7MN

n5.5E-I II)

WM

4.2

IDW

I.4IE-IN

7.29BNII. 1

USEPAII 121

11/15/18K19I4EI474SM

—

WUID

4.K-2 II)I.IE-3 III

W91.2M•ID

MM

41.15.1E-1 III

W

n1.39 III

NM

4.M

IDII

7.47E-2M

PRPIWI28

11/15/88———

HUWI2B-II

IDIDIDIDH

2.K-4 IBJ)94

I.IE-3 IIIIDM

IDI.4E-3 IUI

45.7MM

M1.55 ID)

nID

5.31

HIt

7.2E-2 IUIID

7.19815

• II. 1

USEPAm D

(DUP OF W 12

11/15/88NEI9I5EI47SSI5-

IDIDID

5.I5E-2 II)I.IE-3 (1)

ID

IIIDID

WID

42.15.2E-3 IB)

II

ID1.4 IB)

IDID

4.14

IDID

4.47E-2ID

USEPAHI I2A

B IKS 1 USD)

11/14/88HE IS ItlintSI4-•

IDID

1.5E-3 IB)5.I4E-2 IB)

I.IE-3 III

11194.2ItIDID

IDII

41.44.9E-3 IB)

II

ID4.88E-I (III.K-3 IUI3.K-3 IBJ)

14.3

IDID

4.2IE-2ID

PRPHI I2A

11/14/88—----

GMIM2M1

IDIDIDIDII

ID112

I.7E-3 II)IIID

5.K-2 111ID

54.7IDII

IDB.9E-I (II

IDID11

IDID

7.K-2 IBJI4.K-3 III

7.288458.1

LE»»

LIIfIIILIEDII.I

GMXNIMTa

SOURCE PARKSAIVUNt LOUT10I

USEPA CASE NUNIER IttISDATE SAIVLEDINOHGMIC TRAFFIC REPORT!ORGANIC TRAFFIC REPORIICM. SANKE NUMER I89JHI-INARUN SAMPLE NUIBER INP-)

CHENICM.

INORSANICS lKj/1)

AluinuiAntiionyAruoicUriuItrylliiu

CiinutCjlciu*

CokiltCopptr

IronLH4

UPMIRIE TONNSHIP, NISCONSIN

Ktrcury

NicktlPotiMiuSilMiiuSilverSrtiui

Ilulliue.VuudiuliK

pHSpecthc conductanceTiiperiturePercent solids (I)

USEPAMl 1

11/16/88Kill?tinisi;

NONONO

2.HE-INO

NOU7uNONl

l.i?E-2 IIINOJ7

?.32E-INO

NO(.11 II)

NO1.8E-J IBJI

92.4

WNO

2.1E-1NO

PRPny i

11/16/98

--•

Btll-ll

NONONONOa

2. IE-4 (Ul2«J

1.IE-J IIINOH

WNO51.5

8.18E-1NO

NO4.24 II)UNO94.4

NONO

2.25E-I1.4E-2

6.851411II. 1

PRPUK IIDUPI

11/16/88

-—

WB-91

W6.4E-3 II)W

2.3E-2NO

S.K-4 (101191

I.IE-5 II)NONO

NONO57. b

8.I7E-1NO

W)4.1 II)

NONO91.1

NONO

2.3K-Il.tE-2

USEPAW IJB

11/16)88NtiQi nnt ii IDE»77ISIB

NONO

2JE-J IBJN)4.BIE-2 II)7. IE-4 II)

NO89.3HNOW

NONO41.2

2.7E-3 IIINO

NO1.25 III

NONO6.27

NONO

9.BIE-2NO

PRPM IJB

11/16/88

----

WDM3B-II

NONOMMW

NO117

7.K-4 II)MNl

I.7E-I IWIU51.2NONO

NO1.17 II)UNOS.N

NONO

I.UE-1M

7.31745II. 1

PAPUN 138IDUPI

11/116/88

----

UHM3I-9I

NONOIIINlNO

NOIU

9.K-4 IIIHH

t.K-2 IWINO45.4NONO

W1.31 IIIWNO5.S4

NONO

9.K-25.K-!

USEPAIW IjA

II/I4/B8NEI9I9ET771SI9

NOI.4BE-2 18)J.64E-2

3.51E-2 IIINO

NO179U

3.81-3 II)«

9.14NO61.7

I.I5E-1NO

1.29E-2 (II7.24

l.K-J IIJN)5.8E-! IIJI

M.2

NOND

I.45E-I•0

PRPIN I3A

11/16/88

..--

GWM3A-I1

WNO

2.9E-2NO10

NO239

I.4E-3 II)NONO

9.12NO72.19.3£-2NO

NO7.22NONO52.9

NOND

I.J6E-I1.2E-2

4.951541Ir.l

USEPAFIELD ILANt

11/16/88HEI92IEY772RI9

NONDNDNONO

NDNDNONDNO

I.74E-2 (IINONONDND

NDNONDND

3.7BE-I IB)

NDNDNDND

USEPATRIP BLANKIVOA QNLVI

11/16/88

EY773Rll

NAHANANANA

NANANANANA

NANANANANA

NANANANANA

NANANANA

NANANANA

PRPFIELD BLANK 1

11/86/86

..

FBII-ll

NDNDNDNONO

2. IE-4 IBSIND

3. IE-4 IB)NONO

5. IE-2 IB)NDNDNDND

NDNDNONDND

NDNDNDND

7.52'1113.1

PRPFIELD BLANK 2

18/86/88

--FBI2-II

NDNDNONDND

NDND

3.K-4NDND

1.IIE-1 IBN)NDNDNOND

NDl.OE-l IBN)

NONOND

NDND

1.8E-2 IB)ND

7.72(1813.1

ILIL.

LIIIIIILItIIIII

GROUND WTER SABPIES SUNWWH, NHEEIER PIT, LiPRAUIE lONNSHIP, Ml SOWS IN

SOURCE PARTISAWUN6 LOCATION

USEPA CASE NUMBER 11515DATE SMPLED1NOR6ANIC TRAFFIC REPORTIORGANIC TRAFFIC REPORT!CRl SARPLE MmBER (B1J6ll->

SMW.E NUIIBER I HP- 1

CHEHICAL

IMR6MICS 111)/ II

AluinuiAntiKMyArsenicBiriulbrylliui

CidiiwCilciuiCtirMiuiCabiltCopptr

IronLtid

Itercury

Kickcl

StlmiuSilver

TlulllIVanidiuUK

pHSpecific conductanceTwp<r«turtPirctnt solids ID

DRINKING NATE8CRITER1A AKB1ENT HATER DUALITY CRITERIA

(UxtiulContiiirtintLt.ll IIKL) I-DJ(

I.IJI3 3.1

I.IK 1.141

I.IH I.I

i.m i2)

I.M2

1.1

HeilU ftdvisones

ll-kq CMId

ll-Dif Lonqer-teri Lonqer-ten

S.I 5.1 J.I

1.141 I.M5 1.121

t.l 1.211 I.8N

l.lll l.lll

:: ::I.I I.2N I.UI

71-kq Adult

DUEL

|1.121

i.m

i.iu

i.ml.tM

Innciti

l.lE-i In^fStinqCincer Risk liter 1

Liletlie level ICAGI Qrqanius

1.146I.HI 5. IE-5

5

I.MS -- l.ll

I.IH - US

1.131 1.15

I.H2 -- I.44E-4

I.2H -- I.IU*

Protection ol HuMn Heiltx

Protection Circinoqenicity Protection II)

Inqestinq Inqestinq InqestlnqOrqintsis riiter i Orqanisfts

Only Orqiniiis Only

432.2E-4 I.75E-5

1.7E-4 6.4IE-5

--

-

I.44E-4

I.I

1.151

1.22 1.22

21

1.73 1.73

l.ll1.15

1.113

1.2

I.I4B

E

L

I

LLIIIII

SOURCE PMTtSMVUNG LOCATION

USEPA USE NUMBER 11515DATE SAWtEOIMMGWIC (DUFF 1C RtPOHTIORGANIC TRAFFIC REP08IICRL SAHPIE NUHBER (89J6II-1NARHN SAHPLE NMBtR INP-I

CHEHICAL

VQLAI1LES lui)/l>

ChloroMthaMIroMMthutVinyl cilorideCMorwUlntNfthyltne chloride

ActtoneCarton disulhdel,l-«ichloroetl«ne1,1-dichloroethaoe1,2-dichloroetlwne

Chlorofon1,2-duhlorottliane2-tutwai»1,1,1-trithloroethaneCarbon tetruhloride

Vinyl acetateIroMdichloroMthane1,2-dichloropropanttrans-l,3-dLchloropropeneTrichloroethene

DibroMchloroMthwe1,1,2-tncnlorotthaneIMIMIcii-I ,1-dichloropropene2-cnloroeth»l»iiiylBther

OnwHori2-htianonet-Mtkyl-2-ptntanoneTetracMoroethene1,1,2,2-tetrjcbloroethane

TolueneChlorobenzeneEthylbenieneStyrenelylenes 1 total 1

HCi (II1,1-diMttiylcyclotienanetrani-l,2-dlwthykycloheianecii-l,)-diMthylcycloheianecii-l,2-ii«thylcycloheiane!-ethenyl-2-Mthyll>tniene

USEPAim in

ll/lb/86HE miEI4MSll--

MlNDNDWND

8 (11NDNDNDND

NDNDND*DND

NDNDNDNDND

NDNDNONDM

NDNDND•0

ND (II

1.4 111NDNDNOW

NDNDNDNDNDND

PBPIW (IB

II/I5/BB--

--6HIWI1B-II

NDND*DNDND

NDNDWNDND

NDNDNDNDNO

NDNDNONDNO

NDNDUNDW

NDNDNDNDND

NDNDNDNDND

NDNDNONDNDND

USEPAUN IIA

11/15/88KE1912

E1672512--

NDNDNDNDNO

NDNDNDNDND

NDNONDNDND

NDNDNDNDND

ND•DNDNDNO

NDNDWNONO

NDNDMONDNO

NDNDWNDNDND

PRPBN B1A

IB/IS/SB----

CNHWIA-BI

HONDNDNOND

NDNDNDNOND

NDNDNDNDND

NDNDNDNOND

NONDNDNDr>

NONDNDNDND

NDNONDNDND

NDNDNDNDNDND

USEF-AIU A

18/15/88nmi3EH7:SB:--

NDNDNDNtND

«DNDNDMND

MWNOWW

NOWNDNDND

NONDNDWm

nmNDNOND

NDNDNDNDND

NONDNDNDNDND

PRPM A

11/15/88—

--GNA-II

NDNONDNDNO

NDNOND«DND

NDNDNDNDND

NDNONDNDND

NDNDMND7?

NDNDMNDND

NDNDNDNOND

NONDNDNDNONO

USEPdIW 128

11/15/88HEHUEI4?«Sl<--

NDNONONDND

NDNDNDNDND

NDNOWNDND

NDNONDNDND

NONDNDNDNA

NONDNDNONO

NDNDNDNOND

NDNDNONDNDND

PRP(IN B2B

11/15/88—

BNWB2B-BI

NDNDNDNOND

NDNONDNDND

NDNONDNDNO

NONDNONDND

NDNDNDND77

UNDNDNDND

ND• ND

NDNDND

NDNDNDNDNDND

USEPAW D

IDUP OF UN 121

11/15/88itimEI4J5S15--

NDNDNDNOND

t (11NDNDNOND

NDNONONDNO

NDNDNDNDND

NDNDNDNDNA

NDNDWNDND

NDNDNDNDND

NDN« .NDNDNDND

USEPAW B2A

INS 1 HSDI

11/14/88KI9I1E1748SU--

NDNDNONDNO

NONDNDNDND

NONDNDNDND

NDNDNDNDND

NONDNDNONA

NONDNDNDND

NDNDNDNDND

NDNONONDNOU

PRPNN B2A

11/14/88..-.--

GNIW02A-BI

NDNDNDNDND

NDNDNDND

3 U)

1 UlNDNDNDND

NDWNDNDND

NDND

B.B (JlNDNA

NONONDNDND

0.7 U)NDNDNDND

NDNDNDNDNDHO

13333 33333 S3S33 383SS 33333 33333 3333SS

! 3 3 3 3 333! !33S 33333 33333 33333 33333 33333S

!3S3 33333 33333 33333 33339 33333 333: ! 331

. a SE s :~ 5 13333 = 3333 3S3S8 85333 33833 38333 33333 33388C

3 T33333 33383 28333 38838 8338£ 33833 53333 333381

j3 illif s£< 33383 83838 3881* ***** 8*83* 33833 3333

33388 33»88 88888 83888 88881:: 38383 833SS 3838*4

3 3 3 S 8 388*8 3388* 88388 8338 fc 83883 S3 33 3 38<

SE SUJe/1 -m

3 55<• »• *••» w U4

33333 33338 ***** 8983* 3*338 33833 33333 33383f

, T 33338 33888 5*888 88838 3 8 5 3 F: 83833 ^3^33 333331

33838 33883 88*8* 88*88 3388£ 38333 S3SS3 SS33SS

ia 35SS ' 3833* 88*88 8888* 38888 3*8** 3*933 33333 338S3f

aa

Sit«aSi

II *

iiiiiumuiUiiiiliniiii.ilUilliiit!£ 2 S.S £2,.

a I i '

-*?-—: ' '• r»-

S

CJ

1UJi1i

^

oe

I

iI

5WP1

1K6

LDU

UIM

IKFP

« CA

Sf U

UC

I II5

«S

Jc

Jo

1i

O

i=^

_

0

o

c

,3

1io

I2

1

20

•f~"

!|r*l|• CJ

Ol C C

• - it! h 2

J3j-

r s ~ll1

f - s£.-21— ^ o

.

i

«

r

I

*"™

j.-

iii= !^K B >3 w

U — 1

si

- - S : 2 i i ^ i i i i - x : : ?

, , , 2 ,; i : : ; : ; ; ; : : : : : : ^ '•

MM: M M M i M s * :

M i : i M 2 i : gg i i gin

S ; i i M S» 1 S!|f

: : - ll M i M M i llj--— • r^» -r

33 M 1: i 33 !il{|« ^. — — — m

: I ; S ; ; 3 ; ; 35 ; 3 Hi* • *• v- * I ; 1 f v

i

i _| I t I I I I I I I ! ' r f l l S w *

1

i1 I I

!ji ! i= 5 1 * 1 • g .

1 , ! iHlil J|flli/t *^ ^ — ' S m -—I — . - - — . - T <x —• 3 '"^ Û J U ^ i . A C ^ ' S — • . • ^ 4 = — > * M O J C O k * «

^ — 8 c" — S '•i k_ -!- — CM "^ — . fsi ^ — t.;«. £ «S ^ 1_> J? «i (_> —— —— — • t-J —— ri —— U

: e : : ; = 5 : ; ^ : : g5 : : ; :

. z . , 1 - . 2 3 3 , , z , , a s , , , , ,

5 S , S S 38 , ,: • : : - . : : : : - . : i : i : : -. -. s_ : :

: : ; s : i i i s i i i : i ; * s 5 : :

•

: : : =1 : t i i : i i i 3 i ||M.| :

M,, ; MM, M: | . ||lS§yi -. 3 i--> r- —

i : : a : i i i : i i : : 3 i i : 22 =_ „, _ „

M*,: i ISM i i iii 3133!°* !•*»—> r-t rw -i-

, . , - . . , _, . i is!..,„- S - -SST

i - i• . - ! ^ . . « , . , , , _ , J ' a ~ S _ '

f>7 *^ —

S s ' i — Iii"* •sl^^S l s * I ?l . |TSo ^^r' i2 lS l ^_ J55 t55 t ^ l J C -• ^t. S !S V w ' ^ 5 I r is^^-î'

J 3 C.B B.-3

UOUW HATER SftWlES SUMMV, HHEELER PIT, LaPRftlRIE TOHNSKIP, 111 SCONS IN

L

LLEILLI[LLt

SOURCE PARItSANPL1N6 LOCATION

USEPft USE NWIKR 11515DATE SMMEDINOKDN1C TRAfFIC REPORTIOReANIC TRAFFIC REPORTICRl SANPIE NUHIEft IBfJUI-lNARHN SIMPLE MMBER IHP-)

CICNlCftl

SEniVOUTlLES

Phtnolkisl2-cklorotthyl)ithtr2-cHorotktMl1.3-dicklwabNiifli (i-dichlorobMiHtl1.4-dicklorokoiitni Ip-dichlorokmiMtl

Itftzyl ilcokol1,2-dickloroktnitnt (o-dichlorobMinifl2-Mthylpknol

n-nitrou-dipropylMintHtiachlorottluntNitrobtnintlupkoront2-KitrofktMl

2,4-4iMtkylpl>MOlItnioic ic idbiil2-ch>trttko>)>iftl)ini2,4-dickloropktMl1,2,4-tricklorokmiMt

Hiptktln*4-chlwowiliMHtiuklwoknUdim4-cklwo-I-Mtkylpkml

lpar*~<kUri)-Mti-f riiol I2-MtkylM|tluliM

7,4,4-tncMofOphMol2,4lS-tricklorofhMCI2-ci>lor<»iptki)Mt2-nitrawiliM

Diwtkyl phthilittftctnaptkylntl -ni trouil int

2,1-linitrophenol

USEPANH III

11/15/88KI9IIEI47ISll

HHDHOHDU

HIHINDHOHI

NDNlNlUnNlNlNOHONO

NOHONDHI

ND

NDNDNDNOND

NDNDNDNDND

PRPUN 111

11/15/88--

--BNKNI IB-11

NlNONONlHI

WHDNDNDND

NDNDNDNDHO

NDHONDNlNl

HIHINlHO

Nl

NlNDNDHDNl

NDNONDNDND

USEPAIW lift

11/15/88NES9I2EI472512

NDNOHINONl

NDHDHONDND

HONOHDHDHI

HDWNONDNO

NDMWNl

HI

NDNDNONDM

NDNDNONDHD

PRPIW lift

11/15/88—--

UHMIA-II

NDHDHINDHO

NDNDNDNDND

NDNONDNDHO

NDNDNONOND

HDHOMNt

NO

NDNDNDNDND

NDNDNDNDND

USEPAIW ft

11/15/88HEHIJEU73Sll

NDNONDNDND

NOHHNlU

NONONlNDH

NONlNlNDNl

NlHDMM

U

NDNDNDNDND

NDNDNDNDND

PRPHN A

11/15/88----—

6NA-I1

NDNDNDHDND

HDHDHDUHI

NONDNlNDHI

NOMNlNlNO

NlNOMNl

HD

NlHDNDNDND

NDNDND

• NDND

USEPftIW 121

11/15/88NES9I4

E1474514

NDNONDNDNO

NONDNDNDND

NlHINDWW

NlWNOUW

NOMNlNO

HO

NOHONDNDNl

NDNDNDNDNO

PRPIW 120

11/15/88—--

6MWI2I-I1

HDNDNDNOND

NONDNDNDND

NDNOHOND•

HIHIHIHINO

HIHO•HI

W

NDMNDHONO •

NDNDNDNOND

USEPftIW 0

IDUP OF IW 121

11/15/88HE IS 15EI475SI5

NONONDNDND

NDNDNDNDHD

NONONDNOM

NDNOHINDHO

HONDNONt

ND

NONDNDHDND

HDNDHDNDND

USEPftIW 12ft

(US 1 USD)

11/14/88BE 11 14

EV74BSI4

NDNDNDNDND

NDNDNDNDNDNDNDNDNDNONONDNOMlNO

.NDNOHDNDNDHIHINDNDNONDNDNDNDNDNDNDNDNDNDHI

PRPUN i2A

11/14/88----—

6NIWI2A-II

NDNONDNDND

NDNDNDNDND

NONDNDNONO

NONDNDHDHO

NDNDMND

NO

NDNDNONDND

NDNDNDNDND

III3EIIIIII£IIIIIII

GROUND M1ER SAWLES SUIWMy, NHEELER PIT, LjPRAIRIE TOWNSHIP, N1SCDNSIN

SOURCE MHiySMtPUM LOCATION

USEPA USE NUBIER IKKDATE SAtfLEIINORGANIC TRAFFIC REPORTIORGANIC TRAFFIC REPORTICRl SAWIE NUKBER I89J6II-INARHN SAWLE NUHBER (HP-1

USEPAUN I

PRPIW B

PRPKM BIDUPI

USEPAM I3B

PRPmi us

PRPUN UBIt UP I

USEPA PRP USEPA USEPA PRP PRPUN I3A M ISA FIELD BLANK TRIP BLANK FIELD BLANK I FIELD BUNK 2

IVOA DNiyi

ll/li/BBHEI917EW9si;

11/14/86

6NB-II

11/14/88

GNB-91

U/16/US ll/lt/BB 11/16/88NEI918

SIBGWWIJB-II G«WI!B-91

ll/fe/B8 ll/lb/BB

SWINI3A-U

EY771SI9

U/lt/iaIIEI92I

Ey77?RI9

EV773fill

ll/lb/BB

fBI I - I I

Uitd/fib

FBIMI

CHEI1ICAI

SEKIVO.ATILES luq/l)

Phtnolbtttf-cklofwtfcylltthtr2-clilorQpb*Mll,!-»icHofot»ni«i« li-4ichlorob«ii«iil1,4-dUklorgtMiMt Ip-liclilorobmmil

Idllfl »lCOl»l

l,2-dickli)fOb«iiM lo-dicblorobnttnt)2-MthylphMolti>l2-chloroiupropfHtthtr(-HthylpkiMl

o-nitrou-<ipropyluinfHtuchlorMtluM•itrobMiMwItapkoroM2-nitriflHMl

2,«-diMUylpkMelItoioic Kitbiil2-tiiloritl»xylMtbwi2,«-dicbloropMnal1,2,4-tricblorobMiMt

Mptlulwt4-chlviwihmHtiukloroliitMiMt4-t»lwo-5-Mthyl|il»ni)lIpira-cliloro-wti-criul 1

2-HtkyluptlulMi

H»KKloriKycloptnUdicnt2,4,4-tnctilorophenol2,4,:-trichloroph«uil I2,4,J-TP)2-tnloronipltnline2-nitroMilint

Diwthyl phthiUUAcenjpthylentJ-nitrauilintAccfitpthene2,4-dinitroptienol

DOUWNOND

NluuNtID

mNOMHI11MUNONONO

NONDNOND

NO

NtNDNDNDND

NDNDNDNDNO

NONDNONDND

NONONDNDND

NOMNONONt

MNONDNDNO

NONDNlND

ND

NDNDNDNDNO

NDNDNDNDND

NDNDNONDND

NONDNDNONO

MNDNONONO

MNONONDND

NDNDNDND

ND

NDNDNDNDND

NDNDNDNDND

NDNDNDNDND

NOUNO

NDUNONDND

NDNDWNt

U

NDNDWNDND

NONDNONDNt

ND IIND NND «ND IIW N

WNOMNlNl

UNOH•M

WNDNOU NNl N

HO NH NU NM N

ND N

ND NND NND NND NND N

ND NND NND NND ' NND N

D ND0 NDD ND0 HD 14

NDNDNDNDNO

MNOUHW

NlWNt

0 NOI M

0 NtD NOD H0 M

D U

0 NOD NDD NDD NDD ND

1 NDD ND9 NDD ND1 NO

NDNDND2422

NDNtNONOND

NONDNDNOW

HNtMNDU

NONDNOM

U

NONDNlNDNO"

NDNDNDNDNO

NDNDNDNDND

NDNONONDND

NDNDNDNONO

NONDNDN9ND

WNlNlNO

ND

NDNONDNDND

NDNDNDNDNO

NANANANANA

NANANANANA

NANANA

. NANA

NANANANANA

NANAWNA

NA

NANANANANA

MNANANANA

NDNDNDNDNO

NDNONDNDND

NDNDNDNDND

NDNDNDNDND

NDNDNDND

ND

NDNDNDNDND

MNDNDNDND

NDNDNDNDND

NDNDNDNDND

NDNONDNDND

NDNDNDNDND

NDNDNDND

NO

NDNDNDNDNO

nNDNDNDND

GRDUW MTCR SIMPLES SUtHWWY, IKELER PII, LaPRAIRIE TOMSHIP,

s1r.jf!U

111111

SOURCE PARTYSAWLIW LOCATION

DR1HK1IIS HATERCRITERIA! USEPA CASE NUMER 11515

tATE SMPLEt Health AdvisoriesIMWBANIC TRAFFIC REPORTI .......„....—.........-..-.......................-...........—.....—.-....OR6MIC TRAFFIC REPORTI ll-tq Child 71-kq Adult

MRZYII SMPLE NUMER IHP-I KaiiluiContaminant

CHEHICAL Le.el (KL) 1-Day 11-Day longer-teri Longer-ten DUEL Uletiie

SEIIIVOLAIILES lug/1)

Phenolbnl2-cl»loro»U!yl)«tl»r2-chloropmnol -- -- - - -- 2111,3-dichloroteritne li-diclilorolxnienel ill IP) 9,IM 9,111 9,111 31,111 3,111 6Ml,4-diclilorob<iiiini (i-dichlorotunieflil 75 II, Nt 11,111 11,111 41, IN 4,111 75

Bwiyl alcohol1,2-ticklorotmtn* lo-dichlorobtnientl 6M IP) f,MI 9,111 9, III 31, IN 3,111 6N

j bisl2-cMoroiupropylletherj 4-itUylphtflol

n-nitroso-dipropylaiineB».achlor«thineNitrottnicMUophorone2-nttropktnol

2,4-diMthylph»nolImioic acidbisl2-cliloritlwiy)wthanf2,4-dichlorophwol -- - -- - - III1,2,4-trichlorottflitM

Toiicity

I.K-6 IngestingCancer Risk Hater 1Level ICAG1 Orqanisis

3,511

411411

411

34.7

19,8115,211

3,191

AHBIEfT HATER OUALI1Y CRITERIA

Protection of Huian Health

Protection Carunoqenicity Protection 111

Ingesting Ingesting IngestingOrganises Hater t Orqanists

Only Orqanisis Only

749, Ml1.13 1.36

2,6112,611

2,6M

4,341

1.9 8 .742,131,111521,111

24, 5H

I

II

4-chloroanilineHtiKMorobutadiMe4-cliloro-3-i«thylpl>enolIpara-chloro-Mta-crisol)

2-HtkylMftlialtni

Heiachlorocycloptfltaditne2.4.4-trichlorophenol2.4.5-trichlorophenol 12,4,5-TP!2-chloronapthalene2-nitroanalint

liiethyl pnthalateActnaithylene3-nitroanihneAcenapthene2,4-dinitrophenol

1.15

51 IP) 211 ill 71 311 311 31

313,111 2,111,111

71 -14,311

1.45 5»

216 14,8113 -- -- 1.2 3.6

2.6E-3 3.IIE-2

SROUM HATER SMIPLES SUWARt, UHEELER PIT, LiPMIRlE TONNSH1P, HISCOHSIN

tLi1IIIILI

~f -

I

I

I

I

SOURCE PARTYSAWIHG LOCATION

USEPA CASE NUHER IIHSMTE SAIW.EIHKMGAHIC TRAFFIC REPODTIORGANIC 1IAFFIC REP08TICRL SAHPIE WMBER I89J6II-INMHH SAHPLE HUMER IHP-I

CHEKICAl

4-nitropbMolDibMioturM2,l-di»itrotolutnt2,i-diniUotolu«ii«

USEPAIN III m III

4-cMoropli*nyl ptwiyl ithtrFlourtnt4-MtrMiuliM4,6-4initro-2-Mthylphnol

ll.i-tfimtro-ortlu-criwlln-nitrolodiplwtyluini

4-brMoplmyl phtnyl ittorHtiuhlorobMitntPtntachloroflttnol (PCPIPhmMthrtMAntkrKwc

l>-n-kutylpktluUtiFlwrMtkCMPyrwtButyl tmiyl plitluliti5,1 -tuliloroMnllllint

IwulilMUrKMtbitl2-*UyH»iyllplitlultti

li-n-octyl plttuLjtt

iMioltlpyrmluliMll,2,S-c,dlpyrtM

Itniol), k,ilptrylt<i>

HCs (II5-«eth(l-2-h«<»o(i>1,1,2,2-tltrKklorMthineithml, 2-chloro-, phosptKlel-MUiylithylbnzrnel|!,5-tMMth»ltiMiinf2,2 -iiablt-2-Mtliyl-pro|iinetutriltl-tthMyl-2-wtliylbnttntl-Mtkyl-l-propwylbtnitntll*U»r yni«Mtilii4 (ICt

i*iilMtifit4 TICi

11/15/88Klfll

£1471Sll

IIIHDIIIIIIIII

HOIIINHI

NO

IIIMIIIHDMl

UUinHHI

IIIIII

NDHIHIN9HI

2II UdlII (Jll

NDNDNDNDND

11/15/68

GWIM1I-II

IIINDNOIHND

NDIIIIIINO

KBHONDNDU

IIIHOMlIIIU

IIIIIIIIIIIIM

NDHIWHIND

NDNDNONDNDNDNDNOND

US£P«IW I1A

11/15/88HEIS12EH??SI2

NDNDNDNDNO

HINDHIHI

HI

HIHINHIM

•HIMHIHI

HIt IJIHIHIHO

HINDHINDHO

219 IJAI

ND13 UlNDNDHONONO

PRPIW IIA

U/15/88--

GNHMIA-II

NDNDNDND

- ND

NDNDHOHI

HI

HIHIHIHIHO

I U)HIHIHOHI

HIHDHOHIND

HDNOHDHDND

HONONDNDHDNDNONOND

USEPAUN A

11/I5/B8HE 1913[16)3SI3

HDNDNDNDHD

HINDHHI

HI

HO

HI

HIHIinHIND

HDNDHDNDND

14 IJA)ND»0NOND«DNDND

PRPIN A

II/I5/B8

—

MA-11

NDNDHDNDHI

NDHDWHI

M

HDMMHHt

HIHIHIHIHI

HIHIUHIHI

HIHDHDmND

HONDNDNDNONITHDHDHD

USEPAHH 128

11/15/88HE1?I4EI67<SM

NDNDHDNDM)

NDHDWHI

HI

HOHDHOHINO

HIHIHIWHD

HIHIHOHIHI

HIMHIHIHD

LII IJA)

NDNOHDNDNDNDHD

PUPNH 121

11/15/88----—

EUHNI2B-II

NDNDHDNOHO

HDHDHIHI

HI

HOHOHOMHI

•HIHI•Ht

HO2 IWIHIN«

HIHIHIHOHD

NDNDNDNDNDHONDNOND

USEPAm D

IDUP OF M 128

11/15/88HEI915[1475sn

NDNONONOND

HDNDHIM

ND

NDNDNDHOND

HDHDHDNDHO

NDHIWHIHI

HINDHDHINO

1II IJAI

NDNDNONDHIHDND

USEPAIN I2A

(US 1 ItSOl

11/14/86B[HI4ETUISI6

NDNDNDHDHD

HDHDNDND

HD

NDNDNDNDND .

WNDND11HO

HDHOHDHIHO

NDHDWNOND

1n u«)

NDNDNDNDM'«ND

WPUN I2A

11/14/88—

GHMI2A-II

HDfcONDNDND

NDHDHDND

HD

NONONDNOHD

1 (JlHINDIfNO

ND1 IJINDHDHD

NDNDNDNDND

WNDNDNDNDNDNDHIHO

6KOUM HAfER SAMPLES , MCEl£R Pll, l*PSfll»l£ TCMNSHIP, NISCONS1N


USEPA CASE NUMER 11515DATE SAItPLEOINORGANIC TRAFFIC REPORTIORGANIC TRAFFIC REPORTICRL SAMPLE NUMBER I89JGII-INARiVN SAMPLE NUIIBER INP-I

CHEMICAL

4-iutrophtnolDibmiolurw2,4-dinitrotolimt2,4-dinitrotolutotOittliylplitlulitt

4-chlorophMyl phcnyl itkcrFlournt4-nitroiHilini4,i-di»itro-2-Hthylpl»nol

14,4-dmtro-Of tlw-cr»sol In-nitrM«liplK«yl»int

4-broaoplmtyl plttflyl ttlttrHtuchloroliMtniPnticMoroplwaol IPCPIPhdunthrtM

USEPAM I

POPMl B

POPIW I

(DUP)

Di-n-butylpl\tkil»tfFluorwtlwitPyrwiButyl bMiyl plitlulitiJ.J'-dicMorrtBiiiilini

blt[2-tlkyl>»iyl>pMlulittChryttMDi-ii-Ktyl pttluliUiMiolkllliierwtkwi

tnuolilprrml»<MO<l,2,J-M»p»riMDib«izl<,tlwtliriciMBM!o<|,k,i>p«rylm

HCs II)5-wthyl-2-ktiMonf1,1,2,2-UtrKhlorofthjntttkuwl, 2-ttloro-, pkosplutt1-MttiylttliylbMini1,3,5-triMthylbtfiitnf2,2 -iiotiis-2-wtliyl-pro|unenitriltl-fthMyl-2-wthylb«>»nt1-Mthyl-l-propMylkmimII otktr MidMtilitd HCs17 oUtr MitnttfiH TIC>

11/14/68MI9I711 U?517

NOUNDNDW

NONDNDND

NDNDNDNDND

NONDNONDND

NDNONDNDM

MUND

IBII IJA)

NDNDNDNDNDNDND

1-4] U)

1I/I4/BB

GNB-BI

NlND

NDNDNDW111

NDNDND

I IJIND

HII U)«DMND

NOHONOWW

NDNDNDWWNONDMW

Il/l6/8fl

GKB-91

NDNDNONDND

NDNDNDND

NDNDUWDO

1.7 IJINDNONDND

W2 (Jl

NDNONO

NDNDNDNDND

NDNDNDNDNDNDNDNDND

USEPdIW 13B

11/14/88M19I8£1771518

NDHINONDNO

IDWNONO

W

WNlNOHIU

NONDNDNOND

NDNlNDNDNO

•1WNlNODO

115 IJAI

NOWNONDNONONO

PRPIW 11!

11/14/86

..--

GWWIJB-ll

NDNDNDNDND

NDNDNOND

NO

NONDNOMU

1.8 U)NOND

1 IJINO

NO1 IJINDNONO

NONDNDNDND

NDNDNDNDNDNDNDNDNO--

PRPIW 158IDUP)

ll/lt/88

..--

CNIWISB-fl

NONONDNONO

NONOWU

M

MNO•WU

1.9 IJINO•

2 IJIND

ND1 IJINlNlHI

NlUNlNDND

NDNDNDNDND-NDNDNDND—

USEPAUN lift

1I/I4/8BItEHUEV77ISI?

NDNDNDNDND

NDNONDND

ND

NDNDNDNDND

NONlNONONl

UNlNlMM

NlWMNONO

HII IJAI

NONO

II IJIII IJI25 IJI15 IJI12 IJI

1 - IN IJI

PUPm I3A

11/14/86

--WKNIU-II

NDNDNDNDNO

NONDNDND

ND

NDNDNDNDND

1.1 U)NONDNDND

NO1 U)NOMNO

NDNDNDNDND

NDNDNDNDNONDNDNDND—

USEPAFIELD BLANK

11/14/88ttlWIEV772RI9

NDNONDNDND

NDNDNDND

ND

NDNDNONDND

NONDNDNDND

NDNDNDNOND

NDNDNDNDND

121 IJAI

NDNDNDNDNDNDIII—

USEPATRIP BLANKIVOA ONLY)

11/14/88

E»773Rll

NAHANANANA

NANANANA

NA

NANANANANA

NANANANANA

NANANANANA

NAMNANANA

KANANAHANANAIM

• «ANA--

PUPFIELD BLANK

11/14/88

_.—

f 811-11

NDNDNDNDND

NDNDNDNO

ND

NONDNDNDNO

NDNDNONDNO

NONDNONDND

NDNDNDNDHi

NDNONDNDNDNDNDNDND.-

PRP1 FIELD BLANK

11/16/86

--F 812-11

NDNDNONDND

NDNDNDND

ND

NDNONDNDNO

NDNONDNDND

NDWWWNO

NlNDNONDND

NDNDNONDNDNDKDNONl--

SOUND MTER SMPIES SUIWMr, HHEELEt PIT, liPRAUlE IOKKSHIP, HI SCONS I*

SOURCE PMITSAHPLIK IOCATIW

USF.PA USE IWKR 11515DATE SMPLEIIMK6MIIC TRAFFIC REPORT!ORGANIC TRAFFIC REPORTICRL SAHPIE MMER (89JMI-IMR JO SAflPLE MJKBER IMP-1

CHEHIML

ORIWIN6 WIEBCRIIERIB MIIIENT MIER QUALITV CRITERld

4-nitrophtnolOlbtoiolurin2,4-dinitrotoltiene2,6-dinitrotalMMtietkylpktlulite

4-chloroflwyl ptmyl ithtrFlourtflf4-nitroMilin*4,6-<initro-2-Mtliylph«nol

l4,4-«initro-ortho-cr»Ml In-nitroMdiphMylMint

4-broMphmy) phnyl itl»r

Ptntidilorophcnol (PCPIPhNwthrmi

li->-butylphtluliUFluorwtkmiPyrtmButyl bMiyl plitluliti

iHIOlllMthrKiMHl(2-ltkyld»iyllp»tl«UttCkryMMBi-t-Ktyl phtmiittlw»lt)<lwrHtlii«

DibMila.fcluthrutntB«iiOlt,k,i)pirylKii

TICs II!5-«tthyl-2-(i««non«1,1,2,2-tftrachlorocthii*tttanol, 2-ckloro-, phosphite

1,3,5-triMttiylbtnltnt2,2 -iiotiis-2-Hthyl-prapinenitrilel-tttwnyl-2-ntliylttniNe1-Mthyl-l-propnylbenzenellotktr iwidtntifitd TlCt17 otktr iHUeatifitd HU

Keilth Advisories Protection of

ll-kq Child 71-kg Adult loucity Prottctun

Diiiiui l.lE-i Ingtstinq InvestingCoatuinant Cincer Risk titer 1 OrganistsLcvil IHCI.) l-Diy iB-Diy Longer-ten longer-ten DUEL Li(eti» le»el ICAG) Orgwisis Only

—

351,111 1,811,111

-

13.4 7k5

-

•- 51 51 51 211 11 - I.B22H IP) 1,MB 3N 3BB I,BN I,*M 2N - !,lll 29.4J1

——

3,4N 154,11142 54

—

--

..

1,511 5,IM—

--

..

..----—

Huun Kejlth

Carcinoqenicity

Ingestingniter 1

Organis«s

l.ll

-

2.BE-J

4.9

7.2E-4--

2.BE-32.8E-3

..--

2.8E-3

I.B3E-2

2.BE-3--

2.BE-3

2.K-3

2.IE-32.BE-32.BE-32.8E-32.8E-3

Protection III

IngestingOrginisis

Only

9.1

-

3.I1E-2

-

16.1

7.4E-4--

3.IIE-23.I1E-2

--3.I1E-2

2.I4E-2

l.HE-2—

J.IIE-2

3.I1E-2

3.IIE-23. HE-23.IIE-2J.IIE-23.IIE-2

6ROUND MTER SANPUS SUWARY, NHEELER PIT, LaPRAIRlE IONNSHIP, NISCWSIN

LLItLLLLLL

SOURCE PART*SADPIIW LOCATION

USEPA CASE MIHKR 1 1513MTE SAMPLE!INOR6ANIC TRAFFIC REPORTIORSANIC TRAFFIC REPORT!CRl SIMPLE NUIIIEIt IB9J6II-)VAftiVN SAKPIE NIWIER (HP-)

CHEBICAL

PESTICIOES/PCIi luq/ll

alpha-WCbeta-BHCdelta-IHCqaua-MC (UndiDtlHepUclUor

AldrinHtptKhlor ifoiidtEndOMllin I Ulplu-MdowlUnlDieldrioM'-ODE

EndrinEndotuIlM II lbtU-M*o«iltulM-DDDEn4owlf«i wlfittM -oirEndriii kitnt*

USEPAm in

11/15/88DEIVIIEI671Sll

NDNONDNlND

mMmmM

wMMMl•)

WIIIWinM

nwMM•••

PRPMl 111

11/15/88

----

6WIM IB-11

NDNOWNONO

NDDONDNDNO

HOmmIIINO

MmmNOno

USEPAIW I1A

11/15/881*1912£1672SI2

NONDNDNDND

NDNDNO

UNONDNDND

HONOWW•0NDu

PRPm n«

11/15/88

—

6KIWIIA-II

NDNDNDNDND

NDNDNDNDND

NDNDMNDNO

NDNDNDNDND

NDNONOWWNOW

USEPAIW A

11/15/88HEI1I3EI673513

NDNDNlNOND

U

MMlNDNDND

NONDmNOmNONO

PRPIW A

11/13/88

--

GM-ll

NDNDNDNDND

NONONl1111

IIINlMW11

inwMnoHI

NDnMnwmNO

USEPAUN I2B

11/15/88KEIVHEI674SH

NDmNOwND

NOWWNOND

NONONDWW

IIIHIwwDO

MNONONOUWW

PRPIW 128

11/15/88

----

CNMM2B-II

NDNDNDWND

NDNDNONDNO

NONONDNln

mM

USEPAW D

ID* OF IW 121

11/15/88BEHI5EU75515

NDNDNONONO

NDNONDNOND

NlWNOMND

NONONDNlHI

WUNDNDNDNDNO

USEPAIW I2A

ins I USD)

11/16/88«Ei»i6EV748Sit

NONDNDNDND

NONONDNDND

NOWNDNDND

NONDNDNO«D.

NONDNDNDWNDNO

PRPIW I2A

11/16/88

6MWI2A-II

ND»DNDNDND

NDNDNDUND

NONONDNONO

NDNOMWNO

NONONDNONONONO

tlplu-cklDrdutjUM-cliloriutToiipltMt

AMCLM-llltATOCLOS-I22IABOCLOI-I2J2MOCIOR-I242AMa«-l2MMOC10R-I2M«ROaiM-l2M

til:Not< tlut ill USEPA •oljlile uipit IrKtiwii ticndrd thf rtquirn) UIIKJI holding 'i» of I diys »» II diysi tlwrtlort ill positivt rtsulti trt esUiitnl U).

TIC Ttntitivfly Utntilxd ciwucallsl.IA) lodicitis tlut i TIC u > iusptcttd «ldol-cond«isiti«i produit.Ill lodicitit dttKttd in blink ind in tht tliplt; po»iblt/probiblt olink contuinition.Ul Indicitn in tttmttd vilut.IN) For PRP rtsulti, xadicitts inorqinic spike suplt recovtry is not nitrun control huts.IR) [ndicitts diti is unusiblt.IS) For PRP results, mdicitts >iUr deteriintd by Bet hod of Standard Addition.INI Indicites inttrltrenct.NA Indicitts not inilyztd; othrr chencils inilyied but not detected in iny of the siiples ire not presented in this table.10 Indicates not detected; see diti sheet lor specific detection lull.121 At the source.IP) Profosed.iMitr-ttrt! approiiiitely 7 yttrs, or 111 o* an individual's liletite.

BftOUM MTER SABPLES SlMMV, HH6ELEH PI!, L»WA]«!E TOWNSHIP, NlSCCmSIN

LL[IELL[L

[III1

SOIWCE PW1YSMP11NC LOCATION

USEPA USE NMBEft 11315DATE SAflPUJiNORSAiic TRAFFIC BEPOHIIORGANIC TRAFFIC 8EPQRTICRL SAMPLE NUKBEfi IBfJ6l|-l

SAWLE NUMBER INP-I

CHEKICAL

PESTICIDCS/PCBi lug/11

iIplu-WCMti-WCd<IU-IHC9IMi-IHC ILindintlHtptuMor

Aldrii

E>4owllu IDiildrii«,« -U£

En4rinEntewMw II4,4-MDEntowlfu

Endrii kitooiItethgiyclilorilplu-tklDrdint|MM-ctloTouphm

R-llltdiaCLOII-1221Moam-1232•SOCIW-I242A«oa.n-i24iMOCUM-IUI

USEPAIM 1

11/14/88KI9I7EY74SSI7

NDNDNDNOMl

HINDWNDW

HMNM»

UUNDWU

PRPNN B

ll/li/88

NONOMlNDND

NDmNDNDMl

HM•M11

NDNDMlMU

NDNDNDNDNDNDND

PRPN« BIDUPI

11/16/86

--

SNB-fl

NONDNONDND

NONOWNDND

NOMlNWW

MlNDMlNDND

MlNDWUNDWND

uSEPaNN IJB

11/16/86HE 19 18EY7JISIB

NDNDNDNDND

WNDNOMlU

WUnwM

MlNDNDHIinNDNDNDNDNDNDND

PRPnN us

li/li/88

GWINIIB-II

NDNDNDNDND

HIMMlWW

MMWWUUM

PRPUN I3BIDUPI

li/16/BB

--6NIHI3I-91

NONDNONDND

NDMlMUM

MNOMlMH

NDWNDNDU

WNDWNDNDNDND

USEPAIM I3A

11/16/68Mf 141 Qflt I" ITE«77ISI9

NONDNDNDND

NDNDNDNDU

WM

MlNDNINONDNDW

PRPKN I3A

ll/»t/B8

-.

NDNDNDNDND

NDNDNONDND

NDWNDUN

MlNDWNDND

NDNDWNDNONOHI

USEPAFIELD (LAW

11/16/88

ET772819

NDNDNDNDND

NDNDNONOND

NONDNDNDND

NDNDNDNDND

NONDMNDNDNDND

USEPATRIP BLANKIVOA ONLY!

11/16/88

EY7HRll

NANANANANA

NANANANANA

NANANANANA

NANANANANA

NANANANANANANA

PRPFIELD BLANK

11/14/88

-.FBII-ll

NONDNDNONO

NDNDNONDND

NDNONONDND

NDNON3NONO

NDNDNDNDNDNONO

PRP1 FIELD ILANt

11/16/86

FBIMI

NDNOMlNOND

NDNDNDNDND

NDNONDNDNO

NONDNDNDND

NDNDNONDNDNDND

I1Ir

L[

[L[L

HATER SAWK.ES SUNURt, HHEELER PIT, LaPRAIRlE TONNSH1P, NlSCONS IN

SOURCE PARKSAMPLING LOCATION

USEPA CASE DUMBER 11515DATE SAItPUDINORGANIC TRAFFIC REPORIIORGANIC TRAFFIC REPORTICRL SAMPLE NUMBER IB9JGII-INARZYN SAKPLE NUMBER I IP-1

CHEMICAL

PESTICIKS/PCIs lugMl

alpka-HCbeta-IHC4flta-IHCqaxa-BHC ILindantlHtplacklor

AKrinHeptachlor epoiidiEndosullan 1 lalpha-endosuUanlDieldrin

EndrinEndosuHan II (Deta-endosuKanl4,4-DDD£»dosiillin sullate4,4 -DOT

Endrin ketone•etnoiycMoralpha-cklordaneqaHa-chlordantloiaphtne

ARCO.OH-IIUAROCLOR-I22IAROUOR-1232AMCin-1247AROCLOR-I2W

NaiiiuiContaiinantLevel IKCL) 1-Day

DRINKING HATERCRITERIA

Health Advisories

ll-tn. Child

11-Day lonqer-teri Lonqer-ten

4.1 1,211II

1.2

W1BIEN1 HATER SUALITY CRITERIA

IN

5.1

6,IM

511

1,211II

121

5.1

tJBl

- ——————— —————————— ' Protection o( Huian Health

71.k Mult Toiicity Protection Carcinogenicity

I.K-4 Inqesting Injestinq ln?«tinqCancer Risk Hater i OrqanisM «at«' •

DHEl Liletiw Level (CA6I Orqaniws Only Orqanis«

9.2E-J" „ - 1.4JE-2

:: !.«-! :: :: ;•«;'I.I4E-2 " " '-8t '

7.4E-5

4.IE-4 2'8£-'74 159

7. IE-52.4E-5

1 4 " Ll

'•' - 74 1592.4E-5

74 159- - 2.4E-5

1,751 " " " , "[.,1.4 I.W " " ''j.1.4 M27 " " '«

1.131 - " 7llt '

7.9E-57.9E-5

".. - - T- '£-57.9E-57.9E-5

" .. - 7.9E-57.9E-5

Protection tl)

IngestingQrganisis

Only

3. IE-25.47E-2

6.25E-22.9E-4

7.9E-52.9E-4

7.kE-52.4E-5

2.4E-5--

2.4E-5

4.8E-44. BE -47.3E-4

7.9E-57.9E-57.»E-57.9E-57.9E-57.9E-57.9E-5

AMCLW-I2H

uLiF:

TRAFFIC REPORTS ANDCHAIN OF CUSTODY FORMS FOR

U.S. EPA SPLIT SAMPLING DURINGPHASE I RI GROUNDWATER SAMPLING


TRAFFIC REPORTS ANDCHAIN OF CUSTODY FORMS FOR

U.S. EPA SPLIT SAMPLING DURINGPHASE I RI GROUNDWATER SAMPLING


CE'.'lAl --:G---AL- -BO" 'TO"" SA"~L' ~ 'TA~~PO-~ORGANICS/INORGANICS

THIS FORM IS TO BE USED FOR SAMPLES SENT TO CONTRACT ONLY

CASE NUMBER. MAMPrtPi DATE SHIPPED.

SUPERFUND OU NUMBER.

ACTIVITY NUMBER ____

EPA RPM or OSC (S M S )/(CES). •PAGE OF.

SOIL

CRL LOGNUMBER

ORGANICTRAFFICREPORTNUMBER

INORGANICTRAFFICREPORTNUMBER

ACID

-BAS

E NE

UOR

GANI

C SC

ANM

G-

KG

IS 641

VOLA

TILE

OR

GA

NI

OR

GA

NIC

SC

AN

MG

/KG

YLS 244

CH

LOR

I

MG

/KG

AD

D B

ASE

NE

UO

RG

AN

IC S

CA

N

VO

LAT

ILE

OR

GA

OR

GA

NIC

SC

AN

YLS

314

UlO

X x; XX X X5X672. Aff X X y y Y

S9J60IS03 XX y X

Xy XX X x

MEX9/B yyE/77Z X X y x X

Rio X

SAMPLE DESCRIPTION ftFROM BOX 1)

2 3 4 5 6 7

CONCENTRATION ©t - LOWMED H - HIGH (SAS)

ENVIRONMENTAL PROTECTION AGENCYOffice of Enforcement

CHAIN OF CUSTODY RECORD

REGION 6230 South Dearborn Stre*t

Chicago, Illinois 606O4

PROJECT NAME

Wheeler Pit, LaPrairie Township WIPROJ. NO.

ase# 1505

Relinquished byReceived by: (Sign*tun)

Relinquished byRelinquishedty: (S<an*tur»)

Remarks Carrier1 *Airbill «

Received for Laboratory by:Relinquished by: ($>gn»wr»)

Chain of Custody Seals:Olfttrlbulion While - Accompenies Shipment; Pink — Coordinator Field File*; Yellow — Uboretory File


REGION 6230 South DMfbom Strawt

Chicago. Illinois 606O4

Diatrlbution. White — Accompanies Shipment; Pink — Coordinator Field Files; Yellow — Laboratory Ftte

i Hill!B K f f i

81s ll*82*fl*«al if*

i lPlipH

w"Z«__LJ A£*?'A

AdOO

'J <J .J- - , . ,« .»

USEPA CONTRACT LABORATORY PROGRAM. SAMPLE MANAGEMENT OFFICE

P.O. BOX 818 ALEXANDRIA. VA 22313703/557-2490 FTS-557-2490

CASE NO:•10505SAS NO:

fIF APPLICABLE)

INORGANIC TRAFFIC REPORT(FOR CLP USE ONLYi

TYPE OF ACTIVITY (CIRCLE ONE) 0SUPERFUND—PA SI ESI CRJF& RD RA ER

NPLD OAM OTHER ____NON-SUPERFUND—________PROGRAM

SFTENAME'Wheeler PitCITY. STATE: SITE SPILL ID:LaPrairie TownshipWI N3

REGION NO: SAMPLING COMPANY5___ JacTQhgIPLER: (NAME)

CLPSAMPLENUMBER

(FROM LABELS)

A7£Y 9/2

ME* Jlt>

92O

L

L

-tr

SHIP TO:

Silver ValleyOne Government GulchKellogg ID 83837(208)784-1258

1

SAMPLING DATE: $}

if /88

DATE SHIPPED:

NO:

: a fi CARRIER:EX

RASANALYSIS

HIGHONLY<SAS)

SPECIALHANDLING

SAMPLE DESCRIPTION(ENTER IN BOX A) 4. SOIL1. SURFACE WATER 5. SEDIMENT2. GROUND WATER 6. OIL (SAS)3. LEACHATE 7. WASTE (SAS)

DOUBLE VOLUME REQUIRED FOR MATRIXSPIKE/DUPLICATE AQUEOUS SAMPLE

SHIP MEDIUM AND HIGH CONCENTRATIONSAMPLES IN PAINT CANS

SEE REVERSE FOR ADDITIONALINSTRUCTIONS

STATIONLOCATION

WHfTE - 8MO COPY PINK - CUENT COPY WHITE - LAB COPY FOR RETURN TO 8MO YELLOW - LAB COPY



REGION 5230 South De*rt»om Stre*t

Chicago. Illinois 606O4PROJ NO.

Casef

PROJECT NAME

Pit, LaPrairie Township WISAMPLER

CRL*

89JGQ1

3HDATE TIME

Q.2ou <ro

STATION LOCATION

NO.

OF

CON-TAINERS

Case #

-QTIl MI.IJJ.

REMARKS

TTR

f-

XX

LO/-

SLL

Relinquished by: (Signsturt) Date/Time Received by: Relinquished by: Date / Time Received by:

Date /Time Received by: Relinquished by: Date / Time Received by:

Relinquished by: (Signttur») Date /Time Received for Laboratory by: date 7 Time

Distribution White — Accompanies Shipment, Pink — Coordinator Field Files. Yellow — Laboratory File

RemarksAirbill: I fgj&

Chaihn of CustodySeal Nos.



REGION 5230 South Dearborn Strwt

Chicago, Illinois 606O4-PROJ. NO.

:ase# 15051

PROJECT NAME

Wheeler Pit, LaPrairie Twsp WI

CRL#s^^^^^^^v

89JG01DATE TIME STATION LOCATION

NO.

OF

CON-TAINERS

Case#

REMARKS

ITR NQS.

1110 X

JSe-3 kfsla X

X

X

X/?£/&!/ftm*L\ y

Date / Time Received by: Relinquished by: Date /Time

Relinquished by Date /Time Received by: Relinquished by: Date / Time Received by:

Relinquished by: Date/Time Received for Laboratory by: Date /Time

Dittrlbulion Whit* — Accompanies Shipment; Pink — Coordinator Field Filet. Yellow — laboratory File

Remarks Carrier:Airbill # PedtjcCustodySeal Nos. 4?9,

;i! iBi'secs*** B?§ tffl!0lnffl*!"|5?»»Jîl»tiiii apf cittiiiih 1:1! ?Hl

INORGANICS DATA PACKAGE FORU.S. EPA SPLIT SAMPLING DURING

PHASE I RI GROUNDWATER SAMPLING


INORGANICS DATA PACKAGE FORU.S. EPA SPLIT SAMPLING DURING



PAGE 1 OFUNITED STATES ENVIRONMENTAL PROTECTICN AGENCY

REGION V

.ATE:

JE -CT: Review of Region V CLP DataReceived for Review on

FROM. Curtis Ross. Director (55CRL) — r-Central Regional Laboratory oe

T0: Data User: Q

Mike Valentine*We have reviewed the data for the following case(s).

SITE KAHE; 1MH€EIER PfT , ftll ___________ SMO Case No,No. of ! D.U./Activity

EPA Data Set No. Sp g£Q| Samples; JO Numbers V 3pgf Cg22*J3

CRL No, g°| JGOlSOt - SO?

SMO Traff ic No, M£*<?ll~r Hrs» Required

CLP Laboratory; SfLV'Eg VAU£Y C 1?e |p; _______ for Review:

Following are Our findings:

( ) Data are acceptable for use.(\/) Data are acceptable for use with qualifications referenced above.

x See Data Qualifier sheets and Calibration Outlier forms for flags andadditional comments*

( ) Data are preliminary - pending verification by Contractor Laboratory.See Case Summary above.

( ) Data are unacceptable.

cc: Carla Dempsey.CLP Quality Assurance Officer, Analytical Operations BranchJames Petty, Chief Quality Assurance Research. EMSL. Las Vegas

PAGE OFDATA QUALIFIERS

Contractor: case

Below is a summary of the out-of-control audits and the possible effect on thedata for this case:

fCP

t*3~) JMJ & îf^li y

AAJL * A

' ' '

Q \tAJutsaM •'

* Jfa&t JdlJ? . (M

CRDL**

Reviewed by:Phone:

CASE I _DATA SET ILAU Q.C.IDATE: __lL

QC EXCEPTION SUMMARY KEFOHTSITELAM

fi+5,l*ar

MATRIX:CONC. :

UEViElfEU uV

WATER SAMPLE £>1>K ,WATEH SAMPLE DU1>,SOIL SAMPLE SPK.SOIL SAMPLE OUP.

,!»'!;'.•;a1-!Vv*;?'V';i'unvffl

ne««rvcim

hum

tiwmwmni*wAi

U

It

iftiulti

*nru

*'r1

itutrt

ium

*n

jrn

liufn

It

OVERALL CASE QC

tn»t«*l

H*M«MM

C»l«f>(*M«<**.»*

• .

*«*•* *o

r*t»•ft MM

iCl%•

Kl'.

AO 1OI

MATRIX SPECIFIC QC

l(HO-furU

WMt>41.«

MIUMHMU

•

AQtirt».»

-Td^«?-M

w.ô

U.i..

Toi

SAMPlfÛiMCQC

61 A A

OwnMAA

l»<*«

FIELOOC

MM* DM*

•ro»M«HA

•

REGIONAL QC

•Un4•Uib

Il-n4!?•*•HI

UMUm ii•ro

OTHER/COMMLtm

». ——

Region

CASE NO.

INORGANIC REGIONAL DATA ASSESSMENT

srreLABORATORY

SDG*.

NO. OF SAMPLES/MATRIX ______

SOW*DPO: ACTION FYI

REVIEWER (IF NOT ESD)REVIEWERS NAMECOMPLETION DATE

DATA ASSESSMENT SUMMARY

ICP AA

1.

2.

3.4.

5.

6.

7.

8.

9.

10.

11.

HOLDING TIMES

CALIBRATIONS

BLANKSICS

LCSDUPLICATE ANALYSIS

MATRIX SPIKE

MSA

SERIAL DILUTION

SAMPLE VERIFICATION

OTHER QC

OVERALL ASSESSMENT

0

\/O - Data had no problems/or qualified due to minor problems.M - Data qualified due to major problems.Z • Data unacceptable.X * Problems, but do not affect data.

ACTION ITEMS: I/M f i l f c ~ P . QA *M (V). atfldfot 4?

CYANIDE

O

\

/

: As

AREAS OF CONCERN:

NOTABLE PERFORMANCE:.

7

COVER PACE

U.S. EPA - CLP

- INORGANIC ANALYSES DATA PACKAGE

Lab Name: SILVER VALLEY LABS., INC.

Uib Code: SILVER Case No.:

7/87

EPA Sample No.

Contract: 68-W8-OQ74

SAS No.: SDG NO

< )W No. :Lab Sample ID,

were ICP interelement corrections applied?

l ire ICP background corrections .If yes-were raw data generatedapplication of background corrections.

* omments:

Yes/No

Yes/No l£$

Yes/No

hardcooynara Py package and in thea u t h o r e d by^ -3 Please of the data contained in

computer-readable data ""the Laboratory Manager or the Managerallowing signature. Lab Managcr: __

MANAGER'S OESt€NEEDate: NQVFMRER 3. 1988

COVER PAGE - IN 7/fi7

U.S. EPA - CLP

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET

I

~ab Name: SILVER VALLEY LABS,. INC. Contract; 68-W8-OQ74 |_

Code: SILV£R Case No.; /O5C5 SAS No.: ____ SDG No.:

Lab Sample ID: __Matrix (soil/water): UJffTE&

^vel (low/med):

* Solids:

Date Received: /O/0*J//R/ r

Concentration Units (ug/L or mg/kg dry weight) :

|CAS No. I Analyte |Concentration!Cj Q j M|

Color Before:

Color After:

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-0440-62-2'440-66-6

| Aluminum(Antimony(Arsenic1 Barium| Beryllium| Cadmium[Calcium1 ChromiumI CobaltI Copperllron(Lead[Magnesium(Manganese| Mercury[Nickel| Potassium| Selenium[SilverI Sodium(Thallium1 Vanadium(Zinc ""1 Cyanide1

38.1*f^-SOii cAfc41.O-S1. (01800.3.M

M.1 .5a.qMa»oo.S.I*O.SLII. T

1 83kO-l.fa.T(.oqo. i.no i

L,.<~ \11* 0. 110. ft 11

Clarity Before:

Clarity After:

If!

IUJJ1iZJI F

ifir.IUI.i_i.«4I.

Texture;

Artifacts;

Comments:

FORM I - IN 7/87

Lab Na

Lab Co

Matrix

Level

% Soli

Color

Color

U.S.

INORGANIC Al

me: SILVER VALLEY LABS., INC,j*. SILVER Case Mo . /£<

(soil/water): U}PiT£&

(low/med) : LOti)

ds: O

EPA - CLP1 EPA SAMPLE NO.

t»vi**»vr» r*xm» e»trfr^f»lAiiXSlb UA1A onr.r.1 .- ————————— — ———— .

Contract: 68-W8-0074 | HEX 7/c^ {

'&£ SAS No.: SDG No.: f^lE^^f/

Lab Sample ID:

Date Received: IO/C7/^S* i

Concentration Units (ug/L or mg/kg dry weight) : (jtG/^L

1 1 1 . M i lCAS No. j Analyte | Concentration! C| Q | M(

I I I I I - J(7429-90-5 (Aluminum <38.U (U 1 _ l _ r _ l(7440-36-0 (Antimony^(7440-38-2 (Arsenic _(7440-39-3 (Barium1 7440-4 1-7 I Beryllium(7440-43-9 (Cadmium(7440-70-2 (Calcium _| 7440-47-3 ( Chromium(7440-48-4 (Cobalt __(7440-50-8 (Copper(7439-89-6 (Iron17439-92-1 ILead(7439-95-4 (Magnesium(7439-96-5 (Manganese(7439-97-6 (Mercury(7440-02-0 (Nickel __| 7440-09-7 | Potassium(7782-49-2 (Selenium(7440-22-4 (Silver __(7440-23-5 (Sodium(7440-28-0 (Thallium^(7440-62-2 (Vanadium"(7440-66-6 |Zinc^ ___| | Cyanide1 1

Before : Cc>tfi#k £ S3 Clari

After: f*oit>fa£<£> Clari

crffli^ IM ' . . .I3.S IUI IPIAt , Ifil IF I

48. 1 l&l I?HI.I Iftl 1^11. (* IU 1 1 P \ '•

ôt>cx>. I I i F la.M IUI \V\.T.SL IUI 1^14.^ IUI \T\11.8 IUI iTla * iu I . I F i

4HOO. 1 1 |7HIS.U I I 1 ^ 1o.a. IUI iCPin.i mi iTî

(3i(.0. l&l ll^li.n I&WM ilîa.n I U I M iFikiUo. i i iFi.10 IUI IFI

L.U. IUI 17^135*0. 1 1 IFÎ

10.0 Ifcl I^TlI I I I

h\r DA^nY-A »C-L. fÂr TAV^HT'O •wy DeEQEc •v^*^£flT*^ A tsAUUits •

tv After: £L£/9-£ Artifacts:

Comments:

FORM I - IN 7/87

U.S. EPA - CLP

1INORGANIC ANALYSIS DATA SHEET

Lab Name: SILVER VALLEY LABS., INC. Contract: 68-H8-0074

Lab Code: SILVER Case No.: /&5G5 SAS No.: ____

10

EPA SAMPLE NO.

SDG No.

Matrix (soil/water):

Level (low/med):

* Solids: Q

Lab Sample ID:

Date Received:

Concentration Units (ug/L or mg/kg dry weight) : US./ L-

|CAS No. Analyte lConcentration|C| Q1 1(7429-90-5 (Aluminum(7440-36-0 (Antimony(7440-38-2 (Arsenic17440-39-3 IBarium17440-41-7 (Beryllium|7440-43-9 (Cadmium|7440-70-2 ICalcium(7440-47-3 | Chromium17440-48-4 (Cobalt17440-50-8 (Copper17439-89-6 1 Iron17439-92-1 (Lead[7439-95-4 [Magnesium[7439-96-5 [Manganese(7439-97-6 [Mercury17440-02-0 (Nickel[7440-09-7 [Potassium| 7782-49-2 | Selenium17440-22-4 ISilver|7440-23-5 (Sodium(7440-28-0 (Thallium(7440-62-2 (Vanadium17440-66-6 (Zinc1 | CyanideI 1

0*0 t \&

1 O* t Tj

3U5M9.*4Mf«lo

*f osoo.<5.MS.3<«4,^

fU.to*.*!

Î*JOO.i ?

0.3Lrt.s•5Cfc5>.

I.Mnoao.

.no(o * \^

1 . l10.0

1 1Mll&l

lEiIU.II IM l

. MlpsjIUI W1 1IUIIUIWSImi iI U I M !1 1 1IUI 1IUI 11 I 1IUI 11 1 1

Color Before:

Color After: (*& g?xfl£SS

Comments:

Clarity Before:

Clarity After:

l_l

Texture:

Artifacts:

FORM I - IN 7/87

U.S. EPA - CLP

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET i ;—ii MFY Q/d i

Name: SILVER VALLEY LABS.. INC. Contract; 68-W8-0074 I IL~ "^ I

*ib Code: SILVER Case Ko.: IQScS SAS No.: _____ SDG No.:

Matrix (soil/water): Ii

.evel (low/med): /

\ Solids:

Lab Sample ID:

Date Received: /O/Q'7/f%

O

Concentration Units (ug/L or rag/kg dry weight): US//

Color Before:

Color After:

Comments:

ICAS NO» Analyte jConcentration!CJ

17429|744017440J7440[7440(7440|74401744017440(7440(7439(743917439174391743917440[74401778217440-17440-17440-17440-17440-

-90-5-36-0-38-2-39-3-41-7-43-9-70-2-47-3-48-4-50-889-692-195-496-597-602-009-749-222-423-528-062-266-6

[Aluminum^[Antimony^jArsenic_I Barium__|Beryllium|Cadmium_1 Calciumj Chromium^|Cobalt__|Copper__|Iron___[Lead

4S.QI.I

II,

|Magnesium|[Manganese!|Mercury[Nickel__I Potassium[Selenium_(silver__I Sodium__|Thallium_1Vanadium_(ZincI Cyanide

11.9

.90

T4-T10.0

Clarity Before:

Clarity After:

Texture:

Artifacts:

FORM I - IN 7/87

U.S. EPA - CLP

INORGANIC ANALYSIS DATA SHEETEPA SAMPLE NO.

Lab Name: SILVER VALLEY LABS., INC.

Lab Code: SILV£R Case No.:


Level (low/med): J

* Solids: O

Contract; 68-W8-007A

SAS No.: SDG No.: //£x f//

Sample ID:

Date Received:

Concentration Units (ug/L or ng/kg dry weight):

Color Before:

Color After:

Comments:

|CAS No. Analyte |Concentration)C| Q j M|1 11 7429-90-5 I Aluminum(7440-36-0 | Antimony17440-38-2 [Arsenic17440-39-3 | Barium| 7440-41-7 | Beryllium17440-43-9 | Cadmium[7440-70-2 [Calcium(7440-47-3 [Chromium17440-48-4 [Cobalt[7440-50-8 [Copper17439-89-6 (Iron[7439-92-1 [Lead[7439-95-4 (Magnesium[7439-96-5 [Manganese(7439-97-6 [Mercury[7440-02-0 [Nickel| 7440-09-7 | Potassium[7782-49-2 (Selenium[7440-22-4 [Silver(7440-23-5 [Sodium(7440-28-0 [Thallium|7440-62-2 [Vanadium17440-66-6 IZinc1 j Cyanide1 1

ax.i*ldi*£

oL3_SI.S

1,1l.(*

^/^ccoS.MM.^

M . X£.°l

^SlIOO.5.3^Q.9un,^

1*/OO.t,*1f .1

4 Ot•noL..U

(ot>.T10.0

1 LIULIUI .|(i'-IB)|ft|IUL1 1IUIIULImiIUI|U |V1,1|S|I U IIUII6JIU.I Miy.(Ni iiuiIUIi iIULIi i

I P II P II F II P II P I1 P \I P !i PIi ? i^/ . ir i. P IIP i'£'i PIIF |I P I\P 11 PI1 P 1

1^11 1

Clarity Before:

Clarity After:

Texture:

Artifacts:

FORK I - IN 7/87

U.S. EPA - CLP

A

INORGANIC ANALYSIS DATA SHEETEPA SAMPLE NO

Lab Name: SILVER VALLEY LABS., INC,

Lab Code: 5ILVER


Level ( low/med) :

\ Solids: Q

Case No.: /<2V

Contract; 68-W8-OQ74 |

SAS No.: SDG No.:

Lab Sample ID:

Date Received:

Concentration Units (ug/L or mg/kg dry weight):

i i i—————n j[CAS No. | Analyte |Concentration|C| Q |_u.

Color Before:

Color After:

Comments:

|7429|7440[7440[7440[7440-[7440-[7440-|7440-|7440-17440-[7439-[7439-[7439-[7439-[7439-[7440-[7440-|7782-|7440-[7440-[7440-J7440-17440-

-90-5-36-0-38-2-39-3-41-7-43-9-70-2-47-3-48-4-50-8-89-6-92-1-95-4-96-5-97-6-02-0-09-7-49-222-423-528-062-266-6

[Aluminum^| Antimony_|Arsenic_I Barium__I Beryllium[CadmiumiCalcium|Chromium|Cobalt__|Copper__|Iron___(Lead____|Magnesium |[Manganesej|MercuryjNickel__|Potassium|Selenium_(Silver__[Sodium|Thallium_| Vanadixim_I Zinc

I Cyanide_

Clarity

Clarity After:

Texture:

Artifacts:

FORM I - IN 7/87

U.S. EPA - CLPi

1INORGANIC ANALYSIS DATA SHEET

Lab Name: SILVER VALLEY LABS.. INC. Contract; 68-W8-Q074

Lab Code: SILVER Case No.: 10*505 SAS No.: ____

/yEPA SAMPLE NO.

I —————————————

| ME*SDG No.:


Level (low/med): / f)u).

% Solids: O

Lab Sample ID:

Date Received:

Concentration Units (ug/L or mg/kg dry weight) : UlG_/ /__

Color Before;

Color After:

Comments:

1 1|CAS No. | Analyte1 1|7429-90-5 | Aluminum17440-36-0 | Antimony17440-38-2 |Arsenic17440-39-3 | Barium[7440-41-7 | Beryllium1 7440-43-9 I Cadmium17440-70-2 (Calcium _j 7440-47-3 j Chromium17440-48-4 | Cobalt17440-50-8 [Copper17439-89-6 I Iron17439-92-1 ILead(7439-95-4 | Magnesium[7439-96-5 | ManganeseJ7439-97-6 [Mercury17440-02-0 [Nickel|7440-09-7 [Potassium1 7782-49-2 |Selenium_[7440-22-4 [Silver[7440-23-5 [Sodium __17440-28-0 [Thallium1 7440-62-2 j Vanadium17440-66-6 IZinc| | Cyanide1 1

1 1 1 1 1| Concentration | C| Q | M|

I I I I<5S.kJ3.Sd>.9Lolcfl.O.SMo

mofti<?,M

I U I 1 ^ 1IUI inHI 1^1IUI I P|IU 1 IPI

D , I I \ P \W l I P I

L. IU 1 IP!*f. 1 1UI IPI

/fe/7 161 IPIo».^

31oco9Sa.O.3Ln. 1

IUI - IF 1I I I P II I I P IIUI ICH/IIUI 1 f 1

4f1o. |Bl 1 F\I .H HilM IFI

*?.}? l£»l NJ i P 1qa«joo l l \ f \.no

t.(*<5-lO-

I U I I F II t U I P II I I P I

IG.O IUI 1 (LII I I Ifl&k6£L£-$S Clarity Before:

C0kPfl&-$$ Clarity After:

Cl£A# Texture:

(Ll.&AtL Artifacts :

FORM I - IK 7/87

U.S. EPA - CLP

INORGANIC ANALYSIS DATA SHEETEPA SAMPLE NO.

Lab Name: SILVER VALLEY LABS., INC. Contract; 68-W8-0074

Lab Code: SILVER Case No.: IP'505 SAS No.: ____

Matrix (soil/water) : /jUQTE.# ^b Sample ID:

Level (low/med): LD\J Date Received:

% Solids: O

Concentration Units (ug/L or mg/Jcg dry weight) :

SDG No.: fa*311

Color Before:

Color After:

Comments:

I IJCAS No. j Analyte |Concentration|C| q1 1|7429-90-5 [Aluminum17440-36-0 (Antimony(7440-38-2 [Arsenic17440-39-3 [Barium[7440-41-7 [Beryllium[7440-43-9 [Cadmium|7440-70-2 [Calcium[7440-47-3 [Chromium17440-48-4 [Cobalt[7440-50-8 [Copper[7439-89-6 [Iron[7439-92-1 I Lead[7439-95-4 [Magnesium[7439-96-5 [Manganese1 7439-97-6 | Mercury17440-02-0 [Nickel| 7440-09-7 I Potassium[7782-49-2 [Selenium|7440-22-4 [Silver17440-23-5 [SodiumJ7440-28-0 [Thallium(7440-62-2 [Vanadium[7440-66-6 [ZincI | Cyanide1 1

r^S.UISfc.S<9/14*.l0.1_L.

SSôo.3.4<S.9L-^'\11.*<9.^

MoS-OO .an0.5LM.q

/350.1.4

(a^lO.•no(e>,(of\ ?. 1IO.O

1 1IU 1I U IIftlW

k!I U I1 1IUIIUI!(flIUIIUI W .LI161IUI|(J|I&-IIU.IM II6HM I1 1 1IUI 1IUI 11 1 1IUI 11 1 1

Clarity Before:

Clarity After:

Texture:

Artifacts:

FORM I - IN 7/87

U.S. EPA - CLP

EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET

I

Lab Name: SILVER VALLEY LABS.. INC.

Lab Code: 5ILVER Case No.

Matrix (soil/water): UJflT££

Level (low/med):

* Solids: O

Contract: ^8-W8-OQ74

SAS No.:

/•texf/ySDG No.:

Lab Sample ID:

Date Received: /Q/Q7//S

Concentration Units (ug/L or mg/kg dry weight): Ll<S,/ L-.

\———j j————n r~'|CAS No. | Analyte |Concentration|C| Q ( M

Color Before:

Color After:

Comments:

L(7429|7440(7440(7440(7440|744017440(7440(7440|7440|7439(7439(7439(7439(7439|7440(7440(7782J7440-|7440-(7440-(7440-17440-

1-90-5-36-0-38-2-39-3-41-7-43-9-70-2-47-3-48-4-50-8-89-6-92-1-95-4-96-5-97-6-02-009-749-222-423-528-062-266-6

I.

| Aluminum^|Antiraony_(Arsenic_|Barium|Berylliumj CadmiumI Calcium|chromium|Cobalt__[Copper__| Iron|Lead___jMagnesium|(Manganese)|Mercury|Nickel__I Potassium(Selenium^(Silver__|Sodium__|Thallium_(Vanadium^(Zinc ___(Cyanide

Clarity Before:

Clarity After:

Texture:

Artifacts:

FORM I - IN 7/87

U.S. EPA - CLP

a~ Name. SILVER VALLEY LABS., _ . .

3BLANKS

., INC. Contract: 68-W8-0074

,a Code: SILVER Case No.: IOS0&

reparation Blank Matrix (soil/water) :

r paration Blank Concentration Units {

A alyte

A1 uminumA timonyArsenicBariumB rylliumC-dmiumCalciumC romiumC litCOjiperI~onI adMagnesiumManganese

.M rcury! N-ckeli Potassium;S lenium;s Iver; Sodium: ThalliumV nadiumZincCvanide

' —

iInitial |Calib. • |Blank |(ug/L) C|

1Jl.t, IUI>*.s \u \j.a lui

. JJ.t IUIO-S lUl/. i« Ml

•U.S \u I3. 1 \U\5.1. lul(M \t±\

II. i lul1.4 lul

hlS fej 1l.t lui0.3L lUl/;.« luisols lul

M luiV.U IjJl

/,/.(, lUlo.l lulL.L lui3.1 lUl -

tO.O IUJ1 1

ContinuingBlank

1 C

jj.t, lUl Ifu.S" lul UJ.A IMI ^.

î.i iql ?io.f lu 1 or. u lu 1 /.v/.f lu I v^j-f It/ 1 - *S.JL lui ff.V. f lu 1 •/.

/I.I lUl /I.a.<» lui -»•

</|.S lUl />(.;./ lui i.

<9.X lUl 0;;.i lui /I-

S6\.S lUl Stfl1.4 lu! i.

3.x 14 1 J(//.I, lui U<9./ 16 I ^.6.-U lui t.1.0 l&l -2,

[0.0 \IJ\ 10.1 1

SAS Ho. :

lO#T&£

ug/L or mg/kg) : U<S

•

Calibration(ug/L)2 C 3 C

.(. lUl ^/t, lU. .

SDG Ko. : /T|£X'

LL

Mi i| | Prepa-| j ration| | Blank C :MI I I I . 1II 'P.l \Al\-f \

S lUl U.S IUI 1 ll.S I U I I / 1 1i lUl 3.X lUl 1 J.X lUl l PI.1 IUI 3X1 IUff lul 0.6 IU, .

II Si.\ IUII f 11 o.s lullr* 1

(, lUl !.(. lUl 1 M* \U\\f \.* lul v/./ lu l l ^/.l lu l l /'I.J 161 J.^ IU .1 *.4 l a l l ^X lUl £.X l u l l 5-.X I U | | ^f lul ^.<l l u l l - /w. i I f t l l f^ IUI ll-t I U I I II. / lul If<? IUI J.<i W . ...1 J.<? lul If5 lul fci-5 lu l l ti.i' lul l fS lul ».!• l u l l I.t l u l l Px lul o-i l u l l <?.x lullc/l4 lUl II. 4 lul• 6 lul s*|.5 lul* lul -i.* t^y* K4J.T lUl J.7 lUl• b lUl &l.b lUl7 IUI 0-7 l£lu lul fc-u lui• 7 \A\ - 4-X IAI« lUl 10 0 IUI

I I I I

1 /!.« lu l l P 11 f f o t . f \d\\t\a i.# lui IF i1 J.7 l u l l ^ l1 fc/.fo lu l l / 11 0 .7 W I I P I1 b.b, l«ll^ 11 - ^.7 l A I I ^ 11 ;o.o lUll^l1 1 II 1

FORM III - IN 7/87

U.S, EPA - CLP

3BLANKS

STI VFR VALLEY LABS.,

Code: SILVER Case No.:

Contract: 68- 6-0074

SAS No.:

^reparation BlanJc Matrix (soil/water) :

>r paration Blank Concentration Units (ug/L or mg/kg) :

SDG No

i

? alyte

InitialCalib.Blank(ug/L) C

Aluminum* timonyArsenicBarium .£ rylliumC dmiumCalciumC" romiumr >altCopperTônI adK«gnesiumManganeseh rcury* ckel_j _Potassium£ lenium_S IverSodiumTâllium_\ nadium_2j.nc ""Cyanide

—

—

—

——— —————— —————

•Continuing Calibration

Blank (ug/L)1 C 2 C 3 C¥ 5

.5L LJ 5.9s

<3.1

1.4

n.s

—

U

aB

—

-|.- *4-vio-

(i

—

§

—

—

—

—

—

Prepa-rationBlank C

—

—

—

—

;M

£.

E.

£.

F

FORM III - IN 7/87

U.S. EPA - CLP

5ASPIKE SAMPLE RECOVERY |

IM.M. SILVER VALLEY LABS.. INC. . Contract:: 68-1x8-0074 _ |

EPA SAMPLE NO.

9/6,L b Code: SILVER Case No.:


SAS No.: ———— SDG No.:

Level (low/Bed):

Concentration Units (ug/L or mg/kg dry weight): L

I I|Control|I Limit j Spiked Sample

-lalyte | *R | Result (SSR) C1

atimony Irsenic |

Barium |"arylliumladmium | 15-7 51

calcium | jChromium ITS -t^Sobalt

ironagnesiumjManganese |".srcury |

Seleniumxlver_-odiumThallium |

inadium_ ns-/asiCyanide | S-/aS|

«3Ol?>.ce*»o

l-i'-HOO ~l_

1.OTOOiSl

SampleResult (SR) C| Added (SA)

lUllUl161

i. tooo 1611.0000 iui

*>.0

£.4000 IW

IUIll.fooo U.I IOCX3.O

IUJ

M.ôoo l6f Soo.oIUI |.O

n.ôoo

I. 10. 03.0000

So.OtUI .SOO-Or

fâ.iooo 1 1 . 500.010.0000 KJJ ac,o

/or-r

W7.S

IiZiJ£."

_I£LI*£F

FP

Comments:

FORM V (PART 1) - IN 7/87

Name: SILVER VALLEY LABS., INC.

U.S . EPA - CLP

6DUPLICATES .

IContract: 68-W8-QQ74 I

EPA SAMPLE NO.

SILVER Case No.:

. r*x (soil/water):

oîds for Sample: O

SAS No.: SDG No.:

Level (low/med):

Solids for Duplicate: Q

Concentration Units (ug/L or mg/Jcg dry weight) :

alyte

luminum_*>ntimony_Arsenic_ariura__eryllium

Cadmium_~alcium_hromiuin

Cobalt

rpn1 uead^ ___jMagnesiumj anganeseI rcury1 Nickel__I otassiumj eleniunI Silver_\j codium_I halliumj vanadiumZincyande

ControlLimit

10

JS

SOOQ

Sample (S)

/^.Sooo

II IIC| I Duplicate (D) C| | RPDJ I______. J I____

IUI I â.looo ILLI I____inn

fSl 74000I.IOOOI.UXDO

jS l I.ItAH

A 9iooo IUI |.1.9

o.Xoool.fcooo

i.Mcoo IUII.1^11.jwr

.161

. IUIJUI

0.5

_H >800Q IULI I^ôoo 11LI I.

5,ôoo |U|H.qooo -".111.1n.gooo iaia.ôoo mil

^5510.0000 I 11

Q.aooo IUI-IUI

0.3000ll.looo

S.oooo

10.0000 ;nii rJJI.

IO.OCDO

JUI:Hfi

__________ _ _____IU||/•teko.oooo"'! I I |^50.oooo | | |

.1ocx\ IUI I____.looo IUI I.(a. 1*000 \UA I i<,.(aOOO |U | |

liair.1-11.

H.5

a. 3

Ql M I-Iw^l

IiEi

~\r\:ip.lEi

-If1 1

FORM VI - IN 7/87

U.S. EPA - CLP

LABORATORY CONTROL SAMPLE

Name; SILVER VALLEY LABS., INC.

Code: JILVER Case No.:

o Id LCS Source: EPA-LV

queous LCS Source; EPA-LV

Contract: 68-W8-QQ76

SAS Ko.: SDG Ko

A ilyte

AluminumA :imony_A senicBarium_B rylliumC imiumCalcium

(Oromittm_C aalt__Copper__Iron____L id____M nesiumManganeseM rcury_N 3PotassiumS*slenium_

, S Lver__1 Sodium;Thallium_V iadium_Z ic_i_Cyanide

Aqueous (ug/L)True Found *R

/&I6.D41. O

5cO. o

WM.So515.06

41-3

I1

S^b.oo I

as,oo i

Solid (mg/kg)True Found C Limits

FORM VII - IN 7/87

ORGANICS DATA PACKAGE FORU.S. EPA SPLIT SAMPLING DURING



ORGANICS DATA PACKAGE FORU.S. EPA SPLIT SAMPLING DURING



REGION V

°ATfc

ECT: Review of Region V CLP DataReceived for Review on _____ II- °l -

r :ou. Curtis Ross, Director (5SCRL)Central Regional Laboratory -^__

Ta Data User: S~uperfu*d RPM_____"

Mike VWe have reviewed the data for the following case(s).

SITE NAME; WHEELED PIT . Wi I SMO Case Ho. _____' No. of D.U./Activity : —————

EPA Data Set No, SF5&OI Samples; H Numbers YaO<S>/Cg22NJ3

CRL No, fr^JGOISOl -SO^ j RO? f RfQ _____________________

SMO Traff ic No, EXG"7I " <*75 7C? - 773Hrs* Required

CLP Laboratory; ACOKBX ______________________ for Review; 9

Following are Our findings: /S ^n^. £4^ j/#t to<To& / 5,

> Cl/) ti

-~ 773>,

/PV773

772,

0 '' LOata are acceptable for use.J/TData are acceptable for use with qualifications referenced above. ^

See Data Qualifier sheets and Calibration Outlier forms for flags andadditional comments.

) Data are preliminary - pending verification by Contractor Laboratory.See Case Sumnary above.

( ) Data are unacceptable.

c: Carla Dempsey.CLP Quality Assurance Officer. Analytical Operations BranchJames Petty. Chief, Quality Assurance Research. EMSL. Las Vegas

DATA QUALIFIERSPAGE 2- OF %

Contractor: A?£P ( C a s e / & SI

Below 1s a Summary of the out-of-control audits and the possible effect on thedata for this case:

JL#>AY*/ '

¥/l7f JA *r.'j-*-*uS» s£>t*~<Jk "// ± u,fc-e.

2*

//s>.j , c

lU /

/

Reviewed by:Phone:Date: /

PAGE 3 OFDATA QUALIFIERS

Contractor: I Case

I<> & _S

Below is a summary Of the out-of-control audits and the possible effect on thedata for this case:

Uft J Jen'

<=*-/' Lvt

^/S-^(Lfwf>

IS. VC

S3

Reviewed by:Phone:Date: /

PAGEDATA QUALIFIERS

1.0FV

Contractor: ~ O 8.P \ Case I $ 5

Below is a summary of the out-of-control audits and the possible effect on thedata for this case:

D

7. FIELD

/\

Reviewed by. 6\S t-fsPhone: "3 $'3Date: / /

Contractor:

DATA QUALIFIERS

£>R?

PAGE OF

\ Case

Below 1s a summary of the out-of-control audits and the possible effect on thedata for this case:

77

^cl<tLL$M tit r*^***f- dJ-f, "^feC^rCbXê^. *Jb-H^&4-&-

dn 'l&~s '

d *$ C

Reviewed by;Phone:

Date:2-44-7

CASE/SAS

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDSCONTRACTOR

PAGEJ^ OF g

Instrument i X$oADATE /TIME:

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide

jl.l-Dichloroethane1,1-Dichloroethene

|Trans-l,?-Dichloroethene(ChloroformZ-Butanone1,2-Oichloroethane1,1 ,1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBroTodi-chl oromethane1,2-DichloropropaneTrans-l,3-DichloropropeneTrichloroetheneDibromocMoromethane!JlJ2-TrichloroethaneBenzenecis-l,3-Dichloropropene2-Chloroethyl vinyl etherBromoformA-Methyl-2-Pentanone

|2-Hexanone[Tetrachloroethenelj l j?3?-TetrachloroethaneTolueneCnlorobenzeneEthylbenzeneIStyreneIm-Xylene|o/p-Xylene

AFFECTED w// JSAMPLES: f/^n//

/ Ls&r\,D p y ^ A b j P H C >

Initials/Date: l%wdt/%$

Iml

$*kfLib

/o3

• ^

-

t. Ca*lWi&sfrAM

$7fl

36-jL

1.

*3*

"3*

3

Con-I0ftRP

*oA/

tÔ

\/fa^X^XBy^£& i/£v'm

*

:. t<^Vîo

3i*j

/^ J

i?7/r?*?7^ Vill*7t* 1

il.;/ t*/

•y

T r

•

Mffi•4>

Con1

tftf

:. C

it)

il.*

toni

RF

.. CJ

ibil.*

Com

fef.

.. Ca

id

-.

1.*

These flags should be applied to the analytes on the sample data sheets.

fi/87

CASE/SAS

SEMIVOLATILE HSL COMPOUNDS(Page i)

_____ CONTRACTOR

Instrument 1 4-SOODATE /TIME:

Phenolbis(-2-Chloroethyl)Ether2-Chlorophenol1 ,3-Dichl orobenzene1 ,4-Dichl orobenzeneBenzyl Alcohol1,2-Dichlorobenzene2-Methyl phenolbis(2-chloroisopropyl)Ether4-Methyl phenolN-Nitroso-Di-n-PropylamineHexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2,4-DimethylphenolBenzoic Acidbis(2-Chloroethoxy)Methane2,4-Dichlorophenol1,2,4-Trichl orobenzeneNaphthalene4-ChlT>roamlineHexachlorobutadiene4-Chl oro-3-Methylphenol2-Methyl naphtha! eneHexachlorocyclopentadiene2,4 ,6-Tri chl oropnenol2,4,5-Trichlorophenol2-Chloronaphthalene2-NitroanilineDimethyl PhthalateAcenaphthylene3-NitroanilineAcenaphthene2,4-Dinitrophenol4-NitrophenolDibenzofuran .

AFFECTED / jSAMPLE S \/i /JnJLf

S*\sJr\*Reviewer / ./ /Înitials/Date: l^fJolA ftb

1ml

£/?hf '

ItQC

ffylf

*&

f£i"

&J6i

»?2-

irH

t\*L.1?4-2-

l. CalMtRSD

' ' v.

3^5"

^5/^

1.

*

" i

iy

T

Con1

lb/+kt

/?>

M>

tltfI

fil

t/Y^Q.^yy

. c<ltJiv16

fTt

tft.3-

Wt(1

&.L

5*? *7%TJ A24

»l.'/W*

,7

T

^

•y

•j•^

Con'\ ty*RF

*&

*Lo

r5?"

^lA' '

/5'7

,i-0if/

;. ti'•il — yj

ib

?fjt

?&*£

%AA

^/1 /L

ffy"

i**,!*&/7

il.V^*

"T

T

^

-T-

73

Cont/^?RF

Li/7

m^

*2M'

,&

til

//?. //

,. Ciffff-%D

foA

%?•£

i 2,7

't&t"Vf&

\\.fpttf*

-y

^~

rr

^"

"J"0*

Com

RF

•

:. ti

ID

f t ) .*

* These flags should be applied to the analytes on the sample data sheets. 8/87

CASE/SAS

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIEKS

SEMI VOLATILE HSL COMPOUNDSPage 2

10 5-A5_______ CONTRACTOR

Instrument 1 4&&ODATE/TIME:

2.4-Dinitrotoluene2r6-DinitrotolueneDiethylphthalate4-Chlorophenyl-phenyl etherFluorene4-Nitroaniline4,6-Dinitro-2-MethylphenolN-Nitrosodiphenylamine4-Bromophenyl-phenyl etherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-Butyl phthalateFluoranthenePyreneButyl benzyl phthalateBenzo(a)Anthracenebis(2-Ethylhexy1)PhthalateChryseneDi-n-Octyl PhthalateBenzb b FluorantheneBenzo k FluorantheneBenzo a PyreneIndeno(l,2,3-cd)PyreneDibenzj a. hj AnthraceneBenzo(g.h.? ) Perylene

Init. Cal.$/*/b%RF'

Ml

,L$r/t

ti/7

%RSD it

Cont. Cal^te/21/itf'lRF

\iZ4

/f5•/^

,l&

ID

*7tf

5Sfd

20,0

P

J

-J•3

^

Cont. Cal./3/2tfv(-/on,RF

,"3^./^

-)<7

ID

?frt37.1

2A*

A

TT•y

7

Cont. Cal.jpflr/«î

•/5

ID

U?/7

*

,T

Cont. Cal.

RF ID

i

*

SEE PAGE 1 FOK AFFECTED SAMPLES.

* These flags should be applied to the analytes on the sample data sheets.

Reviewer's Initials/Date^8/87

A ACUREX'v ^ Corporation

Environmental Systems Division

U.S. Environmental Protection Agency <^//; ,*»*, November 11, 1988Contract Laboratory ProgramSample Management Office ^209 Madison St. Suite 200 X r "' <$&>Alexandria VA 22314 % cvAttention: Linda Boynton / '

4/>*£Subject: Data packages for ten water samples and one VOA trip blankCase: 10505SDG: EX671Contract f: 68-01-7416Protocol: WA-87J002 (July 87)Sample ID's: EX671 through EX675 and EY768 through EY773

When samples arrived, we noticed that the chain of custody form had adiscrepancy. In the box labeled "Proj. No.1* it said "case 1505". Onthe upper right corner of the form was written "case 10505". We calledSMO for guidance and were told by Cindy Schreyer that this was ok asis*

This was a rather clean case, no samples in any fraction had to be :repeated or diluted. In the semivolatile fraction one sample, EX673,had one surrogate out of limits. In the volatile fraction, the onlysurrogate out of limits was on a matrix spike duplicate.

Release of the data contained in this hardcopy data package and inthe computer-readable data submitted on floppy diskette has beenauthorized by the Laboratory Manager or his designee, as verifiedby the following signature.

Richard B. ScottCLP Program Managerdate:

If you have any questions regarding this package please call.

Sincerely,

Richard B. ScottCLP Program- Managerdate : if / f ?¥

RS/

cc: USEPA/EMSL/LV944 East Harm an Avenue, Room 226Las Vegas, NV 89109Attention: Data Audit Staff

4d5 Clyde Avenue. P.O. Box 7044. Mountain View, CA 94039 (415)961-5700 Telex: 325961 FAX; (415) 964-5145

USEPA Region VEnvironmental Services Division536 South Clark Street, 10th Floor, CRLChicago, II 60605

3 ib Name: ACUREX CORP.

2AWATER VOLATILE SURROGATE RECOVERY

Contract: 68-01-7416

002

Lab Code: ACUREX Case No.: 10505 SAS No.: SDG No.: EX671

0102030405060708091011121314

EPASAMPLE NO.

EX671EX672EX673EX674EX675EY768EY768MSEY768MSDEY769EY770EY771EY772EY773VBLK1

SI(TOL) f

10110410010110299101100999498100102100

S2(BFB)#

9696979699979494979598989697

S3(DCE)#

1021011001039910297127 *10710210710010199

OTHER TOTOUT

00000001000000

QC LIMITS51 (TOL) = Toluene-d8 ( 88-110)52 (BFB) = Bromofluorobenzene ( 86-115)53 (DCE) = l,2-Dichloroethane-d4 ( 76-114)

# Column to be used to flag recovery values

* Values outside of contract required QC limits

D Surrogates diluted out

page 1 of 1FORM II VOA-1 1/87 Rev.

2CWATER SEMIVOLATILE SURROGATE RECOVERY

135

Name: ACUREX CORP. Contract: 68-01-7416

Lab Code: ACUREX Case No.: 10505 SAS No.: SDG No.: EX671

010203040506070809101112

EPASAMPLE NO.

EX671EX672EX673EX674EX675EY768EY768MSEY768MSDEY769EY770EY771EY772

SI(NBZ)|

748090577378838387599085

S2(FBP)f

908788707178858181729090

S3(TPH) i

10497161 *1031361321291191248985118

S4(PHL) *

647276617169767464628578

S5(2FP)»

647475637168716957668376

S6(TBP) I

9482111161221129710990979177

OTHER•TOTOUT

001000000000

51 (NBZ) = Nitrobenzene-dS52 (FBP) = 2-Fluorobiphenyl53 (TPH) = Terphenyl54 (PHL) = Phenol-d555 (2FP) = 2-Fluorophenol56 (TBP) = 2,4,6-Tribromophenol

QC LIMITS( 35-114)( 43-116)( 33-141)( 10-94 )( 21-100)( 10-123)

I Column to be used to flag recovery values* Values outside of contract required QC limitsD Surrogates diluted out

page 1 of 1FORM II SV-1 1/87 Rev.

L_b Name: ACUREX CORP,

I b Code: ACUREX

2EWATER PESTICIDE SURROGATE RECOVERY

_________ Contract: 65-01-7416

Case No.: 10505 SAS No.: _____ SDG No.:

0327

01020304050607080910111213

EPASAMPLE NO.

EX671EX672EX673EX674EX675EY768EY769EY770EY771EY772EY768MSEY768MSDPBLK1

SI(DBC)f

864887919584338643796792100

OTHER

0000000000000

ADVISORYQC LIMITS

SI (DBC) = Dibutlychlorendate ( 24-154)

# Column to be used to flag recovery values

* Values outside of contract required QC limits

D Surrogates diluted out

page 1 of 1FORM II PEST-1 1/87 Rev,

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Name: ACUREX CORP.__________ Contract: 68-01-7416

SAS No.:

003

Lab Code: ACUREX Case No.: 10505

K-trix Spike - EPA Sample No.: EY768

SDG No.: EX671

COMPOUND

1 , 1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/L)

50.050.050.050.050.0

SAMPLECONCENTRATION

(ug/L)

001.7200

MSCONCENTRATION

(ug/L)

70.352.657.458.157.4

MS%

REC #

141105111116115

QCLIMITSREC.

61-14571-12076-12776-12575-130

COMPOUND

1, 1-DichloroetheneTrichloroetheneBenzene""olueneJhlorobenzene

SPIKEADDED(ug/L)

50.050.050.050.050.0

MSDCONCENTRATION

(ug/L)

71.653.759.558.658.3

MSD%

REC f

143107116117117

%RPD #

-1-2-4-1-2

QC LIRPD

1414111313

LMITSREC.

61-14571-12076-12776-12575-130

% Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits

F D: _2 out ofSpike Recovery:

COMMENTS: EY678I50A

outside limitsout of 10 outside limits

FORM III VOA-1 1/87 Rev.

3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

1 ib Name: ACUREX CORP.__________ Contract: 68-01-7416

SAS No.: _____

0328

I-Lb Code: ACUREX Case No.: 10505

Matrix Spike - EPA Sample No.: EY768

SDG NO.: EX671

COMPOUND

gamma-BHC (Lindane)HeptachlorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/L)

0.2000.2000.2000.5000.5000.500

SAMPLECONCENTRATION

(ug/L)000000

MSCONCENTRATION

(ug/L)

0.1740.1790.1770.4950.6330.437

MS%REC I

87908999127 *87

QCLIMITSREC.

56-12340-13140-12052-12656-12138-127

COMPOUND

ganuna-BHC (Lindane)HeptachlorAldrinDieldrinEndrin4,4'-DDT

SPIKEADDED(ug/L)

0.2000.2000.2000.5000.5000.500

MSDCONCENTRATION

(ug/L)

0.1820.1780.1790.4890.6340.509

MSD%

REC *

91899098

127 *102

%RPD f

-41

-110

-16

QC LIRPD

152022182127

[MITSREC.

56-12340-13140-12052-12656-12138-127

f Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits

I-'D: _ffi out of _fe outside limitsSpike Recovery: _i out of 12 outside limits

COMMENTS:

FORM III PEST-1 8/87 Rev,

Name: ACUREX CORP.

4AVOLATILE METHOD BLANK SUMMARY

_______ Contract: 68-01-7416

004

L-b Code: ACUREX Case No.: 10505 SAS No.: ______ SDG No.: EX671

Lao File ID: MB102201A Lab Sample ID: MB102201A

D te Analyzed: 10/22/88 Time Analyzed: 1415

Matrix: (soil/water) WATER Level:(low/med) LOW

I strument ID: I50A

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

010203040506070809.10111213

EPASAMPLE NO.

EX671EX672EX673EX674EX675EY768EY768MSEY768MSDEY769EY770EY771EY772EY773

LABSAMPLE ID

88100341881003428810034388100344881003458810034688100346MS88100346MSD881003478810034888100349881003410881003411

LABFILE ID

EC1003401AEC1003402AEC1003403AEC1003404AEC1003405AEC1003406AEC1003406SAEC1003406DAEC1003407AEC1003408JAEC1003409JAEC1003410JAEC1003411A

TIMEANALYZED

1516154816201652172317531825185619272317224322112141

MENTS: VBLK1I50A

page 1 of 1FORM IV VOA 1/87 Rev

L b Name: ACUREX CORP.

Lab Code: ACUREX Case No.: 10505

U-b File ID: EC10034WC

D te Extracted: 10/10/88

Date Analyzed: 10/26/88

M trix: (soil/water) WATER

Instrument ID: 4500

4BSEMIVOIATILE METHOD BLANK SUMMARY

________ Contract: 68-01-7416

SAS No.: ______

137

______ SDG No.: EX671

Lab Sample ID: EC10034WC

Extraction:(SepF/Cont/Sonc) CONT

Time Analyzed: 1438___

Level:(low/med) LOW


01020304050607080910'1112

EPASAMPLE NO.

EX671EX672EX673EX674EX675EY768EY768MSEY768MSDEY769EY770EY771EY772

LABSAMPLE ID

8810034188100342EC1003403C88100344881003458810034688100346MS88100346MSD881003478810034888100349881003410

LABFILE ID

EC1003401JCEC1003402JCEC1003403CEC1003404JCEC1003405CEC1003406CEC1003406SCEC1003406DCEC1003407CEC1003408JCEC1003409JCEC1003410JC

DATEANALYZED

10/28/8810/28/8810/26/8810/28/8810/26/8810/26/8810/26/8810/26/8810/26/8810/28/8810/31/8810/31/88

C MMENTS: WBLANK1 1L>1ML BN & A 1:1 WATER BLANK 10/10/88FINN4500

page 1 of 1FORM IV SV 1/87 Rev.

0329

ib Name: ACUREX CORP.

Tib Code: ACUREX Case No.: 10505

Lab Sample ID: EX671-BLK1A

) itrix:(soil/water) WATER

Date Extracted: 10/10/88

I ite Analyzed (1): 10/25/88

Time Analyzed (1): 0226

Instrument ID (1): 3400-2A

( : Column ID (1): SP22502401

4CPESTICIDE METHOD BLANK SUMMARY

_______ Contract: 68-01-7416

SAS No.: ______

Lab File ID:

Level:(low/med)

SDG No.: EX671

LOW

Extraction:(SepF/Cont/Sonc) CONT

Date Analyzed (2):

Time Analyzed (2):

Instrument ID (2):

GC Column ID (2) :

10/25/88

0226

3400-2B

OV1


010203040506070809101112

EPASAMPLE NO.

EX671EX672EX673EX674EX675EY768EY769EY770EY771EY772EY768MSEY768MSD

LABSAMPLE ID

EX671AEX672AEX673AEX674AEX675AEY768AEY769AEY770AEY771AEY772AEY768MSAEY768MSDA

DATEANALYZED 1

10/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/88

DATEANALYZED 2

10/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/8810/25/88

< )MMENTS:

page 1 of 1FORM IV PEST 1/87 Rev.

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

,ab Name: ACUREX CORP.__________ Contract: 68-01-7416

EPA SAMPLE NO.

VBLK1

ja. Code: ACUREX Case No.: 10505 SAS No.:

latrix: (soil/water) WATER

;a pie wt/vol: 5.0 (g/mL) ML

,e •-»!: (low/med) LOW

; Moisture: not dec. ___

:o Limn: (pack/cap) CAP

SDG No.: EX671

Lab Sample ID: MB1Q2201A

Lab File ID: MB102201A

Date Received: ______


Dilution Factor: 1.00

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3———————Chloromethane__________74-83-9———————Bromomethane___________75-01-4———————Vinyl Chloride_________75-00-3-^——————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene_______75-35-3———————1,1-Dichloroethane______540-*59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform______________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone______________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichlorome thane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochl or ome thane_____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5———————i,l,2,2-Tetrachloroethane_108-88-3——————Toluene________________108-90-7——————Chlorobenzene___________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes___________

1010101031055555510551055555535510105555555

UuUuJuuuuuuuuuuuuuuuuuJuuuuuuuuuuu

FORM I VOA 1/87 Rev,

IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO*

Lob Name: ACUREX CORP. Contract: 68-01*7416SBLK1

L o Code: ACUREX Case No.: 10505 SAS No.:

Matrix: (soil/water) WATER

S mple wt/vol: 1000 (g/mL) ML

Level: (low/med) LOW

% Moisture: not dec. ___ dec. ___

E traction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) H_ pH: ____

SDG No.: EX671


Lab File ID: EC10034WC





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

±UO — 5J3"**

111-44-4 ———yo— 3 /— o— — — — —541-73-1 ———106-46-7 ———100-51-6 ———95-50-1 ————

108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————i*O — y^ j— —

105-67-9 ———65-85-0 ————111-91-1 ———

91-20-3-----y ± tt\f w106-47-8 ———

59-50-7 ————

;>3 — Uw — H

o a T A A

131-11-3 ———

——— Phenol——— bis (2-Chloroethyl) Ether——— 2-Chlorophenol——— 1, 3-Dichlorobenzene——— 1,4-Dichlorobenzene——— Benzvl Alcohol—— 1 , 2-Dichlorobenzene——— 2-Methylphenol——— bis (2-Chloroisopropyl) Ether _——— 4-Methylphenol——— N-Nitroso-Di-n-Propylamine __——— Hexachloroethane——— Nitrobenzene—— Isophorone——— 2-Nitrophenol——— 2 , 4-Dimethylphenol

——— bis ( 2-Chloroethoxy ) Methane __——— 2 , 4-Dichlorophenol——— 1 . 2 f 4-Trichlorobenzene——— Naphthalene——— 4 -chloroani 1 ine——— Hexachlorobutadiene——— 4-Chloro-3-Methylphenol——— 2-Methylnaphthalene——— Hexachlorocyclopentadiene ___——— 2 , 4 , 6-Trichlorophenol——— 2 f 4 , 5-Trichlorophenol—— 2-Chloronaphthalene—— 2-Nitroaniline——— Dimethyl Phthalate

—— 2 . 6-Dinitrotoluene

101010101010101010101010101010105010101010101010101010501050101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I SV-1 1/87 Rev.

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

312EPA SAMPLE NO.

Lab Name: ACUREX CORP. Contract: 68-01-7416SBLK1

L b Code: ACUREX Case No.: 10505 SAS No.:


S mple wt/vol: 1000 (g/mL) ML_

I-vel: (low/med) LOW

I Moisture: not dec. ___ dec. ___


GPC Cleanup: (Y/N) fi_ pH: ____

SDG No.: EX671


Lab Pile ID: EC10034WC





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

99-09-2———————3-Nitroaniline__________83-32-9;——————Acenaphthene_________.51-28-5:——————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran____________121-14-2——————2,4-Dinitrotoluene_______84-66-2——————Diethylphthalate________7005-72*3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene______________100-10-6——————4-Nitroaniline__________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1)101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol________85-01-8———————Phenanthrene___________120-12-7——————Anthracene____________84-74-2——————Di-n-Butylphthalate_____206-44-0——————Fluoranthene___________129-00-0——————Pyrene________________85-68-7———————Butylbenzylphthalate_____91-94-1——————3,3'-Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9—————Chrysene_____________117-81-7——————bis(2-Ethylhexyl)Phthalate_117-84-0——————Di-n-Octyl Phthalate____"205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo(k) Fluoranthene_____50-32-8——————Benzo (a) Pyrene_________193-39-5——————Indeno (1,2,3-cd) Pyrene___53-70-3——————Dibenz(a,h)Anthracene____191-24-2——————Benzo (g,h, i) Perylene_____

501050501010101010505021010501010101010102010101010101010101010

(1) - Cannot be separated from Diphenylamine

UUUUUUUUUUUJUUUUUUUUUUUUUUUUUUUU


IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO

Lab Name: ACUREX CORP.SBLK1

1 1> Code: ACUREX Case No.: 10505


5 .mple wt/vol: 1000 (g/mL) ML

r .vel: (low/med) LOW


) rtraction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) fi_ pH:


SAS No.: _____ SDG No.: EX671


Lab File ID: EC10034WC





Vnmber TICs found: _Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER . COMPOUND NAME RT EST. CONC. Qt

1* 1. *** —— */

FORM I SV-TIC 1/87 Rev.

IDPESTICIDE ORGANICS ANALYSIS DATA SHEET

Lab Name: ACIJREX CORP..__________ Contract: 68*01-7416

EPA SAMPLE NO.

PBLK1




I vel: (low/med) LOW

% Moisture: not dec. _ dec. _

£ traction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) N_ pH: ___

SDG NO.: EX671

Lab Sample ID: EX671-BLK1A

Lab File ID: __________






319-84-6——————alpha-BHC________319-85-.7———————beta-BHC__________319-86-8——————delta-BHC________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______[309-00-2——————Aldrin___________1024*57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1———————Dieldrin________72-55-9———————4,4'-DDE_________72-20-8———————Endrin__________33213-65-9—————Endosulfan II_____72-54-8———————4,4'-DDD_________1031-07-8—————Endosulfan sulfate_50-29-3————————4,4'-DDT________72-43-5———————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2————Aroclor-1016______11104-28-2————Aroclor-1221______11141-16-5————Aroclor-1232______53469-21-9————Aroclor-1242______12672-29-6————Aroclor-1248______11097-69-1—————Aroclor-1254______11096-82-5————Aroclor-1260

.050

.050

.050

.050

.050

.050

.050

.0500.100.100.100.100.100.100.100.500.100.500.501.00.500.500.500.500.501.01.0

uuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST 1/87 Rev,


Lab Name: ACUREX CORP.___________ Contract: 68-01-7416

007EPA SAMPLE NO.

EX671



Sample wt/vol: 5.0 (g/mL) ML

L vel: (low/med) LOW

% Moisture: not dec. ___

SDG NO.: EX671

c lumn: (pack/cap) CAP

Lab Sample ID: 88100341

Lab File ID: EC1003401A

Date Received: 10/07/88




74-87-3———————Chloromethane___________74-83-9———————Bromomethane____________75-01-4——————Vinyl Chloride_________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_________________75-15-0———————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene_______75-3.5-3 ——————— 1,1-Dichloroethane______540-59-0 —————— 1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2 —————— 1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-1,3-Dichloropropene_75-25-2——————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_________________108-90-7—————Chlorobenzene__________100-41-4—————Ethylbenzene___________100-42-5——————Styrene________________1330-20-7—————Total Xylenes__________

IP101010

5555551055105555555551010550.65555

UUUU-BJ-WjUUUUUUUUUUUUUUUUUUUUUUUJUUUU

FORM I VOA 1/87 Rev.

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

008EPA SAMPLE NO.

Lab Name: ACUREX CORP.

Ix > Code: ACUREX Case No.: 10505

M?*:rix: (soil/water) WATER

Sample wt/vol: 5.0 (g/mL) Ml

L« 'el: (low/med) LOW


C< .umn (pack/cap) CAP

N iber TICs found: _Q

Contract: 68-01-7416EX671

SAS No.: SDG No.: EX671






CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER COMPOUND NAME RT EST. CONC. Q

r^-r. /-it-

FORM I VOA-TIC 1/87 Rev.

U181A

VOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

EX672

ib Code: ACUREX Case No.: 10505 SAS No.:


; ample wt/vol: 5.0 (g/mL) ML

~ svel: (low/med) LOW


SDG No.: EX671

(pack/cap) CAP

CAS NO. COMPOUND





Dilution Factor: 1.00___


74-87-3*——————Chloromethane___________74-83-9———————Bromomethane___________75-01-4———————Vinyl Chloride_________75-00-3———————Chloroethane____________75-09-2———————Methylene Chloride______67-64-1———————Acetone_________________75-15-0———————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene______75-3^-3 ——— ——— 1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2 —————— 1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2, 2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________

10101010

55555510551055555555510105555555

UUUUUUUUUUUUUUUUUUUUUUUUUUUUU



019EPA SAMPLE NO.

Lab Name: ACUREX CORP.EX672

1 »b Code: ACUREX Case No.: 10505


Sample wt/vol: 5.0 (g/mL) ML

; avel: (low/med) LOW

% Moisture: not dec, ___

» Dlumn (pack/cap) CAP

\mber TICs found:


SAS No.: ______ SDG No.: EX671






CONCENTRATION UNITS:(ug/L or ug/Kg) UG/3>


//5L ;>./^^^— // /.,_,*. > Li



,ab Name: ACUREX CORP.__________ Contract: 68-01-7416

025EPA SAMPLE NO.

EX673

,a Code: ACUREX Case No.: 1050? SAS No.:

latrix: (soil/water) WATER

sample wt/vol: 5.0 (g/mL) ML

:,€ el: (low/med) LOW

5 Moisture: not dec. ___

SDG No.: EX671

:c umn: (pack/cap) CAP


Lab File ID: FC1003403A





74-87-3———————Chloromethane__________74-83-9———————Bromomethane____________75-01-4——————Vinyl Chloride_________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride_______67-64-1---—•———Acetone________________75-15-0———————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene_______75-3.5-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform______________107-06-2 —————— 1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform______________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5———————1, l,2,2-Tetrachloroethane_108-88-3——————Toluene________________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________

10101010510555555105510555555

510105555555

UUUUUUUUUUUUUUUUUUUUUU

UUUUUUUUUUU

FORM I VGA 1/87 Rev,

IEVOLATILE ORGANICS ANALYSIS DATA SHEET


026EPA SAMPLE NO.

Name: ACUREX CORP. Contract: 68-01-7416EX673

"â Code: ACUREX Case No.: 10505 SAS No.:


;a_.ple wt/vol: 5.0 (g/mL) ML

le el: (low/med) LOW

V Moisture: not dec. ___

:c umn (pack/cap) CAP

SDG No. : EX67I






ber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER

•

COMPOUND NAME RT EST. CONC. Q

4"




032EPA SAMPLE NO.

EX674

L< » Code: ACUREX Case No.: 10505 SAS No.:


Staple wt/vol: 5.0 (g/mL) ML

L* 'el: (low/med) LOW


c< .umn: (pack/cap) CAP

SDG No.: EX671







74-87-3 —————

75-01-4 —————75-00-3 —————/ 3 — Us — t — — •" — — —

67-64-1 —————75-15-0 —————75-35-4 —————75-35-3 —————540-59-0 ————67-66-3 —————107-06-2 ————

71-55-6 —————c £ ^ e56-23-5------108-05-4 ————"T C *\ ** Jt75-27-4--- ———

10061-01-5 ———79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————

127-18-4 ————79-34-5 —————' * •* -mJ

100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinyl Chloride—— Chloroethane—— Methylene Chloride— — — AcetonefkV^ln WWi I V*

—— Carbon Disulfide—— 1 , 1-Dichloroethene—— 1, 1-Dichloroethane—— 1 , 2-Dichloroethene (total )—— Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1, 1, 1-Trichloroethane—— Carbon Tetrachloride

vinyA /»wts i*a u«s—— Bromodichloromethane—— 1 , 2-Dichloropropane—— cis-l,3-Dichloropropene—— Trichloroethene—— Dibromochloromethane—— 1 , 1 , 2-Trichloroethane— —Dcntsne—— Trans-1, 3-Dichloropropene ___—— Bromoform—— 4-Methyl-2-Pentanone—— 2-Hexanone—— Tetrachloroethene—— 1 , 1,2, 2-Tetrachloroethane—— Toluene—— Chlorobenzene— — — Ft~hv1 hpn7 An AIwVilJ A.«-" -*I**'ii||

---Styrene—— Total Xylenes

10101010

5 *r10555555105510555555

$*

510105555555

UUUUJSJ-WUUUUUUUUUUUUUUUUUx itUUUUUUUUUUU



033EPA SAMPLE NO.

Lab Name: ACUREX CORP. Contract: 68-01-7416EX674

1 ib Code: ACUREX Case No.: 10505 SAS No.:


1 imple wt/vol: 5.0 (g/raL) ML

T ivel: (low/med) LOW


< >lumn (pack/cap) CAP

SDG No.: EX671






1 unber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L


1'l / > itt. y

FORM I VOA-TIC 1/87 Rev,


,ab Name: ACUREX CORP.___________ Contract: 68-01-7416

EPA SAMPLE NO

EX675

.a: Code: ACUREX Case No.: 10505 SAS No,:


;a.»ple wt/vol: 5.0 (g/mL) ML

^ al: (low/med) LOW

; Moisture: not dec. ___

SDG NO.: EX671

:o amn: (pack/cap) CAP

CAS NO. COMPOUND







74-87-3———————Chloromethane___________74-83-9———————Bromomethane___________75-01-4———————Vinyl Chloride__________75-00-3'——————Chloroethane___________75-09-2———————Methylene Chloride_______67-64-1-——------Acetone^_______________75-15-0———————Carbon Disulf ide________75-35-4 ——————— 1,1-Dichloroethene_______75-35-3 ——————— 1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform______________107-06-2 —————— 1,2-Dichloroethane______78-93-3———————2-Butanone______________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5 ——————— 1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2——————Brottoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene________________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————1330-20-7—————

10101010***55555510551055555575510105555555

UUUU.BJ- UJUUUUUUUUUUUUUUU

UUUUUUUUUUU



Lab Name: ACUREX CORP.__________ Contract: 68-01-7416

052EPA SAMPLE NO.

EY768



S-;nple wt/vol: 5.0 (g/mL) ML



SDG No.: EX671

C lumn: (pack/cap) CAP

CAS NO. COMPOUND







74-87-3———————Chloromethane__________74-83-9———————Broroomethane___________75-01-4———————Vinyl Chloride_________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene______75-3.5-3 ——————— 1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2 —————— 1,2-Dichloroethane_______78-93-3———————2-Butanone______________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane_____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene__75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2, 2-Tetrachloroethane_108-88-3———————Toluene_________________108-90-7——————Chlorobenzene___________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes___________

10101010

555555105510555555*5510105555555

UUU

LitUUUUUUUUUUUUUUUUU

uUuuuuuuuuu



EPA SAMPLE NO.

Lab Name: ACUREX CORP. Contract: 68-01-7416EY768

ab Code: ACUREX Case No.: 10505 SAS No.:


âmple wt/vol: 5.0 (g/mL) ML

svel: (low/med) LOW


Dlumn (pack/cap) CAP

SDG No.: EX671






umber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER

-

COMPOUND NAME RT EST. CONC. Q

v j*. / *L'"'/' 7""

't. "<



UOJLEPA SAMPLE NO.

Lab Name: ACUREX CORP.EY769

] ib Code: ACUREX Case No.: 10505


J onple wt/vol: 5.Q (g/mL) ML

T^vel: (low/med) LOW

\ Moisture: not dec. ___

( ilumn: (pack/cap) CAP



CAS NO. COMPOUND






CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

74-87-3———————Chloromethane___________74-83-9———————Bromomethane___________75-01-4———————Vinyl Chloride__________75-00-3r——————Chloroethane___________75-09-2———————Methylene Chloride_______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-35-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene________________108-90-7——————Chlorobenzene___________100-41-4——————Ethylbenzene ________100-42-5——————Styrene________________1330-20-7—————Total Xylenes___________

1010101051055555510551055555555510105555555

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU




Ot>2EPA SAMPLE NO.

Lab Name: ACUREX CORP. Contract: 68-01-7416.EY769

tx > Code: ACUREX Case No.: 10505 SAS No.:


5< iple wt/vol: 5.0 (g/mL) ML

U -'el: (low/med) LOW

I Moisture: not dec. ___

3< .umn (pack/cap) CAP

SDG No.: E?C$71





Dilution Factor: 1*00

tber TICs found: _QCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER

•"

COMPOUND NAME

'

RT EST. CONC. Q

**-'».£

/ * i



UbtfEPA SAMPLE NO.

Lab Name: ACUREX CORP,EV770

] ,b Code: ACUREX Case No.: 10505


£ jnple wt/vol: 5.0 (g/mL) ML

I-avel: (low/med) LOW

V Moisture: not dec. ___

< »lumn: (pack/cap) CAP

CAS NO. COMPOUND




Lab File ID: EC1003408JA





74-87-3———————Chloromethane____________74-83-9———————Bromomethane______________75-01-4———————Vinyl Chloride___________75-00-3:——————Chloroethane_____________75-09-2———————Methylene Chloride________67-64-1———————Acetone_________________75-15-0———————Carbon Disulfide__________75-35-4 ——————— 1,1-Dichloroethene________75-35-3 ——————— 1,1-Dichloroethane________540*59-0——————1,2-Dichloroethene (total)__67-66-3———————Chloroform_______________107-06-2 —————— 1,2-Dichloroethane________78-93-3———————2-Butanone_______________71-55-6———————1,1,1-Trichloroethane______56-23-5———————Carbon Tetrachloride_______108-05-4——————Vinyl Acetate____________75-27-4———————Bromodichloromethane_______78-87-5———————1,2-Dichloropropane________10061-01-5————c is-1,3-Dichloropropene____79-01-6——————Trichloroethene__________124-48-1——————Dibromochloromethane_______79-00-5——————1,1,2-Trichloroethane______71-43-2——————Benzene _____________10061-02-6————Trans-1,3-Dichloropropene75-25-2———————Bromoform_________________108-10-1——————4-Methyl-2-Pentanone_______591-78-6——————2-Hexanone_______________127-18-4——————Tetrachloroethene_________79-34-5——————1,1,2,2-Tetrachloroethane___108-88-3——————Toluene__________________108-90-7——————Chlorobenzene____________100-41-4—————Ethylbenzene_____________100-42-5—————Styrene_________________1330-20-7—————Total Xylenes____________

10101010510555555105510555555

510105555555

UUUUUUUUUUU



067EPA SAMPLE NO.

Lab Name: ACUREX CORP. Contract: 68*01-7416EY770

I ib Code: ACUREX Case No.: 10505 SAS No.:


5 jnple wt/vol: 5.0 (g/mL) ML

I -ivel: (low/med) LOW


( >lumn (pack/cap) CAP

SDG No.: EX671






1 imber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L


> Hi * ******




EPA SAMPLE NO.

EY771


Matrix: (soil/water) WATER.

S mple wt/vol: 5.Q (g/mL) ML

L vel: (low/med) LOW


C lumn: (pack/cap) CAP

SDG NO.: EX671







74-87-3———————Chloromethane__________74-83-9———————Bromomethane___________75-01-4———————Vinyl Chloride_________75-00-3-r——————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1——————Acetone______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene_______75-35-3———————1,1-Dichloroethane______540-159-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane_______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——————Dibromochlorome thane_____79-00-5——————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane__108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________

1010101051055555510551055555555510105555550.5

UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu



074EPA SAMPLE NO.

Lab Name: ACUREX CORP, Contract: 68-01-7416EY771



S_aple vt/vol: 5.0 (g/mL) ML

t vel: (low/med) LOW


C lumn (pack/cap) CAP

SDG No.: EX671






mber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER

.

COMPOUND NAME•

RT EST. CONC. Q

ffo-tt- It

f f ~/ • •*

.22*7- a- yin - &-4

t**O% * V ** 9 **'^^*^^r - • • •• f j It.It.


1A085

EPA SAMPLE NO.

ib Name: ACUREX CORP. Contract: 68-01-7416EY772

ib Code: ACUREX Case No.: 10505 SAS No.:

itrix: (soil/water) WATER

im le wt/vol: 5.0 (g/mL) ML_

jv**l: (low/med) LOW

Moisture: not dec. ___

SDG No.: EX671

>1 an: (pack/cap) CAP

CAS NO. COMPOUND





Dilution Factor: 1*00


74-87-3———————Chloromethane___________74-83-9———————Bromomethane___________75-01-4——————:-Vinyl Chloride__________75-00-3-———————Chloroe thane____________75-09-2———————Methylene Chloride______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4 ——————— 1,1-Dichloroethene______75-35-3 ——————— 1,1-Dichloroethane______540-59-0--—————1,2-Dichloroethene (total)67-66-3———————Chloroform______________[107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromochloromethane_____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone______________127-18-4——————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene________________1330-20-7—————Total Xylenes__________

10101010510555555105510555555

5510105555555

UUUUU

UUUUUUUUUUUUUUUU

UUUUDUUUUUU

FORM I VOX 1/87 Rev,


096EPA SAMPLE NO.


1 b Code: ACUREX Case No.: 10505 SAS No.:


£ .mple wt/vol: 5.0 (g/mL) ML


* Moisture: not dec. ___

c tlumn: (pack/caP) CAP

SDG No.: EX671







74-87-3———————Chloromethane___________74-83-9———————Bromomethane___________75-01-4———————Vinyl Chloride_________75-00-3-r——————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-35-3 ——————— 1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate__________75-27-4———————Bromodichloromethane_____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48*1——————Dibromochloromethane_____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bromoform_____________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________

1010101051055555510551055555555510105555555

UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu




uy?EPA SAMPLE NO.


I b Code: ACUREX Case No.: 10505 SAS No.:


£ mple wt/vol: 5.0 (g/mL) ML

I~vel: (low/med) LOW


c lumn (pack/cap) CAP

SDG No.: EX671






I onber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L




142EPA SAMPLE HO.

Lab Name: ACUREX CORP.

L


Code: ACURE% Case No.: 10505 SAS No.:


S nple wt/vol: 1000 (g/mL) ML

L-vel: (low/med) LOW



GPC Cleanup: (Y/N) fi_ pH:

SDG No.: EX671

CAS NO. COMPOUND


Lab File ID: EC1003401JC






108-95-2——————Phenol__________________111-44-4——————bis(2-Chloroethyl)Ether____95-57-8———————2-Chlorophenol____________541-73-1——————1,3-Dichlorobenzene________106-46-7——————1,4-Dichlorobenzene________100-51-6——————Benzyl Alcohol____________95-50-1———————1,2-Dichlorobenzene________95-4B-7———————2-Methylphenol____________108-60-1——————bis (2-Chloroisopropyl) Ether_106-44-5——————4-Methylphenol____________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane___________98-95-3———————Nitrobenzene_____________78-59-1———————Isophorone_______________88-75-5———————2-Nitrophenol______________105-67-9——————2,4-Dimethylphenol________65-85-0———————Benzoic Acid______________111-91-1——————bis(2-Chloroethoxy)Methane__120-83-2——————2,4-Dichlorophenol_________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8——————4-Chloroaniline___________87-68-3——————Hexachlorobutadiene_______59-50-7———————4-Chloro-3-Methylphenol_____91-57-6———————2-Methylnaphthalene________77-47-4———————Hexachlorocyclopentadiene___88-06-2———————2,4,6-Trichlorophenol______95-95-4———————2,4,5-Trichlorophenol______91-58-7———————2-Chloronaphthalene________88-74-4———————2-Nitroaniline____________131-11-3——————Dimethyl Phthalate________208-96-8——————Acenaphthylene____________606-20-2——————2,6-Dinitrotoluene________

101010101010101010101010101010105010101010101010101010501050101010




EPA SAMPLE NO;143

Lab Name: ACUREX CORP.EX671

] ib Code: ACUREX Case No.: 10505


I imple wt/vol: 1000 (g/mL) ML

Mvel: (low/med) LOW

V Moisture: not dec. ___ dec. ___

] :traction: (SepF/Cont/Sonc) CON1?

GPC Cleanup: (Y/N) N_ pH: __



CAS NO. COMPOUND


Lab File ID: EC100340UC






99-09-2———————3-Nitroaniline__________83-32-9.———————Acenaphthene___________51-28-5———————2 ,4-Dinitrophenol________100-02-7——————4-Nitrophenol_______132-64-9——————Dibenzofuran____________121-14-2——————2,4-Dinitrotoluene_______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene_______________~100-10-6——————4-Nitroaniline^__________534-52-1——————4,6-Dinitro-2-Methylphenol,86-30-6———————N-Nitrosodiphenylamine (1)"101-55-3——————4-Bromophenyl-phenylether_|118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene___________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene________________85-68-7———————Butylbenzylphthalate_____91-94-1——————3,3'-Dichlorobenzidine___56-55-3——————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis(2-Ethylhexyl)Phthalate117-84-0——————Di-n-Octyl Phthalate____~205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo (k) Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-39-5—————Indeno (1,2,3-cd) Pyrene53-70-3——————Dibenz (a ,h) Anthracene____191-24-2—————Benzo(g,h, i)Perylene_____


5010505010101010105050

1010501010101010102010101010101010101010

uuuuuuuuuu

uuuuuuuuuuuuuuuuuuuu

FORM I SV-2 1/87 Rev



144EPA SAMPLE NO.

i,ab Name: ACUREX CORP.EX671

ab Code: ACUREX


ample wt/vol: 1000 (g/mL) MLT-evel: (low/med) LOW

-» Moisture: not dec. ___ dec. ___

xtraction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) H_ pH: ___

________ Contract: 68-01-7416

Case No.: 10505 SAS No.: _____ SDG No.: EX671

TICs found:








CAS NUMBER . COMPOUND NAME RT EST. CONC. Q•

//0-/2.-3

2. -

H

ItA


IBSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET

Name: ACUREX CORP._________ Contract: 68-01-7416

EPA SAMPLE NO.

EX672



ample wt/vol: 1000 (g/mL) ML

T,evel: (low/med) LOW

•» Moisture: not dec. ___ dec. ___

;xtraction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) 1!_ pH: ___

SDG No.: EX671








108-95-2——————Phenol_________________111-44-4——————bis (2-Chloroethyl) Ether___95-57-8——————2-Chlorophenol__________541-73-1——————1,3-Dichlorobenzene______106-46-7——————1,4-Dichlorobenzene______100-51-6——————Benzyl Alcohol________•95-50-1——————1,2-Dichlorobenzene______95-48-7———————2-Methylphenol___________108-60-1—————bis(2-Chloroisopropyl)Ether_106-44-5——————4-Methylphenol__________~621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1——————Hexachloroethane_________98-95-3——————Nitrobenzene____________78-59-1——————Isophorone_____________88-75-5———————2-Nitrophenol____________105-67-9——————2,4-Dimethylphenol_______65-85-0———————Benzoic Acid_____________111-91-1——————bis(2-Chloroethoxy)Methane_120-83-2——————2,4-Dichlorophenol_______120-82-1——————1,2,4-Trichlorobenzene____91-20-3——————Naphthalene____________106-47-8——————4-Chloroaniline_________87-68-3——————Hexachlorobutadiene______59-50-7——————4-Chloro-3-Methylphenol___91-57-6——————2-Methylnaphthalene______77-47-4——————Hexachlorocyclopentadiene_88-06-2——————2,4,6-Trichlorophenol_____95-95-4——————2,4,5-Trichlorophenol_____91-58-7——————2-Chloronaphthalene______88-74-4——————2-Nitroaniline__________131-11-3—————Dimethyl Phthalate_______208-96-8——————Acenaphthylene__________'_606-20-2—————2,6-Dinitrotoluene_______

101010101010101010101010101010105010101010101010101010501050101010


FORM I SV-1 1/87 Rev,


Name: ACUREX CORP.____________ Contract: 68-01-7416

153EPA SAMPLE NO.

EX672

: ib Code: ACUREX Case No.: 10505 SAS No.:


i imple wt/vol: 1000 (g/ttL) ML

Level: (lov/med) LOW

-. Moisture: not dec. ___ dec. ___

retraction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) H_ pH:

SDG NO.: EX671








99-09-2——————3-Nitroaniline_________83-32-9——————Acenaphthene___________51-28-5——————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene_______________~100-10-6——————4-Nitroaniline_________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1)"101-55-3—————4-Bromophenyl-phenylether^J118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol________85-01-8——————Phenanthrene___________120-12-7——————Anthracene_____________84-74-2——————Di-n-Butylphthalate_____206-44-0——————Fluoranthene___________129-00-0—————Pyrene_______________85-68-7——————Butylbenzylphthalate____91-94-1——————3,3'-Dichlorobenzidine___56-55-3——————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis(2-Ethylhexyl)Phthalate117-84-0——————Di-n-Octyl Phthalate____~205-99-2——————Benzo (b) Fluoranthene_____207-08-9—————Benzo (X) Fluoranthene____50-32-8——————Benzo (a) Pyrene_________193-39-5——————Indeno (1,2,3-cd) Pyrene___53-70-3——————Dibenz (a ,h) Anthracene____191-24-2——————Benzo (g,h, i)Perylene_____

5010505010101010105050

101050101010101010201010610101010101010


UUUUUUUUUUU




154EPA SAMPLE NO.

lab Name: ACUREX CORP.EX672

; ib Code: ACUREX Case No.: 10505


i imple wt/vol: 1000 (g/mL) ML

T-ovel: (low/med) LOW

* Moisture: not dec. ___ dec. ___

: ctraction: (SepF/Cont/Sonc) CONT


Mimber TICs found: 92-J

Contract: fia-oi-7416







Dilution Factor: l.QO



//OH//r-

2- l.ir£;/) it IS



EPA SAMPLE NO





t-vel: (low/med) LOW




SDG No.: EX671

Lab Sample ID: EC1003403C

Lab File ID: EC1003403C






108-95-2——————Phenol__________________111-44-4———"——bis (2-Chloroethyl) Ether____95-57-8———————2-Chlorophenol____________541-73-1——————1,3-Dichlorobenzene________106-46-7——————1,4-Dichlorobenzene_______100-51-6——————Benzyl Alcohol____________95-50-1———————1,2-Dichlorobenzene________95-48-7———————2-Methylphenol____________108-60-1——————bis (2-Chloroisopropyl) Ether_106-44-5——————4-Methylphenol____________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene_____________78-59-1——————Isophorone______________88-75-5———————2-Nitrophenol____________105-67-9——————2,4-Dimethylphenol_________65-85-0———————Benzoic Acid_____________111-91-1——————bis (2-Chloroethoxy) Methane__120-83-2——————2,4-Dichlorophenol__________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8——————4-Chloroaniline__________87-68-3——————Hexachlorobutadiene59-50-7———————4-Chloro-3-Methylphenol____91-57-6——————2-Methylnaphthalene________77-47-4———————Hexachlorocyclopentadiene___88-06-2———————2,4, 6-Trichlorophenol_______95-95-4———————2,4,5-Trichlorophenol______91-58-7———————2-Chloronaphthalene________88-74-4———————2-Nitroaniline____________131-11-3——————Dimethyl Phthalate_________208-96-8——————Acenaphthylene____________606-20-2——————2,6-Dinitrotoluene_________

101010101010101010101010101010105010101010101010101010501050101010




Lab Name: ACUREX CORP.__________ Contract: 68*01-7416

EPA SAMPLE NO.

EX673



_ample vt/vol: 1000 (g/aL) ML

~evel: (low/med) LOW




SDG NO.: EX671








99-09-2———————3-Nitroaniline__________83-32-9———————Acenaphthene___________51-28-5———————2,4-Dinitrophenol________100-02-7——————4-Nitrophenol___________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene_______84-66-2——————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene______________~100-10-6——————4-Nitroaniline__________534-52-1——————4, 6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1)"101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol________85-01-8———————Phenanthrene___________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene_______________85-68-7———————Butylbenzylphthalate_____91-94-1———————3,3'-Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis (2-Ethylhexyl) Phthalate_117-84-0——————Di-n-Octyl Phthalate____"205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-39-5——————Indeno (1,2,3 -cd) Pyrene___53-70-3———————Dibenz (a, h) Anthracene____191-24-2——————Benzo(g,h,i)Perylene_____

5010505010101010105050101010501010101010102010101010101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu





EPA SAMPLE NO

Lab Name: ACUREX CORP, Contract: 68-01-7416EX673



ample wt/vol: 1000 (g/mL) MLT evel: (low/med) LOW

* Moisture: not dec. ___ dec. ___



SDG No.: EX671


Lab File ID: EC1O03403C





number TICs found: _JJ/CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L


A



I ib Name: ACUREX CORP.__________ Contract: 68-01-7416

EPA SAMPLE NO.

EX674

r-ib Code: ACUREX Case No.: 10505 SAS No.:


< imple wt/vol: 1000 (g/mL) ML


3 Moisture: not dec. ___ dec. ___

Extraction: (SepF/Cont/Sonc) CONT

Cleanup: (Y/N) H_ pH: ____

SDG No.: EX671








108-95-2——————Phenol___________________111-44-4——————bis(2-Chloroethyl)Ether____95-57-8———————2-Chlorophenol_____________541-73-1——————1,3-Dichlorobenzene________106-46-7——————1,4-Dichlorobenzene________100-51-6——————Benzyl Alcohol____________95-50-1———————1,2-Dichlorobenzene________95-48-7———————2-Methylphenol____________108-60-1——————bis (2-Chloroisopropyl) Ether_106-44-5——————4-Methylphenol____________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene_____________78-59-1——————Isophorone______________88-75-5———————2-Nitrophenol_____________105-67-9——————2,4-Dimethylphenol_________65-85-0———————Benzoic Acid______________111-91-1——————bis (2-Chloroethoxy) Methane__120-83-2——————2,4-Dichlorophenol_________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8——————4-Chloroaniline__________87-68-3——————Hexachlorobutadiene59-50-7——————4-Chloro-3-Methylphenol____91-57-6——————2-Methylnaphthalene_______77-47-4——————Hexachlorocyclopentadiene___88-06-2———————2,4,6-Trichlorophenol______95-95-4———————2,4,5-Trichlorophenol______91-58-7———————2-Chloronaphthalene________88-74-4———————2-Nitroaniline_____________131-11-3——————Dimethyl Phthalate________208-96-8——————Acenaphthylene____________606-20-2——————2,6-Dinitrotoluene_________

101010101010101010101010101010105010101010101010101010501050101010



1CSEMIVOIATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.






t Moisture: not dec. ___ dec. ___



SDG No.: EX671








99-09-2——————3-Nitroaniline__________83-32-9.——————Acenaphthene___________51-28-5———————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene_______________~100-10-6——————4-Nitroaniline__________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1)"101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene___________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene________________85-68-7——————Butylbenzylphthalate_____91-94-1———————3,3' -Dichlorobenzidine___56-55-3——•———Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis (2-Ethylhexyl) Phthalate117-84-0——————Di-n-Octyl Phthalate_____205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-3 9-5——————Indeno (1,2,3-cd) Pyrene___53-70-3———————Dibenz (a ,h) Anthracene____191-24-2——————Benzo(g,h,i)Perylene_____


5010505010101010105050

1010501010101010102010101010101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu




173EPA SAMPLE NO*

_ab Name: ACUREX CORP.

: ib Code: ACUREX Case No.: 10505


! imple wt/vol: 1000 (g/mL) 1


: Moisture: not dec. ___ dec.

7ctraction: (SepF/Cont/Sonc) J


SAS No.: SDG No. : EX671

GPC Cleanup: (Y/N) E_

. .mber TICs found: _2

pH:








CAS NUMBER . COMPOUND NAME RT EST. CONC. Q:

IIC -li~ 5 Sir £,37



-1OUEPA SAMPLE NO.

L-b Name: ACUREX CORP, Contract: 68-01-7416EX675



S mple wt/vol: 1000 (g/mL) ML_





SDG No.: EX671


Lab File ID: EC1Q03405C




Dilution Factor: 1*00 _


108-95-2——————Phenol___________________111-44-4——————bis (2-Chloroethyl) Ether____95-57-8———————2-Chlorophenol_____________541-73-1——————1,3-Dichlorobenzene________106-46-7——————1,4-Dichlorobenzene________100-51-6——————Benzyl Alcohol_____________95-50-1———————1,2-Dichlorobenzene________95-4'8-7———————2-Methylphenol_____________108-60-1——————bis (2-Chloroisopropyl) Ether_106-44-5——————4-Methylphenol____________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene_____________78-59-1———————Isophorone_______________88-75-5———————2-Nitrophenol_____________105-67-9——————2,4-Dimethylphenol_________65-85-0——————Benzoic Acid_____________111-91-1——————bis (2-Chloroethoxy) Methane__120-83-2——————2r4-Dichlorophenol________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3——————Naphthalene______________106-47-8——————4-Chloroaniline___________87-68-3———————Hexachlorobutadiene________59-50-7———————4-Chloro-3-Methylphenol____91-57-6——————2-Methylnaphthalene_______77-47-4———————Hexachlorocyclopentadiene___88-06-2———————2,4,6-Trichlorophenol______95-95-4———————2,4,5-Trichlorophenol______91-58-7———————2-Chloronaphthalene________88-74-4———————2-Nitroaniline____________131-11-3——————Dimethyl Phthalate________208-96-8——————Acenaphthylene____________606-20-2——————2,6-Dinitrotoluene________

101010101010101010101010101010105010101010101010101010501050101010




J.OAEPA SAMPLE NO.




ample wt/vol: 1000 (g/mL) ML


. Moisture: not dec. ___ dec. ___

"^traction: (SepF/Cont/Sonc) CONT


SDG NO.: EX671








99-09-2——————3-Nitroaniline__________83-32-9——————Acenaphthene___________51-28-5——————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate_________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene_______________~100-10-6——————4-Nitroaniline__________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1)~101-55-3——————4-Bromophenyl-phenylether_118-74-1—————Hexachlorobenzene_______87-86-5——————Pentachlorophenol_______85-01-8———————Phenanthrene____________120-12-7—————Anthracene____________84-74-2——————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0—————Pyrene_______________85-68-7——————Butylbenzylphthalate_____91-94-1——————3,3'-Dichlorobenzidine___56-55-3——————Benzo (a) Anthracene______218-01-9—————Chrysene______________117-81-7—————bis(2-Ethylhexyl)Phthalate117-84-0——————Di-n-Octyl Phthalate_____205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8——————Benzo (a) Pyrene__________193-39-5—————Indenofl, 2,3-cd) Pyrene___53-70-3——————Dibenz (a ,h) Anthracene____191-24-2—————Benzo(g,h, i)Perylene_____


5010505010101010105050101010501010101010102010101010101010101010





182EPA SAMPLE NO.

b »;ame: ACUREX CORP. Contract: 68-01-7416EX675

b :ode: ACUREX Case No.: 10505 SAS No.:

trix: (soil/water) WATER

si e wt/vol: 1000 (g/mL) ML

/el: (low/med) LOW

ic.sture: not dec. ___ dec. ___

n ction: (SepF/Cont/Sonc) CONT

: Cleanup: (Y/N) H_ pH: ____

SDG No.: EX671







*wr TICs found: _gCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER - COMPOUND NAME RT«£== = = ===

EST. CONC. Q

/' - L



EPA SAMPLE NO

I-b Name: ACUREX CORP.EY768

Lab Code: ACUREX Case NO.: 10505

* trix: (soil/water) WATER

Sample wt/vol: 1000 (g/raL)

I :vel: (low/iced) LOW__

?• Moisture: not dec. ___ d<?c. ___

Extraction: (SepF/Cont/Sonc) fiftHI

c >C Cleanup: (Y/N) jj_ pH: ___

Contract: $8-Ol-7416_

SAS No.: ______ SDG No,t KX671

CAS NO. COMPOUND

lab Sample ID: g81Qfl346

Lab File ID: EC10Q3406C


Date Extracted: io/lQ/88

Date Analyzed: 1Q/26/8Q

Dilution Factor: i.oo


108-95-2 —————— Pnenol111-44-4 —————— bis (2-Chloroethyl> Ether95-57-8 ——————— 2-Chlorophenol __541-73-1-- ———— 1.3-Dichlorobenzene106-46-7 —— -•*- — lf 4-Dichlorobenzene100-51-6 —————— Benzyl Alcohol95-50-1 — ————— 1,2-Dichlorobenzene95-48-7 —————— 2-Methylphenol108-60-1 —————— bis (2-Chloroisopropyl) Ether _106-44-5 —————— 4-Methvlphenol621-64-7 —————— N-Nitroso-Di-n-Propylamine __

98-95-3 —————— '-Nitrobenzene78-59-l-< —————— Isophorone88-75-5 —————— 2-Nitrophenol105-67-9*- ———— 2 , 4-Dimethylphenol65-85-0 —— - ———— Benzoic Acid111-91-1 ————— bis (2-Chloroethoxy) Methane120-83-2--- — ——2 f 4-Dichlorophenol120-82-1 —————— lP2.4-Trichlorobenzene91-20-3 —————— Naphthalene87-6fl-3 ——— - ——— Hexachlorobutadienc . ._._. ._59-50-7 —————— 4-Chloro-3-Methylphenol9i~S7~6 —————— 2-Methylnaphthalene ^ ....77-47-4 —————— HexachlorocyclODentadienaas-oe-2 ——————— 2 , 4 f 6-Trichlorophenol95-45-4 —————— -2 f 4 r 5-Trichlorophenol . . .fti-58-7-. ———— --2-Chloronaphthalene „,.„ „BB-74-4— - - ————— 2-Nitroaniline131-11-3 —— - —— Dimethyl Phthalate . „ __snft-Qfi-a —————— Acenaphthylene ,.06-20-?-- ———— ?,6-Dinitrotoluene _ . _ .

101010101010101010101010101010105010101010101010101010501050101010

uuuuuuuuuuuuuuuuuuuuuuuu g:u > -u uiu °cJJ w ;U «(uuuu

COCJ>

GQUJLa.

FOPM I SV-1 1/87 Rev,


Lab Name: ACUREX CORP,__________ Contract: ea-oi-7416

EPA SAMPLE NO

EY768




SDG No.: EX671

( low/med) LOW

% Moisture: not dec. ___ dec.

I traction: (SepF/Cont/Sonc)

GPC Cleanup: (Y/N) fi _ pH:

CAS NO. COMPOUND








99-09-2———————3-Nitroaniline__________83-32-9.———————Acenaphthene___________51-28-5———————2,4-Dinitrophenol________100-02-7———————4-Nitrophenol____________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene______________~100-10-6——————4-Nitroaniline_________534-52-1——————4,6-Dinitro-2-Methylphenol86-30-6———————N-Nitrosodiphenylamine (1)"101-55-3——————4-Bromophenyl-phenylether_J118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene___________120-12-7——————Anthracene____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene________________85-68-7———————Butylbenzylphthalate_____91-94-1———————3,3 '-Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis (2-Ethylhexyl) Phthalate117-84-0——————Di-n-Octyl Phthalate____"205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo (k) Fluoranthene_____50-32-8——————Benzo (a) Pyrene_________193-39-5——————Indeno (1,2,3-cd) Pyrene___53-70-3——————Dibenz (a ,h) Anthracene____191-24-2——————Benzo (g,h, iJPerylene_____

5010505010101010105050101010501010101010142010101010101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu





EPA SAMPLE NO

L b Name: ACUREX CORP. Contract: 68-01-7416EY768






E"traction: (SepF/Cont/Sonc) CONT

Cleanup: (Y/N) H_ pH: ____

SDG No.: EX671







,mber TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER - COMPOUND NAME RT EST. CONC. Q-



EPA SAMPLE NO.

I b Name: ACUREX CORP.

I-b Code: ACUREX Case No.: 10505


S mple wt/vol: 1000 (g/mL)

Leva1: (1ow/med) LOW

* Moisture: not dec. ___ dec.

Extraction: (SepF/Cont/Sonc)

G-rC Cleanup: (Y/N) fi_ pH:

EY769Contract: 68-01-7416


CAS NO. COMPOUND








1 Oft— Q^— 9— — — —AUO — :>o— *— — —111-44-4 ———*f3~3 / »{j

541-73-1 ———106-46-7 ———100-51-6 ———95-50-1 ————95-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————^ O — y^ J/ o — O :* — .1. — — — —DO "? C C

105-67-9 ————65-85-0 ————111-91-1 ———

^ A A* *» «*106-47-8 ———

91-57-6 ————77-47-4 ————

95-95-4 ————

88-74-4 ————131-11-3 ———

606-20-2 ———

——— Phenol——— bis (2-Chloroethyl) Ether——— 2-Chlorophenol——— 1 , 3-Dichlorobenzene——— 1,4-Dichlorobenzene——— Benzyl Alcohol——— 1 , 2-Dichlorobenzene——— 2-Methylphenol——— bis ( 2 -Chloroisopropyl ) Ether _——— 4-Methylphenol——— N-Nitroso-Di-n-Propylamine __——— Hexachloroethane——— Nitrobenzene—— I sophor one——— 2-Nitrophenol——— 2 , 4-Dimethylphenol

—— bis (2-Chloroethoxy) Methane __—— 2 , 4-Dichlorophenol——— 1 , 2 , 4-Trichlorobenzene——— Naphthalene——— 4-Chloroaniline—— Hexachlorobutadiene——— 4-Chloro-3-Methylphenol—— 2-Methylnaphthalene——— Hexachlorocyclopentadiene ___—— 2 , 4 , 6-Trichlorophenol——— 2 , 4 , 5-Trichlorophenol——— 2-Chloronaphthalene——— 2-Nitroaniline——— Dimethyl Phthalate—— Acenaphthylene——— 2 , 6-Dinitrotoluene

101010101010101010101010101010105010101010101010101010501050101010




EPA SAMPLE NO.

Name: ACUREX CORP. Contract: 68-01-7416EY769

Lab Code: ACUREX Case No.: 10505 SAS No.:

Me rix: (soil/water) WATER

wt/vol: 1000 (g/mL) ML_

SDG No.: EX671

( low/med) LOW

i :oisture: not dec. ___

Extraction: (SepF/Cont/Sonc)

^F Cleanup: (Y/N) H _

dec.

CONT

CAS NO. COMPOUND








99-09-2———————3-Nitroaniline__________83-32-9———————Acenaphthene___________51-28-5-——————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene_______________~100-10-6——————4-Nitroaniline__________534-52-1——————4, 6-Dinitro-2-Methylphenol_86-30-6———————N-Nitrosodiphenylamine (1}~101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene____________120-12-7——————Anthracene______________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene_______________85-68-7——————Butylbenzylphthalate_____91-94-1———————3,3'-Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis(2-Ethylhexyl)Phthalate117-84-0——————Di-n-Octyl Phthalate____~_205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8——————Benzo (a) Pyrene_________193-39-5——————Indenofl, 2,3-cd) Pyrene___53-70-3———————Dibenz (a ,h) Anthracene____191-24-2——————Benzo (g,h, i) Perylene_____


5010505010101010105050101010501010101010102010101010101010101010

uuuuuuuuuuuuUuuuuuuuuuuuuuuuuuuu


0? 'C6''1956 09-09 10802 US p. 14



EPA SAMPLE NO,

Name: ACUREX CORP.

Lao Code: ACUREX Case No.:

K< :rix: (soil/water) HATER

Sample wt/vol: 1000 (g/mL) ML

1> 'el: (low/med) LQW

t Moisture: not dec. ___ dec. ___

Extractions (SepF/Cont/Sonc) CONS

G3 : Cleanup: (Y/N) JJ_ pH: „__

Ni iber TICs found: 0


SAS No.: ____

EV769

____ SDG No.: HtfiZL


Lab File ID:

Date Received:

Date Extracted: 1J710/88


Dilution Factor: 3 )Q_


CAS NUMBER COMPOUND NAME RT EST. CONC.=s=^^ciâs«e5»»t*«»

WtXtoM&J f . g if. to1.H /r

/ J

I.It

V f.fplo.\oJO. 1*

f**!5

oft-

/'.//.

FORM x SV-TIC Rev.

** \JIB

SEMIVOIATILE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE NO,


; ib Code: ACUREX Case No.: 10505 SAS No.:


; imple vt/vol: 1000 (g/mL) ML


. Moisture: not dec. ___ dec. ___

"xtraction: (SepF/Cont/Sonc) CONT


SDG No.: EX671








108-95-2——————Phenol___________________111-44-4——————bis (2-Chloroethyl) Ether____95-57-8———————2-Chlorophenol____________541-73-1——————1,3-Dichlorobenzene________106-46-7——————1,4-Dichlorobenzene________100-51-6——————Benzyl Alcohol____________95-50-1———————1,2-Dichlorobenzene________95-48-7———————2-Methylphenol____________108-60-1——————bis (2-Chloroisopropyl) Ether_106-44-5——————4-Methylphenol____________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene_____________78-59-1———————Isophorone_______________88-75-5———————2-Nitrophenol____________105-67-9——————2,4-Diroethylphenol________65-85-0———————Benzoic Acid_____________111-91-1——————bis (2-Chloroethoxy) Methane__120-83-2——————2,4-Dichlorophenol________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene_____________106-47-8——————4-Chloroaniline87-68-3——————Hexachlorobutadiene_______59-50-7———————4-Chloro-3-Methylphenol____91-57-6———————2-Methylnaphthalene________77-47-4———————Hexachlorocyclopentadiene___88-06-2———————2,4,6-Trichlorophenol______95-95-4———————2,4,5-Trichlorophenol______91-58-7———————2-Chloronaphthalene________88-74-4———————2-Nitroaniline____________131-11-3——————Dimethyl Phthalate________208-96-8——————Acenaphthylene___________606-20-2——————2,6-Dinitrotoluene________

101010101010101010101010101010105010101010101010101010501050101010




221EPA SAMPLE NO.

3 Name: ACUREX CORP. Contract: 68-01-7416EY770

ode: ACUREX Case No.: 10505 SAS No.: SDG No.: EX671

:rix: (soil/water) WATER

ip_ s wt/vol: 1000 (g/mL) ML

•e" : {low/med) LOW

oisture: not dec. ___ dec. ___

r ztion: (SepF/Cont/Sonc) CONT

Cleanup: (Y/N) N_ pH: ___

CAS NO. COMPOUND








99-09-2 ————^ v * »»83-32-9 ————w «^ ** *> ^

51-28-5 ————100-02-7 ———132-64-9 ——— •^ -j ft w •• y^ * ^ » ft.121-14-2 ---•84-66-2 ———— -7005-72-3 ——Qfi-7'j— 7 — ,. — — -

100-10-6 ——— •534-52-1 ——— •^ v _/ «• j.

101-55-3 ——— •118-74-1 ——— •87-86-5 ———— •oD — Ul — o — — — — — "^ f\ ^ ^120-12-7 — ---84-74-2 ———— -206-44-0 ——— •129-00-0 ——— -oD— oo— /—————"91-94-1 ———— '•56-55-3 ———— -218-01-9 ——— -

117-84-0 ——— -205-99-2 —— —— -*> V ^ •* ff

207-08-9 ——— -

193-39-5 ——— -53-70-3 ———— -^ rt ^ M *\191-24-2 ——— •

—— 3-Nitroaniline

—— 2 , 4-Dinitrophenol—— 4-Nitrophenol—— Dibenzofuran—— 2 , 4-Dinitrotoluene—— Diethylphthalate—— 4-Chlorophenyl-phenylether—— Fluorene—— 4-Nitroaniline—— 4 , 6-Dinitro-2-Methylphenol __—— N-Nitrosodiphenylamine (1) __—— 4-Bromophenyl-phenylether——— Pentachlorophenol—— Phenanthrene—— Anthracene—— Di-n-Butylphthalate—— Fluoranthene

fj*. CJIC

—— Butylbenzylphthalate—— 3 . 3 ' -Dichlorobenzidine—— Benzo (a) Anthracene

—— bis(2-Ethylhexyl)Phthalate __—— Di-n-Octyl Phthalate—— Benzo(b) Fluoranthene—— Benzo (k) Fluoranthene—— Benzo f a ) Pyrene—— Indeno (1,2,3 -cd) Pyrene—— Dibenz (a, h) Anthracene—— Benzo (g , h , i ) Perylene

5010505010101010105050101010501010101010102010101010101010101010


1) - Cannot be separated from Diphenylamine


108021IS P.17

IPSEMIVOIATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE MO.

Name: CORP, Contract: 68-01-7416EY770

Lab Code: ACUREX

M. :rix; (coil/water)

Sample wt/vol: 1000

U> /e1: (1 ow/med) LOW

I Moisture: not dec. ___

Case No*; 10505 SAS No.: SDG No. i BX671

dec.

Extraction: (SepP/Cont/Sonc) CONT

G : Cleanup: (Y/N) N . pH: ___

TICs found:

Lab Sample ID: flaiQQ348

Lab Kile ID: ^C1QO34Q8JC

Date Received: J.Q/07/B&



Dilution Factor: jj-QQ


CAS NXJH&ER COMPOUND NAME RT EST* CONC.

</

' * ~t

FORM I SV-TIC 1/87 Rev,

10802118 P.13


EPA SAMPLE NO.

EY772L D Name: ACtjREX CORP. _..__. Contract: 68-01-7416

Lab Code: ftCUREX Case Ko. : 10505 SAS No.: ______ SDG NO.: EX671

M trix: (soil/water)

Sample wt/vol: 3.000 (g/ntL) ML

(low/toed) LOW

% Moisture: not dec. _ _ dec* ___

Extraction: (SepF/Cont/Sonc) CONT

G C Cleanup: (Y/N) H _ pH:




Date Extracted: lo/10/88

Date Analyzed; 10/31/88

Dilution Factor: J..OQ

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/fr

108-95-2—————Phenol____________111-44-4——————bis (2-Chloroethyl) Ether95-57-8——————2-Chlorophenol______^541-73-1——————1,3-Dichlorobenzene___106-46-7 —————— 1,4-Dichlorobenzene___100-51-6———•——Benzyl Alcohol95-50-1———————1,2-Dichlorofrenzene95-48-7-—————2~Methylphenol__________108-60-1——•———bis(2-Chloroisopropyl)Ether_106-44-5——————4-Methylphenol___________621-64-7——————N-Nitroso~Di-n-Propylaraine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene___ „_______78-59-1———————Isophorone_____^_______„_._88-75-5-——————2-Nitrophenol.____________105-67-9——————2,4-Dimethylphenol^________65-85-0————•——Benzole Acid_____________111-91-1—————bi9(2-Chloroethoxy)M«than«__120-83-2——•———2,4-Dichlorophenol________120-82-1-—————1,2,4-Trichlorobenzene_____91-20-3———-——Naphthalene____________106-47-8"-'————^4-Chloroaniline__________87-68-3——•>•———Hexachlorobutadiene_______59-50-7——————4-Chloro-3*Methylphenol____91-57-6-——————2-Methvlnaphthalene77-47-4———-——Hexachlorocyclopentadlene___88-06-2——--'—2,4,6-Triohlorophenol_____95-95-4——————-2,4,5-Trichlorophenol______91-58-7———————2"Chloronaphthalene ____88-74-4—r————2-Nitroaniline___________131-11-3——————Dimethyl Phthalate^_________208-96-8——————Acenaphthylene__________606-20-2——————2,6-Dinitrotoluene__-______

101010101010101010101010101010105010101010101010101010501050101010

Q

uuuuuuuuu"Juuuuuuuuuuuuuuuuuuuuuuu

b 25O

t! enUl

FORM I SV-1 1/87 Rev


227EPA SAMPLE NO.

Lab Name: ACUREX CORP.EY771

ab Code: ACUREX Case No.: 10505


âmple wt/vol: 1000 (g/mL) ML

*evel: (low/med) LOW


:xtraction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) fi_ pH: ___



CAS NO. COMPOUND








108-95-2——————Phenol___________________111-44-4——————bis (2-Chloroethyl) Ether____95-57-8——————2-Chlorophenol___________541-73-1——————1,3-Dichlorobenzene_______106-46-7——————1,4-Dichlorobenzene_______100-51-6——————Benzyl Alcohol____________95-50-1———————1,2-Dichlorobenzene________95-48-7——————2-Methylphenol___________108-60-1——————bis (2-Chloroisopropyl) Ether_106-44-5——————4-Methylphenol___________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1———————Hexachloroethane__________98-95-3———————Nitrobenzene_____________78-59-1———————Isophorone_______________88-75-5———————2-Nitrophenol______________105-67-9——————2,4-Dimethylphenol________65-85-0———————Benzoic Acid_____________111-91-1——————bis (2-Chloroethoxy) Methane__120-83-2——————2,4-Dichlorophenol________120-82-1——————1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8——————4-Chloroaniline___________87-68-3——————Hexachlorobutadiene_______59-50-7———————4-Chloro-3-Methylphenol_____91-57-6——————2-Methylnaphthalene_______77-47-4———————Hexachlorocyclopentadiene___88-06-2——————2,4,6-Trichlorophenol______95-95-4———————2,4,5-Trichlorophenol______91-58-7———————2-Chloronaphthalene_______88-74-4——————2-Nitroaniline___________131-11-3——————Dimethyl Phthalate________208-96-8——————Acenaphthylene___________606-20-2——————2,6-Dinitrotoluene________

101010333410101010101010101010105010101010101010101010501050101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuu


1CSEMIVOIATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ACUREX CORP*EY771

I b Code: ACUREX Case No.: 10505


S mple vt/vol: 1000 (g/mL) ML

I -vel: (low/med) LOW


I traction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) fi_ pH: __

Contract: 68-01*7416


CAS NO. COMPOUND








99-09-2———————3-Nitroaniline__________83-32-9———————Acenaphthene___________51-28-5:——————2,4-Dinitrophenol_______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene_______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene_______________"100-10-6——————4-Nitroaniline__________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6———————N-Nitrosodiphenylamine (1)_101-55-3——————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5————————Pentachlorophenol________85-01-8———————Phenanthrene___________120-12-7——————Anthracene____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene_______________85-68-7——————Butylbenzylphthalate_____91-94-1——————3,3'-Dichlorobenzidine___56-55-3———————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis (2-Ethylhexyl) Phthalate^117-84-0——————Di-n-Octyl Phthalate____"205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-39-5——————Indeno(l, 2,3-cd) Pyrene___53-70-3———————Dibenz(a,h)Anthracene____191-24-2——————Benzo (g,h, i) Perylene_____


50105050101010101050

\o1010501010101010102010101010101010101010




229EPA SAMPLE NO.

Lao Name: ACUREX CORP. Contract: 68-01-7416EY771

L t> Code: ACUREX Case No.: 10505 SAS No.:


S nple wt/vol: 1000 (g/mL) ML

I~vel: (low/med) LOW




SDG No.: EX671







i ober TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L


//o - /a S~-

- 47 / f.<3/.

/o

if

//. OfII. 3**

32-

to

/r.73

//.

FORM I SV-TIC 1/87 Rev



259EPA SAMPLE NO.

EY772



ample vt/vol: 1000 (g/mL) MLT evel: (low/med) LOW

-» Moisture: not dec. ___ dec. ___



SDG No.: EX671








99-09-2———————3-Nitroaniline__________83-32-9———————Acenaphthene____________51-28-5———————2,4-Dinitrophenol________100-02-7——————4-Nitrophenol___________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene_______84-66-2———————Diethylphthalate_________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene______________100-10-6——————4-Nitroaniline__________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6———————N-Nitrosodiphenylamine (1)_101-55-3——————4-Broiaophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol________85-01-8———————Phenanthrene___________120-12-7——————Anthracene____________84-74-2———————Di-n-Butylphthalate______206-44-0——————Fluoranthene___________129-00-0——————Pyrene________________85-68-7———————Butylbenzylphthalate_____91-94-1———————3,3'-Dichlorobenzidine___56-55-3——————Benzo (a) Anthracene______218-01-9——————Chrysene______________117-81-7——————bis(2-Ethylhexyl)Phthalate117-84-0——————Di-n-Octyl Phthalate_____205-99-2——————Benzo (b) Fluoranthene_____207-08-9——————Benzo (k) Fluoranthene_____50-32-8———————Benzo(a)Pyrene__________193-39-5——————Indeno (1,2,3-cd) Pyrene___53-70-3———————Dibenz(a,h)Anthracene____191-24-2——————Benzo(g,hf i)Perylene_____


5010505010101010105050101010501010101010102010101010101010101010





260EPA SAMPLE NO.





I-vel: (low/med) LOW


I traction: (SepF/Cont/Sonc) CONT


SDG No.: EX671







TICs found: _yCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER COMPOUND NAME RT:==s=====

EST. CONC. Q

I 10-12.'} f


330ID

PESTICIDE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

EX671

La- Code: ACUREX Case No.: 10505 SAS No.:

*a rix: (soil/water) WATER


Le al: (low/med) LOW

fe Moisture: not dec. _ dec. _

S> raction: (SepF/Cont/Sonc) CONT

SF~ Cleanup: (Y/N) H_ pH: ___

SDG No.: EX671

Lab Sample ID: EX671A

Lab File ID: _____

CAS NO. COMPOUND






319-84-6——————alpha-BHC_________319-85-7——————beta-BHC__________319-86-8——————delta-BHC_________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor________\309-00-2——————Aldrin___________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1———————Dieldrin_________72-55-9————————4,4'-DDE__________72-20-8———————Endrin___________33213-65-9————Endosulfan II_____72-54-8————————4,4'-DDD__________1031-07-8—————Endosulfan sulfate_50-29-3————————4,4'-DDT__________72-43-5——————Methoxychlor_____53494-70-5————Endrin ketone_____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2—————Aroclor-1016______11104-28-2—————Aroclor-1221______11141-16-5————Aroclor-1232______53469-21-9————Aroclor-1242______12672-29-6————Aroclor-1248______11097-69-1————Aroclor-1254______11096-82-5————Aroclor-1260

.050

.050

.050

.050

.050

.050

.050

.0500.100.100.100.100.100.100.100.500.100.500,501.00.500.500.500.500.501.01.0

UUUUUUUUUUUUUUUUUUUUUUUUUUU

FORM I PEST 1/87 Rev.

335ID

PESTICIDE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE NO.


_ob Code: ACUREX Case No.: 10505 SAS No.:

: itrix: (soil/water) WATER


jvel: (low/med) LOW


^traction: (SepF/Cont/Sonc) CONT

-?C Cleanup: (Y/N) H_ pH: ___

SDG No.: EX671


Lab File ID: _____






319-84-6——————alpha-BHC________319-85-7——————beta-BHC_________319-86-8——————delta-BHC________58-89-9——————gamma-BHC (Lindane)76-44-8———————Heptachlor________\309-00-2——————Aldrin___________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1——————Dieldrin________72-55-9———————4, 4'-DDE_________72-20-8———————Endrin__________33213-65-9————Endosulfan II_____72-54-8————————4,4'-DDD__________1031-07-8—————Endosulfan sulfate_50-29-3————————4,4'-DDT__________72-43-5——————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2————Aroclor-1016______11104-28-2————Aroclor-1221______11141-16-5————Aroclor-1232______53469-21-9————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1————Aroclor-1254______11096-82-5————Aroclor-1260

.050

.050

.050

.050,050.050.050.0500.100.100.100.100.100.100.100.500.100.500.501.0

0.500.500.500.500.501.01.0

uuuuuuuuuuuuuuuuuuuuuuuuuuu



EPA SAMPLE NO

Lab Name: ACUREX CORP, Contract: 68-01-7416EX673




evel: (low/med) LOW




SDG No.: EX671


Lab File ID: _____






319-84-6——————alpha-BHC________319-85-7——————beta-BHC_________319-86-8———————delta-BHC________58-89-9———————gamma-BBC (Lindane)76-44-8———————Heptachlor_______'309-00-2——————Aldrin___________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1———————Dieldrin_________72-55-9————————4 , 4 ' -DDE__________72-20-8———————Endrin___________33213-65-9—————Endosulfan II_____72-54-8———————4,4'-DDD_________1031-07-8—————Endosulfan sulfate_50-29-3————————4, 4'-DOT__________72-43-5———————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2—————Aroclor-1016______11104-28-2————Aroclor-1221_____11141-16-5—————Aroclor-1232______53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1—————Aroclor-1254______11096-82-5—————Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.100.500.100.500.501.0

0.500.500.500.500.501,01.0


FORM I PEST 1/87 Rev


345EPA SAMPLE NO.


,ab Code: ACUREX Case No.: 10505 SAS No.:


dample wt/vol: 1000 (g/mL) ML

jevel: (low/med) LOW


:xtraction: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) E_ pH: ___

SDG No.: EX671


Lab File ID: ______






*>X7 O3 /

76-44-8 —————309-00-2 ————1024.-57-3 ———y 3 y yo o60-57-1 —————

33213-65-9 ——72-54-8 —————1031-07-8 ———50-29-3 —————72-43-5 —————53494-70-5 ——5103-71-9 ———f < /\ •» "i * •%8001-35-2 ———1 *i £*7 j| 11 ^

11104-28-2 ——11141-16-5 ——53469-21-9 ——

11097-69-1 ——

_ T — *1* <K nil/1*—— alpna-BHCW**4-« Dtl/— — — oe t a— onL.J«.l « BU/---delta-Brie

—— aamma-BHC (Lindane)—— Heptachlor—— Aldrin—— Heptachlor epoxide—— Endosulfan I—— Dieldrin—— 4. 4 '-DDE—— Endrin—— Endosulfan II.. —— 4 4 '-ODD^ f fcSWk

—— Endosulfan sulfate—— 4, 4 '-DOT—— Methoxychlor—— Endrin ketone—— a . Chlordane—— a . Chlordane—— Toxaphene—— Aroclor-1016—— Aroclor-1221—— Aroclor-1232

k WBdktfW^ AW 1 O A O—— AroClOr- 1242% M>d&«*^ MW 1 Jl O~— Arocior-1248

— — — lT*rtr»1 fiT*— 1 554Ai. WWXWA. X*— »••

—— Aroclor-1260

0.0500.0500.0500,0500.0500.0500.0500.0500*100.100.100,100,100,100.100.500.100,500,501.0

0.500.500.500.500.501.01.0





350EPA SAMPLE NO.

EX675

L, •> Code: ACUREX Case No.: 10505 SAS No.:



L /el: (low/med) LOW

SDG No.: EX671


Lab File ID: _____

% Moisture: not dec. _

E: fraction: (SepF/Cont/Sonc)

GPC Cleanup: (Y/N) H _

dec.

CONT

CAS NO. COMPOUND






319-84-6——————alpha-BHC_________319-85-7——————beta-BHC_________319-86-8———————delta-BHC_________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______\309-00-2——————Aldrin___________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1———————Dieldrin_________72-55-9————————4 , 4 ' -DDE__________72-20-8———————Endrin___________33213-65-9—————Endosulfan II_____72-54-8———————4,4'-ODD________1031-07-8—————Endosulfan sulfate_50-29-3————————4 , 4 '-DOT__________72-43-5———————Methoxychlor_____53494-70-5—————Endrin ketone_____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2————Aroclor-1016_____11104-28-2—————Aroclor-1221______11141-16-5————Aroclor-1232______53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1————Aroclor-1254______11096-82-5————Aroclor-1260______

.050

.050

.050,050.050.050,050,0500.100.100.100.100.100.100.100.500.100.500.501.0

0.500.500.500.500.501.01.0



Name: ACUREX CORP.__________ Contract: 68-01*7416

355EPA SAMPLE NO.

EY768

,_ab Code: ACUREX Case No.: 10505 SAS No.: SDG No.: EX671

; itrix: (soil/water) WATER


avel: (low/med) LOW


^xtraction: (SepF/Cont/Sonc) CONT

PC Cleanup: (Y/N) J|_ pH: ___

Lab Sample ID: EY768A

Lab File ID: _____

CAS NO. COMPOUND






319-84-6——————alpha-BHC_______319-85-7——————beta-BHC_________319-86-8——————delta-BHC________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______\309-00-2——————Aldrin__________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1———————Dieldrin________72-55-9————————4, 4'-DDE__________72-20-8———————Endrin__________33213-65-9—————Endosulfan II_____72-54-8———————4, 4'-ODD_______1031-07-8——————Endosulfan sulfate_50-29-3————————4, 4'-DOT__________72-43-5———————Methoxychlor_____53494-70-5—————Endrin ketone_____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2—————Aroclor-1016______11104-28-2—————Aroclor-1221______11141-16-5—————Aroclor-1232______53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1—————Aroclor-1254______11096-82-5—————Aroclor-1260

0.0.0.0.0.0.0.0.00000000000

00000

050050050050050050050050.10.10.10.10.10.10.10.50.10.50.501.0.50.50.50.50.501.01.0




360EPA SAMPLE NO.


Lcu3 Code: ACUREX Case No.: 10505 SAS No.:

M, :rix: (soil/water) WATER


L «1: (low/med) LOW


E-wcraction: (SepF/Cont/Sonc) CONT

G : Cleanup: (Y/N) JJ_ pH: ___

SDG NO.: EX671


Lab File ID: _____





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/^

319-84-6——————alpha-BHC________319-85-7——————beta-BHC_________319-86-8——————delta-BHC_________58-89-9———————gamma-BHC (Lindane)76-44-8———————Heptachlor_______\309-00-2——————Aldrin___________1024—57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1———————Dieldrin_________72-55-9————————4, 4'-DDE__________72-20-8———————Endrin___________33213-65-9—————Endosulfan II_____72-54-8———————4 , 4 '-DDD_________1031-07-8—————Endosulfan sulfate_50-29-3———————4,4'-DDT_________72-43-5———————Methoxychlor_____53494-70-5————Endrin ketone_____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2—————Aroclor-1016______11104-28-2————Aroclor-1221_____11141-16-5————Aroclor-1232______53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1—————Aroclor-1254______11096-82-5————Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.100.500.100.500.501.00.500.500.500.500.501.01.0




365EPA SAMPLE NO.



K-.trix: (soil/water) WATER

Sample vt/vol: 1000 (g/mL) ML

I ivel: (low/med) LOW


I rtraction: (SepF/Cont/Sonc) CONT

Cleanup: (Y/N) H_ pH: ___

SDG No.: EX671


Lab File ID: _______

Date Received: 01/01/8g



Dilution Factor: l.oo


319-84-6——————alpha-BHC________319-85-7——————beta-BHC_________319-86-8——————delta-BHC_________58-89-9——————gamma-BBC (Lindane)76-44-8———————Heptachlor________\309-00-2——————Aldrin___________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I______60-57-1——————Dieldrin_________72-55-9————————4, 4'-DDE__________72-20-8———————Endrin___________33213-65-9————Endosulfan II_____72-54-8———————4,4'-DDD_________1031-07-8—————Endosulfan sulfate_50-29-3————————4,4'-DDT___________72-43-5———————Methoxychlor______53494-70-5————Endrin ketone____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2—————Aroclor-1016______11104-28-2————Aroclor-1221_____11141-16-5————Aroclor-1232______53469-21-9————Aroclor-1242______12672-29-6————Aroclor-1248______11097-69-1————Aroclor-1254______11096-82-5————Aroclor-1260____

.050

.050

.050

.050

.050

.050

.050

.0500.100.100.100.100.100.100.100.500.100.500.501.0

0.500.500.500.500.501.01.0


370ID

PESTICIDE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

EY771

,ab Code: ACUREX Case No.: 10505 SAS No.:



jevel: (low/med) LOW


ixtraction: (SepF/Cont/Sonc) CONT


SDG No.: EX671


Lab File ID: _____






319-84-6 ————

KO_OQ.O_..._.

76-44-8 —————309-00-2 ————1024.-57-3 ———

60-57-1 —————72-55-9 —————— •i ft ** -/ ;»/ — u— o33213-65-9 ——72-54—8- —————If* *J T W

1031-07-8 ———•» * •» f72-43-5 ———— -53494-70-5 ——5103-71-9 ———5103-74-2- —— -• A W « / •• •>

8001-35-2 ———1 «•» »T J 44 *S

11104-28-2 ——11141-16-5 ——53469-21-9 ——

11097-69-1 ——11096-82-5 ——

K 1 V*lt IK BUS*- — •aipna-oncW^4»« QUO— — — oeta— Bnu

—— delta-BHC—— qamma-BHC (Lindane)—— Heptachlor—— Aldrin—— Heptachlor epoxide—— Endosulfan I—— Dieldrin—— 4. 4 '-DDE—— Endrin—— Endosulfan II—— 4,4'-DDD—— Endosulfan sulfate

4 4 '— nivrf *i LsLJl

—— Methoxychlor—— Endrin ketone—— a . Chlordane—— a . Chlordane—— Toxaphene—— Aroclor-1016

% KA.K *^1^.W> ^ O 1— • — Arocior-1221—— Aroclor-1232—— Aroclor-1242—— Aroclor-1248— — — iT*r»cl nr*— 1 254/VJL \J\f^\J^ ^ > «**4

—— Aroclor-1260

0.0500.0500.0500.0500.0500.0500.0500.0500.100.100.100.100.100.100.100.500.100.500.501.00.500.500.500.500.501.01.0

UuUuuuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST 1/87 Rev,


O 4DEPA SAMPLE NO.




S^Jiple wt/vol: 1000 (g/mL) ML

L /el: (low/med) LOW



GPC Cleanup: (Y/N) H_ pH: ___

SDG No.: EX671


Lab File ID: _____






319-84-6———————alpha-BHC________319-85-7———————beta-BHC_________319-86-8——————delta-BHC________58-89-9———————gamma-BBC (Lindane)76-44-8———————Heptachlor_______\309-00-2——————Aldrin___________1024-57-3—————Heptachlor epoxide_959-98-8——————Endosulfan I_____60-57-1———————Dieldrin________72-55-9 ———————— 4 , 4 ' -DDE__________72-20-8———————Endrin___________33213-65-9—————Endosulfan II_____72-54-8————————4,4'-DDD__________1031-07-8—————Endosulfan sulfate_50-29-3————————4 , 4 ' -DDT__________72-43-5———————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————a. Chlordane_____5103-74-2—————g. Chlordane_____8001-35-2—————Toxaphene________12674-11-2—————Aroclor-1016______11104-28-2————Aroclor-1221_____11141-16-5—————Aroclor-1232______53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1—————Aroclor-1254______11096-82-5—————Aroclor-1260______

0.0.0.0.0.0.0.0.00000000000

00000

050050050050050050050050.10.10.10.10.10.10.10.50.10.50.501.0.50.50.50.50.501.01.0

uuuuuuuuuuuuuuuu


Date post:	27-Feb-2021
Category:	Documents
Upload:	others
View:	3 times
Download:	0 times

SDMS US EPA REGION V -1 · 2020. 11. 29. · 2. ie-1 nd 18/86/88 gub-81 mh b nd nd nd nd 213 i.ie-3...

Documents