Thermo Scientific FLASH 2000 & FLASH 4000 2000 & FLASH 4000 Organic Elemental Analyzers Consumables...

P/N 31708250 14th Edition January 2014

Thermo Scientific

FLASH 2000 & FLASH 4000Organic Elemental Analyzers

Consumables and Spare Parts Catalog

© 2014 Thermo Fisher Scientific Inc. All rights reserved.

FLASH 2000, FLASH 4000, FlashEA 1112, FLASH IRMS, FLASH HT/HT Plus, AI 1310/AS 1310, AI 3000/AS 3000 II, and Eager Xperience, are trademarks of Thermo Fisher Scientific Inc., and its subsidiaries. Other brand and product names may be trademarks or registered trademarks of their respective companies.

Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the product operation. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

The contents of this document are subject to change without notice. All technical information in this document is for reference purposes only. System configurations and specifications in this document supersede all previous information received by the purchaser.

Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or error-free and assumes no responsibility and will not be liable for any errors, omissions, damage or loss that might result from any use of this document, even if the information in the document is followed properly.

This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of Sale shall govern all conflicting information between the two documents.

14th Edition, Released January

For Research Use Only. Not for use in diagnostic procedures.

CContents

Part 1 Thermo Scientific FLASH 2000

Chapter 1 CHN Determination. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Chapter 2 CHN/O Determination. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Chapter 3 CHNS Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Chapter 4 CHNS/O Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Chapter 5 S Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Chapter 6 O Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

Chapter 7 N Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

Chapter 8 N Lubricant Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

Chapter 9 NC Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Chapter 10 NCS Determination. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

Chapter 11 NC-Soils, NC-Sediments, NC-Filters Determinations . . . . . . . . . . . . . . . . 30

Chapter 12 N/Protein, N-Brew Determinations. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

Chapter 13 FLASH IRMS (NC Determination) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

Chapter 14 FLASH HT (O/H and NC Determinations) . . . . . . . . . . . . . . . . . . . . . . . . . . . 36O/H Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36NC Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

Chapter 15 Kits of Consumables and Spare Parts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38Kit for 1000 Analyses for FLASH 2000 . . . . . . . . . . . . . . . . . . . . . . . . . . 38Kit for N/Protein Analyses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41Kit for 1000 Analyses for FLASH for IRMS and FLASH HT

(NC Determination) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42Kit for 1000 Analyses for FLASH for IRMS (NC Determination). . . . . . 43Kit for 1000 Analyses for FLASH HT/HT Plus (NC Determination) . . . 43Kit for 3000 Analyses for FLASH for IRMS and FLASH HT

(NC Determination) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44Kit for 3000 Analyses for FLASH HT/HT Plus (NC Determination) . . . 44

Thermo Scientific FLASH 2000 and FLASH 4000 Consumables and Spare Parts Catalog 3

Contents

Kit for 1000 Analyses for FLASH for IRMS and FLASH HT (NCS Determination) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Chapter 16 Reactors, Absorption Filters, GC Columns and Fittings. . . . . . . . . . . . . . . 46Reactors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46Adsorption Filters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47Gas Chromatographic Columns . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Chapter 17 Reagents and Chemicals. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52CHN Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52CHN-O Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52CHNS Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53CHNS-O Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53S Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53O Determination. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54N Determination. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54N Lubricant Determination. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54NC Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55NCS Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55NC-Soils, NC-Sediments, NC-Filters Determination . . . . . . . . . . . . . . . 55N/Protein, N-Brew Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56IRMS and HT NC Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56

Chapter 18 Analytical Standards and Reference Materials . . . . . . . . . . . . . . . . . . . . . 58Standard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59Reference Material . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59OEA/FPD Reference Solution Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59

Chapter 19 Adsorber for Fluorine Compounds. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60

Chapter 20 FLASH 2000 Upgrade Kits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62Kit for Total Organic Carbon (TOC) in Solid Sample PN 190 041 45 . . 62Conversion Kit from NC to NCS Determination PN 190 042 45 . . . . . 63Conversion Kit from NC to S Determination PN 190 042 40 . . . . . . . . 63Conversion from CHN to CHNS Configuration . . . . . . . . . . . . . . . . . . 64Conversion from CHN/CHNS to Oxygen Configuration. . . . . . . . . . . . 64Sulphur Conversion Kit for FLASH IRMS and

FLASH HT PN 190 037 40 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65

Chapter 21 Sample Containers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66Tin Containers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66Silver Containers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67

Chapter 22 Sample Preparation Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70

Chapter 23 MAS 200R Autosampler for Solid Samples . . . . . . . . . . . . . . . . . . . . . . . . . 72Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72Knurled Screws Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73

4 FLASH 2000 and FLASH 4000 Consumables and Spare Parts Catalog Thermo Scientific

Contents

Switching Box . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74

Chapter 24 NoBlank Sampling Device . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76For Upgrading FLASH System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77For Updating TC/EA and Previous OEA Models . . . . . . . . . . . . . . . . . . 77No Blank Spare Parts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77

Chapter 25 CM2 Manual Sampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78

Chapter 26 AI/AS 1310 Autosampler for Liquids for FLASH 2000 . . . . . . . . . . . . . . . . . 80

Chapter 27 Accessories for Injection of Liquid and Gas Samples . . . . . . . . . . . . . . . 84

Chapter 28 Resting Foot Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86

Chapter 29 Recommended Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88

Chapter 30 FLASH 2000 FPD Option . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90FPD Performance Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91OEA / FPD Reference Material . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91OEA / FPD Detector Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92

Chapter 31 Electronic Flow Controller Module. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94

Chapter 32 FLASH 2000 Electronics and Cables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96Printed Circuit Boards. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96Cables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97

Chapter 33 Eager Xperience Ethernet A/D . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98Ethernet Box Version PN 432 331 37 . . . . . . . . . . . . . . . . . . . . . . . . . . . 98Eager Xperience Hardware Minimum Requirements. . . . . . . . . . . . . . . . 98RS232/USB Converter PN 230 381 31. . . . . . . . . . . . . . . . . . . . . . . . . . 99

Chapter 34 Single to Double Furnace Upgrade Kit . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100

Chapter 35 Furnaces Transformation Kits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 102FLASH 2000 Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 102Transformation Kits Available . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103If the User Wants to Add a New Furnace (and Upgrade the Instrument

Configuration). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 104Transformation Furnace Kits List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105Transformation Furnace Kit: Explanations on Some Items . . . . . . . . . . 109Top Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 109Furnace Adapters. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 110Bottom Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 110Bottom Connections for FLASH IRMS and HT (O/H and

NC Determinations) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 111


Contents

Chapter 36 MAS 200R Driver . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 112

Chapter 37 FLASH 2000 System Qualification Package. . . . . . . . . . . . . . . . . . . . . . . . 114

Part 2 Thermo Scientific FLASH 4000

Chapter 38 FLASH 4000 N/Protein Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118

Chapter 39 Kit of Consumables for FLASH 4000. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120Kit for 1000 Analyses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120Kit for 5000 Analyses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120

Chapter 40 Reactor, Crucible, Separation Column and Fittings . . . . . . . . . . . . . . . . . 122Reactor . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 122Crucible. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 122Separation Column . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 123Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 123

Chapter 41 Consumables and Miscellanea . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124Consumables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124Miscellanea . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124

Chapter 42 Analytical Standards & Reference Material . . . . . . . . . . . . . . . . . . . . . . . 126Standard . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 126Reference Material . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 126

Chapter 43 Sample Preparation Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 128Sample Containers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 128

Chapter 44 MAS 4000 Autosampler . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 130Spare Parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 130

Chapter 45 AI/AS 3000 II Autosampler for Liquids for FLASH 4000 . . . . . . . . . . . . . . 132

Chapter 46 Recommended Spare Parts. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 134Pressure Regulators and Manometer . . . . . . . . . . . . . . . . . . . . . . . . . . . 134Detector Oven. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 134Furnace . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 134EV (electrovalves) Block . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135Regenerative Carbon Dioxide Filter. . . . . . . . . . . . . . . . . . . . . . . . . . . . 135Water Drain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135

Chapter 47 Electronic Flow Control Module (EFCt) . . . . . . . . . . . . . . . . . . . . . . . . . . . 136

Chapter 48 Electronics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 138Mains and High Voltage Printed Circuit Boards . . . . . . . . . . . . . . . . . . 138Low Voltage Printed Circuit Boards . . . . . . . . . . . . . . . . . . . . . . . . . . . 138Fuses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139Fans . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139Cables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139


Contents

Extension Card . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 139

Part 3 Previous FLASH Configurations

Chapter 49 AI/AS 3000 II Autosampler for Liquids for FLASH 2000 . . . . . . . . . . . . . . 142

Chapter 50 FlashEA 1112 Elemental Analyzer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 144Electronic Flow Controller Modules . . . . . . . . . . . . . . . . . . . . . . . . . . . 144Oxygen Line Purge Kit for FlashEA 1112 PN 190 042 60 . . . . . . . . . . 144FlashEA 1112 System Qualification Package . . . . . . . . . . . . . . . . . . . . . 145Transformation Furnace Kit: Explanations on Some Items . . . . . . . . . . 146

Appendix A Customer Communication. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 148How to Contact Us . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 148


1Part

Thermo Scientific FLASH 2000

1

CHN Determination

Table 1. Consumables and Spare Parts for CHN Determination

Refer To: Description Qty Part Number

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40

-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 10

1 Quartz Wool 5 g 338 222 00

2 Chromium Oxide 25 g 338 229 00

3 High Quality Copper 50 g 338 353 12

4 Silvered Cobaltous-Cobaltic Oxide 25 g 338 245 00

R Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70

-- Quartz Crucible 1 252 045 10

-- Prepacked Quartz Reactor CHN/NC - Argon Sealed 1 468 020 09

CC Multiseparation Column (PTFE; 2 m; 6x5 mm) 1 260 082 20

-- Tin Containers 100 240 064 00

-- Forceps 1 205 005 00

-- Small Spatula for Container Filling 1 205 006 00

-- Cyclohexanone STD 1 g 338 224 00

-- Atropine STD 2 g 338 244 00

-- Imidazole STD 1 g 338 354 30

-- Acetanilide STD 2 g 338 367 00

-- Urea STD 2 g 338 400 01

-- Nicotinamide STD 2 g 338 400 19


1 CHN Determination

AS. Autosampler R. Reactor

CC. Chromatographic Column TCD. Thermal Conductivity Detector

IMPORTANT If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to eliminate the Quartz Wool between Chromium Oxide and High Quality Copper and between the High Quality Copper and the Cobaltous-Cobaltic Oxide.


2

CHN/O Determination

Table 2. Consumables and Spare Parts for CHN/O Determination




1 Quartz Wool 5 g 338 222 00




5 Nickel Plated Carbon 5 g 338 238 00

6 Quartz Turning 5 0g 338 223 00

7 Soda Lime 100 g 338 352 35

8 Magnesium Perchlorate (Anhydrone) 100 g 338 219 00

-- Nickel Wool 2 g 338 250 00

R1/R2 Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70


-- Prepacked Quartz Reactor CHN/NC - Argon Sealed 1 468 020 09

F Empty Adsorption Filter Tube (Small Size) without Fast Connectors 1 281 131 04

CC1 Multiseparation Column (PTFE; 2 m; 6x5 mm) 1 260 082 20

CC2 Oxygen Separation Column (SS; 1 m; 6x5 mm) 1 260 079 00


-- Silver Containers for Oxygen Determination 100 240 054 00

-- Forceps 1 205 005 00

-- Spatula 1 205 006 00



-- Benzoic Acid STD 2 g 338 225 00


2 CHN/O Determination

-- Imidazole STD 1 g 338 354 30


-- Urea STD 2 g 338 400 01


Table 2. Consumables and Spare Parts for CHN/O Determination (Continued)

AS. Autosampler R1-R2. Reactors

F. Adsorption Filter CC1-CC2. Chromatographic Columns

TCD. Thermal Conductivity Detector

IMPORTANT CHN DeterminationIf the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to eliminate the Quartz Wool between Chromium Oxide and High Quality Copper and between the High Quality Copper and the Cobaltous-Cobaltic Oxide.

IMPORTANT Oxygen DeterminationIf the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the reactor of pyrolysis. In this case it is necessary to reduce from 30 mm to 20 mm the Quartz Wool in the lower section of the reactor.


3

CHNS Determination

Table 3. Consumables and Spare Parts for CHNS Determination




1 Quartz Wool 5 g 338 222 00

2 Copper Oxide 25 g 338 217 30

3 Electrolytic Copper 80 g 338 353 14

-- Vanadium Pentoxide 1 g 338 375 10


R Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 15

C Quartz Crucible 1 252 045 10

CC Packed Column CHNS/NCS (PTFE; 2 m; 6x5 mm) 1 260 082 15


-- Forceps 1 205 005 00


-- BBOT STD 2 g 338 352 10

-- Sulphanilamide STD 2 g 338 251 00

-- L-Cystine STD 2 g 338 400 18


3 CHNS Determination


CC. Chromatographic Column TCD. Thermal Conductivity Detector

IMPORTANT If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to reduce the Quartz Wool between Copper Oxide and Electrolytic Copper up to obtain a thin layer and to reduce the Copper Oxide proportionally as shown in the figure above.


4

CHNS/O Determination

Table 4. Consumables and Spare Parts for CHNS/O Determination




1 Quartz Wool 5 g 338 222 00




5 Quartz Turnings 50 g 338 223 00

6 Soda Lime 100 g 338 352 35


-- Nickel Wool 2 g 338 250 00

-- Vanadium Pentoxide 1 g 338 375 10


R1 Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 15



CC1 CHNS/NCS Separation Column (PTFE; 2 m; 6x5 mm) 1 260 082 15

CC2 Oxygen Separation Column (SS; 1m; 6x5 mm) 1 260 079 00



-- Forceps 1 205 005 00






4 CHNS/O Determination

-- BBOT STD 2 g 338 352 10


-- Urea STD 2 g 338 400 01

-- L-Cystine STD 2 g 338 400 18


Table 4. Consumables and Spare Parts for CHNS/O Determination (Continued)


F. Adsorption Filter CC1-CC2. Chromatographic Columns


IMPORTANT CHNS DeterminationIf the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to reduce the Quartz Wool between Copper Oxide and Electrolytic Copper up to obtain a thin layer and to reduce the Copper Oxide proportionally as shown in the figure above.

IMPORTANT Oxygen DeterminationIf the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the reactor of pyrolysis. In this case it is necessary to reduce from 30 mm to 20 mm the Quartz Wool in the lower section of the reactor.


5

S Determination

Table 5. Consumables and Spare Parts for S Determination




1 Quartz Wool 5 g 338 222 00

2 Copper Oxide 25g 338 217 30



-- Vanadium Pentoxide 1g 338 375 10


R Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 15



CC Sulphur Separation Column (PTFE; 0.8 m; 6x4 mm) 1 260 078 00


-- Forceps 1 205 005 00


-- BBOT STD 2 g 338 352 10


-- L-Cystine STD 2 g 338 400 18


5 S Determination


F. Adsorption Filter CC. Chromatographic Column




6

O Determination

Table 6. Consumables and Spare Parts for O Determination




1 Quartz Wool 5 g 338 222 00



4 Soda Lime 100 g 338 352 35


-- Nickel Wool 2 g 338 250 00




CC Oxygen Separation Column (SS; 1m; 6x5mm) 1 260 079 00


-- Forceps 1 205 005 00





-- BBOT STD 2 g 338 352 10


-- Urea STD 2 g 338 400 01

-- L-Cystine STD 2 g 338 400 18



6 O Determination




IMPORTANT If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the reactor of pyrolysis. In this case it is necessary to reduce from 30 mm to 20 mm the Quartz Wool in the lower section of the reactor.


7

N Determination

Table 7. Consumables and Spare Parts for N Determination




1 Quartz Wool 5 g 338 222 00




5 Soda Lime 100 g 338 352 35

6 Molecular Sieve 3 Å 100 g 338 018 01

7 Silica Gel plus indicator 100 g 338 400 35

-- Chromosorb® WAW 30/60 mesh 25 g 338 375 30



F1/F2 Empty Adsorption Filter Tube (Large Size) without Fast Connectors 2 281 130 64

CC Nitrogen Separation Column (PTFE; 0.5m; 8x6 mm) 1 260 078 20


-- Forceps 1 205 005 00



-- Aspartic Acid STD 2 g 338 400 22



7 N Determination


F1-F2. Adsorption Filters CC. Chromatographic Column



8

N Lubricant Determination

Table 8. Consumables and Spare Parts for N Lubricant Determination


-- Bottom O-Ring for 25 mm HPAR (Set of 5) 1 290 206 49

-- Top O-Ring for 25 mm HPAR (Set of 5) 1 290 206 82

1 Quartz Wool 5 g 338 222 00

2 Oxidation Catalyst 40 g 338 400 00


4 Soda Lime 100 g 338 352 35



R1 Prepacked HPAR Reactor; 25 mm OD 1 468 020 08

CR HPAR Crucible 1 252 050 11

R1/R2 Empty HPAR Reactor; 25 mm OD 1 468 200 75


CC Nitrogen Separation (N-Brew) Column (PTFE; 1 m; 8x6 mm) 1 260 700 04


-- Tin Disk 30 mm diameter 100 252 080 15

-- Forceps 1 205 005 00

-- Large Spatula for Container Filling 1 205 006 20

-- Atropine 2 g 338 244 00

-- Lubricant Reference Material 2 g 338 352 40


8 N Lubricant Determination



TCD. Thermal Conductivity Detector CR. HPAR Crucible


9

NC Determination

Table 9. Consumables and Spare Parts for NC Determination




1 Quartz Wool 5 g 338 222 00








CC Multiseparation Column (SS; 2m; 6x5 mm) 1 260 079 20


-- Forceps 1 205 005 00




Atropine STD 2 g 338 244 00


9 NC Determination


F. Adsorption Filter CC.Chromatographic Column



10

NCS Determination

Table 10. Consumables and Spare Parts for NCS Determination




1 Quartz Wool 5 g 338 222 00




-- Vanadium Pentoxide 1g 338 375 10


-- Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 15



CC CHNS/NCS Separation Column (PTFE 2 m; 6x5 mm) 1 260 082 15


-- Forceps 1 205 005 00


-- BBOT STD 2 g 338 352 10


-- L-Cystine STD 2 g 338 400 18


10 NCS Determination






11

NC-Soils, NC-Sediments, NC-Filters Determinations

Table 11. Consumables and Spare Parts for NC-Soils, NC-Sediments and NC-Filters Determination




-- Bottom O-Ring for 25 mm OD HPAR (Set of 5) 1 290 206 49

-- Top O-Ring for 25 mm OD HPAR (Set of 5) 1 290 206 82

1 Quartz Wool 5 g 338 222 00




R1 Prepacked HPAR Reactor 1 468 020 08

-- Empty HPAR 25 mm OD 1 468 200 75


R2 Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 70


CC Multiseparation Column (SS; 2m; 6x5 mm) 1 260 079 20




-- Forceps 1 205 005 00



-- Soil NC Reference Material 5 g 338 400 25


11 NC-Soils, NC-Sediments, NC-Filters Determinations





12

N/Protein, N-Brew Determinations

Table 12. Consumables and Spare Parts for N/Protein, N-Brew Determinations


-- Bottom O-Ring for 25 mm HPAR (Set of 5) 1 290 206 49

-- Top O-Ring for 25 mm HPAR (Set of 5) 1 290 206 82

1 Quartz Wool 5 g 338 222 00



4 Soda Lime 100 g 338 352 35



-- Chromosorb® WAW 30/60 mesh 25 g 338 375 30

R1 Prepacked HPAR Reactor; 25 mm OD 1 468 020 08


R1/R2 Empty HPAR Reactor; 25 mm OD 1 468 200 75


CC Nitrogen Separation Column (PTFE; 0.5 m; 8x6 mm) 1 260 078 20

CC Nitrogen Separation (N-Brew) Column (PTFE; 1 m; 8x6 mm) 1 260 700 04




-- Forceps 1 205 005 00


-- Urea STD 10 g 338 400 02


-- Pasta Reference Material 10 g 338 400 24


12 N/Protein, N-Brew Determinations





13

FLASH IRMS (NC Determination)

Table 13. Consumables and Spare Parts for FLASH IRMS - NC Determinations



1 Quartz Wool 5 g 338 222 00


3 Silvered Cobaltous Cobaltic Oxide 25 g 338 245 00

4 Reduced Copper (4-7 mm wire length) 100 g 338 353 00


R1/R2 Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 70

Prepacked Oxydation Reactor NC Determination (FLASH IRMS) 1 468 200 76

Prepacked Reduction Reactor NC Determination (FLASH IRMS) 1 468 200 77

F Adsorption Filter for IRMS/HT Version 1 281 131 02

CC IRMS Separation Column (SS; 3m; 6x5 mm) 1 260 079 31

-- Tin Containers (Set of 100) 1 240 064 00

-- Forceps 1 205 005 00







13 FLASH IRMS (NC Determination)

AS. Autosampler R1 - R2. Reactors

F1 - F2. Adsorption Filters CC1 - CC2. Chromatographic Columns

TCD. Thermal Conductivity Detector CFI. Continuous Flow Interface

IRMS. Isotopic Ratio Mass Spectrometer


14

FLASH HT (O/H and NC Determinations)

O/H Determination

NC Determination

IMPORTANT The HT Pyrolysis chemicals for O/H determination constituted to ceramic reactor, glassy carbon reactor, graphite tube, graphite crucible, glassy carbon granulate, silver wool, and so on, can be ordered directly to Thermo Fisher Scientific GmbH Bremen, Germany.

Table 14. HT Furnace


-- O/H Separation column (SS; 1 m; 6x5 mm) 1 260 079 00

Table 15. Consumables and Spare Parts for FLASH HT - O/H and NC Determinations



1 Quartz Wool 5 g 338 222 00




-- Carbosorb (CO2 Adsorber) per O/H Determinations 50 g 338 352 36


R2 Prepacked Reactor NC/CHN Determinations - Argon sealed 1 468 020 09

-- Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 70

F2 Adsorption Filter for IRMS/HT Version 1 281 131 02

-- IRMS Separation Column (SS; 3m; 6x5 mm) 1 260 079 31

-- Tin Containers (Set of 100) 1 240 064 00

-- Forceps 1 205 005 00



14 FLASH HT (O/H and NC Determinations)






Table 15. Consumables and Spare Parts for FLASH HT - O/H and NC Determinations (Continued)

AS. Autosampler R2. Reactors

F2. Adsorption Filter CC2. Chromatographic Column

TCD. Thermal Conductivity Detector CFI Continuous Flow Interface

IRMS. Isotopic Ratio Mass Spectrometer


15

Kits of Consumables and Spare Parts

Kit for 1000 Analyses for FLASH 2000

Table 16. Consumables for CHN Determination

No Description Qty Part Number

CHN Determination 1 190 024 10

1 Tin Containers Megabox (Set of 1000) 2 240 064 10

2 Quartz Wool (5 g) 1 338 222 00

3 Chromium Oxide (25 g) 1 338 229 00

4 Silvered Cobaltous-Cobaltic Oxide (25 g) 1 338 245 00

5 High Quality Copper (50 g) 4 338 353 12

6 Empty Quartz Reactor Tube (Set of 2) 1 468 200 70

Table 17. Consumables for CHNS/NCS/S Determination (1)


CHNS / NCS / S Determination with Empty Quartz Reactor 1 190 024 11


2 Copper Oxide (25 g) 2 338 217 30

3 Magnesium Perchlorate [Anhydrone] (100g) Only for NCS and S determinations 1 338 219 00

4 Quartz Wool (5 g) 1 338 222 00

5 Electrolytic Copper 4 338 353 14

6 Vanadium Pentoxide (1 g) 1 338 375 10


Table 18. Consumables for CHNS/NCS/S Determination (2)


CHNS / NCS / S Determination with Prepacked Quartz Reactor 1 190 024 12



15 Kits of Consumables and Spare Parts

2 Magnesium Perchlorate [Anhydrone] (100g) Only for NCS and S determinations 1 338 219 00

3 Quartz Wool (5 g) 1 338 222 00


5 Prepacked Reactor for CHNS, NCS, and S determinations 4 468 020 15

Table 18. Consumables for CHNS/NCS/S Determination (2) (Continued)

Table 19. Consumables for Oxygen Determination


Oxygen Determination 1 190 024 16

1 Silver Containers (Set of 100) 10 240 054 00

2 Magnesium Perchlorate [Anhydrone] (100g) 1 338 219 00

3 Quartz Wool (5 g) 2 338 222 00

4 Quartz Turnings (50 g) 1 338 223 00

5 Nickel Plated Carbon (5 g) 8 338 238 00

6 Nickel Wool (2 g) 1 338 250 00

7 Soda Lime (100 g) 1 338 352 35

8 Empty Quartz Reactor (Set of 2) 1 468 200 70

Table 20. Consumables for N OrganicDetermination (1)


N Organic Determination 1 190 024 13


2 Molecular Sieve 3 Å (100 g) 1 338 018 01

3 Copper Oxide (25 g) 2 338 217 30

4 Quartz Wool (5 g) 1 338 222 00


6 Soda Lime (200 g) 2 338 352 30


8 Chromosorb® WAW (25 g) 30/60 mesh 1 338 375 30

9 Silica Gel plus indicator (100 g) 1 338 400 35




Table 21. Consumables for N Lubricant Determination


N Lubricant Determination 1 190 024 30


2 Top O-Ring for HPAR Reactor (Set of 5) 1 290 206 82


4 Quartz Wool (5 g) 2 338 222 00

5 Atropine STD (2 g) 1 338 244 00

6 Soda Lime (200 g) 5 338 352 30

7 Lubricant Reference Material; N% = 0.58 (2 g) 1 338 352 40


9 Oxidation Catalyst (40 g) 2 338 400 00

10 Silica Gel with Indicator (100 g) 1 338 400 35

Table 22. Consumables for NC Determination


NC Determination 1 190 024 14


2 Copper Oxide (25 g) 2 338 217 30

3 Magnesium Perchlorate [Anhydrone] (100 g) 1 338 219 00

4 Quartz Wool (5g) 1 338 222 00




Table 23. Consumables for NC-Soils, NC-Sediments, NC-Filters Determination

No Description Qty PN

NC-Soils, NC-Sediments, NC-Filters Determination 1 190 024 15

1 Tin Disk 30 mm OD (Set of 100) 20 252 080 15


3 Quartz Wool (5 g) 1 338 222 00


5 Prepacked HPAR Reactor 1 468 020 08




Kit for N/Protein Analyses

Table 24. Package A for Solid Samples


Package A of Consumables for Solid Samples 1 190 042 20

1 HPAR Crucible 1 252 050 11

2 Tin Disk 30 mm diameter (Set of 100) 20 252 080 15

3 Bottom O-Ring for HPAR Reactor (Set of 5) 1 290 206 49



6 Quartz Wool (5 g) 2 338 222 00

7 Soda Lime (200 g) 5 338 352 30



10 Aspartic Acid STD (10 g) 1 338 400 23

11 Pasta Reference Material (10 g) 1 338 400 24


Table 25. Package B for Solid Samples


Package B of Consumables for Solid Samples 1 190 042 25


2 Tin Disk 30 mm diameter (Set of 100) 100 252 080 15




6 Quartz Wool (5 g) 8 338 222 00

7 Soda Lime (200 g) 25 338 352 30



10 Aspartic Acid STD (10 g) 2 338 400 23


12 Silica Gel (100 g) 4 338 400 35



Kit for 1000 Analyses for FLASH for IRMS and FLASH HT (NC Determination)

Table 26. Package A for Liquid Samples (AI/AS Autosampler)


Package A of Consumables for Liquid Samples (with AI/AS autosampler) 1 190 042 29

1 Complete Vials 2 SVW Package (Set of 100) 10 240 140 19

2 Vial Solvent 4 mL ST 4-SVQ (Set of 5) 1 240 140 32



5 Septa for Waste Bottle (Set of 5) 1 313 032 18

6 Septa for FLASH 2000 Injector (Set of 50) 1 313 032 30

7 Molecular Sieve (100 g) 1 338 018 01

8 Quartz Wool (5 g) 1 338 222 00

9 Soda Lime (200 g) 3 338 352 30




13 Screw Caps 8-SC (Set of 5) 10 386 060 85

Table 27. Kit for 1000 Analyses for FLASH for IRMS and FLASH HT (NC Determination)


NC Determinations FLASH IRMS 1 190 024 18

1 Tin container (Set of 100) 10 240 064 00

2 Sealing O-Ring for adsorption filter (PN 281 131 00) 2 290 136 03

3 Top O-ring for 18 mm OD quartz reactor (Set of 5) 2 290 229 10


5 Quartz wool (5 g) 1 338 222 00

6 Cyclohexanone STD (1 g) 1 338 224 00

7 Chromium Oxide (25 g) 4 338 229 00

8 Silvered Cobaltous Cobaltic Oxide (25 g) 4 338 245 00

9 Reduced Copper (100g), 4–7 mm wire length 4 338 353 00

10 Empty Quartz Reactor 18 mm OD (Set of 2) 2 468 200 70



Kit for 1000 Analyses for FLASH for IRMS (NC Determination)

Kit for 1000 Analyses for FLASH HT/HT Plus (NC Determination)

Table 28. Kit for 1000 Analyses for FLASH for IRMS (NC Determination)


NC Determinations FLASH IRMS 1 190 037 70




4 Quartz wool (5 g) 1 338 222 00

5 Chromium Oxide (25 g) 2 338 229 00




Table 29. Kit for 1000 Analyses for FLASH HT/HT Plus (NC Determination)


NC Determinations FLASH HT/HT Plus 1 190 037 80




4 Quartz wool (5 g) 1 338 222 00

5 Chromium Oxide (25 g) 3 338 229 00






Kit for 3000 Analyses for FLASH for IRMS and FLASH HT (NC Determination)

Kit for 3000 Analyses for FLASH HT/HT Plus (NC Determination)

Table 30. Kit for 3000 Analyses for FLASH IRMS and FLASH HT (NC Determination)


NC Determinations FLASH IRMS/HT 1 190 037 60

1 Tin container 0.02 mL (Set of 100) 5 240 053 00


3 Adsorption Filter for IRMS/HT Version 1 281 131 02

4 Silicone Sleeve 4 290 036 35

5 Aluminium Ferrule, 2 mm OD (Set of 10) 1 290 240 45


7 Aluminium Ferrule 1.6 mm OD (Set of 10) 1 290 340 44


9 Quartz wool (5 g) 3 338 222 00

10 Chromium Oxide (25 g) 4 338 229 00



13 SS Tubing Nut; 2mm (Set of 10) 1 350 404 03


Table 31. Kit for 3000 Analyses for FLASH HT/HT Plus (NC Determination)


NC Determinations FLASH HT/HT Plus 1 190 037 90

1 Tin container 0.02 mL (Set of 100) 5 240 053 00



4 Silicone Sleeve 4 290 036 35

5 Aluminium Ferrule 2 mm OD (Set of 10) 1 290 240 45


7 Aluminium Ferrule 1.6 mm OD (Set of 10) 1 290 340 44


9 Quartz wool (5 g) 3 338 222 00



Kit for 1000 Analyses for FLASH for IRMS and FLASH HT (NCS Determination)

10 Chromium Oxide (25 g) 7 338 229 00





Table 31. Kit for 3000 Analyses for FLASH HT/HT Plus (NC Determination) (Continued)

Table 32. Kit for 1000 Analyses for FLASH IRMS and FLASH HT/FLASH HT Plus (NCS Determination)


NCS Determinations FLASH IRMS/HT 1 190 037 50


2 Magnesium Perchlorate [Ahnydrone] (100 g) 1 338 219 00

3 Quartz wool (5 g) 1 338 222 00


5 Prepacked Quartz Reactor for NCS Determination for FLASH IRMS/HT 5 468 020 21


16

Reactors, Absorption Filters, GC Columns and Fittings

Reactors

Table 33. Reactor Tubes



2 Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 10

3 Bottom O-Ring 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40

4 Empty Quartz Reactor 18 mm OD CYL (Set of 2) [for IRMS/HT] 1 468 200 60

5 Opaque Quartz Reactor 18 mm OD (Set of 2) 1 468 200 00

6 Empty HPAR Reactor 25 mm OD 1 468 200 75

7 Top O-Ring for HPAR (Set of 5) 1 290 206 82

8 Bottom O-Ring for HPAR (Set of 5) 1 290 206 49

9 Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 15

10 Prepacked HPAR Reactor for N/Protein/NC-Soils Determinations 1 468 020 08

11 Prepacked Reactor NC/CHN Determinations - Argon sealed 1 468 020 09

12 Prepacked Quartz Reactor for NCS Determinations - Argon sealed [for HT/HT Plus]

1 468 020 21


14 Quartz Crucible (13 mm OD) 1 252 045 10

15 HPAR Reactor Extractor (see A) 1 205 006 26

16 Crucible Extractor (see B) 1 205 006 27

16 Cleaning Device for HPAR Reactor (see C) 1 205 006 25

18 Cleaning Device for Quartz Reactor and SS Crucible (see D) 1 276 060 10


16 Reactors, Absorption Filters, GC Columns and Fittings

Adsorption Filters

Figure 1. Fast connection couples

Figure 2. Fast connection couples plus fast connectors adapters

A B

C D

Table 34. Adsorption Filters


1 Adsorption Filter FC (Small Size) without Fast Connectors 1 281 131 04

2 Adsorption Filter FC (Large Size) without Fast Connectors 1 281 130 64

3 Fast Connectors Couple (Male plus Female) - See Figure 1 190 502 08

4 Fast Connector Couples plus Fast Connectors Adapters - See Figureconsisting of:

- Fast Connectors (male + female), Set of 2- Fast Connector Adapters, Set of 2

See Figure 1 and Figure 2.

1 190 502 09

5 Sealing O-Ring for Adsorption Filter FC [PN 281 131 04] (Set of 2) 1 290 036 35

6 Sealing O-Ring for Adsorption Filter FC [PN 281 130 64] (Set of 2) 1 290 100 82

1. Male fast connector 2. Female fast connector

1. Male fast connector 2. Female fast connector 3. Fast connector adapter

1 2

1 2 3



Table 35. Adsorption Filters (Old Types)*


1 Adsorption Filter (Small Size) 1 281 131 00

2 Sealing O-Ring for Adsorption Filter [PN 281 131 00] (Set of 2) 1 290 136 03

3 Adsorption Filter (Large Size) 1 281 130 60

4 Sealing O-Ring for Adsorption Filter [PN 281 130 60] (Set of 2) 1 290 100 82

Note * The Absorption Filters (Old Types) have been mounted on FlashEA™ 1112 Elemental Analyzer till Serial Number 20005214

Table 36. Adsorption Traps (Pyrex Type)**


1 Large Adsorption Trap (Pyrex Type) without Fast Connectors 1 281 131 06

2 Sealing O-Ring for Pyrex Type Large Adsorption Filter (Set of 2) 1 290 036 35

Note ** It substitutes the Absorption Filter (Large Size) with Fast Connectors PN 281 130 65 in N/Protein and NC-Soil Configurations when the sample contains very high humidity percentage and when several daily analyses are required.

Table 37. Adsorption Traps for IRMS and HT Versions


1 Adsorption Filter for IRMS/HT Version (small size) 1 281 131 02

2 Sealing O-Ring for Adsorption Filter (Set of 2) 1 290 136 35

Table 38. Clips for Adsorption Filters


1 Clip for Flash 2000, 12.5 mm (Set of 2) 1 429 001 52

2 Clip for Flash 2000 - N Protein, 29 mm (Set of 2) 1 429 001 56



Gas Chromatographic Columns

Table 39. Gas Chromatographic Columns


1 Multiseparation Column (PTFE; 2m; 6x5 mm) 1 260 082 20

2 Multiseparation Column (SS; 2 m; 6x5 mm) 1 260 079 20

3 CHNS/NCS Separation Column (PTFE; 2 m; 6x5 mm) 1 260 082 15

4 Oxygen Separation Column (PTFE; 1 m; 6x5 mm) 1 260 079 00

5 Sulphur Separation Column (PTFE; 0.8 m; 6x4 mm) 1 260 078 00

6 Sulphur Separation Column for OEA / FPD (PTFE; 0.15 m; 6x4 mm) 1 260 078 01

7 Sulphur Separation Column for IRMS / HT (PTFE; 0.8 m; 6x4 mm) 1 260 070 80

8 Nitrogen Separation Column (PTFE; 0.5 m; 8x6 mm) 1 260 078 20

9 Nitrogen Separation (N-Brew) Column (PTFE; 1 m; 8x6 mm) 1 260 700 04

10 IRMS Separation Column (SS; 3 m; 6x5 mm) 1 260 079 31

Characteristics Analytical Determination

Mat

eria

l

Leng

hth

(cm

)

OD

(mm

)

ID (m

m)

CH

NS

CH

N

NC

S

S (T

CD

)

S (F

PD)

Oxy

gen

N N/P

rote

in

N-B

rew

/ N-L

ubric

ant

NC

NC

-Soi

ls

NC

-Sed

imen

ts

NC

-Filt

ers

IRM

S (N

C)

HT

(NC

)

HT

(O/H

)

Colu

mns

Steel 100 6 5

200 6 5

300 6 5

PTFE 15 6 4

50 8 6

80 6 4

100 8 6

200 6 5



Fittings

Table 40. Fittings & Tubes


1 O-ring for 6 mm OD tube (Set of10) 1 290 305 67

2 Aluminium Ferrule, 2 mm (Set of 10) 1 290 340 45

3 Aluminium Ferrule, 4 mm (Set of 10) 1 290 340 51

4 Knurled nut for Polyethylene Tube PN 420 100 00 1 350 021 24

5 Push Fit Connector Tube; 6 MB Brass (Set of 5) 1 350 341 08

6 SS Tubing Nut; 2 mm (Set of 10) 1 350 404 03

7 Male hose adapter for Polyethylene Tube PN 420 100 00 (Set of 10) 1 350 441 37

8 6 MB Brass Blanking Nut (Set of 10) 1 350 451 00

9 SS Tube; 2x1 mm 3 m 391 025 00

10 Polyethylene Tube, Blue Color; 5x3 mm 5 m 420 100 00

11 PTFE Tube; 2x1 mm 1 m 420 015 00

12 PTFE Tube; 2x1mm 5 m 420 015 01

13 PTFE Tube; 4x2 mm 1 m 420 016 00

14 PTFE Tube; 6x4 mm 1 m 420 017 00


17

Reagents and Chemicals

CHN Determination

CHN-O Determination

Table 41. Reagents and Chemicals for CHN Determination


1 Quartz Wool 5 g 338 222 00




Table 42. Reagents and Chemicals for CHN-O Determination



2 Quartz Wool 5 g 338 222 00





7 Nickel Wool 2 g 338 250 00

8 Soda Lime 100 g 338 352 35



17 Reagents and Chemicals

CHNS Determination

CHNS-O Determination

S Determination

Table 43. Reagents and Chemicals for CHNS Determination



2 Quartz Wool 5 g 338 222 00


4 Vanadium Pentoxide 1 g 338 375 10

Table 44. Reagents and Chemicals for CHNS-O Determination




3 Quartz Wool 5 g 338 222 00



6 Nickel Wool 2 g 338 250 00

7 Soda Lime 100 g 338 352 35



Table 45. Reagents and Chemicals for S Determination




3 Quartz Wool 5 g 338 222 00





O Determination

N Determination

N Lubricant Determination

Table 46. Reagents and Chemicals for O Determination



2 Quartz Wool 5 g 338 222 00



5 Nickel Wool 2 g 338 250 00

6 Soda Lime 100 g 338 352 35

Table 47. Reagents and Chemicals for N Determination




3 Quartz Wool 5 g 338 222 00


5 Soda Lime 200 g 338 352 30


7 Chromosorb® WAW 30/60 mesh 25 g 338 375 30


Table 48. Reagents and Chemicals for N Lubricant Determination



2 Quartz Wool 5 g 338 222 00

3 Soda Lime 200 g 338 352 30





NC Determination

NCS Determination

NC-Soils, NC-Sediments, NC-Filters Determination

Table 49. Reagents and Chemicals for NC Determination




3 Quartz Wool 5 g 338 222 00



Table 50. Reagents and Chemicals for NCS Determination




3 Quartz Wool 5 g 338 222 00



Table 51. Reagents and Chemicals for NC-Soils, NC-Sediments, NC-Filters Determination



2 Quartz Wool 5 g 338 222 00





N/Protein, N-Brew Determination

IRMS and HT NC Determination

Table 52. Reagents and Chemicals for N/Protein, N-Brew Determination



2 Quartz Wool 5 g 338 222 00

3 Soda Lime 200 g 338 352 30


5 Chromosorb ® WAW 30/60 mesh 25 g 338 375 30



Table 53. Consumables and Spare Parts for FLASH 2000 IRMS and HT NC Determinations



2 Quartz Wool 5 g 338 222 00




6 Carbosorb (CO2 Adsorber) for O/H Determinations 50 g 338 352 36


18

Analytical Standards and Reference Materials

Table 54. Analytical Standards


1 Acetanilide 2 g 338 367 00

2 Aspartic Acid 2 g 338 400 22

3 Aspartic Acid 10 g 338 400 23

4 Atropine 2 g 338 244 00

5 BBOT* 2 g 338 352 10

6 Benzoic Acid 2 g 338 225 00

7 Cyclohexanone 2,4 DNPH ** 1 g 338 224 00

8 dl-Methionine 25 g 338 352 20

9 Imidazole 1 g 338 354 30

10 L-Cystine 2 g 338 400 18

11 Nicotinamide 2 g 338 400 19

12 Sulphanilamide 2 g 338 251 00

13 Urea 2 g 338 400 01

14 Urea 10 g 338 400 02

* 2,5 bis (5-ter-butyl-benzoxazol-2-yl) thiophene; ** Cyclohexanone 2,4-dinitrophenylhydrazone

Table 55. Reference Materials


1 Lubricant Reference Material 2 g 338 352 40

2 Pasta Reference Material 10 g 338 400 24

3 Pasta Reference Material for S determination (OEA / FPD) 2 g 338 400 27

4 Soil NC Reference Material 5 g 338 400 25

5 Soil NCS Reference Material for NCS determination and S determination (OEA/FPD)

2 g 338 400 26

6 OEA/FPD Reference Solutions Kit constituted by 4 flasks (2 mL each) containing 10, 50, 100, and 500 ppm for Sulphur

1 338 190 40


18 Analytical Standards and Reference Materials

Standard

Reference Material

OEA/FPD Reference Solution Kit

Standard N% C% H% S% O%

Acetanilide 10.36 71.09 6.71 --- 11.84

Aspartic Acid 10.52 36.09 5.30 --- 48.08

Atropine 4.84 70.56 8.01 --- 16.59

BBOT 6.51 72.53 6.09 7.44 7.43

Benzoic Acid --- 68.85 4.95 --- 26.20

Cyclohexanone 2-4 DNPH 20.14 51.79 5.07 --- 23.00

dl-Methionine 9.39 40.25 7.43 21.49 21.45

Imidazole 41.15 52.93 5.92 --- ---

L-Cystine 11.66 29.99 5.03 26.69 26.63

Nicotinamide 22.94 59.01 4.95 --- 13.10

Sulphanilamide 16.27 41.84 4.68 18.62 18.58

Urea 46.65 20.00 6.71 --- 26.64

Reference Material N% C% H% S%

Lubricant (batch n° O12A) 0.58 76.44 12.00 2.40

Pasta (batch n° H13A) 1.89 --- --- ---

Pasta for OEA/FPD (batch n° N12A) --- --- --- 0.134

Soil NC (batch n° N12A) 0.20 2.01 --- ---

Soil NCS (batch n° N12A) 0.20 2.01 --- 0.032

OEA/FPD Reference Solutions Kit

10 ppm of Sulphur (2 mL flask)




IMPORTANT All the standards and the references material are accompanied with a quality certificate including the storage condition and the lifetime of the products.


19

Adsorber for Fluorine Compounds

Table 56.


1 FluoAdso

Specific adsorber for Fluorine compounds CHN, NC, and N Determinations

15g 338 400 30

100 mm

50 mm

30 mm

20 mm

30 mm10 mm

Reactor: Quartz TubeTemperature: 950 �C

TCD

Temperature: 75 �C

Quartz WoolAdsorber

Chromium Oxide

Copper

Silvered Cobaltous-Cobaltic Oxide

Quartz Wool

Flash 2000-CHN Configuration for�Fluorine-containing Compounds

For more details on CHN determination on Fluorine-containing Compounds require the OEA Application Note n. 11008.


19 Adsorber for Fluorine Compounds


20

FLASH 2000 Upgrade Kits

Kit for Total Organic Carbon (TOC) in Solid Sample PN 190 041 45Total Organic Carbon is a very important parameter for soil or for other organic matrix.

The kit for TOC allows to eliminate all inorganic carbon as Carbon Dioxide by effect of the acidification and heating of the sample in special containers.

Table 57 lists the materials included into the kit.

Figure 3. Sample Holder Plate and Electric Heater

Table 57. Kit for Total Organic Carbon in Solid Sample

Part Number Description Quantity

240 054 05 Silver sample container for solid (Set of 100) 1

334 130 36 Sample holder plate (see Figure 3) 1

354 600 17 Electric heater (see Figure 3) 1

365 005 30 Syringe 1750 LT 500 μL 1


20 FLASH 2000 Upgrade Kits

Conversion Kit from NC to NCS Determination PN 190 042 45Table 58 lists the materials included into the kit.

Conversion Kit from NC to S Determination PN 190 042 40Table 59 lists the materials included into the kit.

Table 58. Conversion Kit from NC to NCS Determination


1 CHNS / NCS Separation Column (PTFE; 2 m; 6x5 mm) 1 260 082 15

2 BBOT* (N: 6.51%; C: 72.53%; S: 7.44%) 1 338 352 10


4 Soil NCS Reference Material (2 g)[The percentage of the elements in this Ref. Mat. will vary batch-to-batch as indicated to analytical data sheet included] Soil NCS R.M. (Batch n. N12A) N%: 0.20; C%: 2.01; S%: 0.032

1 338 400 26

5 Bottom Adapter Connection, 18 mm - 6MB (complete) 1 350 084 33

6 Prepacked Quartz Reactor for NCS Determination 1 468 020 15*2,5 bis (5-tert-butyl-benzoxazol-2-yl) thiophene

Table 59. Conversion Kit from NC to S Determination


1 Sulphur Separation Column (PTFE; 0.8 m; 6x5 mm) 1 260 078 00

2 BBOT* (N: 6.51%; C: 72.53%; S: 7.44%) 1 338 352 10


4 Soil NCS Reference Material (2 g)[The percentage of the elements in this Ref. Mat. will vary batch-to-batch as indicated to analytical data sheet included] Soil NCS R.M. (Batch n. N12A) N%: 0.20; C%: 2.01; S%: 0.032

1 338 400 26

5 Bottom Adapter Connection, 18 mm - 6MB (complete) 1 350 084 33

6 Prepacked Quartz Reactor for NCS Determination 1 468 020 15*2,5 bis (5-tert-butyl-benzoxazol-2-yl) thiophene



Conversion from CHN to CHNS ConfigurationTable 60 lists the materials included into the kit for upgrading a CHN analyzer to a CHNS.

Conversion from CHN/CHNS to Oxygen ConfigurationTable 61 lists the materials included into the kit for upgrading a CHN/CHNS analyzer to Oxygen.

Table 60. Conversion from CHN to CHNS Configuration


1 CHNS / NCS Separation Column (PTFE; 2 m; 6x5 mm) 1 260 082 15

2 Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 15

3 BBOT* (N: 6.51%; C: 72.53%; S: 7.44%) 1 338 352 10

4 Vanadium Pentoxide (1 g) 1 338 375 10*2,5 bis (5-tert-butyl-benzoxazol-2-yl) thiophene

Table 61. Conversion from CHN/CHNS to Oxygen Configuration


1 Oxygen Separation Column (SS; 1 m; 6x5 mm) 1 260 079 00

2 Empty Adsorption Filter (small size) 1 281 131 04


4 Quartz Wool (5 g) 1 338 222 00

5 Quartz Turnings (50 g) 1 338 223 00

6 Nickel Plated Carbon (5 g) 1 338 238 00

7 Soda Lime (100 g) 1 338 352 35

8 Empty Quartz Reactor (Set of 2) 1 468 200 70

9 Silver Containers (set of 100) 1 240 054 00



Sulphur Conversion Kit for FLASH IRMS and FLASH HT PN 190 037 40Table 62 lists the materials included into the kit.

Table 62. Sulphur Conversion Kit for FLASH IRMS and FLASH HT


1 Tin Container (Set of 100) 2 240 064 00

2 Sulphur Separation Column for IRMS / HT (PTFE; 0.8 m; 6x4 mm) 1 260 070 80

3 Capillary SS 1/16-in. x 0.8 mm 1 190 250 08

4 Brass Swagelok Tube Fitting 1 350 001 22


6 Aluminium Ferrule 1/16-in. (Set of 10) 1 290 340 44

7 Aluminium Ferrule 2 mm (Set of 10) 1 290 340 45

8 Sulfanilamide STD 1 338 251 00


10 Straight Connector 2 347 141 00


12 Teflon Tube 5 m 1 420 015 01

13 Prepacked Quartz Reactor for NCS/S Determination 1 468 020 21


21

Sample Containers

Tin Containers

Figure 4. Tin and Silver Containers

Note You will find here an optimized guide for the best choice of containers tailored to your specific analytical needs, through a detailed specification both for tin and silver containers to be used according to the different applications. To avoid deformation problems and to guarantee a complete use of all the sample containers, these are conveniently supplied and protected in adequate plastic boxes in package of 50 and 100.

Table 63. Tin Containers (See Figure 4)

Refer To: Description High Diameter Qty Part Number

A Universal “Soft” Tin Containers 8 mm 5 mm 100 240 064 00

Universal “Soft” Tin Containers Megabox 8 mm 5 mm 1000 240 064 10

B Small “Soft” for Solid Sample 5 mm 3.5 mm 100 240 053 00

C Large “ Soft” Tin Containers for N/Protein and N-Brew Analysis

10 mm 10 mm 100 252 080 00

D “Hard” Tin Containers 6 mm 3 mm 100 240 088 10

E “Hard” Tin Container 4.5 mm 2 mm 100 240 088 20

F “Hard” Tin Container 9 mm 3.5 mm 50 240 072 00

G “Hard” Tin Capillary 5.5 mm 1.06 mm 50 240 070 00

H Tin Disk --- 30 mm 100 252 080 15

I Tin Disk --- 35 mm 100 252 080 18

A B C L M D E F G N

1. “Soft” containers are obtained by pressing light metal foil. 2. “Hard” tin containers are heavier than the “Soft” ones and allow hermetic sealing. For this reason the “Hard” tin containers are obtained by moulding ultrapure tin sheets.


21 Sample Containers

Silver Containers

Tin Container Type Use

A Recommended for solid samples (organics, soils, sediments, food, plastic, coal, and so on), or liquid samples adsorbed on inert solid material Chromosorb® WAW 30/60 mesh (PN 338 375 30). See Figure 4.

B Recommended for solid samples.

C Recommended for N/Protein and N-Brew Determinations.

D Recommended for the analysis of any viscous sample. See Figure 5.

E Recommended for the analysis of any liquids; for volatile liquids we recommended the use of liquid sealing device (PN 205 030 02).

F Suggested for analysis of trace elements (N, C, S) in liquids such as water, wine, beer, milk, urine, and so on.

G Suggested for the analysis of liquid samples when the material is available in very small amounts. Useful for volatile samples. Use of Sealing Device (PN 205 030 02) is highly recommended. For more details on Sealing Device please see Chapter 22, “Sample Preparation Accessories.”

H Use Sealing Device (PN 252 090 10)

I Use Sealing Device (PN 252 090 10)

Table 64. Silver Containers (See Figure 4)

Refer To: Description High Diameter Qty Part Number

L Universal “Soft” Silver Containers 6 mm 4 mm 100 240 054 00

M “Soft” Silvers Containers 8 mm 5 mm 100 240 054 05

N “Hard” Silver Containers 5 mm 2 mm 50 240 051 00

Silver Container Type Use

L Recommended for Oxygen determination for solid samples.M Recommended for Total Organic Carbon (TOC) determination according to the Thermo

Fisher Scientific method (patent n. 90110186.5). See Figure 6.See “Kit for Total Organic Carbon (TOC) in Solid Sample PN 190 041 45,” .

N Recommended for Oxygen analysis of liquid samples (e.g. gasoline). The Sealing Device (PN 205 030 02), is highly suggested for these liquid samples.


21 Sample Containers

Figure 5. Sampling Technique

Figure 6. T.O.C. Determination

Add Chromosorb �1 spatula

Weighing

Liquid Sampling Technique

TM

Add the liquid sample on the Chromosorb �surface

TM

Seal and Weigh

Viscous Sampling� Technique

Ag Capsules Add 5 - 20 mg of sample

WEIGHING

Add 1 drop of HCl 1:1

65 �C

Leave at 65 �C until dry

ANALYSING

1 2 3

4 5 6

Sampling Technique for T.O.C. Determination


22

Sample Preparation Accessories

Table 65. Sample Preparation Accessories


A Sealing Device for Solid Containers 1 205 003 10

B Sealing Device for Large Tin Containers 1 252 090 10

C Sealing Device for Liquid Containers 1 205 030 02

D Pocket Sample Holder for Small Containers 1 240 100 24

E Cleaning Device for Quartz Reactor and Crucible 1 276 060 10

F Cleaning Device for HPAR Reactor 1 205 006 25

-- Forceps 1 205 005 00

-- Crucible Extractor 1 205 006 27

-- HPAR Extractor 1 205 006 26



-- Microsyringe 710 SNR 100 μL 1 365 002 04

-- Microsyringe 10 μl 1 365 020 01

Table 66. Accessories Desciption

Reference Comments

A Available on request.

B Inserted in N/Protein, N-Brew, NC-Soils, NC-Sediments and NC Filters Standard Outfit.

C Liquid device for liquid containers (available on request), allows the analysis of hygroscopic solid compounds and volatile liquid substances without variation of weight.The samples are introduced in the container using a spatula, syringes or generic needles. We suggest the use of liquid tin containers or capillaries according to the viscosity of the liquid sample. The container is then placed in the sealing device slide. The container is to be purged with a flow of Oxygen or Helium before closing. The container is tightly closed and the constancy of weight is monitored by an electronic balance. For liquids with high vapor pressure use tin capillaries: the treatment with inert gas in not necessary because the vapor pressure generated by the liquid sample is sufficient to flush the atmospheric gases from the container.


22 Sample Preparation Accessories

Figure 7. Accessories

D This device, available on request, is used to carry up to 52 weighed and sealed containers from the balance to the autosampler mounted on the instrument.

E Available in all FLASH 2000 Standard Outfit Configurations. Recommended tools to clean the reactor when replacing the catalyst.

F Inserted in N/Protein, N-Brew, NC-Soils, NC-Sediments, and NC Filters Standard Outfit.

Table 66. Accessories Desciption (Continued)

Reference Comments

A B C

D E F


23

MAS 200R Autosampler for Solid Samples

MAS 200R Autosampler for sold samples is shown in Figure 8.

Figure 8. MAS 200R Autosampler for Solid Samples

Spare PartsTable 67. MAS 200R Autosampler for Solid Sample - Spare Parts


1 MAS 200R Autosampler (complete) one drum 1 251 174 00

2 Loading Spring 1 315 052 11

3 Positioning Spring 1 315 052 12

4 Gear Plate 1 358 006 26

5 MAS 200R Geared Motor 1 318 076 28

6 MAS 200R Plastic Front Cover 1 241 055 35


23 MAS 200R Autosampler for Solid Samples

Knurled Screws Kit

7 MAS 200R Complete Shaft (piston) 1 343 015 12

7 MAS 200R Drum No 1 (0 - 32 Position) 1 240 101 35

8 Additional MAS 200R Drum No 2 (33 - 63 Position) 1 240 101 36



11 Window O-ring (Set of 10) 1 290 300 14

12 MAS 200R Internal O-ring (Set of 10) 1 290 300 17

13 MAS 200R Plastic Cover 1 241 044 77

14 MAS 200R Assembly Motor 1 318 076 24

15 MAS 200R Plastic Inner Window 1 301 080 20

Table 67. MAS 200R Autosampler for Solid Sample - Spare Parts (Continued)

Table 68. MAS 200R Autosampler for Solid Sample - Knurled Screws Kit


1 Knurled Screws Kit (Set of 3) 1 190 042 57

This kit allows to further simplify the shaft cleaning procedure. By replacing with the practical finger-tightening knurled screws, the access to the shaft in the MAS 200R autosampler for maintenance, can be performed in a jiffy. This kit is applicable on all MAS 200R models.


23 MAS 200R Autosampler for Solid Samples

Switching BoxFigure 9. Swithcing Box for MAS 200R Autosampler

Table 69. MAS 200R Autosampler for Solid Sample - Swithcing Box


1 Switching Box

When the analyzer is equipped with two MAS 200R autosamplers, it is possible to switch from a channel to the other by using the dedicated Switching Box as schematically shown in the figure below.

1 432 101 52

21

43

MAS200 R"A"

MAS200 R"B"

Autosampler

SWITCHINGBOX

A B

A B


24

NoBlank Sampling Device

Figure 10. NoBlank Sampling Device

NoBlank sampler option is a special device, applied to OEA/IRMS and OEA instrument, which are the primary function to reduce the Nitrogen Blank Peak to a very low value. Reducing the Nitrogen Blank Peak Area means to increase the accuracy and precision power of the IRMS analyzer.

The NoBlank sampler option can be installed on:

• FLASH 2000 models, especially on IRMS and HT configurations

• TC/EA instruments and all previous Thermo Fisher Scientific OEA models as FlashEA 1112, EA1110, EA 1108, NA 2500, and so on.


24 NoBlank Sampling Device

For Upgrading FLASH System

For Updating TC/EA and Previous OEA Models

No Blank Spare Parts

Table 70. NoBlank Sampling Device For Updating FLASH System


1 NoBlank Sampler Option

It is constituted to:

• NoBlank system

• Standard outfit

• Instruction manual

1 432 102 30

Table 71. NoBlank Sampling Device For Updating TC/EA and Previous OEA Models

No Description Part Number

1 NoBlank Sampler Option 432 102 30

2 MAS 200 R with a 32 position drum 432 174 00

3 MAS Driver (for servo air automation to electric signal) 432 101 50

Table 72. NoBlank Sampling Device Spare Parts


1 NoBlank rulon cone complete 281 135 20

2 NoBlank rulon cone o-ring 290 003 56

3 O-ring NoBlank bottom (Set of 5) 290 003 17


25

CM2 Manual Sampler

CM2 manual sampler is shown in Figure 11.

Figure 11. CM2 Manual Sampler

Table 73. CM2 Manual Sampler


1 CM2 Manual Sampler 1 251 026 50

Note CM2 Manual Sampler can be installed on 18 mm OD Quartz Reactor and 25 mm OD HPAR Reactor. The CM2 Standard Outfit contains both connections. The CM2 Standard Outfit also includes parts used for the FLASH 2000 by using 18 mm OD reactors, for the FlashEA 1112 and EA 1110 Elemental Analyzers, and other parts only for any FLASH 2000 Configurations by using the 25 mm OD oxidation reactor. Refer to the following table.


25 CM2 Manual Sampler

Part Number Part Description Instrument Configuration

350 084 17 Adapter for 18 mm OD reactors EA 1110 - FlashEA 1112 - FLASH 2000 All the configurations (*)

350 014 27 Nut 304 EA 1110 - FlashEA 1112 - FLASH 2000 All the configurations (*)

290 009 17 O-Ring 2068 EA 1110 - FlashEA 1112 - FLASH 2000 All the configurations (*)

350 084 18 Adapter for 25 mm OD reactors FLASH 2000 - FlashEA 1112 N/Protein - NC-Soils

350 014 65 Nut 1”1/4 FLASH 2000 - FlashEA 1112 N/Protein - NC-Soils

(*) All the configurations except N/Protein and NC-Soils


26

AI/AS 1310 Autosampler for Liquids for FLASH 2000

AI 1310 AS 1310

Table 74. AI 1310 / AS 1310 Autosampler for Liquid Samples for FLASH 2000


1 AI 1310 for liquids 1 251 175 71

2 AS 1310 for liquids 1 251 175 72

3 Upgrade option AI 1310 to AS 1310 1 190 502 94

4 10 μL syringe 1 365 005 25

5 50 μL syringe 1 365 040 40

6 100 μL syringe 1 365 040 41

7 250 μL syringe 1 365 040 42

8 0.5 μL syringe 1 365 040 45

9 8-position tray with label 1 240 101 40

10 105-position tray for AS 1310 1 240 101 45


26 AI/AS 1310 Autosampler for Liquids for FLASH 2000

11 Waste bottle complete with 5 septa and caps 1 240 124 16

12 Complete Vials 2 SVW Package (Set of 100) - Sample Vials[Screw top cap and septa are included]

1 240 140 19

13 Vial Solvent 4 mL S T4-SVQ (Set of 5) - Solvent Vials[Screw top cap and septa are included]

1 240 140 32

14 Septa 8-ST (Set of 5) [This septa can be used for Sample Vials and Solvent Vial; see points 12 and 13]

1 313 032 18

15 BTO Septa for FLASH 2000 injector (Set of 50) 1 313 032 30

16 Screw Caps 8-SC for sampling vials and solvents vials (Set of 100) 1 386 060 74


18 Insulating Collar 1 321 003 10

19 Insulating Injector for Biodiesel 1 247 052 50

Table 74. AI 1310 / AS 1310 Autosampler for Liquid Samples for FLASH 2000 (Continued)

For more details on Biodiesel liquid samples(AS 1310 and insulating injector & collar) require the OEA Application Note n. 11008


26 AI/AS 1310 Autosampler for Liquids for FLASH 2000

Table 75. AI 1310 / AS 1310 AI/AS 1310Spare Parts


1 AI/AS 1310 M/S printing circuit board assembly 1 152 200 80

2 Complete Base assembly AI/AS 1310 1 221 071 10

3 Complete Top cover assembly AI/AS 1310 1 241 055 70

4 Slide stepper motor AI/AS 1310 1 318 029 25

5 Front door AI/AS 1310 1 333 309 50

6 AI/AS 1310 bracket for FLASH 2000 1 368 127 42

7 Complete Tower assembly AI/AS 1310 1 370 014 40

Table 76. AI 1310 / AS 1310 Cables


1 Power Cable 10A/250V 1 230 330 00

2 Power Cable 10A/125V 1 230 330 35

3 RS232 cable 1 230 435 01

4 Flat Cable Flex 26F/16F 1 230 456 65


27

Accessories for Injection of Liquid and Gas Samples

Table 77.


1 Manual Injection Device for Liquid or Gas Sampling 1 190 041 38

The kit includes:

• Injector body for OEA

• Coupling joint for liquid/gas

• Injection connection

• Different septum holders for every FLASH 2000 and previous OEA models

• Syringes = 10 μL; 100 μL; 500 μL

• Septa BTO 11.5 mm OD (Set of 50)

Manual InjectionDevice


28

Resting Foot Kit

In our continued instrumental design modification based on customer request to cover different lab table types we are now introduced the Resting Foot kit.The foot are robust, aluminum legs painted in the same FLASH color.

The function of the kit is to lift the FLASH chassis off the table top some additional millimeter (height: 25 mm) allowing more room for access the oven and opening of the traps compartment.

The Resting Foot Kit is an option and it can be order separately.

Table 78.


1 Resting Foot Kit (Set of 4) 1 190 042 58


29

Recommended Spare Parts

Table 79. Recommended Spare Parts


1 Complete Furnace (18 mm furnace adapter). *See Note 1 354 600 21

2 Complete Furnace (25 mm furnace adapter). *See Note 1 354 600 22

3 Complete HT Furnace (18 mm furnace adapter, max temperature 1450 °C) 1 354 600 35

4 HWD 430 Detector 1 419 075 10

5 Heater for Oven 1 354 215 10

6 Temperature Sensor Pt 100 for Oven 1 403 110 95

7 Thermocouple Pt/Pt-Rh 1 403 200 05

8 HT Thermocouple Pt/Pt-Rh for FLASH HT 1 403 200 06

9 Furnace Transformer for all FLASH versions except HT 1 413 250 75

10 Furnace Transformer for FLASH HT 1 413 250 76

11 3.6 V Battery 1 219 015 05

12 Fan V2S 1 406 003 00

13 Fuse, slow-blow, 1.6 A, 5x20 mm 1 282 040 18

14 Fuse, slow-blow, 800 mA, 5x20 mm 1 282 050 11

Note * Complete Furnace includes the Pt/Pt-Rh thermocouple


30

FLASH 2000 FPD Option

The OEA / FPD option — PN 432 101 45 — increases the sensitivity in Sulphur determination by using a highly selective and sensitive Flame Photometric Detector (FPD) coupled with the FLASH 2000 Elemental Analyzer.

This FPD option can be applied to any FLASH 2000 configuration and it allows the determination of trace Sulphur (low limit: 10 ppm) in both liquid and solid compounds.

The OEA / FPD option comprises of:

• FPD 1112 detector module that includes the FPD detector and the pneumatic circuit to control the detector gases flows PN 432 098 86

• FPD control module to control the detector parameters PN 432 098 86.

• FPD standard outfit PN 165 001 10

Figure 12. FLASH 2000 with FPD Option


30 FLASH 2000 FPD Option

FPD Performance Specifications

OEA / FPD Reference Material

Table 80. FPD Performance Specifications

Performance Specifications

Low Limit 0.001% (10 ppm) SulphurMax Limit 0.5% (5000 ppm) Sulphur

(for more info refer to FLASH 2000 Technical Specifications)Gas Requirements Helium Chromatographic-grade purity

• Air 99.995%

• Hydrogen 99.995%Power Requirements 120/230 Vac; 50/60 HzHost Hardware Requirements Pentium Processor-operating system Windows® 2000, XP, Vista, or Windows 7Host Software Requirements Eager XperienceDimension Gas Control box: 177 x 235 x 287 mm (l x h x d)

FPD Control Module: 180 x 85 x 485 mm (l x h x d)Mass Gas Control box: 5 kg

FPD Control Module: 6 kg

Table 81. OEA / FPD Reference Material

Description Qty Part Number

Pasta Reference Material for Sulphur Determination (OEA/FPD) 2g 338 400 27

Soil Reference Material 2g 338 400 26

Reference Solutions Kit constituted by 4 flasks (2 mL each) containing 10, 50, 100, and 500 ppm of Sulphur

1 338 190 40



OEA / FPD Detector Spare PartsRefer to the following table:

Table 82. Flame Photometric Detector Spare Parts

Ref. Description Qty. Part Number

1 Mirror plug 350 053 50

2A Maintenance kit for FPD Graphite seal 2 190 045 89

2B Heat shield 2

2C VitonTM O-ring 3106 1

2D VitonTM O-ring 3175 1

2E VitonTM O-ring 75 SH 1

3 Detector body 1 190 501 11

4 Aluminium O-ring 1 290 032 30

5 FPD jet 1 404 045 11

6 Flange and relevant VitonTM O-ring 1 368 142 35

7 Interferential filter for sulphur 1 281 070 00

8 Photomultiplier 1 286 004 50

9 Heater/sensor/coil cable (1.5 m) 1 230 435 87

10 FPD fixing tool 1 205 021 50

Silcosteel tubing 1 m; 0.4 mm OD x 0.25 mm ID 1 391 100 25

Graphite ferrule ID 0.45 for silcosteel tubing (Set of 2) 1 290 134 87

Nut for silcosteel tubing (Set of 5) 1 350 324 23



Figure 13. FPD Spare Parts


31

Electronic Flow Controller Module

Table 83. EFC-t Module


1 EFCt Module (complete) for FLASH 2000 models

The kit includes:

• Flow Sensor

• 2-way Valve (Normally Open)

• 2-way Valve (Normally Closed)

• Proportional Valve

• 3-way Valve

1 425 091 50


32

FLASH 2000 Electronics and Cables

Printed Circuit Boards

Table 84. Printed Circuit Boards


1 TRF1112 Transformer Board 1 236 484 45

2 MB1112 Mother Board 1 236 484 50

3 AC1112 Alternative Current Board 1 236 484 55

4 TCR1112 Thermo Control Board 1 236 484 60

5 HWD1112 TCD Control Board 1 236 484 65

6 CPU1112 Central Processing Board 1 236 484 70

7 PWR1112 Power Supply Card 1 236 484 80

8 DPFC1112 Electronic Flow Control Board 1 236 484 90

9 LTA-1 Thermo Coupled Linearizer Box 1 209 017 00

10 LTA-1 HT 1 209 017 03

10 EV Control Box (Only for FlashEA 1112 with non-thermostatted EFC module) 1 333 209 60

11 Synoptic Panel (Complete) 1 333 105 45


32 FLASH 2000 Electronics and Cables

Cables

Table 85. Cables


1 Power Cable ( Part of the FLASH 2000 Standard Outfit) 1 230 330 00

2 RS 232 Cable ( Part of the FLASH 2000 Standard Outfit) 1 230 334 85


33

Eager Xperience Ethernet A/D

Ethernet Box Version PN 432 331 37This Kit allows to upgrade all Eager 200 to Eager Xperience.

The Eager Xperience Ethernet box comprises of:

• Ethernet adapter box

• Eager Xperience Program (CD-Rom)

• Eager Xperience Software Manual

• Connecting cables for FLASH 2000 and previous OEA modules.

Examples:

Eager Xperience Hardware Minimum Requirements

EA 1110 / Eager 200 EA 1110 / Eager Xperience (with a PC with the minimum requeriments listed below) + Ethernet box

FLASH (TCD) + Eager Xperience FLASH (TCD+FPD) + Eager Xperience + Ethernet box

Table 86. Hardware Minimum Requirements

Component Description

Computer Any PC can be used, including laptop computer

Operating System: Windows™ 2000 / XP / Vista / Windows 7

Hard drive with at least 1 GB free

One free COM port for instrument control

One free COM port for balance, if required

One free COM port for AI/AS 1310 – AI/AS 3000 II autosampler, if required

CD driver

Monitor Color 1024 x 768 or better

Printer Any printer accepted by the operating system


33 Eager Xperience Ethernet A/D

RS232/USB Converter PN 230 381 31The UPort 1110 connects USB to serial adapter enables a serial device to be connected to a computer through the USB port. The unit features a portable design that does not require external power or complicated setup procedures. A CD with drivers is included (Window 98, 2000, XP, Vista, Windows 7). LEDs for indicating USB and transmission data (TxD), and receiving data (RxD) activity are present.

IMPORTANT The RS232/USB converter is now included in the FLASH 2000 standard outfit but it can be ordered separately.


34

Single to Double Furnace Upgrade Kit

The kit allows to transform the configuration of your analyzer, for example CHN or CHNS, equipped with a single furnace, in a configuration having two furnaces (18 mm OD), for example CHN-O or CHNS-O.

The kit is suitable for every FLASH 2000 models.

Table 87. Single to Double Furnace Upgrade Kit


1 Single to Double Furnace Upgrade Kit

It is constituted to:

• Furnace (Complete)

• Plate

• Connections

• Fittings

• Accessories

• Cable

• Instruction manual

1 190 042 77


34 Single to Double Furnace Upgrade Kit

Figure 14. Furnace Compartment

Left furnace Right furnace


35

Furnaces Transformation Kits

FLASH 2000 Configuration

Configuration Furnace L Bottom Conn. L Furnace R Bottom Conn. R

CHN, CHNS, NCS, O yes (18 mm) 2x1 mm no no

CHN/O or CHNS/O yes (18 mm) 2x1 mm yes (18 mm) 2x1 mm

N Org yes (18 mm) 4x2 mm yes (18 mm) 4x2 mm

N Lubricant yes (25 mm) 6x4 mm yes (25 mm) 6x4 mm

NC org yes (18 mm) 4x2 mm yes (18 mm) 4x2 mm

NC Soils yes (25 mm) 4x2 mm yes (18 mm) 4x2 mm

N / Protein yes (25 mm) 6x4 mm yes (25 mm) 6x4 mm

FLASH 2000 IRMS yes (18 mm) 2x1 mm yes (18 mm) 2x1 mm

FLASH 2000 HT yes (18 mm)1 2x1 mm yes (18 mm)2 2x1 mm

1. O/N Determination 2. NC Determination


35 Furnaces Transformation Kits

Transformation Kits Available

IMPORTANT The transformation kits do not include the furnace but the adapters, connectors, plate assembly, and so on.

According to the option reported in Table A and Table B, four different kits are available:

1 Transformation furnace kit (from 25 to 18 mm, bottom connector 2x1 mm) 190 042 51




Example: from CHNS/O to NC Soils model

CHNS/O: 2 furnaces 18 mm; both bottom connections 2x1 mm

NC Soils: 2 furnaces (25 mm, 18 mm); bottom connection 4x2 mm

For this modification needs:

• Transformation kit (from 18 to 25 mm, bottom Conn. 4x2) n.1

• Bottom Connection (18 mm, 4x2 mm) n.1

• 4 x 2 SS tubing and relative joints



If the User Wants to Add a New Furnace (and Upgrade the Instrument Configuration)

In this case the user needs need a complete furnace and a transformation furnace kit. A furnace will be chosen according to the application (18 or 25 mm type) while the kit will be used for find all the top level FLASH 2000 reactor connection (on the top level of the instrument) and for the bottom connection according to the analysis requested:

• 18 mm, bottom connection 2x1 mm




Example: CHN (single furnace) CHN/O (double furnaces)

For this modification needs:

• Complete furnace (18 mm diam) p/n 354 600 21

• Transformation kit (18 mm, bottom Conn. 2x1 mm) p/n 190 042 51

• 2 x 1 SS tubing and relative joints



Transformation Furnace Kits ListThe items inserted in the transformation kits are here listed:

Table 88. Transformation Furnace Kit 18 to 25 mm bottom connection 6x4 mm


Transformation Furnace Kit from 18 to 25 mm bottom connection 6 x 4 mm 1 190 042 71

1 Furnace Adapter 1

2 Bottom O-ring (Set of 5) 1

3 Top O-ring (Set of 5) 1

4 Seal for Furnace Adapter; 25 mm 1

5 Aluminium Ferrule; 2 mm diam. 6

6 Plate assembly (circular) 1

7 6MB nut (Set of 10) 1

8 Fixing Cup 1

9 Cup (5x3 mm) 4

10 Tube connector for PTFE; 5x3 mm 4

11 Top Connector (25 mm) 1

12 Screw (4x20 mm) 2

13 Polyethylene Tube; 5x3 mm; 1 m 1

14 Clip (Filter fixing) 4

15 Pressure Equilibration Cylinder 1

16 Clip (Pressure equil. Cylinder fixing) 1

17 Teflon Tube; 2x1 mm; 1 m 1

18 Bottom Connection (25 mm diam; 6x4 mm) 1

19 PTFE Tube; 6x4 mm; 1 m 1

20 OR/OV Viton 1

21 Nut, M 12x1 mm 1

22 Plate Assembly (rectangular) 1

23 Screws for plate assembly (circular) 3



Table 89. Transformation Furnace Kit from 18 to 25 mm bottom connection 4x2 mm



1 Furnace Adapter 1

2 Bottom O-ring (Set of 5) 1

3 Top O-ring (Set of 5) 1

4 Seal for Furnace Adapter 25 mm 1

5 Aluminium Ferrule 2 mm diam. 6

6 Plate assembly (circular) 1


8 Fixing Cup 1


10 Screw (4x20 mm) 2

11 Clip (Filter fixing) 4

12 Teflon Tube; 2x1 mm; 1m 1

13 Bottom Connection (25 mm diam; 4x2 mm) 1

14 PTFE Tube; 4x2 mm; 1 m 1

15 4 mm OD Ferrule (Set of 10) 1

16 Nut, M1; 2x1 mm 1

17 Plate Assembly (rectangular) 1







1 Furnace Adapter 1

2 Bottom O-ring for 18 mm OD Quartz Reactor (Set of 5) 1

3 Top O-ring for 18 mm OD Quartz Reactor (Set of 5) 1

4 Seal for Furnace Adapter 18 mm 1

5 Plate assembly (circular) 18 mm diam. 1


7 Fixing Cup; 18 mm 1


9 Screw for Filter Clip 2

10 Filter Clip 2

11 Teflon Tube; 2x1 mm; 1 m 1

12 Bottom Connection; 18 mm diam; 2x1 mm 1

13 PTFE Tube; 2x1 mm; 1.5 m 1

14 Ferrule (Set of 10) 1

15 Plate Assembly (rectangular) 18 mm diam. 1







1 Furnace Adapter 1

2 Bottom O-ring for 18 mm OD Quartz Reactor (Set of 5) 1

3 Top O-ring for 18 mm OD Quartz Reactor (Set of 5) 1

4 Seal for Furnace Adapter;18 mm 1

5 Plate assembly (circular) 18 mm diam. 1


7 SS Tube; 2x1 mm 3 m

8 Top Connector 18 mm 1

9 Screw for Filter Clip 2

10 Filter Clip 2

11 Fixing Cup; 18 mm 1 m

12 Bottom Connection; 18 mm diam; 4x2 mm 1

13 PTFE Tube (4x2 mm) 1.5 m

14 Ferrule (Set of 10) 1

15 Fixing Nut 1

16 Ferrule 2x1 mm (Set of 10) 1

17 PTFE Tube; 2x1 mm; 1.5 m 1

18 Plate assembly (rectangular); 18 mm diam. 1




Transformation Furnace Kit: Explanations on Some Items

Plate Assembly

The circular (18 and 25 mm) plate is used.

Top Connections

Circular plate


3 Circular plate Assembly 18 mm 350 084 60

4 Circular plate Assembly 25 mm 350 084 65


1 Top Connector 18 mm 350 084 21

2 Top Connector 25 mm 350 084 23



Furnace AdaptersThe washer adapter (18 or 25 mm) is placed on the top of the furnace.

Under the washer is placed the suitable seal.

Bottom Connections


1 Furnace Adapter 18 mm 267 027 22

2 Furnace Adapter 25 mm 267 027 21

3 Seal for Furnace Adapter 18 mm 290 036 32

4 Seal for Furnace Adapter 25 mm 290 036 33

18 mm diameter 25 mm diameter


1 Bottom connection (18 mm diameter; 2x1) 350 084 33


3 Bottom connection (25 mm diameter.; 6x4) 350 084 26




Bottom Connections for FLASH IRMS and HT (O/H and NC Determinations)

The FLASH bottom connection for IRMS and for HT is different from other OEA configurations. The bottom connection is constituted by the following parts:

According to the FLASH configurations, if necessary to have a complete system the following parts should be ordered:

• Bottom Connection (if requested)

• Reactors (quartz or special stainless steel)

• Crucible (quartz or special stainless steel)

• Filter (small or large)

• Separation column

• Catalysts

• Adsorber


1 Nut 350 114 10

2 Metal Ring 356 032 10

3 Washer 290 029 10

4 Reactor Coupling Union 350 084 27


36

MAS 200R Driver

The MAS 200R Driver is a device which allows to the older OEA models (EA 1110, NA 2100, EA 1108, and so on) equipped with the pneumatically actuated AS 128 or AS 200 autosamplers to be up-graded to the new electrically actuated MAS 200R.

AS 128 / AS200

Pneumatic actuated autosamplers for EA1110, EA 1108 and TC/EA, NA2500, NA1500, and so on.

Utilities: Servo Air + Helium / Oxygen

The AS 128 and AS 200 on previous OEA models can be replaced by this system:

MAS 200R (PN 251 17400) + MAS 200R Driver (PN 432 10150)

Utilities: Helium / Oxygen

The MAS 200R Driver is easy to install and it will be provided with a detailed installation guide.

MAS200 R Driver

AC Adapter


36 MAS 200R Driver


1 MA S200R Driver

The MAS 200R Driver includes:

• MAS 200R Driver base unit

• AC adapter / power module

• Power cord

• Cable provided

• Cable for IRMS

1 432 101 50

Dimensions & mass:

• Dimensions (w x d x h): 80 x 146 x 45 mm

• Mass (MAS 200R Driver base unit): 200 g

• Mass (MAS 200R Driver complete including power module, cables, and so on): 900 g


37

FLASH 2000 System Qualification Package

Qualification is a process to evaluate and certify the performances of the instrument.

Qualification is a process of signing, dating and executing a Set of qualifications which can be stored in the Thermo Scientific Qualification folder.

FLASH 2000 equipment and the relative Eager Xperience software is validated for the installation (Installation Qualifications IQ), and operation (Operation Qualification OQ).

The procedure requires typically two (2) days of “on-site” testing including executing, dating, and signing a Set of qualifications which are stored in the Thermo Scientific Qualification Folder.

For the FLASH Qualification are requested:

• The FLASH Qualification Package folder (PN 199 100 21)

• One (or more) qualification kit according to the configuration which consists of consumables, standards, filters and GC separation column (all components required for the qualification procedure).

Chart of Qualification Kits


1 FLASH 2000 System Qualification Package Folder

Including AI/AS 1310 – AI/AS 3000 II for OEA Qualification Package

1 199 100 21

No Description Qty Part Number1 CHN Qualification Kit 1 190 042 802 CHNS Qualification Kit 1 190 042 853 O Qualification Kit 1 190 042 904 N Org Qualification Kit 1 190 042 955 NC Org Qualification Kit 1 190 043 006 NCS Qualification Kit 1 190 043 057 NC-Soil Qualification Kit 1 190 043 108 N/Protein Qualification Kit 1 190 043 159 N-Brew Qualification Kit 1 190 043 2010 AI/AS for OEA Qualification Kit 1 190 043 25


37 FLASH 2000 System Qualification Package

WARNING The FLASH 2000 Qualification can be done with Thermo Fisher Scientific OEA consumables exclusively.

The FLASH 2000 Qualification can be carried out only by trained Thermo Fisher Scientific OEA specialist.


2Part

Thermo Scientific FLASH 4000

38

FLASH 4000 N/Protein Determination

Table 92. Consumables and Spare Parts for FLASH 4000 N/Protein Determination


Bottom and Top O-ring SI 80, 48 mm OD (Set of 5) 1 290 106 94

Quartz Wool (15 g) 1 338 220 05

Copper Oxide (25 g) 1 338 217 30

Platinum supported on Alumina (100 g) 1 338 390 55

Copper (220 g) 1 338 353 05

Empty HPAR 4000 reactor 1 468 02020

HPAR 4000 Crucible (Complete) 1 252 050 15

Ceramic disk (Set of 20) 1 272 045 05

Crucible Single Tube 1 252 050 35

Silicone O-ring HPAR crucible, 32 mm OD (Set of 5) 1 290 106 84

Lubricant for O-ring (50 g) 1 290 000 57

Separation column N/Protein FLASH 4000, 840 mm length 1 260 082 30

Tin disks; 62 mm diameter (Set of 100) 1 252 080 19

Tin disks; 85 mm diameter (Set of 100) 1 252 080 21

Curved tweezer 1 205 005 00

Plastic flat tweezer 1 205 005 05

Spatula 1 205 006 21

EDTA standard (100 g) 1 338 001 10

Glucose (100 g) 1 338 001 15

Pasta Reference Material (100 g) 1 338 400 28


38 FLASH 4000 N/Protein Determination


39

Kit of Consumables for FLASH 4000

Kit for 1000 Analyses

Kit for 5000 Analyses

Table 93. Kit for 1000 Analyses


Kit for 1000 analyses 1 190 024 40

Tin disks 62 mm OD; 10 μm thickness (Set of 100) 10 252 080 19

HT ceramic disk for crucible (Set of 20) 1 272 045 05

Silicone O-ring HPAR Crucible, 32 mm OD (Set of 5) 1 290 106 84


EDTA Standard (Flask of 100 g) 1 338 001 10

Glucose (Flask of 100 g) 1 338 001 15

Copper Oxide (25 g) 1 338 217 30

Quartz Wool (15 g) 1 338 220 05

Reduced Copper (Flask of 220 g) 4 338 353 05



Table 94. Kit for 5000 Analyses


Kit for 5000 analyses 1 190 024 50

Tin disks 62 mm OD; 10 μm thickness SI80 (Set of 100) 50 252 080 19

HT ceramic disk for crucible (Set of 20) 5 272 045 05

Silicone O-ring HPAR Crucible, 32 mm OD (Set of 5) 1 290 106 84


EDTA Standard (Flask of 100 g) 3 338 001 10


39 Kit of Consumables for FLASH 4000

Glucose (Flask of 100 g) 3 338 001 15

Copper Oxide (25 g) 1 338 217 30

Quartz Wool (15 g) 5 338 220 05

Reduced Copper (Flask of 220 g) 20 338 353 05



Table 94. Kit for 5000 Analyses (Continued)



40

Reactor, Crucible, Separation Column and Fittings

Reactor

Crucible

Table 95. Reactor


1 Empty HPAR 4000 reactor 1 468 020 20

2 Cleaning device for HPAR reactor 1 205 006 25

3 HPAR reactor extractor 1 205 006 29

4 Bottom and Top O-ring SI 80, 48 mm OD (Set of 5) 1 290 106 94

Table 96. Crucible


1 HPAR 4000 crucible complete (upper + bottom parts) Not aligned pins

1 252 050 15

2 HPAR 4000 crucible body (upper part) Not aligned pins

1 252 050 20

3 HPAR 4000 crucible bottom part (ash tray) Not aligned pins

1 252 050 30

4 HPAR 4000 crucible complete (upper + bottom parts) Aligned pins

1 252 050 40

5 HPAR 4000 crucible body (upper part) Aligned pins

1 252 050 45

6 HPAR 4000 crucible bottom part (ash tray) Aligned pins

1 252 050 50

7 HPAR 4000 crucible single tube 1 252 050 35

8 Crucible extractor 1 205 006 29

9 High temperature ceramic disk (Set of 20) 1 272 045 05

10 Cleaning device for crucible 1 276 060 10

11 Silicone O-ring HPAR crucible 32 mm OD (Set of 5) 1 290 106 84


40 Reactor, Crucible, Separation Column and Fittings

Separation Column

Fittings

Table 97. Separation Column


1 Separation column N/Protein FLASH 4000, 840 mm length 1 260 082 30

Table 98. Tubings


1 PTFE white tubing 1/8-in OD 1 m 420 011 00

2 PTFE red tubing 1/8-in OD 1 m 420 011 05

3 PTFE blue tubing 1/8-in OD 1 m 420 011 10

4 PTFE green tubing 1/8-in OD 1 m 420 011 15

5 Copper tubing 1/8-in OD - 1/16-in ID 2.6 m 420 011 20

6 PTFE white tubing 1/4-in 2 m 420 011 25

Table 99. Nuts


1 PTFE nut for 1/8-in tubing connection [Water drain] (Set of 5) 1 350 024 38

2 PTFE nut for 1/4-in tubing connection [Water drain] (Set of 5) 1 350 024 39

3 Brass nut 1/8-in (Set of 5) 1 350 130 63

4 Brass nut 1/4-in (Set of 5) 1 350 130 64

Table 100.Ferrules


1 PTFE ferrule 1/8-in; back + front (Set of 10) 1 290 046 00

2 PTFE ferrule 1/4-in; back + front; single piece 1 290 046 97

3 Brass ferrule 1/8-in; back + front (Set of 5) 1 290 246 66

4 Brass ferrule back + front; single piece; for 10-mm OD tubing 1 290 046 69


41

Consumables and Miscellanea

Consumables

Miscellanea

Table 101.Reactor


1 Sample holder (12 positions) 1 240 100 49

2 Tin disks 62 mm OD; 10 μm thickness (Set of 100) 1 252 080 19

3 Tin disks 85mm OD; 10 μm thickness (Set of 100) 1 252 080 21

4 HT ceramic disk for crucible (Set of 20) 1 272 045 05

5 Lubricant (silicone grease) 1 290 000 57

6 EDTA Standard (100 g) 1 338 001 10

7 Glucose (100 g) 1 338 001 15

8 Copper Oxide (100 g) 1 338 217 20

9 Quartz Wool (15 g) 1 338 220 05

10 Reduced Copper (220 g) 1 338 353 05

11 Platinum supported on Alumina (100 g) 1 338 390 55


Table 102.Miscellanea


1 2.5-mm Allen wrench 1 205 018 03

2 3-mm Allen wrench 1 205 018 04

3 Phillips screwdriver 1 205 026 09

4 1/2-in; 9/16-in wrench 1 205 030 04

5 5.5-mm wrench 1 205 030 05

6 7-mm wrench 1 205 030 07

7 7/16-in wrench 1 205 030 15


41 Consumables and Miscellanea

8 18/19-mm wrench 1 205 030 20

9 Door hinge 1 212 040 50

10 LED panel 1 333 153 10

11 Check valve (It is placed in the carrier line before the vent) 1 405 095 10

Table 102.Miscellanea (Continued)



42

Analytical Standards & Reference Material

Standard

Reference Material

Table 103.Analysis Standards


EDTA standard (100 g) 1 338 001 10

Glucose (100 g) for Blank Analysis 1 338 001 15


Standard N% C% H% S% O%

EDTA 9.59 --- --- --- ---

Reference Material N% C% H% S% O%

Pasta (Batch H13A) 1.89 --- --- --- ---

IMPORTANT All the standards and the references material are accompanied with a quality certificate including the storage condition and the lifetime of the products.


43

Sample Preparation Accessories

Sample Containers

Table 104.Sample Containers


Tin disk 62 mm (Set of 100) 1 252 080 19

Tin disk 85mm (Set of 100) 1 252 080 21

Table 105.Sample Preparation Accessories


1 Tin disk 62 mm (Set of 100) 1 252 080 19

2 Tin disk 85 mm (Set of 100) 1 252 080 21

3 Curved tweezer 1 205 005 00

4 Plastic flat tweezer 1 205 005 05

5 Spatula 1 205 006 21

6 Cleaning device for HPAR reactor 1 205 006 25

7 Capsulator (complete of cylindrical tool) 1 252 053 00

8 HPAR reactor extractor 1 205 006 26

9 Crucible extractor 1 205 006 29

10 Cleaning device for crucible 1 276 060 10

11 FLASH 4000 sample holder (12 positions) 1 240 100 49

Capsulator

Cylindrical tool


44

MAS 4000 Autosampler

The MAS 4000 autosampler is shown in Figure 15.

Figure 15. MAS 4000 Autosampler

Spare Parts

Table 106.MAS 4000 Spare Parts


1 MAS 4000 complete with one sample tray (from 1 to 31 samples) 1 251 175 00

2 MAS 4000 base body without piston 1 247 037 00

3 Plastic cover for sample tray 1 241 011 05

4 O-ring (OR 2056) 1 290 003 15

5 Viewer 1 310 007 00

6 Viewer support 1 310 007 05

7 Viewer lens 1 310 008 00

8 Sample tray motor 1 318 079 10

9 Piston motor 1 318 079 10


44 MAS 4000 Autosampler

10 Sample tray #1 numbered from 1 to 31 1 334 096 00



13 Sample tray #4 numbered form 94 to 124 1 334 096 30

14 Piston 1 343 015 15

Table 106.MAS 4000 Spare Parts (Continued)



45

Recommended Spare Parts

Pressure Regulators and Manometer

Detector Oven

Furnace

Table 107.Pressure Regulators and Manometer


1 Pressure regulator PRV 20M 1 425 091 70

2 Manometer 0–300 kPa (0–3 bar) 1 367 160 60



Table 108.Detector Oven


1 HWD 430 Thermo Conductivity Detector (Hot Wire detector) 1 419 075 10

2 Heater element 70 W; 220 V 1 354 215 20

3 Pt 100 probe complete 1 403 112 70

Table 109.Furnace


1 Furnace complete 1 354 600 40

2 Furnace bottom connector 1 350 084 80

3 Thermocouple Pt/Pt-Rh for FLASH 4000 1 403 200 04


45 Recommended Spare Parts

EV (electrovalves) Block

Regenerative Carbon Dioxide Filter

Water Drain

Table 110.EV Block


1 EV block assembly (complete) 1 425 091 28

2 Three-way solenoid valve 1 405 161 57

Table 111.Regenerative Carbon Dioxide Filter


1 Regenerative CO2 Filter assembly 1 281 140 05

Table 112.Water Drain


1 Water drainage condenses assembly 1 119 320 90

2 Peltier cell (without CLR-EAX board) 1 119 321 00

3 Solenoid valve for Peltier cell 1 333 211 05

4 CLR-EAX board 1 236 491 80

5 Peltier bottle (250 mL) 1 240 145 49


46

Electronic Flow Control Module (EFCt)

Table 113.Electronic Flow Control Module (EFCt)


1 EFCt Module (complete) for FLASH 4000 1 425 091 60


48

Electronics

Mains and High Voltage Printed Circuit Boards

Low Voltage Printed Circuit Boards

Table 117.Mains


1 Transformer 2 kW (complete) 1 206 039 10

2 Breaker 16 A 1 237 099 16

3 PWR EAX (Power supply board) 1 236 491 65

4 ACS EAX (Furnace board) 1 236 491 70

Table 118.Printed Circuit Boards


1 EFC-CS (Power supply for EFXC-EAX board) 1 236 491 45

2 HWD-EAX (Detector) 1 236 491 40

3 FRT-EAX (Status panel) 1 236 491 50

4 MBR-EAX (Mother board) 1 236 491 55

5 CPU-EAX (CPU) 1 236 491 60

6 EXT-EAX (External communication) 1 236 491 75

7 CLR-EAX (Peltier element control) 1 236 491 80

8 EFC-EAX (Control for EFCt) 1 236 491 85

9 MAS 400 Autosampler PCB 1 236 491 90


48 Electronics

Fuses

Fans

Cables

Extension Card

Table 119.Fuses


1 F1A; IEC 127/I; 5x 20 mm (PWR-EAX board) 1 282 000 14

2 T315mA; IEC 127/III; 5x20 mm (PWR-EAX board) 1 282 040 11

3 T3.15A; IEC 127/III; 5x20 mm (ACS-EAX board) 1 282 040 21

4 FF16A; IEC 269; 6.3 x 32 mm (ACS-EAX board) 1 282 040 25

5 FF20A; CH10gC; 10 x 38 mm (ACS-EAX board) 1 282 040 26

Table 120.Fans


1 Rear panel fan 220 V ac; 50 Hz 1 406 003 00

2 Furnace fan (Left side) 1 406 006 95

3 Fan assembly complete (230 V ac) 1 406 006 90

Table 121.Cables


1 Power Cable (Part of the FLASH 4000 Standard Outfit) 1 230 330 25

2 RS 232 Cable (Part of the FLASH 4000 Standard Outfit) 1 230 434 85

3 LAN Cable (Part of the FLASH 4000 Standard Outfit) 1 230 434 89

4 UTP Patch Cable cross. (RED) (Part of the FLASH 4000 Standard Outfit) 1 230 435 93

Table 122.Extension Card


1 FLASH 4000 Extension Card (Useful for service engineers diagnostic purpose) 1 236 491 95


3Part

Previous FLASH Configurations

48

AI/AS 3000 II Autosampler for Liquids for FLASH 2000

AI 3000 AS 3000

Table 120.AI3000 / AS 3000 II Autosampler for Liquid Samples for FLASH 2000


1 AI 3000 Auto Injector for liquids 1 251 175 71

2 AS 3000 Auto Sampler for liquids 1 251 175 72

3 Upgrade option AI to AS 3000 II 1 190 502 94

4 10 μL syringe 1 365 005 25

5 50 μL syringe 1 365 040 40

6 100 μL syringe 1 365 040 41

7 250 μL syringe 1 365 040 42

8 0.5 μL syringe 1 365 040 45

9 8-position tray with label 1 240 101 40

10 105-position tray for AS 3000 1 240 101 45

11 Waste bottle complete with 5 septa and caps 1 240 124 16

12 Complete Vials 2 SVW Package (Set of 100) - Sample Vials[Screw top cap and septa are included]

1 240 140 19


48 AI/AS 3000 II Autosampler for Liquids for FLASH 2000

13 Vial Solvent 4 mL S T4-SVQ (Set of 5) - Solvent Vials[Screw top cap and septa are included]

1 240 140 32

14 Septa 8-ST (Set of 5) [This septa can be used for Sample Vials and Solvent Vial; see points 12 and 13]

1 313 032 18

15 BTO Septa for FLASH 2000 injector (Set of 50) 1 313 032 30



18 Insulating Collar 1 321 003 10

19 Insulating Injector for Biodiesel 1 247 052 50

Table 120.AI3000 / AS 3000 II Autosampler for Liquid Samples for FLASH 2000 (Continued)

For more details on Biodiesel liquid samples(AS 3000 and insulating injector & collar) require the OEA Application Note n. 11008

Table 121.AI 3000 / AS 3000 II Spare Parts


1 AI/AS 3000 II M/S printing circuit board assembly 1 152 200 80

2 Complete Base assembly AI/AS 3000 II 1 221 071 10

3 Complete Top cover assembly AI/AS 3000 II 1 241 055 70

4 Slide stepper motor AI/AS 3000 II 1 318 029 25

5 Front door AI/AS 3000 II 1 333 309 50

6 AI/AS 3000 bracket for FLASH 2000 1 368 127 42

7 Complete Tower assembly AI/AS 3000 II 1 370 014 40

Table 122.AI 3000 / AS 3000 II Cables


1 Power Cable 10A/250V 1 230 330 00

2 Power Cable 10A/125V 1 230 330 35

3 RS232 cable 1 230 435 01

4 Flat Cable Flex 26F/16F 1 230 456 65


49

FlashEA 1112 Elemental Analyzer

Electronic Flow Controller Modules

Oxygen Line Purge Kit for FlashEA 1112 PN 190 042 60The Oxygen Line Purge kit permits to eliminate the diffused air present in the pneumatic circuit of the oxygen line decreasing, at this way, the blank value and optimizing the OEA analysis.

The presence of the diffused air in the oxygen line may be due to the following reasons:

• damaged or worn out cylinder pressure regulator

• the length of the oxygen pneumatic line

The kit contains all the materials required to install the Oxygen Line Purge Kit on your FlashEA 1112:

Table 123.EFC-t Module


1 EFCt Module (complete) for FlashEA 1112 models with serial number S/N upper than 20034906

1 425 091 50

1 EFC Module (complete) for FlashEA 1112 models with serial number S/N up to 20034906

1 425 090 95

Part Number Description Quantity

290 040 45 Aluminium ferrules 10

347 081 03 Tee connection 1

350 004 03 6MB retaining nuts 7

391 024 00 2x1 mm SS tubing 30 cm

405 107 00 Needle valve 1


49 FlashEA 1112 Elemental Analyzer

FlashEA 1112 System Qualification PackageQualification is a process to evaluate and certify the performances of the instrument.

Qualification is a process of signing, dating and executing a Set of qualifications which can be stored in the Thermo Scientific Qualification folder.

FlashEA 1112 equipment and the relative Eager 300 software is validated for the installation (Installation Qualifications IQ), and operation (Operation Qualification OQ).

The procedure requires typically two (2) days of “on-site” testing including executing, dating, and signing a Set of qualifications which are stored in the Thermo Scientific Qualification Folder.

For the FLASH qualification are requested:

• The FLASH Qualification Package folder (PN 199 100 30)

• One (or more) qualification kit according to the configuration which consists of consumables, standards, filters and GC separation column (all components required for the qualification procedure).

Chart of Qualification Kits


1 FlashEA 1112 System Qualification Package Folder

Including AI/AS 3000 for OEA Qualification PackagePN 199 100 05

1 199 100 30

No Description Qty Part Number1 CHN Qualification Kit 1 190 042 802 CHNS Qualification Kit 1 190 042 853 O Qualification Kit 1 190 042 904 N Org Qualification Kit 1 190 042 955 NC Org Qualification Kit 1 190 043 006 NCS Qualification Kit 1 190 043 057 NC-Soil Qualification Kit 1 190 043 108 N/Protein Qualification Kit 1 190 043 159 N-Brew Qualification Kit 1 190 043 2010 AI/AS for OEA Qualification Kit 1 190 043 25

WARNING The FlashEA 1112 Qualification can be done with Thermo Fisher Scientific OEA consumables exclusively.The FlashEA 1112 Qualification can be carried out only by trained Thermo Fisher Scientific OEA specialist.


49 FlashEA 1112 Elemental Analyzer

Transformation Furnace Kit: Explanations on Some Items

Plate Assemblies

The rectangular (18 and 25 mm) plate has been mounted on FlashEA 1112 till fall 2003 (serial n.20034136) and then it has been substituted by the circular (18 and 25 mm) plate. Both Plate Assemblies (rectangular & circular) are inserted in the Transformation Kits.

Rectangular Circular


1 Plate Assembly (Rectangular) 18 mm 334 012 29

2 Plate Assembly (Rectangular) 25 mm 334 012 30

3 Plate Assembly (Circular) 18 mm 350 084 60

4 Plate Assembly (Circular) 25 mm 350 084 65


A

Customer Communication

Thermo Fisher Scientific provides comprehensive technical assistance worldwide and is dedicated to the quality of our customer relationships and services.

How to Contact UsThis appendix contains contact information for Thermo Fisher Scientific office. To contact your local Thermo Fisher Scientific office or affiliate, please refer to:

Thermo Fisher Scientific GmbhHanna-Kunath-Str. 1128199 Bremen, GermanyTel. +49 421 54930

or

Dr. Guido GiazziOEA Product Manager

Email: [email protected]: +39 (0) 2 95059 336


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