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Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology...

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Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering Kanazawa University 30 th Annual Conference on Tire Science and Technology September 13-14, 2011 Akron, Ohio, USA
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Page 1: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku**

* Graduate School of Natural Science and TechnologyKanazawa University

** College of Science and EngineeringKanazawa University

30th Annual Conference on Tire Science and TechnologySeptember 13-14, 2011Akron, Ohio, USA

Page 2: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

1. Introduction and objective

2. Apparatus and methodFriction experiment and conditionObservation methodObservation area

3. Results and discussionsCoefficient of frictionObservation in leading areaObservation in trailing area

4. Conclusions

Table of contents

Page 3: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

1. Introduction and objective

2. Apparatus and methodFriction experiment and conditionObservation methodObservation area

3. Results and discussionsCoefficient of frictionObservation in leading areaObservation in trailing area

4. Conclusions

Table of contents

Page 4: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Studless Tire

Studless tires are designed for use in winter conditions, such as snow and ice

Soft tread compoundIncrease the contact area

A lot of sipes in the tread pattern

Wipe and evacuation the water

Characteristics of studless tires

FIG.1 Tread of studless tire

Page 5: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

FIG.2 Porous rubber surface

Porous rubber is tread compound that has numerious pores both surface and inside.

The tread rubber of studless tire has been devised in various ways.

Design of tread pattern and sipesVarious hard materials in tread rubber

glass fibers, ceramics, nut shell ・・・Development of tread compound

Page 6: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

・ The water removal between tire tread and road surface by water absorption effect of the pores.

Effect of the porous rubber

FIG.3 Water removal image

The real contact area between the tire and the wet road is believed to be increased

・ The decrease in elastic modulus of the rubber

Page 7: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

The removal of the water for absorption by the pores on surface of porous rubber, as the details of the process was not clearly understood.

The purpose of this study was to clarify the effect of water absorption by the pores in contact area during sliding under wet conditions.

Objective

Page 8: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

1. Introduction and objective

2. Apparatus and methodFriction experiment and conditionObservation methodObservation area

3. Results and discussionsCoefficient of frictionObservation in leading areaObservation in trailing area

4. Conclusions

Table of contents

Page 9: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

FIG. 4 Experimental apparatus:1, weight; 2, rubber specimen; 3, dove prism; 4, parallel leaf spring; 5, strain gauge; 6, prism holder;7, linear guide.

A rotating rubber specimen was rubbed against a mating prism.

➢The friction force was measured by strain gauges were attached to the parallel leaf spring.

➢The friction surface between rubber specimen and dove prism is observed through dove prism.

Friction experiment and experimental condition

Page 10: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

60mm

12.5mm

Pore

Formulation of rubber specimen

Natural rubber filled with carbon black

Pore diameter, mmNo pore, 0.5, 1,

2

TABLE 1 Specification of the rubber specimen

FIG.5 Rubber specimen

Page 11: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Rolling direction

Rubber specimen

Mating prism

Syringe

FIG.6 Cross section of contact surface between the prism and the rubber specimen

Sliding speed v, mm/s

3-30

Normal load, N 14.7

TABLE 2 Experimental condition

Pure water

material calcium carbonate

diameter, m 50-80

TABLE 3 Specification of the fine particles

Page 12: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Observation method

FIG.7 Optical systems for the contact area measurement: 1, rubber specimen; 2, dove prism; 3, CCD camera; 4, light sources.

(a)Total internal reflection method (b) Orthographic method

Page 13: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

To distinguish the contact surface against rubber, water, and air.

To observe and visualize the water flow

FIG.7 Optical systems for the contact area measurement: 1, rubber specimen; 2, dove prism; 3, CCD camera; 4, light sources.

(a)Total internal reflection method (b) Orthographic method

Page 14: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

- The total internal reflection method -

When incident light as passes from a medium of high refractive index n1 to a medium of lower refractive index n2,

2211 sinsin nn ・・・ (1)

θ2Medium 2

FIG. 8 Refraction of light as passes from a medium of high refractive index (n1) to a medium of lower refractive index (n2)

θ1’θ1

n1

n2

Incident light Reflected light

Refraction light

Medium 1

n1 > n2

Page 15: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

θ1’θ1

n1

n2

Incident light Reflected light

- The total internal reflection method -

θ2=90°

1

21sinn

nc

Incident angle is increasing, the reflected angle becomes right angle and the incident light completely reflected.

Now, the incident angle is called the critical angle. Based on Eq. (1), the critical angle c was determined as follow:

・・・ (2)

Medium 1

Medium 2

FIG. 8 Refraction of light as passes from a medium of high refractive index (n1) to a medium of lower refractive index (n2)

n1 > n2

Page 16: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Incident medium Critical angle, °

Rubber 83-90

Water 61

Air 41

TABLE 5 Critical angle as the light passes from the prism

Prism 1.52

Rubber 1.51-1.52

Water 1.33

Air 1.0

TABLE 4 Refractive index

Page 17: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

- The total internal reflection method -

water airrubber

prism

θ1

(a) Cross section

(b) Total internal reflection image

41° < θ1 <61°

FIG. 9 Reflected light and the refracted light at the interface of various refractive indexes

θ1 θ1

Page 18: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

- The total internal reflection method -

water airrubber

prism

(a) Cross section

(b) Total internal reflection image

41° < θ1 <61°

FIG. 9 The reflected light and the refracted light at the interface of various refractive indexes

The differences of intensity of the reflected light allow distinction of contact surface variation

θ1 θ1 θ1

Page 19: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

To distinguish the contact surface against rubber, water, and air.

To observe and visualize the water flow

FIG.7 Optical systems for the contact area measurement: 1, rubber specimen; 2, dove prism; 3, CCD camera; 4, light sources.

(a)Total internal reflection method (b) Orthographic method

Page 20: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

(a) t1 (b) t2

(c) Particles at t2 superimposed on the image at t1

(d) Movement direction of each particles from t1 to t2

- Visualized water flow-

FIG. 10 Principle of the particle tracking velocimetry (PTV)

Page 21: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

(x3. y3)

(x4. y4)(x1. y1)

(x2. y2)

- Visualized water flow-

(a) t1 (b) t2

(x1. y1)

(x3. y3)

(x4. y4)

(c) Movement direction of each particles from t1 to t2

FIG. 11 PTV considered relative displace between pore and particles

Δy

(x2. y2)

Page 22: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

- Visualized water flow-

(a) t1 (b) t2

(x1. y1)(x2. y2)

(x3. y3)

(x4. y4)

(c) Movement direction of each particles from t1 to t2

(d) Superimposed image considering the relative distance between pore and particles

(x3. y3)

(x1. y1) (x2. y2)(x4. y4)

FIG. 11 PTV considered relative displace between pore and particles

(x3. y3)

(x4. y4)(x1. y1)

(x2. y2)

Δy

(x1. y1-Δy) (x2. y2-Δy)

Δy

Page 23: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Rubber specimen

The surface transitioned from noncontact to contact with the mating prism.

The surface of transitioned from contact to noncontact with the mating prism.

Leading area

Trailing area

Mating prism

FIG. 12 Definition of the area of contact

Observation area

Rolling direction

Page 24: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

1. Introduction and objective

2. Apparatus and methodFriction experiment and conditionObservation methodObservation area

3. Results and discussionsCoefficient of frictionObservation in leading areaObservation in trailing area

4. Conclusions

Table of contents

Page 25: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

FIG. 13 Variation in coefficient of friction with the pore diameter under wet conditions

Coefficient of friction

Page 26: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Fig. 12 Variation in coefficient of friction with the pore diameter under wet conditions

Coefficient of friction

The coefficient of friction of the rubber specimen with pores was larger than that of the rubber specimen without pores.

Page 27: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

FIG. 14 Rubber surface of leading area observed by the total internal reflection method

Observation in leading area

Slid

ing

dire

ctio

n of

rub

ber

Page 28: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

FIG. 14 Rubber surface of leading area observed by the total internal reflection method

Observation in leading area

Slid

ing

dire

ctio

n of

rub

ber

2mm

Front edge

Page 29: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

FIG. 14 Rubber surface of leading area observed by the total internal reflection method

Observation in leading area

Slid

ing

dire

ctio

n of

rub

ber

2mm

Rear edge

Page 30: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

air

water

rubber

water and air exist coincide in the pore

The pore contained an air bubble during the sliding.

Observation in leading area

Slid

ing

dire

ctio

n of

rub

ber

Page 31: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

Slid

ing

dire

ctio

n of

rub

berair

water

rubber

The front edge became noncontact with the mating prism.

Observation in leading area

Page 32: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

Slid

ing

dire

ctio

n of

rub

ber

(a) Orthographic images of particles at time t2

(b) Displacement of particles and pore from t1 to t2

FIG. 15 Orthographic image of particles and the flow results of PTV in leading area

(iii) t2=0.6s (iv) t2=0.8s(ii) t2=0.4s(i) t2=0.2s

(iii) From t1=0.4s to t2=0.6s

(ii) From t1=0.2s to t2=0.4s

(i) From t1=0s to t2=0.2s

(iv) From t1=0.6s to t2=0.8s

Observation in leading area

Page 33: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

FIG.16 Superimposed image considering the relative distance between pore and particles

The water did not intrude into the pore when the pore was rubbed.

The water flowing along the edge of pore was observed.

Observation in leading area

Page 34: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

The water flow detouring the pore is due to the air bubble in the pore. The air bubble in the pore pushed aside the water.

The water flowing along the edge of pore was observed.

air

water

rubber

The pore contained the air bubble during the sliding.

2mm

2mm

Observation in leading area

Page 35: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

FIG. 17 Rubber surface of trailing area observed by the total internal reflection method

Observation in trailing area

Slid

ing

dire

ctio

n of

rub

ber

Page 36: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

The air in the pore remained even if the pore left the prism.

Observation in trailing area

Slid

ing

dire

ctio

n of

rub

ber

Page 37: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

2mm

(c) 0.6s (d) 0.8s

(b) 0.4s(a) 0.2s

Slid

ing

dire

ctio

n of

rub

ber

The front edge was not contact with the mating prism as with leading area, and the rear edge of the pore contacted with mating prism even if the pore left the mating prism.

Observation in trailing area

Page 38: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

2mm

Slid

ing

dire

ctio

n of

rub

ber

(a) Orthographic images of particles at the time t2

(b) Displacement of particles and pore from t1 to t2

FIG. 18 Orthographic image of particles and the flow results of PTV in trailing area

(iii) t2=0.6s (iv) t2=0.8s(ii) t2=0.4s(i) t2=0.2s

(iii) from t1=0.4s to t2=0.6s

(ii) from t1=0.2s to t2=0.4s

(i) from t1=0s to t2=0.2s

(iv) from t1=0.6s to t2=0.8s

Observation in trailing area

Page 39: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

FIG. 19 Superimposed image considering the relative distance between pore and particles

The water flowed along the pore edge.

No particles were observed to cross the rear edge.

Observation in trailing area

Page 40: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

The water flowed along the pore edge and didn’t cross the rear edge.

2mm

2m

mThe rear edge of the pore contacted with mating prism even if the pore left the mating prism.

The rear edge of the pore was probably rubbed strongly against the prism and wiped the water.

Observation in trailing area

Page 41: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

1. Introduction and Objective

2. Apparatus and methodFriction experiment and conditionObservation methodObservation area

3. Results and discussionsCoefficient of frictionObservation in leading areaObservation in trailing area

4. Conclusions

Table of Contents

Page 42: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

1. The coefficient of friction of the rubber specimen with pores was larger than that of without pores under wet condition.

2. The pore contained an air bubble during sliding under wet condition.

3. The front edge of the pore was not contact with the mating prism. On the other hand, the rear edge of the pore contacted with mating prism even if the pore left the mating prism.

4. The water flow detouring the air bubble in the pore was also observed.

Conclusions

Page 43: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Thank you for your kind attention

Page 44: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.
Page 45: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

-Observation of contact area (Leading area)-

Page 46: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.
Page 47: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

-Observation of contact area (Trailing area)-

Page 48: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.
Page 49: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

(a) t1 (b) t2

(c) Particles at t2 superimposed on the image at t1

(d) Movement direction   of each particles from t1 to t2

・ Observation method- Visualized water flow-

Page 50: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

・ Observation method- Visualized water flow-

(a) t1 (b) t2

(x1. y1)(x2. y2)

(x3. y3)

(x4. y4)

(c) Movement direction of each particles from t1 to t2

(d) Superimposed image considering the relative distance between pore and particles

Δy

(x3. y3)

(x1. y1) (x2. y2)

(x4. y4)

(x1. y1-Δy)

(x3. y3)

(x2. y2-Δy)

(x4. y4)

FIG. 7 PTV considered relative displace between pore and particles.

Page 51: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Studded Tire

Roughening the ice

Providing better frivtion between the ice and the soft rubber

Increased the road wear by the studs

Characteristics of studded tires

FIG Studded tireUse of studs is regulated in most countries, and even prohibited in some located

Studless tires are designed for use in winter conditions, such as snow and ice

Page 52: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Friction force of Studded Tire

Fig Concept of tread pattern design for snow and ice covered road

Page 53: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Fig Rate of frictional force under various road condition

Page 54: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Rubber friction force

Rubber friction force FF = FH + ( FA + FD)

FH : Hysteresis Friction

Energy loss caused by deformation of tread derived from road roughness

Rubber

Road surface

FA : Adhesion FrictionEnergy loss caused by adhesion between tread and road

Rubber

Road surface

FD : Digging FrictionEnergy loss caused by scratching road surface and wearing of rubber itself

Rubber

Road surface

: Friction improving coefficient developed by displacement of water friction

Page 55: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

Fig. Variation in coefficient of friction with the pore diameter

(b)Aspect ratio AR=1(a)Aspect ratio AR=0.5

Page 56: Yusuke Minami* Tomoaki Iwai**, Yutaka Shoukaku** * Graduate School of Natural Science and Technology Kanazawa University ** College of Science and Engineering.

NR 100ISAF CB 2

ZnO 4Stearic acid 2Antioxidant 2

Oil 3Vulcanization accelerator

1

Sulfur 1.5

Composition of rubber specimen


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