REMEDIAL INVESTIGATION ADDENDUM REPORT

WK Groundwater & Environmental Services, Inc.

A Full Service Environmental Consult ing and Remedial Contracting Company

B 0 0 K 1 OF 2

REMEDIAL INVESTIGATION ADDENDUM REPORT

Fleet National Bank (Formerly White Swan Dry Cleaners)

1322 Sea Girt Avenue

Wall Township (Monmouth County), New Jersey

April 2, 2002

Prepared for: Fleet National Bank

3670 Route 9 South

Freehold, New Jersey 07728

Prepared by: Groundwater & Environmental Services, Inc.

1340 Campus Parkway, P.O. Box 1750

Wall, New Jersey 07719

(732)919-0100

)HN H. MONTGOMER^P.G. /

Project Hydrogeologist (NJDEP Subsurface License No. 11126)

Reviewed by

CAMPBEL:

Project Manager

"An Equal Opportunity Employer"

TABLE OF CONTENTS

Section Page

1.0 INTRODUCTION 1

2.0 HEALTH AND SAFETY 3

3.0 PHYSICAL SETTING 4

3.1 Site Location and Description 4

3.2 Topography and Land Use 5

3.3 Surface Water Bodies 6

3.4 Regional Geology 6

3.5 Site Geology 7

3.6 Site Hydrogeology 8

4.0 BACKGROUND 9

5.0 INVESTIGATE METHODS AND FINDINGS 13

5.1 Local Water Supply 13

5.2 Well Search 13

5.3 Utilities 14

5.4 Geophysical Survey 15

5.5 Soil Boring Activities 16

5.6 Monitoring Welllnstallation 17

5.6.1 Monitoring Well MW3D 17

5.6.2 Monitoring Well MW7 19

5.6.3 Waste Classification 20

5.6.4 Monitoring Well Surveying 22

6.0 EXCAVATION ACTIVITIES 23

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002


TABLE OF CONTENTS (continued)

Section Page

6.1 Technical Approach 23

6.2 Field Screening 23

6.3 Initial Excavation and Exploratory Activities 23

6.3.1 Soil Disposal 24

6.4 Resumption of Excavation Activities 24

6.4.1 General Sampling Protocol 26

6.4.2 Soil Sampling Protocol 27

6.5 Absorption Tank 27

6.5.1 Absorption Tank - Post-excavation Soil Analytical Results 28

6.6 Absorption Tank Piping 28

6.6.1 Absorption Tank Piping - Post-excavation Soil Analytical Results 29

6.7 Original Septic Tank 29

6.7.1 Original Septic Tank - Post-excavation Soil Analytical Results 30

6.8 Soil Disposal 30

6.9 Site Restoration 30

7.0 GROUNDWATER MONITORING AND SAMPLING 32

7.1 January 25, 2002 Groundwater Monitoring and Sampling Event 32

7.1.1 Groundwater Analytical Results 33

8.0 TECHNICAL OVERVIEW 35

8.1 Reliability of Laboratory Data 35

9.0 SUMMARY OF FINDINGS 37

10.0 REFERENCES CITED 40

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Mormiouth County), New Jersey GES Project No. 03-02046/March 2002



Section

12.0 DISCLAIMER,

Page

41

List of Figures

Figure 1. Site Location Map

Figure 2. Site Plan

Figure 3. Local Area Map

Figure 4. Well Location Map

Figure 5. Local Area Map - Monitoring Well Locations

Figure 6. Soil Sample Location Map

Figure 7. Site Information Plan (January 25, 2002)

Figure 8. Local Area Information Plan (January 25, 2002)

List of Tables

Table 1. Well Search Summary

Table 2 Groundwater Monitoring & Sampling Comparison Data

Table 3. Soil Disposal Summary

Table 4. Summary of Volatile Organic Compounds in Post-excavation Soil Samples

Table 5. Summary of Volatile Organic Compounds in Ground Water (January 25, 2002)

List of Appendices

Appendix 1. NJDEP - Bureau of Water Allocation Records

Appendix 2. Advanced Geological Services Results of Geophysical Surveying Letter Report

Appendix 3. Monitoring Well Logs

Appendix 4. Monitoring Well Permit

Appendix 5. Drill Cuttings and Development Water (Waste Manifests and Analytical Reports)

Appendix 6. Monitoring Well Certification Form B

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Monmouth Coimty), New Jersey GES Project No. 03-02046/March 2002



List of Appendices (continued)

Appendix 7. Photographs

Appendix 8. Hazardous Waste Manifests & Transportation Logs

Appendix 9. Certified Clean Fill Documentation

Appendix 10. Laboratory Analytical Report - Soil Samples Collected on December 17, 2001




Appendix 14. GES' Quality Assurance and Quality Control Procedures

Appendix 15. Laboratory Analytical Report - January 25, 2002 Ground Water Sampling Event

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002 iv


ABBREVIATIONS AND SYMBOLS

AGS Advanced Geological Services

APV Allstate Power Vac

BEMQA Bureau of Environmental Management and Quality Assurance

bgs below grade surface

B WA Bureau of Water Allocation (NJDEP)

°C degrees Celsius

CFR Code of federal regulations

DCE dichloroethene

DNAPL dense non-aqueous phase liquid

et seq. and the following

FID flame ionization detector

FNB Fleet National Bank

GES Groundwater & Environmental Services, Inc.

gpm gallons per minute

GPR ground penetrating radar

GWQS ground water quality standards

HASP health and safety plan

HCl hydrochloric acid

kg kilogram

L liter

LEG Lewis Environmental Group

MCHD Monmouth County Health Department

MCL maximum contaminant level

MDL method detection limit

mg milligram

mL milliliter

MOA Memorandum of Agreement



ABBREVIATIONS AND SYMBOLS (continued)

MTBE methyl tert-hutyl ether

MW monitoring well

ND non-detect

NJAC New Jersey Administrative Code

NJDEP New Jersey Department of Environmental Protection

NJDHSS New Jersey Department of Health and Senior Services

NJWSA New Jersey Water Supply Authority

OVA organic vapor analyzer

P piping

PA/SI preliminary assessment and site investigation

PCE perchloroethylene (tetrachloroethene)

pH -logarithmic hydrogen ion activity (concentration)

PID photoionization detector

ppb parts per billion

ppm parts per million

PVC polyvinyl chloride

RCRA Resource Conservation Recovery Act

RIAR Remedial Investigation Addendum Report

SE soil excavation

SIR Site Investigation Report

TBA tert-hutyl alcohol

TCE trichloroethene

TCLP toxic characteristic leaching procedure

TDEM time-domain electromagnetic

TICs tentatively identified compounds

ug microgram

USEPA United States Environmental Protection Agency

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Tovmship, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002 IV


ABBREVIATIONS AND SYMBOLS (continued)

USGS United States Geological Survey

VOC volatile organic compound



1.0 INTRODUCTION

Groundwater & Environmental Services, Inc. (GES), New Jersey Department of Environmental

Protection (NJDEP) certification number 0100139, was retained by Fleet National Bank (FNB),

formerly Summit Bank, to continue the environmental investigation at 1322 Sea Girt Avenue,

Wall Township, Monmouth County, New Jersey (hereafter referred to as "subject property").

After confirming the existence of a seepage tank system at the rear of the subject property, GES

observed and documented the dismantling and removal of this structure and collected soil

samples for laboratory analysis. The subject property is depicted on the United States Geological

Survey (USGS) 7.5-minute Asbury Park, New Jersey quadrangle map (Figure 1). A Site Plan

showing relevant features is provided as Figure 2.

A GES Project Hydrogeologist-NJDEP certified subsurface evaluator (License number 0011126)

supervised, observed, and documented the excavation activities and collected post-excavation

soil samples. All excavation and sampling activities were conducted in accordance with NJDEP

Technical Requirements for Site Remediation [New Jersey Administrative Code (NJAC) 7:26E et

seq.] and the May 1992 NJDEP Field Sampling Procedures Manual. Excavation activities were

completed by Lewis Environmental Group (LEG) of Royerstown, Pennsylvania.

The environmental investigation included the preparation of this Remedial Investigation

Addendum Report (RIAR). This RIAR is based on information obtained during GES' remedial

investigation and remedial actions which were conducted in accordance with NJAC 7:26E.

Activities conducted after the Septic Tank Excavation and Groundwater Report was submitted to

the NJDEP include the following:

• Performance of a geophysical subsurface survey of the subject property to locate, delineate,

and plot any anomalies (e.g. backfilled areas, voids, metal objects, tanks, etc.) which may be

indicative of a former septic tank system alleged to be present by the NJDEP;

• Investigate anomalies identified by geophysical survey by excavating these areas;



Disposal of approximately 820 tons of soil on hazardous waste manifests and approximately

1,800 pounds of soil on non-hazardous waste manifests

Collection of 17 post-remedial soil samples for laboratory analysis;

Installation and development of one deep groundwater monitoring well (MW3D) on-site;

Installation and development of one shallow groundwater monitoring well (MW7) off-site;

Survey MW3D and MW7 for location and elevation;

One complete round of groundwater monitoring and sampling at all eight monitoring wells;

Completion of a well search utilizing NJDEP records; and

Preparation of this RIAR, including but not limited to, information obtained from the

aforementioned bulleted activities.



2.0 HEALTH AND SAFETY

Pursuant to GES policies and procedures and NJAC 7:26E-1.9, a site-specific Health and Safety

Plan (HASP) was prepared for all GES personnel involved in field investigative activities. The

HASP is available upon written request. The HASP outlines the required air monitoring

equipment, protective clothing, chemical action levels, chemical exposure limits, anticipated

contaminants, site control, and emergency procedures employed at the subject property. All field

activities were conducted in level "D" protection. Air monitoring of the breathing zone was

conducted using a portable, hand-held, calibrated photoionization detector (PED) or organic vapor

analyzer (OVA) equipped with a 10.2-electron volt lamp. All GES field personnel are trained

and certified according to the United States Department of Labor's, Federal Occupational Safety

and Health Administration's Safety and Health Standards pursuant to 29 Code of Federal

Regulations (CFR) 1910 and 1926 (1989).



3.0 PHYSICAL SETTING

3.1 Site Location and Description

The subject property is at 1322 Sea Girt Avenue in the Blansingburg section of Wall Township,

Monmouth County, New Jersey. The subject property is in an area of the township zoned for

commercial use. According to township tax records, the subject property is designated as Block

706, Lot 2. The property is trapezoidal in shape and occupies approximately 0.47-acres or

20,600 feetl

The subject property is depicted on the United States Geological Survey (USGS) 7.5-minute

Asbury Park, New Jersey quadrangle map (Figure 1). This figure shows the subject property,

local topography, surface water drainage patterns, and other topographic features. The subject

property is located at approximately 40° 08' North latitude and 74° 03' West longitude.

Site features include a single story masonry building currently occupied by a bank branch

containing an office, private restrooms, and customer service area. The subject property is paved

with asphalt, with the exception of the areas bordering the property boundary and adjacent to Sea

Girt Avenue.

The subject property is currently serviced by township drinking water and sanitary sewer service.

The subject property utilizes natural gas to fuel the heating system. Overhead electricic lines and

subsurface telephone line(s) access the subject property from Sea Girt Avenue. The nearest

storm water catch basin is downslope of the subject property approximately 800 feet southeast on

Sea Girt Avenue. There are no known underground storage tanks at the property. A scaled Site

Plan depicting the property boundaries, on-site utilities, and other site features is included as

Figure 2.

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Tovmship, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002


As reported in GES' December 22, 2000 Site Investigation Report (SIR), previously submitted to

the NJDEP, a scaled proposed site plan was prepared on behalf of Ocean County National Bank

by Walter J. Partington, Inc., a licensed land surveyor from Spring Lake Heights and Point

Pleasant Beach, New Jersey on or about September 27, 1983. A portion of this site plan is

provided in Appendix 10 of the SIR. Although this site plan is not an as-built drawing, it does

replicate most of the features as they exist today. Current structures and features existing on the

subject property as shown on the site plan include: the one-story masonry building, parking

spaces (designated P.S.) in iront and rear of the building, property curbs, grassy island, traffic

flow patterns, vegetation (shrubbery, trees, grass), location of the air conditioning units

(designated "a.c"), concrete (designated "cone") pad and walkway. It should be noted that two

features, designated "S.T." and "S.P." on the site plan, are shown at the rear of the building.

Both abbreviations are not defined or described on the site plan. Because the subject property

utilized a septic tank, prior to hooking-up to the sanitary sewer system on or about October 1985,

it is likely the abbreviation "S.T." refers to the location of the septic tank. GES is not aware of

any documentation regarding construction details of the septic tank, particularly the presence and

location(s) of the leach field, laterals, etc. Because this information is unknown, it is reasonable

to suggest the abbreviation "S.P." on the site plan refers to a seepage pit. The presence of the

septic tank and seepage pit were confirmed during excavation activities conducted on-site.

Results of excavation activities are described in GES' Septic Tank Excavation & Groundwater

Sampling Report which was submitted to the NJDEP on August 9, 2001.

3.2 Topography and Land Use

According to the USGS 7.5-minute (Asbury Park, New Jersey) quadrangle map, the subject

property elevation is approximately 50 feet above mean sea level. The property is surrounded by

a variety of commercial and business establishments. The subject property is bordered by Sea

Girt Avenue towards the southwest, a retail Gulf service station towards the west-northwest, a

hotel towards the north-northeast, and a Cumberland Farms convenience store towards east-



southeast. A Local Area Map showing the subject property and surrounding properties is

presented as Figure 3.

3.3 Surface Water Bodies

According to NJAC 7:9B-1.15 (Surface Water Quality Standards), the subject property is within

the Manasquan River Watershed System. The nearest surface water body is Judas Creek

approximately 700 feet south of the subject property (Figure 1). Judas Creek flows toward the

southeast about 6,000 feet before it discharges to Stockton Lake. According to the New Jersey

Surface Water Quality Standards (NJAC 7:9B et seq.), Judas Creek is classified as FW2-NT/SE1

(fi-eshwater, non-trout producing surface water body). Additional surface water bodies within a

one-mile radius of the subject property include Haimabrand Brook 1,900 feet to the north and

Wreck Pond Brook which discharges to Old Mill Pond 3,700 feet to the northeast. Designated

uses of these waters include the following: swimming, secondary-contact recreation, maintenance

and propagation of natural biota, industrial and agricultural water supply, public water supply

following treatment, shellfish harvesting, and other reasonable uses. All the surface water bodies

eventually discharge into the Atlantic Ocean towards the east.

3.4 Regional Geology

The site is located within the outer fiinge of the Atlantic Coastal Plain Physiographic Province, of

New Jersey, approximately 18 miles south of Raritan Bay. This province is characterized by a

wedge-shaped mass of unconsohdated to semi-consolidated marine, marginal marine, and non-

marine deposits of clay, silt, sand, and gravel. These sediments range in age fi-om Cretaceous to

Holocene and lie unconformably on pre-Cretaceous bedrock consisting of metamorphic schists and

gneiss, with local occurrences of basalts, sandstone and shale (Zapecza, 1984). These sediments

trend northeast-southwest and dip southeast toward the Atlantic Ocean. These sediments thicken

southeastward fi-om the Piedmont-Coastal Plain Province boundary to approximately 4,500 feet

near Atlantic City, New Jersey. During the Cretaceous and Tertiary time period, sediments were

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Mormiouth County), New Jersey GES Project No. 03-02046/March 2002


deposited alternately in flood plains and in marine environments during sea transgression and sea

regression periods.

According to Zapecza (1984) and the New Jersey Geological Survey (Geologic Overlay for

Topographic Atlas Sheet Number 29), the Tertiary-aged Kirkwood and Cohansey Formations,

respectively outcrop in the area of the site. The lithology of the Kirkwood Formation is variable.

Along the coast, thick clay beds are dominant with interbedded zones or lenses of sand and gravel.

Updip fi-om the coast (towards then west), the Kirkwood is characterized by white to orange-brown

to gray, fine to medium sand and silty sand. Regionally, thick clay beds occur only in the basal part

of the formation.

Overlying the Kirkwood Formation is the Cohansey Formation. The lithology of the Cohansey

Formation is similar to the Kirkwood Formation. Because both formations are similar in lithology,

it may not be possible to distinguish them apart. Generally, the Cohansey Formation is coarser-

grained than the Kirkwood Formation. It is predominantly a light-colored quartz sand containing

minor amounts of pebbly sand, fine to coarse-grained sand, silty and clayey sand, and interbedded

clay (Rhodehamel, 1973). Thick clay beds may be present in localized areas.

It is estimated the contact between Kirkwood and Cohansey Formations in the area of the subject

property is approximately 20 feet below grade (Zapecza, 1984, Plate 23).

3.5 Site Geology

Based on soil borings logged by a GES Hydrogeologist, site geology, to an approximate depth of

60 feet below grade surface (bgs), is composed of unconsolidated orange to orange-brown to

brown medium to fine quartz sand with varying amounts of well sorted gravels and pebbles with

minor amounts of silts and clays. Bedrock was not encountered during the investigation,

however, a confining unit (grayish-black silty clay) was identified approximately 62 feet bgs on-

site. According to the Sugarman and Owens (1994), this basal clay layer separates the overlying

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Mormiouth Coimty), New Jersey GES Project No. 03-02046/March 2002


Kirkwood Formation from the underlying Shark River Formation. Based on their data, GES

estimates this clay layer is approximately 55 feet in thickness.

Two geologic formations were interpreted at the subject property. Based on lithology

encountered during previous soil borings and monitoring well installation, the Cohansey

Formation outcrops at the subject property, is approximately 25 feet thick, and overlies the

Kirkwood Formation. According to various reports prepared by the New Jersey Geological

Survey, the Kirkwood Formation overlies the Shark River, Wenonah and Mt. Laurel Sand,

Englishtown Formation, and the Raritan-Magothy Formation.

3.6 Site Hydrogeology

Groundwater recharge to this area is primarily from precipitation infiltrating uncapped or

exposed areas (outcrops). Nearby surface water bodies, such as Judas Creek to the east and

Hannabrand Brook to the north, may rise and fall throughout the seasons. If surface water levels

are below ground water table levels, ground water may discharge to the surface water body.

Conversely, if the surface water levels are above the water table, surface water may recharge the

water table. Groundwater at the subject property occurs under unconfmed (water table)

conditions.

The permeability of the shallow water-bearing zone, based on subsurface lithology and field

observations during monitoring well purging activities, is moderate. This appears consistent with

the reported hydraulic conductivity of 102.23 feet per day for the Kirkwood-Cohansey Aquifer

system.

In this area, ground water is classified as Class-II-A. According to NJAC 7:9-6.5(e)l, "The

promaru designated use for Class H-A ground water shall be potable water and conversion

(through conventional water supply treatment, mixing or other similar technique) to potable

water. Class H-A secondary uses include agricultural water and industrial water.



4.0 BACKGROUND

On August 4, 1997, the Monmouth County Health Department (MCHD) was notified by a

township resident of Magnolia Avenue, two blocks northeast of Sea Girt Avenue, that ground

water samples obtained in 1990 from neighborhood irrigation wells contained the solvent PCE at

concentrations up to 1,546 parts per billion (ppb).

On August 15, 1997, MCHD collected ground water samples from five irrigation wells,

including the well containing 1,546 ppb PCE. The MCHD discovered four of the five irrigation

wells contained PCE above the United States Environmental Protection Agency (USEPA)

Maximum Contaminant Level (MCL) for drinking water of 1 ppb. The highest concentration of

PCE detected was 595 ppb. The MCHD also reported lower concentrations of TCE - a

biodegradation product of PCE - that exceeded its MCL of 1 ppb and methyl tertiary-hutyl ether

(MTBE) - a gasoline additive - that did not exceed its MCL of 70 ppb. The MCHD notified the

residents whom wells were sampled and the NJDEP hotline. The MCHD consulted with the

USEPA, NJDEP, and the New Jersey Department of Health and Senior Services (NJDHSS).

According to the MCHD, the USEPA provided a map based on their groundwater modeling for

the Waldick Aerospace Superfund site. Route 35 in the township, north of Magnolia Lane. Their

documentation from their modeling and their monitoring well sampling data indicates the

groundwater plume from Waldick is impacting the Kirkwood-Cohansey aquifer system in the

Magnolia Lane area. The Kirkwood-Cohansey is the water table aquifer for this area and is about

120 feet deep. During their investigation of the Waldick site, they found no indication of any

illegal off-site waste dumping from the Waldick site in the Magnolia area either on the ground or

into septic systems.

The MCHD reported this area is serviced by municipal water and only irrigation wells were

effected. Therefore, this case did not meet the NJDEP's criteria for an Immediate Environmental

Concern. Therefore, funding from the New Jersey Spill Act would not be available for installing

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Moimiouth County), New Jersey GES Project No. 03-02046/March 2002


monitoring wells and remediation (unlike irrigation wells, monitoring wells are accessible year

round for sampling). The NJDHSS advised the MCHD that although the PCE exceeded the

drinking water standard of 1 ppb, their risk assessment literature indicated that groundwater with

levels found here could still be used for lawns and gardens but could not be used for drinking.

In November 1998, the MCHD collected ground water samples from 28 additional irrigation

wells. The MCHD reported the contaminant plume containing various volatile organic

compounds (VOCs) was delineated north at Chicago Avenue to south of Sea Girt Avenue to

Macs Pond Brook, and from Route 35 east to Route 71. Ground water analytical results revealed

VOC concentrations ranging from non-detect (ND) to 1,068 ppb for PCE. Additional VOCs and

their respective concentrations ranges included TCE (ND to 6.4 ppb), ci5-l,2-dichloroethene

[(cis-DCE), ND to 10.5 ppb], halogenated methanes (ND to 44.9 ppb), xylenes (ND to 5.9 ppb),

and MTBE (ND to 12 ppb).

In 1999, the NJDEP - Bureau of Environmental Mangagement and Quality Assurance (BEMQA)

and MCHD began a joint study to determine the extent of PCE in ground water in Wall

Township and the neigboring boroughs of Manasquan and Sea Girt. Moreover, the study was

completed to evaluate the risk to Sea Girt's municipal supply wells. The ground water study

included sampling additional irrigation wells, sampling surface water at Wreck Pond in Sea Girt

and Spring Lake Heights, and monthly sampling of Sea Girt's municipal wells. According to the

NJDEP, a contamination plume extends from Wall Township into Manasquan and Sea Girt

boroughs. No contamination was detected in Sea Girt's municipal wells indicating these wells

withdraw water from a deeper aquifer not affected by the contamination. However, some PCE

was detected in water samples collected from Wreck Pond. Currently, the NJDEP is conducting

a preliminary assessment and site investigation (PA/SI) to identify the source(s) of ground water

contamination. The NJDEP is expected to complete the PA/SI and report its findings in a report

this year.

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Mormiouth County), New Jersey GES Project No. 03-02046/March 2002 10


As discussed previously, the NJDEP - BEMQA conducted an investigation at the subject

property from September 30, 1999 to January 31, 2000. A copy of the June 6, 2000 report

containing analytical results and approximate sample locations was included in GES' Site

Investigation Report dated December 22, 2000.

On June 6, 2000, the NJDEP forwarded analytical results of ground water, soil, and soil gas

samples collected from the subject property. The NJDEP stated the sample results indicate a

source of tetrachloroethene (also known as perchloroethylene or PCE) and trichloroethene (TCE)

originating from the subject property, formerly known as White Swan Cleaning & Laundry, Inc.

An environmental investigation by GES was initiated in response to the NJDEP's findings. Site

investigative activities, conducted from August 2000 through November 2000, included but was

not limited to, the following:

• Review of federal, county, and local government agency environmental records;

• Collection of soil samples for laboratory analysis;

• Installation and development of six (MWl through MW6) , 4-inch diameter monitoring wells

• Installation and development of four, 1-inch diameter, temporary monitoring well points

• Survey of monitoring wells to a reference elevation;

• Collection of groundwater samples for laboratory analysis; and

• Preparation of a Site Investigation Report.

In February 2001, GES confirmed the existence of one settling (septic) tank and one seepage pit

identified during the initial site investigation. In addition, groundwater samples collected from

on-site monitoring wells identified the presence of chlorinated hydrocarbon concentrations above

the NJDEP Ground Water Quality Standards (GWQS). As a result, Summit GES continued the

environmental investigation at the subject property. Investigative activities conducted from

February 2001 through June 2001 included, but were not limited to, completion of the following:



• Pump out liquid from settling tank and dispose on hazardous waste manifest;

• Dismantling settling tank and seepage pit;

• Collect test pit soil samples and post-excavation soil samples near the septic tank and settling

tank;

• Disposal of approximately 20 tons of soil on hazardous waste manifests;

• Collection of post-excavation soil samples for laboratory analysis;

• One round of groundwater monitoring and sampling; and

• Preparation of a Remedial Investigation Report.

On February 28, 2001, FNB and NJDEP entered into a Memorandum of Agreement (MOA)

under the NJDEP Voluntary Cleanup Program for remedial activities at the subject property. In

NJDEP correspondence dated January 9, 2002, oversight of the case was fransferred to the

USEPA - Region 2. Therefore, the MOA between the NJDEP and FNB was terminated on this

date. FNB was instructed to forward all future correspondence and documents to the USEPA.

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002 12


5.0 INVESTIGATIVE METHODS AND FINDINGS

5.1 Local Water Supply

According to the NJDEP's 1991-92 Annual Fee Report and Assessment of Fees (1992), 7.6% of

township residents utilize domestic wells as a source of the water supply (NJDEP, 1990). The

percentage of township residents reliant on domestic wells as a source of potable water was

based on 1980 census data.

Municipal water is supplied by Wall Township Municipal Utilities Authority from eight wells.

In addition, the township purchases water from the New Jersey Water Supply Authority

(NJWSA). The township's wells are between 460 and 730 feet deep and withdrawal water from

the Mount Laurel and Englishtown aquifers. Water from the NJWSA is drawn from the 3+

billion gallon Manasquan Reservoir in Howell Township and treated at the NJWSA facility on

Hospital Road in the township. In addition, the Manasquan Water Treatment Plant now provides

60% of the potable water consumed by the communities of Brielle, Sea Girt, Spring Lake, Spring

Lake Heights, and Wall Township.

5.2 Well Search

In correspondence dated October 23, 2001, the NJDEP required FNB to provide a detailed map

showing all municipal supply wells within a 2-mile radius of the subject property. The NJDEP

also required the location, depth, pumping rate and status of each well.

On December 13, 2001, GES submitted a written request to the NJDEP, Bureau of Water

Allocation (BWA) to complete a search of all available municipal public supply wells within a 5-

mile radius of the subject property. Additionally, GES requested a manual search of NJDEP well

records for all permitted wells within a one mile radius of the subject property. The NJDEP

completed the requested well search on January 26, 2002.

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Tovmship, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002 13


According to NJDEP-BWA well records, two public supply wells are within a one-mile radius of

the site. One public supply well is in Manasquan near Mac's Pond. This well is approximately

3,200 feet south-southeast of the subject property and has a reported depth and pumping rate of

114 feet and 150 gallons per minute (gpm), respectively. The second pubhc supply well is

owned by Richard BahadurianAâlley Park. This well is approximately 4,200 feet north-

northeast of the subject property and has a reported depth of 100 feet and a pumping rate of 22

gpm.

Five domestic wells, two domestic or irrigation wells, three industrial wells, 31 irrigation wells,

and 17 monitoring wells are within a one mile radius of the subject property. It is not known if

the seven domestic wells are utilized for drinking or for irrigation use. A summary of well

information according to NJDEP-BWA file records is presented on Table 1. Wells with

confirmable addresses within a one-half mile radius of the subject property are presented on

Figure 4. Copies of NJDEP-BWA well records and computerized data base search are provided

as Appendix 1.

5.3 Utilities

At least three but no more than 10 business days (excluding holidays) prior to initiating

excavation and drilling activities described in this report, subsurface utility clearances were

obtained by LEG and GES in accordance with the Underground Facility Protection Act (NJSA

48:2-73 et seq.). Public and private utility companies servicing the area were contacted through

the New Jersey One Call toll free number (1-800-272-1000) to provide (mark out) utility line

locations. The township of Wall (water, sanitary sewer, storm sewer), Cablevision (cable

television). Sprint (telephone), MCI World Communication (telephone), Verizon (telephone).

New Jersey-American Water Company (public drinking water). New Jersey Natural Gas (natural

gas), and General Public Utilitity Energy (electric) were notified prior to excavation activities at

the subject property. Where necessary, underground utilities were field verified by GES

personnel for all sampling locations.



The subject property is currently serviced by township drinking water and sanitary sewer service.

The subject property utilizes natural gas to fuel the heating system. Overhead electric lines and

subsurface telephone line(s), water line, and sanitary sewer line access the subject property from

Sea Girt Avenue. No storm drains were observed on the property nor in the immediate vicinity

of the subject property on Sea Girt Avenue. Storm water runoff is collected via storm sewer

inlets towards the southeast on Sea Girt Avenue. A scaled Site Plan depicting the property

boundaries, on-site utilities, and other site features is included as Figure 2.

5.4 Geophysical Survey

GES contracted Advanced Geological Services (AGS) of Malvern, Pennsylvania to perform a

geophysical subsurface survey of the entire subject property. AGS utilized time-domain

electromagnetic (TDEM) and digital ground penetrating radar (GPR) to locate, delineate, and

plot any anomalies (e.g. backfilled areas, voids, metal objects, tanks, etc.) which may be

indicative of a former septic tank or dry well system reportedly on-site when White Swan Dry

Cleaners owned and operated the subject property. The geophysical survey was completed on

November 12, 2001.

Results of the geophysical survey are presented in AGS' Results of Geophysical Surveying letter

report dated November 28, 2001 (Appendix 2). As noted in the AGS' report, a "linear anomaly

was identified near the northeast comer of the building. The anomaly characteristics suggest the

presence of a previously unidentified utility. Further investigation of this anomaly was

performed using GPR. These data corroborate the EM61 data interpretation by indicating the

presence of a laterally continuous hyperbolic anomaly, which is characteristic of buried utilities.

This interpreted anomaly utility extends from the building and ends at the northeast comer of the

property."

AGS reported that "GPR data acquired in the northeast comer of the property exhibited chaotic

reflection events that suggest the presence of disturbed subsurface conditions. In addition.



numerous diffractions and complex anomaly configurations were observed that suggest the

presence of non-native structures or objects. Signal penetration through the suspected stmcture

was observed, which indicates the stmcture is non-metallic, since GPR signals cannot penefrate

metal. The approximate extent of the feature was delineated spray painted in the field." This

interpreted location is presented in Figure 1 of Appendix 2.

AGS also reported "to definitively identify the suspected structure based on solely on the

geophysical data, its location with respect to the detected utility interpreted in conjunction with

historical information indicate that this is a likely location for the suspected former septic

system."

5.5 Soil Boring Activities

As noted in GES' Septic Tank Excavation and Groundwater Sampling Report dated August 9, 2001,

FNB proposed to continue the remedial investigation by advancing a deep soil boring near MW3 to

determine the distribution of hydrostratigraphic units including any impermeable strata (i.e., clay

layer) beneath the site. According to the New Jersey Geological Survey, an impermeable,

contiguous clay layer was identified within one mile of the subject property at an approximate

elevation of-10 feet below mean sea level. Therefore, it is estimated this clay layer may be present

55 feet bgs at the subject property.

The soil boring would be installed near existing monitoring well MW3, which has contained the

highest dissolved-phase concenfration of total VOCs (Table 2). The soil boring would be

completed as a monitoring well but at a deeper screened interval than that of MW3 to determine if

VOCs of concern {i.e. PCE, cw-DCE, TCE, benzene, and MTBE) are present in deeper

groundwater at concenfrations exceeding the apphcable NJDEP GWQS. The well would be

installed to a depth corresponding to the depth of the top of the clay layer or semi-impermeable

layer during the advancement of the deep soil boring. This interval was selected to determine if

DNAPL is present. If the impermeable layer was identified during the soil boring, the bottom 10



feet of the monitoring well would be constracted using 10 feet of factory-slotted screen. Above

this interval, the monitoring well would be extended to near grade using solid PVC casing.

Constraction details for monitoring well MW3D are described in the following section.

On November 16, 2001, a soil boring was advanced on-site under the direction of a GES Project

Hydrogeologist. Representatives from the NJDEP (Mr. Tim Maguire and Ms. Karen Kloo) were

also on-site to observe and document subsurface conditions. The borehole was advanced with a

hollow-stem auger drill rig by Shore Drilling of Oceanport, New Jersey (New Jersey License Driller

No. 1275). Continuous soil samples were obtained via a split-spoon sampler at 2-foot intervals.

All samples were screened with a calibrated PID for the presence of VOCs. Continuous split-spoon

samples were collected beginning at 20 feet bgs. The lithology of this borehole was expected to be

identical to the lithology encountered during the installation of MW3 less than 3.0 feet away.

The general lithology of the borehole is consistent with previously completed boreholes on-site, i.e.,

very coarse to fine sand with varying amounts of gravel, silt, clay and iron mottling. PID readings

ranged from 0 to 613 ppm units. The highest PID readings were observed from 22.5 to 31.5 feet

bgs. A geologic log of all subsurface material encountered during soil boring advancement was

prepared and is included in Appendix 3. Descriptions of the subsurface material encountered

include color, grain size, stmcture or stratification, PID screening results and any other

observations. All samples were screened with a calibrated PID for the presence of VOCs.

5.6 Monitoring Well Installation

5.6.1 Monitoring Well MW3D

The borehole advanced on November 16, 2001 (as described in previous section) was completed

as a deep monitoring and is designated MW3D. The location of monitoring well MW3D was

selected based on suspected and known area(s) of concem (i.e., the highest dissolved-phase

concenfration of PCE at MW3S), site topography, anticipated groundwater flow direction, drill



rig access, and location of underground and overhead utilities. The appropriate well screen

length was pre-determined through discussion with NJDEP representatives. The monitoring well

was constmcted using 10.0 feet of 4-inch diameter. Schedule 40, threaded PVC slotted screen

(0.010-inch) and 50.75 feet sohd PVC casing. A No. 1 unground silica sand was used to fill the

borehole annulus. As the level of the sand pack rose, the auger was gradually removed and the

sand pack was emplaced to approximately 2.0 feet above the top of the screen. Bentonite pellets

were placed directly onto the sand using a tremie pipe to a thickness of approximately 2.0 feet. A

cement-bentonite slurry was prepared using potable water supplied by the well driller. The

cement-bentonite slurry, used as a grout seal, was tremied on top of the bentonite seal to a level

of approximately 1.0 foot bgs. The monitoring well was completed with a lockable watertight

gripper plug placed on top of the casing and secured with a padlock. A flush-mounted steel

manhole was placed over the top of the monitoring well casing and grouted into place within a 2-

foot by 2-foot concrete pad to approximately 2 inches bgs. The pad was completed to grade

using asphalt. The manhole cover was secured with bolts. The locking gripper plug prevents

water infilfration and unauthorized access to the monitoring well.

Prior to installation procedures, a soil boring was advanced and continuous split-spoon samples

were obtained at 2-foot intervals begiiming at 30 feet bgs. The split-spoon barrel was opened and

immediately scanned with a calibrated PID for the presence of organic compounds. PID readings

provide an indication of ionizable compounds that may be present, but the results are neither

qualitative nor quantitative. The observed PED readings ranged from 0 to 613 parts per million

(ppm) units. After scanning each split-spoon with the PID, the amount of recovery and lithology

encountered was recorded in a field notebook.

The monitoring well was developed using a submersible pump and dedicated tubing to remove

sediment from the well bore and filter pack, thus optimizing well yield and the procurement of

representative ground water samples. The well was developed until a turbid-free discharge was

observed. Development was completed after pumping the well for approximately 15 minutes at



an estimated flow rate of 2 gallons per minute. The development water was freated with granular

activated carbon and discharged onto an unpaved area near the well on-site.

A monitoring well log describing the lithology encountered, observed PID readings, well

constmction details, and other information are included in Appendix 3. Monitoring Well Permit

is included in Appendix 4.

5.6.2 Monitoring Well MW7

On January 11, 2002, one monitoring well (MW7) was installed off-site by GES' Probe Services

Division (New Jersey Driller License Number JD1610). This monitoring well was installed

hydraulically downgradient of the site on Begonia Avenue, approximately 40 feet from Laurel

Avenue (Figure 5). The purpose of installing this monitoring well is to delineate the extent of

VOCs of concem in the shallow water-bearing zone. The monitoring well was installed under

the direct supervision of a GES Project Hydrogeologist and NJDEP Certified Subsurface

Evaluator (License number 11126).

The location of monitoring well MW7 was based on NJDEP's recommendation. The appropriate

well screen length was field determined based on stratigraphic and hydrogeologic data collected

during monitoring well installation. Monitoring well MW7 was constmcted using 20.0 feet of 4-

inch diameter. Schedule 40, threaded PVC slotted screen (0.010-inch) and 10.0 feet solid PVC

casing. A No. 1 unground silica sand was used to fill the borehole annulus. As the level of the

sand pack rose, the auger was gradually removed, and the sand pack was emplaced to

approximately 2.0 feet above the top of the screen. Bentonite powder seal (slurry) was placed

directly onto the sand using a tremie pipe to a thickness of approximately 2.0 feet. A cement-

bentonite slurry was prepared using potable water supplied by the well driller. The cement-

bentonite slurry, used as a grout seal, was tremied on top of the bentonite seal to a level of

approximately 1.0 foot bgs. The monitoring well was completed with a lockable watertight

gripper plug placed on top of the casing and secured with a padlock. A flush-mounted steel



manhole was placed over the top of the monitoring well casing and grouted into place within a 2-

foot by 2-foot concrete pad. The manhole cover was secured with bolts. The locking gripper

plug prevents water infiltration and unauthorized access to the monitoring well.

Prior to monitoring well installation procedures, a soil boring using the hollow stem auger

method was completed. Soil samples from drill cuttings were obtained for headspace analysis.

The soil samples were placed in dedicated, clean, amber glass jars, covered with aluminum foil,

secured with a screw top lid and allowed to equilibrate undisturbed for at least 20 minutes.

(Screening the drill cuttings as they arose to the surface was not possible due to light to heavy

rain). PID readings provide an indication of ionizable compounds that may be present, but the

results are neither qualitative nor quantitative. The observed PID readings were less than or

equal to the ambient air concentration of 0.5 ppm units.

The monitoring well was developed using a submersible pump and dedicated tubing to remove

sediment from the well bore and filter pack, thus optimizing well yield and the procurement of

representative ground water samples. The well was developed until a turbid-free discharge was

observed. Development was completed after pumping the well for approximately 30 minutes at

an estimated flow rate of 1-2 gallons per minute. Approximately 45 gallons of development

water was stored in a labeled 5 5-gallon steel drum stored on-site for disposal.

A monitoring well log describing the lithology encountered, observed PID readings, well

constmction details, and other information are included in Appendix 3. The Monitoring Well

Permit is included in Appendix 4.

5.6.3 Waste Classification

Soil cuttings generated during the installation of monitoring wells MW3D and MW7 were

containerized in labeled, 55-gallon steel drams for waste classification and proper disposal. On

November 20, 2001 and January 11, 2002, GES collected composite soil samples from drill



cuttings from MW3D and MW7, respectively. The collected soil samples were stored in an

insulated storage cooler at approximately 4 °C (wet ice) and submitted to Integrated Analytical

Laboratories, LLC, of Randolph, New Jersey (NJDEP Certified Laboratory Identification

Number 14651). The soil samples were analyzed for TCLP (Toxicity Characteristic Leaching

Procedure) VOCs and RCRA (Resource Conservation Recovery Act) characteristics (corrosivity

as pH, ignitability @ \A1 °F, reactive cyanide, reactive sulfide). The TCLP extraction and

analysis for VOCs were conducted using USEPA approved test methods 1310 and 8260,

respectively. The USEPA approved test methods used for the determination of RCRA

characteristics were 1020A for ignitability, 9045C for corrosivity, and Sohd Waste Test Method-

846, Chapter 7.3 for reactivity (i.e. reactive cyanide and reactive sulfide). Results of the waste

characterization sample indicate soil cuttings generated from the installation of MW3D and

MW7 were non-hazardous (Appendix 5).

On December 14, 2001, drill cuttings (eight 55-gallon steel dmms) generated from the

installation of monitoring well MW3D were retrieved and transported by Casie Pro-Tank

(USEPA ID NJD045995693) on non-hazardous waste manifest (NHZ0207771) for recycling at

their facility in Vineland, New Jersey.

On Febmary 6, 2002, drill cuttings (four 55-gallon steel dmms) generated from the installation of

monitoring well MW7 were retrieved by Allstate Power-Vac [(APV), USEPA ID

NJD003812047) of Rahway, New Jersey and transported on non-hazardous waste manifest

(APV03936) to Penn Ohio Corporation in Ashtabula, Ohio (USEPA ID OHR000028837) for

disposal In addition, APV retrieved the 55-gallon steel drum containing development water from

MW7 and transported on hazardous waste manifest (NJA3205300) to Cycle Chem, Inc. in

Elizabeth, New Jersey for disposal.

Non-hazardous waste manifest documenting the disposition of drill cuttings and a hazardous

waste manifest documenting the disposal of development water also are included in Appendix 5.



5.6.4 Monitoring Well Surveying

On Febmary 4, 2002, monitoring wells MW3D and MW7 were surveyed for location and

elevation by Flannery, Webb & Hansen, P.A., a New Jersey licensed professional land surveyor.

The monitoring well casings and ground surface elevations were referenced to a New Jersey

Vertical Datum benchmark (AA5233) having an elevation of 69 feet above mean sea level. All

elevations were taken at a black mark on the top of the monitoring well casing. Monitoring well

casing elevations are provided on Tables 1 and 2. Monitoring Well Certification Form B for

both monitoring wells are included in Appendix 6.



6.0 EXCAVATION ACTIVITIES

6.1 Technical Approach

This project involved source removal (absorption tank and septic tank system) for the

remediation of soil contaminated with chlorinated hydrocarbons at FNB. To serve as additional

source removal, contaminated soil was excavated and transported off-site for disposal. Soil

excavation served as an accelerated remedial strategy which focused on suspected source(s) of

contamination and areas where soil contamination are identified.

During the initial site investigation, which was conducted in September and November 2001,

eight soil samples collected from six borings contained PCE concentrations above the NJDEP

most restrictive soil cleanup criterion of 1,000 micrograms per kilogram (ug/kg). The removal

actions involved the excavation and off-site treatment or disposal of contaminated soil.

Effectiveness of the removal actions was documented with post-excavation soil sampling.

6.2 Field Screening

During excavation activities, the subject property was visually inspected for evidence of a

release. An OVA equipped with a calibrated PID was used to measure total organic vapors

present in the excavated soils and personnel breathing zones. Results of field screening was used

as a qualitative indication of the amount of excavation necessary to remove any impacted

(contaminated) soil when field screening indicates organic vapors are at low concentrations (<10

ppm), samples will be collected from the excavation for laboratory analysis.

6.3 Initial Excavation and Exploratory Activities

GES contracted LEG to conduct an excavation at the northeast comer of the property identified

by AGS as an anomaly to confirm the existence of the septic system (Appendix 2). Excavation



activities were initiated on December 11, 2001. During excavation activities, it was discovered

that the 'septic system' was larger than anticipated by AGS. This 'septic system' was a cinder

block-concrete stmcture (hereafter referred to as an absorption tank), consisting of four separate

chambers. An access way discovered near MWl (Appendix 7) was removed and the interior

inspected. The depth to the bottom of the 'septic tank' was approximately 10.75 feet bgs. The

length of the backhoe arm was insufficient to reach the base of the stmcture. Therefore, the

excavation was covered with 5-mil plastic sheeting and secured with fencing to prevent

unauthorized access until a larger backhoe could be procured. Results and findings of excavation

activities that resumed on December 17, 2001 are described in Section 6.4.

6.3.1 Soil Disposal

On December 11, 2001, approximately 33.59 tons of soil was excavated and contained in two

labeled 30 cubic yard rolloffs for transport and proper disposal. The covered rolloffs were staged

on the subject property near monitoring well MW3. The rolloffs were retrieved by Horwirth

Tracks, Inc., of Northampton, Pennsylvania (USEPA ID PAD146714878) and transported to

CWM Chemical Services, LLC (USEPA ID NYD049836679) of Model City, New York for

disposal. Hazardous waste manifests (NYB9492281 and NYB9492282) documenting the

disposition of the excavated soil is included in Appendix 8. A table summarizing soil disposal

activities, including load date, hazardous waste manifest number, weight of each load, firm name

hauling the waste, and the date the waste was disposed, is presented as Table 3. Certified clean

fill (medium sand) was used to backfill the excavation (Appendix 9).

6.4 Resumption of Excavation Activities

On December 17, 2001 excavation of the absorption tank resumed. As noted in Section 5.1, the

cinder block-concrete stracture (absorption tank), consisting of four separate chambers, was

discovered at the northeast comer of the property. The fourth chamber and the fiill extent of the

absorption tank system were discovered on December 20, 2001. All four chambers were



connected in series and separated by cinder block walls. Each chamber measured 7 feet wide, 11

feet in length and 7.75 feet in depth. The absorption tank system had an open (soil) bottom. The

vertical chamber walls were constmcted of pre-cast masonry cinder blocks in a ranning bond

pattern. Each course was set with concrete; however, the vertical joints between each cinder

block were not cemented. The vertical spacing between each cinder block was approximately 1

inch. All four chambers were covered with 3.0 inches of rebar-enforced concrete which was

approximately 3.0 feet bgs. Overall, the absorption tank measured 7 feet wide, 33 feet long, and

7.75 feet deep. The concrete lid contained three rectangular access ways - one for each chamber.

The 2.0 by 2.0-foot access ways were spaced approximately 10.5 feet on center. When the access

way closest to monitoring well MWl was removed, a sweet, chemical-like odor was noted. The

headspace in this chamber registered a PID reading of >2,000 ppm. The depth of the absorption

tank, as measured from surface grade, was 10.75 feet. Using the dimensions of the absorption

tank, the volumetric content is estimated to be 1,790 cubic feet or 13,400 gallons. Photographs

of the inspection port, cinder block walls and other absorption tank features are presented in

Appendix 7.

During excavation activities, a 4-inch inner diameter, cast iron pipe was discovered above and

near the center of the absoption tank system or approximately 30 feet southeast of the

northwestern property boundary. The pipe was approximately 2 feet bgs and extended south

towards the north comer of building (Appendix 7). This pipe was linear, 42 feet in length, and

constmcted in 5-foot sections. The location of this pipe is consistent with the linear anomaly

reported by AGS.

It is likely the absorption tank received direct discharge from the former White Swan Dry

Cleaners as evidenced by the following:

• PID readings of the headspace were above the maximum limit of 2,000 ppb;

• A sweet odor resembling dry cleaning fluid (i.e., PCE) was noted by several on-site

personnel;



• Laboratory analysis of soil samples collected from two soil borings (SB 1 and SB2) and water

samples collected from monitoring well MWl contained detectable concentrations of PCE;

• Vertical walls of the absorption chamber and the open bottom contained lint (fabric) material

likely generated and discharged with liquid during dry cleaning operations; and

• A 4-inch diameter cast iron pipe was connected to the third chamber and contained elevated

PID readings within the pipe and in subsurface soil.

6.4.1 General Sampling Protocol

Applicable protocols regarding sampling, handling, storage, preservation, reporting,

decontamination of field equipment, and other procedures were conducted as outlined in the

NJDEP Field Sampling Procedures Manual dated May 1992. Soil samples were collected using

dedicated, disposable sampling equipment and transferred immediately to the appropriate

laboratory provided containers.

All analyses were conducted by a New Jersey certified laboratory. The laboratory supplied all

sample containers. Following the collection of each soil sample, each container was labeled with

the appropriate identification and immediately placed into a clean, insulated storage cooler. All

storage coolers were stored away from all possible sources of contamination and sample integrity

was ensured through proper preservation via cooling the samples with wet ice until delivery to

the laboratory and by adhering to applicable parameter-specific holding times.

Written documentation and chain of custody procedures were maintained throughout the

sampling program. Each soil sample was assigned a unique sample number, location, date, time,

matrix and requested analyses were recorded in a bound field logbook. Combined chain of

custody and analytical request forms, indicating the sample information and requested analyses,

were completed and submitted with each storage cooler. The chain of custody forms



accompanied the sample shipments from the site to the laboratory to document possession of the

samples.

6.4.2 Soil Sampling Protocol

Soil from each sampling location was collected from the backhoe bucket supplied by LEG. At

each location, soil was visually examined for staining and odors, and screened for volatile

organic compounds using a calibrated PID. Soil sample locations were recorded by a GES

Project Hydrogeologist onto a scaled site map. Soil samples for chemical analysis were collected

using a special, single use, USEPA approved EnCore® sampling device. This sampling device

allows the collection and transport of soil samples for organic analyses to the laboratory without

preserving in the field. The EnCore® sampler is a device made of an inert composite polymer,

designed to collect, store, and deliver soil in a sealed, headspace-free state. In order to collect the

sample, the EnCore® sampler is attached to a reusable T-handle that serves to assist in pushing

the sampler in the soil. An airtight sealing cap is then attached creating a self-contained package.

An additional sample of (unpreserved) soil was collected to allow for a determination of moisture

content, and the normalization of data to a dry-weight basis. The devices and moisture soil

samples are preserved with wet ice in an insulated sample shuttle, transported to the laboratory

where the device cap is opened and the undisturbed soil sample is immediately placed in the

appropriate preservation fluid, methanol or sodium bisulfate. This preservation step must be

completed within 48 hours of sample collection.

6.5 Absorption Tank

After the absorption tank was dismantled, the material and surrounding soil suspected to be

impacted by VOCs, as evidenced by PID readings, were loaded into trailers via a backhoe

provided by LEG. Residual liquid was not observed in the absorption tank.



The approximate final dimensions of the absorption tank excavation were 15 feet wide, 50 feet

long, and ranged in depth from 10.5 at the east end to 21.0 feet deep at its center (Figure 6).

Groundwater was not encountered in the excavation. Soil could not be excavated at a greater

depth because of the nature of the surrounding material and the reach of the backhoe. The

surrounding material was larger in diameter than the surrounding indigenous soil and was not

cohesive. Consequently, any soil removed from the excavation floor was immediately filled with

surrounding material slumping into this area from the sidewalls.

Seven post-remedial soil samples (SEl through SE7) were collected (Figure 6). Soil samples

SEl, SE2, SE5, and SE7 were collected from the excavation floor. The remaining three samples

(SE3, SE4, and SE6) were collected from the excavation sidewalls. Soil sample depths ranged

from 17.0 feet at SE6 and SE7 to 21.0 feet at SE2 (Table 4). The collected soil samples were

stored in an insulated storage cooler maintained at approximately 4 °C (wet ice) and submitted to

Accutest Laboratories of Dayton, New Jersey (NJDEP Certified Laboratory Identification

Number 12129). All samples were analyzed for VOC-MO via USEPA approved test method

8260+10.

6.5.1 Absorption Tank - Post-excavation Soil Analytical Results

No targeted VOCs or TICs were reported by the laboratory in the seven soil samples. A

summary of analytical results, including laboratory reported method detection limits, is presented

in Table 4 and Figure 6. The certified laboratory analytical reports for soil samples collected on

December 17, December 18, December 19, and December 20 are included as Appendices 10, 11,

12, and 13, respectively.

6.6 Absorption Tank Piping

On December 19 and 20, 2001, approximately 40 feet of 4-inch diameter cast iron piping was

excavated and removed. The pipe did not contain any residual liquid. The bottom of the pipe

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Monmouth Coimty), New Jersey GES Project No. 03-02046/March 2002 28


was approximately 2.0 feet bgs and slightly sloped toward the building. Soil beneath the pipe

was excavated until PID readings decreased to approximately 10 ppm units. Five post-remedial

soil samples were collected (PI through P5) beneath the piping (Figure 6). Soil samples were

biased to locations showing the highest PID reading and beneath the piping joints. Samples PI

and P4 were obtained 6.0 feet bgs, respectively. Samples P2 and P3 were obtained 5.0 feet bgs.

Sample P5 was obtained 7.0 feet bgs. The soil samples were stored in an insulated storage cooler

maintained at approximately 4 °C (wet ice) and submitted to Accutest Laboratories, of Dayton,

New Jersey (NJDEP Certified Laboratory Identification Number 12028). All samples were

analyzed for VOC-ÎO via USEPA approved test method 8260+10.

6.6.1 Absorption Tank Piping - Post-excavation Soil Analytical Results

PCE was detected at a concentration of 577 ug/kg in P5. PCE concentrations were 152 ug/kg at

P3 and 118 ug/kg (estimated). No TICs were detected in the soil samples. The concentrations of

PCE reported in these samples are less than the NJDEP's most restrictive soil cleanup criterion of

1,000 ug/kg. A summary of analytical results is presented in Table 4 and Figure 6. The certified

laboratory analytical report is included as Appendices 12 and 13.

6.7 Original Septic Tank

As the excavation of absorption tank proceeded towards the southeast, a cinder block wall was

encountered. The walls were constracted of pre-cast masonry cinder blocks in a ranning bond

pattern. Each course and cinder blocks were set with concrete, i.e., no gaps existed on the

horizontal and vertical joints. The absorption tank was covered similar to the septic tank, i.e., it

was covered with approximately 3.0 inches of rebar enforced concrete which was approximately

3.0 feet bgs. Overall, the septic tank measured 7 feet wide, 20 feet long, and 7.75 feet deep. The

septic tank had an open bottom, i.e., the floor was uncapped. The concrete lid contained one

rectangular access way at the northwest end.. When the 2.0 by 2.0-foot access way was removed,

a faint but discernible sewage-like odor was detected. The depth of the septic tank, as measured

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Township, (Monmouth Coimty), New Jersey GES Project No. 03-02046/March 2002 29


from surface grade, was approximately 8 feet bgs. Using the dimensions of the septic tank, the

volumetric content is estimated to be 1,085 cubic feet or 13,400 gallons.

The approximate dimensions of the excavation were 15 feet wide and 50 feet long. The depth of

the excavation varied from 8.5 feet bgs at SEll to 17 feet bgs at SE8. Groundwater was not

encountered in the excavation. Soil could not be excavated at a greater depth because of the

nature of the surrounding material. The surrounding material was larger in diameter than the

indigenous soil and was not cohesive. Consequently, when the backfilled material was removed

from the excavation floor, the area was immediately filled with identical material slumping from

the sidewalls.

The septic tank was dismantled in situ, excavated and placed onto trailers for disposal. Soil on

each side of the rectangular septic tank and the bottom was excavated. The backfilled material

surrounding the septic tank was comprised of well-sorted pea gravel with some miscellaneous

constraction debris (e.g., bricks, concrete, stone).

During excavation of the septic tank, a section of cast iron 4-inch diameter pipe (identical to the

pipe observed during the excavation and removal of the absorption tank) was discovered

approximately 2.0 to 2.5 feet bgs at the western end and extended southwest. One section of pipe

contained a 45° elbow approximately 7 feet west of the septic tank. Further excavation yielded

an 11-foot section of pipe and appeared to be constracted in 5-foot sections. This pipe

terminated approximately 31 feet from the rear of the building (Figure 6).

6.7.1 Original Septic Tank - Post-excavation Soil Analytical Results

PCE was detected at concentrations of 6,530 ug/kg in P6, 3,510 ug/kg in SE9, 7,740 ug/kg in

SEIO, and 4,710 ug/kg in SEll . In addition, cw-l,2-dichloroethylene was detected in soil

samples SEIO and SEll at estimated concentrations of 149 and 65.1 ug/kg, respectively. The

concentrations of PCE in soil samples P6, SE9, SEIO, and SEll are above the NJDEP most



restrictive soil cleanup criterion of 1,000 ug/kg. No TICs were detected in the soil samples. The

estimated concentrations of cis-DCE in soil samples SEIO and SEll are less than the NJDEP's

most restrictive soil cleanup criterion of 1,000 ug/kg. A summary of analytical results is

presented in Table 4. The certified laboratory analytical report is included as Appendices 12 and

13.

6.8 Soil Disposal

Approximately 787 tons of soil and miscellaneous debris (concrete, cinder blocks, and bricks)

were excavated and contained in trailers for transportation and proper disposal. The covered

trailers were transported by six waste hauling firms to CWM Chemical Services, LLC (USEPA

ID NYD049836679) of Model City, New York for disposal (Table 3). Hazardous waste

manifests and transporter logs documenting the transport and disposal of excavated soil is

included in Appendix 8.

6.9 Site Restoration

FNB secured services of a contractor to restore the excavation area to its original condition. The

area affected by excavation activities was repaved to near existing grade using asphalt. The

excavation area is fiilly capped with an impermeable surface. Thus during precipitation events,

rainfall does not infiltrate the former excavation area and recharge ground water. Stormwater

and roof leader ranoff is follows the topographic gradient before it flows on Sea Girt Avenue.



7.0 GROUNDWATER MONITORING AND SAMPLING

GES performed a groundwater monitoring and sampling event on January 25, 2002. Ground

water samples were collected from all seven on-site monitoring wells (MWl through MW6,

MW3D) and one off-site monitoring well (MW7). Applicable protocols regarding well gauging,

well purging, sampling, handling, storage, preservation, reporting, decontamination of field

equipment, and other procedures were conducted as outlined in the NJDEP Field Sampling

Procedures Manual dated May 1992. A description of GES' Quality Assurance and Quality

Control Procedures is included in Appendix 14.

7.1 January 25, 2002 Groundwater Monitoring and Sampling Event

On January 25, 2002, depth to the static, unconfmed ground water table, as determined from the

top of the monitoring well casing ranged from 18.31 feet in MW7 to 24.00 feet in MWl (Table

2). At each ground water monitoring well, the depth to ground water measurement was

subtracted from the well casing elevation to determine the ground water elevation. The

calculated ground water elevations were used to constmct a ground water contour map. Ground

water flow on-site was towards the east under an average hydraulic gradient of 0.0091 feet/foot

(Figure 7). Ground water flow off-site also was towards the east under an average hydraulic

gradient of 0.0097 feet/foot (Figure 8). The calculated hydraulic gradients are indicative of a

groundwater table that is nearly horizontal. In addition, the calculated hydraulic gradient on-site

for this ground water monitoring event is consistent with the June 11, 2001 ground water

monitoring event. On June 11, 2001, the calculated hydrauhc gradient on-site was 0.0087

feet/foot.

Because MW3 and MW3D are proximate to each other and are screened at two different depth

intervals, the vertical hydraulic gradient was calculated. The vertical hydraulic gradient is equal

to the difference in ground water elevation or ground water depth between the monitoring wells

divided by the distance between the midpoint of the well screen intervals. The calculated vertical



hydraulic gradient is upward at 0.0021 feet/foot. This indicates ground water flow is towards the

shallow zone from the deeper zone.

Prior to ground water sample collection, each monitoring well was purged of at least three, but

no more than five times the volume of standing water to ensure representative ground water was

sampled. A dedicated disposable Teflon® bailer was utilized to collect a sample of the

groundwater in each well after completion of the required purging activities and allowance for

sufficient groundwater recharge into the monitoring well. Each sample of groundwater was

transferred directly from the bailer into 40-milliliter (mL) glass vials. Hydrochloric acid was

present in each vial to preserve the sample to a pH <2. Precautions were taken during sample

collection to ensure that no headspace was present in any sample. The ground water samples

collected were stored in an insulated storage cooler maintained at approximately 4 °C (wet ice)

and submitted to Integrated Analytical Laboratories, LLC of Randolph, New Jersey (NJDEP

Certified Laboratory Identification Number 14751). The groundwater samples were analyzed for

VOC+10 via USEPA approved test method 624 calibrated to include MTBE and tert-hutyl

alcohol (TBA).

7.1.1 Groundwater Analytical Results

On January 25, 2002, PCE was detected in all monitoring wells. PCE concentrations were 82.9

micrograms per liter (ug/L) at MWl, 7,190 ug/L at MW2, 1,720 ug/L at MW3 and MW4, 452

ug/L at MW3D, 4.7 ug/L at MW5, 239 ug/L at MW6, and 299 ug/L at MW7. TCE was not

detected at MW5 and MW6. Detectable TCE concentrations were reported for MWl (1.02

ug/L), MW2 (46 ug/L), MW3 (54.3 ug/L), MW3D (7.21 ug/L), MW4 (10.2 ug/L), and MW7

(1.96 ug/L). cw-l,2-DCE concentrations were 1.11 ug/L at MWl, 88.1 ug/L at MW2, 24.1 ug/L

at MW3, 7.27 ug/L at MW4, and 13.8 ug/L at MW5. cis-l,2-DCE ND at MW5, MW6, and

MW7. MTBE was detected at MWl, MW3, and MW7 at concentrations of 1.02, 13, and 3.88

ug/L, respectively. MTBE was not detected in any other monitoring wells.



The reported concentrations of PCE and TCE exceed the NJDEP GWQS of 1 ug/L for each

compound. The concentration of cw-l,2-DCE at MW2 (88.1 ug/L) exceeded the NJDEP GWQS

of 70 ug/L. The MTBE concenfrations reported at MWl, MW3, and MW7 are less than the

NJDEP GWQS of 70 ug/L.

No other targeted compounds or tentatively identified compounds (TICs) were reported by the

laboratory. A summary of groundwater monitoring data, analytical data including compound-

specific method detection limits (MDLs) and promulgated NJDEP GWQS for each volatile

organic compound (VOC) is provided on Table 2. A summary of ground water quality for this

monitoring and sampling event is provided on Figures 8 and 9. A historical summary of ground

water monitoring data and analytical data is provided on Table 2. The laboratory anal34ical

report for the January 25, 2002 ground water sampling event is included in Appendix 15.



8.0 TECHNICAL OVERVIEW

A GES Project Hydrogeologist was on-site to observe, document and conduct soil sampling. All

soil sampling activities were completed by an experienced GES Project Hydrogeologist.

Excavation and restoration activities were conducted by LEG.

All laboratory analytical services were provided by Accutest of Dajôn, New Jersey (NJDEP

Certified Laboratory Identification Number 12129). All soil samples were analyzed using

USEPA approved test methods. A summary of USEPA approved test methods utilized by

Accutest is included in their reports (Appendices 10 through 13, Appendix 15).

All field sampling activities were conducted according to generally accepted sampling procedures

as outlined in the NJDEP's Field Sampling Procedures Manual dated May 1, 1992. A detailed

description of GES' Quality Assurance and Quality Confrol procedures implemented on-site is

provided in Appendix 14.

8.1 Reliability of Laboratory Data

In accordance with the Technical Requirements for Site Remediation (NJAC 7:26E-3.10), reliability

of laboratory analytical data was reviewed for compliance with sample holding times, ability to

achieve method detection limits and other indicators of data reliability. The results of this review is

summarized as follows:

• All laboratory reports included a cover page hsting the NJDEP Laboratory Certification

Number, Table of Contents, facility name and address and date report was submitted.

• All laboratory reports included summary sheets listing analytical results for all targeted

compounds and TICs.

• Each laboratory report was bound, paginated and legible.

• Chain of custody forms for all sampling events were included in the laboratory reports.



All samples were submitted to the certified laboratory within 48 hours of sample collection.

All samples analyzed by the certified laboratory were completed within the required holding

times.

MDLs were provided for each sample analyzed by the laboratory.

Elevated MDLs were reported by the laboratory for water and soil samples analyzed for

VOCs. The elevated MDLs were adjusted to account for the dilution factor utilized by the

laboratory. The laboratory dilutes aqueous samples if targeted analytes are present at high

concentrations.

All samples analyzed for VOCs were conducted using USEPA approved test methods.

Non-Conformance Summary sheets for all analyses were included in all laboratory reports.



I

i 9.0 SUMMARY OF FINDINGS

• On November 12, 2001, a geophysical subsurface survey of the subject property was

completed. Using TDEM and digital GPR to locate, delineate, and plot any anomalies (e.g.

backfilled areas, voids, metal objects, tanks, etc.) which may be indicative of a former septic

tank system alleged to be present by the NJDEP. Four anomalies were identified justifying

additional investigation was required.

• In December 2001, the geophysical anomalies were investigated and two potential source areas

were identified. GES observed and documented the excavation and removal of an absorption

tank, a septic tank, and associated piping on-site. Both tanks were constmcted of pre-cast,

concrete cinder blocks constracted in situ. To the extent possible, surrounding soil suspected

of being impacted by VOCs was excavated and transported off-site for disposal on hazardous

waste manifests. More than 820 tons of impacted soil was transported off-site to a licensed

facility for disposal.

• Seventeen post-excavation (remedial) soil samples, collected from the sidewalls and bottom of

the former absorption tank, original septic tank, and piping excavations were laboratory

analyzed for VOCs. PCE was the only targeted analyte identified at concenfrations above the

NJDEP most restrictive soil cleanup criterion of 1,000 ug/kg. PCE concentrations were above

the NJDEP most restrictive soil cleanup criterion in three soil samples collected from the

original septic tank excavation and in one soil sample from beneath the piping associated with

this feature. Generally, soil containing PCE concenfrations above the NJDEP most restrictive

soil cleanup criterion remain on-site in the unsaturated zone at the north-northeastem portion of

the property.

• Impacted soil remains below the asphalt paved parking area. To date, the only VOC detected

above the NJDEP most restrictive soil criterion of 1,000 mg/kg is PCE. Above the water



•

•

•

table (vadose zone), PCE concentrations exceeded the 1,000 mg/kg criterion at P6 (6,530

mg/kg at 6.5 feet bgs), SE9 (3,510 mg/kg at 12.0 feet bgs), SEIO (7,740 mg/kg at 10.5 feet

bgs), SEll (4,710 mg/kg at 8.5 feet bgs). The parking area is completely covered with an

impermeable surface preventing direct physical contact with subsurface soils.

A deep soil boring was advanced on-site to confirm the existence of a confining unit. The

top of the confining imit (grayish-black silty clay) was identified approximately 62 feet bgs.

This confining unit reportedly separates the overlying Kirkwood Formation from the

imderlying Shark River Formation. The estimated thickness of this clay layer is 55 feet. This

deep soil boring was completed as monitoring well MW3D, which was set on top of the clay

unit with 10 feet of well screen. There was no evidence of NAPL during drilling of this

borehole and DNAPL is not present in MW3D. These data indicate DN7\PL is not present at

the interface of the Kirkwood and Shark River Formations below the subject property.

On January 25, 2002, depth to groundwater, as determined from the top of the monitoring well

casing, ranged from 18.31 feet in MW7 to 24.00 feet in MWl. The general direction of

ground water flow across the subject property is east which is consistent with previous

monitoring events. DNAPL has never been detected in the monitoring wells. Utilizing

groundwater elevation data for MW3 and MW3D, the vertical hydraulic gradient is upward at

0.0021 feet/foot. This indicates there is a component of ground water flow from the deeper

zone is towards the shallow zone.

Laboratory analyses of groimd water samples collected on January 25, 2002 from the seven on-

site monitoring wells (six shallow, one deep) and one shallow off-site monitoring well showed

concentrations of PCE and TCE above the NJDEP GWQS of 1 ug/L for Class H-A

groundwater. The concenfration of cw-l,2-DCE detected at MW2 (88.1 ug/L) is above the

NJDEP GWQS of 70 ug/L. Dissolved-phase VOC concentrations has not been delineated.



The dissolved-phase concentration of PCE in the deeper zone (452 ug/L at MW3D) is less than

the concentration of PCE in the shallow zone (1,720 ug/L at MW3).

MTBE (associated with unleaded gasoline) was identified at concentrations of 1.02 ug/L in

MWl, 13 ug/L in MW3, and 3.88 ug/L in MW7. This compound is not associated with any

current or historical operation of the subject property. Therefore, it is not a compound of

concem for this site. The presence of PCE in monitoring well MW6 and MTBE in monitoring

wells MWl and MW3 suggest these compounds are migrating onto the subject property.

According to NJDEP-BWA well records, two public supply wells are within a one-mile

radius of the site. One public supply well is in Manasquan near Mac's Pond. This well is

approximately 3,200 feet south-southeast of the subject property and has a reported depth and

pumping rate of 114 feet and 150 gpm, respectively. The second public supply well is owned

by Richard Bahadurian/Valley Park. This well is approximately 4,200 feet north-northeast of

the site and has a reported depth of 100 feet and a pumping rate of 22 gpm. In addition, the

well records indicate five domestic wells, two domestic or irrigation wells, three industrial

wells, 31 irrigation wells, and 17 monitoring wells are within a one mile radius of the site.



10.0 REFERENCES CITED

Rhodehamel, E.C. 1973. "Geology and water resources of the Wharton Tract and Mullica River

basin in southern New Jersey," New Jersey Department of Environmental Protection, Division

of Water Resources Special Report, No. 36, 58 p.

Sugarman, P.J. and Owens, J.P. 1994. "Geologic map of the Asbury Park quadrangle, Monmouth

and Ocean Counties, New Jersey," New Jersey Department of Environmental Protection and

Energy, New Jersey Geological Survey, Geologic Map series GMS 94-2.

Zapecza, O.S. 1984. "Hydrogeologic framework of the New Jersey coastal plain," U.S. Geological

Survey, Open-File Report 84-730, 61 p.



11.0 DISCLAIMER

The opinions, findings, and conclusions expressed herein are based upon information gathered

during GES' on-site investigative activities and from outside sources presumed to be accurate and

complete. No changes or alterations shall be made to this report without prior written

authorization from GES. No other presentation of findings, conclusions or recommendations

may be represented as GES', without prior written documentation by GES. Because the findings

and conclusions of this RIAR are subject to professional interpretation, differing conclusions

may be possible. GES cannot guarantee the subject property contains no hazardous materials,

environmental degradation or impacts beyond those detected or observed during the course of

this investigation. GES reserves the right to change, modify, or expand any of its statements if

additional information/documentation becomes available regarding this investigation.

Fleet National Bank (formerly White Swan Dry Cleaners) Remedial Investigation Wall Tovraship, (Monmouth County), New Jersey GES Project No. 03-02046/March 2002 41


Figures


SOURCE: USGS 7.5 MINUTE SERIES TOPOGRAPHIC QUADRANGLE 1989 ASBURY PARK, N.J. CONTOUR INTERVAL = 5 '

NEW JERSEY

QUAORANGtE LOCATION

DRAHED BY:

W.A.W. (WALL)

CHECKED BY:

J.M.

REVIEWED BY:

NORTH

SITE LOCA-nON MAP

FLEET NATIONAL BANK (FORMERLY ffHITE SWAN DRY CLEANERS)

1322 SEA GIRT AVENUE WALL. NEW JERSEY

Groundwater & Environmental Services, Inc. 1340 CAMPUS PARKWAY, P.O. BOX 1750, WALL, NJ 07719

SCALE IN FEET

2000

DATE

2-19-02 RGURE

1

SEA GIRT LODGE

o

t I 1 J 1

z

I

i

i

SEA GIRT LODGE

lEQEND

9

A

^

- G

~ W -

— T -

UE

MONITORING WELL

BENCH MARK PK NAIL ELEVATION = 44.92 FEET (NEW JERSEY VERTICAL DATUM)

UTILirr POLE

GAS LINE

WATER LINE

TELEPHONE LINE

UNDERGROUND ELECTRIC LINE

MWl M W 3 D ^ ^

MW3

SEWER CLEANOUT MW2 MW4

COLONIAL HAIR SALON/

CUMBERLAND FARMS

i SEA GIRT A VENUE

DRAFTED BY:

K.C. (WALL)

CHECKED BY

J.M.

REVIEWED BY

NORTH

SITE PLAN

FLEET NATIONAL BANK (FORMERLY WHITE SWAN DRY CLEANERS)

1322 SEA GIRT AVENUE WALL, NEW JERSEY

Groundwater & Environmental Services, Inc. 1340 CAMPUS PARKWAY. P.O. BOX 1750, WALL, NJ 07719

SCALE IN FEET

30

DATE

3-18-02 FIGURE

2

E

s

i « i

' I I i

3

B E 3

(0

m l i c .2 z

<)> o !c a. S O

a. S.

NOTE:

BASED ON WALL TOWNSHIP TAX MAPS DATED MARCH 28, 1969

DRAFTED BY

K.C. (WALL)

CHECKED BY:

J.M.

REVIEWED BY

NORTH

LOCAL AREA MAP




SCALE IN FEET

120

DATE

2-28-02 FIGURE

3

I

LAUREL

I

I I

i

I

I PS

2

s : a . 5 O

SEA GIRT LODGE

T"

SEA GIRT AVENUE

AVENUE

I I

• ' •

I RESIOENTW. ' RESIDENTIAL I

I I / I

I I I

L I I

I. r

RADIATOR CENTER

LEGEND

A

MONITORING WELL


LOCAL AREA MAP-MONITORING WELL LOCATIONS


1322 SEA GIRT AVENUE WALL. NEW JERSEY

G r o i j n d w a t e r & E n v i r o n m e n t a l S e r v i c e s , I n c . 1340 CAMPUS PARKWAY, P.O. BOX 1750, WALL, NJ 07719

SCALE IN FEET

60

DATE

2-28-02 FIGURE

5

ORIGINAL

ABSORPTION

TANK

ORIGINAL

SEPTIC TANK

SB5

Hi

S 1 ^

I

t

I I

< m

S S

in c o

a. &

Q. E

P SEioJ ^^"^ I MW3 •^ SEll J

i.-^ >

SB12

SB13

\

^ M W 4

Sample

P1 P2 P3 P4 P5 P6

SB1

SB2

SB3

SB4

SB5

SB6

SB7

SB8 SBg

SB10 SB12

SB13

SB14

SE1 SE2 SE3 SE4 SE5 SE6 SE7 SE8 SE9

SEIO SE11 ST1 ST2 ST3 SP4 SP5 SP6 SP7 TP1 TP2 TP3

Sample

Date

12/19/01 12/19/01 12/19/01 12/19/01 12/20/01 12/10/01 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14/00 9/14A)0 9/14/00 11/6/DO 11/6/00 11/6/00 11/6/DO 11/6/DO 11/6/00 11/6A)0 11/6/00 11/6/00 11/6A30 12/17/01 12/18/01 12/18/01 12/18/01 12/19/01 12/19/01 12/19/01 12/19/01 12/20/01 12/20/01 12/20/01 5/22/01 5/22/01 5/22/01 5/22/01 5/22/01 5/22/01 5i'22A)1 2/19/01 2/19/01 2/19/01

Sample Depth

(feet bgs)

6.0 5.0 5.0 6.0 7.0 6.5

8.5-9.0 20.0-20.5 15.5-16.0 21.5-22.0

7.0-7.5 19.0-19.5 22,0-22.5 9.0-9.5

15.0-15.5 21.0-21.5 11.5-12.0 19.5-20.0 11.0-11.5 19.5-20.0 15.5-16.0 19.5-20.0 19.5-20.0 11.0-11.5 19.5-20.0 19.5-20.0 11.0-11.5 19.5-20.0 11.0-11.5 19.5-20.0 16.0-16.5 19.5-20.0

17.5 21.0 18.5 20.0 19.0 17.0 17.0 17.0 12.0 10.5 8.5 6.5 6.5 6.0 13.5 12.0 fl.5 8.5 7.5 7.5 7.5

NJDEP most restrictive sdl cleanup criteria

Vdatite Organic Compounds micrograms/kilogram (dry wetglit)

Ctiiorobenzene

300U 280U 240U 270U 260U 250U 540U 590U 500U 630U 550U 600U 670U 630U 550U 580U 550U 560U 600U 580U 51OU 590U 560U 560U 630U 550U 710U 700U 420U 610U 550U 550U 340U 320U 280U 280U 330U 31 OU 280U 31 OU 260U 240U 220U

86J 590U 580U 490U 570U

86J 660U 540U 580U 61 OU

1,000

cyV1,2-DCE

300U 280U 240U 270U 260U 250U 540U 590U 500U 630U 550U 600U 670U 630U 550U 580U 550U 560U 600U 580U 510U 590U 560U 560U 630U 550U 140 J 140 J 420U 610U 550U 550U 340U 320U 280U

2eou 330U 310U 280U 31 OU 260U 149 J 65.1 590U 590U 580U 490U 570U 550U 560U 540U 580U 610U

1,000

PCE

300U 280U 152 118J 577

6,530 110U 1,100 100U 3,800 110U 120U 4,200 360 230

4,100 400

8,200 180 990

100U 1,000 110U 110U 110U 120U

9,600 15,000

84U 3,000 79J 150

340U 234J 280U 280U 330U 310U 280U 522

3,510 7,740 4,710 300 85J 190 170 500 170

9,100 170 200 280

1,000

TCE

300U 280U 240U 270U 260U 250U 110U 120U 100U 130U 110U 120U 130U 120U 110U 120U 110U 69J

120U 120U 100U 120U 110U 110U 120U 110U 140U 140U 84 U 120U 110U 110U 340U 320U 280U 280U 330U 310U 280U 310U 260U 62.3J 220U 110U 120U 120U 98U 110U 110U 130U 110U 120U 120U

1,000

lESEtlD

9 MONITORING WELL

A BENCH MARK PK NAIL ELEVATION = 44.92 FEET (NEW JERSEY VERTICAL DATUM)

- ^ SB - SOIL BORING LOCATION

- ^ ST - SOIL BORING (SEPTIC TANK)

- ^ SP - SOIL BORING (SEEPAGE PIT)

• INSPECTION PORT

= - INFERRED LOCATION OF CAST IRON PIPE

B TP - TEST PIT SAMPLE LOCATION

SE POST-EXCAVATION SOIL SAMPLE

P POST-EXCAVATION SOIL SAMPLE BENEATH PIPING

BGS BELOW GROUND SURFACE

C'W-1,2-[)CE cis-1.2-DICHLOROETHENE

PCE TETRACHLOROETHENE

TRICHLOROETHENE

ESTIMATED CONCENTRATION

TCE

J

U NON - DETECT AT METHOD DETECTION LIMIT INDICATED

NQIL:

HIGHLIGHTED PCE CONCENTRATIONS ARE ABOVE THE SOIL CLEANUP CRITERION.

Z MW5

DRAFTED BY: K.C.

(WALL) CHECKED BY;

J.M.

REVIEWED BY

NORTH

SOIL SAMPLE LOCATION MAP



G r o u n d w a t e r & E n v i r o n m e n t a l S e r v i c e s , I n c . 1340 CAMPUS PARKWAY, P.O. BOX 1750, WALL, NJ 07719

SCALE IN FEET

20

DATE

2-28-02 FIGURE

6

I a.

%

E 3

z < m

E E 3

C o

J) o IE s

o. S Q

SEA GIRT LODGE

cis-DICHLOROETHENE 24.1 TRICHLOROETHENE 54.3 TETRACHLOROETHENE 1,720 METHYL i-BUTYL ETHER 13

lEQEm

A

TOC

DTW

GW EL

cis-DICHLOROETHENE TRICHLOROETHENE TETRACHLOROETHENE

COLONIAL HAIR SALON/ CUMBERLAND

FARMS

cxs-DICHLOROETHENE TRICHLOROETHENE TETRACHLOROETHENE

TOTAL XYLENE TETRACHLOROETHENE

MONITORING WELL


TOP OF CASING (feet)

DEPTH TO WATER (feet)

GROUNDWATER ELEVATION (feet)

MW 1 2 3

3D 4 5 6 7

TOC 47.74 45.52 45.61 45.85 45.61 43.44 46.26 36.35

DTW 23.74 21.77 22.45 22.62 22.15 19.52 21.92 18.31

GW EL 24.00 23.75 23.16 23.23 23.46 23.92 24.34 18.04

NOTES:

GROUNDWATER ELEVATION CONTOURS IN FEET.

ALL ANALYTICAL RESULTS IN MICROGRAMS PER LITER.

MW3D NOT USED TO GENERATE CONTOURS.

MW7 LOCATED OFFSITE (NOT SHOWN ON MAP).

GIRT A VENUE

DRAFTED BY:

K.C. (WALL)

CHECKED BY;

J.M.

REVIEWED BY

NORTH

SITE INFORMATION PLAN 25 JANUARY 2002

FLEET NATIONAL BANK

(FORMERLY WHITE SWAN DRY CLEANERS) 1322 SEA GIRT AVENUE

WALL, NEW JERSEY

G r o x m d w a t e r & E n v i r o n m e n t a l S e r v i c e s , I nc . 1340 CAMPUS PARKWAY, P.O. BOX 1 7 5 0 , WALL, NJ 07719

SCALE IN FEET

30

DATE

2-28-02 FIGURE

7

i

^ ^

I I M

I 1 1

i i 1 i I

1

MONITORING WELL


TOP OF CASING (feet)

DEPTH TO WATER (feet)

GROUNDWATER ELEVATION (feet)

1 MW 1 2 3

3D 4 5 6

1 7

TOC

47.74 45.52 45.61 45.85 45.61 43.44 46.26 36.35

DTW

23.74 21.77 22.45 22.62 22.15 19.52 21.92 18.31

GW EL J

24.00 23.75 23.16 23.23 23.46 23.92 24.34 18.04 1

NOTES:

GROUNDWATER ELEVATION CONTOURS IN FEET.

ALL ANALYTICAL RESULTS IN MICROGRAMS PER LITER.

LOCAL AREA INFORMATION PLAN

25 JANUARY 2002

FLEET NATIONAL BANK

(FORMERLY WHITE SWAN DRY CLEANERS)

1322 SEA GIRT AVENUE

WALL, NEW JERSEY


SCALE IN FEET

60

DATE

2-28-02 FIGURE

8

SOURCE: USGS 7.5 MINUTE SERIES TOPOGRAPHIC QUADRANGLE 1989 ASBURY PARK, N J . CONTOUR INTERVAL = 5 '

5 8

1, 2, 4, 6, 22, 24, 31 - DOMESTIC SUPPLY WELLS 3 - PUBUC SUPPLY WELL

7-14, 48-50, 52-57 - MONITORING WELLS 15-23, 25-47, 51 - IRRIGATION WELLS

5 - INDUSTRIAL WELL

REFER TO TABLE t

NEW JERSEY

QUADRANGLE LOCATION

DRAFTED BY:

WAW. (WALL)

CHECKED BY:

J.M.

REVIEWED BY:

NORTH

WELL LOCATION MAP

FLEET NATIONAL BANK

(FORMERLY WHITE SWAN DRY CLEANERS) 1322 SEA GIRT AVENUE

WALL. NEW JERSEY Groundwater & Environmental Services, Inc.

1340 CAMPUS PARKWAY, P.O. BOX 1750, WALL, NJ 07719

SCALE IN FEET

1000

DATE

2-19-02 FIGURE

4

Tables


Table 1. Well Search Summary Fleet National Bank (formerly White Swan Dry Cleaners)

Wall Township, Monmouth County, New Jersey

• - • .' •'• 0\yher's^Jame / "^.....

:.?i •".'.!....'• > ' " 1 .:±^ :.}y.: '

* Manasquan Boro/Mac's Pond

•Atlantic Club •Atlantic Club *Bahadurian, Richard/Valley Park 1. Edward Peterson 2. Edwin Loesser 3. Wall Towne Shopping Center 4. Frank Muller 5. Eastern Shopping Centers Inc.

6. Diambrosio (McDonalds) 7. Waldwick Aerospace Devices 8. Waldwick Aerospace Devices

9. Waldwick Aerospace Devices 10. Shell Oil Company

11. Shell Oil Company

12. Shell Oil Company 13. Shell Oil Company 14. Shell Oil Company

15. Matt McKay 16. Arnold Kurmin

17. Melvin Price Jr. 18. Paul Gils 19. First Jersey Bank 20. William Tully

21. William Huber 22. Richard Campbell

23. George Groh

24. Mr. Gilligan

25. Frank Gagliano

26. Manasquan Saving and Loan

27. Edward Ahem 28. George Bower

29. Kevin Markland

30. Howard Gannon

31. John Conley

32. Anthony Lopomo 33. Frank Cristell

34. Bryan Patrick

35. Joseph Minion 36. Robert Larson

37. John Verga

38.TomTimko

39. Lee Reverendo 40. Dan Duffy

41.EdPalluzzi

42, Paul Doliner

43. Donna Williams

44. Steven Biserta 45. Gary Horan

• - . > ' - : . • . - • . . • ^ i - • ^ - ^ ; ; ^

• "WellLocation -i)

• - : : ^ • • • • , • / ' • • . • ' . ; • / • ' ? . . - . . • ; ' . . : 4

na

na na na

Magnolia Avenue

Brielle Circle Rte35

Blansing Road Circle Plaza Center

MacDonalds Route 35 Wall Twp.

Wall Twp. Wall Twp.

Rte 35 & Manasquan Circle Rte 35 & Manasquan Circle

Rte 35 & Manasquan Circle Rte 35 & Manasquan Circle

Rte 35 & Manasquan Circle 1106 New Brunswick Ave.

Meeting House Rd. 1015 New Brunswick Ave. 1210 New Brunswick Ave. Begonia and Sea Girt Ave.

1010 New Brunswick Ave. 2114 Redwood Drive

2202 Lincris Lane

1112 New Brunswick Ave.

2152 Redwood Drive

Magnolia Avenue

Meeting House Rd. & RT 35 Camden and Atlantic Aves.

2178 Old Mill Rd.

1008 New Brunswick Ave.

2150 Cottonwood Dr.

2207 Christine Lane 2206 Christine Lane

1210 Hemlock Ave.

1213 Hemlock Ave.

1225 Candlewood Lane 2156 Old Mill Rd.

2100 Old Mill Rd. 1220 Candlewood Lane

1014 Altlantic Ave.

2169GladfieldDr.



1206 Hemlock Ave.

Distaince. froiri'site.

:''<iniiles)i'4

0.60

0.70 1.70 0.80 0.41

0.28 0.24 0.41 0.37 0.07 0.49

1.49 2.49

0.40 1.40

2.40 3.40

4.40 0.40 0.17 0.43 0.40 0.06

0.50 0.30 0.40

0.40

0.30

0.50

0.20

0.37 0.20

0.46

0.26 0.23 0.23

0.40

0.40

0.30 0.46

0.46 0,30

0.43

0.37

0.30 0.50

0.30 0.21 0.41

'I'Direc'tiori

' from site}

'jim^m^ BSE

na na

NNE E

SSW SSW

SE SW SW N

N N

S

S

s s s

SE WSW

SE SE E

SE NE E

SE

NE

E

SW

SE E

SE

N

S S

NE

NE NE

NE

NE

NE

SW

W

NE

N

NE E

NE

Well -depth

.:ifeet)i •;

114

170 171 100 93 84 150 42

na 66 32

32 32

15

15

15 15 15

67 53 25 80 59 50

88 37

83

77

97

51.5

60 100

119

40

28 32

115

28

110 110

110

98

75

66

98 103

102

110

105

' "Screen *

. lerig'th .

•''Ifeeti ,

na

na

na na

9.25

3 20 3

na 6 10

10 10 4

4

4 4

4

10 8 15 20 10 10 15 10

20

20 20

6

10 10

5

8

18 10 20

4

10

10

10

10

10

10

10 10

10

10

10

Puinpingi

.• 'rate' .,• '.

• feftmi-;

150

50 51 22 5

8 407

5

150 16 na na

na

na

na na

na na 4.5

15 5

40 10

40 10 25 12

20 20

15

15 25

na

50 15

15 60

15

20

20

20

20

20

20 20

20

20 20

20

^lJse.df:-:

"welt: I , • _ . : . . _ ' - •

PS

IN IN PS D D PS D

IN D

MW MW MW

MW

MW

MW MW MW

IR IR IR IR IR

IR IR

D/IR IR

D

IR

IR

IR

IR

IR

IR

D/IR IR

IR

IR

IR IR

IR IR

IR

IR

IR

IR

IR IR

IR

: . . ;pafe .'-

; Installed' i '• • '

na

na na na

11/23/51

7/29/53 1/3/57

na 5/18/66 3/28/01 1/21/83 1/22/83 1/23/83

5/14/84

5/15/84 5/16/84

5/17/84 5/18/84

8/9/85 9/15/85

na

6/10/88 8/1/88

9/14/88 10/13/88 5/15/84

7/7/89

8/10/89

4/26/01

11/30/99

8/19/91 12/10/91

7/1/92

10/1/93 8/8/94

10/18/01

7/10/96

3/28/97

12/6/97

12/5/97

12/17/97

5/29/98

6/25/98

9/20/01 3/29/99

6/25/99

6/24/99

6/28/99

8/19/99

Page 1 of2


Table 1. Well Search Summary Fleet National Bank (formerly White Swan Dry Cleaners)

Wall Township, Monmouth County, New Jersey

r.— i r ' a ' - ' . " •Owner's Name Well Location

•'; Distance'; ••.DireTstion '•$. -from'site^-j-' fi-pm sitev 1 " (mifes)}'"' W ^ M M r :

Well' depth. (fee^

Screen Pumping 'tlse.of . p a t e " lengthv ^ rate •• ' ' \v;ell' , ' Installed'

:(feet>' -(gpm)'' ' : _ ' •

46. Jim Thopmkins 47. Mario Paniscotti 48. Summit Bank 49. Summit Bank 50. Summit Bank 51.PauI VanAnda 52. WaWa Inc. 53. WaWa Inc. 54. WaWa Inc. 55. WaWa Inc. 56. WaWa Inc. 57. Fred Kurfes

1217 Candlewood Lane

1221 W. Chicago Blvd.

1322 Sea Girt Ave. 1322 Sea Girt Ave. 1322 Sea Girt Ave.

1215 Hemlock Ave, 2110 Rte. 35

2110 Rte. 35 2110 Rte. 35

2110 Rte. 35 2110 Rte. 35

2204 Lincris Lane

0.50

0.50

0.02 0.02 0.02

0.40 0.20

0.20 0.20

0.20 0.20 0.40

N

NE

N N N

NE N

N N N N E

97

101

30 30 30 106 27

27 27

27 27

50

10 10

15 15 15 10

20 20 20 20

20 14

20

20

na na na

15 na

na na na na 20

IR

IR MW MW MW

IR MW MW

MW MW MW MW

8/20/99 6/29/00

8/11/00 8/11/00 8/11/00

2/27/01 1/15/01

1/15/01 1/15/01 2/12/01 2/12/01 3/17/01

Explanation of terms: D: domestic; IN: industrial; IR: irrigation; MW: monitoring well; na: not available/reported; PS: public supply well; *: information obtained from computer well search.

Page 2 of2


Table 2. Groundwater Monitoring & Sampling Comparison Data Fleet National Bank (formerly White Swan Dry Cleaners)

1322 Sea Girt Avenue Wall Township, Monmouth County, New Jersey

Well

ID

MWl

MWl

MWl

MWl

MW2

MW2

MW2 MW2

MW3

MW3

MW3 MW3

Ground Water

Sampling

Date 8/25/00

10/30/00

6/11/01

1/25/02

8/25/00

10/30/00

6/11/01 1/25/02

8/25/00

10/30/00

6/11/01 1/25/02

Top of Well

Casing

47.74

47.74

47.74

47.74

45.52

45.52

45.52 45.52

45.61

45.61

45.61

45.61

Depth to Ground

Water

feet 21.15

22.18

21.05

23.74

19.96 20.17

19.09 21.77

20.64

20.85

19.49 22.45

Ground Water

Elevation

26.59

25.56

26.69

24.00

25.56

25.35 26.43

23.75

24.97

24.76

26.12

23.16

Benzene

;:;:i "i 2.6U

2.6U

9.5U

0.6U

65U 26U

95U 30U

65U

130U I90U

6U

Toluene 9

,45000

3.0U

3.0U

9.0U

0.66U

75U

30U 90U

33U

75U 150U

180U 6.6U

Ethyl-

benzene

•7OO0

2.6U

2.6U

9.5U

0.6U

65U

26U 95U 30U

65U

I30U 190U

6U

Total Xylene

Methyl/-

butyl ether

r-Butyl

alcohol

cis -Dichlor

oethene Tetrachlor

oethene NJDEP Ground Water-Quality StandaSls for.Glass II-A, ug/L

1,00.0 70,3, filO i i a70 ,.sa 1 . 3.1U

3.1U

9.5U

1.8U

78U 31U

95U 90U

78U

160U

190U 18U

2.5U

2.5U

9.5U

1.24

62U

25U 95U

53U

62U

120U 190U

13

170U

170U

290U

1.02U

4,300U

1,700U 2,900U 102U

4,300U

8,600U 5,800U 20.4U

10 8,4

47

1.11

98U 47 210

88.1

110

560 1,200U

24.1

1,700

1,300

5,400

82.9

27,000

10,000 36,000 7,190

29,000 84,000

120,000

1,720

Trichloroethene

Total Volatile Organics

f 1^1.^'' I m ' • 8.0

6.8

25

1.02

lOOU

41U 160U

46

230 650

760 54.3

1,718.0

1,315.2

5,472.0

86.05

27,000 10,047 36,210

7,324.1

29,340

85,210

120,760 1,811.4

MW3D 1/25/02 45.85 22.62 23.23 1,5U 1.65U 1.5U 4.5U 2.65U 5.1U 7.27 452 10.4 469,67

MW4

MW4 MW4

MW5

MW5 MW5

MW6

MW6

MW6

MW7

Trip blanl

10/30/00

6/11/01 1/25/02

10/30/00

6/11/01 1/25/02

10/30/00

6/11/01 1/25/02

1/25/02

1/25/02

Explanation of terms:

45.61

45.61

45.61

43.44

43.44

43.44

46.26

46.26

46.26

36.35

—

20.65

19.49 22.15

17.80

16.77 19.52

20.03 19,15

21,92

18,31

—

24.96 26.12

23.46

25.64

26.67

23.92

26.23

27.11 24.34

18.04

—

6,5U

19U 6U

0,3U

0,2U 0,3U

5.2U

9,5U

1,5U

1,5U

0,3U

7,5U

18U 6.6U

0.3U

0.2U

0.33U

6.0U

9.0U

I.65U

I,65U

0,33U

6.5U

19U 6U

0,3U 0,2U

0,3U

5,2U

9,5U

1,5U

1,5U

0,3U

7,8U 19U

18U

0.3U

0.2U

0.9

6.2U

9.5U 4,5U

4.5U

0.9U

6.2U

19U 10,6U

0,4

0,2U

0,53U

79 62

2,65U

3,88

0,53U

430U

580U

20,4U

17U

5,8U

1,02U

340U

290U

5,1U

5,1U

1,02U

14

50 13,8

0,4U

0,2U 0,27U

7,8U

9,0U 1,35U

1,35U

0,27U

2,800 11,000 1,720

16

13 4.7

1,900 6,200

239

299

0,38U

11 38

10.2

0,4U

0,3U

0,26U

13

32

1,8U

1.96

0,36U

2,825

11,088 1,744.0

16,4

13

4,7

1,992 6,294

239

304.8

0

D: Secondary dilution; U: Not detected at method detection limit indicated; ug/L: micrograms per liter Detectable concentration in bold type exceed Ground Water Quality Standard

Page I of 1


Table 3. Soil Disposal Summary Fleet Bank (formerly White Swan Dry Cleaners)


'H'lioad^'Date'^

12/11/01

12/17/01

12/18/01

12/19/01

12/20/01

.:': Ma nlftis t Nii rrib|iti;;'

NYB9492282 NYB9492291

NYB9675063 NYB9675054 NYB9675045 NYB9675036 NYB9675126 NYB9675135

NYB9675072 NYB9675081 NYB9675099 NYB9675027 NYB9675108 NYB9675117 NYB9675324 NYB9675333 NYB9675342 NYB9675414

NYB9675207 NYB9675216 NYB9675351 NYB9675369 NYB9675171 NYB9675378 NYB9675189 NYB9675225 NYB9675729 NYB9675234 NYB9675765 NYB9675738 NYB9675387 NYB9675153

NYB9675828 NYB9675837 NYB9675846 NYB9675855 NYB9675864 NYB9675774 NYB9675783 NYB9675792

Total pounds: Total tons:

^?iWeighii;ii(pb;unds)Sf

35,100 32,080

46,220 47,780 37,880 48,360 38,580 36,220

36,940 46,460 43,160 42,800 41,980 43,840 38,140 43,340 46,660 56,300

37,320 42,720 42,240 45,560 41,760 47,140 45,360 35,360 43,940 26,080 37,820 42,420 40,560 30,740

42,680 43,320 42,180 34,600 40,900 35,800 42,460 38,140

1,640,940 820.47

g.'''Date BSeceiy(|j}:';i

12/17/01 12/20/01

12/18/01 12/18/01 12/18/01 12/18/01 12/18/01 12/18/01

12/19/01 12/19/01 12/19/01 12/19/01 12/19/01 12/21/01 12/19/01 12/21/01 12/19/01 12/19/01

12/20/01 12/20/01 12/20/01 12/20/01 12/20/01 12/20/01 12/20/01 1/3/02

12/20/01 12/20/01 12/20/01 12/20/01 12/20/01 1/3/02

12/21/01 12/21/01 12/21/01 12/21/01 12/21/01 12/21/01 12/21/01 12/21/01

Truck Number

Rolloff Rolloff

534 85

530 556

CVl-141 CV-GMC

544 453 6733 3158 528 702 543

6881 6840 465

CV-GMC 141 541 574

9600 85

11000 138

9800 143

8000 8200 531 141

5241 1163 7000 195

3158 5800 6573 4726

fe>:4::WaslgH^lp(5-:j

Horwith, Inc. Horwith, Inc.

Horwith, Inc. Horwith, Inc. Horwith, Inc. Horwith, Inc.

Clean Venture, Inc. Clean Venture, Inc.

Horwith, Inc. Buffalo Fuel Corp.

Page ETC Page ETC

Horwith, Inc. Horwith, Inc. Horwith, Inc.

Buffalo Fuel Corp. Buffalo Fuel Corp. Buffalo Fuel Corp.

Clean Venture, Inc. Clean Venture, Inc.

Horwith, Inc. Horwith, Inc.

Price Trucking Corp. Horwith, Inc.

Price Trucking Corp. Clean Venture, Inc.

Price Trucking Corp. Clean Venture, Inc.

Price Trucking Corp. Price Tmcking Corp.

Horwith, Inc. Clean Venture, Inc.

Page ETC Price Trucking Corp. Price Trucking Corp. Price Trucking Corp.

Page ETC Price Trucking Corp.

Page ETC Page ETC

Page 1 of 1 "An Equal Opportunity Employer"

Table 4. Summary of Volatile Organic Compounds in Post-excavation Soil Samples Fleet Bank (formerly White Swan Dry Cleaners)


Sample Identification Number Lab Identification Number Sample Date Sample Depth (feet below grade) Concentration Units » [J..

Targeted Compound Acrolein Acryloniteile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis -1,2-Dichloroethene trans -1,2-Dichloroethene 1,2-Dichloropropane cis -1,3-Dichloropropene trans -1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Ten:achloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes Tentatively identified compounds

PI ; . N5065-1 12-19-01

6.0 ug/kg

3,000U 3,000U

60U 300U 300U 300U 300U 300U 300U

1,200U 300U 300U 300U 300U 300U 300U 300U 300U 300U 300U 300U 300U 300U 300U 300U 60U

300U 300U 300U 60U

300U 300U 300U 300U 300U 120U

0

; .P2 NSp65-2

"^12-19-01 5.0 J ,

, ug/kg ll

2,800U 2,800U

56U 280U 280U 280U 280U 280U 280U

I.IOOU 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 56U

280U 280U 280U 56U

280U 280U 280U 280U 280U llOU

0

P3 N5065-7

- 12-19-01 5.0

ug/kg

2,400U 2,400U

49U 240U 240U 240U 240U 240U 240U 970U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 49U 240U 240U 152 49U 240U 240U 240U 240U 240U 97U

0

P4 N5065-8 12-19-01

6.0 . . ug/kg

2,700U 2,700U

53U 270U 270U 270U 270U 270U 270U


270U 270U 118J 53U

270U 270U 270U 270U 270U llOU

0

P5 N5213-1 12-20-01

7.0 .5Ug/kg

2,600U 2,600U

53U 260U 260U 260U 260U 260U 260U


260U 260U 577

260U 260U 260U 260U 260U 260U llOU

0

NJDEP Soil

Quality -Criteria* ^

1 ug/kg"'

NA 1,000 1,000 1,000 1,000 1,000 1,000 1,000 NA NA

1,000 10,000 1,000

50,000 100,000 100,000

NA 10,000 1,000 8,000 1,000

50,000 10,000 1,000 1,000

100,000 1,000 1,000 1,000

500,000 50,000 1,000 1,000 NA

2,000 67,000

**

Explanation of terms: J: Estimated concentration NA: No criterion has been established for this constituent U: Not detected at method detection limit indicated ug/kg: micrograms per kilogram (dry weight) *: Criteria listed is most restrictive soil cleanup criteria **: Total volatile organic contaminants criterion is 1,000,000 ug/kg

Page 1 of4 "An Equal Opportunity Employer"

Table 4. Summary of Volatile Organic Compounds in Post-excavation Soil Samples

Fleet Bank (formerly White Swan Dry Cleaners)

1322 Sea Girt Avenue

Wall Township, Monmouth Coimty, New Jersey

Sample IdentincatiohNumBef; j iab Identification | j .umber; '; •

Sample:'Pate ; . ' ' | 3 - , ' '•';^''' • '' u Sample Depth (feet,below g r a d e ) g

tflfiicehtration # n i t s .'• ••• ••.'.• ••• ' m

Targeted Compound

Acrolein Acrylonitrile Benzene Bromodichloromethane

Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis -1,2-Dichloroethene trans -1,2-Dichloroethene 1,2-Dichloropropane

cis -1,3-Dichloropropene trans -1,3-Dichloropropene Ethylbenzene

Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane

Trichloroethene Trichlorofluoromethane Vinyl chloride

Xylenes Tentatively identified compounds

' • • ; : - ' •P6:^: : 'V

• : . N 5 i l 3 - 5 . i '

j 12^10-01 ,

r, ' ' ' \6.5]'; :' ••'- u g / k g i -

2,500U 2,500U

51U 250U 250U 250U 250U 250U 250U

1,000U 250U 250U 250U 250U 250U 250U 250U 250U 250U 250U 250U 250U 250U

250U 250U 51U

250U 250U

6,530 250U 250U 250U 250U 250U 250U lOOU

0

• ' / • ' • • • S E l , , . ..^•

'.•fN*873-l;'f

r-": ug/kg,. II

3,400U 3,400U

67U 340U 340U 340U 340U 340U 340U

1,300U 340U 340U 340U 340U 340U 340U 340U 340U 340U 340U 340U 340U 340U

340U 340U 67U

340U 340U

340U 67U

340U 340U

340U 340U 340U 130U

0

:;-::{:rSE2 ::•',';

:'uv-4945'-iV' •'niiis-rftiV'

':k-2lJ^]:-: ; - ' U u g % ; : i

3,200U 3,200U

63U 320U 320U 320U 320U 320U 320U

1,300U 320U 320U 320U 320U 320U 320U 320U 320U 320U 320U 320U 320U 320U

320U

320U 63U

320U

320U 234J

67U 320U 320U

320U 320U 320U 130U

0

. \ , S E 3 •";.;•;'.;

: N4945-2' ' ' '

12-18-01 ,

.-.lis iig/kg

2,800U 2,800U

56U 280U 280U 280U 280U 280U 280U

1,100U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U

280U 280U 56U

280U

280U 280U 56U

280U 280U 280U 280U 280U l lOU

0

- : f . - \ S E 4 : . " : '

^ N # 4 5 - 3 ;•,••

, -12£l'8.-dl;': •

" •s'Jo'.b.;'',' '• .ug/kg'd-

2,800U 2,800U

56U 280U 280U 280U 280U 280U 280U

1,100U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U

280U 280U 56U

280U 280U

280U 56U

280U 280U 280U 280U 280U l lOU

0

^vK'irpoEP...,.;:' ;•• .';;."• .So i l ' . ' '^•• '

',': .Qualit); ":' •'•["•Critetia'!^-:-l

'•*'.''ue/*^'••'•-

NA 1,000 1,000 1,000 1,000 1,000 1,000 1,000 NA NA

1,000 10,000 1,000

50,000 100,000 100,000

NA 10,000 1,000 8,000 1,000

50,000 10,000

1,000 1,000

100,000

1,000

1,000

1,000 500,000 50,000 1,000 1,000 NA

2,000 67,000

**


Page 2 of4



1322 Sea Girt Avenue Wall To-wnship, Monmouth County, New Jersey

Sample Identification Number Lab|ldentification Number ^ Sample Date' Sample Depth (feet below grade) Concentration Units

Targeted Compound Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis -1,2-Dichloroethene trans -1,2-Dichloroethene 1,2-Dichloropropane cis -1,3-Dichloropropene trans -1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tenrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes Tentatively identified compounds

SE5 , N5065-3

/ 12-19-Oi' . 19.0,, ug/kg'

3,300U 3,300U

65U 330U 330U 330U 330U 330U 330U


330U 330U 330U 65U

330U 330U 330U 330U 330U 130U

0

SE6 1 .N5065-4,

12^19-01 ,

r|7.o: , ug/kg

3,100U 3,100U

62U 310U 310U 310U 310U 310U 310U


310U 310U 310U 62U

310U 310U 310U 310U 310U 120U

0

SE7 , N5065-5 12-19-01

17:0 ' , ug/kg

2,800U 2,800U

56U 280U 280U 280U 280U 280U 280U

I.IOOU 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 280U 56U

280U 280U 280U 56U

280U 280U 280U 280U 280U llOU

0

. SE8 ' N5065-8 12-19-01

17.0' ug/Ug i

3,100U 3,100U

62U 310U 310U 310U 310U 310U 310U

1,200U 310U 310U 310U 310U 310U 310U 310U 310U 310U 310U 310U 310U 310U 310U 310U 62U 310U 310U 522 62U

310U 310U 310U 310U 310U 120U

0

. SE9 ''N5213-2.

12-20-01 12.0

ug/kg

2,600U 2,600U

53U 260U 260U 260U 260U 260U 260U


260U 260U 3,510 53U

260U 260U 260U 260U 260U llOU

0

NJDEP Soil

Quality Criteria*

ug/kg

NA 1,000 1,000 1,000 1,000 1,000 1,000 1,000 NA NA

1,000 10,000 1,000

50,000 100,000 100,000

NA 10,000 1,000 8,000 1,000

50,000 10,000 1,000 1,000

100,000 1,000 1,000 1,000

500,000 50,000 1,000 1,000 NA

2,000 67,000

**





Sample Identification Number , Lab Identification Number Sample Date Sample Depth (feet below grade) Concentration Units

Targeted Compound Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Diclilorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1 -Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans -1,2-Dichloroethene 1,2-Dichloropropane cis -1,3-Dichloropropene trans -1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylenes Tentatively identified compounds

SEIO,, N5213-3 12-20-01

10.5 ug/kg

2,400U 2,400U

48U 240U 240U 240U 240U 240U 240U 960U 240U 240U 240U 240U 240U 240U 240U 240U 240U 240U 149J

240U 240U 240U 240U 48U 240U 240U 7,740 48U 240U 240U 62.3J 240U 240U 96U

0

SEl l N5213-4 12-20-01

8.5,

' "S/kg

2,200U 2,200U

45U 220U 220U 220U 220U 220U 220U 900U 220U 220U 220U 220U 220U 220U 220U 220U 220U 220U 65.IJ 220U 220U 220U 220U 45U 220U 220U 4,710 45U 220U 220U 220U 220U 220U 90U

0

-

'

!

*

NJDEP Soil

Quality Criteria*

ug/kg '

NA 1,000 1,000 1,000 1,000 1,000 1,000 1,000 NA NA

1,000 10,000 1,000

50,000 100,000 100,000

NA 10,000 1,000 8,000 1,000

50,000 10,000 1,000 1,000

100,000 1,000 1,000 1,000

500,000 50,000 1,000 1,000 NA

2,000 67,000

**



Table 5. Summary of Volatile Organic Compounds in Ground Water (January 25, 2002) Fleet National Bank (formerly White Swan Dry Cleaners)


Sample Idehltificati'oh ^fumb'e^' • Lab'Identification* Number .! T.opofCasingElevit ipn,(feet) ' Depth tq Ground Water (feet) G ^ u n d VS/atier Elevatidn (feet) !,Dilut.iqn''Factor-.; ' ; 'v '!4^.. '' ' Cdnceht'ratidniiFnits- .' • r=^;' ' . '

Targeted Compound Chloromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane Acrolein 1,1-Dichloroethene Methylene chloride Acrylonitrile tert- Butyl alcohol trans -1,2-Dichloroethene Methyl tert- butyl ether 1,1 -Dichloroethane cis-\ ,2-Dichloroethene Chloroform 1,1,1 -Trichloroethane Carbon tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane 2-Chloroethyl vinyl ether cw -1,3-Dichloropropene Toluene frawi' -1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Xylenes Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorohenzene

•TMW-lV'l 06i8-bp4t^

•'•.;'-^47.74? ••,:','

' '•, 23;74."fV. .; •' l'24ioo;;*:;.,. . ; : ! : . . : 2 ' . . ; "•}. ,

' • . * * U g / L ' • • ' • ! : :

1,22U 0,66U 0,94U 1.3U

0.76U 11.9U

lU 3.82U 2.54U 2.04U 0.78U 1.24

0.66U 1.03

0.62U 0.76U 0.78U 0.7U 0.6U

0.72U 0.5U 0.5U 0.5U

0.38U 0.66U 0.54U 0.62U 82.9

0.62U 0.56U 0.6U 1.8U

0.56U 0.54U 0.44U 0.44U 0.38U

, ] „" ' :MW-2. ' , ; '

r66i,8|007:.'' ;;''::45i52 '.5;.;; • ' % 2 V ^ ^ i t ' /

, !• • • •41 - ' ^ • - • . I • .

-'•^?.W'r'3v' •::.'. i;ue/L-vî;

61U 33U 47U 65U 38U

594U 50U 191U 127U 102U 39U 53U 33U 88.1 31U 38U 39U 35U 30U 46

25U 25U 25U 19U 33U 27U 31U

7,190 31U 28U 30U 90U 28U 27U 22U 22U 19U

' . • V i v i w - s , :•••.•

l:'-S6d-b08 S;;'"l5i6i.'''•"•'' v/'V<.22;4Sr;--

:.-e-23ii6,:^^? \ i > ' wil' p- ^ : ' .W= ' . 'UE /L i . . ' . ^ .

12.2U 6.6U 9.4U 13U 7.6U 119U lOU

38.2U 25.4U 20.4U 7.8U

13 6.6U 24.1 6.2U 7.6U 7.8U 7U 6U

54.3 5U 5U 5U

3.8U 6.6U 5.4U 6.2U 1,720 6.2U 5.6U 6U 18U 5.6U 5.4U 4.4U 4.4U

3.8U

•:, •.MW-3D • .•: 618:0b2DIL i / . 45.85': ','

,'::'22.62 •';•,, ,V.i'23^23'-'--'• ' ' • ' . ; ' i 6 . ; ' :•••,

;::.^.ue/L'l'^

6.1U 3.3U 4.7U 6.5U 3.8U 59.4U

5U 19.1U 12.7U 10.2U 3.9U 5.3U 3.3U 6.32 3.1U 3.8U 3.9U 3.5U 3U 10.4 2.5U 2.5U 2.5U 1.9U 3.3U 2.7U 3.1U 452 3.1U 2.8U 3U 9U

2.8U 2.7U 2.2U 2.2U 1.9U

..•••M:W,r4., :,

: ; 6 1 8 - 0 0 6 ' ; [:;V;'45i6i„;,; i •";'., 22;i'5.„;'

- \J?A^::\: v'";îd..';.':

,'. ' . U E / L ' ^ '

12.2U 6.6U 9.4U 13U 7.6U 119U lOU

38.2U 25.4U 20.4U 7.8U 10.6U 6.6U 13.8 6.2U 7.6U 7.8U 7U 6U

10.2 5U 5U 5U

3.8U 6.6U 5.4U 6.2U 1,720 6.2U 5.6U 6U 18U 5.6U 5.4U 4.4U 4.4U 3.8U

'.ViyODEPi^V.

Orpuhd.Wiater

' Quality ;< ; f. Criteria.•:';.':; 1

:-';ciiss'itA'': ' • • • . , ' . " ' , ' . , — ' • • • ' , • • ' ! ,

' • • M i f h ' ^ - '

30 5 10

NA NA NA 2 2 2

100 100 70 50 70 6

30 2 2 1 1 1 1

NA NA

1,000 NA

3 1 10 50 700

1,000 4 1

75 2

600

Explanation of terms: NA: No criterion has been established for this constituent; U: not detected at method detection limit indicated; ug/L: micrograms per liter Concentrations in bold type are more than NJDEP Ground Water Quality Criteria

6 Page 1 of2


iMp

Table 5. Summary of Volatile Organic Compounds in Ground Water (January 25, 2002) Fleet National Bank (formerly White Swan Dry Cleaners)

1322 Sea Girt Avenue Wall Township, Mormiouth County, New Jersey

Sample Identification Number LabTdentification Number. Top of Caiing:Elevation (feet<)_ Depth t6 <ir<|iiiWd)Water^(fee't)j, ) ôund 'Wate i Elevation (ieet) i Dilution "Factbpi:' .. J ' -, ' dl>ncehtratibh%niis '•"" -'" >

Targeted Compound Chloromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane Acrolein 1,1-Dichloroethene Methylene chloride

tert- Butyl alcohol trans -1,2-Dichloroethene Methyl te:rt- butyl ether 1,1 -Dichloroethane cis -1,2-Dichloroethene Chloroform 1,1,1 -Trichloroethane Carbon tetrachloride 1,2-Dichloroethane Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane 2-Chloroethyl vinyl ether cw -1,3-Dichloropropene Toluene ran.y -1,3-Dichloropropene

1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene Xylenes Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene

MW-5. 618-003

43.44 ='19.52 '% h 23i92

1 S I

1 ug/L

0.61U 0.33U 0.47U 0.65U 0.38U 5.94U 0.5U 1.91U 1.27U 1.02U 0.39U 0.53U 0.33U 0.27U 0.31U 0.38U 0.39U 0.35U 0.3U

0.36U 0.25U 0.25U 0.25U 0.19U 0.33U 0.27U 0.31U

4.7 0.31U 0.28U 0.3U 0.9U

0.28U 0.27U 0.22U 0.22U 0.19U

MVV-6 618-005> ,46.26 ^ 21,92

' 24.34

3 ^ \ Ug/L

3.05U 1.65U 2.35U 3.25U 1.9U

29.7U 2.5U 9.55U 6.35U 5.1U 1.95U 2.65U 1.65U 1.35U 1.55U 1.9U

1.95U 1.75U 1.5U 1.8U 1.25U 1.25U 1.25U 0.95U 1.65U 1.35U 1.55U 239

1.55U 1.4U 1.5U 4.5U 1.4U 1.35U I.IU I.IU .95U

MW-7 618-001

36.35 18J1 18.04

5 ug/L

3.05U 1.65U 2.35U 3.25U 1.9U

29.7U 2.5U

9.55U 6.35U 5.1U 1.95U 3.88

1.65U 1.35U 1.55U 1.9U

1.95U 1.75U 1.5U 1.96

1.25U 1.25U 1.25U 0.95U 1.65U 1.35U 1.55U 299

1.55U 1.4U 1.5U 4.5U 1.4U

1.35U I.IU I.IU .95U

%. i

{: L\

*!

I*

. ..r jJDEP',:,;'••; Ground Watier

.Quality',-'':; ; - t e i t e r i a 'E - Class il-A 'I

•Vu^/L:-:-:^

30 5 10

NA • NA NA 2 2 2

100 100 70 50 70 6

30 2 2 1 1 1 1

NA NA

1,000 NA 3 1 10 50

700 1,000

4 1

75 2

600

Explanation of terms: NA: No criterion has been established for this constituent; U: not detected at method detection limit indicated; ug/L: micrograms per liter Concentrations in bold type are more than NJDEP Ground "Water Quality Criteria


Appendix 1

f

' NJDEP - Bureau of Water Allocation Records


"1 r ri r ! i

SUBJECT TO REVISION

100,000 GPD WATER WITHDRAWAL POINTS ONLY AND CONTAMINATED SITES WITHIN 5.0 MILES OF:

LATITUDE 400808 LONGITUDE 740345

FT SCALE: 1:63,360 (1 Inch = 1 Wile)

X 100,000 GPD W/ITER WITHDRAWAL POI^^TS ONLY

i CONTAMINATED SITES

1 MILE AND 5 MILE RAOII INUCATEO

co^^•AMl^lATED S I T E U S T AS OF 0 3 / 2 1 / 9 5

PLOT PRODUCED ST;

NJDEP WATER SUPPLY ELEMENT BUREAU OF WATER AaOCATION C N - 4 2 6 TRENTON. NJ 08625

DATE; 0 1 / 2 6 / 0 2

401200

SUBJECT TO REVISION 400400

Paoe I of C».Tfl«!ff i IEI' BITES HITHiN 5,0 HILES DF 400BOE LfiT. 740345 LOH. AS ff 03;'2!-'?5 ! IH 1 M B : B'Y SITE R K E R ) - 0 j / : ' i , '02

SITEJ Nfiff

539 fiUffi BEI f f iERI tB W C m " H f l t f i A T E D

1017 ANOCtI SERVICE STATION BELHAR' BOROUGH

1022 DfflA MARINE

1031 BEL RAY COHPfW INCORPORATED

1032 DORRERS CORNER 6ARA6E

1033 « A a AUTD I K O : E R S

1057 AHOCO S S f i n STATICN ffiiD; TWEHIP

1058 BRICK TOMJSHIP LANDFILL

1351 aiLF SEF iICE STATION BEUBR' BOROUSl

1342 DONIKR HMIFACTURINS CtRPOfflTION

1343 TOfflUTH TOOL i ECWFTIBii uS-PAN? INC

1368 BPA'.'EreW) JSALTii' INTERESTS

1406 THE OCEAN COUNTY UTIL fiUTH WS 8

1692 GA,RDEN STATE PARKWAY U M F I L L

1693 HEfiUY AUTWBTI'^ CENTER;

1714 JANES H JAHES LANDFILL

1715 RIDffi ROAD LANEf l a

1728 FDINT PLEASANT BEACH BOROUffl SATER DEPT

2881 114 19TH AVENUE

2892 TECfffllCAL SYSTEMS

2883 29D IHUERRY COiRT

2934 SCHAFER OIL COHPfiJJY INCORPORATED

2957 STAT AKBULANCE.

2982 JCPSL COHPAfff ST0a:T0li SUBSTATION

2985 107 1ST AVENUE

2986 407 HASIINGTON AVENUE

2990 PLASTI aAD ICfAL FIfflDUCTS INCORFHiATH)

2991 SERVICE STATIDfJ BALL TOtSEHIP

2995 NJ TRANSIT INOKFORATB

2999 43 ADAIR DRIW

3004 JCPSL CffiPAff? S i L ' e T f f l SUBSTATION

3006 S H a i SER-JICE ETATIOii' BRICK T!KNSHIP

3046 POINT VILLAGE NAU

3047 US POSTAL SERVICE POINT aEASANT BEACH

3048 AKOCO SER'.'ICE STATI9I FtHlfT PLEASiWT

3194 BELHAR COAL GAS (JCPa S tUf f i )

3394 BONITOF: DE'.'ICE: I ICORfWSTB

3395 KALDIO; AEROSPACE DEVICES INCORPORATED

3417 BRETON HARBORS GR'D HF: C»JT.« ( INHTIDN

5226 AVON FUEL OIL INC0SP0R6TED

5227 A\m-BV-Ti£-5Efi BOROUGH ffilNTENAHCE YARD

5228 BELNAR BOR0U5H HASINA

5229 FREEDHANS BAt;ERY INCDRFWSTEB

5230 STERN ASSOCIATE

5231 1£SS SERVICE STATIKi WADLEY BEACH H M

5232 BREILLE ANCHORAGE

5233 HOFFHANS MARINA

5309 EKON SERVICE STATION MANASOUAN BaROUSH

5310 HOUARD HEISTT AUTO

5311 NOBIL SERVICE STATIffii HA.*IASfflim BMSJGH

5312 MOBIL SEFMCE STATIOfi fKNASQUAN BORIMH

5313 SUNKO SERVICE STATIB) HANASffilAN BOROBI

5353 GETTY EERinCt STATION l £ P T « £ CITY E t M

5365 HOmUTH OIL BURNER i FUEL COMPANY INC

5369 NnSH FARMS

ADDRESS

1730 RTE 34

1200 HAIN ST

381 BRIELLE RD

111 BONMAfi m

1460 RTE 34

1818 H ST

18TH AVI t HEREERTS'.iILLE RD

SALLY IKE RD

1801 RTE 71 i ISTH m 206 MIN ST 30 BROAD ST REAR 905 5TH m KEANA'.'E GS PHY MS 98.9 2801 BELMAR BLVD

SCHIOHOIEERD

RIDGE RD

416 m Yoa; AVE

114 19TH AVE

1309 H ST

29D MULBERRY ET

5 MAIN ST N

60 STEINER' AVE

RTFS 71 i 524

107 lET A'.€

407 BASHINGTON AVE

RiDGaTO RD

RTE 35 i LA.'iEIMD RD

TNILifflT DR

43 ADAIR DR

HOOPER Al^ I BRICK BLW RTE 88 65! ARNOLD AVE 410 ARNOLD ffff 3201 RTE 88 16TH 5 RAILROAD A l B

RTE 34 (AIRPORT ACCESS RD)

2117 TO 2121 RTE 35

BRETON HARBOR' DR

616 NORBOOD AVE

S STATION m .

90O MARINA AVE 803 MAIN ST 713 13TH AVENUE 1009 HAIN ST 512 GREEN A'TE 602 GREEN AVE RTE 71 4 MAIN ST 38 TAYLOR AVE 21S PARHR Af f (RTE 71 N)

RTE 71 4 CURTIS A l t

RTE 71 4 SEA GIRT AVE

SYLVAJfIA t NEPTUa AVES

38 RTE 35

703 OLD CDR1IE5 A l t

m

HALL TaSJEHIF

BELMAR'BDRffJSH

HANASQUAH BiKtlUGH

m i ToaigiiP ISLL T K H I P

BALL T'DtmSHIP

BRIO: 'mmw

mm immip KLMAF; BtROUat

M»iaSOUAN HiRttHI

KA»miAN S M I H

IKEBl TOiaSHIP

POINT HEaAf i l BEACH m s m

m i ToaisHip HALL TiMSHiP

BfiiO; TOafflflP

BRIEt; TOSailP

POINT PLEASANT EtHJlH

MLMARHM0!

BELMAR BORHIGH

BRIELLE BOfitJiai

MANASQUAN BOROiffl

NEPTUNE CITY BOROUGH

SEA GIRT BffiOUGh'

SFfiING L A f I EORt tH l

SPRING i M £ FOROUai

B lT iS l f f iK IP

HALL TOlfflSHIP

BAY l£AD BOROiHl

BRICK TOtKSilP

BRICK TWEHIP

BRIO: TIMBHIP

POim FIEASANT EEAOt B S M K

FBINT FIEASANT BEAOI BffiOOffl

POINT . lEASANT BOROUGH

BELMAR-BORaSH

BALL TDBJSHIP

HALL TOiJiSHIP

D R S TOSSSHIP

AViBi-BY-THE-SEA BOROiSH

A'ffiN-B'Y-THE-SEA B f f a W

BELMAR BOR'SiGH

EaMSRBOROm

BELMAR BORWGH

KiADLEY BEACH OTHEH

BRIELLE BOROISH

BRiEUE m a m

MANASQUAN BOROUGH

MANASQUAN B0F:0U6H

MAfJASOUAH BORffiJGH

MANASaJAN BORUH)

MANASQUAN BOROUGH

icPTiK c m - BtmUSH

NEPTUff TOiSJSHIP

HEPTUIC TtJiHSHIP

COUITY

fiiSMWTH

HOmiTH

MffifflJTH

HONrffiUTH

WMUTH

NOfmiTH

OCEAN

OCEAN

HOmUTH

fllMtOUTH

MONMOUTH

HMSITH

OCEAN

MONMOUTH

MOIMUTH

KEAN

ffiEAN

EEAN

HOmUTH

MOmOUTH

lEfKJJTH

MOMJJTH

MONMOUTH

MiMOUTH

MONMOUTH

MMIOUTH

MffilMOUTH

MOfraiTH

OCEAN

OCEAN

DCBiN

OCEAN

OCEAN

OCEAN

OCEAN

mMJUTH

HOtraUTH

MONKfflJTH

OCEAN

HOtSIOUTH

MOWMH

miOUTH

KMSJIK

fJMOUTH

MONMOUTH

MONMOUTH

MOWWJTH

MONMOUTH

MONMOUTH

NOmOUTH

MONMOiJTH

IfflNMOUTH

troouTH HOTBUTH

MOfMUTH

CSLS

NJ11980778450

WL000070524

NJL60012572B

NJD002145S11

NJL600035406

NJL000010512

NJLOOC069S80

WD98050517i

NJL00006SB33

NJL500009402

NJL600023402

IHL60016Ci'343

NJL60O145'»7

NJD932274292

NJL600239065

NJL000042119

NJD981173354

NJL830002431

NJL00OO45971

NJL00006I291

WL00005(61B

NJD011417649

NJL000045245

KJL800075004

NJL00iiO63917

NJL800089849

NJD980770655

NJL800093627

NJD00«K6!4

NJLSOOOgiOSl

NJD982281750

NJL880001490

NJL800104B2(i

NJ4180000099

NJLB00010514

NJS9B0770481

NJD98052940B

NJD054931337

.NJL000030B90

NJD01107S763

NJL600249973

NJC8760-0S17S

NJL6001311B9

NJL600195653

NJL600055727

NJL000053073

NJL6O0O9045O

NJD986603a65

NJL6(iO054431

NJD9B6606;76

NJD986606184

NJD931142235

WL400O10706

NJL600194054

NJL60012133?

CfiSEJ

E50169

9 4 0 J 7 4

531230

MD0C121458I1

9405182

9503113

531228

521232

930722

940260

0035-796

94«9iC!

0221799

930193

950591

9Si7127

9304166

930116

9 2 0 6 1 7 1 ^

9304061252

52!03fil502

87111601

950655

940712163600

9308119

940921090757

9:«310952

941011115721

5209181359

540731092237

940712162100

9007271548

941205111000

930730

950423111909

NJD98077043I

M072

(i)D054931337

NJL000030S90

0069753

0069744

0200512

0234040

0237286

0087870

0144380

0143039

0';iS6772

0085930

0062723

0305138

0148133

0016166

0043553

0190538

LAT

401110

401042

400641

400953

400953

400953

400541

400626

400953

400715

40072'3

401003

400445

40105Ci

401045

400710

400724

400512

40101!

401035

400631

4Ki733

401146

400759

400826

400918

400836

400953

400449

400520

400520

400520

400529

400550

40C445

401038

401107

400336

400520

401141

401130

400953

401056

401035

401158

400631

400628

400715

400722

400740

400719

400719

401160

401141

401214

LON

•40653

740131

740232

740501

7405.01

740501

740553

740707

7405*1

740243

740304

740201

740347

740607

740400

740628

74064!

740237

740103

740143

740414

740314

740128

740227

740139

740147

740556

74050!

740347

740654

740654

740654

740310

740251

740522

740142

740711

740333

740654

740113

74005S

740501

740126

740134

740108

740254

740:^58

740413

740251

740242

740413

740413

740205

740130

740411

DISTANCE CONTAC

4.4 BEECRA

3.5 BFCH

2.0 BFCM

2.3 BFCM

2.3 BFOi

2.3 BFCM

3.4 ffOI

3.5 BFOI

2.3 EFOi-6

1.3 BFOI-6

1.0 ffCM-6

2.7 BFEB-6

3.3 BFOi-6

3.7 BFO-CA

3.0 BFO-CA

2.6 BFO-CA

2.7 ffO-CA

3.5 tfO-CA

3.3 BFO-S

3.3 BFO-S

1.5 BFO-S

O.S BFD-S

4.6 BFO-S

1.2 BFO-S

1.5 ffO-S

2.2 BFO-S

2.0 BFO-S

2.3 BFO-S

3.8 BFO-S

4.2 BFO-S

4.2 BFO-S

4.2 BFO-S

3.1 BFO-S

3.1 BFO-3

4.1 BFO-S

3.4 B3CM

4.4 ESS

0.5 BSfi

4.2 BSM

4.4 BUST

4.6 m i 2 .3 BUST

3 . 9 BUST

3 .4 BUST

5 . 0 BUST

2 . 0 BUST

2 . 0 BIST

1,0 BUST

! . 2 BUST

1.1 asT 1.0 BUST

1.0 BIBT

4.7 HBT

4.5 BUST

4.7 HJST

[ G

Mj

i-i n

n

CO

o-

-"

!"> u-J

03

ro

ro

ro

r--> t^

, -~

, t-'i <!>

aa e

t e

^ c-~t t--* ~

a e

a -a

- o

- -^^ o

o

•-•> o

- r-o

r-.

g (-5

--.

—, —

.T r.j

t-J

—..

.^

iT'

r-3

c- r^

rj

—i C

- —

^ l~-V

-tr

-^r

•••- ^ r^

t-"" r-^ -a

- r-1

ro

ir

"^

ro

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6 F E E N E R ; I I ^ A S S O C I A T I O N

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GREEI\ERIAF; I I ! -CME01*ERS ASSOC

GF£B^1BF;IAR I I HOR-EOW!'-EF.S A S S O C

GREENBRIAR' I I HCÊOL•!NERS A S S C E

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4.034FS m l'!ATER SUPPLY Al,ITH'JF:ITY 4035PS SFR'ING lEHDOW HXF CCLRSE .K:'36PS' N . J . WATEF: S1.FPLY j' JlT-iCFilTY 5019 h!EW JERSP/-Aê-VIt:AM klATER' CD.

hEW JERSEY-AI'-'ER'ICPN UJAiTEF: CO. NEW JERSPf'-Al^RICAW Wi TER CO.

r-cw JEFSEY-c-rB^;io'ir-J WATER CO. hEW .lEKiEY-AfERKM^T I'ftTER' CO.

5063. ÊW JEr..SEY-Pf-'ERia-W b!ATER CO. hEW JEFSEy-i^VEF:^^^-! WXrSP. W .

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F'acie P P E L i m t ' m ^ y SLR'-'ETr" CF WATEF: WITHDF;AI)!AL. POINTS WITHIN MILES OP" 40':e;)S L A T . 7 4 0 : > 1 5 LCf'J. ( I N CPIJEF: B Y F E R T - H T .fNLMEER) - 0 1 / 2 6 / 0 2

MJ-IEEP; r-Jf'ME SCUPCtlD u a i i D LCf'! U-AiCC DISTAiCE CajT-JTY MJt'J DEP'TH GEOl GE02 CAPACITY

EQJ-'IAF: EiffiOLGH EEU1AR BOF,a. r+J

5 1 4 9 WALL TOWNSHIP (.'JA'TER DEPT.

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I'iALL TCW-J3HIP I'JATER' DEFT.

WALL T » , ^ & I I P mTER' DEFT.

W i X T t t i r -EHIP I'JATEP; DEFT.

WALL TDMl-'iSJ-JIP WATEF: DEFT.

WALL. TOUrjEJHIP I-IATHR EEFT.

5 1 5 3 POINT FLEASAWT BOPflJGH

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E F ; I 0 . ; TCWISHIP M . U . A .

H; : ID. ; TowrâÎp M . U . A .

BF:IO.; TOWNSHIP M . U . A . E R I D ; TOWÎSHIP M . U . A . BF;IO.; TOWTvEHIP M . U . A . ERIO.; TOWhOHIP M . U . A . BRIO.; TOUTJSHIP M . U . A . ERID. ; TOMJÎSHIP M . U . A .

5184 P'AF1.,'1'!AY I'JATEP: Ca'E'ANY

PARKWAY WATEF; COhPAT-IN-' F'AFKl'JAY KlAiTEF: CCW-'AJW PAFS'-'.ViAY WATER COhPi'-Wr FARKVJAY I'JATER LXltT-'ArJY PARKWAY MATER CCMTÂWf' F'AFKltf^Y WATER aj''PAJ'-JY

5237 SEA GIRT EQ=£ilJ3H

SB'4 BIRT la'Sf-XJO-l SEA GIRT ECROLKBH

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5279 EFilELLE EOROUCH ERIELLE BaâXBH BF:IBJ_E Ea=.ajBH

52'97^ PT . PLEASANT EEACH ECROUGH

F T . FLEASAf'.fT EEATJH BCF.OJa-l

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4.2 3.4 1.2 1.1 3.7 3.1 3.4 2.9 3.1 3.6 3.7 3.8 3.8 4.6 3.6 1.1 1.1 1.1 1.1 1.1 5.9 5.9 5.9 5.9 6.0 6.0 5.9 5.9 6.0 6.0 5.3 6.0 5.9 .6.0 6.0 4.5 4.3 4.7 4.7 4.7 5.3 4.4 1.1 1.1 1.1 0.8 ill 1.1 2.0 2.1 1.6 1.6 3.5 3.0 2.8 5.4

! 5 25 s 25 25 .2: .25 ,25 25 25 2=? ,29 29-29 29 25 25 25 25 25 ,29 29' 29 29 29 29 29 29 29 29 29 29 29 29 29 25. 25 25 25 ,25 255 ,25 25 r25 25

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[ ]

Page 5 o-f PFELIMir-.i-'RY a_FÊY CF WATEF! WI"lP![F;Ai!-JAL F-OIOTS WITOIN 5 . 0 MILES CF AiXeCB LAT. 740345 LCW. (IN rRi:eR BY f-EPniT NLMBEF:) - 01/26/(:)2

r-jLir-iEeF; r-«rE SOLFCEID LOCID LAT ta-s LLACC DISTATCE axwry MLN DEF'TH C-EOI GEO2 CAF'ACITY

MC ra.ELL , FFED PO'JD ^C EOWELL , .!=FED 49o;K:ei MC DOWBX , FFED 490.;i0a2 MC Ea«ELL . FFED 4-9i:>;:)'-:)83. I-C DCJ-ELL . PP.'ED 49tX>:e4 MC DOWELL . FFED 49.:K:»':IS5 t 'C DCtELL . FRED 490i:iOS6

H-!.:)7-qR L . B . FOFCELLATI ,!-: SOr.B KLR^RY 2940031 L.B. FCRCELLATI & SOl-B r\LR^RY 2944650

000:03 n-JLLET MAF.TIN FCfJD

WB_L 1 WEIX 2 WEaX, 3 I'JELL 4 I'JELL 5 I'JELL 6 I'JELL 1 I'JELL 2 1

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4(31210 400946 4-;>;)946 400422

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7Ai'JZ<>i> 740922

F F F F F F F F

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5,

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90 90

90 530

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GTD; GTD; BTD; GTD; GTD; GTD.;

GTD; a.:]>1M a.O'Tj

14

750 733 750 753 '750 733 733 H:x3 !«)

GTCH S O E T 450

NLimber of O b s e i ^ ' a t i o n s : 233

Form DWR-138A 10/87

G

G

G

G

^

r-

CD

?-0 o

o

STATE OF NEW JERSEY -j^DEPARTMENT OF ENVIRONMENTAL PROTECTION

i y y DIVISION OF WATER RESOURCES

WELL RECORD

iTlr (SrJuucAfd T^^<n»o^

COORD:

PERMIT NO

APPLICATION NO

COUNTY

m^ 1. OWNER N I f C ^ r ^ l A J W U r-^?T\<S^<:^r\ AnnnP^s > I lO lVyvr^ \U^

Owner's Well No. I SURFACE ELEVATION

2. LOCATION K j \ \ j CSljCVJir \

3. HATF rnMPi FTFn • I / 2 ' 4 / S > DRILLER

\ u ^ PW, . Sgg-^ (c)ir\

3o (Above mean sea level)

-Feet

^

/ / . / } . A - /g rS h S c ^ / S C

4. DIAMETER: Top.

5. CASING: Type fil K

slot

. inches Bottom

6. SCREEN: Type.

Range in Depth { Top.

^-7 r> Size of Opening f-"'^

_ inches

Diameter

Diameter

1. 3>'L

TOTAL DEPTH.

Inches

Inches

^93 Length.

Length.

S3 <?'3 / /

-Feet

.Feet

.Feet

Bottom 3 '6" Feet

Feet

Tail Piece: Diameter. Inches

Geologic Formation ^ m y fxVXr^. 5<Vvd - ^ ^ f B V A ^ ^ '

i '6>" Length

WELL FLOWS NATURALLY

Water rises to

/ lO Gallons per minute at

Feet above surface

8. RECORD OF TEST: riatp / / / < 3 3 / 5 / Yield.

-Feet

Feet above surface

Gallons per minute

Static water level before pumping

Pumping level LS2.

Drawdown T 7 Feet

3L\

feet below surface after IL Feet below surface

^ _ _ _ _ _ hours pumping

Specific Capacity. Gals, per min. per ft. of drawdown

How pumped r o C L C ^ d d ^ pt/•:><. How measured /y)u>icj~i eJtc -h-sh^

Observed effect on nearby wells n&>'UL.

PERMANENT PUMPING EQUIPMENT:

Type C b c O l d s " T U J I A ^ ( J r

5 Capacity .

Depth of Pump in well

_ G.P.M. How Driven

~ 7 ^ Feet

Mfrs. Name _ <3)Cvjlcl-S

H.P. / ^ R.P.M. 3GoQ

Depth of Footpiece in well / 3

O Depth of Air Line in well

10, USED FOR d!e>Vrt f .A i - tCj

Feet Type of Meter on Pump (XXC <^cvuv»_

Average

Size.

Feet

.Inches

AMOUNT

11. QUALITY OF WATER

Taste C b o c ^ d

% J ^ { Maximum.

Gallons Daily

Gallons Daily

Odor, AC>. Vje. Color.

Sample: Yes, No

Temp. 6^ 12. I CiC. X>f^ h6U i ^ ^ ( \ A j k ^ r c y - /a 2 M ^ / t c / & ^ r g"^^ " Vre samples available?

(Give details on back ofsneeroronSpardteslieet If electric log i^Sâde, please furnish copy.)

°F.

13. SOURCE OF DATA _

14. DATA OBTAINED BY n... / / /U /S / TKu 0CK.

(NO TE: Use other side of this sheet for additional information such as log of materials penetrated, analysis of the water, sketch map, sketch of special casing arrangements, etc.)

G

G

G

L

Form 87-5"-£) ^, ^ iP DEPARTMENT OF CONSERVATION

^ , AND ECONOMIC DEVELOPMENT

Permit No. " 2 . S - * ? ^ /

Application No.

/Ô^ Division of Water Policy & Supply WELL RECORD S

County

3^. 33- sea*

1. OWNER fzJ\Aj\\^ L OB<^S F ' ^ ADDRESS 2 V \ e L L ^ C ', ^ c l < . ^[^ -.V U^

Owner's '.Yell No. SURFACE ELEVATION (&b«** M a n t e a 1 * T « 1 )

Feet

2 . LOCATION ' U v . ' e . L L C C v V C - - ^ - ^ H V C <- ^/-•<... '

3 . DATE rhMPiPTFn >^(^^\/ Q- ^ 6"J'nHTI.l.F.R - ^ o k v y / T ^ . i rileî- :

4 . n T AMF.TFR: TVip 3 Inches Bottom —^ Inches TOTAL DEPTH: O T" Peet

5 . CASING:15T)e Diameter, .Inches Length

6 . SCREEN: Type \ Oppnlng / o ^ L f C Diaineter_l_4£__lnches Length ^ L _

Top Feet Geologic Poraation ,

Peet

Peet

Range In Depth { Bottoa

Tail piece. Diameter

Feet Inches Length Peet

7 . WELL FLOWS NATURALLY

Vater r ises to

,Gallons per Minute at .Peet above surface

.Feet above surface

8 . RECORD OF TEST: Date ^ ^ / ^ ^^ 5 ^ ^ Afield


Pumping level

Drawdown

m .feet below surface after

. Gallons per minute

Feet below surface

hours pumping

Peet êclfic Capacity. .Gals, per min. per ft.:of drawdown

How Pumped How measured

Observed effect on nearby wells

9. PERMANENT PUMPING EQUIPMENT:

Type ^ " ^ N^ u-i^ -T) Capacity 1 How Driven ^ L£c-f-.v\r Horse Power, K

.Gallons per minute

R.P.11.

Depth of pump in well .Peet Depth of Air Line in' well.,

10. USED FOR 00—-^*^<. h

. Peet Depth of Foot piece in well

Feet Type of Meter on Pump

1^— { Average J ~ ^ ^ Gallons Daily

AMOUNTS ' Maximum ^ ^ ^ Gallons Daily

Sample: Yes No. • 1 1 . QUALITY OF WATER.—: ^ ^ ^ ^ Odor / J^>i ^ Color ^ L ^ o - V " ._. Temperature Taste

1 2 . LOG _ (Give d e t a i l s on back of sh«e t or on s e p a r a t e shee t )

Are samples available?.

1 3 . SOURCE OF DATA

1 4 . DATA OBTAINED BY > r o W , V:le^ J e ^ DATE ^ ^ L Y ^ ^ ' ^

(<«ote: Use o ther s i d e of t h i s s h e e t fo r a d d i t i o n a l I n fo raa t l on such as log of a a t e r l a l s p e n e t r a t e d , ana l j r s l s of th* e a t e r , ske t eh nap, s k e t c h of s p e c i a l ca s ing a r r a n g s a e n t s , a t e . )

WELREC 112 2688

[

m . . . ^

"''^-fi-. « •

"v. V „ /S:-,

WELREC 112 2689

" ^ 1^" STATPOPNBVJPBSPY , PERMIT NO. <?? 9 ' t 3 - / 9 < f DWR-138A ^ k; STATE OF NEW JERSEY " ^ DEPARTMENT OF ENVIRONMENTAL PROTECTION

DIVISION OF WATER RESOURCES

G

G

G

APPUCATION NO.

COUNTY. ._

W E L L RECORD COORD. c 3 9 . 3 $ - 5 ' 3 3

1. OWNER EasAfrVN ' l ^ ^ p p > > ^ G ^ W ^ . \ AC Annmpgg L \ X ( \ i A \ \ ^ i . \ t ^ V k j r \ I ^ V

Ownw'f Well No. SURFACE ELEVATION . * ^ ^ . P'^'^t

2. LOCATION \MM\ln\iLl irN > > K » . y p ; ^ C fl^Nd^r . K J - ^ S " ^ fi:4Û^K:. Arvr<- - UJcyU T t M p

3. DATE COMPLETED ^ / I j Û DRILLER ^ - ^ - L - < x n Y>v«tf% ^

4. DIAMETER: Top JSkZ—inches Bottom _ S _ inches TOTAL DEPTH / S O—_Feet

5. CASING: Type ^ Diameter Inches Langth : Feet

6. SCREEN: Typ* " 3 3 Sze of O p e n i n g - i H ^ ^ Diametar £ Inches L e n g t h . ^ i i O .

f T o o 5 7 , F e e t ^ ^ ^ W V , r \ / ^ , ^ ^ r \ ' ^ Range In Depth i " ^ t / f;a/u«qi>. c»>m.ti»n \<^\T w-t.>^<a«^<J^

/ Bonom L-jT ^**! t l3C* f U " !

Tail Piect: Diameter Inches Length Feet

7. WELL FLOWS NATURALLY ^ ^ Gallons per minuta at . Feet atiove surface

Water rises to Feet above surface

8. RECORD OF TEST: n » f 3 > / S ^ S 7 y i d d _ _ _ I I ^ _ L _ _ Gallons per minute

Static water level before punping S L J L • Feet below surface

Pumping level feet below surface after hours pumping

Drawdown ' Feet Specific Capacity _ , Gals, per min. per f t . of drawdown

How pumped How measured

Observed effect on nearby wells '


Type , \ Mfrs. Name _ -

Capacity G.P.M. How Driven ^___ H.P. R.P.M, ^ . • • • ^ • • •

Depth of Pump in well ^ _ _ _ _ _ Feet Depth of Footpiece in well _ ^ _ _ _ - _ _ ^ _ _ _ Feet

Depth of Air Line in well Feet Tvpe of Meter on Pump Size Inches

( Average Gallons Daily

Mavimiim Gallons Dally

11, QUALITY OF WATER ^ Sample: Yes No

Taste _ _ _ « ^ _ ^ _ _ _ _ _ Qrinr Color Temp. op.

12. L O G . — , Are samples available? _ _ _ ^ _ _ _ _ _ _

(Give drtailt on badt ofthmt or on M M » « M sh—t If tficirie log vmn made. plea»e furnish copy,)

13. SOURCE OF DATA Proî^ <i3- VWc^.-iCg w I CX.. ,

14. DATA OBTAIN en BY ran. ^ / / ^ 7

(NOTE: Use other side of this sheet for additional information such as log o f materials penetrated, analysis o f the vMter, sketch map, sketch o f special casing arrangements, etc.)

.Feet

WELREC 112 2419

. /

BY . . . i i DATEj^/^S' i j r jS SUBJECT. , . ' ' . . . ' . . . . . . ; . : . : . . . . . .', SHEET NO * OF,,

CHKD. BY DATE

i^%--}>

* j r '

/ • • •

./

^ 4 ' ,

c

G

G l^^

M 7 ' / s^

A J > / .:r:

.Jk^4tC'r.<9W..A>f....S:/i!0Afi//i^& JOB NO.y.:^.:.G..:y...

i5^Vl5£D 3-10-57

\3 .40

Vxr

i

^-*/

—(f/9^''v6- 6"D''-^ (A/ &uêHT Sr^BL

BLT^/^K S£cyfCi^ (3"£>M s.Te-e-ii Q0SfNi&

-~Scfi i££hj / i s / fSoi^£

1 . ' - A

WELREC 112 2420

-Eastem Sliopp:^g Centers, Inc . 61 M«ll WJLUC - Cross County Ctr . YoQkera, New York

C. W. Launan & Conâny, I n c . P. 0 . Box 235 Bettapage, Hew York

29*33.533 G 29-2198

L, 53-55

5 5 - 6 3

_i 6 3 - 6 6

- 66 - 7U

L 121 - 126

G 126 - 127

127 - 131

131 - 136

136 - u a

l U l - 1U7

No samples frora 0 - 5 3 f e e t .

Light yelloHish-gray udxture of very coarse sand and veiy f in* ft«4i<« 0*M«t«*-| sand. Scattered ^ pebbles .

Llgiht ye l lonlsb-gray , moderately ndcaceoua, very s U ^ t l y clayBy« f ine sand t i l th sca t t e red Tery coarse gra ins . HeaTles good.

Light p inkisb-gray, f a i r l y c lean , s l i g h t l y iaieaceoTis> f ine sand tf i th small percent of neditm t o coarse g ra ins . Fine sand s l i g h t l y l a r g e r than 55-63. Heavies f a i r t o good.

L i ^ brovnish-gray, f a i r l y c lean, nediim sand. Unlike any TkH, more l i k e Teh. Sand subangolar t o sobrounded. Heavies very poor.

Qrayisb-orange, moderately clayey and micaceous, very f i ne sand. Heavies f a i r .

Gray, somewhat d i r t y , f ine t o mediim sand with sca t t e red very coarse g r a in s .

Gray, moderately micaceoos, sandy c lay .

Sane as 121-126.

Sane.

Gray dayey rasditm sand.

Sane, slightly clayey.

Hewy Minerals examined from 130-llt7« In general contains more jnaik minerals than yellowlcih Tkv sand. Very fine haaTies, mostly ilnenlte but naoh more staorolite and garnet i Larger sized heavies contain approximately 25^ garnet, 25^ sta'orollte. This is more typical of the true marine sands of the coastal plain.

Kv*-K»ta<l

1

G",

^j^^^^ym^'

WELREC 112 2421

|SUMH.Y ÊLL tOG 2 . ^ ' 3 3 •S3'i>

job \?.T.!^.L^.k^Î!i^...§}^9.M^M..9.?.9:^.'?..^.

^Date Stwtcd ....M^9.h..^.Jt....^?.^2 Conqileted...

Diaineter...3fi."....X...a!' In.

_Depth.........l4.7... Ft. .0. In.

w p c G jyô^"€>m<t.r",-.!tw-v

• j o . Dan EMI br ....C.....IallDiaa mx:9±.X.X.,...X9.p.

:'i Measlred from clade JB Yes Q N o " * ^ " ^ | ^ ^

1 i-- ,1 A$Â<\r--' Abovi. F4i Ii In. Be o*r.... ;..Ft.. ?ff

Static Level.....?.*. Ft.. f ,J(

,in. 1 Eievaj^ .54...|..::;...'..:.:i.Ft. P I I L S o r H I B U H

G. Dan4&&

.Jn.

'•HT'IT.ASOJ no H""V1.V; 1"-^'

Sandy Loaji A , Sand & Clay - brovn

Brown Or11

Madium do#raa with 8tre%kt| of white olay 1 ^ 10^

Medium filio aand, aone g r i ^ and clay

Fina Brown a m ^ M ' ^ m B t a .<.ta-,ijl>: ffwi ,<ifini t nox t-!'.-(\':n c;u-t U'if' ilr.-vi i

lfad]|ipar--(«fbir»fl^<>bi(ib«n'>«aiiid;âad'^.|^^ TTTT- t lfaltioolol»ed olay and g r i t , aoawhar^ps

-O-'A-if. 1') ' - { '

%

„ J

Solid bla^le a lay

Very fine g r i ^ sand - d i r t y

so l id blaâc a3.ay

f i ^ J t ^ a a H i i hTft^lr gjlfcy w i t h sfcrwAks of f l aw

Solid blaak olay yE'z. Salld blaok olay wlth.,fl!^^faâ,:<^, 1%^^.,.^^^ ,•111

Fine medlufi ooarae gray aaad^ g r i t a , ao«e olay .11 ( .'II,.!;.'! o < * y

Solid biaak oJLay and atreaka of aand

Madiam aofra^ aaad with atraaka of olay so l id blank dlay

Coarao grMy apnd, g r i t a,, with atraaka of olay

Solid gray olpty iftth. atreaka of f ine aand

Coarae gray n n d and g r i t , aoae olay

Solid brown oây

Oreett JJarSj. (Stolid Ctarwen Clay) Maaitaqttan fowMtttan

WELREC 112 2422

MtA|KiMNe f01|># ) ;'ivi

o i , , . TtiarftBiO

^ -.n. y.f'.i ri!qi»a

. i l . k::i.. b r i . l aitcja

G" - # r ^ ^ • i - -Ttr .,.,4!S..

-•^,,-,L.,,,t.,a&l. :^ ' ! ! : ' T " " ^ • r

1 • 'S:^

WELREC 112 2423

G

G

G

G

G

G

FORM 8 7 .

i ; .

DEPARTMENT OF CONSERVATION Permit N O . ^ ^ - ^ 3 2 ^ < ^

^ \ 0 AND ECONOMIC DEVELOPMENT Appl icat ion Ho.

^ ^ A ^ DIVISION OF WATER POLICY & SUPPLY County ' r 7 :,

^ WELL RECORD t

I . OWNER g r a n k M u l l e r ADDRESS B l a n s i n g Rd. ManaBguan W. ,T.

O w n e r ' s We l l No. SURFACE ELEV'ATION . ^ _ _ ^ F e e t {Aho-ve m e a n s e a l e v e l )

2. IQr.ATIOH B l a n s i n g R<i. MaBawgtiat i V. .T. ._

3. DATE COMPLETED _ _ ^ Z 4 DRILLER ^ r e d D e n n J n

DIAMETER: t o p ^ i ^ l ! L _ I nches B o t t o n _ i ! ! l _ l n c h e s TOTAL DEPTH _ j 4 2 . ^ _ _ _ F e e t

5. CASING: Tyofi s t e e l D i a n i e t e r _ J i ! ! ] _ _ l n c h e s Length ^ f l * F P a t

5. SCRFFN: typfi ? ^ i n t Opening # 6 0 : . Diameter 1 ^ I n c h e s Length ^ F a e t

Feet Geologic Formation ( T o p _

I Bottc R a n g e

:om Feet

T a i l p i e c e . D iame te r Inches Length Feet

WELL FLOWS NATURALLY Ga l l ons per M ino te a t Fee t above s u r f a c e

Wa te r r i s e s t o [ Fee t above s u r f a c e

RECORD OF TEST: na te Jây Y i e l d _ _ _ _ _ 5 G a l l o n s per m i n u t e

S t a t i c w a t e r l e v e l b e f o r e pumping 4 2 Fee t below s u r f a c e

Pumping l e v e l f e e t below s u r f a c e a f t e r _ h o u r s p u m p i n g

Drawdown Fee t S p e c i f i c Capac i t y Gals, per min. per f t . of drawdown

How Pumped P o r t a b l e n u a n How measured ' ^ G a l C o n t a i n e r

Observed e f f e c t on nearby w e l l s


Type M f r s . Name ,

C a p a c i t y G.P.M. How Dr i ven H . P R.P.M,

Depth o f Pump i n w e l l Feet Depth o f F o o t p i e c e in w e l l F e e t

Dep th o f A i r L i ne i n w e l l Feet Depth o f Meter on Pump

10. USED FOR AMOUNT Average G a l l o n s D a i l y

Maximum _ _ 6 a l l o n s D a i l y

1 1 . QUALITY OF WATER _ _ _ £ £ 0 d Sample: Yes No

12.

T a s t e __SOOd Odor n o n e Color ctlc^si-r Temp : .°F

I na o n "hâck ^ ê s amples a v a i l a b l e ( G i v e d e t a i l s on b a c k o f s h e e t o r on s e p a r a t e s h e e t . I f e l e c t r i c l o g w a s m a d e , p l e a s e

f u r n i s h c o p y )

13. SOURCE OF DATA

m . DATA OBTAINED BY _ _ _ ^ _ Date

( N O T E : U s e o t h e r a i d e o f t h i s s h e e t f o r a d d i t i o n a l i n f o r m a t i o n s u c h a s l o g o f m a t e r i a l s p e n e t r a t e d , a n a l y s i s o f t h e w a t e r , s k e t c h m a p , s k e t c h o f s p e c i a l e a s i n g a r r a n g e m e n t s e t c . )

^ N o t e : » h i s w e l l was d r i l l e d by C * . LaTUoan <* C o . , Aug. l b , 1957 . 8 " DLa. 1^7' d e e p . Our p r e s e n t work c o n s i s t e d o f p u l l i n g

^MMC7 punp, t e s t ing axid developing well , to e lbnia t te sftnd .oonditloa. OEPAItiNQiT €F «OilQ|VATlM Nmjj^Jt^JtSSl0^|2L

r-^Jgtf-

t i / NV^

i , MHQt l a t t g t t ShODi^Jlg 0 » a t T a » H M t o t a a ^Ti ^ 1 1 " •^^ ' Ogo»« Coonfcy Oagfeer

•«a«r«a M M l » . ^ SURFACE ELEVATIOi § 2 . F « « t

i . LoeATIW ^l j?t t l» g i a « a S h o p p i n s 0<igfc«gt liMiMqo*n» J . J .

1 . MTC CWPLEtCD .. LOKIUER ^ - -. -

«. i 1 M € T B | : t e a . . . _ . . l « e k « « • • t t M a . . _ « * l « e l i « « TflTW. aCFW F<et

6. eaaiMfc T«« ( t e t t M F^«t

G,. Ta i l »tae«f MmmmUr....,^ ^.laekai ^ ' " t t * ^ «*«•

« E U F L i M i f tTMiLLY t a t U a * par Nlaata «• Fact ateva a a r f a e a

Vatar rtaaa * • f » » * akava aar faea . . \

^8. I I C M 0 # ^ni 'T ' •«*« Y l a N ^tallaaa M r a l a a t a

t t a t i c w a t a r l a V a l ^ i ^ r * y » t « f , - • • ><i;>* kalaw a a r f a a a

Faaplaf «^*"« * • • • bate* aarfaea • * * * * , fc»«r« t a a i l i i

*—"'* ' ' ' *• ' * * * Spaeif ie CaMci ty , . .,. .tala. par aia. par f t . af dnwdMni

••M »M»—^ .,: , . low aaaaar^^ . , • •

fkaarvatf a f f a « t oa aaarky wal la

I « . FERMMiaiT F IMFMM EQUIFIIEIfT:

G

G

* r M • :' • • • ' : • ' : N f r a . t

l immMtt t iy -V. |--. .-:.a.»îi. aew f r i vaa I . F . . t . P . N . _ ^

•apth a f * | f f *":.fr^*^*-; 4 , ^ : " * * ^ * * * ' *^ Faatplaea la wa l t . ^ . . ^^ _ . „ . . — N a t

t ap th af il|>^ i l i laa: i^%fM£i^ Faat Type o f Natar aa Faap ^ . . ^ t 1 i a . ^ l a e l i a a

\ i ta i i iaaa • a l l a a a l a i I y

I I . ^ I l i i n y HP » * g a Sa«p1a:Yaa-^ la>

• < : • pn - t ^ ( * * • " < * a«i ia<« t a l l y

T * * * ^ 0 4 a r _ _ Cal.er.^ _______ Taip..

12. LOG , -i • Ara saaplaa avadab la? fWlr* ^ t m i t t i »m t a c t • / «A««( a r ^m m t p t r m f mh*9t. i t a i t t r i * i » e 9m» rnrnH:, wlamam

tmral t tk apinr} y

13. SOURCtOFiATA

L n . DATA mAWED BY K a j ^ WÛ 3?r3,lliJBg. I n c . P«ta J toie 7 . 1066 /•wori

-1 WELREC 112 2424

May 18 to June l, 1966 ^ * ^ 5 ^ t ^ i ^ l « ^ 25 H.P. aPurbini, bidlad «3bi Wfi»d i w S l / ^ d r t e d ftCX) llp.tl9»r «eid, suvmd^«ad lMda.#a «*3;l iuLln, and diiT9los«d;

. - I- _->«i-

lltairted tas t a t 1^0 fflv, nitli | i aa^ aaxid. abated for 3 daja, startJjig aad ato^?ipi% puap, and en naaa. t aa t , piuq»d 400.0»,- aand jbraa water.

KJaye Well O d l l i x i g , I n c .

c c G^

G

• • > : ' •''• . • i . « .

-'':m

- * f » I

• } • • - ' - « - ^ f

#

50..,. m

i •." ^Ô

f n

* ^ 1*1

^

r,.a n -"JSPOI

WELREC 112 2425

? S S' -33 6/5 ^.rmDWR-138 :>- STATE OF NEW JERSEY ^ , , r.-lSp

DEPARTMENT OF ENVIRONMENTAL PROTECTION PERMIT NO. o<H'~ I f O / A \ J I % DIVISION OF WATER RESOURCES

APPLICATION NO. N

I ' ^Â ^ ^ • ^ ^ • ~ '

1. OWNER "0/4-mb hr) <0 ^'McDoncJci^ LnnRF^^^^/6 M f / u . ^ ^ 3 ^ Jâ)^^.yjff^W

Owner's Well No. ' SURFACE ELEVATION '. Feet Pt/J <->v y U l i ^ I - , ' I 'o*'"''® '"ean sea level)

2. LOCATION ///cT>>ir\cJt(y> /Tr, ^ ^ 3 ^ f y ^ f l f^(î^\h^p 3. nATFrnMPiFTFn / ^ / U - ^ / l 2 9 ^ H ? < DRII i FR TUHlrvAc. C N t i r r \ < : , y \ :

4. DIAMETER: Top_^£__ inches Bottom _ y i _ _ inches TOTAL DEPTH ^ d " •. Feet

5. nA.qiIMn- Typp U L Q C K O ^ f ^ . Diameter _ 2 _ _ _ Inches I sngth / O - { Feet

6. SCREEN: Typp O - ^ Ri7P nf Oppning / C s S L o T niamPtBr f Inrhes Length a _

Top r_ Feet n A / t v ^ X f Geologic Formation ( 0^0 l Ct. y

Bottom ^ ^ Feet / /

U.'' JO ^ / Tail Piece: D iame te r___x l Inches Length__1 Feet

7. WELL FLOWS NATURALLY Gallons per minute at Feet above surface

Water rises to , t Feet above surface

8. RECORD OF TEST: DatP 3 / Z - 9 / J ^ / YJPIH " & Gallons per minute

_Feet

I Static water level before pumping v.? O -. : Feet below surface

Pumping level ^ feet below surface after : hours pumping

I Drawdown ^ Feet Specific Capacity " ^ Gals, per min. per ft. of drawdown

How pumped ^Cf tS* How measured w J 7 K . V . i ^ ^ l C ^

Observed effect on nearby wells S\l0i0G 9. PERMANENT PUMPING EQUIPMENT:

[ Type S u i ^ , Mfrs. Name C S O O P c t ^

Capacity ' ^ G.P.M. How Driven ^ f c ^ f ^ i C H.P. - ^ / f R.P.M. i ^ Q O

Depth of Pump in well "-^ ^ Feet Depth of Footpiece in well Feet

Depth of Air Line in well Feet Type of Meter on Pump ' Size Inches

T ^ C? <? I C A - t - 1 / I X I f A v e r a g e O ^ O Gallons Daily .0. USED FOR X ^N I v:) n i \ u i \ i AMOUNT ] ^ ^ ^

I Maximum/ ^ ^ K J Gallons Daily

1. QUALITY OF WATER Sample: Yes No

: T a s t e C ^ O < ^ I ^ O d o r M l ^ ^ £ _ _ _ C o l o r _ C U ^ i ^ _ _ _ T e m p . ^ I Z L . ^F.

2. LOG Cx/V ^Pj/Kyr\ Are samples available? (Give devils on back of sheet or on separate sheet If electric log was made, please furnish copy.)

13. SOURCE OF DATA . - U ^ M j / f f ^ ^ , ,

4. DATA OBTAINED e / ^ ^ / l ^ i SAjPei^SO^ n.t. ^ A i V ^ /

(NO TE: Use other side of this sheet for additional information such as log of materials penetrated, analysis of the water, sketch map, sketch of special casing arrangements, etc.)

'm^'^'''^^^ y STATE OF NEW JERSEY ' " ' ^ •''.:>'?.•)« , DEPARTMENT OF ENVIRONMENTAL PROTECTION PERMIT NO. J2L3j=J.25£fl_

DIVISION OF WATER RESOURCES APPLICATION NO.

- ^ O m y ^ ^ WELL RECORD ^ ^ ^ ' d ^ ,,,,,, Monmouth

I. nwNFR Waldick Aerospace Devices ArnRF«;<; Wall Two. . N.J. 07719

Owner's Well No. n b g , # 2 : SURFACE ELEVATION , _ _ _ _ F e e t _ , iAbO¥» m«»n iM hvtO

. . ^..>.^.^... Same a s above >. LOCATION

3. pATF roMP i FTFn 1 - 1 4 - 8 3 DRILLER A . C . Sr.HHT.TRS & S O N S , I N C ,

" l . DIAMETER: T o p _ _ 4 ^ inches Bottom 4 inches TOTAL DEPTH 1 ? F „ j

5. CASING: Typp P . V . C . . Diameter 2 - ' " c h e * Length_25—_^_Feet • ^ • ^ ' Size of Opening _z .9 .20 Diameter i _ Inches Length _ J J L _ _ _ F e e t

G 7

G

G

G

{ Tnp 2 2 ' 6 " Feet

Range in Depth ^ Geologic Formation Bottom 3 2 ' 6 " Feet

Tail Piece: Diameter _ ^ Inches Length Feet

7. WELL FLOWS NATURALLY Gallons per minute at Feet above surface •


8. RECORD OF TEST: Date Yield Gallons per minute

Static water level before pumping Feet below surface


Drawdown •. Feet Specific Capacity . Gals, per min. per f t . of drawdown

How pumped How measured .


). PERMANENT PUMPING EQUIPMENT:

Type Mfrs. Name , :

Capacity '. G.P.M. How Driven H.P. R.P.M.

Depth of Pump in well Feet Depth of Footpiece in well Feet

Depth of Air Line in well Feet Type of Meter on Pump Size Inches

" -,. . . f Average Gallons Daily

10. USED FOR O b s e r v a t i o n AMOUNT i ^Maximum Gallons Daily

QUALITY OF WATER Sample: Yes No

Taste Odor Color . ::;: Temp. ° F .

LOG ffîa a- i -^^r -hQ>^ _ __._ ; .. Are samples available? (Gi¥* detail! on back of sheet or on separate sheet. If electric log was made, please furnish copy.)

' \ SOURCE OF DATA D r i l l e r ' s L o g _

':. DATA OBTAINED BY A . C . .qCHTTT.TRR/Bi T l . T o f f o > - y e Date ^ - ' ) ^ - a 7 ^

(NO TE: Use other side o f this sheet for additional Information such as log o f materials penetrated, analysis of the water, sketch map. sketch of special casing arrangements, etc.)

WELREC 112 1638

G

C

G

G

b" s t e e l P ipe & ( ••

GROUNC

X 1- =

-1 ro

o

1

o: III z

2 '

'

1

r

*

4 "

- •—CASING—»•

P.V.C.

^ p Q , A.C.OCHULT

29 '33 -37 ) rES & SONa INC. . ^ ^ . ^

, 2 '6 " SINGLE CASE WELL ^ * ^ - U ^ ^

WELL LOG

1 F i l l

Tan sand

Stones & sand

Brown sand , c l a y i s h

F E E T FROM GROUND

SURFACE

0 TO 5

5 15

15 20

20 33

'

NAME OF OWNER

WfVLDICK AEROSPACE DEVICES

Job ' IQ^ f i ?

Location R t . 35 , W a l l Twp. N.

Well No. Ctos. #2

Hr». PumpedBlowed 2 H r s .

Copocify G.P.M. 3

Stotic Leve l 1 7 ' 4 "

Pumping Leve l

Speci f ic Copocity

Diam«»erofw«ii 10" h o l e 4 "P ipe

Depth of Well (ground) 3 2 ' 6 "

Length of Casing ^ 3

Dis tance to Top of Packer (gr.)

Type Screen S l o t t e d P . V . C .

S i x e o l Screen 4 " P i p e S l z e

Length of Screen 1 0

Top Screen F i r t i ng M . l .

Boltom Screen F i t t i ng P l U g

Blank

Slot Size . 0 2 0

D r i l l i n g Machine No. # 7

Driller A . Haniiond

G„. , , Yes M o r i e #1

Bogs of Cement 9

Dole Well Completed 1 - 1 4 - 8 3

^

Rotary Table opprox. 3' obove ground leve l

FORM 300

WELREC 112 1639

TiDWR-138 . . . . . STATE OF NEVfV JERSEY 10 DEPARTMENT OF ENVIRONMENTAL PROTECTION PERMIT NO. P Q - I :>'^fi1


WELL RECORD <^ ' " ^ ^ ^ ' rnn^Tv Monmouth WELL RECORD ^ ^ ^ ^ ^ ^ ^

OWNER W a l d i n k flernspacp DevicQC Annppgg W a l l Twp. N . J . 07719

Owner's Well No. O b s . # 3 SURFACE ELEVATION , P x t (Above mean see level)

LOCATION Sctme as s±>ove 3: DATE COMPLETED ^ - 1 8 - 8 3 DRILLER A - C SCHULTES & SONS, I N C .

~ DIAMETER: T o p _ _ 4 _ _ inches Bottom 4 inrhBt TOTAL DEPTH i 3 Feet P . V . C . . _ -

3 CASING: Type : Diameter _ 2 Inches Length_zJ!2___Feet

R- SCREEN: Typg P • V • C . Size of Opening _ IOL?.0 Diameter _ i Inches L e n g t h _ l J [ l _ _ F e « t

C [

Top 2 3 Feet Range in Depth { Geologic Formation

Bottom 3 3 Feet

Tail Piece: Diameter Inches Length Jêet

7. WELL FLOWS NATURALLY Gallons per minute at Feet above surface

Water rises to : Feet above surface

8'. RECORD OF TEST: Date Yield Gallons per minute



Drawdown Feet. Specific Capacity Gals, per min. per f t . of drawdown

How pumped How measured


[ [


Type Mfrs. Name : \

Capacity G.P.M. How Driven H.P. R.P.M.


Depth of Air Line in well Feet Type of Meter on Pump Size Inches

( Average Gallons Daily

Maximum Gallons Daily

QUALITY OF WATER Sample: Yes No

Taste Odor Color Temp. ° F .

LOG .q<=>p Af--t-ar;h*^H Are samples available? (Give tiatails on beck of sheet or on separate sheet If electric log was made, please turnip copy.)

^ SOURCE OF DATA D r i l l e r ' s Log

DATAORTAiNFnRV A . C . SCHULTES/BJ l l J e f f e r v s °" Date __JLr21=flJ3

(NO TE: Use other side of this sheet for additional infonnation such as log of materials penetrated, analysis of the water, sketch map. sketch of special casing arrangements, etc.)

WELREC 112 1640,

[

[

Cas

GROUNl

1 .

Ln

1

z l -

- 1

o

ir

. z o ;

r

g & Cap

4 " . « — C A S I N C - * -

P.V.C.

_ A.C.OCHULT rES & SONS INC. ^ ^ 1 ^ ^ ' ^ . i

1 . . v . . S'^GLE CASE WELL ^ ^ 3 ^ . 3 ^ ^

WELL LOG

F i l l

Tan sand

Sand & g r a v e l

Sand, v e l l c w

Sand & g r a v e l

Sand, y e l l c w

1

FEET FROM GROUND

SURFACE

O T O 3

3 8

8 13

13 20

20 27

27 34

NAME OF OWNER

WALDICK AEROSPACE DEVICES

Job ••: 19362

Locotion R t . 35 W a l l Twp . , NJ

Well No. O K Q . « ^

Hrs . Pumped B l C W 1*5 H r S .

Capoci ty G.P.M. 5

Stotic Leve l 1 7 ' 0 "

Pumping Leve l

Speci f ic Capaci ty

D iomete , o( Well 1 0 " h o l e 4 " P i p

Depth of Well (ground) 3 3

Length o l Cos ing ^ ^

Dtstonce to Top o( Paclter (gr.)

Type Screen S l O t t e d

S i , . o( <;.,—„ 4 " P i p e

Length of Screen -LU

.r , =, . M . T . l o p screen t - i t t i ng

Bottom Screen F i t t i ng P l U C f

Blonk

Slot Size . 0 2 0

D r i l l i n g Mochine No. # 7

Driller A . Hainmond

Grovel Yes #1 M o r i e G r a v e l

Bogs of Cement O

Dote Well Completed 1 - 1 8 - 8 3

Rotory Table opprox. 3' above ground level

WELREC 112 1641'

(V) ,k^ 0"

f j ' d ' - K

a'i - 33 ^11 / no" " * ' " ' ' ^ ^ STATE OF NEW JERSEY 2 9 - 1 2 5 6 2 "*" DEPARTMENT OF ENVIRONMENTAL PROTECTION PERMIT Mf>


WELL RECORD l^^^^ 3^^ COUNTY Monmouth

I. OWNER Waldick Aerospace Devices AnnREs.«! Wall Twp., N.J. 07719

Owner's Well Nn O b S . # 4

I. LOCATION Same as above

Owner's Well No. O b S . # 4 SURFACE ELEVATION , Foot (Above mean sea level)

T o p _ r 2 Feet Range in Depth i 3 3 Geologic Formation

Bottom Feet

c

3. DATE COMPLETED _ _ l l i ± : 1 3 DRILLER A . C . S C H U L T E S & S O N S , I N C .

~ l . DIAMETER: T o p _ _ 4 _ i n c h e s Bottom _ _ 4 _ _ inches TOTAL DEPTH 1 3 Feet

6. CASING: Typg P . V . P . Diameter 4 Inches L e n g t h _ 2 5 _ _ _ F e e t

'5. SCREEN: Typg P . V . C . Size of Opening _i.22^0 Diameter _ _ _ * Inches Length _ iO____Fee t ,

th i

r ^ Tail Piece: Diameter Inches Length Feet

7. WELL FLOWS NATURALLY Gallons per minute at \ Feet above surface


8. RECORD OF TEST: Date Yield Gallons per minute



Drawdown Feet Specific Capacity Gals, per min. per f t . of drawdown

How pumped How measured i_


i. PERMANENT PUMPING EQUIPMENT:

Type Mfrs. Name .

Capacity G.P.M. How Driven H.P. R.P.M.


Depth of Air Line in well Feet Type of Meter on Pump Size inches

_ , . . , Average Gallons Daily

10. USED FOR O b s e r v a t i o n AMOUNT

0

f Avera

Maxin Maximum Gallons Daily

.A. QUALITY OF WATER Sample: Yes No

Taste Odor Color Temp. "F.

J . I c\n S e e A t t a c h e d Are samples available?

(Give details on back of sheet or on separate sheet If electric log was made, please furnish copy.)

T SOURCE OF DATA D r i l l e r ' s L o g

A. DATA QBTAiNFn BY A . C . S C H U L T E S / B i l l J e f f e r y s n, t . l r - 2 1 r . 8 3

(NO TE: Use other side of this sheet for additional information such as log of materials penetrated, analysis of the water, sketch map, sketch o f special casing arrangements, etc.)

WELREC 112 1642

c [

3" S t e e l •

GROUN 3

TO

TA

L

DE

PT

H

- F

T.

33

'

o 5 C >

'

0

1

Pipe & Cap ^

1

4 " - • - C A S I N G - * -

. E . V . X . . . .

=_

_ A . C . O C H U L . ' ]

2 9-33 .39; ?ES&SONaiNC. _oa /jjo-.^

,2* SINGLE CASE WELL J ^ I '^^J, < t LEVEL Z ' ^ ' 3 3 . 3 1 1

WELL LOG

Top s o i l

F i l l

Sand

G r a v e l & sand

Tand sand

Brown sand

C l a y i s h sand

Y e l l o w c l a y i s h sand

F E E T FROM GROUND

SURFACE

0 TO 1

1 3

3 6

6 11

11 19

19 22

22 26

26 34

NAME OF OWNER

WAIDICK AEROSPACE DEVICES

Job« 19362

LocoiioRt. 35 , W a l l Twp. N .J

Well No. Obs. #4

Hr,. Pumped Slowed 15 H r s .

Capaci ty G.P.M. 5

S.aric Leve l 1 6 ' 9 "

Pumping Leve l

Specif ic Copocity

4 "

Diomeler of Well 1 0 " H o l e & P i p e

Depth of Well (ground) 3 3 '

Length of Cos ing ^ ^

Dis tance to Top of Packer (gr.)

Type Screen S l o t t e d P . V . C .

Size of Screen 4 P X p e

Length of Screen i .U

Top Screen F i t t i n g F . T .

Bottom Screen F i t t i ng P l U ^

Blank

Slot Size ,020

D r i l l i n g Mochine No. # 7

Driller A . Haimond

Grovel #1 M o r i e

Bags of Cement 9

Date Well Completed J a n 1 9 8 3

Rotary Tab le opprox. 3' obove ground level

WELREC 112 1643

so* . '•^ssea^gBsg^

HanclGx ^ q . 3 3 . 0 i /

BORING LOG Well No. ?

HANDEX CORP., 703 Ginesi Drive, Morganvi l le , New Jersey 07751 (201) 53i

Application No. 2.^,35.611

Date Drilled Mat/ 7 4. \ n ^ County Location Rou.t£ 35 (x.nd Mayuuguan (UA-dlz, MayuL6qaa.n, Maw JgA6

Uomoatk Permit No.

Use £4L

Owner SkoZl Olt Compa.nu 4>otid augeAJ, Drillinq Method

Hole Diameter Casing:

Type ScrBcn*

Type" ?VC SchzduZz 40

Address fUc-f t. On^ngp, Mm 7o/rAPu

S" Sampling IVIettiod dutt lngi

PVC SckzduZz 40

Gravel Pack Size _ Static Water Level

#7 S l o t ^ l

Diameter

Diameter

4"

Total Deptti

Length

15'

5'

4" Casing.Seal ^ b&ntoyuxe.

Length 10'

Geologic Formation ê-d&n^ DEPTH BELOW

SURFACE

10'

20'

30'

SAMPLE NUMBER

BLOWS PER 6" ON SAMPLER

WELL DESIGN

S

IDENTIFICATION OF SOILS/REMARKS

0 ' -3 '6" OAjCULgz bn.ou}n meiLijum to ^^m SAMV, tfiacz 6Alt, tAacz- iZviz QM.veJL

3 '6"-4 '6" V(VLk bn.om mzcUjutm to i l nz SANV, t U t l z - hUX fvxdz- iiyiQ. gA.aveZ

4 '6" -7 ' OAjdngz bfiown mzcUum to ^Znz SANV, t/ixLcz- iZnz QnjxvzL, tHjuaz 4xXt

7 ' -S ' Ofia.Y\QZ bKoWYi doaJtMZ to £Znz SANV, Lut t t z - £X.nz gAavzt, tAJxaz iXZt

S'-15' Onjxngz bfiovsn. mzdUim to { Znz SAW, tnjxdz- i XJLt, tAuzz ^ynz gnjvjoZ

NOTE: ilJzt cut W , no gcu

15' Gfizy hn.oviYi medium to ÎYIZ SANV, tUXtz+ 6AZt, 4,(xtuAxitzd, no gtu

0

"^SSH^SfSSy l-janclcx

J ^ 33^'.'

BORING LOG Well No. z

HANDEX CORP., 703 Ginesi Drive, Morganville, New Jersey 07751 (201) 536

g.q ^S. i ^ l )

_ Application No Permit No 29-7 3706 County Moymoath Date Drilled Mat/ u . 19s

Location Roatz 35 and Mayuuqaan tAAcZZf anaj>qujcx.n. New JzAA Use monltofi

Owner skziz oyt comvcinu Drillinq Method ô tcd aage^ Hole Diameter I!! Casing:

Type Pl C SckzduZz 40 Screen:

type Pl/C Sdhzdulz 40

m-AddreSS fiJe^t OJumaz. Now J z u z u Sampling Method aatt'Lna^


#7 i w

Slot zg Diameter Casing.Seal • bzrvtonAjiz

Total Depth

Diameter 4" Length

Length

16'

6'

4" 10'

Geologic Formation A.zcznt

[

c

[

DEPTH BELOW

SURFACE

10'

10'

30'

SAMPLE NUMBER


WELL DESIGN

•a)

CO

3


0 ' -3 ' light b OMn aoouuz to i lnz SAMD, LUtlz mzdium to {Ajfiz g/iavzt, tîacz 6i£t

3 '-7 ' Onxingz hKown mzdMm to ^Znz SANV, tnxidz- iînz gKOLvzZ, tnacz i ^ l t

T-13 ' Onjoungz bn.oiaYi mzdUim to iZnz SANV, t;ra.c.z+ i-iZt, tnacz t -cne gnxweZ

13'-H' Van.k gfizy c- a.yzy SILT, 6omz- mzdMm to {i.nz .iand, tnjxdz {inz gA/wzt

NOTE: No g(i6otLnz

z S« HandGX 5 3 u- I)

BORING LOG Well No 3

HANDEX CORP., 703 Ginesi Drive, Morganvil le. New Jersey 07751 (201) 536-8500

Application No. ^''•^^'^" Permit No z9-73707 Mat/ 74. 7 9g4 County \honmovjtk Use moncton. Date Drilled.

Location RouXz 35 and U.(j.YWL6qujxn tin.zLz. MancUQCuin, Nm Je/uzi^ Owner SkzLt OAJL Commny Drillina Method Hole Diameter Casing:

Typfi PVC SchzduZz 40 Screen:

Type Pl'C Schedalz 40

i o t i d auozfU) Address ^ ^ ^ Oiangz, New Jziuzy

8" Sampling Method cuttlngi

Diameter


#7 U '

Slot ^ 1 ^ _ Diameter Casing.Seal bzntonitz

_ Total Depth U L

f L _ Length 5'

4" Length '' ô'

Geologic FonTiation êcznt DEPTH BELOW

SURFACE

10'

10'

30'

SAMPLE NUMBER


WELL DESIGN

tn

3

J


0' -14 ' On.angz bAown mzdum to ^ inz SANV, tAazz ^-inz grave l , tfvxcz 6AIX.

14 ' - IS ' VoJik gn.zy bAouin oAangz SILT, lozt, ômz+ mexium to ^Znz Aand

NOTE: No odon.

J ^

^ 3 - HandGX 3^,' u ' l

HANDEX CORP., 703 Ginesi Drive, Morganville, New Jersey 07751 (201) 536-8500

Application No. ^ ' ^ • ^ ^ • ^ " Permit No. 29-7370^ Date Drilled May 74^ 79g4 County Monmouth Use mnv^Jtn}, Location P-oatz 35 and Mayuuqaan CAACIZ, Mayuuquan, New Jziuzy

BORING LOG Well No 4

Owner ShelZ on. C(mpanu _rillinq Method Hole Diameter _ Casing:

Screen: Type ^^c SckzduZz 40

Address i)}eAt Ofiangz, New J z u z a Aoild cuigeAA

S" Sampling Method cuittlng.&

19'

PVC SchzduZz 40 Diameter


»i Slot 20 Diameter Casing. Seal bznton i tz

_ Total Depth

1 1 _ Length ^ 9'

i ! L _ Length ^J1.

Geologic Formation -tac^ni

DEPTH BELOW

SURFACE

10'

20'

30'

SAMPLE NUMBER

1


WELL DESIGN

3


0 ' -4 ' OAJingz bAown mzdUbm to Înz SANV, Zl t tZz mzdLam to ^Znz gfiavzt, txjazz -iiZt

4 ' - 5 ' Laye/u o^ black clayzy SILT, 4>omz mzcUwn to IZnz iand

5'-10' Tan mzdMm to ^Znz SANV, t/iacz ^Mnz gAaveZ, tAa.cz &iZt

10'-15'-^ BAouin mzdMm to înz SANV, tAacz+ i i Z t , tnjacz

iMnz gnxvjeZ

NOTE: Wzt a t 1 1 ' , ga&oZMnz odoA

IS ' -19 ' Bôwn mzdMxm t o i l n z SANV, l U t l z + iUX, tAa.cz i Jê gAjjL\jeZ

http://tAa.cz

http://tAa.cz

\e '

yc^ l-jandGx BORING LOG Well No.

HANDEX CORP. 703 Ginesi Drive, Morganville, New Jersey 07751 (201) 535-851

Aoolication No. m May 14. 19S4 County Mo mouth Permit No.

Use 29-13109

Date Dr i l led, ^ Location Rou-te 35 and Uana&qaan COicZz. Mana^qaan. New Jejuzu Owner Ske£J o n Cnmpnv u Address ^<î OAangz, New Jzfuzy

mpyUtoA

4>oLcd (xuazu Drillinq Method Hole Diameter Casing:

Typp PVC SchzduZz 40 Screen:

Typp PVC ScheduZz 40

B" Sampling Method

Diameter

cutting^

-To ta l Depth

JH Length

17'


#7 » / i l l -9'6

Slot 20 Diameter 4" Length U L Casing.Seal . bzntonMtz Geologic Formation Azcznt

DEPTH BELOW

SURFACE

10'

10'

30'

SAMPLE NUMBER

„


WELL DESIGN

CO

3


O'-l ' BAoiJOn cZayzy SILT, 4ome mzdMm to {y.nz ând, t i t tZz mzdMm to \Mnz gAaveZ

l ' -13 ' Onangz bAown mzdMrn to i-inz SANV, tM.cz îZt, tAacz £Znz gAaveZ

13'-17' ' Po/Lfe gAzy cZayzy SILT and medMm to iZnz SANV, tnxLCZ ^Znz gAaveZ

http://tM.cz

Form DWR- 138 11/80

c

[

[

5 ^

Coord; STATE OF NEW JERSEY

DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER RESOURCES

WELL RECORD

2933611

PERMIT NO. .

APPLICATIOr^C^j

2914962

.muuLIi' COUNTY.

1. OWNER MCKAY, MATT 1106 NEW BRUNSWICK AVE.

ADDRESS

Owner's Well No. SURFACE ELEVATION

2. LOCATION L o t : 3&4 B l o c k : 303

3. DATE COMPLETED ^ ~'-3 ^ - ^ cS

Municipality: Wall Twp i**'"'*'" an ea/e.«/;

~ Tiger Construction corp.

-Feet

. ^ 4. DIAMETER: Top.

5. CASING: Typs P V C

6) SCREEN: Type J c i A K i i .

inches Bottom

DRILLER

&4. inches

Diameter X

Range in Depth { Top.

_ Size of Opening i_CZ.7 Diameter ssfei

<>ir7i 5 "— Feet

TOTAL DEPTH.

. Inches

Inches

' ( s ^ i >y> Feet

Length A l l_Xi j5ZFeet

Length / O Fppt

Bottom (r, 1 , S ^ Feet. Geologic Formation f r i U i ^ ^ g L i^

Tail Piece: Diameter. Inches Length.


Water rises to

Gallons per minute at.

Feet above surface

8. RECORD OF TEST: Date - 1 - ^ - 9 : . ^ Yield. J-O.

-Feet

Feet above surface

Gallons per minute


Pumping level / ^ t>

Drawdown / \ Feet

.2J. feet below surface after

Feet below surface

hours pumping

Specific Capacity. ^.5 How pumped C\\ R How measured

Gals, per min. per ft. of drawdown

XfiL

Observed effect on nearby wells n QK e


Type Î(JJ .\-e:T-

Capacity ^ 5 " G.P.M,

Mfrs. Name .

Depth of Pump in well

10. USED FOR

Depth of Air Line in well

How Driven / " ^ f e 0 1 ^ . ( 0 H.P.

Feet Depth of Footpiece in well

Feet Type of Meter on Pump Size.

R.P.M. > j ^ . ^ O

Feet

Inches

i ^ Or\ AMOUNT

11. QUALITY OF WATER

Taste

12. LOG On G^ftd^ Odor. Color.

( Average g L G O O Gallons Daily

Maximum ^ D O ^ Gallons Daily

Sample: Yes No ' — "

Temp. OF.

(Give details on back of sheet or on separate sheet I f electric log was made, please furnish copy.)

13. SOURCE OF DATA t N g 1 W e d

14. DATA OBTAIN

Are samples available? Jin..

lEDBY ^ ^ v \ V \ \ ^ ~ ^ , \ ^ ^ \ j \ l Date 7 A><7 , I 9 ^ S -

(NO TE: Use other side of this sheet for additional information such as log of materials penetrated, analysis of the virater, sketch map, sketch of special casing arrangements, etc.)

[ [ c L [

Form DWR- 138 11/80

i-OR IRRIGATION PURPOSES ONLY

1. OWNER KURMIN, ARNOLD

STATE OF NEW JERSEY C o o r d : 2 9 3 3 2 9 9 DEPARTMENT OF ENVIRONMENTAL PROTECTION PERMIT NO. ?QT ' ^ 0 5 4


WELL RECORD p r l ' l - ^ ^

APPLICATION NO.

COUNTY Monmouth

ADDRESS MEETING HOUSE RD.

Owner's Well No . . / SURFACE ELEVATION (Above mean sea level)

-Feet

2. LOCATION L o t : 32 Block: 807 Municipality: Wall Twp.

3. DATE COMPLETED

4. D I A M E T E R : T o p . ^

.f^Xy^-^ inches

DRILLER C r e s t v i e w Well D r i l l i n q

ot tom . inches

Diameter 5. CASING: T ^ p j ^ / C & ^ J ^ ^ ^ ~ ^ ^ / .»....v>.. . - . ^ c / ^ ^ ^ ^ X - r ^ A ^ - .*:^*^^/<i<2r" ^ y ( x .

~ ~ Size o f O p e n i n ( y l i l £ l ± ^ Diameter / / ^ ^ I

T O T A L DEPTH.

^ Inches

SB

6j SCREEN: Type

Range in Depth

^ ^ S - .

{ T o p . ^

Inches

2^ Bottom ^ ^

Feet

Feet

Tail Piece: Diameter. - ^ Inches

Geologic Formation

/ ' 7

/^y^^-Ay

Feet

Length / ><^ Ffpt

Length _ ^ 2 _ ^ Z _ F e e t

/ ' / Length. -Feet

WELL FLOWS N A T U R A L L Y

Water rises to

Gallons per minute at . Feet above surface

, Feet above surface

8. RECORD OF TEST: Date J ^ / ^ / / ^ J ^ Yield _ Z ^ Gallons per minute


Pumping level

Drawdown

2£_ ^

How pumped ^ ^ ' ^

_ feet below surface after

Feet Specific Rapacity

. Feet below surface

hours pumping

Gals, per min . per f j..pf drawdpwn

^ / T ' f ^ How measured < 5 ^ ^ ' C A ) ' ^ / y y ^ / y ? y ' < $ ? ^ j



Typp ^ ~ : ^ y ^ y ^ ? ^ y . ^ : ^ ? < y ^ y . < : r

Capacity / ^

Depth of Pump in well _

Depth of Ai r ,L ine in well

10. USED FOR

^

Mfrs. Name

How Driven ^ ^ t i f T - ^

Feet Depth of Footpiece in well

Feet Type of Meter on Pump

/ S ? v^/fx^3g:7-

y AMOUNT

11. Q U A L I T Y OF WATER

Taste _ z ^ 2 ^ _

12. LOG

( Average

Maxi imum.

Gallons Daily

Gallons Daily

Odor A ^ ^ A Color.

pie: Yes N o .

Temp. _ OF.

(Give details on back of sheet or on separate sheet I f electric log was made, please furnish copy.) Are samples available?

13. SOURCE OF DATA

14. DATA OBTAINED BY

^ ^

& ^ g ^ ; n... ^ ^ y < ^ y / r y ^

I N D T F - I I f P nthtu- eiHo n f thl<! <:hetft f n r aHr l i t i nns I I n f n r m a t i n n a i r h ac Inn n f m a t t f r i a h nor to t ra tar l

Form DWR-138 11/85

i"!-' NEWJERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION f ,Cf DIVISION OF WATER RESOURCES

WELL RECORD

PAGE 1 OF 2

Well Permit No. 2SL - MV?79. Atlas Sheet Coordinates ?Q : _ _ 3 3 _ filfi D

OWNER IDENTIFICATION - Owner P P T r g Mg^VTW .TO

Address 11915 BEW BRDNSWICK AVE. City MaNASOJM State -Û- Zip Code

WELL LOCATION - If not the same owner please give address. Address County

Owner's Well No.

_, WELL USE P o r y ^ ^ p s n c Municipality wflr.r. TWP Lot No..

Status.

WATER USE X ^ f U L \ ' 4 I ' V T I ^ | J L ( Average / 000 gals, daily

-48- Block Mo- 3 ] 2

Maximum Ô&O gals, daily

[

c

c

WELL CONSTRUCTION BOREHOLE DIMENSIONS

Land Surface Elevation at wrell Casing Height (stick-up) above land surface

Date well completed Depths: Total Diameter: Top

.ft.

DEPTH TO TOP (FT.)

Casing 1 Casing 2 Casing 3 Screen 1 Screen 2 Tail Piece Gravel Pack Grout Grouting Method

A£L

j n .

I.ENGTH (FT.)

10.

/ . f t . in.

Finished. Bottom _

Elevation was determined using

DIAMETER (IN.)

. ^

f t . in.

TYPE AND MATERIAL Screens: Note Slot Size(s)

5etff^ 40 P\/C^

A / ^ = > U 7 D A ; /

^^f2Ji<l\ W WELL FLOWS NATURALLY gals, per min. at f t . above the land surface. Water rises to ^ f t . above the land surface.

RECORD OF TEST Static water-level before pumping. Water level was measured using _

' Discharge rate measured using . Well was pumped using

. / . / . Test Date / ^ f t . below land surface. Water level

• Drawdown j A T f

_ft. below land surface after

pomP Observed effects on nearby wells

": Water Quality (taste, odor, color, etc.)

AlOAl,

Discharge Rate Specific Capacity

. hrs. of pumping.

. gals, per min. gals, per min. per f t . of drawdown

/jfiP £ Installed by_ PERMANENT PUMPING EQUIPMENT

Mfrs. Name A O U L - b p CAPACITY: Pump rifilivpr.^ f i ~ GPM at POWER: V 3 HP at RPM

^ ^ Model.

Pump Type J / ? /

.7P3 3 0

DEPTHS: Pump FLOWMETER: Model

ft. Footpiece

RSI pressure. Power Source _

ft . Airline . f t . installed on . in. diameter pipe.

CONTRACTOR - Name of Drilling Contractor.

Address

REH-RAYMCM> M&ÊK mO,

City Name of Driller /e/?v /n/Ni^n^

State _ Zip Code . ^ . License No. i / ( I

-Signature of Contractor Date

Form DWR-138 11/85

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION

DIVISION OF WATER RESOURCES PAGE 2 OF 2

WELL RECORD

Driller: Please use the space below for the log description. Note water bearing zones or geological formation.

Are samples available? d l Yes L^No

Drilling Method ^^^TfWL^^

Type of Rig

Aquifer/Geo. Fm.

Mot)

LOG

O - I T^P^DIU

3£>1 <iCiUib u t ^ m u

0

[

[

Well Permit No. ^ ^ = ^ 7 - ^ ^ ^ ^ 7 ^

PEP USE ONLY

Storet Hydrogeo Code

USGS Hydrogeo Code

Depth to Bedrock

Bedrock L i t h . Code

Bedrock Fm. Code

f t .

Completed by

Date

Thick. L i t h . Fm.

GWPI No .

1 atirude °

Lat-Long Accuracy • 1 " [ U S "

USGS Quadrangle

Drainage Basin Code

OTHER FILES: • Lithologic Log

• Geophysical Logs

Checked bv

1

D 1 0 " n 2 0 "

Q Samples Available

• Water Chemistry

NJPDES

Longitud

Cou^ tv /^

• / D P

Date

1

No.

B °

lunicioalitv Code

Aquifer Test

ol lut ion Case

/ /

1 I I

• Water Level Data

Form DWR-138 11/85

NEWJERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER RESOURCES

WELL RECORD

PAGE 1 OF 2

Well Permit No. 2 9 — 2 ^ 6 5 Atlas Sheet Coordinates 2 9 : 3 3 615 D

OWNER IDENTIFICATION - nwnprGTTf i . PWIT. W?.

Address 1 2 1 0 NRW H f f l H f W T n g AVR.

City WWgqTAN State JJJL Zip Code 0 8 7 3 6

_ WELL LOCATION - If not the same owner please give address.

Address \

c c

G

[ [

Owner's Well No.

County Monmouth Municipality MATJ. T M B - Lot No. 8 & 0 BlockJlo..j_

WELL USE I r r i g a t i o n Status.

WATER USE I r r igat ion Average gals, daily Maximum gals, daily

Date well completed 4 / 19 / 8 8 Depths: Total 8 0 ft. ^ Finished 8 0 ft. Diameter: Top 8 in. Bottom 8 in.

1 1 2 ft. Elevation was determined using Casing Height (stick-up) above land surface c ^ .-. ft.

WELL CONSTRUCTION

BOREHOLE DIMENSIONS

Land Surface Elevation at well topography map #29

D E P T H T O T O P (FT . )

L E N G T H (FT.)

D I A M E T E R ( IN. )

T Y P E A N D M A T E R I A L . Screens: Note Slot Size(s)


.20-

10

60 80

M d <;rfi An pvr

.Ulb" slot FVC

300# Df #1 sand

drop

WELL FLOWS NATURALLY gals, per min. at ft. above the land surface. Water rises to ft. above the land surface.

RECORD OF TEST Test Date 4 / 1 9 / 8 8 Static water-level before pumping _ 3 0 ft. below land surface. Water level 50 ft. below land surface after 1 hrs. of pumping. Water level was measured using d r o p i i n e / m - S C O p e Drawdown 20 ft.

Discharge rate measured using b u C k e t Discharge Rate 5 0 gals, per min.

Well was pumped using ^ ^ ^ Specific Capacity ^ ' - ^ gals, per min. per ft. of drawdown

Observed effects on nearby wells

Water Quality (taste, odor, color, etc.) none

PERMANENT PUMPING EQUIPMENT Mfrs. Name Red J a c k p t

Installedhy David Van Brun .1r. PumpType Submersible Model

J 5 -CAPACITY: Pump delivers .

POWER: 3/4 HP at 3450 GPM at -40-

- DEPTHS: Pump RPM

Footpiece

PSI pressure. Power Source _

f t Airline e lec t r i c i t y

FLOWMETER: Model installed on . in. diameter pipe.

TUSR OOHSmJCTICN 0C1?P. CONTRACTOR - Name of Drilling Contractor \ Address 806 H i g h w a y 7 1 . P .O. Rnx .394 City g;pring I akp Hpight<; State JLJ. Name of Driller Dennis Buchanan

Zip Code 07762

Signature of Hnntrartnr ' \

g u n I ^—Liumigi i t i i i y, y^

COPIES: White - DEP Canary - Driller

License No. .1 1393

• t _ > j ./ 10 88

Pink • Owni Goldenrod - Health Dept.

c

[

c

Form DWR-138 11/85

NEWJERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER RESOURCES

PAGE 2 OF 2

WELL RECORD Well Permit No


Are samples available?

Drilling Method

• Yes jpNo Mud Rotary

Type of Rig Fai l ing CF-15

Aquifer/Geo. Fm.. Cohansy

LOG

fl-1 Topsoil

i - i y uoarse sand & gravel

19-60 Medium s i l t y sand

60-75 Medium reddish yellow sand

75-77 Yellow & brown d a y

77-79 Fine gray sand.

/y-8U liray clay

GWPI No.

Latitude

• V 0 5" Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code

OTHER FILES: • Lithologic Log • Geophysical Logs

Checked by

• lO" 0 20"

^ ^ 3 3 - ^ / ^ PEP USE ONLY

Storet Hydrogeo Code USGS Hydrogeo Code

Depth to Bedrock Bedrock Lith. Code Bedrock Fm. Code

f t .

Completed by Date

Thick. Lith. Fm.

NJPDES No.

Longitude

County/Municipality Code

Q Samples Available IIII Aquifer Test

• Water Chemistry • Pollution Case


Date . / . / .

(S), '.U>

, Fofri DvVn- 133 11/80 f p ^ .4-

Coovuo^ D . V l l - % . \ S '

[ G

C

C

c

STATE OF NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION


WELL RECORD

an-jLCiTi9 PERMIT NO.

APPLICATION NO.

n 1- OWNER

Owner's Well No.

LOCATION ^yrtj^^jue. DATE COMPLETED 7€jll^^

ADDRESS

SURFACE ELEVATION

{/^M- 77^/g; (Above mttn tea ievti)

.Feet

A. DIAMETER: Top. . inches

DRILLER _ i ^ 2 ^

Bonom yr inches

/ • . J Û t . ^ i ^±^^M ^

L.

5. CASING: Type . . . / ^ < K ( ^ ( y ^ ^ J ^ i r U U .

6. SCREEN: Type { r L y . C ^ . j Sizs of Opening _ J ^ D

\ Top 1 3 ' ' 6 > Feet

Diameter — J L .

ameier /

TOTAL DEPTH.

1 inches

Inches

.re J r t i t

Length S 3 ' ^ f set

Length _ X j ( Z _ _ _ r e e t

Range in Depth 1 Bottom

Feet

Feet Geologic Formation , CC iitSi. *ts^y

Tail Piece: Diameter. . Inches Length.

7. WELL FLOWS NATURALLY .

Water rises to .

Gallons per minute at,

-Feet

Feet above surface

Feet above surface

8. RECORD OF TEST: Date g / g y Yield. JUL. Gallons per minute

Static water level before pumping / gT.

Pumping level 1? - ^ , ,.

Drawdown Jf' / Feet Specific Capacity .

feet below surface after ^

Feet below surface

hours pumping

How pumped <UC4g<<^ C <* i ^ w » | t f t f r i ^ i / / # f f ^ ^ ^ How measured

Observed effect on nearty wells ^ ^ l ^ j t t - j i f > i ^ ^

Gals, per min. per f t . of drawdown ^

£4^


Type S^/ f / r j /y / i r /A/^^ Mfrs. Name

Capacity / P G.P.M. How Driven / ^ y c f K ' c H.P

^ ^ Feet '

R.P.M. f:?A Depth of Pump in well Depth of Footpiece in well

Depth of Air Line in well I

I

^ Feet Type of Meter on Pump - ^ — .

I - i - ' \ \ Average T ^ ^ 10. USED FOR . J . ^ 1 7.1 r J ^ ^ L f . y x - ' y { _ 6 \ l U f . AMOUNT

Size.

eet

.Inches

tr i 11. QUALITY OF WATER

Taste. ^ ^ 7 " ^ • ^

.< '• / /?-

Odor.

_ Gallons Daily

^ M«yimiim / • < <? Gallons Daily

Sample: Yes No * / ^

Color ^ / ^ ^ J S f f t , r ' Temp. , ? ^ . ^F .

12. LOG / ? A y J^j7^.Jr-(Give Oetaih on tack of sheet or on stotnn sheet If Htctrie log wu msOe. plett* furnish copy.)

Are samples available? MO_

13. SOURCE OF DATA f J O T A n - y 0 < R / i ^ L ^

14. DATA OBTAINED BY . • ^ ^ ^ ^ / y T , i C < i r / ^ / ^ f ^ ^ • • . i . / , ' ^ / : t ^ D a « . ^ y / ^ T . yf<fj^

r^î~^t^? ya (NO TE: Use other side of this sheet for additional information such as log of materials penetrated,

analysis of the water, sketch rnao. sketch of special casing arrangements, etc.)

WELREC 113 0202

C-^ . • i iCC•t ' - I CCf... ' ^ - . . • j : .Cc ,Cc - \ C^^-iî^'U

c c

WELREC 113 0203

Form DWR-138 11/85



c [

WELL RECORD Well Permit m.J3.-^DSn.

Driller: Please use the space below for the log description. Note water bearing zones

or geological formation.

Are samples available? • Yes E T N O

Drilling Method fri/rflr?'-, ,

Type of Rig

Aquifer/Geo. Fm.

-ri/C 1^->/>

i^dH^r*iW7

ZIT.^F.'^T-PEP USE ONLY

Storet Hydrogeo code

USGS Hydrogeo Code

Depth to Bedrock

Bedrock L i th . Code

Bedrock Fm.Code

Completed by

Date

LOG

S - 3 r u<i- -, fi^fû Iff!(dill s/ ' O'f 6-/?/n >/

•?-r-iZ' yyif'Oiujr' i}9lhu'rA^/l S ^ - G r /0>/ r/iytyj/iAD. n7/>/fj />/A^

^ r - j ^ /yfro^ t cr/ 'jf />.<(- J A ^

-

GWPl 'No .

Latitude 0 . „

Lat-Long Accuracy • 1 " D 5 " D 10" • 2 0 "

USGS QuadranfliB

Drainane Basin Code

OTHER FILES: • Lithologic Log • Samples Available

• Geophysical Logs • Water Chemistry

Checked bv

NJPDES

Longitud

County/^

• > • f

Date

Thick. L i th . Fm.

No.

°

Municipality Code

aquifer Test

'ol lution Case

/ /

1 I t


[ G

C

C

C

Form DWR-138 11/85



WELL RECORD Well


or geological formation. XX

Are samples available? ' ^ u ! ^ ^ R o Q ^

Drilling Method

F a i l i n g CF-15 Type of Rig

Aquifer/Geo. Fm..

Cohansey

-0-3--5-?-

LOG

Brown gravol and aand

- f-a-Orange medium to fine sand

11-19 Brown clay and yiavel Gray coarse sand

19-45 Yellow line sahd 45-54 Keddish fine sand b4-/u Yeiiow medium to coarse sand

(COHANSEY)

Permit No. c > n — g A ? \ o A )

PEP USE ONLY

Storet Hydrogeo Code'

USGS Hydrogeo Code

Depth to Bedrock

Bedrock L i th. Code

Bedrock Fm.Code

f t .

Completed by

Date

Thick. L i th . Fm.

GWPI No.

r Latitude

• r

NJPDES No.

Longitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code


• 5" • 10" • 20"


Checked by

• Samples Available

• Water Chemistry


• Aquifer Test

^ • Pollution Case


Date . / -

^ ^ ' ^ . „ i -orm uvyi-s-iJO ' ^ ^ \ l 1 / 8 5 " 5 ' ' DIVISION OF WATER RESOURCES

„FormDWR-138 " ^ iT NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION PAGE 1 OF 2 )N OF WATER RESC

WELL RECORD

Well Permit No. 2 9 ~ 2 1 1 6 3 I I Atlas Sheet Coordinates ^ 33 BIB-

OWNER IDENTIFICATION - OwnernJLLY^W]I I . ] :AM & LQEfftAlME

"^'^'''^ 1010 MEW EBDiCWICK AVEN^ A ^ ^ V / City _ _ _ _ _ M f l M f l g q j A H State j ^ ^ ^ Zip Code ^ ^ / r _ < ( n

WELL LOCATION • If not the same owner please give address. Owner's Well No. Address ^ 1 _ _ _ ^

County f u C T v y y \ y t ^ r f Y r ^ ~ Municipality ^ - j . ^ _ j p Lot No.. Block No.

WELL USE ' t r ^ r L l O - A ^ ]

WfiLL TWP. "^""•5 513~ Status

WATER USE / - (2 (?,(' r y / ^ ] r ^ Y ^ . .^ Average gals, daily Maximum gals, daily

WELL CONSTRUCTION Date well completed. _ _ Z _ / - L _ / Q O , BOREHOLE DIMENSIONS Depths: Total ( r j O ft. Finished h O ft.

Diameter: Top lr> in. Bottom (~f in. c s ^ - , / j \ / ^ " ^ Land Surface Elevation at well _ _ 0 _ 0 _ f t . ^ ^ Elevation was determined using / n ^ D Cf /f J ^ ( j y l f ^ U f M r j / r ^ < ^ Casing Height (stick-up) above land surface fcg ft.

^ n ^ n q ^ f ^ j ^ o L u

D E P T H T O T O P L E N G T H D I A M E T E R T Y P E A N D M A T E R I A L (FT.) (FT.) (IN.) Screens: Note Slot Size(s)

r Casing 1 . ^ O A <^C^LÔ ^ VC^

L i Casinn 2 • ' Casing 2 Casing 3 Screen 1 Screen 2 Tail Piece Gravel Pack

_S:n. /o ^ . ' ( ^ / ^ " $lcf Pf./o.

G Grout I

Grouting Method C \ I L o f WELL FLOWS NATURALLY gals, per min. at ft. above the land surface.

Water rises to ft. above the land surface.

RECORD OF TEST Test Date [ / I / Q 0 / . Static water-level before pumping / y * ft. below land surface. Water level " 7 0 ft. below land surface after | hrs. of pumping. Water level was measured using O j L p p L i VAO I " ^ C ^ ( ^ Drawdown J ) , j L ft.

Discharge rate measured using ^ ^ ^ CJL;ig>\, i _ Discharge Rate ^ ^ j ,-.''^*^- P^""'"'"• Well was pumped using J H t V-- Specific Capacity < Q gals, per min. per ft. of drawdown

Observed effects on nearby wells \A & y ~ <?- \

Water Quality (taste, odor, color, etc.)

PERMANENT PUMPHJIG EQUIPMENT Installed b y _ _ _ ± Pump Type ( J ) - g - ^ | ; Mfrs. Name f oêafj \ A Q . Model.

PIDIG EQUIBMp

G^P> f fO;^ p delivers ^ ^ O GPM at Y PSI pressure. p ^ / / ^ ^ f i HP at RPM Power Source V^X ^ C - j ^ Q l Q l ^ (^

CAPACITY: Pump delivers POWER: I DEPTHS: Pump ft. Footpiece ft. Airline FLOWMETER: Model installed on in. diameter pipe.

CONTRACTOR - Name of Drilling qnryractor ^ ^ O C I g i - H l X j r I O H O C T g

AdHrp,ss ..g-Qb H).)(i,. / / . /x/P-O- \S<^^ l ^ y j ,1 n \ ^ - j / n City ^ p ^ i f ^ (.l\%<r' M~V i State M > \ J l Zip Code g) / / f? i , Name of Driller 11 ( . ^ > License No.

V^Û- (b)^^yZ'J^jJf'^-^^Ji^ G^J^' Date _ 4 _ l J y L l J S r COPIES: White - DEP Canary - Driller Pink • Owner/ Goldenrod • Health Dept.

Form DWR-138 n / 8 5



PAGE 2 OF 2

WELL RECORD Well Permit No!



Are sampies available?

Dril l ing Method

Type of Rig •

Aquifer/Geo. Fm

• Yes No

^ u r ^ e ( ^ -

LOG

[ c c [

G

C

y i t l / o r n r ' ^ / ^ H , r ^ • S ' A ^ ^ yÛSZMZtti

VS^-fô ^ e l l o n . r / / A ^ C / . S / K J ^

PEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock


Bedrock Fm.Code

Completed by

Date

Thick.

GWPI N o .

Latitude

• l" • 5"

NJPDES No.

Longitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code



Checked by

• 10" • 20"


• Samples Available • Aquifer Test


f t .

L i th . Fm.


Date . / . . / -

FofrnDWR-138 11/85

® -MS

NEW JERSEY DEPARTIWENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER RESOURCES

WELLRECORO

PAGE 1 OF 2

Well Permit No. 2 9 - — 2 1 2 B 5 Adas Sheet Coordinates 2 9 '• 3 3 -Z7&- D

c c

OVWHER lOENTIFICATION - Owner n j j g - ( ^ W I L L K Y 1 Address City

2 1 ^ nDDWDOD DRIS^ SEA CEHT State -Nd- Zip Code

r~. WELL LOCATION - If not the same owner please give address. 1 Address ^

Owner's Well No.

County IVIunicipality W L J _ T W > .

Lot No. Block No._ 7 2 2 -

WELLUSE. irr igation Status.

WATER USE Average gals, daily Maximum gals, daily


Date well completed 1 0 / 1 3 / Depths: Total H O ft. Finished 1 1 0 Diameter: Top 8 in. Bottom 8

Land Surface Elevation at well 5 0 ft. . Elevation was determined using .

ft.

*Ebpography map 29


)ve land surface

DEPTH TO TOP (FT.)

88

ft.

L E N G T H (FT.)

88

ib

78 5

29 78

D I A M E T E R (IH.)

TVPE A N D M A T E R I A L Screens: Note S lo t Size(s)

sch 40 PVC

.015 PVC screen

•drop-holeplug

WELL FLOWS NATURALLY Water rises to

. gals, per min. at . f t . above the land surface.

23' Test Date RECORD OF TEST

Static water-level before pumping Water level was measured using _ Discharge rate measured using bucket Well was pumped using a i r

10 / .

. ft. above the land surface.

13 / . 8 8

ft. below land su rface. Water lave! d r O P l i n e / ^ M s c o p e Drawdown

65 42

Discharge Rate. Specific Capacity

J t . below land surface after 1 hrs. of pumping. . f t .

. gals, per min. . gals, per min. per ft. of drawdown

Obsen/ed effects on nearby wells n n n P Water Quality (tiste, odor, color, etc.)

PERMANENT PUMPING EQUIPMENT Mfrs. Name Red Jacket

Installed hy DavJd Van Brunt J r . p,„p Type submersible Mndfli7 GC Red Jaclcpt

CAPACITY: Pump delivers 10 GPM at 40 PSI pressure. POWER: 1 HP at 3450 RPM Power Source filf^rtrirify DEPTHS: Pump 8 3 ft. Footpiece ft. Airline . f t . FLOWMETER: Model installed on . in. diameter pipe.

CONTRACTOR - Name of Drilling Contractor. Address 806 HwV. 71

City

TIGER C0N5TRJCTICN CCFP.

Spring Lake Hts, Name of Driller Dennis Buchannan

State N t J . •'^'y^^^f^^

Signature of Contractor J M U tyyutax ctlo^ MutoL Cou) ®

COPIES: White • DEP Canary - Driller Pink • Owner

License No

Date /°^ / '^'7 I <fif Goldenrod • Health Dept.

WELREC 112 1712

c c

G

Form DWR-138 11/85

NEWJERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION


PAGE 2 OF 2

WELLRECORO Well Permit No.



Are samples available? CI l Yes CS No

Drilling Method Mud Rota ry

Type of Rig F a i l i n g CF-15

Aquifer/Geo. Fm. C o h a n s e y

1

LOG

0-21 Coarse Sand 21-47 medium whi te and gray sand 47-72 brown and gray c lay 72-104 vpry f i n e to f i n e quartz sand

(Kirkwood) 104-108—gray and brown sandy clay 108-110—gray/green clay

GWPI No.

O i " D S "

Latitude .

Lat-Long Accuracy

USGS Quadrangle Drainage Basin Code



Checked by

• 10" • 20"

DEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock

Bedrock Lith.Code Bedrock Fm.Code

f t .

Complated by

Date

Thick. Li th. Fm.

NJPDES No.

Longitude





Date ./- / •

WELREC 112 1713

Form DWR-138 11/85

,M^ NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION


/

WELL RECORD

PAGE/l aF/2

Well Permit No. Adas Sheet Coordinates

29 - 2 2 5 0 1 2 9 " 33" "613

OWNER IDENTIFICATION - n«,nprnAMPPKrJ., RTCHARD

Address 2 2 f f P r t T W H T S TA.

D

City -HA£L- State N J Zip Code

G

C

C

WELL LOCATION-If not the same owner please give address. Owner's Well No.

Address \ _ ^ _ ^ _ _

County Municipality —yâTJ. T W ^ LotNo. -£Ee_ Block No..

WELLUSE_

WATER USE

'X>^r^^v^^^ C . V g- N<;^\OY^ Status

Average \ B O O gals, daily Maximum

WELL CONSTRUCTION

BOREHOLE DIMENSIONS

Land Surface Elevation at well Casing Height (stick-up) above land surface _

D E P T H T O T O P (FT. )

Date welj^completed _ J / P * ^ / — ' . ' Depths: Total ^ ^ X ) f t Finished H " ^

gals, daily

_ Diameter: Top

? g ^ ft , y * ^ Ptouatti

Bottom. . f t .

in.

. f t .


31

^ 1 ^

L E N G T H


D I A M E T E R (IN.)

Ik Doî£y^

T Y P E A N D M A T E R I A L Screens: Note Slot Size(s)

^ ^

H: ~ \ j ^

XS ^ l U ^ ^

WELL FLOWS

Water rises

IWS NATURALLY i f i - J ^ gals, per min. at J ^ ^ , p _ _ f t

to v ^ V ^ - * ^- above the land surface,

. above the land surface.

RECORD OF TEST Test Date Static water-level before pumping Water level was measured using _ Discharge rate measured using -r-r-^ Well was pumped using ^ ^ J « ^

f t below land su rface. Water level Drawdown

J t . below land surface after O hrs. of pumping.

Observed effects on nearby wells Water Quality (taste, odor, color, etc.)

Vo^^^

Discharge Bate Q ^ ^ gals, per min.

Specific Capacity \ gals, per min. per ft. of drawdown

Q r - ^ a ^ VsQf C\S/^('

Installed hy Ô^VSXtU' PERMANENT PUMPING EQUIPMENT Mfrs. Name ^ j — i g s ^ \ > , S .

CAPACITY: Pump riPliv^' ' ^ S ^ ^ ^ ^ ^ \ g < ^ PSI pressure

POWER: \ HP at 3 4 5 ^ " P " ôwer Source

DEPTHS: Pumo ' 3 - E > ft. Footpiece ^ K ft-

FLOWMETER: Model

Pump Type S^^V Model ; ? 5 ' e . M < = » H ^ ^

V ^ Airiine t ^ * - ^ f t

installed on \ . in. diameter pipe.

CONTRACTOR - Name of Drilling Conlj actqc AdHrpss \ 1 T S V >

City Name of Driller

V\iovajL.v

GRIM ETJNfraXSER ^ o V

^ State J^£-

J 5 C s ^ Zip Code <^mi\

License No.

Signature of Contractor X^_J> g * ^ ^ - — X ^ ^ ^ ^ V ' " » j - > ^ o . ~ - - ' Date ^ , ^ / ^ COPIES: White - DEP Canary • Driller Pink - Owner Goldenrod - Health Dept

c

[

[;

Form DWR-138 11/85



WELLRECORO Weil Permit No. \St9_33SO/




Drilling Method

Type of Rig

• Yes > ^ ^

Aquifer/Geo. Fm. . e - -

^ - < >

LOG

^ ? . - ^ A \ .g> ^ " t < ^

<r' - ^ ^S^^ssv. ^ ftv. V ^ j ^ . C ' ^

^ - \ ^ ^ ^ in; r-rôs^ 1 i L N6;ir -v^V xlr wA c ^

- <,n^^t^ s ' ^ q j ^ ^ ^ v ^ ^ Q y ^

[ "^^^ S i ^\-^-^^^^\v^/^-v-^

PEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock


Bedrock Fm.Code

Completed by

Date

Thick.

GWPI No .

Latitude

• l- • 5"

NJPDES No.

Longitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code

OTHER FILES: D LithologicLog


Checked by

n 10" 0 20"


O Samples Available • Aquifer Test


f t .

Date ./- . / .

L i th . Fm.


FormDWR-138 . "fj * ^ ' 11/85 O '

SoO^< .s

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER RESOURCES

WELL RECORD

Well Permit No. Atlas Sheet Coordinates

E 9 -

. S 2 _

OWNER IDENTIFICATION - Ow/ner G r p h , G e a r q e

... 1115 New SrUhsWiek AVS. Address City

PAGE

ES87E

J3a_ ilH_ ^^

W a l l State ^ N 3 -

Zip Code

D

WELL LOCATION - If not the same owner please give address. Owner's Well No. Address S a m e A s ftbove

County M o n m o u t h Municipality M a l l ^ U 3 " Lot No. Block No.,

[ c

0

[

WELL USE i ^ i t h d r a w a l Status. I n Use

WATER USE Irrigation

Date well completed WELL CONSTRUCTION BOREHOLE DIMENSIONS

Diameter: Top Land Surface Elevation at well ^ Q ft. Casing Height (stick-up) above land surface T g l J ' O ft

Average .

8 9

2 0 0 0 gals, daily Maximum

4 0 0 0

Depths: Total ^ ^ ^ ft. 8 . 5 "

/ . 0 7 ^ 0 7

Finished . Bottom _

Casing 1 Casing 2 Casing 3 Scteen 1 Screen 2 Tail Piece Gravel Pack Grout Grouting Method

D E P T H T O T O P (FT. )

0 3

LENGTH (PT.(

8 3


D I A M E T E R ( IN.)

so- - « F ^

7 3

S u r - f a c s "73

4 " H . b "

P r e s s u r e , T h r u T r e m i e P i p e

ft. in. Topographic Map

WELL FLOWS NATURALLY gals, per min. at ft. above the land surface. Water rises to ft. above the land surface.

gals, daily


S c h e d u l e Ô PVC

SclieUulfa; Ô P V C / . 0 0 0

. 0S5 B l e n d e d id'JV mesh t s e n t o n i t e

RECORD OF TEST 3 6

Test Date 8 9 ^ 0 7 ^ 0 7

Static water-level before pumping Water level was measured using E s t i t n a , e d Discharge rate measured using M e a s u r e d C o n t a i n e r Discharge R a t e _ _ i ^

.ft. belowlandsu rface. Water level Drawdown -

7 ^

A i r L i f t Well was pumped using Observed effects on nearby wells N o n e Water Quality (taste, odor, color, etc.)

Specific Capacity O . ^

_ft. below land surface after.

.ft. _ gals, per min.

.hrs. of pumping.

lis. per min. per ft. of drawdown

Good

PERMANENT PUMPING EQUIPMENT Mfrs. Name R r n i T r l

Installed K y ^ f i W ^ ^ C K W E L L D R L G p^^^.^^^ S u b m e r s i b l i

m 0}jm, Mnriei l O E J O s ^ g g IE . GPM at ^ O CAPACITY: Pump delivers

POWER: 1 ^ 1 HP at 3 ^ 5 0 , RPM ,•.-;

DEPTHS: Pump ft. Footpiece O FLOWMETER: Model ,

.PSI pressure.: Power Source . 1 - E l e c t r i c

. f t * Airiine installed on

.ft. . in. diameter pipe.

PICKWICK WELL DRILLING CONTRACTOR - Name of Drilling Contractor ^ ^ - _ - - . „ . . • . — - „ „ t=-%/^j\ Adrirass P . O . Box 6 , F a r m i n q d a l e , NJ 0 / / c ; 7 < g O i ; V30 b3QO

City DiTivi''? P r imn&t - -MlOîl- State Zip Code

Name of Driller

Signature of Contractor

A l l e n H r i m o s t . J l ^ o / License No.

^ / : ^

COPIES: White • DEP Canary • Driller Pink - Owner

Date

Goldenrod - Health Dept.

-2^

Form DWR-138 11/85



WELLRECORO Well Perm


Are samples available? • Yes W No

Drilling Method / )0<7/ ) f ^ l Q ^ j

Type of Rig X//. ~DfiJDie:

Aquifer/Geo. Fm. \ U M J ( ^ L M I ^ ^ ^

LOG

0 - / 0 d/hupJ

/ D - ^ 5 " (^Jnrjfê. I d n Snr^rj

A I S - ^ Fine. Ian ^ n c j /OCJ^rc S i / f

3G-SS F.nP.i- /r)ed. l ^ n yr^nri / Dt^hrTSTTF

I n O - l S r\r^p - k i n Sa r^ /^'/-fcf OO.I re ( Jmi

nS- r O ^,1-h, hrrrnr) ('Ja^j / -Fine. Q^rori

[ HO-ICZ F i h e r^r^r. p a n e / / ^ a r K j ^ , ^ y y

Q^ '33'LIS. PEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock


Bedrock Fm.Code

f t .

Completed by

Date

Thick.

GWPI No.

U v D S "

Latitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code



Checked by

NJPDES No.

Longitude

• 10" • 20"




83' aîsl-

L i th . Fm.


. / - / .

c G

C

[

0

orm DWR-138. .1/85 ,

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION PAGE

-3


' , i>s6 WELL RECORD \IA.\

. ^ Well Permit No. _ Adas Sheet Coordinates

29-. .23121. . ^ : _3a: 364 D

OWNER lOENTIFICATION - Owner.

Address City

RTTiTiTfiAN. m

2152 REEWOOD ED-SEA GIBT State - M i - Zip Code

) l \Ul f Mtthesame WELL LOCATIOI\|r^lf j;>qt the same owner please give address.

Address.

Owner's Well No.

Aooress i ^ -QV-^ v v ^ : County y M f ^ ^ Y W / Y t ^ ^ T T n Municipality W ^ A M T W T Lot No.

WELL USE. hrrrU"hrAujL. Block No..

WATER USE tSpm Status. • ^ A / Q j ; -p

-?22-

mry-^r- Average J S O O


Land Surface Elevation at well Casing Height tstiSinrp) above land surface

gals, daily Maximum ^ ^ gals, daily

Date well completed ?> I \ Q / SX-J-QJ^ ' ' Depths: Total j ( ^ O ft. Finished ^ f / p . ft.

, / / Diameter: Top C*-^' in. Bottom Sc in.



Elevation was determined using 'k t^m D I A M E T E R

( IN . )

^ / / - pi /d

T Y P E A N D M A T E R I A U Screens: Note Slot Size(s)

-¥ -hf- . o / s . yPiy^^

/y i / - tLM^=r fyf>y^ ^ t ^ ^ .C Or~f


Water rises to W o .gals, per min. at 0 . ft. above the land surface.

. ft. above the land surface.

RECORD OF TEST Static water-level before pumping Water level was measured using Discharge rate measured using Well was pumped using

Test Date g / i. D / < f i 9

^ L -ft. below land surface. Water level C ^ i U\.^,r-^ Drawdown

f KoU^-^y^ Discharge Rate

Specific Capacity

f ^ ^ £ h r s . of below land surface aftei

lals. per min. gals, per min. per ft. of drawdown

pumping.

Observed effects on nearby wells Water Quality (taste, odor, color, etc.]

PERMANENT PU Mfrs. Name

0UHA<,rA4:^^^^ '%^^M'^^ -G EQUIPMENT Installed by_ ¥ -CAPACITY: Pumo delivers g=>^CJ GPM at POWER: / ^ H P a c ? ^ C S ~ 1 ^ RPM

nFPTHS: Pump" ' ^ . J ^ ' * ft. Footpiece

FLOWMETER: Model

I ^ . PSI pressure.

IJ^vyet Source

ft.

o:?:^0t/^c7^ Airiine A - y ^ A ft.

installed on in. diameter pipe.

CONTRACTO Address

EOEERT AZDRAK R».âme of Drilling £antractor_,^ ^ ^ T N .

City ' yx>^ j ^ "z^rTl/ v> State y ^ ^ n Zip Code

Name of Driller License No. / T Y . v ^

Signature of Contractor ^ / / ^ / ^

COPIES: White • DEP Canary • Driller Pink - Owner

Date


c [

[

FormDWR-138 1T/85 ' ,



PAGE 2 OF 2

WELL RECORD Well Permit No.




Drilling Method

liable? y ^ Y e s " ^ N o

1 /af7~?^^y Type of Rig c^c ro J ^ y CfA r L A

y: Aquifer/Geo. F m . . / t ^ f - A ' J U ^

LOG

y^- ^ ' S.^^. e6y -%- y y ' . p : ^ ^

y-/ > - eV</' ' SV(^7 /^'y - ^ ( Ngv<iv^^JV<y-/)-^^

PEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock


Bedrock Fm.Code

f t .

Completed by

Date

Thick.

• l- • 5"

GWPI No.

Latitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code



Checked by

NJPDES No.

Longitude

• 10" • 20 "



• Water Chemistry • Pollution Csss

i!l^,.

L i th . Fm.


. / -

Form DWR-138 11/8P,


/ \ ? ^ \

T-' DIVISION OF WATER RESOURCES

\ ^ WELL RECORD

Well Permit No. ^ — 2 4 5 5 3 Atlas Sheet Coordinates 2 9 : 3 3

PAGE 1 OF 2

cy

3 8 4 D OWNER IDENTIFICATION - Owner aAnr .TAWn, FRAffiT

Address Mflf iHOTJA AYR

City WaLL State -JtL Zip Code

[

[;

L

WELL LOCATIOI\[j lf.nqt the sjme owner please give address. Owner's Well No. Address.

County n \ { S t \ ^ i y ^ ^ ( m r \ Municipality H f l L L TWP7

WELL USF 1 A / ^ 7 ~ ^ r > t A - t j u f C

Lot No. - 3 4 - Block No..

Status. ::rA/ (/s r WATER USE ^ c^n. o.^f^^nn t ^ J - Average f O \ J ^ ^ gais_ daily Maximum A V I / r t Ti WELL CONSTRUCTION BOREHOLE DIMENSIONS

Land Surface Elevation at well Casing Height jstrckiop) above land surface : hiiuk-up) aboi

Date well completed i- T — ^ ^ — I . •>> / Depths: Total f o L O ft. Finished "T / / f t

/ I Diameter: Top /JT in. Bottom ^ in. K J J ) ^ ft. , Elevation was determined using / . ^ / /h

DEPTH T O T O P (FT. )


L E N G T H (FT. )



¥' Pv±

j ^ l ! c ' — ^ ^ c;/s- A^C

35 FF^^C/r : ^

u-

WELL FLOWS NATURALLY Water rises to VJ

a .gals, per min at ^ . ft. above the land surface.

ft. above the land surface.

Test Date RECORD OF TEST Static water-level before pumping Water level was measured using —• ~ - . ^ ^ > - ~ ^ . Discharge rate measured using ^ ^ ^ - ^ t X _ ^ U C / K H ^ Well was pumped using 5^

......... ^ / J S A I ^ D • Q ^ ' . -ft. below land surface. Water level ' l V s 3 < X i > V - - L . Drawdown

- ^ f i & -

gals. daily

r o ^ hrs. of .ft. below land surface after ^

ft. Discharge Rate j O O ' T " ' gals, per min. Specific Capacity 1 1 ^ gals, per min. per ft. of drawdown

pumping.

Observed effects on nearby wells

Water Quality (taste, odor, color, etc.)

lO^QOIPMENT^ Installed hy f s ) O ^ ^ V r j r h ^ f A ^ / C Pump Tvpe ^ V m - ^ J ^ i b U ~ f >

p^Tr^y^jQK— Model S l ^ r ^ O ^ l ^ n CAPACITY: Pump.delivers e 3 J ? GPM at v . S ~ ^

PERMANENT PUMPINOÊaUIPMENI, Mfrs. Name

POWER: / H P a t ^ ^ ^ l S L ) RPM

DEPTHS: Pump ( ^ ' C ^ ft. Footpiece

FLOWMETER: Model

. PSI pressure. ^

Power Source Q L S Q 0 0-

h y l h - ~ ft. Airiine h ^ I h ft. installed on . in. diameter pipe.

CONTRACTOR - Name of Drilling C ° n t r a ^ ^ ^ m . Address


Zip Code.—jQ ^ ^ \ , 7 -

COPIES: White ^DEP Canary - Driller Pink • Owner

Date


c

G

0

FQrrnDWR-138 11/85



WELLRECORO Well Permit No.




Drilling Method

Type of Rig

Aquifer/Geo. Fm • ^ : r

/C>(/^/tLu^&ltr^

L O G '

y y - B^^ i^-a^ (Ûv

PEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock


Bedrock Fm.Code

Completed by

Date

Thick.

GWPI No.

Latitude

• V • 5"

NJPDES NO.

Longitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code



Checked by

• TO" • 20 "




f t .

Wxx n?^* , / •

L i th . Fm.


[

c [

C

Form DWR-138 11/85

NEWJERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION / - . ,_^ DIVISION OF WATER RESOURCES

K t ^ >îWELL RECORD

PAGE > OF 2 . '

OWNER IDENTIFICATION - Owner Address

5,^ Well Permit No. - ^ ^ Adas Sheet Coordinates

24709

^ 3 ^ -sr -gsr 0

WALL 'iWP.

W F M 1 OCATION - I f n n t t h " same nvi/nerplRasR give address, Owner's WPH Nn

Address ^ A ^ / t ^ ^

Nd Zip Code

County Municipality

WELL USE.

WATER USE

•mp. Status.

Lot No Block No.. 807

Average gals, daily Maximum gals, daily

WELL CONSTRUCTION

BOREHOLE DIMENSIONS

Land Surface Elevation at well

Date well completed / ^ / " ^ ^ / y ^ r ' ^ > ^ Depths: Total y ^ ^ ^ ft. Finished - ^ ^ ' ^ ft.

• ^ ^ in. Bottom. Depths: Total ^ ^ Diameter: Top - - ^

ft. Elevation was determined using

Casing Height (stick-up) above land surface ft.

Casing 1 Casing 2 Casing 3 Screen 1. Screen 2 Tail Piece Gravel Pack Grout Grouting Method

D E P T H T O T O P (FT. ) __

S^

L E N G T H (FT . )

- ^

D I A M E T E R (IN. )


^ ^ ^ . . 5 ^ ^ . s 5 2 ^ . ^ - ^ ^ ^

-^Mz ,5: s5 \ . 2 ) ^ / ^ ^ ^ . ^ ^ i ^ y ^ r f '

^

WELL FLOWS NATURALLY gals, per min. at ft. above the land surface.


/ / . /

/ ^ ^ RECORD OF TEST , Test Dajp / / ' - •T) r ^ i Static water-level before pumping y ^ . ^ f tê low land surface. Water level ^ ft. below land surface after ( ^ ^ Water level was measured using CS2^^C7\ ^ Z ^ - / ^ ^ ^ / < S ^ > Drawdown ^ ^ ^ Discharge rate measured iisin55^^»4^ < / a g < ^ ^ 4 ? ^ 5 ^ ^ 7 / ^ £ y O Discharge Rate y^ ' ^ gals, per min. Well was pumped using .. " ^ • y g ' ' / ^ ^ > ' J ~ ' * ' 7 ^ ^ i y ^ > ^ Specific Capacity _ , £ ^ l i K _ _ gals, per min. per ft. of drawdown

Observed effects on nearby wells Water Quality (taste, odor, color, etc.)

hrs. of pumping.

^ r r

~7^

PERMANENT PUMPING EQtyPMENT Mfrs. Name ^ S ^ ? ^ ^ " ^

Installed hy<::^.^^^ %îrf.''?ry9AfjO^ Pump Type S^ CAPACITY: PumpripJjtfgp ' ' O ' ^ v ^ GPM at J<:tP

POWER: 3 / ^ 6 HP at > ? ^ r g ^ RPM

ft. Footpiete

Model.

DEPTHS: Pump ^ ^ r ^

PSI pressure. ^,,^ ___

Power Source j ^ Z ^ . ^ ^ i

f t Airiine

j 8 W ^ < x < y , > g C r > ^ ^ > > - V ^

FLOWMETER: Model installed a{\>^''^ynSe:e/^n. diameter pipe.


Address I'TPgfTrvTg-? WETL rexT.LTM? City Name

y " ^ ^ y ^ V - ^ . * ^ ? ^ ^ ^ ' State - . j ^ ^ t ienfRril ler >Cr>^0- <^. -y~^^J^y?^r^y.^!€)

Signature of Contracto r . ^ ^ ^ l ^ ^ ^ J

1 Zip Code License No. <» J \ j~T«i_

^ ^ y i A ^ "

COPIES: White-DEP Canary - Driller Pink - Owner

Date ^ W ^ I ^ P

Goldenrod- Health Dept.

FormDWR-138 11/85



WELLRECORO Well Permit No

Driller: Please use the space below for the log d^cription. Note water bearing zones


Are samples available? ^ ^ Yes

Drilling Method

-^ . - S N O ^ ,

Type of Rig > /

Aquifer/Geo. Fm.. y ^ _ ^ ^

LOG

^ ^ ^ ^ ^ / i r j L / ^

r y ' ^ t - ^ , y ^ ^ ^ ^ ^ ^ ^ <^'-^ - 2 ^ ^ y

G E

PEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrock

Bedrock L i th. Code

Bedrock Fm. Code

f t .

Completed by

Date

Thick.

GWPI No.

• r • 5" Latitude

Lat-Long Accuracy

USGS Quadrangle

Drainage Basin code

OTHER^FILES: • Lithologic Log

. • Geophysical Logs

Checked by

NJPDES No.

Longitude

• 10" • 20 "




s ^ Date ' - ^ '

L i th . Fm.


. / -

[ G

G

G

C

Form DWR-138 11/85

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER RESOURCES

PAGE 1

0. WELL RECORD

OWNER IDENTIFICATION • Owner.

Address City

P H F T H , F f iMPRn


2 9 - 2 6 6 4 9

2 9 : 3 3 - 6 1 4 D 2 1 7 HICnHMftY 7 1

MPfHRigaiPN- State -fclJ- Zip Code

WELL LOCATION - If not the same owner please give address.

Address

Owner's Well No.

County

WELL USE.

-Camden and Atlantic Avenue M o n m o u t h Municipality

I r r i g a t i o n WPLL TVJP. Lot No. 1 ^ Block No.. - 3 0 ; ^

Status.

WATER USE Irrigation


Land Surface Elevation at well Casing Height (stick-up) above land surface _



Date well completed Depths: Total '/^ Diameter: rep'^/^

4 0 f t ;

Average

8

5 0 0

/LJl/ . gals, daily Maximum

3 0 0 0 gals, daily

ft. . in.

TTir Finished ft. Bottom ^ ^ / ^ in.

Elevation was determined using TOPO HAP f<i3

. f t .

L E N G T H (FT . )

fin

D I A M E T E R ( IN. )


S r h . 40 PVr

-&0- - t O - .015" s l o t PVC

-55- N«aL CfciumuL Pressu re t remie



Test Date 3 1

RECORD OF TEST Staric water-level before pumping. Water level was measured using _

Discharge rate measured using

Well was pumped using

Observed effects on nearby wells n o n e

8 • / '

91 7-

. ft. below land surface. dropline/M-scope bucket+watch a i r

Water level " _ Drawdown 24_

_ft. below land surface after .hrs. of pumping.

Discharge R«w

Specific CapaciJ^* 25

. gals, per min.

gals, per min. per ft. of drawdown

'— Water Quality (taste, odor, color, etc.) CTOOd

PERMANENT PUMPING EQUIPMENT Installed h^>enn^•'; R. D a v i s Pump TypeJEL.

Mfrs. Name GQIILUS Model J L I O N CAPACITY: Pump delivers 15 GPM at POWER: 3 ^ HP at _ DEPTHS: Pump ft

3 4 5 0 »PM Footpiece

4 0 PSI pressure. Povwer Source _

ft.

/

Airline e l e c t r i c i t y

. f t

FLOWMETER: Model installed on . in. diameter pipe.

CONTRACTOR - Name of Drilling C^rgct i

Address

Signature of Contractor LyirU COPIES: White - DEP Canary • Driller Pink • Owner

Date

Goldenrod • Health D ^ t .

Form DWR-138 11/85

:^ ^ NEWJERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION - : ^^ DIVISION OF WATER RESOURCES

PAGE E l / O F 2 .

Atlas Sheet Coordinates Z 9 .• 3 3 . 3 7 9 | |

WELL RECORD

Well Permit No, 2 9 26991

OWNER IDENTIFICATION • Owner. Address City

Bmm. (iiHgL ?i7B cm Hnj. m

Zio Code Q i ^ l ^ Q HKA fflHT State JUL

G

G

G

G

WELL LOCATION - If not the same owner please give address. Address.

Owner's Well No.

Hoaress pp, County \ )CC>VT)DOTH Municipality

WELL USE U > $ T V 4 ^ & a ^ X 3 J < \ l -

HAM. THP. Lot No.. Block No.. JU-Status. " ^ V ) ^

WATER USE 'Tw^gûvtc^rxoO Average \âo gals, daily Maximum ;ôco gals, daily


Date well completed ' ^ / ^ / ' ' | Depths: Total \ " \ 0 ft. Finished _ L V O _

I Diameter: Top * ^ in. Bottom I s lanrtSiirfaM Fluuatinnatwpll cAC> ft. Elevation was determined Using _ Casing Height (stick-up) above land surface ^ ft.

ft. in.

- - ^ B D . m^p


DEPTH TO TOP (FT.)

\oo

(FT.) D I A M E T E R

(IN.)

\oo -1^\/C T Y P E A N D M A T E R I A L

Screens: Note Slot Size(t)

: ^ - ^ pyg .o^c 6vcy\

WELL FLOWS NATURALLY O gals, per min. at Water rises to O ft. above the land surface.

o . ft. above the land surface.

RECORD OF TEST Static water-level before pumping Water level was measured using Discharge rate measured usi| Well was pumped using

I "313.

Test Date lowland surface. Water level

^2,-4^ I • ^ ^ ' _ l ft. below land surface after _L

Observed effects on nearby wells k J C V J > C > ^ Water Quality (taste, odor, color, etc.) O ' ^ C a r O ^ Q C ^ J l S f e ^ ^ C U S e ^ ^ ^ ~ -

Drawdown ) 3 ft. Discharge Rata 2 i O ^ gait, par min. Specific Capacity ^ • J gals, per min. per ft. of drawdown

. hrs. of pumping.

MPING EQUI PERMANENT PUMflNG EQUIPHgNT Mfrs. Name

Installed h^rS^^ggxat^Ls^-Vi^fcJtJL Pump Type 5o farofc^^TifaLfc^

CAPACITY: Pump delivers _ _ s i : ^ _ _ . GPM at POWER: \ \ HP at 2 > * i 6 0 DEPTHS: Pump \ C O ft.

ISl Model < ^ O ^ - P M & . O a X - 0 l

. PSI pressure.

FLOWMETER: Model

RPM , , . Power Source (JJJUI^^^^SL^ Footpiece ' Q • ft. Airiine O

C2. installed on _Q_ ft.

CONTRACTOR - Name of Drilling ' ' " " • " ' f l n g ^ t T J g MBTJ- D C . ^ Address —,—„ ^_ ^ r i \ City \ J [ i ^ ^ i s y O C O O ^ M,n.Pnfnrill,r " ^ ^ K O ? ^ ^^((eX^KSlSJ^

State t - ^ - O '

in. diameter pipe.

Signature of Contractor \cX5wa^Lo~ ' 3Zs~7 ^ z:z ' S t - JHsJ-V^

^ COPIES: White-DEP Canary • Driller Pink • Owner

Zip Code O y i O / License No. \ C > M ' H

Date 1 ^ / J O _ / 5 i Goldenrod • Health Dept.

WELREC 112 1719

Form DWR-138 11/85



WELLRECORO Well Permit No


or geological formation. >

Are samples available? (HI Yes S i No

Drilling Method

Type of Rig fi^crnajg^

Aquifer/Geo. Fm.. ^ ^ X i i ^ ^ t y j

G

G

G

G

G

G

LOG

^ ^

^ Z r j L j : ^ Pznau:^

- ^ ^

^gTto' U2£

^

^? 33 ^09 DEP USE ONLY


USGS Hydrogeo Code

Depth to Bedrocl<

Bedrock Lith. Cods Bedrock Fm.Code

f t .

Completed by

Date

Thick. Lith. Fm.

GWPI No.

Latitude

• l" 0 5"

NJPDES No.

Longitude Lat-Long Accuracy

USGS Quadranala

Drainage Basin Code _ _ _ _ _ _ _ _ _ _ _ _

OTHER FILES: • Lithologic Log EH Geophysical Logs

Checked by

• 10" • 20"


CH Samples Available • Aquifer Test

• Water Cheinistry • Pollution Case


Date . / . . / .

WELREC 112 1720

DWR-138 8/91

New Jersey Department of Environmental Protection and Energy Bureau of Water/Ulocation

WELLRECORO


PAGE 1 4 ^ F 2 ' i i :

y

D OWNER lOENTIFICATION - Owner.

Address

City

r»sjy-.>::i jiavirj-

State Zip Code

WELL LOCATION - If not the same ownerplease give address. Address / ( / e i o 2 i ' U h S i ^ / r k . A y & ~

Owner's Well No.

County yÂ/ i nt 0 u f h Municipality

WELL USE y i - Âr^ .u . : ^ . I

± . Lot No.

Status 1/T, U s e

Block No..

" WATER USE T i r y i , " ^ : ^ ? &yi Average gals, daily Maximum gals, daily

I r

G

G

WELL CONSTRUCTION

BOREHOLE DIMENSIONS

Land Surface Elevation at well

Casing Height (stick-up) above land surface

4- / . / ^ Date well completed _ _ , _ _

Depths: Total ' ^ ^ ft.

/M .1 Diameter: Top s H in,

/ u ft. Elevation was determined using

_ Z ft.

Finished / - ^ - ^ ft,

Bottom V / / !^ /^s ^J t^ê/ '

D E P T H T O T O P ( F T . )

G

Casing 1

Casing 2

Casing 3

Screen 1

Screen 2

Tail Piece

Gravel Pack . . .

Grout y f d ^ ^ 0 a h S c t - f ^ ^ r - ' 5 u r h c y

Grouting Method y ^ c s s u r - f

L E N G T H ( F T . )

D I A M E T E R ( IN . )

y

JL

i'.yc.

T Y P E A N D M A T E R I A L Screens: Note Slot Size(e)

/4svyi_

'M- p .y^ - ^Sh : / ' ^ g ^ o

^•2^ lyefp J e f T


Water rises to . ft. above the land surface.

/-^ RECORD OF TEST

Static water-level before p u m p i n g ^

-, Water level was measured using T T ^ ^ H € - ^ S U f t - '

Discharge rate measured using ^ . y ^ i - Q i ^ z r c a ri>it' '

- Well was pumped using / /» ' f Cyp/>.pr - f^ , -s t a / "

• I / ; Test Date i

I ft. below land surface. Water level

Drawdown

_ft. below land surface after. . hrs. of pumping.

Observed effects (jn.nearby wells

Water Qiiality (taste, odor, color, etc.] /y<:)Af.

Discharge Rate

Specific Capacity

/ o gals, per min.

gals, per min. per f t . of drawdown

j r e ^ ^ J z PERMANENT PUMPING EQUIPMENT Mfrs. Name •

Installed by_ m. L t ^ Pump Type.

Model.

CAPACITY: Pump delivers

POWER: _ _ _ _ _ _ _ _ _ _ HP at .

DEPTHS: Pump

FLOWMETER: Model

. GPM at

ft.

: RPM

Footpiece

PSI pressure.

Power Source .

ft. Airline . f t .

installed on . in. diameter pipe.

CONTRACTOR - Name of Drilling Contrartor

AririrPss £ ^ / L J-:.-M-ajC 2^

City ^ ^ 3 l / . c i ^ ' > 0 * n

Name of Driller p ^ ? ^ k f ^ r U f o n p i State ~ M ^ Zip Code

License No.

Signature of Contractor ^X^ru<^, tygj^ y oAjAÔ Date 1 / i l l -

DWR-138 P- 8/91

New Jersey Department of Environmental Protection and Energy Bureau of Water Allocation

PAGE 2 OF 2

WELLRECORO Well Permit




Drilling Method

• Yes C3p No

ôM^ Type of Rig

Aquifer/Geo. Fm.

A^y^^/.

A/>//^f? oJ

G

G

LOG

^-Oô ' - rlr-ûf^sc 6p/>?,/î?/

GWPI No.

Latitude

D v • 5" Lat-Long Accuracy

USGS Quadrangle

Drainage Basin Code

OTHER FILES: • Lithologic Log • Geophysical Logs

Checked by

D I G " 0 20"

'y\ 33 (o\L P E P USE ONLY


USGS Hydrogeo Code

Depth to Bedrock

Bedrock Lith. Code

Bedrock Fm. Code

Completed by

Date

Thick.

NJPDES No.

Longitude


[m Samples Available Q Aquifer Test

• Water Chemistry . • Pollution Case

Lith. Fm.


Date / . / .

G

G

G

G

DWR-138 8/B1

New Jersey Department of Environmental Protectton and Energy Bureau of Water Allocation

WELL RECORD

2 » Well Permit No. Atlas Sheet Coordinates 29 3 3

PAGE 1 OF 2

A y

OWNER IDENTIFICATION - Owner. Aririreit Z I M COTTONUOOB DRIVE

nitv SE* e n r r

WELL LOCATION • If not the same ownerplease give address. Owner's Well No. Addren ^ A M ^

State • • ^

/

Zio Code

County NCMMOVni Municipality UMLL T U P . Lot No.. Block No.. T2m

WELL lifiF /RA/SAT/OAy Status. ^T&A^r^h/f^f^ ( JS-^

WATER USE /^fi-V^/^


Land Surface Elevation at well Casing Height (stick-up) above land suiface _

DEPTH T O T O P ( F T . |

Average

9 ^3o gals, daily

/ - 2îS^ Date well completed Depths: Total ^ O ft, Diameter: Top n in

& ( ^ ft. Elevation was determined using

Finished y » f t . Bottom j?" in.

. f t .

Maximum

-MJL^

/ O o O gal,, daily


L E N G T H (FT.)

j o


T Y P E A N D M A T E R I A L Screens: Note Slot Slxe(»)

PVC -^cji^Dfjf.^yf^» 2>

} U ^

^9r JJ2=. -as:

J ^

f(^9fi>vfi^ Afz-ou-r

pi/c^\AJtx.e~ iJuaijAyp yyg.s^^^ r

WELL FLOWS NATURALLY gals, per min. at ft. above the land surface. Water rises to < — ft. above the land surface.

RECORD OF TEST Static water-level before pumping. Water level was measured using _ Discharge rate measured using Well was pumped using Observed effects on nearby wells

TestOate g / / ? / 9 3 / y ft. below land surface. Water level ^ ^ ft. below land surface after " y hrs. of pumping.

fp^TC^ti- Drawdown / / ft. /? fir / C^ Discharge Rate gals, per min.

^ H ^ C c i f > / \ p ^ ' S ^ S S o / \ . Specific Capacity gals, per min. per ft. of drawdown

^ - Water Quality (taste, odor, color, etc.) - / u ^ t L 2:

C.Oia/K/*^

PERMANENT PUMPING EQUIPMENT Mfrs. Name .TTA. t ^ i t i r

Installed by_ Pit? 1,1^^^

CAPACITY: Pump deliwrs ^ HP at J i j ^ r o . POWER:

V ^ j L - G P M a t - ^ . PSI pressure.

Pump Type ^/'/'//f^l^^fjfir Model fj-/YCfl3^^

DEPTHS: Pump / C ft. RPM

Footpiece Power Source ^ ^ f / e - f c ^

FLOWMETER: Model MICH. 6UNTHER WELL &


•OWMOU-1 3 ^ . in. diameter pipe.

City /^torrr--'' S D E T t t ^ s H : ^

Name of Driller / ^ / C / i 4 i i ^ ^ i / / J ^ / / / f -t K ^ ' i^ ^ '>^ '

State -\ 1 \ S - •

. / / • ^ Zip Code f f - 7 ? J License No. -M2-

Signature of Contractor Date Jî.y—i£f. COPIES: Whha-DEPE Canary - Driller Pink-0¥vner GoUenmd • Health Dept

WELREC 112 1710

G

G

G

G

G

DWFH38 8/91

New Jersey Department of Environmental Protection and Energy Bureau of Water ADocatren

PAGE 2 OF 2

WELL RECORD Well Permit No


1 ^ 0 Are samples available?

Drilling Method

Type of Rig

• Yes

M A H y £ V ^

Aquifer/Geo. Fm.. c o/^f\ t ^ ^ f y

LOG

( p - * ^ ^ A / t ^ y J ^ C U / i y ' ^ 6/ iAuJ9£. g - - ^» - -ôf^-T Af ixfWH j> / i / ^ />

(SP-fiVfi ^ -,-g ^ - ^ ^ f i i K ^ ^ y e / , c ^ i / ^ ^ A f o f i < & - C U A y

^ f \ t ^ t > i M t - ^

yg-J to =• &^ficK c i^ f iy

DEP USE ONLY


USGS Hydrogeo Code Depth to Bedrock Bedrock Lith. Cods Bedrock Fm.Code

Complatsd by Date

Thick. Lith. Fm.

GWPI No .

Latitude

NJPDES No.

Longitude Lat-Long Accuracy I D l " O S " • 10"

USGS QuadranBia Drainage Basin Code

• 20"

County/Municipality Code OTHER FILES: • Lithologic Log


Checked by

• Samples Available CD Aquifer Test O Water Chemistry [H Pollution Case


Data ./-m^Mmmim

! v c . v.- !•.; i * 1 ..* ? '•

WELREC 112 1711

DWP-13»^ 8/B1

^ . . " .r NwivJereayDepMtmantofEiwIrennwntelProlKalonandEnMgy

BuTMtu of WtiM AfccHion PAGE 1 OF 2

WtllPMrmitNo ^ _ — _ _ ^ Atlas ShMtCoordinatti S

OWjiER IDENTIFICATION - Owner. Ad4rm

City

MMIg . t?QBH 2agr fflMsngJABE-

Sti t i -KL ZIP Code e ^ 8 7 S - 0

WELL LOCATION - If not the ama owner plun give iddmi OiMMr'i Wall No. Addren

CoUnty

G

G

G

G

G

jxMfnm- Municipality. W^TJ. 1W» Lot No.. _2SL_ Block No.. 2 ^ L .

WELLUSE_

WAITER USE

<^rte*%TZXL. A-.

WELL COWTRUCTION

BOREHOLE DIMENSIONS

Lai d Surface Elevation et «mll Casing Height (stIck-up) above land surface _

DEPTH TO TOP (FT.)

l i ^

y^fU^/9^?r(?*J

Avtrags

n.<«ii«llgnmpltiH ^ j (s> / ^ ^

Depths: Total ¥ t f ft. Finished * ^ ft. DiametK: Top & '

Status " ^ l - t > ^ S

^ ^ ' ^ ^ giis. daily Maximum i r 0 o gals, daily

_fL - Z^

_ in. Bottom Elevation was datarminad using inad using ' S ? r ^ ^ f * ^ ' ^ i ^ e

LENQTH (FT.I

DIAMKTKR (IN.)

Casing 1 Casing 2 CasmgS Screen 1 Screen 2 Tall Place Gravel Pack Grout Grouting Method

Jli ^ l ^ ^ * , ^ < ^ TYPE AND MATERIAL

Screens: Note Slot Bl*e(e)

'U<^

I ^ . ^ » . ^ ^ C / .<?fS-"<,d>r ' \

/ • z - f a ' T

f /Pr WELL FLOWS NATURALLY ^ y / f - gals, par min. at ft. above the land surface. Wal{ar rises to f t above the land surface.

RECORD OF TEST Static watar-leval befora pumping Water level «MS measured using Disfharga rats measured u»ng

TestOate ^ / fe? / * ? S ^

f t ^ o w land su rface. Water level ( ^ n j f / n . / f j ^ _ Dnwdown

Weil was pumped using A f r t f "^fiTT^

f y J t below land surface after. / hrs. of pumping.

Observed affects on naaiby walls A J p r ^ ^ :

DIsthaiga B«t» / J gi l i . per min.

Specific C^Mcity ^ - ^ " gals, par min. per ft. of drawdown

Water Quality (taste, odor, color,ete.l i r ^ * ^

PEIÎANENT P U p N G EQUIMENT Instilled

Mfn-NaiM / ^ • c ^ ^

hy g y f r ^ ^ - ^ Trrfi

2 ^ .GPM at CAPACITY: Pump delivers POWER: / . HPat l S ^ I " o RPM DEPTHS: Pump f * / A - ft. Footpiece FLOWMETER: Mndri A / ^ ^

^ Modil.

Pump Typi ,. ^ C7g g 7 ~ ^

PSI pressure. Power Source .

ft

T ^ ^ ' U O t . T / f fv iP! tn -û Airline

installed on .f t .

. in. diameter pipe.

. T K S R OGHSIBDCnCN OGBP


COPIES: WMla-DEPE Canmy-Driihr Pink-Ommr QeUmwod-HeekhDapt

WELREC 112 2870

oWR-ias 8/B1

New JareeyDepwttmni of DwfcpiwamalProacilon and Energy BuiMu of Water Mocalion

PAGE 2 OF 2

WELL RECORD Wall Permit No

Ori ier: Plaasa use the ^Moa below for the log dascription. Note water bearing zones or geological formation.

Are samples awHaUeT

Dril

• Yes [^No

lling Method ^ i ^ f T i ^ y i ^

Typie of Rig ^ > ^ T < - ^ A A ^ C^-rr

Aqtîfar/Gao. Fm. ^ *^y9^S. ^

L06

•f i- i^VK.

^ ' / r \ f0 *< j>^ i I ^ W T t T + t t m i ^ 3i6-v^^ 4 _ '-J^ ^ / t ^ ^ g j n

r t ^ - « ^ j t f -A) i / m ^ ^ < y u ^ ^ > ^ ^ » ^ ^ V

G

G

2-°>-3l.'520

DEP USE ONLY

Storet Hydrogeo code USGS Hydrogeo Code Oapth to Bedrock — Bedrock Lith. Coda Badrook Fm. Coda

f t .

Completed by Oet*

Thick. Lith. Fm.

(JWPI No. ^

I latitude Lat-Long Aoeuracy

USG6( • l" 0 5 "

NJPDES No.

Longitude D I O " DZO"

pralnagi Elaein Cede _ _ _ _ _ _ ^ _ _ _

.pTHER FILES: • LItholooie Leg I a Qeophytical Logs


• SamptatAwillabte • Aquifer Test O Water Cbemiitry D r^>llution Case

a Water Level Data

isdby Date . / -

WELREC 112 2871

G

G

G

DWR-138 . 8/91

^

y^' \ d : s New Jersey Department of Environmental Protection and Energy • ^ ^ ^ Bureau of Water Allocation

WELL RECORD

Weil Permit No. Ades Sheet Coordinetes

OWNER lOENTIFICATION • Owner. Address City

L d O O , MTEHON?

SBAUIKI'

WELL LOCATION - If not the same owner please give eddress.

Address, County , Huwu/m Municipelity .

Owner's Well No.

wan. THP.

State

/

-IKT ZinCnde <^.S^7J'C?

Lot No.. -2r Block No. . -28S-

WELL USE

WATER USE

A Z7f3-

gals. daily Maximum "ôt^v gals, dally


/ ^ ^ Date well completed ' ^ / Depths: Total y - ' g - f t . Finished. Oiemeter: Top V ' ^ in. Bottom

Lend Surface Elevation et well _ _ 2 ^ _ f t . _ Elevetlon was determined using r ^ r ^ r I f T r (fi »J" in.

Cssing Height (stick-up) above land surface - 7 -^


DEPTH TO TOP (PT.)

LENGTH (FT.)

T^L

DIAMBTER (IN.j

TYPE AND MATERIAL Screens: Note Slot Sized)

:ki2. 7T -A : L 2 .

f " ^ ^fl^ff^î? yyhfrnf f f

^ A H». WELL FLOWS NATURALLY ' ^ ^ f f gals, per min. at ft. above the land surface. Weter rises to ft. above the land surfece.

TestOate ^ < ^ j / 6 / 9 ^ I T ^ ftrtelo w lend su rface. Water level

nîcOff^ ^Mf^^^B Drawdown

Discharge rate measured USIM ^ V I

RECORD OF TEST Static water-level before pumping Water level wu meesured using

/r

Well was pumped using -Observed effects on neerfoy wells ^ A ^ g " Weter Quelity (taste, odor, color, etc.)

^ - i c O / f f JhKi>i^f^S

nÔf^rr ^ lA/ATZ.^ Dischaqia Rate.

_ft. below lend surfece after.

.ft.

1 hn. of pumping.

Specific Capecity f - ^ gals, per min. S \ 0 gals, per min. per ft. of drawdown

f ^ e h

PERMANENTPU Mfrs. Name

6 EQUIPMENT Installed by / ^ f C M / H ^ . ^»^/^*Cl/7-a Rump Type C M t t ^ i ^ W ( ? ^ ( J ^ ^

T ^ PSI pressure. CAPACITY: Pump delivers / r " GPM at POWER: f HPat l ^ r h RPM

DEPTHS: Pump , ft. FLOWMETER: Model - T C ^

Power Source Footpiece - — ft.

»>>/g Airiine

instelledon < .ft .

. in. diameter pipe. cr r rph4

CONTRACTI AdHres$^_jfc "fiSym

•nCSR OQHSIBDCnON OGBP

Name of Driller

Signature of Contractor Date /<P f ^ ^ f 9 ^

CO'IES: WtwH-DEPE Canaiy-Dtaer PUt-Omar GoUenrod-HeMtOept.

WELREC 112 2872

c G

DWfV138 8/91

I4ew Jersey Dapaitmant of Environmental Protection and Energy Bureau of Water AUocadon

PAGE 2 OF 2

W E L L RECORD Well Permit No

Drill|er: Please use the specs below for the log description. Note water bearing zones or geological formation.

^ C T N O Are samples availi

Drilling Method

l«6K? Q Y e s Si

Type of Rig ^ J ^ W^f^ C^^'T' y^

Aquifer/Geo. Fm.

LOG

^ ' 7 n/iî*^ '(Z^ t$îr^ ^ /4ai*vgr^

7- ^2^ /v~/^ y t ^ / / 7W- " ^

^ m L

^ 1 33 6a/ DEP USE ONLY

Storet Hydrogeo Cods

USGS Hydrogeo Code

Depth to Bedrock

Bedrock L i th. Coda-Bedrock Fm. Cods _ _

Completed by

Date

Thick.

GWPI No.

Latitude

NJPDES NO.

Longitude

Lat-Long Accuracy • 1 " • 5 " • 10" • 20"

USGS Quadrangle

Drainage Basin Code County/Municipality Code

OTHER FILES: • L i t h o l o g i c L o g • Samplas Available • Aquifer Test

• Geophysical Logs • Water Chemistry , • Pollution Case

Checked by Date ./ / .

Li th . Fm.

• Water Laval Data

WELREC 112 2873

r

G

G

G

G

G

OWF ISS SI9B

New Jersey Oepartnient d Environmental Protection Bureau of Water Allocation

WELL RECQHP Well Permit Number

2 9 - 355at.

OWMER.

Address

City

CRISTHJj, JRMJK & LflflBA 12W BOBJOCR AVE

Atlas Sheet Coordinates

29 3 a - : - .JZ6-

VULL State -w Zip Code

WELL LOCATIONADOgCSS. County VU^liXjm

1210 EOaaX. AVE Owner's WeH No. Municipality Lot No. Block No. z/8.in.

WELL USE IHBIGATION DATE WELL STARTED DATE WELL COMPLETED

WELL CONSTRUCTION

Total Depth Drilled / / • > y

Finished Well Depth / / /

Borehole Diameter:

.ft.

ft.

T o p _ Bottom

.in-- in-

Well Casing Begins:

71 .ft. above grade or ,ft. tMlow grade

RECORD OFTEST ^ .

TestOate * 7 ' ^ ^ ' % ^ Static Water Level ( p ? 3 _ ft. Dei Water Level Measured Using \ j f ^ - i p (

Note: Maeawe an depths from land surface

Single/Inner Casing Middle Casing (lor triple cased viwlle only) Outer Casing (largest dameter) Open Hole or Screen (No. Used ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft)

/ '

9 / '

?/ ' r

Dapttilo Bottom (ft.)

9r

/ / / '

. / / / *

?/

Diameter (Inches)

< / ^

i ^ f i

r' ^ ' ^

Material

j p ^ t / e

A<^

S»**^xl Neat Cement Bentonite

WfiL/RatInQ (iba/ach no.)

^ C A ^

Su^^r

•70 0 lbs

c ^ Z C I b s

b low land surface Grouting Method. Drilling Method _

^

Pumping Water Level. Well Was Pumped Using _ Well Yield ^ / l - ^ gpm If Pump Tested: Discharge Rate _

Duratton of Test

ft. befcnv land surface i j r _

.gpm hours

PERMANENTPUIMPING EQUIPMENT Instaled by ^ . ^ . g ^ J ^ ^ - ^ Reg. No. € > t i l n l S ^

Pump Type £ t . M l r t ^ . f ^ r i C x Depth of Pump below land surface Capacity S d gpm

^xL Horsepower

/ certify that I have constructed the above referericed well In accordarKo with all well permit requirements and applicable State rules and regciations.

Drilling (Company

Well Driller (Print) l ^ A > * . j ^ A , ^ i ^ ^

Driller's Signature J c y L J ^ ^ r " ^ ^

Registration \ia.O0(h / " ^ ^ 0 Date ^ I ^ I 9 ^

GEOLOGtC LOG

Note each depth where water was encountered in consolidated fomâtions. ^ ^ ^ ^ f ^ ^ ^ ^

^ ^ - ^ y ' ;g.cr-/>-VY

< - ^ ' / / y ' s^c?^^ ^ ' . ^ . . j ^ ^ -

r/^ -g. y y * ^

/ /«/ ' //jr^ ^ ^ .7 - ^^

COPIES: White- DEP Canary - Driller Pink-Owner Goldenrod - Health Dept.

WELREC 164 1093

G

G

G

G

G

DWR-138> 5/95

.1 y ^ New Jersey Department of Environmental Protection i / f ^ Bureau of Water Allocation

OWNER.

/Vddress

Chy

H'

P A T R i r y . BRYAN T.

WELL R5CQRP

112 BEADNATER DR

Well Permit Number 99 - a f l m a

Atlas Sheet Coordinates 29: 33 : 387.

"HHDRIBD" state "W

WELL L 0 C A T I 0 N A I ) D R ^ ^ _ ^ 1 ^ ^ ^ _ ^

Zip Code

County

WELL USE IRRIGATICM

Municipality H&I i i ' i W . Owner's Well No.

Lot No. T Block No. zib.va DATE WELL STARTED . 3 .

DATE WELL COMPLETED j ^ I

WELL CONSTRUCTION T

j y _ n . Total Depth Dr i l led,

Finished Well Depth

Borehole Diameter: y ) Top y ; yUC.

^ y t in. Bottom

Well Casing Begins:

• / -

.ft. above grade or .ft. below grade

RECORD OF TI Test Date TU.

Note: Measure ail depths from land surface

Single/Inner Casing Middle Casing (for triple cased wells onlyj

Outer Casing (largest diameter)

Open Hole or Screen (No. Used / )

Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft)

^ / / "

C ^

c ^ y

Depth to Bottom (H.)

r?/

-2r>

^ '

Diameter (inches)

• i ^

/

y

Material WgtTRating (Iba/ach no.)

^ s f S ^ ^ r / ^ ^ X T"" ^

S^r

^ . . ^ ^ ^

Neat Cement Bentonite

^ ^

/Ar. lbs lbs

ft. below land surface Static Water Level X t < ^ * Water Level Measured Using ,^;^:^^^^g^^ ^ / t - ' y ^ S y & O Pumping Water Level ^ y ' * C J ^ ft. below land surface Well Was Pumped Using ^ " S ^ . • y ^ < i r ^ v ^ ' f c ^ ' ' ^ / ^ Well Yield y y V gpm

Grouting Method ^ Drilling Method ^ ^ / V J ^ / ^ ^ ^

If Pump Tested: Discharge Rate. Duration of Test

.gpm hours

PERMANENT£.UMPIN

Installed b y < r 7 ^ / Pump Type . < S ^ < ^ .

QUJPMENT ^ <f/i^/yKeti. No. ^ & ^ f

Depth of Pump below land surface . - , 2 / Capacity / d ^ gpm Horsepower.

/ csrtity that I have constmcted the above referenced well in accordance with all well permit requirements and applicable State rules and regulations.

CRE?rVIEH HELL DRILLINS Drilling Company Well Driller (Print;

Driller's Signatun

Registration No.

G E O L O G I C L O G

Note each depth where water was encountered In consolidated formations.

f ^ - y / ' /9:?dsr}r /^:ky2s^ îtê^j<T

y ^ A . ^ r / / J / ^ ^ i ^ ^ ^ ^ j o W(^ j ( ,>y:^^

^ ^ —

/ ^ y ? € ^ Date f " > - ^> ^

COPIES: White- DEP Canary - Driller Pink-Owner Goklenrod - Health Dept ,^.'

^ • • ' ^ ^

WELREC 164 1104

G

G

G

G

G

DWR-138 5/95 ?) New Jersey Department of Environmental Pro|j

Bureau of Water Allocatlon> Hon

WELLRECQRPi Well Permit Number

a » — — 37715

OWNER—MiHiotT. j o c a n i w n


^ - ' - 3 3 = - 3 ? 6 -Address 1225 nANDLEWOQD LANE

SEAGIRT City

WELL LOCATION ADDRESS 1225 CANDCEHOOD LAHE County MOmxyrH Munidpanty WMJ< 1WP.

.State NJ Zip Code

Owner's Well No. Lot No. 1 Block No278.02

WELL USE TRRTGftTIQH DATE WELL STARTED fP- I ^ I 7 "? DATE WELL COMPLETED /«g / 6 / 7

WELL CONSTRUCTION

Total Depth DriBed H ^

Rnished Well Deptti / ^ 3

Borehole Diameter ^ Top. Bottom

Well Casing Begins:

-ft.

. f t .

.In. .In.

f t above grade or f t below grade

RECORD OF TEST TestOate ID . / / ^ / ^ 7 Static Water Level ^ ^ O

Note: Measure all deptha from land surface

Single/Inner Casing Middle Casing (for triple cased wells only) Outer Casing (largest diameter)

Open Hole or Screen (No. Used 1 ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth tio Top (ft)

/

f3

f3 C^

Depth to Bottom (ft.)

f3

l P 3

/z>3

^ 3

Diameter (Inches)

r Material

PYC

Fv^^

^ l ^ ^ x / ^ L -Nwtpemant

^BentonitS^

Wgt/Ratlng (Iba/ach no!)

SftH'/o

lbs ? j r > lbs

. f t below land surface Water Level Measured Using H f ^ ^ Pumping Water Level 3Lg^ ft below land surface Well Was P u m j ^ Using / i / g - l A I ^ T ' WellYleW.

Grouting Method 'P/gg3Vt.^g^''i*<iats»«J>^»/ ^TggVnug Drilling Method '\^€9^0QttJ>f

umoedl

gpm If Pump Tested: Discharge Rate _

Duratton of Test _ -OPm

.hours

Note each depth wfiere water was encountered In consolidated formaUons.

PERMANENT PUMPING EQUIPMENT

Installed b y d s i l ^ i l d f l ^ ^ ! Reg. N o ^ i J i f M . Pump Type j S E ^ a m ^ i A ^

^g^taîvig^s-tbrîa^gîdK^b t v / / / ^ w t g L ^ G ^ ' y

i r r ap^ i . ^ ,2 .<^>J . K^j irfG^CJL^\^

J^^L Depth of Pump below land surface. Capacity ^ ^ gpm Horsepower i H ^

ft. f o - L ^ ^ w e ^ A r ' h ^ { ^ 0 ^ <riîlY

I cwrtHy thai I have constructed Vie above referenced w^\ In _ . . .. 8f^>MU.}ft^t€h ( • \ ( t i ^ 4 e 9 * ^ w / uLxafT Ba»rdanc9 whhaH well permit reqwrernerrts and apiî^mt-'SMe}, " ',, njles aiKl regulations.

Drilling Company MARSH OOHSTROCTIOHAIRAIQ y ^ ^

Well Driller

Driller's Sign iati<m , A ^ ^ / * S

Registration U o . f f l ' f S ^

COPIES:

_ Date / ^ - /.<2g / f 7

IVWte - OEP Canary • DrWer

GEOLOGIC LOG

^ . g i 3 | i ^ » i ^ ^ < ^ l ^

\H444^

Plnl(-Owner Qoldeniod • Health Dept

WELREC 164 1096

G

G

G

G

G

G

G

DWR-138 5/95

New Jersey Department of Environmental Protection ^ Bureau of Water Allocation

«^'^ WELL RECORD Well Perniit Number

^ - — 37710

OWNER.

Address

City

LADOOH, ROOEBT W PLSfi nr.n M H T . HD


29=—93—'•—3=?e-

SEA GIRT

WELL LOCATION ADDRESS 2156 OM) ttTTJ. RD County W m X S m Municipality WALL TWP.

.State NJ Zip Code

Owner's Well No Lot No. 2 Block No. 278 .02

WELL USE TTOTRATTnW DATE WELL COMPLETED / ^ I S~ I ? 7

DATE WELL STARTED

WELL CONSTRUCTION

Total Depth Drilled f / O

Finished Well Depth )C>S

Borehole Diameter

.ft.

. f t

Top Bottom.

8 yj3L

.in. - In.

Well Casing Begins: . ft. above grade or . f t below grade

RECORD OF TEST TestOate / Z . I ^ I ' f l Statk: Watw Level J l o ^

None: Meaauraalldaptha from land surface

Single/Inner Casing Middle Casing (for triple cased wells only)

Outer Casing (largest dameter)

Open Hole or Screen (No. Used / ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Deptlito

/

13

^ 3

o

Depth to Bottom (ft)

fs

/ ^ 3

/ ^ > ^

f3

Dlametar (Inches)

r

^ "

Material

/Vc

e^yc

Nmt Cement C Bentonite^

WgURatlng (Ibsteeh no!)

SCJH4*>

SCMHP

lbs \ S - f lbs

.ft. below land surface Water Level Measured Using j ^ / ^ g " Pumping Water Level ^ S ^

Grouting Method "PggS<otf«? T M O t ^ ^ ^ t ^ * ^ i g Drilling Method ' ^ ^ t A ^ i z y

Weil Was Pumped Using A l O - t - l ^ ^ Well Yiekl l o P gpm If Pump Tested: Discharge Rate _

Duratton of Test _

. f t below land surface

-flpm .hours

Note each depth where water was encountered In consolklated formations.

PERMANENT PUMPING EQUIPMENT Installed by O z A i i ^ W i A d J ^ Reg. No-CTlt/'S^ Pump Type ( tk f* < ^ ^ g r K ^ < a 4 t < S c ^ Depth of Pump below land surface ^ S Capacity a t ^ gpm Horsepower \ i i P

ft

^ ^ S i D ^ i i ^ i g < A u . y . u ^ \ t ^ a ^ / ^ - 4 ~

I certify Oiat I have constmcted the above referenced well in ^ accordance with all wellpennit requirements and applicable State mies ar)d regulatlorts.

Drilling Company MARSH OONSTRDCTKM/CRAIG MAtJaft-

Well Driller f P r i n t j ^ / d ^ t j i U i ^ e ^ t ^

A7> Driller's Signatme

Reglstratten No. C P * / " - ^ ^

COPIES:

•in^>f _ Date l 7 . I 1 o i ^ y

While • DEP Canary • Driller

GEOLOGIC LOG

2 ^ '^S-fn^t. To Cj,îf i i^ 4a>^ fiâAx^xÔA^

c t r - ^ o i^ i t ,<£<A*yh

i ^ o i i a n n ^ 6 ^ ^ 4^*.t, U ^ [ U J ^ « > K ,

:y:;yv^

rt'—1.1 . ' • '

Pink • Owner Ooldenrod - Health Dept

WELREC 164 1095

G

G

G

G

G

DWR-138 5/95

New Jersey Department of Environmental Pi Bureau of Water Allocation

WELLRECORP

OWNER.

Address

VMBA. x m

Well Penmit Number a t - 37861

Atlas Sheet Coordinates 2 » 33 : - 376

2160 eE4> tBELL i S . S » G I R f

City .State -RT

ZipCode

WELL L-OC13|| [^^m»e88. County

2160 OLD m U , RD. -Httt-nr:

Owiier's Well No.

Municipality Lot No. T Block No. 278.02

WELL USE msLGnnxM DATE WELL STARTED / A / / "7 / ^ 7 DATE WELL COMPLETED / . ^ I / I I ^ 7

WELL CONSTRUCTION

Total Deptti Drilled I f O

Finfehed WoH Depth 1 ^ '

Borehole Diameter :^ Top: Q , Bottom. a-

^

.in. _in.

Well Casing Begins: . f t above grade or . ft. t>elow grade

RECORD OF TEST Test Date I S L I J B / * ? 7 Static Water Level «^<?

ff

f t

> or

Note: Measure eO daptha from land surface



Open Hole or Screen (No. Used / )


Tailpiece

Gravel Pack

Grout

Depth 10 Top (ft)

/

f^^

^ - ^

o

B ^ m ( f t )

fr-^

/ a f ^

l o £ ^ fr^

Diameter (Inches)

V"

r

Material

pVc

e/c

t ^ ^rh&>£L^ Neat Cement TBentonif^

Wgt/Ratina (IbaAch n<x)

^^^h

lbs 3i!S_lbs

. ft. t>ek>w land surface Water Level Measured Using \ A c ^ ^ Pumping Wider Level 3 » - ^ ft. below land surface WeH Was Pumped Uslno ^ I f - L - l f T WellYlekl.

Groutlna Method ' P a e S 6 * 4 t e ' m n e > i ^ ^ 4 ^ T g i T w i ^ ' Drilling Metttod T ^ p T ^ a ^ L y

Pumped Using.

flpm If Pump Tested: Discharge Rate _

Duration of Test _ .gpm

.hours

PERMANEKT PUMPING EQUIPMENT Installed b y O u H ^ t l U A t t f ^

Note each depth wliere water was encountered In consolidated ionnatlons.

. Reg. No »<rt4s<? Pump Type H k f A i ^ A M ^ ^ H t S j a ^ u T Depth of Puthp below land surface t e S ^

Capacity ^ l O gpm Horsepower / H P

f t

/ c e r f ^ that I have constmcted the above referenced ^ l^y>V B ;' I accordance with all well permit requirements and afîcabJe State'-mies and ref la t ions.

Drilling company Mt^f iH O O H g l W m O H / G B f t | i B ^ g g *

Welt Driller (Print;

Driller's Si{

Registration N o . ^ J / ^ / ^ f ' Date / 2> / A : ? 1 ^ 1

GEOLOGIC LOG

t C ' t J r ^ l , ^ 4 l » e ^ t \ a^ t ^ - t / % a ^

B O ' M O M ^ ^ S f c ^ ^ ^ A * ^ L>^t<w<:.v i^ i ^ / . K .

. T " ,—ro»-

COPIES: White-DEP Canary - Driller Pink-Owner Goldenrod - Health Dept

WELREC 164 1094

c

G

G

G

DWR-138 5/95

New Jersey Department of Environmental Protection ^ Bureau of Water Allocation

WELL RECORD Well Permit Number 9a — . ^ 4 7 R

OWNER

Address

City

TTMO. Tf^ Atlas Sheet Coordinates

2 9 ^ : - 3 3 • 384 1 2 3 3 QMQjElffiQD LA SEA Giiî'

WELL LOCATION ADDRESS 1220 CAWELSWOOD LA

County ^ ™ ™ ^

. State "KT

Zip Code osnô

Municipality WALL 'IVd:'. Lot No ^ ijvner's Well No.

Block Nd: 278"

wELLusgroRiG^TiQW DATE WELL STARTED ^ /O?^ 7 7 < ^ DATE WELL COMPLETED ^ I ^ " ^ I 1 z i

WELL CONSTRUCTION

Total Depth Drilled K ^

Finished Well Depth " ^ P

Borehole Diameter:

.ft.

_ft.

Top Bottom.

- ^ .in. in.

Well Casing Begins: . ft. above grade or . ft. below grade

RECORD OF TEST

Test Date ^ I ^ " ^ I f ^ Static Water Level. l ^

Note: Measure all depths from land surface



Open Hole or Screen (No. Used / ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft)

- /

B3

ee " ^ ^


&€>

IB

IS a'8

Diameter (inches)

f

^

Material

F^^

PV<L

4 l^ ,^ j^ bletf£efflent

( Bentonite^

WgtTRating (Ibs/sch no.)

r^^ô

. £ 3 1 ^

, - lbs y^fZ^^lbs

.ft. below land surface

Water Level Measured Using f 4 ' £ > i ^

Grouting Method F / g e : $ S * J ^ g ^ ^ / ^ ^ - ^ ^ ^ ^ ^ » ^ ^ t o Drilling Method t »-M- C r Z e s ^ U r t ^ ,

Pumping Water Level c ^ ^ ft. below land surface Well Was Pumped Using A ( t 2 ^ i - ^ t ^ ^

Well Yield " ^ ^ gpm

If Pump Tested: Discharge Rate gpm

Duration of Test hours

PERMANENT PUMPING EQUIPMENT Installed by C^t,y^rZ4,\4 ^ Reg. No.-^Hi^H. Pump Type ^ J ^ ^ A t ^ ^ ^ » S U = i

Depth of Pump below land surface S ' s ft.

Capacity / P ^ gpm 1-lorsepower _Jt

Note each depth where water was encountered in consolidated formations.

ci^-/ie> ^ ^ ^ O ^ n . ^ - 1 <it3'^h .

/ certify that I have constmcted the above referenced well in accordance with all well permit requirements and applicable State mIes and regulations.

Drilling Company * « ^ ^ COKSrraXTnCM/CRAIG MAESI

Well Driller (Print;

Driller's SignatuJ

Registration No. C T ^ v B v Date ^ I X " ^ I T ^

GEOLOGIC LOG

- , , , , . — . • , ^ ^ ,

COPIES: White- DEP Canary - Driller Pink-Owner Goldenrod - Hoaiih n^nt

G

G

G

G

DWR-138 5/95

I i y New Jersey Department of Environmental Protection <,...^\ Bureau of Water Allocation

WELLRECORP W e l l P e i ^ N u m b ^ j ^

OWNER.

Address

REVERENDO, LEE Atlas Sh^MCoocdinates „ r >

1014 ATLANTIC AVE.

City "W5n7

. state Twr

Zip Code

WELL LOCATip.

County _

DRESS. Ii314 ATLAirriC AVE. WAUi TWP.

Owrwr's Well No.

Municipality Lot No. T

Block No. -380-

WELL USE IRRIGATION DATE WELL STARTED DATE WELL COMPLETED

WELL CONSTRUCTION

Total Depth Drilled. .2^ . f t .

Rnished Well Depth 7 ^ ft-

Borehole Diameter:^ ' f Top Q ^ — I n . Bottom e r In.

Well Casing Begins:

/ *" ft. below graide

RECORD OF TEST -

Test Date . ^ L _ / £ ^ C / J ^ 3 _ Static Water Level < 3 J i

Note: Maaaure all deptha from land aurfaee



Open Hole or Screen (No. Used )


Tail Piece

Gravel Pack

Grout

Depth to Top (a)

UL

(r3

M. / '


ir^'

ml

511 &r

Diameter (Inches)

y i ^

Material

P\y(L

Q L L ^

^ ' ^ ' ^ j f / S / i ^

Bentonite

. ft. betow land surface Water Level Measured Usln^ , ^ " W ^ p ^ l / ^ ^ - ^

Pumping Water Level ^ 3 , ft. below land surface

Well Was PumpedUsing ^ V

Well Yield i . 3 " ^ > ^ gpm

Grouting Method fl^-^^ f/lT-f

Drill ing Method /T/TNA-r^

WgtTRatIng (Iba/ach noO

^cAÛC

%xh^

•fes ,£CQ_lbs

If Pump Tested: Discharge Rate.

Duration of Test.

.gpm

.hours

PERMANENTraMMNGEQUIPMENT

Installed by , ^ ^ W > ^ ^ ^ c / y ^ ^ Reg. No. / / < ; 6 ? T

Pump Type ^ V r Junn f f ~ . < d J j l ^ ^ [

Depth of Pump below land surface J f ^ O ft.

Capacity ^ O gpm Horsepower /

/ certify that I have constructed the above referenced well in accordance with all well permit requirements and applicable State mIes and regulations.

Drilling Company RCBSBT AZDRAK

Well Driller (Print).

Driller's Signature

£- iL ^

^ ^ - l ^ y t ^ A/rn

Registration No. / / S f O - ^ Date / - 2 - / / 1 ^ ^

GEOLOGIC L O G

Note each depth where water was encountered In consolidated Ibrmaflons. i ' '

QfT^y^L

/ y ' y<7^ X z i ^ ^ s ^ 2 j h ^

%<. ' - 0 / y j ^

COPIES: White - DEP Canary - Driller Pink - Owner Goldenrod - Health Dept

WELREC 187 1076

_ A U G - 3 1 - 2 0 0 0 1 1 : 1 1 PM

DWR-138 S/96

P . 0 2

Nsw JeFsey Oepartmsnt of Environmental Protection Bureau of Watsr Allocation

WELLRECORP Well Permit Number

OWNER DUggY^ DAN

Alias ShMt Coordinates

29- = 3 3 • —299-i^ddress 2169 GLATglELD 1»

.ity WALL .State

NJ Zip Code

WELL • n rATiQM A n n a g f l a 2 1 6 9 GLADFIKLD DR

bounty M(l«HX7rH Municipality WALL TWP. . Owner ' s Well No

Lot No. ^ Block N o . - ^ 8 _

M/ELL USE IRHIGATIOH DATE WELL STARTED f I TC) I f i DATE WELL COMPLETED J ^ 'J^-S^ t

V /ELL CONSTRUCTION

total Depth Drilled ' ^ 0

G inished Well Depth. ik .ft.

.'ft.

Borehole Diameter Top c Bottom.

..In. _ln.

Weil Casing Begins: - j B y ft. above grade or ^ f ft. below grade Gi

RECORD OFTEST

i s tDate _ J jitic Water Level


Single/Inner Casing Middle Casing (for triple cased wells only) Outer Casing (largest dlametar)

Open Hole or Screen (No. Used . O / ^ )


Tall Piece

Gravel Pack

Grout

Depth to Top (ft)

- / '

r i , '

s r / '


5-6'

u '

/ , ( ,

S¥'

Diameter (Inches)

Y"

r

fl' 3y

Material

/ ' l /C

/ ' ly

^ / f ^ Neat Cement Bentonite

Wgtâting (Ibs/seh no.)

a/f¥C)

S'OOUs -ZS2_lb8

lbs

riCcr

\ 9 i ^ ft. below landsurfi 9I0W land surface Grouting Method. Orilling Method _

n g . . ft below land surface

Water Level Measured Usin; R-"Tiping Water Level « ill W a s Pumped Using f M , C L > ^ p t m / ) /l^ll Yield 9 ^ qprn*^ ' f ,ûmp Tested: Discharge Rate 2 \ J QQi^ .gpm

GEOLOGIC LOG Note each depth where water was encountered In coneolidatsd fbrmaHona.

Duration of T e s t . hours

'ERMANENT PUMPING. EQUIPMENT w ailed by CummiAf X i n a t l t t t i Reg. No. i n l T j •>P Type CXid lL f ' - ' ' ^

)epth of Pump below land siJrfaca . ^ O ^ ft.

acity p O gpm Horsepower / h ^

certify that I have eonatructed the above referenced well in i irdancB with all well permit r equ i rement a n d a f ^ c a b l e State i[ t and regulations. • . { /

rtlllng Company. D e ^ f e ^ n C W ^ / / O c i l k ^

I Driller (Print)_i5iliHo*aV E S ^ C p j ^ c i J f r

•iller's Signature - ^ ( y b y i i U t O ^ U ^ A ^ i f ^ j f j ^ ^ ^

^ Watlon No. \ H ^ y ] i ^ t e % I U S L I ? 8

O - f O

:iâ. Me<J

- J O I T

r £ n p r r f > y/V^c Z_ //-

3 > ; - ^ / H P W jr<inrJ j ^ 6 y / y A < ^ ^

/ • / • //

a/j-yo A- / f

' ZSZdEspi

c G

[

DWR-138 5/95

• ' " ^

New Jersey Department of Environmental Protection Bureau of Water Allocation

WELL RECORD Well Permit Number

2 9 — ~ 40112

OWNER

Address

City

PALLUZZI , ED Atlas Sheet Coordinates

2 r - ' ^ 3 • -3 8 ^ i ? i « ; PflMr>i Funnn i a SEA GIRT .State NJ Zip Code

WELL LOCATION ADDRESS. County MnNMOUTH

171S HANniFwnnn i A. Municipality SEA GIRT BORO

Owner's Well No.

Lot No. __A Block No. 278.01

WELL USE TPDTRATTnN 3 , c29 / ^? DATE WELL STARTED DATE WELL COMPLETED 3 /«^*? / ^ ^

WELL CONSTRUCTION

Total Depth Drilled. M£L

Finished Well Depth. ^2'A 'Q- ft.

Borehole Diameter; Top Bottom

.in. - i n .

Well Casing Begins:

J L ft. above grade or f t below grade

RECORD OF TEST Test Date Static Water Level

' S J ^


Single/Inner Casing

Middle Casing (for triple cased wells only)


Open Hole o f ^ c r e e n ^ (No. Used p T Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout Q

Depth to Top (ft)

- /

eet

sn'k


ne%

n^t

H&% en%

Diameter (inches)

r

r

Material

fi\/(L

P\i(L

• ^ ^

<^/.31ÂJD

QBentonite^

WgtVRating (Ibs/sch no.)

StUtiD

^ •vL . , / i i ^ - '

. _ lbs t f e lbs

s . ft. below land surface

Water Level Measured Using _ Pumping Water Level _ e?g>. Well Was Pumoed Using Well Yield A ^ O gpm

If Pump Tested: Discharge Rate. Duration of Test.

/oê^

Grouting Method ff- f .^ '^ l /^ Û)rOU/jln ^ e / r i / &

Drilling Method IÛQ ^T^k fJu

^ , ft. below land surface

.gpm . hours


^^p^metJS^f&Lpr Installed by Pump Type Depth of Pump below land surface. Capacity j f g f r ff-^ gpm

ReaNo.T/^^9

.M. Horsepower.

/ certify that I have constructed the above referenced well in accordance with ail well permit requirements and applicable State mIes and regulations.

Drilling Company MARSH CONSTRUCTION/CRAIG HARSH

Well Driller ^Print) ^ I J L f f i G , l f Y \ A ^ }

Driller's Signatur^

y . , „ . w . V,

GEOLOGIC LOG

Note each depth where water was encountered in consolidated fonnations.

.±11 Vna Ôndi '^•/iirt XTv^^y 31 ^ ^ ^ ^

<^^''iy^' P - i*^

1/^ âncL QrtKj ^sbimtcJEij

/n^gic^ S < ^ ^

f ^ P - H O I4n^b S<?Â t ^ f t ^ t f t f b *

Registration No. ' \ ^ \ ^ ? f \ Date .f_/^/31 COPIES: WhifB- DEP Canaru - nrillttr Pink - nu/nor r ^n l r i onmr l _ t - laal th Horyt

[ c c

[

DWR-138 5/95


WELL RECORD Well Perniit Number 29 _ 4 0 2 6 8

OWNER.

Address

City

DOLINER, PAUL Atlas Sheet Coordinates

2 9 - 3 3 . 3 7 6

2164 OLD MILL RD

SEA G IRT State NJ Zip Code

WELL LOCATION ADDRESS.

County MONMOUTH

2 1 6 4 OLD M I L L RD Owner 's Well No.

Municipality — S E A GIRT BORO Lot No. _4_ Block No. 2 7 3 . 0 2

WELL USE I R R I G A T I O N

DATE WELL STARTED

DATE WELL COMPLETED ^

6) /(9S/gl

WELL CONSTRUCTION

Total Depth Drilled I I P ) ft.

Finished Well Depth I 0 3 ft.

Borehole Diameter: Top Bot tom. is:

in. _ in .

Well Casing Begins:

X , ft. above grade or . ft. below grade

RECORD OF TEST

Test Date

Static Water Level


Single/Inner Casing


Outer Casing (largest diameter]

Open Hole o ^ c r e e n ; (No. Used I )


Tail Piece

Gravel Pack

Grout

= TEST ^ ^

Level / ^ > ft. below land surface

Water Level Measured IL'ting r N f i p y .

Depth to Top (ft)

' / '

^3'

^: i o

Deoth to Bottom (ft)

33L

lea'

U>2

V-

Diameter (inches)

±

Material

PVC. ^ ^ ' - { C

~ ,0l5S|o-(

• ^Ver ^ \ ÔTiA

Neat Cement Sentonite)

Wgt/Rating (Ibs/sch no.)

S € M - ^

, lbs

Grout ing Method

Dri l l ing Method _

Pumping Water Level

Well Was Pumpe i j ^ s i ng

Well Yield s 0 4 ^ gpm

If Pump Tested: Discharge Rate _

Duration of Test _

^ S ft. below land surfade

Oir \ \ ^

.gpm

.hours

PERMANENT PULPING EQUIPMENT - T i n

Installed by L • W N f X r S K Reg. No. O l H ' ^ n

Pump Type • ? ; i i h i r v > P J f S t b \ e ^

Depth of Pump below, land surface.

Capacity " ^ f e ' ^ / y ^ g p m

' ^ ..ft. Horsepower.

/ certify that i have constmcted the above referenced well in accordance with ai l well permit requirements and applicable State mIes a n d regulations.

Drilling Company H A R S H n n N f ^ T R l i n T i n N / n R f l T R M6R?^H

Well Driller (Prints

Driller's S ign

Registration No. J 3 i ! ± ^ _ _ _ Date O i J - Y I I f


Note each depth where water was encountered in consolidated formations. , .

Oo'-^s' - mpri-4^ ccâ^^. snrA-QV-QLvjei

g^rSf* . . Q V e y ^^ r iA^ t J i5?/VY\g C l iCu h (QYgy

Kd^-LBS^ - ^ r > p j ^ 9 ^ ? a n ( \ o ] n / ( ^ f I

:W

yh' -4S' - mpc\ nr-A/ f aaA - voivvj 9 ^

COPIES: White- DEP Canary-Driller Pink-Owner Goldenmd-Health Dept

c

c

DWR-138 5/95

LNew Jersey Department of Environmental Protection sr Bureau of Water Allocation

WELLRECORO Well Permit Number 29 40451

OWNER

Address

City

WILLIAMS, DONNA r z i t i fANULtWUUU LA.

Atlas Sheet Coordinates 29 .33 .384

SEA GIRT State NJ 1210 CANDLEWOOD LA.

Zip Code

WELL LOCATION ADDRESS. County MONMniiTH

Owner's Well No. Municipality SFfl R T R T Rngn Lot No. 34 Block No. 778

IRRIGATION WELL USE DATE WELL STARTED t ^ l ^ i / " ^ J

DATE WELL COMPLETED I f l , X * T I ^ 7

WELL CONSTRUCTION

Total Depth Drilled. ill Rnished Well Depth.

Borehole Diameter^ Top ^

jffl!4ft.

Bottom. .in. _in.

Weil Casing Begins:

I . ft. above grade or . ft. below grade

RECORD OF TEST Test Date i c / Q» M / M H Static Water Level I >! . ft. below land surface Water Level Measured Using M t ^ f c l ^




Open Hole (k^creen) (No. Used 1 T Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft)

-1

q^'i^

qi'/a 0

Death to Bottom (ft)

^b'/a

ICft'/?-

oa.'/a-9 iV^

Diameter (inches)

4"

4"

Material

(^C

A/d

^\syun(\

( n i e n t o r i i ^

WgtTRatIng (Ibs/sch no.)

<^0! ^C

•

/ lbs SK^> lbs

rkt^LXfCAhrpLia h 4rfloo. e Grouting Method Drilling Method i fT \U D TC

Pumping Water Level . - O N ! ^ ft.Aelow land surface Well Was Pumped IJ.sjng 0 1 ( ~ l \Ar T '

Well Yield ÔL .gpm If Pump Tested: Discharge Rate.

Duration of Test. .gpm

. hours

PERMANENT PUMPING EQUIPMENT , Installed by (_'. f A O f ^ h Rea. No. < J ] H C H Pump Type ^ g j 1 K p f y J r 5 3 h l C ^

Depth of Pump belowlandsurface ^ Q

Capacity ; 0 ( 3— gpm Horsepower. .ft.

/ certify that I have constructed the above referenced well in accordance with all well permit requirements and applicable State mIes and regulations.

Drilling Company MARSH CONSTRUCTION/CRAIG MARSH

Well Driller ( P r i n t ) ^ ^ ^ f / l l f j U \ ( l r S i r \

Driller's S\qnaXme y ^ l ^ ^ f ' ^ i T ^ C y t i

Registration No. c ^ ] « - f ? H Date n~y£M.

GEOLOGIC LOG

Note each depth where water was encountered in consolidated formations. . py i

^ 3 ^ ^ t\a\{ lrTi<:es ,QC!-3S'~ inr^d-tn C f y \ . r ^ ^ 0 / \ a

5b'-30' T. ,ryf , ^ r r \ -T m c^ y j sc\fy\ yo\cuy{

t ^ ' i n ^ ' - JiA^.nm/<yi/vf a7)t| ^fî^rl

yn'-us'- \ryQ M(-eu FiQAd

<^w-\uy- ^.fi.u^rtxi ^ a n c

COPIES: White - DEP Canary - Driller Pink - Owner Goldenrod - Health Deot

[ c [ c c [

DWR-138 5/95


WELL RECORD Well Permit Number 2 9 _ 4 0 5 5 6

OWNER.

Address

City

BISERTA, STEVEN Atlas Sheet Coordinates

2 9 - 3 3 • 3 7 9

2 1 6 6 OLD M I L L R D .

SEA G I R T State NJ Zip Code


County MONMOUTH

2 1 6 6 OLD M I L L R D .

- Municipality SEA GIRT BORO

Owner 's Well No.

Lot No. 2 0 Block No.. 2 7 8 . 0 2

W E L L USE IRRIGATION

DATE WELL STARTED tf> / " ^ / ^ i ^ DATE WELL COMPLETED ^ I t ^ ^ l ^ ^

WELL CONSTRUCTION

Total Depth Drilled i i £ ^ ft.

Finished Well Depth 1 ^ 3 ft.

Borehole Diameter: Top Bot tom.

. in . _ i n .



Single/Inner Casing


Outer Casing (largest diameter'

Open Hole (No. Used \

o fSc ree iV^


Tail Piece

Gravel Pack

Grout

RECORD OF TEST ^

Test Date j f e _ A j ^ i . / j f 7 _

Static Water Level l ^ ft. below land surface

Water Level Measured Usirig r\OS€i

Depth to Top (ft)

- /

15

^ ^

<D

Deoth to Bottom (ft)

^ 5

U>S

los ^3^

Diameter (inches)

4 l(

Material

P</(L 6CI4MO

f\/(U

PV(L 'Sai>-io ^ ) SOA^


lbs lbs

df^s5u<re,%tû/jQU \rtmi€y Grouting Method

Dri l l ing Method YCWJ { ) r i

J ^ CJM'

Pumping Water Level .

Well Was Pumped Using.

Well Yield 4 * > ^ apm

If Pump Tested: Discharge Rate _

Duration of Test _

ft j3e low land surface . ftJjeic

1S± .gpm

hours


Installed by (* . f ( \ n r < ^ k Reg. No. ^ ^ 4 3 9

Pump Type ^ \ x ) o r r \ P J r S \ \ c > \ ^ ;

^ ^ ft^ Depth of Pump below land surface

Capacity ^ ^ gpm Horsepower / _

/ certify that I have constmcted the above referenced well in accordance with al l wel lpenni t requirements and applicable State mies and regulations.


Well Driller (Print)^

Driller's Signatij

Registration No. n-i43g| Date WMM^

GEOLOGIC LOG Note each depth where water was encountered in consolidated fonmations.

ri-^QO' - 4Ar>f>. - k r f l g r ^ e ' ^ n r ^ - o J ^ l e n s e s s- n rojd i

^ ' - U S ' - - ^ r ^ Q Y - f v l c-SflAdj l^JO(^ •SOYYVe ^ H-

k 'oS C ' T^^near-e^ sflnd, uinori - in -^r\Tp. S^ /Y \¥ /J i7 f ^ A / i

S^ ' -HS ' - - ^ r ^ . ^ m^/i-SQAd^ U )mH "

MS'-no ' ' ty>pri T?nnr1^ \Ai6n1^

COPIES: White- DEP Canary - Driller Pink - Ownnr nnlr lonmrl - Health nont

[

c

c

DWR-138 5/95


<v\ M^ WELL RECORD Well Permit Number

29 41205

OWNER.

Address

HORAN, GARY Atlas Sheet Coordinates

29 .33 .384

1206 HEMLOCK AVE

City SEA GIRT State NJ Zip Code


County MONMnilTH

1206 HEMLOCK AVE

Municipality —SEA GIRT BORO

Owner's Well No. • Lot No. _6 Block No. ?7

IRRIGATION WELL USE DATE WELL STARTED

DATE WELL COMPLETED. ' . ^ ^

WELL CONSTRUCTION

Total Depth Drilled 1 1 O ft.

Finished Well Depth ) C f c > ft.

Borehole Diameter: Top Bottom. s: . in.

In.


RECORD OF TEST -

Test Date ^ / | H / H '

Static Water Level.


Single/Inner Casing



Open Hole o<[gcreen) (No. Used f ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft)

-1

qs

M4 D


^S

loS

)0S 0,4

Diameter (inches)

4"

+"

Material

iPv^C

pvt

=^lsand Neat Cement

<§en {On i t i - ^


Sl MC

S^^> lbs

sni Water Level Measured Usina_ Pumping Water Level O ' Well Was Pumped U s i m . Well Yield ^ H J - gpm If Pump Tested: Discharge Rate _

Duration of Test

B L ft. be

'/cJL . ft.

below land surface Grouting Method^l^/^<3JL/£.S-^rauql> 4nen^(<£-Drilling Method CCW] f ) r?^ 'Tk l / '

. ftêlow land surface

0\r hi-T-GEOLOGIC LOG

.gpm . hours

PERMANENT P Installed by

Pump Type

UMPING EQUIPMENT __ , 0 . m ( I r - S h Reg. N c Q i i t M

Depth of Pump below land surface.

Capacity t ^ - i O — gpm un.

Horsepower. ft.

/ certify that I have constmctedjhe above referenced well in accordance with all well permit requirsfnente and applicable State rules and regulations. ' ' ..'"".'-/G.'f


Well Driller (Print ^^ | L Q C 1 1 < ^ \ l V ^ | A ^ r \

Driller's Signatui(

Registration No. V J \ 4 - 3 ^ Da.;y2^/M/ft


yV- 2f ' - mer\ ^r^cnars^ sand oiriiI tensf^ s{-^rav;er

c^- rj^' - r r ^ io Qoinc ^ n a NrLI \erseS^Qraju^ w

:- L.tp>~ tr^d^nnt:i4x^ô ' ^' - &:>' -Ajr^ (irgj -sand uj / NÛJ^

^ ^ ^lAyâ

^- (^s' - rwn Kana \» \ lA cm Q; - - (lo^ - {Tffi ^ n n Lo/ W F Y J

COPIES: White- DEP Canarv - Driller P i n k - D w n / s r r^nlH/snrnH . l - leal th r i o n f

c [ 0

DWR-138 5/95


WELL RECORD Well Permit Number 29 41206

OWNER.

Address

THOMPKINS, JIM Atlas Sheet Coordinates

29 .33 .384

1 2 1 / CANDLEWOOD LA

City SEA GIRT .State NJ Zip Code 1217 CANDLEWOOD LA


County MONMnilTH Municipality SPA GIRT RORn

Owner's Weil No.

Lot No. _3 Block No. 778 01 IRRIGATION

WELL USE ^'^4^ DATE WELL COMPLETED ^ I C ^ I ^ H

DATE WELL STARTED

WELL CONSTRUCTION

Total Depth Drilled. iin. Finished Well Depth.

Borehole Diameter: < Top ,

9-7 .ft.

.ft.

Bottom. . in .

in.

Well Casing Begins:

I . ft. above grade or . ft. below grade

RECORD O F ; Test Date __

static Water Level ' S


Single/Inner Casing



Open Hole cfsScreeji-? (No. Used ^ )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

-1

^-1

% ^

0


) i i

R-l

q i %

Diameter (Inches)

M'

4'

Material

fvc

ipvt

-

* sand Neat Cement

^ ^ e n t o R J i ^

WgtiRating (Ibs/sch no.)

%ai o

3Ci4 JD

, _ lbs

(K£L_\ts

Water Level Measured Using V \ D S C >

Pumping Water Level S ^ _ Well Was Pumped Using Well Yield (.cD"^ gpm

If Pump Tested: Discharge Rate. Duration of Test.

ft. below land surface

Grouting M e t h o d ^ l P < ; . ^ a r P . 4 h « ^ - t > A ^ ' ^ ' ^ g ' ^ ' ^ .

Drilling Method.

^ , ft.êlow land surface

gpm hours

PERMANENT RUMPING EQUIPMENT Installed by C! . O n a r ^ h Reg. No. 0 ^ 1 4 - ^ 9 Pump Type Q j J o n n P J T S i 171 C >

Depth of Pump below land surface I O U

Capacity Qp-fS-^ gpm Horsepower.

GEOLOGIC LOG

I / certify that I have constmcted the above referenced well in accordance with all well permit requirements^!^ applicable State mIes and regulations. ' • ". ' - t >.'


Well Driller (Print) ..-^r^j^j-l r \ j ( Y M X f ^ n -•..

Driller's S\qna.t.v(e^-'T'li i4>

Registration No. 0 ^ 4 3 ^ ai43?q DaT/^^/^/^f

Note each depth where water was encountered in consolidated formations. ^ ,

^ m-Le^ i ' ::ir^ Q

olgL/ûjo!

SZW h Htne i S ^ n d ~TT

.<ann -17'- !^

COPIES: White- DEP Canary - Driller Pink - Owner Goldenrod - Health Deot

c [

[

DWR-138 5/95

New Jersey Department of Environmental Protection •v /T ) Bureau of Water Allocation

WELL RECORD WelLPermit Nuj fMi

OWNER

Address

City

PANISCOTTI, MARIO Atlaq^Sheet Coordinates^ _

i ?? i w. cHTCAGn Rl vn. SEA GIRT

WELL LOCATION ADDRESS 1221 W. CHICAGO BLVD.

. State NJ Zip Code

County MONMOUTH Municipality SEA GIRT BORO Owner's Well No.

Lot No. 25 Block No. 278

WELL USE IRRIGATION DATE WELL STARTED JQ I 7 DATE WELL COMPLETED (_(?

WELL CONSTRUCTION

Total Depth Drilled / / 0

Finished Well Depth

Borehole Diameter: Top

io\ .ft.

ft.

£ Bottom. YL

in. _in.

Well Casing Begins: . ft. above grade or

" ^ I ft. below grade

RECORD OF TEST

Test Date ll) I ' ^ Q I ^ Static Water Level I X —




Open Hole orcScreeTT" (No. Used ' p ^ ? Blank Casings (No. Used

Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

zl

il

U. A


I i

31. I b i

lAl ^

Diameter (inches)

^

l i> U

±

Material

^ L

fi/c

P]/a

•4 / S a n d Negt-Csmert ^Bentonite )


Jd/i v^

^c^t /Ô

lbs ( Q ^ lbs

. ft. below land surface

Water Level Measured Using / i f W J Pumping Water Level 2 . 0 ^ ft. below land surface

Well Was Pumped Using / I j f / i - p - h Well Yield f iZ) -^ gpm If Pump Tested: Discharge Rate gpm

Duration of Test hours

Grouting Method f ) n S . S L / - r i / f h n . l • b n n ^ \ j > _

Drilling Method f Y \ I//) i^b t r Z r U

PERMANENTPUMPING EQUIPMENT

Installed by r . f D a / 1 ^ h Reg. h i o - Z l M l A .

Pump Type X ( J /-> rCK} r S i /-) I C

GEOLOGIC LOG


u i j 1 P r n i / J JL

Depth of Pumg below land surface

Capacity

imp below 1 S^ gpm Horsepower \_

ft.

/ certify that I have constmcted the above referenced well in accordance with all well permit requirements and applicable State mies and regulations.

Drilling company "^RSH CONSTRUCTION/CRAIG MARSH

Well Driller (Prirr

Driller's Sign;

Registration N o . T / H , ^ ^ Date A ) I / I I ^ ^

COPIES: White- DEP Canary - Driller

^/^'-^/g> U/nff nr/ i juf <<r^nn u ) /

i r n ^ j i / j J

Y ^ - Q.y ' I J i n o JTi n n ac-J, ( y rm .Tr / i r l

cL

9.fT'^ni^* mori .nrrs .^tv^W

Pink - Owner Goldenrod - Health Dept

: DWR-138 M 11/98


MONITORING WELL RECORD Well Permit No. 29 -43503

'o^^r^^t' OWNER IDENTIFICATION - Owner Address

SUMMIT BANK Atlas Sheet Coordinates. 29 : 53 3:77

301 CAPNFfilE RENTFR, RnX ?Qf>ft City. PRINCETON State NJ , Zip Code

WELL LOCATION - If not the same as owner please give address. Owner's Well No. County HnHMOilTH Municipality SEA GIRT BORO Lot No. 2

MW-3 Block No. 706

Âddress. 1:^77 SFA GTRT AVE.

TYPE OF WELL (as per Well Permit Categories). .^Regulatory Program Requiring Well

MONITORING DATE WELL STARTED 8 /11 /GO

DATE WELL COMPLETtD Q / I 1 / 00

Case I.D.#

M J O N S U L T I N G FIRM/FIELD SUPERVISOR (if applicable)

WELL CONSTRUCTION

Total depth drilled 36 ft.

Tele. #

^Weil finished to -ao- ft.

0Borehole diameter: Top n . Bottom J J -

. in. in.

/Veil was finished: \3 above grade [g flush mounted

If finished above grade, casing height (stick pup) above land surface ft.

LiVas steel protective casing installed? DYes 13 No

DStatic water level after drilling 20 ft.

Vater level was measured us i ngJnd i ca toe

[ Well was developed for. t 2 gpm

. 5 hours


Single/Inner Casing


j Outer Casing (largest diameter) Open Hole or Screen (No. Used. 0 1 0 )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

.5

15

12

2


15

30

30

12

Diameter (inches)

4

4

11

11

Material

PVC

PVC

#1sand Neat Cement

Bentonite

Wgt./Rating (Ibs/sch no.)

sch40

sch40

7001b lbs.

60 lbs.

Method of development c e n t r i f u g a l Grouting Method T r e m i e Drilling Method TT . .q. a

I Was permanent pumping equipment installed? QYes H No

L'ump capacity gpm

Pump type:

Lj^rilling Fluid Type of Rig A . M . S

Health and Safety Plan submitted? D Yes • No

.evel of Protection used on site (circle one) None vp) C B A

/ certify that I have constructed the above referenced well in accordance with all well permit requirements and applicable

State rules and regulations.

GROUNDWATER & ENVIRONMENTAL

William Lovenbei/g

Drilling Company

Well Driller (Print)

iriiier's Signature "^ J l . ^ ^

Registration No. .^X") \ ( g l * ^ Date ^ ^ ^ / /£>^

• ^ — 1

GEOLOGIC LOG Note each depth where water was encountered in consolidated formations.

0 - 9 " A s p h a l t

9"-5' Silty Rrown Sand

5'-20' Brown Sand and Gravel

: ? 0 ' - : ^ n ' Wh-H-«^ M« ri Sanrl

3E-

COPIES: White-DEP Canary - Driller Pink-Owner Goldenrod - Health Dept.

_;,iDWR-138M 11/98


y j MONITORING WELL RECORD 0 ,03 .1^ vfe» Well Perniit No..

OWNER IDENTIFICATION - Owner. Add ress

29 43504

Atlas Sheet Coordinates. 29 : 33 377

SUMMIT BANK 301 CARNEGIE CENTER, BOX 2066

City. PRINCETON State -NX . Zip Code.

WELL LOCATION - If not the same as owner please give address. Owner's Well No. MW-2 County H"WM""TH Municipality S F A RTRT BORO Lot No. 2

-•Address

Block No. 706

1397 SPA GTRT AVE. DATE WELL STARTED 8 / 1 1 / 00

T Y P E O F W E L L (as per Well Permit Categories). —Regulatory Program Requiring Well

MONITORING DATE WELL COMPLETED 8 / 1 1 / 0 0

Case I.D.#

bONSULTING FIRM/FIELD SUPERVISOR (if applicable).

n- WELL CONSTRUCTION

Total depth drilled 3 0 ft. Well finished to " O ft.

Tele. #

CBorehole diameter: Top U . Bottom 1 1

in. in.

p/Vell was finished: D above grade L j [^ flush mounted

If finished above grade, casing height (stick Hup) above land surface ft.

L-iVas steel protective casing installed? D Y e s H No

DStatic water level after drilling 2 0 ft.

Vater level was measured using I n d l era tc^T"

-Well was developed for . 5 hours •t 2 gpm

"Method of development Q e n t r i f u g a l


Single/Inner Casing



Open Hole or Screen (No. Used . 0 1 0 )


Tail Piece

Gravel Pack

. i : Grout

Depth to Top (ft.)

.5

15

12

2


15

30

30

12

Diameter (inches)

4

-

4

11

11

Material

PVC

PVC

#1sand Neat Cement

Bentonite


sch40

sch40

7001b lbs.

6 0 lbs.

Grouting Method T r e m i e Drilling Method H . S . A

"Was permanent pumping equipment installed? nYes [^ No

-Pump capacity gpm

-Pump type:

-Drilling Fluid. .Type of Rig A . M . S

-Health and Safety Plan submitted? D Yes D No

.evel of Protection used on site (circle one) None ( ^ C B A



GROUNDWATER & ENVIRONMENTAL Drilling Company.

-/Veil Driller (Print) W i l l i a m L o v e n b e y g

)riller's Signature <^

Registration No. O ^ ^ )(g-t^ ./J!L/Q^

GEOLOGIC LOG Note each, depth where water was encountered in consolidated formations.

0-9" Asphalt

9"-5' Silty Brown Sand

5'-20' Brown Sand and Gravel

20'-30' White MP-d Sanri

SE-


Well Permit No. 29

)WR-i 38 M / " ^ ^ " ^ '*^®^ Jersey Depar tment of Environmental Protect ion 11/98 / "KT^ \ Bureau of Water Al location

0 ) MONITORING WELL RECORD

} j ( f ^ - 4 ^ Atlas Sheet Coordinates

)WNER IDENTIFICATION - Own^r SUMMIT BANK • -Address 3 0 1 PARNFRIE CENTER, BOX 2066

City \ pRij^PFTOM State [ tU. Zip Code

43505

29- :—33- .:577

VELL LOCATION - If not the same as owner please give address. Owner's Well No. "County MnNMniiTH Municipality SEA GIRT BORO Lot No.

MW-1 Block No. 706

-Address 1377 fiPft GTRT AVE.

"TTPE OF WELL (as per Well Permit Categories). Regulatory Program Requiring Well

MONITORING

DATE WELL STARTED 8 / 1 1 / 0 0 DATE WELL COMPLETED B / 1 1 / 0 0

Case I.D.#

CONSULTING FIRM/FIELD SUPERVISOR (if applicable).

, - WELL CONSTRUCTION

3tal depth drilled ^ ft. Well finished to 3H ft-

Tele. #

0

c orehole diameter:

Top 1 1 . Bottom 11

. in . in.

ell was finished: D above grade [^ flush mounted

If finished above grade, casing height (stick r,p) above land surface ft.

'.4'as steel protective casing installed? D Y e s Q No

pat ic water level after drilling 2 0 ft.

Uater level was measured u s i n g j j u d j ^ c a t o t

. . ^ hours Well was developed for. [ 2 gpm

Method of development r - t an t r i f uC fT^T


Single/Inner Casing



Open Hole or Screen (No. Used. 010 ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

- 5

15

12

2


15

30

30

12

Diameter (inches)

4

4

11

11

Material

PVC

PVC •

#1 sand Neat Cement

Bentonite


sch40

sch40

700 l b lbs.

60 lbs.

Grouting Method T r e m i e Drilling Method H , . q , A

• Vas permanent pumping equipment installed? ^ Y e s 0 No

_iump capacity : gpm

Eump type: ,

_Tilling Fluid Type of Rig j ^ ^ ^ ^ s

Health and Safety Plan submitted? D Yes • No

3vel of Protection used on site (circle one) None '{6) C B A



GROUNDWATER & ENVIRONMENTAL n.rjiiing Company.

rv'eil Driller (Print) W i l l i a m L o v e n b ^ r g ^

ruler's Signature \

Registration No. O * ^ l U l O


0-9" Asphalt 9"-S' Silty Rrnwn Sand 5'-20' Brown Sand and Gravel ?n'-30' White Med Sand

st-

COPIES: Wh i te -DEP Canary - Driller P ink-Owner Goldenrod - Health Dept.

G

C

G

G

DWR-138 5/95

I'lloO 1^ New Jersey Department of Enviranmental Protection

Bureau bf Water Allocation

WELL RECORD y/eil Permit Number

29 ~ 4 4 0 9 9

OWNER.

Address

City

VAN ANDA, PAUL Atlas Sheet Coordinates

2 9 ^ 3 3 ZET ^ '?^^ HPMi nf^K avF SEA GIRT ; State NJ Zip Code

WELL LOCATION ADDRESS. County MONMOUTH

l y i s HPMi nrK A V F . Municipality WALL TWP.

Owner's Weil No. Lot No. .^5 Block No.. 2 7 8 . 0 2

WELL USE IRRIGATION DATE WELL STARTED DATE WELL COMPLETED. 1 - / i n I o \

WELL CONSTRUCTION

Total Depth Drilled. loQ'

Finished Well Depth


lik. .ft.

ft.

'%.<>

Bottom. :sr . in . in.

Well Casing Begins:

H ^ . ft. above grade or . ft. below grade

RECORD OF TEST Test Date ' L I 1 ^ I Static Water Level L ! ^


Single/Inner Casing





Tail Piece

Gravel Pack

Grout

Depth to Top (f t )

l o

H

[0 1 l - h

\o

Depth to Bottom (f t )

^ /

l o l

lOG (or^ ^-b

Diameter (inches)

4

H

H %S ?,r

Material WgtVRating (Ibs/sch no.)

P/C- "^J^^ô

?Ho ^^M O

H o SejU/*/^ "Ek**<M


,0-LS-lbs

3SrC7lbs

OX ft. below land surface

Water Level Measured Using A v l ^ A ^ U < ^ ^ 0 - p v P g

Pumping Water Level f ? ^ ft. below land surface

Well Was Pumped Using A l / ^ ^ P T '

Well Yield " 7 * ^ gpm If Pump Tested: Discharge Rate gpm

Duration of Test i hours

Grouting Method j ^ ^ ^ ^ ' ^ T V - ^ D " ^ ^ 1^^M.|tS-p) i?E

Drilling Method yk ty fa ^ T A - R H

GEOLOGIC LOG

PERMANENT PUMPINaEQUIPMENT

^ R M t f r ^ 5 t 0 L g Installed by Pump Type Depth of Pump below land surface.

Capacity 1 2 gpm

. Reg. No .Ml3>H-l

6?o Horsepower. JL

ft.

/ certify that I have constmcted the above referenced well in accordance with'all well permit requirements and applicable State mies and regulations. "1

Drilling fômoanv ' PICKWICK WELL DRILLING

Well nrillf.r YPrint^ V l U ^ ^ ^ ) ^ ^ ! ^

Driller's Signature ^ i •

Registratioh :|Qo.AA I- I2>S2-I_01

Note each depth where water was encountered in consolidated formations. .

0 - ^ r l:tbtM)i:i A»)T? A^^^^H^ 6LA^^>y

^ ' t ^ o S L ^ £>«' tO grÂy

"DWR-138 M 11/98

OWNER IDENTIFICATION - Owner. •Address


^ MONITORING WELL RECORD 0^ ._. Well Permit No.. 29 - 44224

Atlas Sheet Coordinates.

WAWA, INC. 29 • 35 5«-

260 WEST BALTIMORE PIKE Ci t y . WAWA State PA 7';? Code

. . . W E L L LOCATION - If not the same as owner please give address. Owner's Well No. H W " / County ÔNMOUTH Municipality WALL TWP. Lot No. 1 & 10 Blocl< No. 79?.

"Address 2110 ROUTE 35

TYPE OF WELL (as per Well Permit Categories). -Regulatory Program Requiring Well •

MONITORING DATE WELL STARTED / / V S / O /

DATE WELL COMPLETED / / / . ^ / Q /

Case I.D.#

'CONSULTING FIRM/FIELD SUPERVISOR (if applicable), Tele. #

WELL CONSTRUCTION

< ^ 1 ft. a~7 ft.

Total depth drilled Well finished to

CBorehole diameter: Top J l Bot tom. -U

. in . in.

iWell was finished: Lâbove grade \~] flush mounted

. If finished above grade, casing height (stick up) above land surface ^ ft.

Wals steel protective casing installed? m Y e s Q No

Static water level after drilling / O ft.

Water level was measured us ing-^J '^y t fS '

-: Well was developed for _ at I gpm

Method of development.

s /nC

. hours


Single/Inner Casing



Open Hole or Screen (No. Used - 0 \ 0 )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

H ^

/

S

0


1

5 1 •

21 5

Diameter

(inches)^

^

H

l \

l \

Material

P/^

pyC

^/S^^xcl Neat Cement

Bentonite


Sî-VD

^cUUb

/ /oo ' ^^ lbs.

/OO lbs.

/ Grouting Method Drilling Method _

Trr..mi L

Was permanent pumping equipment installed? HIlYes y ^ o

- Pump capacity gpm

" - Pump type:

Drilling Fluid Type of Rig /? H J)

hACxLh

Health and Safety Plan submitted? D Yes ^ No

Level of Protection used on site (circle one) None 1/0/ C B A


State rules and regulations. _ -Drilling Company GROUNDWATER & ENVIRONMENTAL SE

Well Driller (P rint) UJ.l)

Driller's Signature ?,

\(Lm [A'^v\ am b ^

Registration No. 0 /) I ^ f O Date o^ I I ^ l b )


n - ^ \ -hf) mud Sr.^d KJ^ lS(\Yy P

5 ravz:

i -IY>' ftmov) n ^ ^ Q / K i \yij.5oh^^ ^ME

y ^ - ^ l - -iTAr S . l f y S ^ y x d i P / h f r l / ' CK\l


'dWR-138M 11/98

New Jersey Department of Environmental Protection , „ , Bureau of Water Allocation W , ' , MONITORING WELL RECORD

Well Pennit No.. 29 - 44225

Atlas Sheet Coordinates. WAWA, INC.

29 : 33 377

)WNER IDENTIFICATION -Owner Mddress 260 WEST BALTIMORE PIKE

City WAWA State PA Zip Code.

vVELL LOCATION - If not the same as owner please give address. Owner's Well No. H W ' t / County _

îiddress,

MONMOUTH 2110 ROUTE 35

Municipality. WALL TWP. Lot'No. 1 4 10 Block No. 723

TYPE OF WELL (as per Well Permit Categories). ""Regulatory Program Requiring Well

MONITORING DATE WELL STARTED / / / ^ / <^/

DATE WELL COMPLETED / I 1 3 I C>(

Case I.D.#

CONSULTING FIRM/FIELD SUPERVISOR (if applicable)

"' WELL CONSTRUCTION

„rotal depth drilled D l ft. Well finished to 19 ~7 ft.

Tele. #

0 I -iorehole diameter: ' Top [L

Bottom. I L in. in.

j 'Veil was finished: ^ above grade ' - ' Q flush mounted

i-lf finished above grade, caging height (stick j ûp) above land surface p ft.

Was steel protective casing installed? pYesDNo

j ptatic water level after drilling ' ^ ft.

Water level was measured using30/(Vif .Sf

, hours

A f A tWell was developed for _

Jt L gpm

Method of development . .. .

I Was permanent pumping equipment installed? QYes Df No

Pump capacity gpm '

~t Pump type:

- Drilling Fluid Type of Rig ?A H J>


Single/Inner Casing



Open Hole or Screen (No. Used - 0 | 0 )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

^;s

1

^

0


n

97

^7 5

Diameter (inches)

H

\ \

H ^

Material

'^vc

? M ^

^\S(Kr\a Neat Cement

Bentonite


ScUÔ

ScwÔ

11 OD lbs.

/ O O l b s .

Grouting Method Drilling Method _

~b-g hOf/ / b A ^

^ Health and Safety Plan submitted? D Yes [3;ffiJo

-.Level of Protection used on site (circle one) None P Jc B A


State rules and regulations. GROUNDWATER & ENVIRONMENTALiSE Drilling Company.

Well Driller (Print) W i ] \ ( a > ^

ture L—^JL^

Q-y^^b<i.^'

Driller's SignatL ^

Registration No. J d / ^ / ( ^ Date ( y I I j I D r


O-U' ^\r\ Y\rJifi yCksrA lOysomF" ^yk£L l

^-if.' .jSrojon rmA Sr i d uyôiup' sU

C/asj


'DWR-138 M 11/98

New Jersey Depar tment of Environmental Protect ion ^ '^x Bureau of Water Allocation

70) MONITORING WELL RECORD ^ n v.»f^ ': Well Permit No.. 29 -44226 .

Atlas Sheet Coordinates. WAWA, INC. OWNER IDENTIFICATION - Owner

Address 260 WEST BALTIMORE PIKE City

- 2 9 - — 5 3 ^572-

WAWA State PA . Zip Code.

WELL LOCATION - If not the same as owner please give address. Owner's Well No. County . " " " ^ " " " I " Municipality WALL TWP. Lot No. Address

MONMOUTH 2110 ROUTE 35

\ . p i ^

1 & 10 Block No. 7?.^

TYPE OF WELL (as per Well Permit Categories), ' Regulatory Program Requiring Well

MONITORING DATE WELL STARTED / / /CT l O /

DATE WELL COMPLETED / I JfK / d f

. Case I.D.#

CONSULTING FIRM/FIELD SUPERVISOR (if applicable)

WELL CONSTRUCTION

Tele. #

_, Total depth drilled . Well finished to -xSi

_ft. .ft.

Borehole diameter: I- ' Top

Bottom. H , in.

in.

Well vyas finished: H above grade Q flush mounted

(- . If finished above grade, ca|ing height (stick : up) above land surface f ) ft.

" Was steel protective casing installed? H Y e s Q No

J Static water level after drilling J y> ft.

" Water level was measured usingOQ/jJQiSX

G Well was developed for ' !2> at j gpm

hours


Single/Inner Casing


Outer Casing (largest diameter) Open Hole or Screen (No. Used - O p )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

' 'S

1

^

D


1

9 1

^ 1 5

Diameter (inches)

^ /

1

L;

1

Material

^vc

pyc

^ \âA Neat Cement

Bentonite


5CKL/0

5ckW0

i i oO lbs.

/ O O lbs.

ALC Method of development.

Was permanent pumping equipment installed? QYes Nff

Pump capacity gpm

Pump type:

Grouting Method Drilling Method _

-frgyYlti /4v\

No

^

Drilling Fluid. . Type of Rig. / )H.S

C B A

Health and Safety Plan submitted? D Yes No

Level of Protection used on site (circle one) None m j



Drilling Company GROUNDWATER & ENVIRONMENTAL SE

Well Driller (Print) ^ ^ \ \ \ q \ A A •; / ^ \ r ( y \ b ^ r y ^

Driller's Signature 1 .—c l -^

GEOLOGIC LOG Note each depth where water was encountered in consolidated fonnations.

0-U'.JC\/) rNuk^CkÂ iOSOrvdl dâifCi

m

Registration No. ^ O / ^ / ^ Date o^ / / 7 / O /

COPIES: White - DEP Canary- Driller Pink - Owner Goldenrod - Health Dept

JDWR-138M 11/98

New Jersey Department of Environmental Protection

Bureau of Water Al locat ion

MONITORING WELL RECORD 29 ^ ^ - : Well Permit No.

44375

DWNER IDENTIFICATION - Owner Add ress.

WAWA INC. Atlas Sheet Coordinates. 29 33 372

260 WEST BALTIMORE PIKE City. WAWA State. -PA- . Zip Code.

/VELL LOCATION - If not the same as owner please give address. Owner's Well No. H ^ " ^ County MONMOUTH Municipality —WALL TWP. Lot No. i & i p Block No. 723

-^^ddress 911 n pni iTF ^ ' i

TYPE OF WELL (as per Well Permit Categories) ...Regulatory Program Requiring Well

MONITORING

DATE WELL STARTED c9 / I'D I O } DATE WELL COMPLETED g> I j ' ^ I O \

Case I.D.#.

CONSULTING FIRM/FIELD SUPERVISOR (if applicable), . Tele. # .

WELL CONSTRUCTION

'otal depth drilled "Well finished to _ ft.

CSorehole diameter: . Top L\ in. Bottom \ \ in.

CVeil was finished: ^ above grade r~| ftush mounte mounted

If finished above grade, casing height (stick ^jp) above land surface _ i _

ing hen

:2_ft.' Vas steel protective casing installed? m Y e s C l No

n'at ic water level after drilling I ( ft.

L..Vater level was measured using \ ' ^ ( i ' \ C o n ^

.5 hours Well was developed for. I t 1 ^ gpm 1/Iethod of development \/^\VNni/()_ T { \ x v \ O i

Vas permanent pumping equipment installed? QYes TO No

?ump capacity gpm

Pump type:

j r i l l i ng Fluid Type of Rig / \ - lA. J>


Single/Inner Casing


Outer Casing (largest diameter) Open Hole or Screen (No. Used ^ )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

• t - ^

\ ^

lO

D


B

9 1

d l 10

Diameter (inches)

V

^

11 n

Material

?\/d

^ C

• ^ )5« iw : j



SCWMO

• OloSlof-

ôoLi5< ( ^ 0 lbs.

lbs.

Grouting Method. Drilling Method _

\ T p r v ^ \ Q Gn v D i A j k : mk

Health and Safety Plan submitted? D Yes [^ No

evel of Protection used on site (circle one) None AD) C B A

. . / certify that I have constructed the above referenced well in accordance with al l well permit requirements and applicable

- State rules and regulations.

Drilling Company RRnitNnuftTEi^ i FNVTRdNMFNTAL SE

.Veil Driller (Print)

Tiller's Signature

Registration No. ^ O ^ 6 r ( > Date ^ I N 7 fij

GEOLOGIC LOG Note each depth where water was encountered in consolidated fonmations.

O ' T i O ' C o o f ^ r- rn :)x/ brAuvrlK(-^/-g\u^

f r ) ' X l ' m k 9 f)iDY\ . S \ ^ ^^^<^

COPIES: Wh i te -DEP Canary - Driller P ink -Owner Goldenrod - Health Dept

; D W R - 1 3 8 M 11/98


^ j MONITORING WELL RECORD 29 44376 Well Permit No.

OWNER IDENTIFICATION - Owner Address

WAWA I N C . Atlas Sheet Coordinates. 29 33 372

260 WEST BALTIMORE PIKE City _ -UAWA- State -EA- . Zip Code.

WELL LOCATION - If not the same as owner please give address. Owner's Well No. County MnNMOUTH Municipality Wfli i T U P , Lot No

\AW' \ 1 & 10 Block No. 725

r-Address. 7110 ROUTF 35

TYPE OF WELL (as per Well Permit Categories). ^Regulatory Program Requiring Well

MONITORING

DATE WELL STARTED P I Id- j O I DATE WELL COMPLETED c9 I I d I Cy I

Case I.D.#.

CONSULTING FIRM/FIELD SUPERVISOR (if applicable). Tele. #

- WELL CONSTRUCTION

Total depth drilled c/ ' ft. Well finished to P 1 ft.

r Borehole diameter:

L Top^ IL Bottom. ±

in. in.

Well was finished: 0 above grade Q flush mounted

If finished above grade, casing height (stick up) above land surface • f '5 ft.

as steel protective casing installed? raYesQ No

'Static water level after drilling j ' ] ft.

-Water level was measured using jYA/jiYgiff i^-

Well was developed for ; O hours

It U S - gpm "Method of development l i^VvaJLe, Y\.KVv\\P

"Was permanent pumping equipment installed? QYes | \ I

-Pump capacity •

„Pump type:


Single/Inner Casing



Open Hole or Screen (No. Used 0 )


Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

t ^

O

10

0


IS

3~l

p-7 10

Diameter (inches)

H

i)

) l II

Material

?vc

pvc

•îSA^d Neat Cement

Bentonite

Wgt ./Rating (Ibs/sch no.)

SoVxMO

SOW H O ' 0 ) 0 : s \ o {

ÔOIB£ I b V lbs.

lbs.

Grouting Method. Drilling Method _

\ r?^yY\ \ t A r m ^ m S ^

No

.gpm

^Drilling Fluid. . Type of Rig. A h . S ..Health and Safety Plan submitted? D Yes fej No

Level of Protection used on site (circle one) None 6 b B A

;^n-yn 'mpcl p.rou3/\ S^\^ S(KV^

I certify that I have constructed the above referenced well in accordance with all well permit requirements and applicable


Drilling Company. GROUNDWATER & ENVIRONMENTAL SE

-Well Driller (Print)

Driller's Signature

Registration No. • ^ O ^ ^ S ' X Date c? / ]§. / 0 \


n - T ^ O ' ( h a ^ s g .j^rnvtÂ .So.w.cJi b (-r^mArr I


G

C

[

C

DWR-138 5/95


( j .MwxAf i WELL RECORD Well Permit Number

2 9 ~ 4 4 4 9 8

O W N E R .

Address

City

KURFEHS, FRED 9 9 n A T.TWr!RTR T.ANF.


—29—"^s^ '-ete-

WALL . state NJ Zip Code

W E L L LOCATION ADDRESS.

County MONMOUTH

7.7.Q4 T.TNCRTS T,ANF. Owner 's Wel l No.

Municipality WAT.T. TWP. Lot No. /

Block No. 7 1 3

W E L L USE TRRTGATTQN DATE WELL STARTED 5 ^

DATE WELL COMPLETED 3 I '/^ I O /

-/liÔj

W E L L CONSTRUCTION

Total Depth Drilled J T O

Finished Well Depth


tSL i .ft.

. f t .

Bot tom.

O ^ in.

in.

Well Casing Begins:

ZT . ft. above grade or . ft. below grade


Single/Inner Casing





Tail Piece

Gravel Pack

Grout

Depth to Top (ft)

-I

cJ£

Yo M-

RECORD OF TEST

Test Date 3 / /? / / ) ^

Static Water Level / . ^ ft. below/ land surface

Water Level Measured Using . j ) i r r \ / : > C ^ f i U ' i

±


241

9o

n i M$-TM

Diameter (inches)

± \ \

L f H

!± l (

M

Material

F(yQ

Fu <L

JcyyL. ' I S A ^ Mint Gomont ^

Bentonite

WgtTRating (Ibs/sch no.)

I c A ^

SSJL^^

?U ^ 6 9-oocn .CO

. lbs

. lbs

Grout ing Method .

Dri l l ing l\/lethod _

/^CS^ uf-f 'J^-Jl^r-^

Pumping Water Level .

Well Was Pumped Using y r / / f

Well Yield / Q Q - f - gpm

If Pump Tested: Discharge Rate

Duration of Test

. ft. below land surface

.gpm

. hours

• PUMPING EQUIPMENT ,

3 below land surface ~ ^ 2

PERMANENT PjJjMfJING EQUIPI)JENT

Installed b y .

Pump T y p e . No. / / /2T

Depth of Pump below land surface.

Capacity C J U gpm Horsepower /

/ certify that I have constmcted the above referenced well in accordance with al l well permit requirements and applicable State mies and regulations.

Drilling Company ROBERT AZURAK

Well Driller (Print).

Driller's Signature

Registration No. / y ^ Q -


Note each depth where water was encountered in consolidated formations. / .

V- / / ' A>^1/^^

i r Y9' ^rCTy g ^ ^ V I - ,rt) f ' f . ^

I I J J i O I


Appendix 2

Advanced Geological Services Results of Geophysical Surveying Letter Report


Reference: 01-122-1 sMysucLane MalvertvPA 1 (610)722-5500 (610) 722-0250 (fax)

November 28,2001 ! S 7 -5 0 W

Mr. John Montgomery Groundvâter & Environmental Services, Inc. 1340 Campus Parkvây P.O. Box 1750 Wall, New Jersey 07719

Subject Results of Geophysical Survejdng Fleet Bank Site Wall Township, New Jersey

Dear Mr. Montgomery:

Advanced Geological Services (AGC) is pleased to present this letter report that summarizes the results of a geophysical survey performed at the above referenced site. The objectives of the stirvey were to locate a former imderground septic system and other anomalies that may be of environmental concem. To achieve these objectives, an integrated geophysical investigation was performed using high-sensitivity metal detector (EM61) and digital groimd penetrating radar (GPR) techniques.

Integrating two or more geophysical techniques provides a complementary effect resulting in higher confidence levels and more complete subsurface information by reducing the inherent ambiguities in interpretation that may exist if only one method was used. The EM61 was used to provide complete site coverage to locate buried metal anomalies that would indicate the presence of USTs or reinforced concrete structures. The GPR survey was performed to provide a cross-sectional image of both metallic and non-metaUic structures.

1.0 METHODOLOGY

1.1. HIGH-SENSmVITY METAL DETECTOR (EM61) METHODOLOGY

Buried metal objects such as storage drums and tanks can be effectively located using a Geonics EM61 High-Sensitivity Metal Detector. The EM61 is a time domain electromagnetic (EM) system that can discriminate between conductive soils and metal objects. It has numerous advantages over other commonly used metal detection devices.

The EM61 generates rapid electromagnetic pulses and measures the response of the subsurface between pulses. Secondary EM fields are generated in the groimd after each pulse. These fields dissipate rapidly in earth materials but remain for a longer time in buried metal objects. The EM61 measures tiie prolonged metal response only after the earth response has dissipated.

The EM61 uses portable time-domain transmitter and two receiver coils. The data received from second receiver coil can be used to reduce the unwanted effects from interference and near-surface objects that can mask deeper and more significant objects.

Very high-resolution data are automatically recorded as the sensors are pulled along the groimd surface. Survey wheels attached to the sensors facilitate data collection by allowing direct

Mr. John Montgomery November 28,2001 RefererKe: 01-122-1 Page 2

measurement of the distance traveled. The lateral position of each measurement is automatically recorded using a data logger. This method allows data to be recorded virtually as fast as the operator can walk. Consequently, detailed site coverage can be achieved in a cost-effective maimer.

For this investigation, data were acquired at less than 2-ft intervals along Unes spaced 5-ft apart to provide continuous site coverage over tixe survey area. The data were processed and interpreted in the field to identify anomalies that may indicate the presence of buried structures. These anomalies were further investigated using GPR.

1.2. DIGITAL GROUND PENETRATING RADAR (GPR) METHOD

The GPR survey was performed by recording continuous data along orthogonal transects established over suspected target locations. The GPR method uses focused high frequency electromagnetic pulses to produce a continuous, cross-sectional image of the subsurface. These pulses are transmitted into the subsurface using an anterma. When the pulses reach a layer or object possessing contrasting electrical properties, part of the energy is reflected back to the surface where it is detected by a receiving anteima. A continuous cross-sectional image is generated as the receiving and transmitting antennas are pulled along the ground surface. The received signal is sent to a controlling unit where it is processed and displayed in real time to allow in-field interpretations. The data are also digitally recorded for high-resolution computer processing.

A GSSISIR-2000 Subsurface Interface Radar Systems and a 400 megahertz (MHz) anteima were used with a recording window of 60 nanoseconds (ns) to provide the required depth penetration (approximately 10 feet) and subsurface detail. The GPR data were acquired along orthogonal transects over the survey area. Detailed surve5ring was performed over anomalies identified by the EM61.

2.0 SUMMARY OF RESULTS

Figure 1 presents an EM61 anomaly map of the survey area. AH anomalies shown on the map are caused by buried metal objects or cultural interference. Cultural interference caused by above ground metal structures was encountered aroimd the perimeter of ihe existing bank building. Additional points of cultural interference were observed at discrete locations aroimd the site. The anomalies — caused by monitoring wells, metal posts, and a dumpster ~ are identified on the figure.

Discrete buried metal objects were also observed at locations shown on the map. These objects were further investigated using GPR. However, these results indicated the objects are asjmnmetrical and appear to be buried scrap metal or construction debris. These objects do not appear to be drums, USTs or objects associated with a septic system.

A linear anomaly was identified near the northeast comer of the building. The anomaly characteristics suggest the presence of a previously unidentified utUity. Further investigation of this anomaly was performed using GPR. A representative GPR profile of the object is shown in Figure 2. These data corroborate the EM61 data interpretation by indicating the presence of a laterally continuous hyperbolic anomaly, which is characteristic of buried utilities. This

Mr. John Montgameiy November 28,2001 Reference: 01-122-1 Page 3

interpreted utility extends from the building and ends at the northeast comer of the property. Detailed GPR coverage was performed in this area to help identify the subtie EM61 anomalies located near the end of the suspected pipe.

The GPR data acquired in the northeast comer of the property exhibited chaotic reflection events that suggest the presence of disturbed subsurface conditions. In addition, numerous diffractions and complex anomaly configurations were observed that suggest the presence of non-native structures or objects. Signal penetration through the suspected structure was observed, which indicates the structure is non-metaUic, since GPR signals cannot penetrate metal. An example GPR profile over the suspected structure is shown in Figure 3. Although the profile shown in the figure appears well defined, the majority of the data show a more complex configuration that obfuscated three-dimensional characterization. Nevertheless, the approximate extent of the feature was delineated and spray painted in the field. This interpreted location is presented in Figure 1.

Although it is impossible to definitively identify the suspected structure based on solely on the geophysical data, its location with respect to the detected utility interpreted in conjunction with historical information indicate that this is a likely location for the suspected former septic system. However, direct evidence from test pits would be required to confirm this interpretation.

3.0 CLOSING

The data collection and interpretation methodologies used in this investigation are consistent with standard practices applied to similar geophysical investigations. The correlation of geophysical responses with probable subsurface features is based on the past results of similar surveys although it is possible that some variation could exist at this site. Due to the indirect nature of geophysical data, no guarantees can be made or are implied regarding the presence or absence of additional objects or targets beyond those identified.

Please contact us if you have any questions regarding this survey. We appreciate your business and look forward to wôrking with you again.

Kind regards.

Advanced Geological Services

M. Seeftt McQuown, M.Sc., P.G. Senior Geophysidst

Figure 1 EM61 Anomaly Map

Fleet Bank Site Wall Township, New Jersey

20E 40E 60E 80E 100E 120E 140E 160E 180E

10

- N -

10 20

feet

Response (mS/m)

30

-0.7 2.7 4.9 7.1 9.3 11.5 14.0 16.6 20.2 25.7 35.6 54.0 119.1 1391.6

P

LEGEND

© Monitoring well - - Detected utility © Unidentified burled metal object

Figure 2 Example GPR Profile of Suspected Conduit

Fleet Bank Site Wall Township, New Jersey

YP000000.01T 0 1

0 1

ID

DISTANCE [FOOT] 3 4 5 6 7

20

111 30

40

50

m ^ ^

Appendix 3

Monitoring Well Logs


MONITORING WELL LOG Sheet 1 of 4

Project Name: Fleet Bank Branch Street Address: 1322 Sea Girt Ave., Wall Twp, NJ 07719 Tax Map Address: Block 706, Lot 2 County: Monmouth

Owner: Fleet National Bank Owner's Representative: Gary Skowronski, V.P. Owner's Address: 3670 Route 9 South, Freehold, NJ 07728 GES Project Manager: John H. Montgomery, P.G. GES Case Manager: John H. Montgomery, P.G. NJDEP Case Number: Not applicable NJPDES Permit Number: Not applicable

Driller: Shore Drilling, Inc. Driller's Address: 23 Branch Avenue, Oceanport, NJ 07757 Driller's License Number: MD1540

Well Identification: MW3D Well Coordinate Number: 29.33.377 Well Permit Number: 29-45875 Latitude: North 40° 08' 9.4"; Longitude: West 74° 03' 44.9" Casing Elevation: 45.85 feet; Surface Elevation: 46.13 feet Well Depth: 60.75 feet Screen Length: 10 feet; Casing Length: 50.75 feet Drilling Method: Hollow stem auger Well Diameter: 4.0 inches Borehole Diameter: 12.0 inches Sampling Method: Split-spoon Static Water Depth: feet Logged By: John H. Montgomery, P.G. Completion Date: November 16, 2001

Depth (feet)

Sample Number

Well Detail

PID (units)

Blow Counts Recovery (inches)

Hand augered to 5 feet

Depth (feet)

Lithology/Remarks

(Modified Burmister Classification)

0

3

4

5

6

7

8

9

10

11

12

13

14

15

16

17

18

19

0 0-0.33: Asphalt

0.33-1.0: Gravel/roadstone base

0.5-4: Tan Silty fine to medium Sand, trace Clay, trace quartz Gravel (md) dry, no odor, no stain

4-15: Same as above

15-20: Light tan/white medium Sand, some quartz Gravel (md), moist

^ y : Bentonite-cement grout Bentonite powder seal Sand/Gravel pack

Well Construction Materials and Completion Details: Schedule 40 PVC, 0.010-inch machine slotted threaded screen and threaded solid casing, Morie #1 sand, bentonite powder seal. Flush mounted, bolt down, 12-inch diameter manhole. Locking, watertight gripper plug.

INote: Numbers in the column labeled "Blow Counts" refer to the number of blows required to drive a standard split-spoon sampler a distance of 6.0 inches using a 140-pound drop weight falling 30 inches. A standard spUt-spoon sampler is 2.0-inch outer diameter and 1.375-inch inner diameter.


MONITORING WELL LOG

Project Name: Fleet Bank Branch

Street Address: 1322 Sea Girt Ave.,

Tax Map Address: Block 706, Lot 2

County: Monmouth

Owner: Fleet National Bank

Wall Twp, NJ 07719

Owner's Representative: Gary Skowronski, V.P.

Owner's Address: 3670 Route 9 South, Freehold, NJ 07728

GES Project Manager: John H. Montgomery, P.G.

GES Case Manager: John H. Montgomery, P.G.

NJDEP Case Number: Not applicable

NJPDES Permit Number: Not applicable

Driller: Shore Drilling, Inc.

Driller's Address: 23 Branch Avenue Driller's License Number: MD1540

Depth

(feet)

20

21

22

23

24

25

26

27

28

29

30

31

32

33

34

35

36

37

38

39

Sample

Number

Well

Detail

^

^ ~

~ ^

= ^ z

= ^ ~

= ^ ~ ^

~ ^ ^

E ^ 1 ^ ZI ~

~

i H H

^

=

—

^ —

~ ^

= — ^ [JUJ

^ ~ ~

^ — ^

222 ^ ^

E mmm

=

E ~

Z! ~

1 1^

^ IZI

PID

(units)

26-96 -~

— 219 613 281 —

13.6 118 87 -

211 133 151 384 171 249 190 — -

168 272 -23 52 20 —

47.3 21.8 34.8

11 10 18

2 7

Key: JZ

g Bentonite-cement g Bentonite powder s Sand/Gravel pack

Note: Numbers in the column labeled "Bio inches using a 140-pound drop weight falli

, Oceanport, NJ 07757

Blow Counts

Recovery (inches)

11,12,15,16 22

11,12,13,13 23

6,7,12,13 24

3,7,10,18 24

8,14,15,14 24

2,2,5,5 14

10,14,18,20 22

5,6,10,9 18

6,8,11,12 24

3,5,8,11 24

rout eal

w Counts" refer to t ng 30 inches. A star

Depth

(feet)

20-22:

22-24:

24-26:

26-28:

28-30:

30-32:

32-34:

34-36:

36-38:

38-40:

Sheet 2 of 4

Well Identification: MW3D

Well Coordinate Number: 29.33.377

Well Permit Number: 29-45875

Latitude: North 40° 08' 9.4"; Longitude: West 74° 03' 44.9"

Casing Elevation: 45.85 feet; Surface Elevation: 46.13 feet

Well Depth: 60.75 feet

Screen Length: 10 feet; Casing Length: 50.75 feet

Drilling Method: Hollow stem auger

Well Diameter: 4.0 inches

Borehole Diameter: 12.0 inches

Sampling Method: Split-spoon

Static Water Depth: feet

Logged By: John H. Montgomery, P.G. Completion Date: November 16, 2001

Lithology/Remarks


20.3-20.9 feet: Gray VF silty Sand. PID = 96; 20.9-21.2 feet: Gray VF Sand, some (-I-) silt. PED >60; 21.2-21.7 feet: Orange yellow VF Sand. Wet. PID = 26; 21.7-22 feet: Yellow-white coarse Sand, some (-) silt. PID = 59. 22.4-23 feet: Grayish-yellow very coarse Sand; 23-23.3 feet: Orange-yellow coarse Sand, some (+) silt; 23.3-24 feet: Yellow-orange medium to coarse Sand, trace (-I-) well rounded qtz pebbles, some iron motthng at 23.75 feet. 24.5-25 feet: Orange-yellow VF Sand, some (-) silt, trace (-) clay; 25-25.1 feet: Very coarse qtz pebbles, some (+) well rounded Sand; 25.1-25.6 feet: Orange-yellow to gray VF Sand, some (-) medium to coarse Sand, trace (+) sih. 26-27 feet: Pale gray to grayish-white very coarse, well rounded qtz Sand, some (-) m-f Sand, trace (+) silt; 27-27.5 feet: Orange-yellow to pale yellow f-m Sand, some (+) silt, trace (-) clay; 27.75-28 feet: Grayish-white very coarse Sand, some (+) VF to medium Sand, trace (+) silt. 28.5-29 feet: Orange-brown to light gray very coarse to coarse Sand, some (+) f-m Sand, trace (-I-) silt; 28.5-30 feet: Grayish-white very coarse Sand, some (+) VF Sand and some iron mottling at 29.5 feet. Fallback = 0.5 feet. 31-31.75 feet: Light grayish-white medium to coarse Sand, some (-I-) fine Sand, trace (-) silt; 31.75-32 feet: Orange-yellow to light brown VF Sand, some (+) clay, trace (+) silt.

32.6-33.5 feet: Orange-yellow to light gray to brown coarse to very coarse Sand, little well rounded qtz pebbles, some (+) fine Sand to sih. 22.5-24 feet: Orange-yellow to yellow-brown f-m Sand, some (+) silt, trace (+) coarse Sand. 34.5-35 feet: Brown medium to coarse Sand, some (-) clay, trace (-I-) fine Sand; 35-36 feet: Orange-brown to dark brown VF to fine Sand, some (+) silt, trace (-I-) clay.

36.5-38 feet: Brown to dark brown VF Sand to silt, some {+) clay, trace (-) well rounded coarse qtz Sand and iron mottling. Fallback = 0.5 feet

Orange to orange-brown to yellow VF to fine Sand, some (+) clay, trace (+) silt.

Well Construction Materials and Completion Details: Schedule 40 PVC, 0.010-inch machine slotted threaded screen and threaded solid casing, Morie #1 sand, bentonite powder seal. Flush mounted, bolt down, 12-inch diameter manhole. Locking, water- | tight gripper ] 3lug.

le number of blows required to drive a standard split-spoon sampler a distance of 6.0 idard split-spoon sampler is 2.0-inch outer diameter and 1.375-inch inner diameter. |


MONITORING WELL LOG

IProject Name: Fleet Bank Branch

Street Address: 1322 Sea Girt Ave.,

Tax Map Address: Block 706, Lot 2

{County: Monmouth

lA/allTwp, NJ07719

lOwner: Fleet National Bank

Owner's Representative: Gary Skowronski, V.P.

Owner's Address: 3670 Route 9 South, Freehold, NJ 07728

GES Project Manager: John H. Montgomery, P.G.

GES Case Manager: John H. Montgomery, P.G.

NJDEP Case Number: Not applicable

NJPDES Permit Number: Not applicable

Driller: Shore Drilling, Inc.

Driller's Address: 23 Branch Avenue Driller's License Number: MD1540

Depth

(feet)

40

41

42

43

44

45

46

47

48

49

50

51

52

53

54

55

56

57

58

59

Sample

Number

Note: Numbers in t inches using a 140-

Well Detail

1

y

lie

he 301

1

PID

(units) 3

1.2

0.2 1.2

1.4 1.2 0.4

0.2 1

0.6

0.2 0

0 0 0

0.5 0.2 0.1 0 0 0 0 0 0 0 0

y: Bentonite-cement g Bentonite powder s Sand/Gravel pack

;olumn labeled "Bio ind drop weight falh

Oceanport, NJ 07757

Blow Counts

Recovery (inches)

3,3,8,5 24

6,4,9,13 14

5,8,27,26 20

8,8,12,13 22

6,14,22,49 16

13,17,33,24 21

7,39,49,36 18

5,5,8,8 22

5,5,3,3 24

2,1,1,1 12

rout eal

w Counts" refer to t ng 30 inches. A stai

Depth

(feet)

40-42:

42-44:

44-46:

46-48:

48-50:

50-52:

52-54:

54-56:

56-58:

58-60:

Sheet 3 of 4

Well Identification: MW3D

Well Coordinate Number: 29.33.377

Well Permit Number: 29-45875

Latitude: North 40° 08' 9.4"; Longitude: West 74° 03' 44.9"

Casing Elevation: 45.85 feet; Surface Elevation: 46.13 feet

Well Depth: 60.75 feet

Screen Length: 10 feet; Casing Length: 50.75 feet

Drilling Method: Hollow stem auger

Well Diameter: 4.0 inches

Borehole Diameter: 12.0 Inches

Sampling Method: Split-spoon

Static Water Depth: feet

Logged By: John H. Montgomery, P.G. Completion Date: November 16, 2001

Lithology/Remarks


40.5-42 feet: Varied colors (hght gray to orange to orange-brown) VF Sand, some {+) silt, trace (+) clay and iron mottling. Fallback = 0.5 feet.

43-43.5 feet: Orange-brown to yellow brown VF Sand, some (-) silt, trace (+) clay; 43.5-44 feet: Orange-brown to yellow to yellowish-gray coarse to VF Sand, trace (-I-) semi-rounded qtz Sand, some (+) silt. Fall

back = 2 inches. 44-45 feet: Orange-brown to light grayish-brown fine to VF Sand, httle m-f Sand; 44-45 feet; Orange-brown to light grayish-brown fine to VF Sand, some (-I-) medium qtz Sand, red clay stringer (0.25 feet thick) at 45 feet. 46.8 to 48 feet: Orange to light orange brown m-f Sand, some (-) silt, trace (-) clay. Fallback = 8 inches.

48.8-50 feet: Brown to light brownish-yellow m-f Sand, little silt, trace (+) clay, some iron mottling.

50.5-51.2 feet: Orange-brown very coarse to medium Sand, some (-) silt, trace (-) semi-rounded qtz pebbles; 51.2-52 feet: Orange to orange-brown m-f Sand, little silt. At 51.25 feet: 1 inch layer of reddish-brown medium Sand. Fallback = 3 inches. 52.5-53.7 feet: Orange-brown to reddish-orange-brown to light gray fine to VF Sand, some (-) silt, trace (+) clay and iron mottling; 53.7-54 feet: Dark reddish brown fine Sand.

54.8-56 feet: Orange-brown to dark brown fine to VF Sand, some (-) silt, trace (-) clay and iron mottling. Some thin layers of gray VF Sand. Fallback = 7 inches.

56.5-57.5 feet: Orange-brown to light brown fine to VF Sand, some (+) silt, trace (+) clay; 57.5-58 feet: Grayish-brown to gray clay, plastic, semi-dense, some (-I-) silt.

59.75-60 feet: Dark gray to black dense clay. Fallback = 6 inches.

Well Construction Materials and Completion Details: Schedule 40 PVC, 0.010-inch machine slotted threaded screen and threaded sohd casing, Morie #1 sand, bentonite powder seal. Flush mounted, bolt down, 12-inch diameter manhole. Locking, watertight gripper plug.

he number of blows required to drive a standard split-spoon sampler a distance of 6.0 idard split-spoon sampler is 2.0-inch outer diameter and 1.375-inch inner diameter.


MONITORING WELL LOG Sheet 4 of 4

Project Name: Fleet Bank Branch Street Address: 1322 Sea Girt Ave., Wall Twp, NJ 07719 Tax Map Address: Block 706, Lot 2 County: Monmouth

Owner: Fleet National Bank Owner's Representative: Gary Skowronski, V.P. Owner's Address: 3670 Route 9 South, Freehold, NJ 07728

GES Project Manager: John H. Montgomery, P.G. GES Case Manager: John H. Montgomery, P.G. NJDEP Case Number: Not applicable NJPDES Permit Number: Not applicable

Driller: Shore Drilling, Inc. Driller's Address: 23 Branch Avenue, Oceanport, NJ 07757 Driller's License Number: MD1540

Well Identification: MW3D Well Coordinate Number: 29.33.377 Well Permit Number: 29-45875 Latitude: North 40° 08' 9.4"; Longitude: West 74° 03' 44.9" Casing Elevation: 45.85 feet; Surface Elevation: 46.13 feet Well Depth: 60.75 feet Screen Length: 10 feet; Casing Length: 50.75 feet Drilling Method: Hollow stem auger Well Diameter: 4.0 inches Borehole Diameter: 12.0 Inches Sampling Method: Split-spoon Static Water Depth: feet Logged By: John H. Montgomery, P.G. Completion Date: November 16, 2001

Depth

(feet)

Sample

Number

Well Detail

PID (units)

Blow Counts

Recovery (inches) Depth

(feet)

Lithology/Remarks (Modified Burmister Classification)

60

61

62

63

64

65

66

0.6 0.5 0.5

0.9 0.2 0.5

4,5,9,17 24

16,21,22,29 23

10,15,28,30 18

60-62: Yellow to yellow-brown medium to fine Sand, little silt, trace (-) clay.

62-64: 63.75-64 feet: Dark grayish-black clayey silt. Fallback = 20 inches.

62-64: 64.5-66 feet: Dark grayish-black silty clay. Dense.

K i ^ End bonng at 66 feet

Bentonite-cement grout Bentonite powder seal Sand/Gravel pack

Well Construction Materials and Completion Details: Schedule 40 PVC, 0.010-inch machine slotted threaded screen and threaded solid casing, Morie #1 sand, bentonite powder seal. Flush mounted, bolt down, 12-inch diameter manhole. Locking, watertight gripper plug.

Note: Numbers in the column labeled "Blow Counts" refer to the number of blows required to drive a standard spHt-spoon sampler a distance of 6.0 inches using a 140-pound drop weight falling 30 inches. A standard spht-spoon sampler is 2.0-inch outer diameter and 1.375-inch inner diameter.


MONITORING WELL LOG Sheet 1 of 1 Project Name: Fleet Bank Branch Street Address: 1322 Sea Girt Ave., Wall Twp, NJ 07719 Tax Map Address: Block 706, Lot 2 County: Monmouth

Owner: Fleet National Bank Owner's Representative: Gary Skowronski, V.P. Owner's Address: 3670 Rte 9 South, Freehold, NJ 07728 GES Project Manager: John H. Montgomery, P.G. GES Case Manager: John H. Montgomery, P.G. NJDEP Case Number: Not applicable NJPDES Permit Number: Not applicable Driller: GES Probe Services Division Driller's Address: 1340 Campus Parkway, Wall, NJ 07719 Driller's License Number: JD1610

Well Identification: MW7 Well Coordinate Number: 29.33.377 Well Permit Number: 29-46075 Latitude: North 40° 08' 09.4"; Longitude: West 74° 03' 38.1" Casing Elevation: 36.35 feet; Surface Elevation: 36.89 feet Well Depth: 30 feet Screen Length: 15 feet; Casing Length: 15 feet Drilling Method: Hollow stem auger Well Diameter: 4.0 inches Borehole Diameter: 11.0 inches Sampling Method: Drill cuttings Static Water Depth: 18.45 feet Logged By: John H. Montgomery, P.G. Completion Date: January 11, 2002

Depth

(feet)

Sample Number

Well Detail

PID (units)

Blow Counts

Recovery (inches) Hand augered

to 4 feet

Depth Lithology/Remarks (feet) (Modified Burmister Classification)

10

12

14

16

18

20

24

26

28

30

^ ^

0-0.33: 0.33-1.0:

1-18:

Aspnalt Gravel base Yellow-orange to light brown well sorted Gravel, some (+) very coarse sand, trace (-) cobbles. Moist at 16 feet.

18-26:

26-30:

Light orange to pale yellow very coarse Sand, some (+) gravel, trace (-) very fine sand. Brown to yellow-brown silty Sand, some (+) gravel, trace (+) clay. Moist at 20 feet.

Pale gray to hght orange-brown very coarse Sand, some (-I-) fine sand, trace (-) gravel and silt. Wet at 24 feet.

i:sy^ End boring at 30 feet

Bentonite-cement grout Bentonite powder seal Sand/Gravel pack

Well Construction Materials and Completion Details: Schedule 40 PVC, 0.010-inch machine slotted threaded screen and threaded sohd casing, Morie #1 sand, bentonite powder seal. Flush mounted, bolt down, 12-inch diameter manhole. Locking, watertight gripper plug.

Note: Numbers in the column labeled "Blow Counts" refer to the number of blows required to drive a standard split-spoon sampler a distance of 6.0 inches using a 140-pound drop weight falling 30 inches. A standard split-spoon sampler is 2.0-inch outer diameter and 1.375-inch inner diameter.


Appendix 4

Monitoring Well Permit


' WR-133M koo


TRENTON, NJ

-»?•'

MaUTo: ?: NJDEP . pBUREAU OF WATER ALLOCATION

pbBdX426 >:TRENTO

MONITORING WELL PERMIT '^

VAUD ONLY AFTER APPROVAL BY THE D.E.R

CGORK#:

P. Permit No.

yip.jry

^M^y>J)/A J . y

Driller-

Address _etj Address rj i ii> y jy / y2^j^ ^&? A j<y^d r ^ / f \ 7

Name of Facility yy^^ ' / yjy^^ x^ ddress yôp ^ - i X^Jr^ y ^ ^ y ^

[_ Lot#'

Diameter ofWell(s) # of "Wells Applied for (max 10)

^ Inches

/

Proposed Deplh of WeU(s)

Type of Well (see reverse)

' y ^ r , , - i u ' " LOCATTQN OEWELL(S) ' ~ t # ' ^ " [Block# J iMimicipality/ ICounft \ / \

r J \y^Â \ ^ M / / \/Ajj(^yt//^

^ y f Feet Will pumping equipment be utilized' If Yes give pump y ^

capacity j / >^^^

YESD 6 J I ^ ^

cumulative GPM

[ State Atlas Map No. r y ^

c d

[

0

j ^ M l .

Draw sketch of well(s> nearest roads,buiIdings, etc. with marked distances in feet Each well MUST be labeled

' with a name and/or number on the sketch.

M

__>. r r ^ -i^j(-s; J ! 3 ^ \ C i f W ^ h \ \ ^ ' f 'i ••% k

3 :

'MSSMM^ WSh^ '

-i • ^

S ••?•

^

(fe

/ i 4 ^ ^

yô'

I -v

'

- • • • • -i • i

Nf l ^&RMOi®ORIl^PiL£Si 'REt ;6yERY WELLS, OR PIEZOMETERS, THE FOLLOWING MUST BE COMPLETED BY

\ t B ^ l i S 9 X l § 0 f W £ k S % m p i t l S S . WHY THE WELLS ARE BEWG INSTALLED

• f Bl&Site:^^ , . ' • ^ S . ' CEKOCA (Snj ifund) Site

D RpRASite:,-U

El<i^ndergrpund Storage Taiik Site

—Q': (3peral3onalGround Water Pennit Site

{r];v Ketreatmcint andResidtials Site

0'.: Water mdHazidous Waste Eiiforceirient Case

P*f:Vr^ty;SupptyAijuifeTfestpbse^ '' ' ;!|-.

E):/;Oilier ffexplain'): • , "-•••'• ' • ' •'•••• • • ' • '. "'' ' ••

CASE LD. Nuinber

. r- • -'. f Vr

This Space for Approval Stamp

WELL PERMIT APPROVED • N.J.D.E.P

NOV 8 2001

V, 3 ' ^ ' • .

' tuREAU.OF WATER ALLOCAT

J i i -F O R ' D' Issuance of tliis pennit is subject to the conditions attached, (see next page) b,EJ>L ^ F o r monitoring ptftposes only USE El

P Tje well(s)im£iy not be completed'witii more than 25 feet of total screen '» oruncased-.bprehole; "' :..

lEE REVERSE SIDE FOR IMPORTANT PROVISIONS PERTAINING TO THIS PERMIT. _n compliance with NJ.SA.58:4A-14, application Is made for a permit to drill a well as d^cribed above,

Date J ^ T--voy Signature of Driller. y 0 0 ' _ ^ . Jsri-A..ji. A

Signature of Property Owner. L^Jtj/ Reastration No. y j / A / T ^ A ^

A yyei'/£:,A.^^/f/ ^ ^ J /

COPIES: Water Allocation - White Health Dept - Yellow Owner - Blue/Dril ler - White e / D r

DWR-138 M 3/OOf

New Jersey Department of Eriyironmental Protection Bureau of Water Aiidciaitibn

MONlTOmNG WELLRECORP Well Permit No.

29 45875

Atlas Sheet Coordinates. 29 33 377

JOWNER IDENTIFICATION - Owner

I Address 'jH ' City J '

TLEET HriTIOHAL SANK

3670 RT 7 GOUTli State.

- i « -. Zip Code.

WELL LOCATION - If not the same as owner please give address: Owner's Well No. County ^>>v.^r.,.T,, Municipality ua; j r t t o Lot No. ^ Blocl< No,

Afu/-7 f/i\A/^-3D >.i»-i>iî-»liT{; TIwrrrTljTTTTt

A d d r e s s t - r o ^ <!?.r-A f T r i - r A u r WHCt—i rit ' / \ JO

TYPE OF WELL (as per Well Permit Categones). Regulatory Program Requinng Well

rtOHITORIHG' DATE WELL STARTED 1 1 I i S / < ^ /

DATE WELL COMPLETED / / / / /T 1 / 1 /

CasehD.#

CONSULTINGFIRM/FIELD SUPERVISOR (if applicable).

WELL CONSTRUCTION - _.

Total deptK drilled:; h J . ft-' Well finished to / f / ft.

Tele-. # .

Borehole diameter: Top A2_ in. Bottom. f l in.

[ Well was finished. D above grade

" ' %'-C S^l'ush mounted ' -«• ' ^ i - .L ' r ? * . ' / i",

\{ finished abaê gfade^,casing; hefght (stick up) ab"bye"larHlsbfface£^£4_ft. " ' ' \ \

i/Vas" steePprotective'casingliistalfed^'f ' ' ' '

Statfe water level after dr i l l ing^ J ft ,

yVate} level was measured using J n t r ^ -

Well was developed for > O hours at ^ gpm

Method of development J i O V A J n H a J i b

Note:''Measure"all depths -from land surface

Single/Inner Casing

Middle Casing (for tnple cased wells only)

Outer Casing (largest diameter) Open Hole or Screea (tsjoruse'd / ' )

Blank Casings 1[Np.:lJsed )' ^ '

.Taij-Piece

Gravel Pack

Grout

DeptB to Top (ft)

n

^

5-/ \

- ^ " '>. H ^

V? 0

~ Depth to Bottom (ft)

.5"/

*"

(S,/

\

r. r ' ^ 9

Dramefer (inches)

V

t^ /

-

12 1 ^

' - Matenal ""

PMC

J

mc ' ^ \ , V-

- , - ~ .

SM)b Neat Cement

,<BehtonSe

Wgt./Ratrng (Ibs/sch no)

S c h i ^

i&M- ,

-

OO lbs.

.20 n lbs.

Grouting Method Dniling Method _

YreHtf^" / ( j t-z^^ât^f kf 'hn

Was permanent pumping equipment installed' Q V e s ^

Pump capacity A J n gpm

Pump typer- ' - /4/"-4" :: • /"

No

Dniling Fluid. AJA Type of Rig A ' ^ O O

Health and Safety Plan submitted? D Yes Q No

Level of Protection used on site (circle one) None D C B A

/ certify that I have constructed the above referenced well in accordance with al l well permit requirements and applicable

State rules and regulations. r II r o^. f^^RY PARENT/SHORE DRIG. INC, Dniling Company ' 1

GEOLOGIC l£OG , Note each depth where water was encountered in consolidated - formations. - - - —

U l 1 - -5 '"Kn^>?/ -'

> - ^ / j1r^ K i l / i ' ^ ,, 'y-rr- c / ( i n r t /

r In /•<=!> ^ r

Well Driller (Pnnt).

Dniler's Signature.

yniew'f

y. \—7 V;.

Registration No. / / / ) f S ' H ' O Date / / / 6 l 6 ^

COPIES: Wh i te -DEP Canary - Driller P ink -Owner

AS-BUILT WELL LOCATION (NAD 83 HORIZONTAL DATUM)

NJ STATE PLANE COORDINATE IN US SURVEY FEET

NORTHING: EASTING:

O , ^ ^ LATITUDE: ' . _ " LONGITUDE:


)WR-133M ^00

Mail To: NJDEP BUREAU OF WATER ALLOCATION PO BOX 426 TRENTON, NJ 08625-0426


TRENTON, NJ ^ •. n MONITORING WELL PERMIT

VAUD ONLY AFTER APPROVAL BY THE D.E.R

COORD #:

Permit No. .9 H y oon„

29 • ^ • •$77

ivner F l e e t N a t i o n a l Bank

Address. 3670 Route 9 South

F r e e h o l d , HJ 07728

Driller

Address

GES

134(3 Campus Parkwav

w a l l . WJ 0 7 7 1 9

Mame of Facility _

ddress

F l e e t Bank

1322 S e a - G i r t Avenue •'' '- ^

W a l l , NJ 08750 ' * ' . .r , . •-•-' LOCATION 0]

Diameter ofWeU(s) 4 Inches

Applied for (max 10) ' '' ' " TypeofWeU (see revere) M O H l t O r i n g

^WELL(S) . ' ,> ..i

Proposed Depth of WeU(s) 1 0 Will pumping equipment t»utili2e(i' If Yes, give pump capacity

> i ' - '

Feet

YESD N O n '

cumulative GPM

. . . . M

[ c

Lot# Block# 7 0 6

Municipality

Sea G i r t County

Mbnaioutli ,

State Atlas Map No. 29

40 0 10 '

Draw sketch of well(s) nearest roads,buildings, etc. with marked distances in feet. Each well MUST be labeled

.with a name and/or number on the sketch.

-.40 '08

C

O

• L-AuRLv .A i£

Mr4K

S£h S\AT hiH

,Nf FOR MONITORING WELLS. RECOVERY WELLS, OR PIEZOMETERS, THE FOLLOWING MUST BE COMPLETED BY THE APPUCANT PLEASE INDICATE WHY THE WELLS ARE BEING INSTAT .1 .ED

D Spill Site

J ISRASlte

• CERCLA (Supetfiind) Site

1 RCRA Site \ y ' r ••:-::...• CASE LD. Number

T Underground .Storage Tank Site ,. N / A

• Operational Ground Water Permit Site „

] Pretreatment and Residuals Site

] Water and Hazardous Waste Enforcement Case ' ^'^

D j ^ t e r Supply Aquifer Test Observation Well '^ , 4 \ \ r ' A

icrotherfexpiain) Owners " I h v e s t i q a t i b r i . •• v.' •

This Space for Approval Stamp •

WELL PERMIT APPROVED NJ . D.E.R

DEC 2 7 2001

BUREAU OF WATER ALLOCATION •

F O R D Issuance of this permit is subject to the conditions attached, (see next page)

. c / . r . ^,.»a^p(jf momtonng purposes only . j s E n • • — ' - — ' — ' • — • — - — ' • • ' " ' ' •' -'••• ^",' • — - ^ _

y . - ^ The weli(s) inay not be completed with more than 25 feet of total s •- or uncased borehole.

_iE REVERSE SIDE FOR IMPORTANT PROVISIONS PERTAINING TO THIS PERlvUT. . I In compliance with NJ.SA.58;4A-14, application is made for a pennit to drill a well as descrilied above,' /.'

'-'ate / ^- " /'t''C:'- • • Signature of DriUer__li;::r ''" // Registration No. " " 6"' ^

Signature of Property Owner ^

"•- • ,.'-.....,....i::..-:-—--7 Registration No. _ l ! i ! _ £ i j ^

/ ^ / n o j r r . Ti7_*— Ati ^ -

_ ; R - 1 3 8 M New Jersey Department of Environmental Protection Bureau of Water Allocation

MONITORING WELL RECORD Well Permit No. _22 - 4<Sn7'>

Atlas Sheet Coordinates. 7NER IDENTIFICATION - Owner

jress

-59- -53- -577-TLCET NATIONAL DANK

5670 ROUTE 9 SOUTH îty. -LINDEN State -NJ- . Zip Code.

1] -LL LOCATION - If not the same as owner please give address. Owner's Well No. oUnty MOMMniiTH : [ Municipality SFA RTRT RORn Lot No.

MW-7

. Block No. 706 \ddress. 1.^79 •< FQ GTRT flVF

DATE WELL STARTED "> / 11 / 02

PI PE OF WELL (as per Well Permit Categories) Regulatory Program Requiring Well

MONITORING DATE WELL COMPLETED J _

, Case I.D.# N / A

"/11 HJT

. INSULTING FIRM/FIELD SUPERVISOR (if applicable)

WELL CONSTRUCTION

r4 3l depth drilled ^ n ft.

GES Tele. # 7 3 2 - 9 1 9 - 0 1 0 0

rl lie /^c« fii finished to 3XL .ft.

apehole diameter 11

Bottom JJ_ in. in.

C was finished: d ajjeê grade [ 0 ^ s h mounted

f finished above grade, casing height (stick iT^l above land surface . ft.

4 J S steel protective casing installed? UVesfM No

Spitic water level after drilling 1 4 ft.

Jer level was measured using I n d i c a t i w?

Veil was developed for. 2 gpm c

hours


Single/Inner Casing



Open Hole or Screen (No. Used . 0 1 0 ) Blank Casings (No. Used )

Tail Piece

Gravel Pack

Grout

Depth to Top (ft.)

. 5

1 0

8

0


1 0

30

3 0

8

Diameter (inches)

4

4

11

11

Material

PVC

PVC

#1Sand Neat Cement

Bentonite


^ C H 4 0

SCH40

lOOOlbs lbs.

sn lbs.

Method of development. Whale Pump

r Grouting Method T r e m i e G r o u t Drilling Method H . S . A

'- s permanent pumping equipment installed? OYes [ 0 No

mp capacity gpm

Pump type: •.

lining Fluid Type of Rig A . M . S

Health and Safety Plan submitted? D Yes [ 0 No

I vel of Protection used on site (circle one) None/^DJ C B A


State rules and regulations. GROUNDWATER & ENVIRONMENTAL SE Drilling Company

Ls l l Driller (Print) William Lovenberg

iller's Signature 2= -JL ^Registration No. JP1 61 0 Date I u / I oX


0-6" Asphalt 6"-3' Course brown aand & cobbles 3'-6' Medium sized cobbles fi'-1R' Fine tan sand 18'-::>q' Course tan sand ^KtX^HXKXMMXKMMXMaMgXX 2.'5'-30' Course tan sand with some

clay

AS-BUILT WELL LOCATION (NAD 83 HORIZONTAL DATUM)

NJ STATE PLANE COORDINATE IN US SURVEY FEET

NORTHING: EASTING: 0 , OR

_. ' • _ " LONGITUDE:. LATITUDE


Appendix 5 ^

Drill Cuttings and Development Water (Waste Manifests and Analytical Reports)

G

G

G

G


03/01/02 FRI 14:54 FAX 1 732 815 9892 NJ OFFICE ii002

' * NON-HAZARbO.U.SwSsTE MANIFEST Please prinl cr lype iFormdroiBnedtoruBBondi icdZpi idi) lypawiiiar)

NON-HAZARDOUS WASTE MANIFEST

1. C-ermmiars US EPA ID No.

4r APV

" ' j ' . - ^ <A Z, Page 1

3. Gonsralor't Name and Mailing Address

r <J. Goneraior's Phone ( )

Fl<?eT Hatiozml Eaiii: ;i670 Rout.fr .9 Sovit'h

Sita Addross

APV J o M o3-o3n( 5. Transporter 1 Campany+jBrne ' '• •*

'•.'] . i . y i " - . ' ^ . - '.•' w^^•'• l • V - T . C 1 US EPA ID Numbef

• • I ' '•' •'• ? • S . 1

A. SiBtt Trensponei's I D P - \ " ' - '^ '^F:

B.Tranaponer 1 Phano . ' ^ I ' V ' . P^(."',_Cif^,Q

7. Tiansponer 2 Compangr Nome

I i 1'l.'.-t..=rtv- P'-iTJfir V?ir

B. US EPA ID NumPB^

|-3 .T I ' f) Ci 3 6 1 C. sifltcTransponBrs ID [^1 ; ' i / ^? f - ,

0 d D. Tranaponni z Phonn ,• is-7p,..q-^.-:.

B. Daslgnaied Facility Nama and Slle Address

Ipfenn Ohio Corporatiorj |4B13 Woodman Avenvie

10. US EPA ID Number E. StaiB Faciny's 10

b H R 0 0 0 n ? 8 P 3 'j' F. Faclllty'o prione

11. WASTE DESCHIPTION 12. Conlainat^

No. Type

13. TelBl

•uoniliy

1 < 1 . Unh

WI./Vdl.

Hon Regulated Mater ia ls tOl!ly Ptaenj-Non DOT/Noji RCRA : ^

( ^ D H I f lOJL 9

G, Addllional Deaeripiiora tor Matadala Listed Atwva

a-CS)

t . Soil and Debris

d.

H, Handling Codes for Waalas Listed Above

b . d.

15. Spcdal Handling Inainjcitone and Addltlenal Intormalisn

- • ^^^ • •OÔÔt -6

Emergency Contact - 800-876-9699 On Call Suparvisor APV Truck*:

16. GGNEHATOR'S c e n n n c A T I O N : I nanaby ceiliry that (he oonisncs ol Itila ahlprrant arg lully and ataj ialdy descflbad and aia In all reapeeia In propar condiuen lor tranapiui. The maieiuls deeeribad on iNs manllBat a n m l subjact lo fadaial hazardous waste laguiatkma.

Dais

iMin'yped Name i j . . '

\ioUv^ rlnV\-oow>f> g: Monm O t y , Yaar

.17, Tranapoitar 1 AcknoMadsemeni a( Sreeelpt of Male(lala< O&le

prIniBd/Typed Name lame • . \ j . ^ ^ ^ Uonm Day ' Yaar

' 16.'TrsnspoiiBr 2 ADKneMledgomoni ol RacQlpI ot Kflaionale Date

PilnledTyped Nama SlBnalure Monrli Day Year

IS. Discivcancy indlcailon Space

20. Facility Oitner or Operator, Csnlllcailan ot reeBlpi ol ItiB waste materials covered by Diis manllcs.!, except as rtotad In nam 19.

Jix Dole

PrinlodrTypoi) Namo

H \ chn-^rn \ Signature.

v>. J^ ,-d-M.. ., ' " \ > j < , v v r 7 v ^

Mioflin Day Ymr

http://Rout.fr

03/01 /02 FRI 14:54 FAX 1 732 815 9892 NJ OFFICE V - . .-».-„,...,«-. ^: 1 StataofNewJ8rs.ey

., Departmerit of Environmental Protection . Hazarclpua Waste Fttguiatlon Program

Manifeflt Section ' P.O. B o x 4 2 1 , T i ¥ n t o n , N J 0 8 6 2 5 - 0 4 2 1

Please type or print in block letters. (Form.deaignet) for lisa on ejlta (l2'Pitch) typewrrtef.) 1 3 ^ ^ " * " ^ ^ ."• ' • 11 r5flnQratnr*B 11.^ PPA i n Wn /

iaoo3

•':^r<'-'.vr.*".'

Form Approved)- • •••• OMBNa. 2050-0039.

UNIFORM HAZARDOUS WASTE MANIFEST

3. Generator^ Name and Mailing A d t J r o s / * * " * ' '

.1. Gerierator'a US EPA ID No. 9r©iftl0|3|7iSîi6i9 II j J h « r [ . » | « | » M

IT

." Manila !fti- a. Page Paga.1<" •.-,: o r •.•/.'*••*;''••

';,'• irifotmatibn'iri'tHeshadsd sreas ;..,'.'. .'c.la'hol requifed byj'.Fecleral lajiv;, .

a. Generator's Phone'( 732,

367Q ifouts 9v^ t t th f r9i iM»i(l"HJ ..97728 . i 3 3 5 •••••

A.' Swi8.Mar1HBSft'0iSt:wm|nf I

5. TrainspottBr 1 Company,Name. •..,.

•' All'Otnto... Powos- VfliO-6. US EPA ID Number

», j ,D i f t i » ,3 ,av . i i ' a i« i4 |T 7. Transporter 2 Company Nama

Allot3t«.>gw«r Vac • 8. . US EPA ID Niimber •

M I J I i> I & I d 1 3 | . ^ i 1 1 2 | 0 1 4 1 7 .

9. Deaignated Facility Name and Sits. Address

Cyi;X0 Ctom, Inc. 217 South F i r s t St jwet ' El izal iot]) »J «l72ai&

10. u s EPA (D Number

| 3 | { > l « ) , ' ® , 2 | 2 , « | 0

11.,' OS'DOjr Oestrlpll6n f /nc/ue(ftig'fifopO("JSh/{)j9ing Wamej' Haian*C(ass of OiVrs/on,. '•', '

H M .• •

14,.6

^MB^^^!m^m^'''-^ym'^^^

•H;!JilBc:l(ilV'sPhDnB'']!S'»S' j

[ i a . Coniaitiara'

. " T t - f i - i . . . . .

No, îp^SSM. ,, ,-. ...

tftiiyl^w?) 9. Ulf3«a2r t i l F«92. IM939 Oi'«i,.^.i

0 ^^ '^ I s . f t J in i r - . i ' i i ; ; ; ; . .

Bt <3ti itty>inaf.i--^prli'l'tir:l^^

•'tt:<.'v'v.''i'.iv..'.f".' ::„-i?*ll.'rJl'iU.,j;'J,v.i;:/;;.'i;j'..-',^3UEL fl,-,. ."Ill , L . l . " J S . « ; * 3 [ 3 ' . | B i 1 J L J W r ^ . ' J , , , , L . ....l.,,,,'i •,; ....-.'..•"?- '."••..W.-.j.V

'•::uH\,:%t>*t>rj\iur,r-;ivt:-i-y-'-

:cfc;^ . . . * • ; • •

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IS. special Hanailnglnstruaions i

Av io .iiV ; x3i

[Additional, -9i&SI9/Qii» Ceil Svtpvrvimr

5 : .. i'.^^^'i-: (• ^

iS,dei ' f f lOfM^| l6 ' '4^Rîn6ATION: I hereby declare tliatttie contents of this consignment are ful/y and accurately dasorlbad above by proper shipping name and'ara .. classirt^, pbcked, marked, and Isêlad, and are in all re jec ts in proper condition for trarisport by. highway according to apqilcablo international and national government

regulations. ' • ' •' '. i . ' ' •• i . ' ' • ' " . ' ' i , ' . ' i • ; . ' ' ' ''• •

If I am a large quanlily generator, I cerlity that I have a program in place to reduca the volume and toxicity ol waste generated to the degree I tiavo deterrHinsd lo be economlcally'praalcablB and that 1 have selectea.ttie praclicable molhod ol troatment, .storage, or disposal currently available lo ma which minlrnizes the present anO tutura threat to human health and the environment; OB, 1(1 am a small quantity generator, I have made a good faith effort to minimize my wastegcneration arid select the best waste rnanaqement method that Is available to me ,' nd that I can afford.

Piintad/Typed NaipQ

UsSi^^ g - l * v t / M r f t Month -.Day.- Yaar

';"2ic.|îrii K 17. Transporter 1 Acknowlqqafement of Rec^pt of Materials

Prinled/Typod Nfime ^ XWW ./^-^ . 18, Transponer 2 Aci<lriowiedgement of Receipt ofMaierlals

PAonth Day /ea/

<:S7 < ^ $ 2 ^ - ^ ^ Prinled/Typed^me g ? - - ^ ^ / ^ ^ Sl!;)nature

19. Olscrapancy Indication Space-

< r ^ ) < / ^ ^ ^

Month Day Year

KE££miMAAJM. 20. Facility Owner or Operator: Certlllcation of receipt of hazardous inalerial.'i covered by this manifest except as noted in Item l9, / .

V PrlniedH'yped Name ,

X ^ — . i . i« ' • l l .

Signature Mpnth DBjf- Year.

•fc-^T

02/01/2002 12:59 CfiSIE PROTflNK ^ 17329190916 NO.898 D003

^mE. PROTANK E N V I R O N M E N T A L S E R V I C E S

Pleaie typ« or print in block latlcrt. (Form dealaned lor use on wllte (T2-pHch) typewriter.)

NON-HAZARDOUS MANIFEST

1,-Generator's u s EPA ID No. . ' , , . I Docurnent No.

N (0 IN IE IR IE 10 lU II IR lE ID 16 l8 10 14 lO 3. Generator's Name and Mailing AadrBBBp^gg.j^ N 3 t . i o n a l B a n k

i322 seagrii- Ave

4. Generator's Phone (

5, Transponor 1 Company Name

Wall .NJ.07719 73? ) 449-5510

u s 6PA ID lûmber

Casie Ecology Oil- Salvage. I n c . W -J ID 10 l4 1.' \9 lg 15 l5 I9.,l3 I 7. Transporter 2 Company Name US EPA ID Number

S. Dsslgnated Facility Name and Site Address

c a s l e Ecology Oi l Salvage, I n c . T/A 3209 N- HllJ Rd / c a s i e pro tank Vineland NJ 08360 •

Mil 10. u s EPA ID Number

IWIJIDIO 14 IS 19 19 15

11. US DOT Description (i 'ing proper Shipping Name, Haz&ni Class, and ID Number)

Sagolino Contaminated Solids Non -DOT Regulated

61913

2. Page 1

of

A. Non-hazarilous Manifest Document Number

77771 NHZ020 B, Stale Generator's ID

SAME

C, Slate Trans. ID }>?l>ff^Z6<!?i^ D. Transporrer's Phone (( g 5 6 ) ) 6 9 6 - 4 4 0 1

E. Stale Trans. ID I

F, Transporter's Phone (

Q. StatePaciiityslO0614DlHP05

12. Containers

No. Type

M. PecHity's Phone ( 8 5 6 ) 6 9 6 - 4 4 0 1

8 o..i..q \ ^ DIM

13. Total

Quantity

0|D 'OO

14. Unit

WlA/ol Waste No.

P12 | 7

J J.. Additional Descriptions for Materials Listed'Above

(S)

K. Handling Codes for Wastes Listed Aoove

^

1S. Special Handling Instructions and Addllional Intormalion

a.?4 hr emergency response #609-685-23 56 G.CALL 16. GENEnATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are tully and accurately deaoribad at)Ove by

proper shipping name and are classified, pacHad, marKed, and labeled, and are in alt respects in proper condition for transport by highway according to applicable international and national govemmenl regulations.

(.hereby certify thatttie above-named matariai Is not hazartlous waste aa defined by 40 CFR Part 261, 2M and 279 orany applicable state law.

Printed/Tvoed Name^,^., y y y

J /7/fhr^^ . } a>y:7fhBi^ Month Day Year

17. Tranf iparter 1 Acknow ledgemen t of Reinelpt of Materials

J'rinjgdAryped Natufi ^ ^ _ . y-

18. Transporter 2 Acknowledgement of Heoeipi of Mate.'iftls

Month D»y Year

\P\'Pr(\^Î Printed/Typed Name Month Pay Yaar

19. Discrepancy indication Space

SecKDr. l i f t ShOjA-ici Jle£*4; N/Or\ HctTo«^Jou^ hâvTLr'4cUCS0» 'll)

won t jcrr iJ^^t^cL-vM 20. Facility Owner or Operator. Certification of receipt of non-hazardous itnatftrials ooverad by

Prin'led/Typi 'yrmsie^^j^ signature

;l except as notad in Hem 19.

T^rH^ . . . . r m L l u t lCTT tK I K f i l B I R O N Al L COPIES

.02£01/2002 12 :59 CflSIE PROTflNK -. 17329190916 NO.898 0002

i\©£ PROTANK E N V I R O N M E N T A L S E R V I C E S

.PlBBH type or prlnl Ift blocK lotlw*. (Form dc*lened tor use on glUe (12-pllch) lypewrltcf.)

NON-HAZARDOUS MANIFEST

1.' Generator's US EPA ID No.

N l O | y ! I E l K l L : l O I U l l T tSeneralor's Name and Mailing Address ip-j gg- j . pfaC. l o n i l l ' B a n k

223 Buffalo Ave

Egg HarDor NJ 08215

i . Generator's Pfione ( 7 3 2 ) 9 1 9 - 0 1 0 0

, , I Doctjmem ,_. R . 1 E I D 1 0 I 0 1 3 I 1 1 1

INO. iii

5. Transporter 1 Company Name US EPA ID Number

C a s l e EcolQ<i^ O i l S a l v a g e . I n c . W J ID 10 14 l5 19 19 15 l6 I 9 I 3 7. Transporter 2 Company Name

9. DesignelBd Facility Name and Site Address

Casie Ecology Oil Salvage, Inc. T/A

10.

u s EPA ID Number

L'\ M M M u s EPA ID Number

D C

3209 N. m i l Rd V i n e l a n d NJ 08360

7 Casie Protarik I N I J I D I 0 | 4 | 5 | 9 . | 9 I 5

11. u s DDT Description (Incluaing Proper Shipping Name, Hazard Class, and ID Number)

Gasoline coataminated Solids

Non DOT Regulated .

6 1 9 1 3

2. Page 1

Ol

A. Non-hazardous Manilest Document Number

NHZ020 79927 B. State Generator's ID

SAME:

C. state Trans, ID

D. Transporter's Phtine ( ( g S 0 ) 6 S ^ 4 4 0 1

E, State Trans. ID

F. Transporters Phone ( ) G. State Fflciiiyg ID 0 5 1 4 D l H P g 5 H. Facility's Ptione(r 355)1) 6 9 B - 4 4 0 1

1Z. Containers

No.

Bf9 ofeH

Type

DIM

13. Total

Quantity

14. Unit

WtA/ol Waste No.

Jj Ul 2 I /

C »

c

J. Additional Descriptions for Materials Listed Above

(S)

J . _ _ K- Handling Cooee for Wastes Usied Above

Sol

tats . Special Handling Instructions and Additional Information

a.24 hr emergency response-#609~6S5-2156 G.CALL 16. GENERATOR'S CERTIFICATION: 1 hereby declare itiat the contents of this consignment are luHy and accurately described above by

proper snipping name and are claBsified, packed, marked, and labeled, and are in aU respects in proper condition for transpon by highway according to applicable international and national government regulations.

I hereby certlty that the abova-namsa matariai Is not hazardous waste aa defined by 40 CFR Part 281, 264 and 279 or any applicable atata law.

[ K/> art i < l l o h r O p Printedn'yped NaiTie '

<t^-2-Signature Month Day Year

J ^ 17. Tranaporter 1 Acknowledgement of Receipt of Materials

^^-a-inted/Typed Name _ ?

fl/9/.^-Z-18. Transporter 2 AcknowledgemenijRReteipl of Materials

Sigrtature

r^^J^y^y^y^^ Prihted/TypeO Name Signature

^ ^

Month Day Year

Month Day Year

19. Discrepancy Indication Space

3hit 20, Fadlity Owner or Operator; (iertifitatlon of receipt ol non-^Bzatdous materialB coveted by this mi hilest except as noled In Item 1S.

Priritei Signature Month P B » / Year

i » i e n o M a T i n N W O S r B E LEGIBLE O N ALL COPIES

j n t e g r a ' t e d

l a l y t i c a l

L a b s

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In tegrated Analyt ical Laborator ies, LLC. 273 Franklin Road Randolph, N.J. 07869

ANALYTICAL DATA REPORT for

Groundwater & Environmental Services 1340 Campus Pkwy

P.O. Box 1750 Wail.NJ 07719

Project: FLEET BANK - WALL Lab Case Number: E02-0258

Date Report Prepared: January 30, 2002

CLIENT SAMPLE ID

SOIL DRUM

LABORATORY SAMPLE ID

0258-001

Phone:973 361-4252 Fax: 973 989-5288

Ail required protocols were followed during analyses. These data have been reviewed and accepted by

Michael H. Leftin, Ph.D. Laboratory Director

c 0

[

R E C E I ¥ E i FZS 0 1 21ffl!

The liability of Integrated Analytical Laboratories, LLC. is limited to the actual cost of the analyses performed.

lAL is a NELAC Certified Lab # 14751 and maintains certification in Connecticut # PH-0699, New York #11402 and Florida # E87670

c

INTEGRATED ANALYTICAL LABORATORIES, LLC.

TABLE OF CONTENTS

Page

Qualifiers 1 Conformance / Nonconformance Summary 2 Laboratory Deliverables Check List 3 GC/MS Nonconformance Summary 4

Summary Report 5

Analytical Results TCLP Volatiles 6

General Analytical Sulfide, Reactive 7 Cyanide, Reactive Ignitability @ 142T/Flash Point pH

Methodology Summary 8

Quality Control TCLP Volatiles 9

Tuning Results Summary Method Blank Results Summary Calibration Summary Surrogate Compound Recovery Results Summary Matrix Spike/Matrix Spike Duplicate Results Summary Internal Standard Summary Chromatograms

General Analytical 31 Blank Results Summary Spike Sample Results Summary Duplicate Sample Results Summary

Sample Tracking Chains of Custody 35 Laboratory Chronicle 38


MATRIX QUALIFIERS

" A - Indicates the sample is an Aqueous matrix.

O - Indicates the sample is an Oil matrix.

S - Indicates the sample is a Soil, Sludge or Sediment matrix.

_ X - Indicates the sample is an Other matrix as indicated by Client Chain of Custody.

DATA QUALIFIERS

_: B - Indicates the analyte was found in the Blank and in the sample. It indicates possible sample contamination and warns the data user to use caution when applying the

r results of the analyte.

C - Common Laboratory Contaminant.

D

C

c c

D - The compound was reported from the Diluted analysis.

D.F. - Dilution Factor.

E - Estimated concentration, reported results are outside the calibrated range of the instrument.

J - Indicates an estimated value. The compound was detected at a value below the method detection limit but greater than zero. For GC/MS procedures, the mass spectral data meets the criteria required to identify the target compound.

MDL - Method Detection Limit.

Ml - Indicates compound concentration could not be determined due to Matrix interferences.

NA - Not Applicable.

ND - Indicates the compound was analyzed for but Not Detected at the MDL.

REPORT QUALIFIERS

All solid sample analyses are reported on a dry weight basis.

All solid sample values are corrected for original sample size and percent solids.


CONFORMANCE / NONCONFORMANCE SUMMARY

Integrated Analytical Laboratories, LLC. received one (1) soil sample(s) from Groundwater & Environmental Services (Project: FLEET BANK - WALL) on January 11, 2002 for the analysis of:

(1) TCLP Volatiles (1) Sulfide, Reactive (1) Cyanide, Reactive (1) Ignitability® 142°F (1) Corrosivity as pH

G

C

C

E

A review of the QA/QC measures for the analysis of the sample(s) contained in this report has been performed by:

Reviewed by' Date


LABORATORY DELIVERABLES CHECK LIST

Lab Case Number: E02-0258

C

c

c

1. Cover Page, Title Page listing Lab Certification #, facility name & address and date of report preparation.

2. Table of Contents.

3. Summary Sheets listing analytical results for all targeted and

non-targeted compounds.

4. Summary Table cross-referencing Field ID's vs. Lab ID's

5. Document bound, paginated and legible.

6. Chain of Custody.

7. Methodology Summary.

8. Laboratory Chronicle and Holding Time Check.

9. Results submitted on a dry weight basis (if applicable).

10. Method Detection Limits.

11. Lab certified by NJDEP for parameters or appropriate category of

parameters or a member of the USEPA CLP.

12. Nonconformance Summary.

Check If Complete

y

QC Reviewed "by

y

and y

y

y

y

y

y

y

y

tegory of y

y

1 1 ^ . D l Date

c c E

INTEGRATED ANALYTICAL LABORATORIES CONFORMANCE/NONCONFORMANCE SUMMARY

GC/MS VOLATILE ANALYSIS

Lab Case Number: E02- O A S ?

c

1. Chromatograms Labeled/Compounds Identified (Field Samples and Method Blanks).

2. GC/MS Tuning Specifications: a. BFB Passed

3. GC/MS Tuning Frequency - Performed every 24 hours for 600 series, 12 hours for 8000 series and 8 hours for 500 series.

4. GC/MS Calibration - Initial calibration performed within 30 days before sample analysis and continuing calibration performed within 24 hours before sample analysis for 600 series, 12 hours for 8000 series

5. GC/MS Calibration Requirements:

a. Calibration Check Compounds

b. System Performance Check Compounds

6. Blank Contamination - If yes, list compounds and concentrations in each blank:

7. Surrogate Recoveries Meet Criteria (If not met, list those compounds and their recoveries which fall outside the acceptable range)

if not met, were the calculations checked and the results qualified as "estimated"?

8. Matrix Spike/Matrix Spike Duplicate meet criteria (if not, list those compounds and their recoveries/% differences which fall outside the acceptable range)

9. Internal Standard Area/Retention Time Shift meet criteria

10. Extraction Holding Time Met If not met, list number of days exceeded for each sample:

No

-/

Yes

s ^

_ k ^

Hf^

MP>

^

na

/

^

H*^

11. Analysis Holding Time Met If not met, list number of days exceeded for each sample:

V

12. Sample Dilution Performed ^ High Target High Nontargef

Compounds Compounds

13. Comments:

Matrix Interference Other

iZ-'-p €i>^-rn$-Pvcrr

y_

Organics Manager 1-17-^'

Date


[ G

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SUMMARY REPORT Client: Groundwater & Environmental Services

Project: FLEET BANK - WALL Lab Case No.: E02-0258

Lab ID: Client ID:

Matrix: TCLP Matrix:

Sampled Date: PARAMETER(Units)

TCLP Volatiles (ppm)

Vinyl Chloride 1,1-Dichloroethene 2-Butanone(MEK) Chloroform Carbon Tetrachloride 1,2-Dichloroethane(EDC) Benzene Trichloroethene Tetrachloroethene . Chlorobenzene 1,4-Dichlorobenzene

General Analytical

Sulfide, Reactive (ppm) Cyanide, Reactive (ppm) Ignitability @ 142°F (Yes/No) Corrosivity as pH (S.U.)

0258-001 SOIL DRUM

Aq Soil ueous

Leachate 1/11/2002

Cone

ND ND ND ND ND ND ND ND ND ND ND

ND ND NO 7.04

Q MDL

0.0095 0.022 0.015 0.008 0.014

0.0045 0.0065 0.0095 0.011 0.008 0.007

17.8 11.1 NA NA

ND = Analyzed for but Not Detected at the MDL

INTEGRATED ANALYTICAL LABORATORIES

TCLP VOLATILE ORGANICS

Client/Project: GES/FLEET BANK - WALL

.—

- ,

l _ i

|—

[;

L-i

Lab ID: 0258-001 Client ID: SOIL_DRUM Date Received: 01/11/2002 Date Analyzed: 01/16/2002 Data file: K9000.D

Compound Vinyl Chloride 1,1-Dichloroethene 2-Butanone(MEK) Chlorofoim Carbon Tetrachloride 1,2-Dichloroethane(EDC) Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene

T ' ^ j . ^ l T^ „ * / - » „ « ,

Concentration ND ND ND ND ND ND ND ND ND ND ND

^ A „ . r\

Q

'

GC/MS Column: DB-624 Sample wt/vol: 0.1 mL Matrix-Units: Aqueous-mg/L (ppm) Dilution Factor: 50 % Moisture: 100

MDL 0.0095 0.022 0.015 0.008 0.014 0.0045 0.0065 0.0095 0.011 0.008 0.007

Total Target Compounds


GENERAL ANALYTICAL

G

G

Client/Project: GES/FLEET BANK - WALL

Lab ID: 0258-001 CUent ID: SOIL DRUM Date Received: 1/11/02 % Moisture: 10.1

Compound

Sulfide, Reactive Cyanide, Reactive Ignitability @ 142°F Corrosivity as pH

Result

ND ND NO 7.04

Matrix Q Unit

Soil-mg/Kg Soil-mg/Kg Soil-Yes/No

Soil-S.U.

DF

1 1 1

NA

MDL

17.8 11.1 NA NA

Date Analyzed

1/17/02 1/17/02 1/15/02 1/15/02

G

G


METHODOLOGY SUMMARY

Analvtical Parameter

TCLP Volatiles Sulfide, Reactive Cyanide, Reactive Ignitability® 142°F/Flash Point pH

Aqueous Samples Method #

NA NA NA NA NA

Soil/Other Samples Method #

EPA 1311/624 EPA 7.3.4.2 EPA 7.3.3.2

HZWAS CHP.7 EPA 9045C

G r

G

G

G

G

VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

L. -

_,.

E — 1

p

—

— i

--T

_ 3

—:

z

l—

Lab File ID:

Inst ID:

m/z

50 75 95 96 173 174 175 176 177

This check applies

Client ID

20-PPB-STD 5-PPB-STD

100-PPB-STD METHOD-BLK LFB

MS 8340MW-1B 8340MW-2 8340MW-3

- TB011002 MW-25

MW-20 MW-20D

FB011002 NJTA_6S_INF

K8968.D

MSD K

Ion Abudance Criteria

15-40.0% of mass 95 30.0 - 60.0% of mass 95

BFB Injection Date:

BFB Injection Time:

01/15/2002

9:28

%Relative Abundance

17.6 48.7

Base peak, 100% relative abundance 100.0

5.0-9.0% of mass 95 Less than 2.0% of mass 174 Great than 50.0% of mass 95 5 .0-9.0% of mass 174 95.0- 101.0% of mass 174 5 .0-9 .0% of mass 176 1-Value is % mass 174

to the following SAMPLES, MS,

Lab Sample ED

20-PPB-STD 5-PPB-STD 100-PPB-STD

METHOD-BLK LFB 0090-002MS

0090-002 0090-003 0090-004 0248-001 0248-002

0248-003 0248-004

0248-005

0252-001 NJTA_6S_A/S_EFE)252-002

NJTA_6S_B1'WN

NJTA_6S_EFF NJTA_6N_EFF TRIP_BLANK

_ 0252-003 0252-004 0252-005 0252-006

FUelD

K8969.D K8970.D K8971.D K8976.D K8977.D

K8978.D K8981.D K8982.D K8983.D • K8984.D K8985.D K8986.D K8987.D K8988.D K8989.D

K8990.D

K8991.D K8992.D K8993.D K8994.D

Page 1 of 2

2-Value is 92

6.8 0.5 76.2 4.3 76.6 4.7

) mass

( 0.6 )1

( 5.6 )1 ( 100.5 )1 ( 6.1 )2 176

MSD, BLANKS and STANDARDS:

Date Analyzed

01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002

01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002

01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002

Time Analyzed

10:06 10:33 10:59 15:17 15:43

16:10 17:30 17:57 18:24 18:50 19:16 19:43

~ 20:09 20:35 21:01

' 21:28 21:54

22:20 22:47 23:13

FORM 5

VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

G

Lab File ID:

Inst ID:

m/z 50 75 95 96 173 174 175 176 177

K8968.D BFB

MSD K BFB

1

Ion Abudance Criteria 15 - 4U.0% ot mass 95 30.0-60.0% of mass 95 Base peak, 100% relative abundance 5 .0-9 .0% of mass 95 Less than 2.0% of mass 174 Great than 50.0% of mass 95 5 .0-9.0% of mass 174 95.0-101.0% of mass 174 5 .0-9 .0% of mass 176

Injection Date :

Injection Time:

%ReIative Abundance

17.6 48.7 100.0 6.8 0.5

76.2 4.3

76.6 4.7

(

( ( (

01/15/200

9:28

0.6 )1

5.6 )1 100.5 )1 6.1 )2

1-Value is % mass 174 2-Value is % mass 176

G This check applies to the following SAMPLES, MS, MSD, BLANKS and STANDARDS:

' _

-

\—:

• - ^ ^

~'-.;

—

-^

Client ID

MW-1 TRIPBLANK FIELDBLANK TCLPMB SOIL_DRUM

MW8

MW9 MWIO MW14 MW15 FIELDBLANK TCLPMS MS MSD MSD NJTA_6S_INF

MW8

Lab Sample ID

0257-001 0257-002 0257-003

METHOD-BLK 0258-001 0265-001

0265-002

0265-003 0265-004 0265-005 0265-006 TCLPMS 0252-003MS

0252-003MSD 0090-002MSD 0252-001

0265-001

File ID

K8995.D K8997.D K8998.D

K8999.D K9000.D

K9001.D

K9002.D K9003.D K9004.D K9005.D K9006.D K9007.D K9008.D K9009.D K9011.D

K9013.D K9016.D

Page 2 of 2

Date Analyzed

01/15/2002 01/16/2002 01/16/2002

01/16/2002 01/16/2002 01/16/2002

01/16/2002

01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002

01/16/2002

Time Analyzed

23:39 0:32 0:58

1:25 1:51 2:17

2:43 3:10

3:36 " 4:02

4:29 4:55

- 5:22 5:48 8:45 9:39

10:55

FORM 5

VOLATILE METHOD BLANK SUMMARY

Lab File ID: K8976.D

Date Analyzed: 01/15/2002

Instrument ID: MSD K

Time Analyzed: 15:17

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS & MSD:

G

G

G

G

Client ID

LFB MS 8340MW-1B 8340MW-2 8340MW-3 TB011002 MW-25 MW-20 MW-20D FB011002 NJTA_6S_INF NJTA_6S_A/S_EFF NJTA_6S_BTWN_GAC NJTA_6S_EFF NJTA_6N_EFF TRIP_BLANK MW-1 TRIP_BLANK FIELD_BLANK TCLPMB SOILDRUM MW8 MW9 MWIO MW14 MW15 FIELD_BLANK TCLPMS MS MSD

Lab Sample ID

LFB 0090-002MS 0090-002 0090-003 0090-004 0248-001 0248-002 0248-003 0248-004 0248-005 0252-001 0252-002 0252-003 0252-004 0252-005 0252-006 0257-001 0257-002 0257-003 METHOD-BLK 0258-001 0265-001 0265-002 0265-003 0265-004 0265-005 0265-006 TCLPMS 0252-003MS 0252-003MSD

Date Analyzed

01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/15/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002 01/16/2002

Time Analyzed

15:43 16:10 17:30' 17:57 18:24 18:50 19:16 19:43 20:09 20:35 21:01 21:28 21:54 22:20 22:47 23:13 23:39 0:32 0:58 1:25 1:51 2:17 2:43 3:10 3:36 4:02 4:29 4:55 5:22 5:48

Page lo f2 FORM 4

VOLATILE METHOD BLANK SUMMARY

Lab File ID: K8976.D




THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS & MSD:

'

; 1 (

-!

Client ID

MSD NJTA 6S INF MW8

Lab Sample ID

0090-002MSD 0252-001 0265-001

Date Analyzed

01/16/2002 01/16/2002 01/16/2002

Time Analyzed

8:45 9:39 10:55 •

0

G

G

Page 2 of 2 FORM 4



Client/Project: NA

I l j

—

- j

r-

Lab ID: METHOD-BLK Client ID: METHOD-BLK Date Received: NA Date Analyzed: 01/15/2002 Data file: K8976.D

Compound Vinyl Chloride 1,1-Dichloroethene 2-BuTanone(MEK) Chloroform Carbon Tetrachloride ) 1,2-Dichloroethane(EDC) Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene

1


GC/MS Column: DB-624 Sample wt/vol: 5mL Matrix-Units: Aqueous-mg/L (ppm) Dilution Factor: 1 % Moismre: 100

Q MDL 0.00019 0.00044 0.0003 0.00016 0.00028 0.00009 0.00013 0.00019 0.00022 0.00016 0.00014

Total Target Compounds:

n



Client/Project: NA

G Lab ID: METHOD-BLK Client ID: TCLPMB Date Received: NA Date Analyzed: 01/16/2002 Data file: K8999.D

Compound Vinyl Chloride 1,1-Dichloroethene 2-Butanone(MEK) Chloroform Carbon Tetrachloride 1,2-Dichloroethane(EDC) Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene


Q

GC/MS Column: DB-624 Sample wt/vol: O.lmL Matrix-Units: Aqueous-mg/L (ppm) Dilution Factor: 50 % Moismre: 100

MDL

0.0095 0.022 0.015 0.008 0.014 0.0045 0.0065 0.0095 0.011 0.008 0.007

Total Target Compounds:

Method Title Last Update Response via

Response Factor Report MSD_K

C:\HPCHEM\1\METHODS\KA011502.M (RTE Integrator) VOLATILE ORGANICS BY EPA METHOD 624 Tue Jan 15 14:59:48 2002 Initial Calibration

Calibration Files 20 =K8969.D =K8970.D 100 =K8971.D

---

: :

G

"~T

"T

r-T

J

^

__

r

[ —

— •

Zi ::

1 2 3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 25 26 27 28 29 30

31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49

) I ) T ) P ) C ) T ) T ) T ) T r MC ) T ) T > T ) T > T T T T

) P T T

) T ) T ) T ) c ) T ) T ) T ) T > s

) I ) M ) M > c T T T T T T

) S ) MC ) T ) T ) T ) T ) T ) T ) T

Compound

Pentafluorobenzene Dichlorodifluorometha Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethan Acrolein 1,1-Dichloroethene Acetone Carbon Disulfide Vinyl Acetate Methylene Chloride Acrylonitrile t-Butyl Alcohol(TBA) trans-l,2-Dichloroeth Methyl-t-Butyl Ether( 1,1-Dichloroethane Diisopropyl Ether(DIP cis-1,2-Dichloroethen 2,2-Dichloropropane 2-Butanone(MEK) Bromochloromethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,1-Dichloropropene 1,2-Dichloroethane(ED l,2-Dichloroethane-d4

1,4-Difluorobenzene Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane 1,4-Dioxane Bromodichloromethane 2-Chloroethylvinyl Et cis-1,3-Dichloroprope 4-Methyl-2-pentanone( Toluene-dS Toluene trans-1,3-Dichloropro 1,1,2-Trichloroethane Tetrachloroethene 1,3-Dichloropropane 2-Hexanone Dibromochloromethane 1,2-Dibromoethane(EDB

20 •

0 1 1 0 0 0 0 0 0 3 2 0 0 0 0 2 1 2 0 0 0 0 1 0 0 1 1 0

1 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0

554 169 075 683 .646 .807 .042 .529 .228 .128 .668 .842 .259 084 901 502 747 805 917 976 316 291 301 .976 .739 .083 .090 .919

.421

.332

.391 194 003 457 .211 611 284 .193 .871 .547 .251 .260 .566 .206 .249 .264

5

0 1 1 0 0 0 0 0 0 2 2 0 0 0 0 2 1 2 0 0 0 0 1 0 0 1 1 0

1 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0

603 269 147 772 761 918 042 660 269 409 780 949 264 092 898 551 729 830 908 996 400 292 319 968 697 075 108 951

417 332 389 192 003 445 219 594 294 193 871 533 258 255 568 213 234 270

100

0 1 1 0 0 0 0 0 0 2 2 0 0 0 0 2 1 2 0 0 0 0 1 0 0 1 1 0

1 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0

T CTTl XolLJ

726 227 015 568 688 995 042 571 233 992 676 878 259 087 836 515 722 819 887 910 333 313 413 997 782 160 216 921

T QTTl

.564

.362

.430 217 003 508 258 693 314 240 995 642 288 .286 661 .228 .303 .317

Avg

0 1 1 0 0 0 0 0 0 2 2 0 0 0 0 2 1 2 0 0 0 0 1 0 0 1 1 0

- 1 0 0 0

" 0 0 0 0 0 1 0 0 0 0 0 0 0 0

628 222 079 674 698 907 042 587 243 843 708 890 261 087 878 523 732 818 904 960 350 299 344 980 739 106 138 930

467 .342 403 201 003 470 229 632 297 209 913 .574 .265 .267 .599 .216 .262 .284

%RSD

14 4 6

15 8

. 10 0

11 9

13 2 6 1 4 4 1 0 0 1 4 12 4 4 1 5 4 6 1

5 5 5 6 7 7

10 8 5 2 7

10 7 6 9 5

13 10

13 10 13 17 38 38 92 37 24 43 31 12 07 57 16 00 75 45 72 70 76 23 47 52 76 27 01 90

72 12 74 88 57 10 82 37 24 24 83 .31 .41 .23 .10 .01 .84 •ll' l / ". -:

--• 50 " 51 ,-, 52 G' 53

54 55 56

... 57 58

- 59 60 61

.. 62 63

T. 64 65

~ 66 -i -67

68 -. 69

70 -' 71

72 ! 73 ^ 74

75 -^ 76 ; 77 " 78 -r 79 : 80 -' 81

82 ' I 83

I MP T C T T T P

) T ) s ) P ) T ) T ) T T T T T T T T T T T T T T T

) T ) T ) T ) T ) T ) T

Chlorobenzene-d5 Chlorobenzene 0 1,1,1,2-Tetrachloroet 0 Ethylbenzene 1 m,p-Xylene 0 o-Xylene 0 Styrene 1 Bromoform 0 Isopropylbenzene 1 Bromofluorobenzene 0 1,1,2,2-Tetrachloroet 0 Bromobenzene 0 1,2,3-Trichloropropan 0 n-Propylbenzene 2 2-Chlorotoluene 1 1,3,5-Trimethylbenzen 1 4-Chlorotoluene 1 tert-Butylbenzene 0 1,2,4-Trimethylbenzen 1 sec-Butylbenzene 1 1,3-Dichlorobenzene 0 4-Isopropyltoluene 1 1,4-Dichlorobenzene 0 n-Butylbenzene 1 1,2-Dichlorobenzene 0 1,2-Dibromo-3-chlorop 0 1,2,4-Trichlorobenzen 0 Hexachlorobutadiene 0 Naphthalene 0 1,2,3-Trichlorobenzen 0 1,l,2-Trichloro-l,2,2 0 Methyl Acetate 0 Cyclohexane 0 Methyl Cyclohexane 0

930 282 815 679 679 186 151 590 633 410 353 376 129 314 363 539 938 423 570 628 089 644 254 586 054 259 098 522 162 282 239 582 464

0.934 0.266 1.797 0.665 0.656 1.152 0.143 1.576 0.631 0.412 0.352 0.396

093 304 345 502

0.937 1.405 1.551 0.626 1.082 0.649 1.223 0.586 0.064 0.350 0.115 0.799 0.263 0.214 0.247 0.495 0.413

ISTD-1.035 0.324 1.968 0.722 0.736 1.288 0.182 1.714 0.620 0.447 0.391 0.412

214 411 475 661 012 533 646 694 181 710 306 653

0.064 0.302 0.104 0.649 0.191 0.216 0.240 0.531 0.435

0 0 1 0 0 1 0 1 0 0 0 0 2 1 1 1 0 1 1 0 1 0 1 0 0 0 0 0 0 0 0 0 0

967 291 860 689 690 209 158 627 628 423 366 395 145 343 394 567 962 454 589 649 117 668 261 609 061 304 106 .657 .205 .237 .242 .536 .438

6 10 5 4 5 5

12 4 1 4 6 4 2 4 5 5 4 4

• 3

5 4 5 3 6 9

15 7

21 25 16 1 8 5

14 33 04 36 97 87 98 69 06 90 02 49 89 42 06 31 42 76 19 98 95 48 34 40 51 12 76 13 39 22 84 12 81

(#) Out of Range

KA011502.M Tue Jan 15 14:59:55 2002 MSD K

VOLATILE SURROGATE PERCENT RECOVERY SUMMARY

c G

G

C

Date Analyzed:

Lab Sample ID METHOD-BLK LFB

0090-002MS 0090-002 0090-003 0090-004 0248-001 0248-002 0248-003 0248-004 0248-005 0252-001 0252-002 0252-003 0252-004 0252-005 0252-006 0257-001 0257-002 0257-003 METHOD-BLK 0258-001

01/15/2002

Matrix

AQUEOUS AQUEOUS

AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS

SMCl = l,2-Dichloroethane-d4 SMC2 = Toluene-d8 SMC3 = Bromofluorobenzene

FUelD K8976.D K8977.D

K8978.D K8981.D K8982.D K8983.D K8984.D K8985.D K8986.D K8987.D K8988.D K8989.D K8990.D K8991.D K8992.D K8993.D K8994.D K8995.D K8997.D K8998.D K8999.D K9000.D

Concentration

30 ppb 30 ppb 30 ppb

SMCI

89 90

89 91 92 93 94 95 95 96 97 98 99 99 101 100 101 101 101 100 102 102

# SMC2

95 94

94 95 95 95 95 95 97 96 97 98 97 97 97 98 98 98 98 98 98 98

Aqueous

69-140 86-113 82-112

# SMC3 # 97 97

96 96 96 97 97 96 97 97 98 98 97 98 98 98 98 100 98 98 98 98

# Column to be used to flag recovery values

Page 1 of 2 FORM 2

VOLATILE SURROGATE PERCENT RECOVERY SUMMARY

—

""'

„ j

—.

- ?

:

L j

Date Analyzed:

Lab Sample ID

0265-001 0265-002 0265-003 0265-004 0265-005 0265-006 TCLPMS 0252-003MS 0252-003MSD 0090-002MSD 0252-001 0265-001

01/15/2002

Matrix AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS AQUEOUS

File ID K9001.D K9002.D K9003.D K9004.D K9005.D K9006.D K9007.D K9008.D K9009.D K9011.D K9013.D K9016.D

SMCl # 103 102 102 103 102 102 101 101 101 99 102 104

SMC2 97 98 98 97 97 98 98 98 98 97 98 97

# SMC3 # 99 99 97 100 .98 99 100 100 100 99 99 99

G r'

SMCl = l,2-Dichloroethane-d4 SMC2 = Toluene-d8 SMC3 = Bromofluorobenzene

Concentration

30 ppb 30 ppb 30 ppb

Aqueo

69-140 86-113 82-112

# Column to be used to flag recovery values

Page 2 of 2 FORM 2

AQUEOUS VOLATILE MATRIX SPIKE/SPIKE DUPLICATE RECOVERY

Matrix spike Lab sample ID: 0090-002

Batch No. QVK0009

G

G

G

G

G

G

Compound

1, l-Dichloroethene Benzene Trichloroethene

Toluene

Chlorobenzene

SPIKE ADDED

(ug/L)

20.0 20.0

20.0

20.0 20.0

SAMPLE CONG.

(ug/L)

0.0 0.0 0.0

0.5

0.0

MS

CONC.

(ug/L)

17.6 18.2 19.2

17.7

19.8

MS

%

REC #

88 91

96

86 99

QC

LIMITS

REC.

70 - 145 84 - '118 82 - 128

79 - 118

83 - 121

Compound

1,1 -Dichloroethene Benzene

Trichloroethene Toluene

Chlorobenzene

SAMPLE

CONC. (ug/L)

0.0 0.0

0.0 0.5

0.0

MSD

CONC. (ug/L)

19.1 17.8

18.6 16.8

18.8

MSD

%

# REC

96 89

93 82

94

%

RPD #

9 2

3 5

5

QC LIMITS RPD

12 6

8 7

6

70 84

82 79

83

REC.

- 145 - 118

- 128 - 118

- 121

# Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits

NC Non calculable

RPD: 0 out of 5 outside limits

Spike Recovery: 0 out of 10 outside limits


MS/MSD SPIKE REPORT

r

G

C

G

G

G

Lab ID: 0090-002 Client ID: 8340MW-1B Date Received: 01/04/2002 Date Analyzed: 01/15/2002 Data file: K8981.D

GC/MS Column: DB-624 Sample wt/vol: 5mL Matrix-Units: Aqueous-/ig/L (ppb) Dilution Factor: 1 % Moisture: 100

Compound Chloromethane Vmyl Chloride Bromomethane Chloroethane Trichlorofluoromethane Acrolein 1, l-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroform 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane(EDC)

Benzene Trichloroethene 1,2-Dichloropropane Bromodichloromethane 2-Chloroethylvinyl Ether cis-1,3 -Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene total-Xylenes Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene

Cone. Add 20.0 20.0 20.0 20.0 20.0 200 20.0 20.0 200 20.0 20.0 20.0 20.0 20.0 20.0

20.0 20.0 20.0 20.0 20.0 20.0

, 20.0 20.0 20.0 20.0 20.0 20.0 20.0 60.0 20.0 20.0 20.0 20.0 20.0

Sample 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0

Cone. MS 15.2 15.9 15.1 15.3 16.1

130.0 17.6 15.2 167.5 15.9 15.5 18.6 18.5 17.9 17.3 18.2 19.2 17.9 18.3 18.3 18.5 17.7 19.1 19.2 18.5 19.8 19.8 18.7 56.7 21.0 20.5 20.3 20.4 20.0

%Rec. MS 76 79 75 77 80 65 88 76 84 79 78 93 93 90 86

91 96 90 91 92 93 86 96 96 92 99 99 94 95 105 103 101 102 100

Sample 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0. 0.0 0.0 0.0_ 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0

Cone. MSD 18.3 15.5 15.1 15.1 15.0

113.0 19.1 15.7 163.0 16.2 15.0 18.3 16.7 15.6 18.4

17.8 18.6 17.5 17.6 17.0 16.5 16.8 17.0 17.9 16.0 17.6 18.8 16.6 48.8 17.2 18.0 16.9 16.9 16.6

%Rec MSD

91 77 75 75 75 57 96 78 81 81 75 91 83 78 92

89 93 88 88 85 82 84 85 89 80 88 94 83 81 86 90 84 85 83

AQUEOUS VOLATILE MATRIX SPIKE/SPIKE DUPLICATE RECOVERY

Matrix spike Lab sample ID: 0252-003

Batch No. QVKOOIO

G

Compound

1, l-Dichloroethene Benzene Trichloroethene

Toluene Chlorobenzene

SPIKE

ADDED

(ug/L)

20.0 20.0 20.0 20.0

20.0

SAMPLE

CONC. (ug/L)

0.0 0.0

0.0 0.0

0.0

MS

CONC.

(ug/L)

19.0 19.0

194 18.1 19.6

MS

% REC #

95 95 97 91

98

QC

LIMITS ,

REC.

70 - 145 84 -• 118

82 - 128 79 - 118

83 - 121

G

G

G

Compound

1, l-Dichloroethene Benzene

Trichloroethene Toluene

Chlorobenzene

SAMPLE

CONC. (ug/L)

0.0 0.0

0.0 0.0

0.0

MSD

CONC. (ug/L)

19.7 18.5

19.2 ' 17.6

19.3

MSD

% # REC

99 93

96 88

97

% RPD #

4 2

1 3

1

QC LIMITS RPD

12 6

8 7

6

70 84

82 79

83

REC.

- 145 - 118

- 128 - 118

- 121

# Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits

NC Non calculable

RPD: 0 out of 5 outside limits

Spike Recovery: 0 out of 10 outside limits


MS/MSD SPIKE REPORT

Lab ID: 0252-003 Client ID: NJTA_6S_BTWN_GAC Date Received: 01/11/2002 Date Analyzed: 01/15/2002 Data file: K8991.D

GC/MS Column: DB-624 Sample wt/vol: 5mL Matrix-Units: Aqueous-jug/L (ppb) Dilution Factor: 1 % Moisture: 100

G

G

Compound Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane Acroleiii 1, l-Dichloroethene Methylene Chloride Acrylonitrile trans-1,2-Dichloroethene 1,1-Dichloroethane Chloroforiu 1,1,1-Trichloroethane Carbon Tetrachloride 1,2-Dichloroethane(EDC)

Benzene Trichloroethene 1,2'-Dichloropropane Bromodichloromethane 2-Chloroethylvinyl Ether cis-1,3-Dichloropropene Toluene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Tetrachloroethene Dibromochloromethane Chlorobenzene Ethylbenzene total-Xylenes Bromoform 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene

Cone. Add 20.0 20.0 20.0 20.0 20.0 200 20.0 20.0 200 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 60.0 20.0 20.0 20.0 20.0 20.0

Sample 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0

Cone. MS 15.4 17.6 15.6 16.0 18.1 126.0 19.0 16.4 168.5 15.5 15.6 19.5 20.1 19.1 19.4 19.0 19.4 19.1 18.8 17.8 18.1 18.1 18.5 19.3 17.9 18.4 19.6 19.4 56.0 17.8 19.4 19.3 19.1 18.7

%Rec. MS 77 88 78 80 90 63 95 82 84 77 78 98 100 95 97

95 97 95 94 89 90 90 93 97 90 92 98 97 93 89 97 96 96 93

Sample 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0

0.0 0.0 0.0 0.0 0.0 0.0 0.0. 0.0 0.0 0.0 _ 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0

Cone. MSD 15.2 16.4 15.4 15.0 18.0

118.0 19.7 15.8

165.4 15.5 15.2 19.3 19.7 18.8 19.1 18.5 19.2 18.8 18.5 17.6 17.6 17.6 18.2 18.9 17.4 18.4 19.3 18.9 54.8 18.0 19.6 19.1 19.1 18.5

%Rec MSD

76 82

• 77 75 90 59 99 79 83 77, 76 96 99 94 95 92 96 94 93 88 88 88 91 95 87 92 96 95 91 90 98 96 95 93

VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY

F Lab File ID (Standard): K8969.D




G

C

01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22

30UG/L

24 HOUR STD UPPER LIMIT LOWER LIMIT

LAB SAMPLE ID

5-PPB-STD 100-PPB-STD METHOD-BLK LFB 0090-002MS 0090-002 0090-003 0090-004 0248-001 0248-002 0248-003 0248-004 0248-005 0252-001 0252-002 0252-003 0252-004 0252-005 0252-006 0257-001 0257-002 0257-003

IS1 AREA #

502751 1005502

251375.5

488014 511341 644523 653441 651295 638289 627542 620567 602944 597456 584540 569797 557667 547788 546519 547847 531850 529709 524699 520376 532219 527039

RT # 6.18 6.68 5.68

6.17 6.18 6.17 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.18 6.17 6.18 6.18

IS2 AREA # 1163978 2327956

581989

1162607 1199274 1500396 1516139 1510206 1483519 1468284 1463715 1424088 1409707 1371328 1356634 1339390 1306220 1311998 1305119 1292284 1267972 1252251 1249761 1282040 1268130

RT # 6.99 7.49 6.49

7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00 7.00

IS3 AREA # 1093333 2186666 546666.5

1090341 1187052 1394984 1371916 1369850 1349540 1332641 1321659 1289325 1279230 1250719 1234686 1212316 1192603 1206457 1191032 1182719 1156069 1160916 1157775 1170498 1158977

RT # 10.33 10.83 9.83

10.33 10.33 10.33 10.33 10.33 10.34 10.34 10.34 10.34 10.34 10.33 10.33 10.33 10.33 10.34 10.34 10.33 10.33 10.34 10.33 10.33 10.33

151 = PENTAFLUOROBENZENE 152 =1,4-DIFLUOROBENZENE

153 = CHL0R0BENZENE-D5

AREA UPPER LIMIT = +100% of internal standard area

AREA LOWER LIMIT = -50% of internal standard area

RT UPPER LIMIT = +0.50 minutes of internal standard RT

RT LOWER LIMIT = -0.50 minutes of internal standard RT

# Column used to flag values outside QC limits with an asterisk

* Values outside of QC limits.

Page lo f2 FORM 8

VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY

Lab File ID (Standard): K8969.D


Date Analyzed: 01 /15/2002

ime Analyzed: 10:06

G

C

G

G

23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44

30UG/L

24 HOUR STD UPPER LIMIT LOWER LIMIT

LAB SAMPLE ID

METHOD-BLK 0258-001 0265-001 0265-002 0265-003 0265-004 0265-005 0265-006 TCLPMS 0252-003MS 0252-003MSD 0090-002MSD 0252-001 0265-001

ISI AREA ,#

502751 1005502

251375.5

518746 510638 503181 508558 518538 508897 515154 518815 523088 524533 524440 542745 514123 492162

RT # 6.18 6.68 5.68

6.18 6.18 6.18 6.18 6.18 6.18 6.17 6.18 6.17 6.18 6.18 6.17 6.17 6.18

IS2 AREA # 1163978 2327956

581989

1244248 1229686 1245658 1227449 1241488 1237126 1244348 1243949 1243142 1238824 1244436 1295671 1218679 1173705

RT # 6.99 7.49 6.49

7.00 7.00 6.99 7.00 7.00 7.00 7.00 7.00 7.00 7.00 6.99 6.99 7.00 7.00

iS3 AREA # 1093333 2186666 546666.5

1137348 1133484 1133438 1136116 1146585 1126495 1131871 1139053 1131660 1140669 1144583 1178875 1111171 1067709

RT # 10.33 10.83 9.83

10.33 10.33 10.34 10.33 10.33 10.33 10.33 10.33 10.33 10.33 10.33 10.33 10.33 10.33

151 = PENTAFLUOROBENZENE 152 =1,4-DIFLU0R0BENZENE

153 = CHLOROBENZENE-D5

AREA UPPER LIMIT = +100% of internal standard area

AREA LOWER LIMIT = -50% of internal standard area

RT UPPER LIMIT = +0.50 minutes of internal standard RT

RT LOWER LIMIT = -0.50 minutes of internal standard RT

# Column used to flag values outside QC limits with an asterisk

* Values outside of QC limits.

Page 2 of 2 FORM 8

Quantitation Report (QT Reviewed)

G

G

G

Data File : C : \ H P C H E M \ 1 \ D A T A \ 0 1 - 1 5 - 0 2 \ K 9 0 0 0 . D

Acq On : 16 Jan 2002 1:51 Sample : SOIL_DRUM,0258-001,A,0.ImL,100 Misc • : GES/FLEET_BANK_-_WALL,01/11/02,01/11/02 MS Integration Params: LSCINT.P Quant Time: Jan 16 9:49 2002

Vial Operator Inst Multiplr

28

K MSD 1.00

Quant Results File: KA011502.RES

Quant Method Title Last Update Response via DataAcq Meth

C:\HPCHEM\1\METHODS\KA011502.M (RTE Integrator) VOLATILE- ORGANICS BY EPA METHOD 624 Tue Jan 15 14:59:48 2002 Initial Calibration KA011502

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Pentafluorobenzene • 31) 1, 4-Dif luoroberizene 50) Chlorobenzene-d5

6 7

10,

18 00 33

168 114 117

510638 1229686 11334-84

30 30 30

00 00 00

UG UG UG

0.00 0.00 0.00

G

System Monitoring Compounds 30) 1,2-Dichloroethane-d4 6.50 Spiked Amount 30.000 Range 80

41) Toluene-d8 8.67 Spiked Amount 3 0.0 00 Range 8 0

59) Bromofluorobenzene 11.74 Spiked Amount 3 0.0 00 Range 8 0

Target Compounds

65 484612 30.60 UG 0.00 120 Recovery = 102.00% 98 1451368 29.29 UG 0.00 120 Recovery = 97.63% 95 698086 29.42 UG 0.00 120 Recovery = 98.07%

Qvalue

U (#) = qualifier out of K9000.D KA011502.M

range Wed

(m) Jan

= manual 16 10:05

integration 23 2002 MSD K Page 1

Quantitation Report

Data File : C:\HPCHEM\l\DATA\01-15-02\K9000.D Vial Acq On : 16 Jan 2002 1:51 Operator Sample : SOIL_DRUM,0258-001,A,0.ImL,100 Inst Misc : GES/FLEET_BANK_-_WALL,01/11/02,01/11/02 Multiplr MS Integration Params: LSCINT.P Quant Time: Jan 16 9:49 2002

28

K_MSD 1.00




Abundance

2300000

2200000

2100000

2000000

1900000

1800000

1700000

1600000

1500000

1400000

1300000

1200000

1100000

1000000

900000

800000

700000

600000

500000

400000

300000

200000

100000

n u -

rime->

•

L. 2.66'' 3.66' ' 4.66' '5.66

0) c 0)

2 0

E Q

4

Ico s §

1 1

-- '6.66' 7. DO

TIC: K9000.D

0)

c

c

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1

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c 0)

x> 2

i a

3

2 5 5 5

V

r

's.bo' 9.bo' Vo!o'o' Vi!o'o' 'i'2!o'o' Vslob' 'i4!ob" Vslob' Velob' 'iV.'ob' Vslob*

K9000.D KA011502.M Wed Jan 16 10:05:23 2002 MSD K Page 2

G

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Quantitation Report

Data File : C:\HPCHEM\l\DATA\01-15-02\K8999.D Acq On : 16 Jan 2002 1:25 Sample : TCLPMB,METHOD-BLK,A,0.ImL,100 Misc : NA,NA,NA MS Integration Params: LSCINT.P Quant Time: Jan 16 9:49 2002

(QT Reviewed)

Vial: 27 Operator Inst Multiplr

K MSD 1.0 0



C:\HPCHEM\1\METHODS\KA011502.M (RTE Integrator) VOLATILE ORGANICS BY EPA METHOD 624 Tue Jan 15 14:59:48 2002 Initial Calibration KA011502


G

C

1) Pentafluorobenzene 31) 1,4-Difluorobenzene 50) Chlorobenzene-d5

System Monitoring Compounds 30) 1,2-Dichloroethane-d4 Spiked Amount 30.000

41) Toluene-d8 Spiked Amount 30.000 59) Bromofluorobenzene Spiked Amount 30.000

Target Compounds

6 7

10

6 Range

8 Range

11 Range

18 00 .33

50 80 .66 80 74 80

168 114 117

65 - 120

98 - 120

95 - 120

518746 1244248 1137348

491283 Recove

1473815 Recove

700005 Recove

30 30 30

30 ry

29 ry

29 ry

00 00 00

54 = 40 = 40 =

UG UG UG

UG 101 UG 98

UG 98

80%

00%

00%

0 0 0

0

0

0

00 00 00

00

00

00

Qvalue

(#) = qualifier out of range (m) = manual integration K8999.D KA011502.M Wed Jan 16 10:05:21 2002 MSD K Page 1

Quantitation Report

Data File : C:\HPCHEM\1\DATA\01-15-02\K8999.D Acq On : 16 Jan 2002 1:25 Sample : TCLPMB,METHOD-BLK,A,0.ImL,10 0 Misc : NA,NA,NA MS Integration Params: LSCINT.P Quant Time: Jan 16 9:49 2 0 02


27

K MSD 1.00


Method Title Last Update Response vij.


Abundance

2400000

2300000

2200000

2100000

1

2000000

1900000

1800000

1700000

1600000

1500000

1400000

1300000

1200000

1100000

1000000

900000

800000

700000

600000

500000

400000

300000

200000

100000

r\ U

rime-> 2.66' ' 3.66" • 4.

3 4.

_.

N C Q) £1 S CO I t B i (U (D

CL £ 0)

-.

9

1 1 1 1 1 1 1 i > - T ^ T r- 1 •

30 5.00 6.00 7. 6'

TIC: K8999.D

g CD

2

c C

^

• -

•

* A

a s. £ c

\ 1 3 C

I \

'

... 1

D 1 3

\ 5

CO to c 0)

o c c E 1 Q

! 3

5

i

8.60 9.60 10.00 11.00 12.00 13.00 14.00 15.00

\

-

"

'

'Veloo' 'i'7lo6' 'I's.'ob''"


c

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Quantitation Report

Data File : C:\HPCHEM\l\DATA\01-15-02\K8976.D Acq On : 15 Jan 2002 15:17 Sample : METHOD-BLK,METHOD-BLK,A,5mL,100 Misc : NA,NA,NA . MS Integration Params: LSCINT.P Quant Time: Jan 15 15:37 2002

(QT Reviewed)


4

K 1.

MSD '00



C:\HPCHEM\1\METHODS\KA011502.M (RTE Integrator) VOLATILE ORGANICS BY EPA METHOD 624 Tue Jan 15 14:59:48 2002 Initial Calibration KA011502


G

C

1) Pentafluorobenzene 31) 1,4-Difluorobenzene 50) Chlorobenzene-d5

System Monitoring Compounds 30) l,2-Dichloroethane-d4 Spiked Amount 3 0.000

41) Toluene-d8 Spiked Amount 30.000 59) Bromofluorobenzene Spiked Amount 3 0.000

Target Compounds

30 30 30

00 00 00

UG UG UG

0 0 0

00 00 00

6.17 168 644523 7.00 114 1500396 10.33 117 1394984

6.49 65 533387 26.69 UG . 0.00 Range 80 - 120 Recovery = 88.97%

8.66 98 1719330 28.44 UG 0.00 Range 80 - 120 Recovery = 94.80%

11.74 95 850225 29.12 UG 0.00 Range 80 - 120 Recovery = 97.07%

Qvalue

(#) = qualifier out of range (m) = manual integration K8976.D KA011502".M Wed Jan 16 10:04:17 2002 MSD K Page 1

Quantitation Report

Data File : C:\HPCHEM\l\DATA\01-15-02\K8976.D Acq On : 15 Jan 2002 15:17 Sample : METHOD-BLK,METHOD-BLK,A,5mL,100 Misc : NA,NA,NA MS Integration Params: LSCINT.P Quant Time: Jan 15 15:37 2002


4

K MSD 1.00

Quant Results File: KA011502.REE



TIC: K8976.D Abundance

2700000

2600000

2500000

2400000

2300000

2200000

2100000

2000000

1900000

1800000

1700000

1600000

1500000

1400000

1300000

1200000

1100000

1000000

900000

800000

700000

600000

500000

400000

300000

200000

100000

0

a

01 Z

a. c

« e o b

rime-> 2.66' 3.66' ' 4.66' ' 5.66'' eio' 7.66'' 8.66' 6.66' 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00


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Integrated Analytical Labs Certified for NJDEP, NY(DOH) 273 Franklin Road NJ ID#14751 Randolph, NJ 07869 NYID#11402 1/17/02

General Chemistry Quality Control

Matrix: Soil Batch ID: AP044-0002 Units: S-mg/Kg

Blank

_ _ _Paramete_r _ _ JMetho^ B]ank_ JWDL _ _ A]ialYsis_Dat^ _

Reactive Sulfide ND 16;0 01/17/2002

Duplicate Recovery

Duplicate RPD _ _ ârameter_ _ _Qp_§aQlPle_ _Result_ _ Result _ _RPp _ JLirnits_

Reactive Sulfide 0074-001 ND ND NC NC

Spike Recovery

Spike %Spike %Rec. _ _ ârameter_ _ _QC_Sarnple_ _Result_ _Sp[ke_Added_ êsi i l t _ Recoêry_ _Limits _

Reactive Sulfide NA NA NA NA NA 75-125

The above blank result applies to the follow samples E02-f

0074-001 0229-001 0074-001D 0258-001 0126-004 ' 0342-001 0176-001 0348-001 0188-001 0330-001 0220-009 0331-001

+• = No Flash - Sample boiled at 100C NA = Not Applicable ND = Not Detected NC = Non calculable RPD due to value less than the detection limit No = Does Not Ignite Yes = Sample Ignites

©2000 lAL Inc. All rights reserved

Integrated Analytical Labs 273 Franklin Road Randolph, NJ 07869 1/17/02

Matrix: Units:

Certified for NJDEP, NY(DOH) NJID#14751 NYID#11402

Soil S-mg/Kg


Batch ID: AP045-0002

Blank

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_ Z^'iL"]?!^.'' Method Bjank MDL. _ _ Analysisâte^

Reactive Cyanide ND 10X1 01/17/2002

Duplicate Recovery

Duplicate RPD _ ârameter_ _ _QC_Sarnple_ _ _ _ _ _Result_ _ ^ e s j i l t _ _RPp _ _Liniits_

Reactive Cyanide 0074-001 ND ND NC NC

Spike Recovery

Spike %Spike %Rec. _ .Parameter_ QC_Sample_ _Result_ _Sp[ke_Added_ êsj i i t _ Rjcoêry_ _Lirnits _

Reactive Cyanide NA NA NA NA NA 75 -125

The above blank result applies to the follow samples E02-

0074-001 0229-001

0074-001D 0258-001 0126-004 0342-001 0176-001 0348-001 0188-001 0330-001 0220-009 0331-001

•n- = No Flash - Sample boiled at 100C NA = Not Applicable ND = Not Detected NC = Non calculable RPD due to value less than the detection limit No = Does Not Ignite Yes = Sample Ignites


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Integrated Analytical Labs Certified for NJDEP, NY(DOH) 273 Franklin Road NJ ID#14751 Randolph, NJ 07869 NY ID#11402 1/15/02


Matrix: Soil Batch ID: AP043-0010 Units: S-Yes/No

Blank

_ _ _Parameter_ _ _Metho^ Bjank_ JVIDL _ _ ArialYsis_Dat£^ _

IGNITABILITY NA NA 01/15/02

Duplicate Recovery

Duplicate RPD

£a''in]?t®J' ?P_§?!]1PJ® .f ®®".'* JResjult _ _RPp _ .Liniits _

IGNITABILITY 0229-001 NO NO NC NC

Spike Recovery

Spike %Spike %Rec. _ _ parameter _9?_§?!I!PJi- —'^^^"'L _Sp[ke_Added_ JRes^lt _ Recovery_ _LinTits _

IGNITABILITY NA NA NA NA NA 75 - 125


0229-001 0285-001 0229-001D 0278-001 0258-001

++ = No Flash - Sample boiled at 100C NA = Not Applicable ND = Not Detected NC = Non calculable RPD due to value less than the detection limit No = Does Not Ignite ©2000 IAL Inc. Yes = Sample Ignites " All rights reserved

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Integrated Analytical Labs Certified for NJDEP, NY(DOH) 273 Franklin Road NJ ID#14751 Randolph, NJ 07869 NY1D#11402 1/15/02


Matrix: Soil Batch ID: AP023-0009 Units: SU

Blank

_ _Pararnetej;_ Method_Blajik _ MpL_ _ _Ana[y^sjs Date_

ey NA NA 01/15/02

Duplicate Recovery

Duplicate RPD

Paran}?*.®!.. _ . _ 9.2 ?in}PL®. Result ?®?uil RPD .mn'ts

^H 0229-001 6^85 6^90 1 20

Spike Recovery

Spike %Spike %Rec. _ _Pararnetej;^ _ _QCSatTigle Result _ ^pike Added _ Rûjt^ _Recovery_ Limits

eH NA NA NA NA NA 75-125


0229-001 0285-001 0229-001D 0278-001 0258-001

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++ = No Flash - Sample boiled at 100C NA = Not Applicable ND = Not Detected NC = Non calculable RPD due to value less than the detection limit No = Does Not Ignite Yes = Sample Ignites


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CHAIN OF CUSTODY

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Case No.: E02-258 P.O. #: Project : FLEET BANK - WALL Client/Project: GES/FLEET BANK - WALL Client Address: Billing Address: Groundwater & Environmental ServiQeeundwater & Environmental Services 1340 P.O. Wall

Campus Pkwy Box NJ

1750 07719

Date Received: Time Received: Report Format:

01/11/02 18:30 Reduced

# of Containers lAL ID # Client ID #

jyiatrix Sample Date Sample Time

VO, TCLP Sulfide, React. Cyanide, React. Ignite/FP pH/Corrosivity % Solids Electronic Del.

2 258-001 SOIL DRU M

Soil 01/11/02 11:00

/

y V y /

V /

1

Comments:

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1340 P.O. Wall

Campus Pkwy Box NJ

1750 07719

Verbal Due: Jan 2 8 Report Due: Feb 4

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INTEGRATED ANALYTICAL LABORATORIES, LLC

SAMPLE RECEIPT VERIFICATION

CASE NO: 0258 I CLIENT: C J>

V COOLER TEMPERATURE: 2° - 6°C:

CHAIN OF CUSTODY: COMPLETE / INCOMPLETE

( See Chain of Custody)

Comments:

Sample Bottles Intact: Sample Labels Intact/ Correct: Sufficient Sample Volume: Correct bottles/ preservative: Samples received in

holding time/ prep time: Headspace/ bubbles in voa samples: Samples to be subcontracted:

Preserved Sample pH checked: (Excluding voa samples)

ADDITIONAL COMMENTS:

-/ Comments: V V ^

V X

c^:

KEY = YES = N0

I > N / A

SAMPLE(S) VERIFIED BY: INITIAL

CORRECTIVE ACTION REQUIRED

/R^ DATE rfrrSo^

YES 1 ;SEE BELOWO NO

CLIENT NOTIFIED:

PROJECT CONTACT:

SUBCONTRACTED LAB: DATE SHIPPED:


YES I i Date/Time: NO

VERIFIED/TAKEN BY: INITIAL j t ^ DATE

REV 10/00

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Case No Client Project

Integrated Analytical Laboratories, LLC.

Laboratory Custody Chronicle

E02-2 58 Groundwater & Environmental Services FLEET BANK - WALL

GC/MS V EXTRACT ANALYSIS

VO, TCLP

Sulfide, Re 5act. Cyanide, React. Ignite/FP pH/Corrosivity % Solids

Electronic Del.

258--001

WETCHEM 258-258-258-258-258-

AIR 258-

-001 -001 -001 -001 -001

-001

S

S S S s s

s

DATE TIME INITIAL

^

- > •

^

\ la K/

DATE TIME

\ > n

INITIAL

a^ * ^

A\\\ \ ^ i/

^ i^

r;; •»•

-— ' "-

REVIEW & APPROVAL: i^ REMARKS :

f^C^h^J^

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L a b s

Integrated Analyt ical Laborator ies, LLC. 273 Franklin Road Randolph, N.J. 07869

ANALYTICAL DATA REPORT

for Groundwater & Environmental Services

1340 Campus PIcwy P.O. Box 1750 Wall,NJ 07719

Project Name: FLEET BANK - WALL Lab Case Number: EOl-8197

Phone: 973 361-4252 Fax: 973 989-5288

MDL = METHOD DETECTION LIMIT

TCLP Volatiles

Lab ID: 8197-001 Client ID: SOIL DRUM Matrix-Units: Aqueous Leachate-mg/L Percent Moisture: 100

Date Sampled: 11/20/01 Time Sampled: 11:00 Date Analyzed: 11/27/01

Lab ID: 8197-001 Client ID: SOIL DRUM Percent Moisture: 13.8

Parameter

Sulfide, Reactive Cyanide, Reactive Ignitability® 142°F Corrosivity as pH % Solids

Compound

Vinyl Chloride 1,1 -Dichloroethene 2-Biitanone(MEK) Chloroform Carbon Tetrachloride 1,2-Dichloroethane(EDC) Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene

Cone

ND ND ND ND ND ND ND ND ND ND ND

General Analytical

lUM

Q MDL

0.0465 0.051

0.0185 0.026 0.0245 0.028

0.0175 0.028

0.0225 0.034 0.019

Date Sampled: 11/20/01 Time Sampled: 11:00

lesult

ND ND NO 5.51 86.2

MDL

18.6 11.6 NA NA NA

Matrix-Units

Soil-mg/Kg Soil-mg/Kg Soil-Yes/No Soil-S.U. Soil-%

Date Analyzed

11/27/01 11/27/01 11/26/01 11/26/01 11/26/01

ill ND = Analyzed for but Not Detected at the MDL

All required protocols were followed during analyses. These data have been yeview/SJi and accepted by:

Michael'. Laboratory 1

The liability of Integrated Analytical Laboratories, LLC. is limited to the actual cost of the analyses performed.

H. LeftiH, Ph. 3 atory Director /

!l ^•Ccc„

lAL is a NELAC Certified Lab # 14751 and maintains certification in Connecticut # PH-0699, New Yoric # 11402 and Florida # E87670

I i

a

CHAIN OF CUSTODY

Case No.: EOl-8197 P.O. #: Project : FLEET BANK - WALL Client/Project: GES/FLEET BANK - WALL Client Address: Billing Address: Groundwater & Environmental ServiQceundwater & Environmental Services 1340 P.O. Wall

Camp Box NJ

)us Pkwy 1750 07719

Date Received Time Received Report Format

11/21/01 18:35 Standard

1340 P.O. Wall

Campus Pkwy " Box NJ

1750 07719

Verbal Due: Dec 10 Report Due: Dec 17

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# of Containers lAL ID # Client ID #

Matrix Sample Date Sample Time

VO, TCLP Sulfide, React. Cyanide, React. Ignite/FP pH/Corrosivity % Solids

2 8197-001 SOIL DRU M

Soil 11/20/01 11:00

/

V / / /

y 1

Comments

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G

INTEGRATED ANALYTICAL LABORATORIES, LLC

SAMPLE RECEIPT VERIFICATION

CASE NO: 8197 I CLIENT: C-ss 6°C: • COOLER TEMPERATURE: 2

CHAIN OF CUSTODY: COMPLETE / INCOMPLETE

( See Chain of Custody)

Comments:

Sample Bottles Intact:

Sample Labels Intact/ Correct:

Sufficient Sample Volume:

Correct bottles/ preservative:

Samples received in

holding time/ prep time:

Headspace/ bubbles in voa samples:

Samples to be subcontracted:

Preserved Sample pH checked:

(Excluding voa samples)


• Comments:

V V •

•

' j jas^^ 'a fS^P^

i^ KEY

y =YES ^ =N0

<:2II>N/A

SAMPLE(S) VERIFIED BY: INITIAL| fyL^

CORRECTIVE ACTION REQUIRED: YES

DATE nf^/ht

] ;SEE BELOW) NO

[ ] CLIENT NOTIFIED:

- - PROJECT CONTACT:

' - SUBCONTRACTED LAB: DATE SHIPPED:


YES I I Date/Time: NO

VERIFIED/TAKEN BY: INITIAL % - - DATE

REV 10/00

G

G

G

Case No Client Project

Integrated Analytical Laboratories, LLC.

Laboratory Custody Chronicle

EOl-8197 Groundwater & Environmental Services FLEET BANK WALL

GC/MS V EXTRACT ANALYSIS

VO, TCLP

Sulfide, React. Cyanide, React. Iqnite/FP pH/Corrosivity % Solids

8197-001

WETCHEM 8197-001 8197-001 8197-001 8197-001 8197-001

S

S S S S S

DATE TIME INITIAL

• 11 SL - q"icc; J . ^ ^ ^

• ,

DATE /'/AV/O,

11 \ L y

TIME IN 1 : ^

\QlOU

ITIAL

^^rt>

-JK^ ' 4y l l j X G 1 ^ / ? ^ i ^

Y REVIEW & APPROVAL: REMARKS :

QAcuUf/ugiuyitA

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L'lTjia

Appendix 6

Monitoring Well Certification Form B


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• FLANNERY, WEBB & HANSEN, P.A. CIVIL ENGINEERS • LAND SURVEYORS • SITE PLANNERS LANDSCAPE ARCHITECTS • ENVIRONMENTAL CONSULTANTS

1011.605 Febmary 5, 2002

Groundwater and Environmental Services, Inc. Monmouth Shores Corporate Park 1340 Campus Parkway P.O. Box 1750 Wall, New Jersey 07719

Attn: Dene O'Connor

Re:FORMER SUMMIT BANK #1322 SEA GIRT AVENUE WALL TOWNSHIP, N.J.

G.E.S. No. 03^02046-XX-XX

Dear Dene:

The following list of well casing elevations are based on a Bench Mark with an elevation of 69.0'. All elevations were taken at a black mark on the top of the well casing.

MW# 3D 7

PVC 45.85 36.35

REM 46.13 36.89

Field measurements were made on 02-04-02. An on-site Bench Mark (PK) was found with an elevation of 44,92. See attached well location for further details. Should you have any questions or require additional information, please do not hesitate to contact this office.

Sincerely,

Doc: 1011605 A

RO. BOX 456 • LAKEWOOD • NEW JERSEY • 08701 • PHONE (732) 797-3100 • FAX (732) 797-3223

Appendix 7

Photographs

"An Equal Opponunity Employer"

EXCAVATION PHOTOGRAPHS Fleet National Bank (fomierly White Swan Dry Cleaners)

1322 Sea Girt Avenue Wall Township (Monmouth County), New Jersey

North view of excavation following removal of absorption tank and septic tank.

1 » ^ 1 ^ -

1

1 « • .

- i ^ ]

Ii k • " •' 1 I--1 t '

• , t

fl -^«id

•M-y(yiy^

1

Northeast view of excavation sidewall showing alternating layers of sand and gravel.

EXCAVATION PHOTOGRAPHS Fleet National Bank (formerly White Swan Dry Cleaners)

1322 Sea Girt Avenue Wall Tovraship (Monmouth County), New Jersey

Liiua

North-northeast view of access manway to first chamber of absorption tank. Notice absence of concrete mortar between vertical joints of cinder blocks.

Northeast view of cinder block wall in first chamber of absorption tank. Notice absence of concrete mortar between vertical joints of cinder blocks.

EXCAVATION PHOTOGRAPHS Fleet National Bank (formerly White Swan Dry Cleaners)

1322 Sea Girt Avenue Wall Township (Monmouth County), New Jersey

Lnxja

West view of excavation. Cinder block separating first and second chambers of absorption tank. Dark-stained soil near surface resulting from naturally occurring

organic roots.

East view of cinder block wall separating third and fourth chambers of absoiption tank. Notice gaps between vertical joints of cinder blocks. Four-inch diameter cast iron pipe

Appendix 8

Hazardous Waste Manifests & Transportation Logs


MONITORING WELL CERTIFICATION FORM B - LOCATION CERTIFICATION

Name of Owner: F L E E T N A T I O N A L . B A N K Name of Facility: FLEET BANK BRANCH Location: #1322 SEA GIRT AVENUE, WALL TWP., NJ. Case Number(s): (UST #, ISRA #, Incident #, or EPA #)

LAND SURVEYOR'S CERTIFICATION Well Permit Number: 29-45875 (This number must be permanently affixed to the well casing.)

Owners Well Number (As shown on application or plans): MW- 3D

Longitude!, West 74°- 03'- 44.9" Latitude: North 40°- 08'- 09.4"

New Jersey State Plane Coordinates NAD 83 to nearest 10 feet:

North 474739.54 East 614451.02

Elevation of Top of Inner Casing (cap off) at RIM 46.13 r Reference mark (nearest 0.01'): PVC 45.85

Source of elevation datum (benchmark, number/description and elevation/datum. If an on-site datum is used, identify here, assume datum of 100', and give approximated actual elevation.)

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PREVIOUS DATUM

Significant observations and notes:

AUTHENTICATION

I certify under penalty of law that I have personally examined and am familiar with the infonnation submitted in this document and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe the submitted infonnation is true, accurate, and complete. I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment.

SEAL

02-05-02 PROFESSIONAL LAND SURVEYOR'S SIGNATURE DATE

William P. Scheme! - License No. 36275 ' PROFESSIONAL LAND SURVEYOR'S NAME AND LICENSE NUMBER (Please print gr type)

1658 Route 9. Toms Riven N.J. 08755 f732) 797-3100 PROFESSIONAL LAND SURVEYOR'S ADDRESS AND PHONE NUMBER

MONITORING WELL CERTIFICATION FORM B - LOCATION CERTIFICATION

" Name ofOwner: F L E E T N A T I O N A L B A N K Name of Facility: FLEET BANK BRANCH Location: #1322 SEA GIRT AVENUE, WALL TWP., NJ.

I Case Number(s): (UST #, ISRA #, Incident #, or EPA #) i


Owners Well Number (As shown on application or plans): MW- 7

Longitude: West 74°- 03'- 38.1" Latitude: North 40°- 08'- 09.4"

^ New Jersey State Plane Coordinates NAD 83 to nearest 10 feet:

I North 474745.81 East 614975.26



G PREVIOUS DATUM


AUTHENTICATION

I certify under penalty of law that I have personally exEimined and am familiar with the information submitted in this document and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe the submitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting felse information including the possibility of fine and imprisonment.

SEAL

. < ^ ^ ' ^ 02-05-02 PROFESSIONAL LAND SURVEYOR'S SIGNATURE DATE

William P. Schemel - License No. 36275 PROFESSIONAL LAND SURVEYOR'S NAME AND LICENSE NUMBER (Please print er type)

1658 Route 9. Toms Riven N.J. 08755 (732) 797-3100 PROFESSIONAL LAND SURVEYOR'S ADDRESS AND PHONE NUMBER

: MONITORING WELL CERTIFICATION FORM B-LOCATION CERTIFICATION

Name of Owner: F L E E T . N A T I O N A L . B A N K Name of Facility: FLEET BANK BRANCH Location: #1322 SEA GIRT AVENUE, WALL TWP., NJ. Case Number(s): (UST #, ISRA #, Incident #, or EPA #)


Owners Well Number (As shown on application or plans): MW- 3D

Longitude; West 74°- 03'- 44.9" Latitude: North 40°- 08'- 09.4"

~ New Jersey State Plane Coordinates NAD 83 to nearest 10 feet:

North 474739.54 East 614451.02


G G G G


PREVIOUS DATUM ^


AUTHENTICATION

I certify under penalty of law that I have personally examined and am familiar with the information submitted in this document and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe the submitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment.

SEAL

02-05-02 PROFESSIONAL LAND SURVEYOR'S SIGNATURE DATE

William P. Schemel - License No. 36275 PROFESSIONAL LAND SURVEYOR'S NAME AND LICENSE NUMBER (Pleaseprint grtype)

1658 Route 9. Toms Riven N.J. 08755 (732) 797-3100 PROFESSIONAL LAND SURVEYOR'S ADDRESS AND PHONE NUMBER

n i MONITORING WELL CERTIFICATION FORM B - LOCATION CERTIFICATION

^ Nameof-Ovmer: F L E E T N A T I O N A L BANK Name of Facility: FLEET BANK BRANCH Location: #1322 SEA GIRT AVENUE, WALL TWP., NJ.

I Case Number(s): (UST #, ISRA #, Incident #, or EPA #)

LAND SURVEYOR'S CERTIFICATION Well Permit Number: 29-46075

(This number must be permanently affixed to the well casing.)

Owners Well Number (As shown on application or plans): MW- 7

Longitude: West 74°- 03'- 38.1" Latitude: North 40°- 08'- 09.4"

^ New Jersey State Plane Coordinates NAD 83 to nearest 10 feet:

I North 474745.81 East 614975.26



PREVIOUS DATUM

G

G

Significa:nt observations and notes:

AUTHENTICATION

I certify under penalty of law that I have personally examined and am familiar with the information submitted in this document and all attachments and that, based on my inquiry of those individuals immediately responsible for obtaining the information, I believe the submitted information is true, accurate, and complete. I am aware that there are significant penalties for submitting false information including the possibility of fine Eind imprisonment.

SEAL

ytky^'.<- 02-05-02 PROFESSIONAL LAND SURVEYOR'S SIGNATURE DATE

William P. Schemel - License No. 36275 PROFESSIONAL LAND SURVEYOR'S NAME AND LICENSE NUMBER (Please print or type)

L 1658 Route 9. Toms Riven N.J. 08755 (7321 797-3100 PROFESSIONAL LAND SURVEYOR'S ADDRESS AND PHONE NUMBER

Dec':Z1-0l 03:a9pin F rora-CWM Cham i ca I Ss rv i ess ' , , . , . ^,, +7167540211

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3. Gencraioft Name and Mailing Aoaross ••• , .

FLEET BANK 30(^n\_^'i'^^j^'feri323-3ri'rtirtT ^Ksy::"--'

4. Ganeraloi^TBlephonerÊbr 0 8 7 - 3 1 0 7 p r ^ / l ^ g f o / l , j S J P * ^ B ^ ' M ^ - O l D f e ^ , 5. Transporter 1 (Company Name)

HORWITH TP.UCKS, liJC. 7, Transporter 2 (Comptsny Name)

8. -US EPA ID NutTlBer -

Pa-rA,-©,. 1 [ 4 ,'S T.T 1114,8 ,7 ,8 ' l - i - i ^ l O l . f ; !

9. Designated Fîllt/ Name and Site Address CWa CHEMICAL SERVICES. L .LGC 1550 BAUffiR ROAD hODEL CITY, NY 14107 '

> s,raj5'EPA ID Namt»er-

3:111 I '" i I .,. JO^-US EPA ID Number

J L _ L

y i , Y , . i : > i 0 i 4 i 9 i 3 , 3 . 1 . 1 5 , 6 | 7 i 9

11, U8 DOT OtsatfODn (inauotng Proper snipping Name, Hazard Cjaas and 10 Number)

-Jhh •HAZARDOUS HASTE, SOLID,; n , p - s . +-;r.

X (TSTRAGHLOROETHYLENE) (512157) 9,^307-7:; .-111 . ..-v. • .

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PACKIHG SLIPS ATTACHED FORI CLARIFICATION EMERGENCY

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16. G E N E R A T O R ' S C E R T I F I C A T I O N : i hereby dociaro ihot iho contofiis af.jnis eonfflgnttianl; ciassined. pschod. marKed and labelea, and are in aU respects In proper condition for uanspon bir'hiijhi and auue lavra and regulations. i .. . . .i tr 1 am brga quAniicy gonaralor. I ecHify that I havo a program In pfaco to raducA.uia volume.aiio.CCUtl practicable and Uial I have aelaclod the pracHcatald molhod ot traaiment. sterago, or disposal currently ; and the environment; OR il lam a smallar ganorator, I hava matJa a goad (aUh,qf{orr,to mlnlmiamny-was to ma and tfiat I can afford. ; -"- '

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Printed/Typed Name

l7.Transponer 1 AcKnovuledgemsnt OT Receipt of liitaterials

ra luay;and acsuraialy descntod abova Dy proper shipping name and are 'ay according lo epplicablo IntamAtionsU «nd national govAmmom rogulotiono

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COPY 1-DISPOSER STATE .-..MAILED BY TS.D FACILITY

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t l l lM I IpUtHfei ,: .Qv?!?^^ r~ l Tankm f ~ l T f a m t o n n w

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.,;L;.4-7le754D211/."-jC)K^T^2S7 P.003Vo27 F-939

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Ki J R "Q lO lOjQ '3 17 i& [fl-«>_ 3. Generatoi'a Name and Mailing Address - v • - . - i , - ^ -

FLEET BAWK p d . Q o Y d ^ L z KitlB :gi:A..QlnT ii>.VDilL& -.

4. GeneratorisTalBOhanatfcBrjater 9 8 7 - 3 1 0 7 O Q & 4 0 ~ ' ^ - ^ L J c 5. Transporter 1 (Company Name)

H O R W I T H T R U C K S , I N C . 7. IhuisporterZ (Company Name)

9. Designated {^cility Name and Site Addrcsa

c m CHEMICAL SERVICES, L .L.C 1550 B<^LnER ROAD nODEL CITY. NY 1^107

6. USEPA ID Numb >r '

P"iA iD | l . i ^ i 6 . . 7 . - t l - . i ^ ,B ,7",fi K- u s EPA !p Numb- *..

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a- HAZARDOUS WASTE, SOLlJi, n - o ^ s .Viaviii.., W # ^ L X £TETRACHLOROETHYLENEO < S12iS7>' 5',fciA3;0^|«, I I ^ % ; i- %

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16, (3ENERATOR>S CEHTIFtOATION; i maratiy daaaro tcial ing.camea[s,.al mis consignmi nt ore iuily ancifaixurately dascribed above by prapor shipping name and are" dosstfied, padiad, martted and labalad, and cis In aU'rosseosin Draper conaiuon tor transpoir by.ti shvsy si««aTdIns'feappUoQbis invmnailonaiand tiîanal goiammont regulations and nata lows ana raguianons. jjj - - . v .- : , • • . - . • . . ; .r.'-rr-j'i'J'" III era lot^ quantlly genaiaior. I cartify that (fiave a program in place toiraduca the volume and axicity ol waste ganeratad to the dagiae 1 have osterminsd to be economically practicable and that I have selocted the practijaibiB mbtliod of traaimaht. jsiorada.'or disposal'^mn ly avnilsibie lo me nhlch minrnrizos ihs pncsoni and luiura mraat to numan neaitn snd ma anvlTonmeni; OH It I am a emallar gehaiaior, Ihave ffladeaôodlailh aNoit to mlnlmlzomy- «aste gonsralltin and saloct the best tiasto manageinent method that Is avaaaUa to me and That I ean ottoid. "r' ' • -"• . ; ..;/•;~^....-. •.:..-.'.-• v • ! • • •

Prinled/Typod Nama..,

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XLL IT.Tranaporwr 1 flîowladgêra o( RocoiK o( Materials Prlntad/Typsd Name . . _...-—"

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1 a. Ttsnsporler 2 Aeknowlodgement of Receipt of Materials Printadnypad Name SIgnaiura Ma Day Tsar

I I T ' l 1 19. Discrepancy Indication Space rcpancy uiui«iuan opacs

X4Ur,l<~L-20, Facility Owner or Operator: Csrtilicatlon of receipt ol hazardous maierlate'coverad by iSIs ma u'feat' okcept a^ Tioted in Ham 19.

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Dec-31-01 03i01pni From-CWM Chemical Services

T r g n e p o r t e r iôg CWM Chemical Services, Inc. Model City. NY

+7167540211 T-267 P.004/027 F-999

f tgea ip t i t ' Trad'er

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Data 7!hMr tn ' TTnia Otrf

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[ ~ 1 Laakar • P m n i t V to la t ion Q Ptecamilng/Veft. 1.0- VJotatten

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Commei ts

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Smo idna o r aa t ing In .prah ib l lad a raaa .

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S e c u r i t y G u a r d I n i t i a l s : ( inHicat ing raca ip t o f Wash Say pass, i f necessary}

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Received Dec-31-Z001 14:S9

Pink: CavireaiDcntar'

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Coldemm: Driver

,To-ONYX EWVJRONMENTAL S Page 003

Dec-21-01 03:19pin From-CWM Chemical Serv ices * ' "+7167S40211 UEJIKHIMtNI tJ?i-'&NVTRONM(5NT»15e<T4SSRVATlON •'' •*

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NYB9675063

T-164 p.007/034 F-831

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HAZAROaUS WASTEJfl \NIFEST- -R O . B o x 1 2 ^ ^ b a n j ^ ! ^ N e ^ ftirk 1 2 2 1 2 ; •

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UNIFORM HAZARDOUS "; WASTE MANIFEST ^

3. Generator's Nama and Mailing Addrasa i - ~

F L E E T BANK ' , ^ 3 a i C f lRNEBIE CENTER, PO BOX £1265 PRINCETON N J , 0 f l 5 4 0

4. Senetaiors Telephone i > i 6 ^ f ^ 6 7 - 3 l j 3 7

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5. Ttansponerl (Company Name]

HDRUITH TRUCKS. INC.

rS.?-U,S-SPA ID Number'

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3. Pas« 1 el

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p. TTanEponersTBIapnoneSÔ g ^ l - g S g P 7. fhinsponorS (Company Nama)

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S. Designated Fadlity Name and Site Address ;

CWM CHEMICAL SERUICES, L - L c . ISSQ BALMER RQAO MODEL CITY NY. 14107

8.:-us EPA ID Number E. staie Ttansportsrs ID

^fi-f I F. iransporeraisiephona ( ,10. US SPA ID IMomber .Q. sisie l= icnRy I D

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716 7S4-6S31 12, Coniainera

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STATE

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K n .n 15. Special Handling Instmctione and AddiUaroU tnfermatlon

NVDc^ - ^ e ^ ^ - 2 ^ '^Qg fê . g s K ^ y ^ «!> z,/>^^r -#/:^3^^>r(C7

16. GENERATOR'S CERTIFICATION: l heracy aaclara inai tne cQblantspr itila consiijnrlierit. ir^ fully and aqgut^y deacnliBd abovs by proper shipping nama and ara clasatlled. paeted, msriced and labeled, and ars Injall raapects in pi^por condluon'br transpon by higir ray acconjing toapplirabia Intamatlonal and national government regulations and Biats lawa and raflutalions. . . , ir I am larga quantity genenztor. I sortiiy that I hnvs q prorjrjm'lr; piace to nduce Uio volume iTA tmr rity ol waste generated to tho degree i nave daierminod to be sconomically piactlcable and mat I have sslaaed mo practicable r.iethod a< trsaitnenl; stoiaoa. ar disposal currently i ioilabla lo ma which minlml=ac tho pxisont snd rutura iniaai to numan neaitn and Iho oryirironmeni; OR It I am a Smaller ganeraier,: i .hava.in8dea.good fajihjjttoa to inlnimiza jny ivai :a generation and solect me best waste management maiftod that is available la me and that I can altord.

Priiited/Typad Name .

•.Ttangportar 1 Acl<Boy<ladgemaftTOf Receipt of 17, Materials'

MO. Day Year

TlplBcinyped N a m e / ; ^ MO. Day Tear

IB.Tlwisporter 2 Aclmowlodgement of Receipt of .Vlaterlals pnnted/TVpod Name Mo. Day Yaar

-I 1 .,!, I I , 1 a. Discrepancy Indication Space c|Âi 11^ iiiuieaHun opitLitJ ) ^ ^

^ ^•^gg'^ ' ty Owner or operaior Cflnincôn of receipt of hazardous materials covered by this manife g' sxcepi aa noted in liom 79. P r j n t o d / ^ p o ^ N a m

kbK) pAfCyU. Signal

Racaivad D8C-21-2001 15:08

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Dec-21-01 03:20pin From-CWM Chemical Services

Transporter Log ; CWM Chemical Services. Inc: Model Cfty, NY

r -St:* tt -.+7167540211 .< +.V

l A I ^ T-1E4 P.008/034 F-831

Receipt It ^ Trailer Uearisiaj^^ftejf aiMSfate

SemcaReq.* _ Profita # • Pmni t *

S tortarttan^ TraetonTeaUer/Roll-oft'M; . -

bt jvai 'a Namm

Scheduled Arrival:

Actual Arrival:

Senarafor t . •

Oata l i m a

Dam Tirne'lh ~-

/ - # 0 i

U G 1

y y i / M ; ^ .#: /oi ^ - ^ ^ Receiving: C? y

In/ttais Commanta

Arrived during Blackout? Y / N ; Notified DEC? Y / N

[~] LMker • PonnH VIoiaUon . [ 3 PUe«nflnijiVBh:lE Vfelatlon-

Q O t h o r ( « p « e l f y -•" -• •• • ^ - " • • - ' .

^

,.. * ih^ Laboratory

_ . i

_ i

L_i

—;

—

Stabilizaiion

Landfill

Otner

Aqueous Treatment

Faciirtv Pe

Tima In

Tana In

Vmain

Tuna In

Time In

rsonnel (o/«

Smoidng

Falluralo

FaOurato

Unairfadi

Odnr ( i p

TimaOut •- l n i t i ^ \ : : : \ "> ... .

^ ' . , 1 . . . ....

Tuna Out » Irulials

. ; . • • ; • • ' V - -

77ms..a.'J /n/Vafeu- >• v T c .- . ;«'>? •..••#.?jit'/,;.

• • ' • • • • ; • • • • • ' • • ' ^ - " ' • '

Time Out . . . ^ IniHals ;.ij. .-

' • • ' • - ' - • - • • • - ' • -

Comwie^ IS ;" i -..

" : . " • : - ' - - ' ' ' ; • •

Gross W. Comments

• - ; - . • • . : • " • • • • • • . '

Oommei fS

..;,/ ; ^ . .'

Commoi its

• • • • • ^

TimaOut •'' SiahatuiB (NG Initials)' , ; " • ' ' Comments

" " " . ' ' ' ' . " y ^ •'.'•*'

lasB initial) v

er «ailng in prohibhmi araa*

otmy imfnuelfcKM of tecHHy poraonnol

MMT appropriate PPE

IWnil pnteifie**'

HdfWt

Ortwf»cui iwwii» ^ . „ ._ . . .

Received Dec-21-2001 15:08 iiroin-+71575:40211 ..... ,;.-. ... .

, Laavino micic uiurttandwl . . • . ' • - ; . • i ^ . . . . . . i

, Faliuro to dl«pUv ovwwolaiit ftmc

Improper tarplna or dotwpin

OvMvntaht upon urhral

•xr

Security Guard Initials: (Indicating receipt of Wash Bay pass, if necassary)

Goldcmw; Driver,

,--:. T(iu-QN>X ENVIRONMENTAL S Page 008

D8i-21-0t 03i21Pi frm-Cm Cherai

PIsaae type or pnnt. Do not staple.

H7167540211 oal Services • ' - —»<=.-'"<oa3/,w,-

, HAZARboUSWASf E M fVNiFEST ii R.O. Box T2820, Albany, Newr torR" t22l 2

T-1B4 P.009/034 F-831


1. Gon8ra«ot*Bus sWvNo. ' iwanifeajDoe,Na Ml JiR lg fg le iB i3 i7 |6-ig-ig ( ^ - ( { O i t iT :

2. Paga 1 ol

i Informallon wimin heavy tlOld line is not required &y ^deiai Law, ,

a. cansraiora Name ana MalTing Address FLEET BANK 301 CARNEGIE CENTER,PO BOX 2066 PRINCETON NJ, 08540 4. Goneratof's Tblephone IvlS^f ^ f l 7 ~ 3 1 ^ 7

IK NYB9675054

,B. Ggggto^^T^ NJ, I387t5l3 1 3 Z 2 S>6ivg-^rt iHyg. 4. / 5

J. it-ansporter 1 (Company Name)

HORWITH TRUCKS. INC.

. JCLU.S.S=A ID Numoer ~

PTfi tD^^l |4feg,7 | i" l4 |B |7 |B C State TransporrersiE D. Tranaponer'sTei iJ(8 £ ^ - £ 2 2 8

7. Transporter 2 (Company Name)

0

3. Oeaignaied Hacilliy Name and Silo AOdress '';

CWM CHEMICfiL SERVICES, L,liiC. 1530 BflLMER ROAD MODEL CITY NY, 14107

;.&;; WS:EPA to Nuniosr

-1 -t -I t r r - r I _i i £ Satallanspo

E Transpoftor^ Tal^phona ^kL*/6ar/P*

to.: <JS SPA IQ Numoer...

N | Y | D , g , 4 , g , 8

S . Suae FaciUty lU

N/fl

5 6 ^ 9 H. Facility Telepfioni? { )

716 754-3231

11. us DOT Desertp&in (Including Proper Snipping Na/ne.Hazaiii Class and 10'Number).. i|Z. Containers

.NLunbariTVpe

13. Total

QusmJtv

1<t. Uni!

Wtvol I. Waste No.

^HflZflRDQUS UOSTE. SOLID, N. 0 . S-, y -.-:..; (TETRflCHLORDETHYLENEl C512157) 9,'Nfl3077» m / ^

•ggr F002

"iV* 3^^ iL-L ^ t ^ i o i o i c STATE

EM . . - .-_H-J

STATE t i J—L :-L I . I J 1

EPA

STATE

J , 1 - 1 ...l

G em

STATE

J - .U J. AddltforaliOpicrlfifens for Materials listed Abow '•. K. >-<andling ( i jdes jor Wastes Uasod ABove

eftvji jg i ^ r r E D J .

n n iS.Speeial Handling Instnietions and Additional Information

v! :'.:;y .c

A\Di:- -sfc^ ^"^3^05 ^ yae.OeA<vg f av "nfefe/ ryg"5"V^r/

c 16. G E N E R A T O R ' S CERTIFICATION: i howby iiocinreitfiai me contonta_pf iWjsjspnsignmont a r e j illy.atirf accurately dsscribe^ above tsy proper snipping name and are

eiaaolitcns. pacKed, marked and labeled, and are in all raepacls In prouer cpndltion'ibr vanspen by hlgiway ; XBidinjpo appllcat)(o*lnternatIanaI and national goveffimam regulations and slate laws and ragulatlona. , ' . i

If I am largo quantity gensramr. I eortlry that I have a pn>gram in placa to reduce trip volume and toxldi^; I waste geneiated to the dagnre I hovo dotsminea to Ce oconomliially piacllcatsle and that I have selected the piaclicable metnod a( treatment, storaqe. w dispanJ (Mn-oniiy avaiia •» ta tag wMcn minimizes the present and future inrsal la human noaiin and the enviranment; OR HI s/n a iwiaiier sonsrsosr, i nave made a good faltn oHprt 'a rTiii::lmlza my wa-îo.se vimiion.and saiMa th> boct 'naste management mctivod that Is available w ma and tltat I can atldid. '• ' ~'

Mo. Vbar

55 W M ^ .

Day

I ; PrI' Tfan=poner 1 Ai Receipt of Materials"

Priniod/Typed Nome

I la.Thinsporli

L — P -p. *c^<^.

Thinsportar 2 ArtnowiGdgoment of i=?ctMlpt of Materials

Mo. Day 'War

J (igiAiTlrg/.

Pfinted/Typed Name { SIgnatu~a Mo. Day Y&ar

I I I I ! ! -19.D(Serepartcyindlea<ion Space A j ^

4cMy.J A^.J 4 ..' ^hr. -Igfai^ /A"Q^^ X r -20 , Faciliiy Owner or Operaton Cartinoation of receipt of h'azaitiouB materials ccryerad by iWa manliest axe 'pt a s n o i ^ In Horn 13,

Primed/Tv T^mX2j^^y^/t

Sigrt:

i ^ J ^ dJAj&iZ: ' M M COPY 1 - D l S P P S E R l 3 J A l ^ > MAILEp;'P; ' 'TSd FACILITY

Received D8C-21-200V 15:08 Fr(Jiii-+71675402V i>

-ONYX ENVIRONMENTAL S Paas 009

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Dec-21.-01 03:23pin From-CWM Chemical Services

Transporter L o g CWM Chemical Services, inc. Model City. NY '

Ui 71S-7§4g211 r / T-1S4 P.010/034 F-831

Cuotciams

i p t t ' ( Receipt Mm-

la i lerpianse Ptat&'fandrStm'':':

/JranaporterAtowe rransportor

:i2 ' r /Tra i te f /RiM^^ i

bihiei'stama

. tfactor/Tratler/RolHfff* » -^

:)inw<s Mama /Qenerator • i;,; f" " "

Scneduled Arrival: / ^ 1 ^ Oy />? ?> ^ '

Aciual Arrival: / ^ / 5 r / ? / / 6 ^ - Y > < 1 ; . / - ^ Ti inain- - — ~ -7»77>i> O u * .

Arrived during Blackout? Y / N Notified DEC? V^%N f,

n Loalcw Q ParmltVlotatlon • Plw!Brdlnfl/V«h,J.D.yiolallon

I I Other (specify -' ' ? " v " - .r_

Receivihg; irlg* J y ^ — • fniffjsts Commanta

^^T/€ulk loL•^«M1l l p~j NoWWtllne I [~| ^ I b o d ;;:jg} StaBaizaOoifl [ " j Dnjnw Q Tanlwr Q Tr.o.loriiwrr«

L a b o r a t o r y - . 7 > v. > . ^ " ' ~ : "•^•••" '- _ '" •• -•'• • y ^ • Time In TuneOyt'i Initials. Comma Its

Stabilization

Landfill

Time In Time Outi Initials Grass.\l 't Commanta

Tims In Time Oia • Initials -T^ Commt nts

Otiier

Aqueous Treatment

Time In Time Out Initials Commt ntS;

Tana In TJwe-.Out SignatuiB (NO Initials) Caawnents

c Facility Personnel (piease inisai.)

Smoldnfl or aailng In prehlbhad ia»m»

Faitura lo oboy Inamieilona of facility pofsonnal

Falliira to waar appropriata PPE

Una«fa drtvlnfl pracllcaa

OlfMr (•poetry) : —

Laavinfl injcic unMlwidod

Failure to display overMeigM tlag

^'ziZ. ZL Improper larping or detarpin

Ovanwilflht upon arrival ^ h

Secur i ty Gua rd init ials: (Indicating racaipt o l Wash Say pass, i f necassary)

Drivar^ CafnuMfila

While Reeotds C n en a . CMBvy. Acox R!K.

Received Deo-21-2001 15:08

Pink: EmuronibciBTal'' '

Frora-+71E75402T1

Goldenn d: Orivo-

To-ONYX ENVIRONMENTAL S Page 010

Dec-21-01 03:59pra From-CWM Chemi.cal .Services +7m754(l211 T-188 p.031/034 F-831

iB^Ti'lri?V)i-,VM';M'iiniri |-| HTi'i"l'i''ifl TTiriufi i i i im.».[ i»it f<nMi "iflL. .>i\f-. .lOIVISB»N.pC SOMO .4 HAZAPIDOUS'^ ATCH1AI.S

-i HAZAREiO^SA/W^STEJm \N1FEST i -PÔ. Box 12820, Albany, Nevir' 'ork 12212

CCWM

.V .QBno.mtDr:9 .UB EPA No. ; IVIanilc^t DOOL NO.

LT IR g - g r i a irgr:3i 7i 6i--0l-- iC!?:|.-|'- i.O| t i l 3. Qenerator's Name and l\âiling Address

PLEET BANK .,,„,, 301 CfiRNEEIE CENTER,PO BOX 2065 PRINCETON NJ, 08540

4. Generawi'3Telephone N t&B§ p S 7 - 3 1 | g l i 7 ; |

e. Pago 1 of Information vrllhin heavy bold line is not required by Paaoral Law..

NYB9675045 - °"SEJP'^'fRT, NJ,. 08750

132Z 5eA GliHr i4-v6. 5. Transporter 1 (Company Name]

HORWITH TRUCKS, I N C

iS?;;t^;ERA ID NiirtiBar' ? r f-'^

'.:^'l 'SC'bt 1 | 4 i . y . ^ - ' t ; . - 4 , a , 7 , ' 1 B J ~ D . Transporter^Telephone"Sjirb ^ l - j

C. State Tianspottei^ II

7, Transporter 2 (Company Name) V: ' US EPA ID Number ^ ;

• • j ' I I I C ' i I- ' r I I

E. Stats Ttansponerl ID

F. Ttansponerl Telephone (

3. Designated i=^cility Nama and Site Address

CWM CHEMlCflL SERVICES, L-L.C. 1550 BflLMER ROAD MODEL CITY NY, 14107

. i a ua EPA ID Number Q. State Fatality ID

N/fl

N,- -^>g^ 4,-3, ( I , ' 3 , 6 , 6 , 7 , 5 H. Fadlity Telephone ( }

71S 754-6231

11. u s D(3T Oeseripijon (Including Prppor Shlsplng Name, i ia ia i t i Class and ID Number). 12:-'Contain8rs

Number., Type

13. Total

Quantity

14. unil

VWVol I. Waste No.

HflZRRDOUS WnSTE. SOLID, NJbwS,.;:.. .;, î ; . . . (TETRflCHLDROETHYLENE) (5 i e i 5>% ' -9 , Nfl3077^, P

EPA

FB0S •-.;!; I jy m ' . D , T , 440iOi^

STATE

SPA

STATE I I I 1

EPA

STATE I I I

d. EPA

STATE

J__L J. Additional Descriptions Tor Materials listed Above

an&ttrAcU&ftne^^ tewg I'S r T i • e-

K. Handling Codas for Wastes Listed Above

_L n n

15. Special IHandling Instructions and Additional Information

y3<s^^^3S~'

6. GENERATOR'S CEFITIRCATION: l neraby dedaie that tha contents pi this epiiafemi nt are lully and aceurat 16. GENERATOR'S CEBTIRCATION: l njraby declare that tho, corttents pf this epiisignmi nt are lully and accumtoly dosoibod above by prepef shipping name and are classified, padced, maritBd and laboled, and arelrr ail tafipecta In proper condition for transport by Y ghway acisomlng lo applicable Intemadonai and national government reguladona and state laws and reoulations. If I am large quantity ganarater. I eanlfy Ihat l have a program in place to redui:e the volume ;,;td Isxleily at vvasto gcnoiated to Iho degree 1 have determined to be economically pracueable and thall have soloctod ihe praellcafile meinod oriraaimant. storage, or oisposai cuirsr lly avaUaUe to me wnicn minimizes the prasent and future threat lo numan healin and ma orTvIicmnent: OR if I am s smaller qonerator, I have mads a good iai4i atici'; to minimizs my ivaste generation and select the best waste management malhod mat Is availa&Ie to mo and Ihat I can afford.

prinieanyped/iMame C-f tSÔ/v^^ ,

Mo. Day Year

/ i 2 . i ; i 7 , 0 i / 17. Transporter 1 lowledgament oi Receipt of Materials Prinii W^ fj^fy 70.T7anspdhsrz Acxnowiaogemsni or Hocaipccf Maioriais Prinlad/TVpcd Nome Mo. Day Ybar

U I I

:ropancy Indication Space '' . . ^ ^ ~ ^ ^ J & ^ ^ ^ ^ J ^ • ' i ' ^ ^ ^ ^ ^ y 2 £ ^ - ^ ^ d - £ ^ ' C £ ^

^J:&,^ i^-arj/- S>-20. Facility Ouunpr or Oporalen Cartilieaên of faeiaipt o( haaanjous maWrlalc eovorod by this rr anifost oxeact as nolod in Ham 19.

Prinled/TVped Nama /"> '' -Slgni

^ . - ^ L ^ . a ^ L jxwr COPY. TVDISPOSERrSTATE-M;a iLED BY TSD FACILITY

Recaived Dec-Zl-ZDIJl 15:57 Froiii-+71B7540Zri To-ONYX ENVIRONMENTAL S Page -004

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Deo-21-01 03i59pra Frora-CWM Chemical-Services- • • ' - ' • -

Transportar Loffl , „ . ..^ .;; ._ C W M Chemical S ^ v i c e a , Inc.

ModelCity,NY : ;^ ^ ! - - - ^ £ i ' ; .

ReeejDtit, , TianerUcense Plate* and State.

' ^\oS^^Jsyô o t ^ y ' y m n l ^ R e q . * . J P n O a t t f e t ^ U T T

:.+ 18754021-1 7-168 P. 032/034 F-831

icVuds '

7ij?2!3 L3 G 2

fT tamoi , tOQitarName T fac to r / r ra i je r / l ^ t ^ f f * , -: W'] r/a>Mgarter

Genorator

Scheduled Anrn/al:

Actual Arrival:

32900 L B G l

7^1 ^ r c P S ^

Data Time In. • , Timapik : '»^l

Arrived during Blackout? Y / N Notified DEC? X:;/ N ^ ^

r i teener Q ] PermRVioiMion i [~| Ptoe»rdlng/V<rti. L P . vtohMten ^

r n other (specify • _• •..:' ". •-

' Receiving: ^ ^ Initials Comments

X / f B u l k t e Landf i l l ( ^ N(»«H««iliui' [ n F latbed

Daboratoty Time In TimaOut-

SiabiUzaiioitrl; f ^ l -O rums _ [ ^ Tanker [ "1 Transfonneni

..Gornr lanis'.

SiaOiiization

Landfill

Other

Aqueous Treatment

T fma in

-

Tima In

TUnaln

Time In

TSnaOttt .

r" ,, "-''" .-

Ti im- jOiMt— -,-r.s,.. ' 3 . , •

1

Tnna Oii/r .

-. -

Tirrw Ouf

inftf^/G. . .

f : ~5' 1.

' • • ' • • • - : " • • • • • • • • . '

, , I n i t i a l s . . .

— - • ^ • - • : . • - • • " •

/ . . . . . • ; • .

eA>s..wt.

. . " , s •

- Coin, nanis

• '• . f - ' ' .

^- Cam nants

-. ^.- - , ' ^

agnatana (NQ Initialsh \ - ^ -'•/ Comrne/ iB

Faci l i ty P e r s o n n e l (fiUmîniaai)

G

G

SmoWng or «ellii>a In prohibited area»'

FaiUira t o oOey IsistniCl ions o f n c l l h y parmonnot

FWhiro t o w a a r c p p r o p r b n v PPE

Unea le d t lw lng pin>cte««t

0 1 f M r ( a p M i f y t •:: " _ _ _ •_

LMnrtng t r vsk u iur t londed

Fai lure t s diaplay o v a n m l g h t t l as

Improper t v p h i o o r datarp in

Q w t w i B h t u p o n arr iva l

_ Secur i ty Guard Init ials: _ ^ _ _ ^ _ _ ^ _ _ ^ _ ^ _ (ladicating mt»lpt of Wash Bay pass, i f necessary)

M g ^ ^ g - ^ X J o l i a arad:.l>i«er

Frora-t71B7540Z11, To-ONYX ENVIRONMENTAL S Pago 005

Dec-21-01 03i26pra From-CWM Chemical -n iop i euO ' '

ymmsasG Please type or print. Co not staple^

+7ie7S4£211

•^^'^^^•^*"-^^'^° n " - ~ . ^ , ^ - _ DIVISION OF,SOUD & HAZAHDOUS MAT SwCS ' . ,.

.Services • - • , » - .

T-164 P.013/034 F-831

IHA2ARDOUS WASTENTAr IIFEST :IP,0. BOX 12S20, A I D a n y , IMewyOi k T2Z12

CCWM


1. Generator's u s EPA Na Ma iitesi Doe. No.

i.t p PI a gi.wrff..i7 ifi lanq tO i l i d iQ^ .

2. Page 1 ol

- L Inlormaiion wilhin heavy bold One Is not required by Federal Law.

3. Genefators Name and Mailing Address

FLEET BANK

301 CARNESZE CENTER,PO BOX 20e&

PRINCETON NJ. 0aS40 ^ _ „-i A. Ganera to r '8Te [ephone l6 f t fe fSp7"31y7 ;

NYB9675036 êf ' ig^^T. NJ, 08750

5- Transporter 1 (Company Name)

HORWITH TRUCKS. INC.

:,S, ys ; iPA ID Number.,., ,

JPiRî'il i4 i6 i7 .|1 ^ g 7 g C. State Transponei's ID ^ j i • I ^ M Q " P h

0. Transponer'sTalephon£lj0 2 & 3 ' ' 2 2 2 0 7. Transporter 2 (Compaiiy Name)

9. Designated Facility Name and Site Address '.

CWM CHEMlCflL SERVICES, L-L.C. 1530 BflLMER ROAD MODEL CITY NY, 14107

8.i US EPA ID Number

•> I I 1 - I I •!•

E. State Transporter's ID

F. Tiansponer's Telephone ( 10. US EPA ID Number 13. State Facilitv II KiPfl

N|Y |D ^ ,4|9-.ff-r3 ^ & .7 p H. Facility Telephone ( )

716 754-8231

11, US DCrr Desoriptlon (Including Propar Shipping Namo, Hasard G M X and IO Number) ,T2, Coniainors

Number Type

13. Total

Quantlly

14. Unit

Wt/Vbl I. Waste Na

HRZORDQUS WASTE, SOLID, N.Q, S, (TETRflCHLDROETHYLENE) (512157:) 9 , Nfl3077, t l l -

bPA

FI9e2

:LL ^ i - ^ O P Q STATE

EPA

STATE I I

C EPA

STATE JLJL I I I I

EPA

STATE I I I I

J, Additional Descriptions for Materials listed Abo>/a

± L

K. Handling Cages for Wastes Uated Above

b. J i n n 15. special Handling Instructions and Addilional Information

oenffigi

^y^^ -7^ 16. GENERATOR'S CEHTIFICAT10N: I horciiy dcdara that ihe contents of tnis consignrhent-a 8;fijlly and acxumioly described above by proper shipping name and am

dassifiod, packod, martted and labeled, and are In all respects in proper condifiorTfqr Innspon byliigtivt ly according to applicable International and national govemmant regulations and suata laws and raguloIlanA. 'j

' • . - . 1 • ' . . . • ' . -

If I am large quanlity genoralor. I certify that I have a orogiiun in placa to ladiica the volume and tbxK ly of vvasis geneiatcd lo the degrae I have determined to be economically piactii=]bla aird that! have selacied Ihe practicable method of treatment, smtago, or disposal curronily a' ailablo to mo which minimizes the preeeni and luiura tnreal to numan neaitn and tho onvironmont; OR Ir 1 Am A Amnllop gonoracpr, I hAV«mneaa good faith .affon to iTiinitn}xo..my M tPt»gananalon and aaiooE tha eaatvusutM manAgAmantmathodihACift AvAjlAbla to ma and Ihal 1 can aftorei. ^

Prlntacinypeq Name Mo, Day Year

iS.OIserepancylndicah'on Space A ; Z^Û^ /^. - - C 0 1 , D /

20. Rscility Owner or Opsraton Csnlllcallon of receipt of hazardous materials coyersd by this manlfe » except as noted in Item 13. PriniBdnvoed Name

( % C t Z A A : ^ signatun

yjdAî^zr. COPY i1-DISPOSER -STATE - MA lUcP-BY TSCT FACILITY

••V f• . ; iîî : , ; , a

Recaived Dac-21-2001 15:03 Froin-t7157540211 To-ONYX ENVIRONMENTAL S Page 013

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Dec-21-01 03i28pm From-CWM Chemical Services Tranaponer 1.05?. C W M C t m n l c a l Senrloes, Inc.

Model City, NY

+7167540211 T-164 P.014/034 F-831

V^L\M : i . _ CutueTiiude

%]^^JH£7Q^ ^ < - ^ - ^ .I-;; ' . Receiptrt TrgMer Uceiae Plate * and State

Seivica Req. H Pmina 4t

Tra/tsportef Name

Drivel's Name

Schedulied Arrival:

P ^ 7 A ^ Pe/wijf #

<:<i / V J

TraGtorfTtaBet/Roll-otf *

Qenaiator

ISvtm A c t u a l Arris/91:

ein I Time a

Yf30^^ H ^ Z ^

Receiving .JI . Initials Commams

Oata Time In / TimaOut

A r r i v e d d u r i n g B lackou t? Y / N No t i f i ed D E C ? Y / N

n l.aalcer Q Pennit VkHailon -' Q Placardlng/Veh. I.D, Violation

r~\ Ottimr (apeeffy '

r n Bulk lo LBniinil r~ j NO wet llnv r~] Flatbod [ ^ S««blIIzBUon Q Drum* | Q Twifcar ^ ] Tran«torni«r»

' ;•.•,/ '•:• t • .. . . . . . ' X ' . . u ;

Laboratory - ^ Timain Time Out Initials Comma lis

Stabilization

Landnn

Otner '

Aqueous Treatmerrt

Timain

Timain

Time Out . .,

'

Time Out

. . . - . ' - : • ! • : • • •

Initials

" Initials- ^

. . , . . . • . . •

Gross VL

Comma its

Comments

_. •

" ! •

Timain

Timain

Tuna Out

Time Out

Initials.

- • - • • • -

Comms nts

- Signature (NO Initials}

•

Comments

Facility Personnel {piaasa miBai)

SmoUng or eating in prohibited areas

Fauure to obey Instiruettons of facility personnel

Failure to urnar appropriate PPE

Unsafe driving pradices

Otner (specify) _ ^ _ _ _ _ _ _ ^ _ ^ _ _ _ _ ^ _ ^ _

Ijaaving tnicK unattended

Failure to display overwaiglrt flag

Improper tarplng or datarpin

Overweight upon arrival

Secur i ty Guard Init ials: . __ (Indicating receipt of Wasn Bay pass, i f necessary)

Orivsff'sCiNiiiiieiitB ._

W|)iic: Iteeordi Green A Canair. Acas Kee, Knit: Envunnmeatai GoldcurD I: Oriwr

Received Dec-Zl-2001 15:08 " From-+7167540211 To-ONYX ENVIRONMENTAL S Paga 014

NYB9675126 Please type or print. Do not staple.

STATE OF NEW YORK DEPARTMENT OF ENVIRONMENTAL CONSERVATION

DIVISION OP SOLID & HAZARDOUS MATERIALS

HAZARDOUS WASTE MANIFEST P.O. Box 12820, Albany, New York 12212

CCWM

(Hazardous Waste Manitest 5/00)

UNIFORM HAZARDOUS WASTE iVIANIFEST

1. Generator's US EPA No. Manifest Doc. No.

N | J | R | 0 | 0 | 0 | 0 | 3 | 7 | S | 0 | 9 | O | | iOiOi7 2. Page 1 of

1 Information within heavy bold line is not required by Federal Law.

3. Generator's Name and Mailing Address FLEET BANK 301 CARNEGIE CENTER,PO BOX 2066 PRINCETON NJ, 08540

4. Generator's Telephone N§l'J^r ^ 8 7 - 3 1 ^ 8 7

A.

NYB9675126 B. GgEs^togî^j^ ^ j ^ 0Q750

s\ai lys^^f i i^ i f :^\sr '-S'TH CA V


CLEAN VENTURE, INC.

6. US EPA ID Number

N| J | 0 | 0 , 0 | 0 | 0 | g , 7 | l ,9 ,3 'q-

D. Transporter's Telephone908 3 5 4 - 0 2 1 0

7. Transporter 2 (Company Name) 8. US EPA ID Number

I I I -I I I i I I I I


F. Transporter's Telephone ( 9. Designated Facility Name and Site Address

CWM CHEMlCflL SERVICES, L.L.C. 1550 BALMER ROAD MODEL CITY NY, 14107

10. US EPA ID Number

N , Y , 0 , 0 , 4 , 9 , 8 , 3 , 6 , 6 , 7 ,9

G. State Facility ID

N/A H. Facility Telephone ( )

716 754-8231

11. US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 12. Containers

Number Type

13. Total

Quantity

14. Unit

Wt/Vol I. Waste No.

^HAZARDOUS WASTE, SOLID, N.Q.S. (TETRACHLOROETHYLENEX512157) 9, NA3077, III

EPA

F002

PJLL AA\bOt:, STATE

EPA

STATE

I I I I EPA

STATE I I I

EPA

STATE

. ^ - L I L J. Additional Descriptions for Materials listed Above K. Handling Codes for Wastes Listed Above

b. J. \ L D D IS.Speeial Handling Instructions and Additional Information

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16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled, and are in all respects in proper condition lor transport by highway according to applicable international and national government regulations and state laws and regulations. ,

If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that Is available to me and that I can afford.

Printed/Typed Name.

17. Transporter 1 Ay^ylowledggftpnt of Receipt of Materials

Mo. Day Year

1/ | 2 - l / n \ 0 ) /

Printed/Typed Name

18. Transporter 2 Acknowledgeyient of Receipt of Materials Ji

Mo. Day Year

Printed/Typed Name Mo. Day Year.

! I I I I iscrepancy-lndication Space I / O

,y¥^. is.ôc/-dy~~ 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

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^Jafl-09-2Q02 17:50 From-ONYX ENVIRONENTAL SERVICES

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Tfansoofter LOQ CWM Clwmleal Services, Inc.

Model Ciy, NY

+2155336799

-• • •• 4-71S7546S1

T-978 p.003/003 F-7Q9

T-1S4 p. 001/034 F-aai

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£'j(C-21-01 03:24pra From-CWM Chemical Services 4-7167540211 T-164 p.011/034 F-83

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' # r " i ! ; " jÂZARDOUaWASTE M/.NIFEST •• P.O. B o x 13S20 ; .A lbany . N e w N o r k 12212

CCWM (Mwai^WBi w»3>v ftaa/.il97t :wo»

WASTE HAZARDOUS MANIFEST _

1. . aonorator'aySBPA.Np. , ; : .Itonifost Doc. No.

M IT IP ll?l IP» lOt i <» t3 i 7 16 i B l s i 3 | ( _ l < & | O L ^

;'l>liuno and Maillna Addrass j

a ^ i J R S E S I E CENTER, PO BO 2066 ^ I N C E T O N N J , 08540 ^ i " ^ Bpnai^tefa Telephone NSf lSr ^ 6 7 - 3 1 ^ 7 '3 . Transponor 1 (Company Nama)

C L E A N V E N T U R E . I N C .

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• NYB9675135 '^ ' ' fgrgfftT, NJ, 08750

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SJ. Doslgnatad Pna'Iity Name and Site A'tataait .i

CWM CHEMlCflL SERVICES, L-ll.C, 1S5Q BALMER RCAO I MODEL CITY NY, 14107 !

10. u s EPA ID Ivlumber

N : , Y , D , 0 , 4 , 9 ,B 3 ,6 6 ,7 ,9

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716 754-8231

11 . US DOT Description (Including Proper Shipping Name, Hseard aass.and ID Number) 12, Coniainors Numbiar Typo

13. Total

Quantity

14. Unit

WttVbl waste IMo.

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m c. < > ^ 4 ^ ^ g s Wof^^vm^¥'''$e};^^< • rTy /^^^ 'A)^ T ^ ^ IB, QEiMEHATDR'S CEFiTIRCATSON: I naraby declare that Iho cpntonts of.jhis consignman; ara fully and accurately descflSefl above By proper shipping name and are

dasiflod, packed, mailced and labeled, and are in all respects In proper condition tor Iranspori Oy Mg way according to applicable Inlemallonal and national govarnmant ragulallons and state laws and regulations. I ' ' , " " • • . . If I am larga quantity gcnorator, I certify that I have a pmgram In placo.to rsduco Iho volumo.ond tc licityol waste generated lo tna dagres i have dstcrmined lo bo economicolly prHct)cafe'« and that i havo soloelod lh« prscllcaalq m«mod of.traatmonc, storapu, or dij:posal cuirantl) Avnjinbio lo mo ujhteh minirriiso* Iho prosant and fuluro thraac ro human hoaith and Ihe snvlronmant; OR if I am a smaller generalor. I have mada a good.taiih atfoci to minlmlze.nny. wi ste generation and solcci the' best wasia management method that la available ? « m o a n d t h a t 1 c a n a f r a r d . •<•,-.. " , _ . "- , ' - , . .• -,.-•• . .

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Mo, Day Year

COP-V V-DtSPOSER'STATE - MAILED BY TSD FACILITY

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Transporter Loq +7187540211 T-1S4 P.012/034 F-831

^ g ^ ^ CWM Ch«nlcaJ Serrfc«, Inc. ' ^ i " Mcdet City. NY / / / i ^

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Landfill

Other

Aquss3us Treatment

Time tn TimaOut initials Gross m. Comments

Time In Time Out IniiJBls Common s

Time i n Time Out Initials. Common is

Time in Time Out Signature (NO Initials) Commants

' FealStv figrsor^raei iptaasainitial)

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0 » s n » i Q l i i iiJBOiB arr ival

Security Guard Jnitials: (indicating mcaipt ot Wash Bay pass. If necassary)

Whine: RscanJi Gr«sn .& Canary! Aesis SIM. ?ink: Hsmromnoiiai Ooidmreai Dover

Rscaivaii Dsc-Sl-ZOOl 15:03 FrDU-i-Tl 67540,211, To-ONYX ENVIRONMENTAL S Pase 012

[— Deo-21-01 03158pm From-CWM Chemical .Se.fyices •+716754021-1 T-168 P.029/034 F-831

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Please typo or print Do not seipte. P.O. Box 1289btAlbany, Nev -S iprli; 12212


3, Generators Name and Malcne AddrasK FLEET BANK - i 301 CARNEGIE C£NTER,PO BOX. 806& PRINCETON NJ, 08540 4. Genaiaiof'BTelephonalsfifl^^B7-3lp7

1 . Gena ia to r^ u s EPA No, UsnUact O o c N ^

N J iR 10 10% 10113 i7 i5 li-iî P T I I OI ITJ

5. Transporu^r 1 (Company Nome)

HORmtH TRUCKSj^ INC. 7 . Tians:porter a (Compsity Name)

' 0 . . U S SF¥\ ID Numca-.

P , A T D i l , ^ 4 | S , ^ 1 i ^ i B i f i B

9. bosignmBct Paeilily Noma and Site Addrojis

CWM CHEMlCflL SERVICES, L:L*C. ISSa BflLMER ROAD . ~ '•' MODEL CITY NY, 14107 ' n

a.- U3 eP)\ 10 Ntjtmjis

T "' ' I I I I I I 1.0. u s SPA ID Numfac r

N , Y , D , 0 , 4 , g < . 1 l , ( 3 - * , 6 : 6 , 7 . 9

11. US DOT Oescnpfion (Ini:ludlng Proper Shipping tslatne, Hazard'Class and ID Number).

Z, Paga 1 o l

1 information within haiwy bold Eiia IS net required by Federal Law,

NYB9675072 °geB"gi^T, NJ, 08750 ^.xJi

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Number [Type

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"HAZARDOUS WASTE, SOLID, N,Q.S, 'i > (TETRflCHLDROETHYLENE) (512157r 9, Nfl£J»77," ili

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STATE

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STATE

I i; I I I I SPA

STATE

1.1 I I I J. Aaotsipnal Oesertptlons for Materials listed Above K. Handling Codas for Wastes Usted Above

±. n n

19, Special Handling Instructions and Additional Informatfon

16- GENERATOR 5 CERTIFICATION; l hereby declare that me..contonts'jif this cdnqlsntnt rit ara fiilly and aQcumtaiy described above by pioper stilpping name and are dssslfled. paeKsd. marlcoa and u lmr iH , and ata In an respaeix in prspoccsndlllbn-far trompoit ^ h glnfsy/accaiOing to appllcaoia international antl national gevomment regulations and alala laws and regulations. j - : - ' : . , : ' IT 1 am large quaniliy ganeraior. I csrtlly thai l-havo apmgiam In place to reduce tho volume and i^cTty of waste generated lo ihe degree I have dolsrminsd lo ba economically practicable ano thsjt • tuiva saladoa ina pnctisabio mainod ot traaimani, sioragoi or dlcpoEur diirror! ly aTsilsbla lo ma wnich minimizes ma prasont and luiure threat (o human heallh and the anvlronmoni; OH III am a smallflr.ssne[ator, l nava made a good .^.th .sfoit to ffllniffli2;9.iTiy. Ofte ganeraiion and select the best waste manaaement method that is available to mo and that I ean afford.

Pripl^drtVped Name

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^ ^

Mo. Day Year

7 i 2 i h ' h t x i 17.Tfans i»nQf 1 A I l odgemiW o( RacelpfSf Matoriolc '

Prim Name

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19. Discrepancy Indication Spaco i n c y inaicaoon apaco ^ — j

fyuy:: zuJL y U W ' M^¥<^ r^ .y--20.Faclliv Owner or Operator: Ccnilication of receipt df-hazardous materials covered by ihla ms nfest except as noted in Item 19.

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Tuna I n . TimaOut Initials Comment:

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Comments

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Faci l i tv P e r s o n n e l (p/easa /ni<«/)

Smoidna er aaling In j^rehibMed araaa -:

Failimi lo obay inatnictiona of facilhy panannal

FaKura lo waar approipriata PPE

Uitaafa drMng practlcaa

Otitar (apMity)

Laawlng tmcK unaoandad

FaUura to diaplay avarwaiahi flag

iRiDropar tavpine or datarpin

Owanwatglrt upon arrival

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' STATE OF NEW YORK.. DEPARTiMEl^jQfÊNVIRONMENTAL CONSERVATION

DlÎSIONOF»SOUD & HAZARDOUS MATERIALS '

HAZARDOUS WASTE MANIFEST P.O. Box 1282d, Albany, New York 12212

UNlfrORM HAZARDOUS WASTE IVIANIFEST

(Hazaitiou3 Waste Manifost 5/00)

3. Generator's Name and Mailing Address

FLSe t .8i2^M 3 ^ i C P i m m i E CEHTER, PO SOX BWf.& PSI-^n:ETSNl NJ , ©aS-'f@ _

4. Generator's Telephone lumber ^ p •• ~ •- * P '

1. Generator's US EPA Na Manifest Doc. No.

NiJ iRiaivgiaig?i.3i?i£.iiai9bil lOil f->. 2. Page 1 of

Information within heavy bold line Is not required by Federal Law.

A.

(NYB9675081 8. Ggggtogâ^^ W/ ,3^753

5. Transporter! (Company Name) ^ ^ ^ ^ - ^ ^ ^ . ^ , a , \

• ^ T ^ T S T H ' ^ T ' ^ ' I " ' t - ' I '»i»3"'v7-|.'S>

C. State Transporter's ID < ^ U '5^ .4^^ ,»^V^

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9. Designated Facility Name and Site Address

€.Un 0-€i^?CAL SERVICES, L..L. C. (55© &SLHES fiOAD • MOrCL CITY i-iV. i4i'*^7

10. u s EPA ID Number

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11. u s DOT Description (Including Proper Shipping Name, Hazard Class and ip Number)

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12. Containers

Number iType

13. Total

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14- Unit

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--V,r:r4/^7/^' 16. GENEflATOR'S CERTIFICATION: I hereby declare (hat the contents of this consignment are fully and accurately described above by proper shipping name and are

classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations.

If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat lo human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Printed/Typed Name Signature Mo. Day -, /fear

I I I - I'- I- I '• 17. Transporter 1 Acknowledgement of Receipt of Materials

Printed/Typed Name

iWiv rf iNfûoriy; Signature

t " < t . < / (....-SL-: "^./'yyK^y'iy) Mo. Day Year

• H -18. Transporter 2 Acknowledgement of Receipt of Materials / ( Printed/Typed Name Signature / Mo. Day Year

I I I I I 19. Discrepancy Indication Space

A^^-r.J' . / , • • • ^ .•/ '/ .y:/ ' i >o J / d 7

20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

Printed/Typed .Name

hi/Mty^,) C.A:..rz::y^ Signature -^

/ .y ^ y . £ L ~ cyy.. Mo, .Day Yea.-

/ / / C f / • ; /

COPY 7-TRANSPORTER COPY - RETAINED BY TRANSPORTER.

f-"v

r"

G

G

\ S ^ B S B

Transporter|.o^: ^ i f l CWM Chemical Services, inc.

ModelCity.NY

113:86 ^ ^ Cubicy^nte

J<r/ '^'CMr~f f - y ^ /•'> y

Receipts >tif . . _ TiaUer Ucense P la ta * and Slate l * ~' / . _ 7iaf7er U c & : ^ Bate # antf

PetmU* Serwce'Req. a '• ProBle4t

BurF-fuxj n^^c CaiP_ HK^ Pty3o^ Transporter Name Tractor/TraHer/Roll-off it

Driver's Name Generator ,S<c.

Scfieduled Arrival: i , B . / i < i j g i . ^ j ^ Q / . O O r . J S L J / . - ' . - • . / . - '

Actual Arrival:

Receiving: Q'' 'initials Comments

lâte Time In Time Out

Arrived during Blackout? Y / N Notified DEC? Y / N

[~} Laaicer [ ^ Parmit Vriolation Q Piacarding/Vali. 1.0. Violation

I [ other (specify

/ -^Q- 'Bu ik to Landfill Q No wet line F l Flatt>ad Q Stabilization Q , jD ruma [ " ] Tanker [~] Transformers

Laboratory

Stabilization

Time In

Time In

Time Out

Time Out

# Initials Comments

Initials Gross Wt. Comments

Landfill Time In Time Out Initials Comments

Other

Aqueous Treatment

Time In

Time In

Time Out

TimeOut

Faciiitv Personnel (pieasa initial)

Initials Comment

Signature (NO Initials)

Smoidng or aating in proiiibited araaa

Failure to obey inatructions of facility personnel

Failure to wear appropriate PPE

Unsafe driving praciicas

Othar (specify)

Comments

Laaving trucic uitattendsd

Failure to diaplay overwaiglit flag

improper tarplng or detarpin

Overweigitt upon arrival

Secur i ty Guard Initials: \ (Indicating receipt of Wash Say pass, if necassary)

Orivar'a Csnunenls

u f k : . ^ » - . . - j - < ? _ . . . .^ r^-

yyDUMP^% ROLL-QFFq fmC^MNl^f^'frStB^l^r^KERS. * , S ^ - p ^ j = ^ M ^ £ D ^ ^ l S i ^ •

LOADS

TERMINALS

WORK ORDER #

•-rnî

4370 Packard' Rd. Niagara Falls, New York 14304

(SCO) 577-3002 PÊ-GHT SILL NC. (OFHCE USE ONLY)

TRUCK OWNER

TRUC< OWNER

DRIVER DRIVER NO., DRIVER DRIVER NO. •

TFiUCKNO. J TRAILER n o . TRUC<NO THAILIR NO.

STREET

l.f ...' - i ^ :

2IR CODE

STREE'

;TY STATE , ZIP CODE

.iDD'TIONAL iNFO./EQUIP. NEEDED ADDITIONAL INFO./EC.UIP. MEHDED

SPOTTED:-

r..,-; .\;.s;jl3^jE-aSSB:

I GALLONS ' a ; 3 0 X > | .=ICi<ED UP:

I "ARDS I j . • i I

.i?i>a'S.ii^j?;

ABRiVAL TiME .

AM

PM REL-. i .SE : liVlE

AM

,=M ORIVER .

THAILEF. EiViPT/ 'JPCIM ARRIVAL ri (if not, 3xp!ain bsiow)

)\?' ^/;E.•-.SL'RS;Vl£îT••(Ta^:•<a^s Only) •.

I

j . i i ^R iVALT lME .

. DATE . AM

?M RELEASE TiiViE ,

Aivi

_J 'V3S U >iC ! , , . - . , i TR.îLER :E;«irTY UPON CE?.i\RTUR

:;\iG;-;ES ' •ti;-r,otr-3>!piai!Vbalovv) • • D r'ES .MC

; CCMiviEMTS: ( E X F L i i N .4.LL DELVE'S .^.i\iC / C r i LCADIi- IS TiiWE). MVilViEN < S: (cXFLî iM - U L DELAYS AivID / OR LOADli'-iG . i™i t ) .

R'S 3iGMATUR£

SHIFREn'S SIGiMAfuRc:

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-pacing .^^tqin ! HOLDING TIME

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rlB.'. 12-00

5iJB9675099 Please type or pnnt Oo not stapl&

: . • , : - ..' STJWEOiFNEWYORK^ ; / • • * - ' / f r : ; i DEPARTMENT OE0JVIRONMENTAL ( ® N S E R V A T I O N

•* IVIS10f i t ) i^ ^ U ^ & Hf iZARDOU^M/i te i lALS

HAZARDOaS W A S T ^ A W E S T RO. Box 1l282ip, Albany New Yoric 12212 ;rf7;i5ysK=Jvr ?i!*iki

UNIFORQA HAZARDOUS WAS-RE MANIFEST

1. Geneiatoi^ US EPA No. Manifest Doc. Na

H\j \nm^m ig i31716 m \^\0\t P< IA 2. Page 1 of 'liifbrmation within heavy bold liiiis

is not required byTSderal Law. f -


sm ep^csiE cENtEs PO m% safes

4-. Generator's Telephone h feS^ r ^ ^ - 3 j ^ 7 5. Transporter 1 (Company Name)

7. Transporter 2 (Company Name) [ . • • ^ l ^ l ^ I'

k i u i | ^ ^ ^ o o 4 7

8. US EPA ID Number

' ' I - I 1 " I r I "^

"ia*f?*"lS

A.

NYB9675099

C. state T ranspo r te jS i y ' g ' Ô^ I • : ^

D. Transporter's Telephonefe*ft«'^^fefcjS<

E. State Transporter's ID m f i f ^ »

F. Transportet's Telephone ( • )

2

f r t o


csm cÊHicm. SERVICES, C i^c , i^m mLMSi m m mssL CITY m, t«i«ST ,

10. US EPA ID Number G. State Facility ID •J-

N-|Y ,g |@ |,» i-S-iB: |3„|S.-;r|T-.|f H. Facility Telephone ( ;: .'• . )

1.1. }J$ DOT Description (Inclucling Proper Shipping Name, Hazard Class and ID Number) .^. ' ^ . ' . ^ y 12.. Containers

Nuiriber TVpe

13, Total

"'iQijantity

14. Unit

WVVoI I.. Waste Na

.^tiîsmsKS iiif sTEi. •â.is, M.i3.-3. - •-. • EPA

J 7 i ^ i » P ^ \ ' STATE •,:

b. :%

«

EPA

STATE

I' I r I EPA

STATE

tf;. EPA

STATE

J _ l J. Addltlenal Descriptions for Materials listed Above

i y^d^<:y^ (h^ \Mh>^ \i> ^ \ I

K. Handling Codes for Wastes Usted Above

B D b. Ii D D IS.Speeial Handling Instructions and Additional Information

/4tic ^fi4^^z3H5g r A. nlnlyi Ik^mrj :fysy^7Ji7

L j

o o

16. GENERATOR'S CERTIFICATION: l hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled, and are In all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations. If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that Is available to me and that I can afford.

Printed/Typed Name Signature

.A. Mo. Day Year

J_LLiL )

17. Transporter 1 Acknowledgement of Receipt of Materials

Printed/Typed Name

JgJtH lAtJKCi ^.->~i Signature i •: ( ] /

T 18. Transporter 2 Acknowledgement of Receipt of Materials U U "

Mo. Day Year ,- ->• f i O I

\< \ H ( \ \ I

Printed/Typed Name Signature Mo. Day Year

I I I r I 19. Discrepancy Indication Space pancy Indication Space n

i ^ ^ , ; . , /;• -offZ-d y 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

PrintednypedName/ / .., _. / ' A • .,^_^. SignaturejT .-? ^CyAya hy^f i "U/^fcTf COPY 7-TRANSPORTER COPY - RETAINED BY,TRANSPORTER

c G

lAc; Trahjgpoiicr L o f ?rt > - ^ .-

CWMXhemicai Sendees, Inc.

ModerCity. NY

9m02 -?.:!e^-: Cubic Yards-^ '

Receipt it S y e / J - / A/y / ^n / .o

i - V •-• Li' -> ^ 7fa/7er Ucense Plate it and State!

Service Req. it Pnoffire#

f

Permit tt i •-? -^- ::

Transporter tteme_ Tractor/Trailer/Roll-off ft

Driver's Name

Scheduled Arrival:

Actual Arrival:

Generator

Data Tinfe ,' / / - ^"''

Oafs 77rne In Time Out


n Lealcer Q PertnH Violation Q Placarding/Veh^ 1.0; Violation

QrÔther (specify • ' ' \ . / . • •

1^1 Bulk to Landfill Q ] No wet line Q Flatbed Q Stabilization Q Druma [~] Tanker Q Transformers

l_aboratory

Receiving: . ^ ' • Initials . Comrpents

Time In TimaOut Initials Comments

Stabilization

Landfill

Time In Time Out Initials Gross Wt. Comments'

Time In TimeOut Initials Comments

Other

Aqueous Treatment

Time In

TimeIn

TimeOut

TimeOut

Initials Comments

Signature (NO Initials) Comments

Facility Personnel (piease initial)

SmoUng or eating In proliilitted araaa

Failure to obey inatructiona of facility peraonnai


Unsafe driving practlcaa

Other (specify) ^

Leaving trucic unattended

Failure to diaplay overweigirt flag

Improper tarplng or detarpin

Overweigirt upon arrival

* Security Guard Initials: (Indicating receipt of Wash Bay pass, if necessary)

Oflvai'a CoiniiMiita'

White: Records Green A Canary. Accts Rec Pink: Environmental Goldeoiod: Driver


.•STATEOFNEWVORK DEPARTMENT OF ENylRONMENTAUCONSERVATlON

DIVISION'^^ SOulaa HAZARDOUS MATERIALS

HAZARDdU#WASTE MANIFEST P.O. Box 12820jfAlbany, New York 12212

e • \ '"• - . ; J (Hazardous V feste ManKest 5/00)


I 1. Gtinerator's US EPA No. Manifest Doc. No.

r« . .?;i?.©-®, 0.0.-3.7. s. 0. «i 3...Genfieator:sJtone and Mailing Address

livS^ « a 7 - 3 1 0 7 •• 4. Generator's Telephone Number ( ) ^

I I I I I I I l{ idPlS

2. Page 1 ot Infermatlon within heavy bold line '' is not required by Federal Law.

' NYB9675027 B. Gêialor iOK r, t-ii, m >S«i

5. Transporter 1 (Company Name) ^ ^


6. US EPA ID Number C. state Transporter's ID j l ^ f ^ W W f ^ J ! ^ ^ ' l^"'.'j'^¥.'"'J!ilJ!!(Biii!' L

D. Transporter's Telephone

E. State Transporter's IDt ' •--SS^^S^ i

I I I I H Transporter's Telephone (,

c

[1 Ul


CWM CHSMICi L SERVICES, L .L .C. 155® H#U-HER ROAO ?c<D£L c i j y t4y, I-Mm

10. US EPA ID Number G. State FacllityjJD.rt

f-K. |g 1^ |4 |9 ,3 |,3 |S |6- ,7 |9 H. Facility Telephone (

7.IS ?3 ' i -8£3i


Number i Type

13. Total

Quantity

14. Unit

WtA/ol I. Waste Na

HSIARDOUS MM-STE, 50LED. N, 0.-5. 'TGTRACHL.OHCETHVta'iSJ (S ic 157) 9, m M 7 7

V T I

EPA

! i 4 lO iQ lO STATE

EPA

STATE

J L I I I EPA

STATE

J L I I I I EPA

STATE

± - L X J I J. Additional Descriptions for Materials listed Above

a'-tî-i...;;/V,},-r/.r-4v..l,,;^*:. I'S yT I " - ^

K. Handling Codes for Wastes Listed Above

D c. n u

E

n n IS.Speeial Handling Instructions and Additional Information

:yr;s^7yi

0) .,-E

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations. If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford. - _ _ _ _


!•- I ' I '-r- \'' 17. Transporter 1 Acknowledgement of Receipt of Materials

Printed/Typed, Name

i

Signature Mo. Day Year

I *• i ^' I ' l / I •••' l /



I I I I I


V

J i 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.


.•/ 1 I I- I I

COPY 7-TRANSPORTER; COPY - RETAlNED'BY TRANSPORTER / . . n ,.••

^ 2 B ^ B S H ^ O B I

W Transporter Loff CWM Cheinlcai Services, Inc. >': ' ModelCity.NY \ ,

'pM3>

G

G

G

G

c: J V '/. '-y : 'y • ' / y \ Receipt It Trailer Ucense Plate ft and State

C u M ; >£vcE5 . . - ^ " ' •

K, -r:

Service Req. # PtoOeff

Transporter Naine , ^

Pemut0

Tractor/rrailerôUipff ft 1 A ' - / ^ • /

r ? .C. .,:• Driver's Name

Scheduled Arrival:

Actual Arrival:

GeneraiDr

Oafa

Date TimeIn TimeOut


[~| Uaker Q PerniH Violation Q ] Placarding/Veh. LO. Violation

I I Otiier (specify

Receiving: ,.,JC1. Initials Comments

•r .' Y £.:

JT/] Bulk to Landfill | | No wet line Q Flatbed [~] Stabilization | | Orume | | Tanker Q TjansTorniarst-'

\ " " . . - ^ ^ . ; / ^ . ' - •

Laboratory

TimeIn TimeOut Initials Comments

Stabilization

Landfill

TimeIn Time Out Initials Gross Wt. Comments


Other Time in

C Aqueous Treatment

TimeIn

TimeOut

TimeOut

Initials Comments


Facility Personnel (pieasa initial)

Smoidng or eating In prohibited areaa

FaHura to obey inatructiona of facility peraonnel

Failure to laear appropriate PPE

Unaafa drhdng practlcaa

Otttar (specify)

Leaving truck unattended

Failure to diaplay overweight flag

Improper tarping or detarpin


Security Guard Initials: (Indicating receipt of Wash Bay pass, if necessary)

Drivat a Commants-

White: Records Gteen A Cknarv: Acox Rec Pink: F.nvimnfln«ntai r i n U ^ n m A ' T^nv

Pec-21-01 03:42pin From-CVM Chemical Services +7137540211 TrISS p.017/034 F-B31

_ _ . _ _ _ IgMSERVAnON'" •DlVISiar4 OFSbUO S HAZAROqU! i MATERIALS

HAZARDOUS WASTE I /lANIFEST P.O. B o x 1 2 8 2 0 , A l b a n y , Ne\ / YorK 12212^

CCWM

(HKIKIaM Wan* MUkknl SIDOI


,1. Qeneratora u s EPA Na ManBaat Doc, No.

M. IJ iR 10.18 ra l a 13 r 71 S I a , 3 | 0 i 1 |C I i T7 2. Page l of

1 Information within heavy bold line Is noi required oy Federal Law.

3. Genantor's Nama and Mailing Address FLEET BAl>4K ' 301 CARNESIE CENTER,PO 30X 206&

PRINCETON NJ, 865419 1 4. Generator's Talsphone N ^ B ^ r ^ Q ' ^ ' ^ ^ P ' ^

A.

NYB9675108 ^-°SES"B1'RT, NJ, 08750

1372. ^ t H G-rg-h i4t/e>g g 5. Transporter 1 (Company Nama) 1

HI3RWITH TRUCKS, INC.

$. US EPA ID Numb« r .

P , f f , D , l , 4 | 6 | 7 - , - l , 4 , 6 , 7 | a q Stale TVansporter's ID Y ^ < ^ 1 f

0 , Transporter's Telephon66:(8 S ^ ^ 7. Transporter z [company Name) 0. u s EFA ID IMUmCC t

_ l I ' • I T • I I

£. State TVansporters 10 F. Transporter's Talaphone (

9. Oesignaica Facility Name and Slie Address

CWM CHEMlCflL SERVICES, tl. L. C, 1550 BRLMER RORD i MODEL CITY NY, 1*187 !

It}, u s EPA ID Numc sr

N , Y , D , < a , 4 , S , 6 , 3 , 6 , 6 ,7 ,g

G. State Facility ID N/A

H. Facility Telephone ( ) 716 754-8231

11. US DOT Descrlpfion (Including Proper Shipping Name. Hazard Classand ID Number)., . 12. Containers

Num'iei' I Typa

13, Total

Quantity

14. Unit

WtA/'oI I. Waste Na

'•HflZflRDQUS WASTE. SDLID i N.OiS. r:: "* (TETRflCHLOROETHYilENE) (512157) 9 ,Nf l30Z7i T i l

EPA F00a

tDTiu 4i4)OiQio STATE

SPA

STATE

' I I I EPA

STATE 1 1 1 !

EPA

STATE

J__L J _ L _ L J. Additional Descilptlons for Materiala listed lAbove

a-i;gt-fAt:1nWcfrHto \&Jê 1 ^ Jit gfgi^=H>^/£Wg

K. Handling Codes tor Wastes Ustod Above

J d. J L. n d. n l5.Speci3l Handling Inatructions and Additional Information

< , ^ ^ CrO:^^^ ^^yX7yi\^ t t i)eWefy îfS-^^-p^l 1S- GENERATOR'S CERTIFICATION: ,{I hereby, deelara.thal Iha esnienls sf tru's consignr ent aro fully and.accuratsly described above by proper shipping name and aro

dassifiod, packed, mailed and ladeled, and ara In all iaspoett in pmper caiidilion Tor transisort by -lighway according to applicable inismalional and national govammsm regulations and state laws and regulations, { If I am large quai;tity generator, | conlfy lhal:I havg a pregram In placs.: to-reduce ma volume an I toxicity el waste generated to Ihs dagree I hava determined lo Be economically practicaBio and that I nave sslacteo me practicable meinca dl ireatrneni, sioraga, or disposal aim nuy avallaoie lo me wnich mlnimi2es iha present and fuiuro threat lo human hcaiin and the anvlronmant; OR If I am a'smaller geiiarater, I have mada a good.taiih affbrr to rninimiso m ' waste generation and select the best waste managomcnt msinod that Is available Ionia and that I can alford. i •

Pf Irrtodnypod Name meiase

icyywi m l ^ ^ -T iyLJr r^ ^Qfy^y^-Ma Day Tear

^ 2 ' ? i ? l O l / 17. 'rtanspaner i Act^^ywieagerrgfH or Recatpi or Matertals

icd Mame

c*-^<-'S

Mo, Day Year

le.Trancportora Acknomiodgemcntot Rocoipt Of Mniariala Printod/Typeo Name SIgnaiura Mo. Day Year

I I I I I 19. Discrepancy Indication Space lacrepancy indication Space / O

20. Faeilliy Owner or OpBraiar; Cartilicalibn ol ffeealpt of hazardous materials coverod by this r .anifesl except as notod in Horn 10.

v-^-iffe^ )^ --a ay -"^T^ Printed/TVpsa Name -sz &y ^:^t^ f ^ f i ^ ^ ^ .^âk^ /5:wM

C-QPY 1-DISPOSER;STATE - W f l L E D BY,TSD FACILITY

Recaived Dec-21-2001 15:40 '•Froiii-t7r6754tl211 To-ONYX ENVIRONMENTAL S Page 003

c

Dec-21-01 - 03:42pin From-CWM Chemica l -Serv ices

T r a n s p o r t e r Lo<y CWM Clwinlcal Seiylces, Inc. ModBiCiiy,NY

--+7167540211 - -

Rece ip t H __

' sfc9 Ra<^ » PttJilm *

' <ff . . . - J . d^rfirôtT'

Jiaihr 'UcaBsgF' lsaB::*.and Sta te : '•

scheduled Arrival:

P a f m i r '

T-1S8 p.018/034 F-B31

O/burV&rdls

Traetar/TraBer/Rol l -o l f t

Gene ia iw

i l 12

13

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h'a.

•d£.

753SD LS

01 339.90 L5

G

G

2

1

Qoiie Actual Arrival:

U/lMl 4^f(f^/^

Receiving: ^ Tnioai Comments

Data t i inain TimeOut;

Arrived during Blackout? Y / N [ , ^Notified DEC?„Y / N i. . "-:

n Leaker Q Panntt Violailon j Q Placardlna/Valt. I.D. Viotatiofj

[~1 Other (apecify ! ' • ••' •••••••• •-•:-'•

>^^/eul lc to Undf l i l { ^ No wet line I 1~] Batbad _ f T I S'abUlzatlon :: f ^ Druma \ ~ ] Tanker {~ ] Tranafbrmara

Laboratory I

Time In Time'Out Initials ComiTH fits

Stabilization

Landfill

Other

Aqueous Trieatnient

Timain

TimeIn

Timain

Timain

1 ...• 1 1

1 .

Time Out

i

TTfwajOcft -• r • • • "

i • • • • "

1

Timo.Out 1 , ..

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• • • • - " ; " • '

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Initials

Initiais -

Initials . : ,

- • -

• ' * '

GrosslML

Comrn. mfs

, . i ,

Comrn tms

Signature (NO Initials)

-

; - . ,..'.'.. Comments . -

. . . . • . • . . .

Comments

: • • - • • . •

* " * • • " • ' .

Faci l i ty P e r s o n n e l {pieasa initial)

Smoidng or • a d n g i a p reh ib i tvd araaa I " • " • ' • . " - . • •

Pai lura ta obey InatpietkuMi of fac i l i t y poraonnel a%raietl<

Fol lura t o waar apcirapr iaie PPE I-

Uitaafa dr iv ing prac j i ica*

r(apeeify)

L«Mi ing t m e k unanandad

Fal lura t a d isp lay ovanHeigtrt f lag

Improper l a rp ing or detarpin

Ovarwaig iR u p o n arrtvai

Received Dec-21-2001 15:40 ?rom-+71S7540211 To-ONVX ENVIRONMENTAL S Pa»e 004

Jf lN-15-2002 0 7 : 4 9 LEWIS ENUIROMENTflL

^3ea-81-Qr D2t23pm Fi-om-CWM Chemical Sarviaes I;' . T . r > - ^ ' 5 . f * S " " r.

DivistoM QP SOUS & HAZARDou; KMreniALa

'B9675117 HAZARDOUS WAS&i»ANlFEi§t ttypa orp^LlDonotatapla -; \ < P.O. BOX 12821^ Alban^-Mei if.,Yerlc i a ^

610495GS97 P.02

CCUH

I v n

UNIFORM HAZARDOUS l y A S T E MANIFEST

a."(aenaial<prs Natna and Mailing Address '

F l £ E T BANK _ ! 302 CARNOalE CENTER,PO SOX £ 0 6 6 PRINCETON N J , M S W A GaneiaiertiTolBptione N o S ^ ° 6 7 -

, 1 . QaneiBWrÔSSPANa

f J . T - . B - i i a ' i ^ . . a - H l i 3 i 7 - i 6 i g i 3

>itaatOaa,Na.

5. ^ n c p o i a r l (CompanyN»ma)

H O R M I T H I TRUCKS. INC.

2i'9i7:

7. i ianspanara (Company Name)

9. Deeignated Fadlity Name and Slto A d d r a a * ™ "

CUM CHETItCAL SERVICES, L L L . C . 1550 BflLMER ROAD | n Q K L P I T Y NY, 1A^187 J ' "

8j:->U5EFAI.P:NUfflbe'

4 i 6 i 7 ' , l 8s. l i s BPA 10 Numta

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± Information wimin Heavy cold ime is not required by Federal Law.

3, Ganerator'B Name and Mail ing Address

FLEET BANK 301 CflRNE6IE CENTER,PO BOX SeSB PRINCETON N J , 08540 4, Sanerator's Telephone r6 l3Br^B7-3 ip7

NYB9675324 SEfl GIRT NJ, 06750

C StaioTltinsporiBrs ID X G r ^ O f e 5 ' ~ 7 f ^ h 5. Tianspsorwr 1 (Company Nsimo)

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6. US EPA ID Nuniber

Pf f t 'D i i i 4 i<^ i - i r i i 4 i y r f t ;S r & Transporters laiepnona j ^ t p )^^^ 1 7 ^ 0 7. Trans;porljar a (Company Name; a: 'US.'EPA ID Nunibsr

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F. Tianspciner'& Telephone ( ) 9 . Opfdgnated Rteil l ly Name and Site Address

CWn CHEMICBL SERVICES, L-L, C' ISSQ Bf^LPIER RORD MODEL CITY NY. 14107 :

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Number [Type 13. Itsial

quanlily

14. Unit

WtfVol I. Waste No.

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"HRZORDQUS WRSTE. SOLID, N. 0,S, (TETRflCHLDROETHYLENE)(S12157) 9,Nfl3077, I I I

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STATE

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STATE

I ! EPA

STATE I I I

J. Additiyial 0< [aterlals listed Above K. Handling Codes for Wastes Usted Above

n n 15. Special Handling Insfructiona and Additional Iniormailon

MDC 5 R * 623430 FQI^ DBÎViiRY ON i £ / i 3 / 0 i ' "

- Rys^'yyji^ IS. GENERATOR'S CERTIFICATION: I Hereby deriara mat.tha.contanta..ol>this conalgnmer

elA9 *no<d« pacUad, msrkad ar\d tabolgd, and oraiin all racpocta In propar condition'tor ironaporl by hi; and stale laws and regulations, ' 111 am large quantity generator. I cenify mat I riave a program in placa to rcduco the volume, and l pmctlcsbin 5êl that I havo solactcd Uie pracEleai3fo method of Iroatmont, clorago, or dlcpooal currontl and ine envlronmont; OFl If I am a smaller generator, I havo mado a good -iailh effon to minimize my •* to me and that I can afford.

I .arg,.fully and accurately described above by proper shipping name and ara mmy according to oppiicacie iniamauonai and national government reguiaaons

xlclty ol.wasia gonaratod to the dagrsa I have detamilned to ba economically ' avaUoUe to mo -nhich mlnlmlEsa tna prvsanl and luturs ihroac to numan neaitn ê.gencrôn and select tna aast waste managemeni pnothod that is available

PrlnKsd/Typad fUnme

i^.TVansportor i /CsKnawlsiigemont of

MO. Day "rsar

I'^'g^f lyi ° / Roooipi o[ MaconQic

pnfltbd/Typed Name ^ / ) \ ^ l i MO. Tear Day

, r , - ^ / i ^ i C i y 18.TranEporT9r 2 AeKnowlsdgamonl of Rscelpt of Materlale

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' I ' l l ' IS-Dlacreoano Indication Space

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O-^ < ^ , S - 7 - i f J t i ^ . / / ^ . ^ ^ 20. Facility Owner or Operator: C^f lcat lon of racsipt of hazardous materials covered by this mat Ifest excapt as noted In Hem 19.

Prlntod/^pad Name

(3?/^rz>H_^ ^ : ^ . . . • d ^ ^ s : ^ T^T^yy COPY T-DISPOSER-;STATE --jyiAII lED B.Y TSD FACIUTY

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vstm Dec-21-01 03:43pm From-CWM Chemical Services

Transporter Loo: CWM Ctiemlcai Secvlces, Inc. Model cay. NY

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Receipt It JDaTer Ucense Plata It and Slate:

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Actual Arrival: / / " ) 3 Data

T-IBB P.020/034 F-831

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'Receiving; r.€_y Initials Comments

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TimaJn Time Out.. Initials Gross \fL Comments

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OtiMr (Bpaeity)

Leaving truck unattandad

Failure to diapiay ovonwaifllit flag


OvatweigM upon arrival

Secur i ty Gua rd Init ials: (Indicating receipt of Wash Bay pass. If necassary)

Oiiuai'a CciiiiiMiita

While; Record. a n a \ A Canuty: Aeeti Kt=, Pink: EaviranaKitUil ~ Coidcon d: Oliver

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Dec-21-01 03:50pm From-CW Chemical Services +7167540211

RDooEirorefflKcs-T-166 p.027/034 F-831

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^ UNIFORM HAZARi30US WASTE MANIFEST

HAZARDOUS WASTE MANIFEST P.O. Box 12820, Albany, NevYork 12212

CCWM IHaianlDiitWsslgManilui timt

1. Generaloi's US SPA Na Manliest Doc. No.

\i IT g CI Of ift a It i7 lA la ic) IQO in i ^ 1^ 3. Generators Nama and Mailing AddiEas

FLEET BANK 301 CfiRNEEIE CENTER, PD BOX £066 PRINCETON NJ, 08S40 i.. aeneiatoHe Telepnona i f i f t f e r S P 7 - 3 1 ^ 7

2. Paga 1 o(

± Information within heavy bold Una is not retûircd by Federal Law.

A.

NYB9675333 SEfl BIRT NJ, 08750

S. Transporter 1 (Company Name) 6. US EPA ID Niimbe • C. State Transporter's ID />/'/fc^tto>r/_ A / J ^ / f i r ' j J C ) , fH ^ / / ; j r 7 i Z . i V OTransponefg Telephone ' (' g [ X . ' l 2 c : i / ' 9 i ? y ?


9. Designated Facility iNlame and Site Address

CWM CHEMICAL SERVICES, L.L.C. 1550 BflLMER ROflD MODEL CITY NY. 14107

i i US EFAIONumbe-

' I ' I 1 I .

E. Slate Transponef's ID

i a us EPA ID Nuran .r I ' l l F. Ttansportar's Telephone (

State Facility ID N/fl

N lY ,D ,0 ,4 ,3 , i 3 a:& 7 9 H. Facility Telephone ( )

716 754-6231

n . u s DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 12. Containers

Number iType

13, Total

Quantity

14. Unil

Wt/Vol 1. Waste No.

^ f l Z f l R D O U S WASTE, S O L I D , N- O. S. C ' ' '^" , (TETRflCHLQROETHYLENE) t 5 i a i S 7 > 9 , NR3077 , - I I I

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J L ) T 4 i A i O i Q i o STATE

EPA

STATE

I I I L SPA

STATE J L I 1 I I

EPA

STATE

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C E n X

• n IS.Sposial Handling Insmioiions and AddHiorâl Informalien

IMDC SR# 623430 FOR DELIVERY ON 12/J,g/(3l

£ys^ry^<=X, i e . CENEHATOR'S CERTIP1CAT1CN: l ncroOy dociaro mat tnelcûntsnlB of ihla.'.t on lsra wnt are fully and-jiccuratbly dsscribod Dbova by praoor ohlppin^ name and oro

classified, packed, marked and labeled, and are in all rsspipcts in piupercdnditlon lor transpon b) highway according to applicable International and national govemmem rogulations and state laws and ragulallons. ' If t nm large qutsntlty ganorator. I csnlfy t h^ l have a pro^nur..in ploco ai ngia>,iro cha -.ciui io or' i toxicity at noaio-gr^norotod to tno dogroo I riavo dotortnlnod lo bo oconomlcally pracHcablo and that I have selected tho pracdealta machod ot treatms.'it, sloraue, or dlsposai sun- mdy availablo to mo which minimisoa Iho present and luiura Ihreal to human health and the errvironmant; OR il 1 am a smallar gmoiaL-'r. I riavo.madu a good-!a,m e;lon to mlnlml2s.rr / waste generation and select the Best wasta managemonl mcinod inat is avaiiaoie

_(°rna and that I can affotcU _ » _ _ _ _ Ma Day Year Printad/TVpad Name

17,TransDortBr1 Ackni

P r l i f t e d ^ e d Name

amem evReceipt o! Materials : ^ n ^ ^ . ^ J , ^ t-iignanJra

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Mo. Day Year

i/ ^^^2J{(^^/ iS.'Hansponor 2 AdffiowiBdgemam of Receipt of Materials Printetl/Typed Name . Signature Mo. Day Year

1 I I I I l_ 19. Discrepancy Indication Spaca

t : L t : A Z ^ ^ A L C J ' ^ ^ S ^ O ; ^ , \^j^7y;^ a f ô / 20. Facility Owner or Operator Certification of receipt ol hazardous materials covorcd by this nanifefst except as noted In Item 19,

Printod/Typo Signature

^ 2 ^ ^ Csud^r- h f ^ M J CO.PY 1-D!SPCfS.O..SJATE:--t/I.Al.t.ED BY,.XSD FACILIP/

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'Dec-21-01 03:53pra From-CWM Chemical Services

T r a n s p o r t e r I jocr -J CWM Chainical S e i n ^ i ^ , Inc. ModelCity.NY

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';;471'87540211 - ,:, T-188 P.028/034 F-831

O M c ' ^ r d s

Driver's Narfie

S c h e d u l e d Ar r iva l :

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Xreû/rraaat/RicUf'aiff^ .v'Il;:i' '-tij

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GaiMrafOr .£.15.01 ¥ ^ B > ' ^ 0 ) Data M ^ Data Tihteln '. JifnaOtip

Arrived during Blackout? Y / N ,, Nptifiwi DEC?-"Y ,/i N

[~| Leaker [ j | Pwmtt Violation '• [T^. Plaeiurding^Vek UO^

[~| Other (apecify ^

BUIKto Lansnn Q Nowati lna [~[ .FWI>WI> rTf-SiiaBlllzailon*-" [ " J ' p ruma Q Tanker [~| Tranalorntera

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Stabilization

Landfill

Other

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TimeIn

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TimeOut

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Comments

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Time Out.

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. - • • - • - - -

Commt nts

Comirii nts

••: Signatum (NO initialsf _;, '

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-fiir.c

Convrrenis

Faci l i ty P e r s o n n e i (pieasa initial)

SntoUna or aating in prohifaitad araaa . .

Fallura to obey Inatructiona of facility pwaonnei

Fallura to toaar appropriate PPE

UrukBfa driving pracdcea

Ottiar (apecify) • - ' -

i.aavina truck unattandad

Failure to dlapiay ovonHeiflin flag


Ovarwralgirt upon arrhral


ftivar'a Coflimantv

White Rccordi Green A Canary: Aceu Rec Pink: Eaviroanetiiil''' Goldtmo :: DHvcr

Received Dec-21-2001 15:57 .Frcm-+7r6f 54.0211 To-ONYX ENVIRONMENTAL S Page 001


£ ^ _ ^ STAfe/^F NEWYDRK * D u ' - i r l E N T OF ESjyiRONMENTAL CONSERVATION

r p " - . tllvlS'lGN OF SOLflD & HAZARDOUS M A T E R I A L S ' "

. HAZARDOUS WASTE MANIFEST P.O." Box 12820, Albany, New York 12212

cam (Hazaidota V/bsta Manltest 5/00)


1. Generator's U S EPA No.


FLEET mmi. [email protected]€ CENTER, PQ SOX 2SeS PRIWCETCSI NJ, SiB5m 4. Generator's Telephone I J a i ^ r ' ^ 7 ~ 3 t ^ 7

>4 ih m t m.st

Manifest Doc. No. 2. Page 1 of

L Information within heavy bold line is not required by Federal Law.

1^N^B9B?534^2 - ^ f ^ ' ^ mm m



6. US EPA ID Number

M^f fl,l <an5 IOI^..ifJI ^ r f l ^ l ^ Q r I C CDA i n M(,rr<Kar * • * ^ ^

C. State Transporter's I D W 3 U > 7 y 7 ' y j 8 ^

8. OS EPA ID Number

I r I I

D. Transporter's Telephone (•


I I I F. Transporter's Telephone

[1

[j


Qkm c £.»iicftL soy ICES, L.L. c. 10. US EPA ID Number .

H |Y |D |i -|-i» I? ,8 |3 |&


H. Facility Telephone ( )

11. US DOT Description (Including Proper Shipping Name, Hazard Glass and .ID Number)

: / JL

12. Containers

Number Type

'mmnmus wASTf.= SOLID, N.O.S, .-\\ (TETftACf^L0RCETH'YLEN£><3i2157f 9,m?.@77, i l l ;}

: • • — ' . •: L —

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mm STATE

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STATE

I I I I EPA

STATE

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STATE

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J L D D c

C ca u

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Jr/'iTyy^ / 16. GENERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are'


if I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined lo be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health ,and the environment; OR if I am a smaller generator, I have made a goodfaith effort to minimize my waste generation and select the best waste .management method that is available to me and that I can afford.

Printed/Typed Name Signature Ma Day Year

I • I f V l - V l -11


PrintedHVped Name" ./ ' ire

}r- ''f.;<-- . z d k U ^ I r l ^ ^ Mo. Day Year

I . i-î .1 n J . 'iTf 18. Transporter 2 Acknowledggfufnt ot flereipt c(f Materials fi^ /

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l^LLZ-Printed/Typed Name Signature Mo- Day Year


y(^^-<yy^^^_^ / i i . y ^ i ^ //

Y&6y?6/ ' ;.^.r U. yD-oo / 20; Facility Owner or Operator: Certification of receipt of hazardous materials covered by this ritanifest except as noted in Item 19.

Printed/Typed Name' ,

y A

Signature j^^^~Y MML COPY 7-TRANSPORTER COPY - RETAINED,BY TRANSPORTER,

/ • ; K ^ . - •'.^.- '• - -

lACy 'M^m^msy.. i-dum-.....///

CWR/i Ctiemi«»il, Model City, NY

i - ^ t t i ^ % g / 90'jnifl p y Trailer LJceBsp.ffêA and State .. jpJ^MeMand

Permit 0^ , Service Req. it ^„~ Profile #

: ^Sf^ Transporter Name-. § / V" -—7 Tractor/Trailer/Roll-off i t

Driver's Name Generator i i i f f < ^ ^ ' ^ - ^ •

Scheduled Arrival;

li^S4 ' ^30lE''ci:"

••> t M t l -•>'!•*•

O- iay\}X 3: 0 ie-£111:1

^6yy>o r Date

Actual Arrival: Tune

Data Time In Time Out


[~1 Leaker [ [ ^ Permit Violation Q ] Placarding/Veil. I.G(|inoIation

I [ Otiier (apecify ' ' < ;

• ^ ^

Receiving: - ^ — ' Initials

^

Comments

.. _ .. - 1

c G

p n Bulk to Landfill Q No wet line Q Flatbed ^ Q ^tabi l l^ t ion Q Druma Q Tanker | [ Tranaformara I .

Laboratory Time In TimeOut Initials Comments

Stabilization

Landfill

Other

Aqueous L Treatment

TimeIn

Time In

Time Out

TimeOut

L *

Initials

f

Initials

' .

Gross VW. / /

Comments

Oomments . ' ' ' • : ' . - . • '

•

TimeIn

TimeIn

TimeOut

TimeOut

Initials

Signature

Comments

••-'• .. f

(NO Initials)

_ , . • ' - ' -

/ /'v--V"V

Comments

'

r-

Facility Personnei {pieasa imtiai)

Smoidng or eating in prohibited araaa

— Failure Jo obey-Înatnictiona of faciIlty,peraonnei -. ^ ? v'J. .y

— V. . . : -- Failure to wear.aopropriatePPiE^>~;~,.; - A ' ' /

y^^-^ . ^ - ' i / ^ .^!;4JmMrieWiyingpractieaa^/' ' l ? ' ' ' y & ~ 7 y £ ^ ~ ^ - ' ^


Failure to diaplay ovarweigitt flag


Ovarweigirt upon arrival ,

- . . / •

iOther (sp«cify) £ .

^ ' MfH/^-f4p,ji yy f i i 'Ay f Securi ty-Guard Init ials: \ (Indicating'receipt of Wash Bay pass, i f necassary)

Orivar'sCoiiMMnto ••.-'

Wh;i» 3mtn4< Rrem A Caiurvr Aecu See. Pink-^ HnviraniBental ' '-' GoUeBitxl: Driver 4 \iK y'i / w

.+14 , lot staple.

DEPARTMEN^F ENVIRONMENTAL CONSERVATION , ^ , : . - -0 |<ts iON OF SCUD & HAZARDOUS MATERIALS

H A Z A R D O U S W A S T E M A N I F E S t P.O. Box 12820, Albany, New York 12212

ORM HAZARDOUS WASTE MANIFEST

1. Generator's US EPA Na , Manifest Doc. Na 2. Page 1 of

L

cam (Hazaitioua Waste ManHea 5/00)

Infbmnation within r , t » ^ ôfd line is not required by Federal Law.

3. Generator's Name and Mailing Address «

FLSeT Qfmi 3^1 cmmis iE CENTESTPO BOS s m ^

4. Generator's Telephone l ^ m & e r ' ^ ^ ? ' 3 ' ^ ?



6. US EPA ID Number

»4iyiaiQiOiO|Oi^,5i7i:2i^ 8. US EPA ID Number

I I I I I I I I I I

A.

NYB9675414 SEft 6.1 ST m , 55S7S0

C. StateTransporter'slD^y 4 .6Z ' I1 ,?«4

D. Transporter's Telephone ( f j ^ Q ) t i j ^ ^ j j



c o o


-cw?--! cr^ imc^-. SEftvices. L . L . C iS50 .R.iiLMES SGftD HODEL CtTY NY, iî®7

10.. u s EPA-ID Number G. State Fadlity ID

M , v p ^ r ^ ^ ^ P ^ ^ " P H. Facility Telephone ( )

•''16 ?:K(-623.1


Number Type

13. Total

Quantity

14. Unil

WtA/ol I. Waste No.

]-tf;7RnD0US WR5TE, s a j f i * W.G.S, / EPA

( T£7RAi:i-§.fitilJErHVLENe) «5l£t,57) 9, f-ift,3®??, r n ./<._ ^ J L T 4 , 0 | 0 P | C

STATE

-ten > z

I I

EPA

STATE

I I I I EPA

STATE

J L J LJ L EPA

STATE

J. Additional Descriptions for Materials listed Above

'301!. WITH TR{2C£ y -*. K. Handling Codes for Wastes Listed Above

H . -D n D

- 1 ^

"3 z


•C-C G f l &2343S> FOft SSLIÊRY Qti l £ / 1 5 / ^ i

S^sy'^yyd^ 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are

classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and rsgulations.

If I am largs quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated lo the degree I have determined to be economically practicatjle and that I have selected the practicable method of treatment, storage, or disposal cunently available to me which minimizes the present and future threat to human health and the environment: OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Printed/Typed Name

IT.Transponer 1 Aokno'.vledgement of Receipt of.Materials


I I I I I I '

Printeclijyped Name

1 a. Transporter 2 Acknowledgement of Receipt of Materials Printed/^petj ivjaîe ' '

Signature ^ i,'. Ma Day Year '••/ r \

.c.,-\. I i I Cl - I - . ; I ^1 j

19. Discrepancy indication Space


I I I I I I

'" / ^ ^ 'V'y-7., /") ^..'/ /? / 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest Printed/Typed Name.

exceot as noted in Item 19.

^ : . c / U J A y ( y (y:n.K^ Signature...-^., Mo. _ Day Year

y y ) / i : y / } y

COPY 7-TRANSPORTER COPY - RETAINED, BY TRANSPORTER

Transporter l-oo . , .^^ CWIM Chemlcai Services, Inc. ModelCity.NY

91413 J

/ y ^

CutsicYanis

• ' / \ y ' r y y ^ ^ Receipt i^ , ..

< L > ^ - ^ ' < • • . . • / , - • / j '

-jAx-i^îiAyLL-^'y Trailer License Plate # a n d State.

y

Serv ice Req. i t

'• " . ^ I ' V K . . v . :

P r o f i l e * P e r m i t * ' : : . . ' • :. y

{ s.- '-.:-i

Transporter Name

Driver's Name

Scheduled Arrival: >X- ry-<.

Tractor/Trai ler /Rol l -of f *

Generator

Data

Actual Arrival: Time'- •>,

j_VG<^3 Date T imeIn T imeOut


[ I Leaker Q Permi t V io la t ion Q Placarding/Ve| i . I . O . ^ I a t i o n

^

Receiving: r- ^.-Initials Comments

. _. 1 [ [ o t he r (specify j ' t

n Bulk to Landfi l l Q No in«t l ine Q Ratbed Q Sta i i i l iza i ion Q Oruma P ] Tanker Q Transformers

i

Laboratory Time In Time Out Initials Comments

Stabilization

Landfill

77mo In Time Out Initials Gross Wt. Comments

Time In Time Out Initials ' Comments

y \ .

G

Other

.. Aqueous Treatment

TimeIn Time Out Initials--' .. Comments

Time In TimeOut Signature (NO Initials) Comments


SmoMng or aat ing In proh ib i ted araaa

Fai lure t o o i j ey Instruct ions of faci l i ty personnel

Fai lure to wear appropr ia te PPE

Unsafe d r i v ing pract lcaa

Ott ier (apecify)

Leav ing t ruck unat tended

Fai lure t o d isplay overweigir t flag

Improper ta rp ing or datarp in

Ovefwe ig i t t upon ar r i va l

S e c u r i t y G u a r d I n i t i a l s : ; ( Ind ica t ing rece ip t o f Wash Bay pass, i f necessary)

Cr ivor 's Cof f lmants

-White: Records Green 3L Canary: Accu Rec r a ^ : ^vtronnienuii > ' > < GoM &DWK

Dec-31-01 03:27pm

H A Z A R D O U S

From-CWM Chemical Services r+n 67540211

HAZARI30US WASTE M ANiFgST P:6. BOX 1 2 8 2 0 , A l b a n y , ' N e w YorK 1 2 2 1 2

I

i

S E

1. (SonaraJor^ US EPA Na Manitast Doc Na.

gUSsTE MANIFEST N vT iR » ig i8 i^'i3 i7 |6 \Z |9 jO,6:^D, i ,1 ^jKOananlDrs.Name'.ond Mailing Address

i j leFcPRNEBlE CENTER. PO BOX 2066 rpRINCETON NJ, M S W ^ . : 4 . - a B n e r a t o i ' i s T a l e p t t o n o l « H a r i ° 7 - J X y 7 S. Ttansponarl (Company Name)

CLEAN VENTURE, INC. 7. Tiansportera (Company Name)

3. Deslgnalad Faculty Name and mia Address

CUH CHEMlCflL SERVICES, L.L.C. 1550 BflLHER RQHD HOOBL CITY NY, l4l07

6. US.EPA ID .Number .... - i j

8. US EPA ID Ndmber

' ' ' ' ' ' ' ' • I 10. US EPA ID Number

N ,.Y ,D ,8 ,4 ,9 ,B ,3 ;6.> ,7 .9.

T). US DOT Daserlplian (IndudinQ Proper Shlpplno Naime, Hazard Class and ID (dumber}'

^HflZflRDDUS MflSTE, SOLID. N, 0 .5 , ' CTCTRROiLDROETWYLENE) ( 5 l k l 5 7 ) ;3rNfl30.77i. i l i

",i»;,'S-ig(- 'i ) I i ; ; r : , i . a . r t j . U;'' •••

2. Paga 1 o l

1

T-270' P.013/027 F-989

IHazu*givn«aMaTiltai siao)

Intormalian within heavy bold Una la not roqujred iiy Padoral Lavir.

NYB9675207 " '^ lO 61 RT OUENUE BIRT NJ, 0a7sa_^,^

C Slate Transporter's ID

'' D. Tiansportor's Telephoni Mi B^&fiS E. Stale Tfantportat's ID

F. Ttansponet'sToIephona (

G. State Facility ID N / f l

K RidGty Telephone ( • 71S 754-8231 )

12. Containers

Number X^pa

I .L

13: Ibial

Quantity

4i4iô,o

I I I t

i4.Unii|

WlAfol waste Na EPA

roes STATE

EPA Jâ

S1ATE

EPA

V • ' • ' • • : • 'V-a-Ti i : . - -STATE

v D

I 1 i I

' -K' :" • . ' . ' . • • d u . .

EPA-

J, Additional Descriptions for Materials listed Above • ' r < > 0 \ ' l u * ! * * * * T T J K f i , '

J _ J - ' 1 1 1 1 STATE

D . • - • ' -••'i-->t, - • • - • . - - • 1 - i - t •• t • • d ' . • - . ; - ' r : - * - ^ .

I ' - l A .

K. Handling Codes ler TOBtas Listed Above •

C

E

J •» -1 16, Special Handling Instructions and Additional Inioimallon • ' , . . . . . . • . - • . .

MDC S R # fcZ--?.45Z . . F O R D E L I V E R Y ' ON , l i S / S a

- ' I '• * i _ ^ •' :• .-..•-liv't.S.' :. I "1,

'_i!!.rj)_ :;rll (iiil-i'

r e i

1S. GENERATOR'S CERTIRCATION: I herBby dgdarelhat tha canlsnts df this conslanmer classified, packsd, matkea and labeled, and oraln all respects In pmpercandlVon tor Iransponly hl( and state laws and roBulatlona. . . . . , • If I am laise quaniity genaralsr. I certify that I have a pmgram In placa la mdusa ma veiume'and.fi pracUeabla and that 1 have selsdod the practlcaBia mathod of irdatment,;itdiagB,"dr disposal iMriBntl and tha enviranment: OR If I am a smaller aaneiataf,.l.haye made a 0oocLlaUb.efbn.lD •nInimiza.rincM to me and that I can atlord. 1 .

T U - i s : j i ^ r ^ / ^ ^ f f f j -J i^T-^ i^ i r . t ara hilly and .'accurately dasolbed above ty pteoer sMppine iraniB'iind Aro hway aenniing'tD applicable Iniemslisnal and national government reguIaOons

Kiclty of waste goneiaied to iho dsgrae I have determined lo bo oconomlcally ' availabla to me which minimizes the present and futuno ihraatto human haann JSlessraiialion jwd icolc«< tha oaat wosta managsmonl molhcxl thai la ovallttble

lUionypeoNape ,. .

^ e m e n t y H i

- Ma Day .-.Vfear

i ? i 2 i h ' i T d f i7.itansponer 1 AcimovirfâmBnt ffRecalpi of Maieriafe Printei Bjrwped Namo

A / l S 16. Transporter 2 Acjaiowledaement ol Receipt ol Materials

Mo. Day Yaer

i / a ^ / i 9 i ^ i ;

Prinled/Typsa Name .Signature Mo. Day Year

I I I t I

<J7c 20. Fadlity Owner oi* Qpomtor: Coniflogtlon gf rocnlpt ui hazsirdaus matBrlalnf covorad byf^farmgR lIBst excepi as noted In Item 19. Printod/iyp^d Morne

'U MO. Day Year

CO PY J-DISPdSSR.-Sa>^ ED BY TSD FACILITY

Ci:..-'.- \-Hi

Reiielved Dsc-31-2001 1S:2S Frora-+7167540211 ;. Tb-ONYX ENVIRONMENTAL S Page 002

http://0oocLlaUb.efbn.lD

Deo-31-01 03:27pm From-CWM ChemicîH'Sefrvices''.; i,'.!::!."". • 1 Sivil .-.-.tl

••• +'7167540211 T-270 P.014/027 F-988

h l A l » ^ S S ^ CWM Chemlcai Servie^. Inc. ModelCay.NY

CuMsVanfe

y,-<f:

P y ^ ^ 7 ( ^ rVr^9M.y&r 7--;vf;.o L5 5 •-

Rece ip t i t Vafferueensei'latet'mtirStap..:

Service Req. It Pratiie # Pamtff # i -

TrmaportarUiuna Tractot/TraUer/Hgl

^ j c J ^ j ^ 6Lyc<!^y<s \y=2efrr^K. Orive/sMama

Scheduled ArdvaJ:

Ganorator

3S1SC LB G I 1.0 .1 no _ ^

i^jiiim Data

Actual Arrival: i3afa Tbna'ln-

^•sn> y n - m TimaOut

Arrived during Blaci<out? Y / N Notified OeC?LY.;î^N

r ~ i Laakar Q PwrnN V io la t ion Q Placwrdlng/Voh; t n l ' y i p l « t i o n

L J /Mher (apecify ,

^ Bu i i ( tO l .andfn i Q No w e t l ine • IJa lbad g j . S t e b l l b a t l o n : - ; ^ £ ^ j ~ ] Tankar Q T rans fo rmer .

Laboratory

Stabilization

LandRM

TimeIn TimaOut Initials Corfinieni.

Tima in TXmo OCJT ' Initials Gross W L Comments

Other

Aqueous Treatment

Time In

TimeIn

TimaO/a -•-

TrJTieOuir >•

- initials. -

- • • . • • - '•

u Iniiiala,:,.

:!>:"!

' - - " • " • • •

Cbmmenft

" . " • ' ^ J : :

Comment!

••'• '"fi

T imeIn TimeOut Sianati j reJNQinit ials). i~ .1.. I? Comments

Facilitv Personnel (p/wsa initial)

G Sfn^dng or MOing In pratiitHted areaa

Failurs 10 obey (natnicitona of facility peraonnai

FaOuro t o tnoar approfartata PPE

Unaafa Alving pracHcon

^(-pwMy>

Laaving truck unattandad

FaOura to diaplay ovenMigM flag

impropM tarplng or detwpin

OVMiMlght upon arrival

DiUa«'aCemil>a«ita

WMie Rccoidi Green *. Cinuy: Accu Rec

Received Dec-31-2001 1S:28

Security Guard Initials: (indiam'ng rmcefpt of Wasn Bay pass, rr necessary)

fink EoviraninenUl

From-+7167540211

GoUenrad: Ot t«er

To-ONYX EWIRONMENTAL S Paga 003

Oec-31-01 03i22pra ' '-". .;. • . . •»- ': '+71B-7540211

From-CHChemicai-^SerA ices-:. _ : : --;^ T y ^ J ^ ^ u ^

âs ' x \ . - : . « . ^ i -a ' i s !Sa !£S | : j ^J^PQl jS W A S T ^ I W A N I F E S T «;princoo not staple. P.O. Bbjt::f2820, Albany, N« w Y o r k 12212

T-269 p.011/027 F-99S

CCUI

(HttaidaaVnnaiinlba sna


1 Gaiieiatoi^ u s EPA No. • : , ; : , :: MBnlfaatDoe.Ntt • i - a s : : .• '<-••• - • — " I ' . ! •

N..ti ft

a. Pago 1 of

L Information within r»avy bold She Is net raquirad by I 'Mnal LSVK

3. CtanorBter's Nomo and Mainng Address

SPc«RNEBIE CENTER, PD BOX 2066 PRINCETON NJ, 085*0^^ , , ^ 4. aeneraiDraT6iephonai«Wfer^P^'"'3*yr ^

NYB9675216

S, Transportorl (Company NamaJ

CLEflN VENTURE, INC.

6.:USEPAlD'N(jmb)r, .4-: "^g^^r>g?^"

reKfaiepitbnîaiB 35|fr 7. TianspoftefZ (Company Name) • 8,v^S ERA JD NiHnb If \ .

I l l ' I I I I 1 .

e. SialDTransptnterslD

P. TtanapotwrsTBIepnone ( 9. OaslgnatodRicIlIlir Name ana Site Addross ,

CWM CHEMICAL SERVICES, L.L,,C. 1550 BflLMER ROAD >^ .. MODEL CITY NY, 141B7 .: V;1 ^

10. US EPA.1P Numl er G. Slaio Piadllyip. Ki>°«

L-| N i Y , D . , ^ h ^ ; . , 9 . . a ^ ^ ^ 7 ?

H. Badlily Tolophono I )

71B 754-8231

11 . US DOT Description (Including Proper Shipblfio Name. Hsuard Cla«» and Ip'Number) 12. Comainecs

Number (Type

ia.Totoi

Quantiiy

[l-4.Uni<l

VWVbl I, Waste Na

;<^5SSfflifl^^bl?<i?Sii?^.ei«»iti U'^ri.m F002

u. • • -^ •Oic* i f t STATE

;••? EPA

STATE

-cm I I I I , EPA

STATS JL 1- 1 , I, I

, £ " J j u r ••;.:£;.• EF»

STATE

J. Adaittpriai oe^pdons for Materiala listed Atjove J . ^ J .

K. Handling Codns for Wagtes UEieO ADOVB

_L^

-L iCTi:;-~''j •

ie.apBdai Hanoiing Inetmctlons and AddWontsl Irrfbrmailqn h o c SR* 4 2 ^ C f l 5 2 - • 'TOR' DELIVERY-ON 12 /2 ( / 0 l

16. GENERATOR'S CERTIFICATION: I nerBby declare Ihat tha.contarits.tj this ednswun? x jm««% ond «=ucKGty aeaoitied abova by proper snipping nama andjro dassHIad padnxi, nwlisd ana laDateo, and aro In all reapscips In pmpar cpndlllbn for transport by hi Itwsyaccaidlns to sppllcabla Intsmaliisnal and natloiwi gsrammsnt roguUniena and Btala laws and regulallons. '"• • " • _ - ' If I ara tai^B quantity ganaiator, I certlly tnat I have a ptogtam In placs^to i ^ u w tho voIiima'*Kl:i iMelly. pi waste genatatBd lo tna dcgtea 1 trara detamilned to ba eeonomteaHy ptadicafala and thai 1 havo aelecJod the pjacBcaBla method oi treatment, Btomga, or dlapoBal cunant ravaUobte to me which minlmieos tha otosant and fumr* ihrasi le human hPMjtn and the anvjmnmani; OB If I am a smaller penaistor, I have mada n BCK<.(aiih.Bffon la mlnimbo mr v isto-generanon and select ths bast waste management meinod that Is availafale lo mo nnd mai I can attoM. •_ _ • - , '_

PrIntod/IVpod Namo .;,.,.. ,:

17.Transportorl AcJi^WledgSI

Prtn»dn"v

s f i ^ i o r

Mo. Day. -rear

; < l 2 i i ] ' i \ 0 \ l Fieeolpi of Materials

portorS AotaiowledgeiSmof Ftecalpt 0(:J4atarials

luia Day "rear

Prtnted/TVped Itomo SIgnatiwa Mo, D B / Y6ar

T9. Olseii>pBncV (ndlatioi

w^ - - , I I I I I -

aO-'FaSlity t^wnerotppormoi:c^r<illcallon of Vocoipfof hantaous maiPflaigcpverga pyttlls man 'est-axcept as noted In Item 19.

Primad/Typed

'MLM>(l-QAA>yL <yL> Slgtiatuj

'yyufdA.:^.. y^m C O P Y 1 ^ l S P d S E R ; S T A T E - - M A I L ^ S - B Y T S O I F A C I L I T Y

:-s v : l i

•,J-.:ii.-,.ui:-

; I • : • ! ? • . , ; ;

Received D9C-31-2001 15:21.~ Froiii-+71675402T1' To-ONYX ENVIRONMENTAL S Pane 0D2

Oec-31-01 03i27piii From-CWM Chemical Services

CWM Chemical Setvlces. Inc. ModelCity.NY

-+71-67540211 T-270 P.012/027 F-999

RqceiptH,^.— Traaer'Ucanse'PtatafBndSaia^sK

SetvicB Rea.» PtoOla * ' • -pimiiiWj;- ~. ':

Tia/aoprtarNama . tiiactor/TrattatyRofhaifr*

'S^M C/ Wf . P K ^ r 3cit^M, Drivel's Name

Scheduled Arrival:

^ . . I J ••••• j s ; ^ - ) »

jSofMuofer,

-euofeytutis

. 2 / ; i O ;

/ - JOV i~3 :- i

Date

34SSC LB G 1

i2./2D/01 ^ ^ - ^ ^ a Time "•'

Actual Arrtvai: ^#''#>S¥^^"

c

Oafa 77/ne /n Tana i

A r r i ved d u r i n g B lac i tou t? Y / N Nci t i f ied D E C ? Y / / - N

p i Leaker Q Permit VMaikm Q PiMavdins/Veh. l & vtoistion

Q Other (apecify . ,-.

' 'y^ \ - - .ffecelving:, ic Initials Commanta

Bulic to Landfill ^ No tmet line , i ; Q Flatbed - pâ^^StablUzattorjr^^ , " ^ Druma V ' T " ! Tanlcar f~\ Tran»form«f»

ir.;--,:-> , T ' ' i - ' '

Labora to ry .;: ''' -, ,

TimeIn TimeOut KlnitKkls Commer.ls

stabilizaiion

LandliU

Other

Aqueous Treatment

G

G

[

TimeIn

TimeIn

Timain

Timain

77in» Oirfc,;.w iwi

TimeOut -V

" • - : '

TimeCia

Tuna Out

/•.' - i j i " ,• • ;,:>, i ' , ic :^

'.".' ^ •>; .-1 pr ystteto ^;, c

V • • • • " • • , : ; ; - ,

Initials-- J ~ -

' = ^ v . ^ . , . ' •"

l n i t i a l s , i . . ; ; . c

- -

.-?-.wi-..-. . • *

Orruam

f :....'; ... ' C&inrn<anS

:' yy.y,z Qcunmen s ;

SiignatoB 7NO:iniii8isjiii»-;

Cammems

!- • - J .•

• ' • • *

Comments

Faci l i ty P e r s o n n e l (piease Mbai)

Smoidng or eatbig In proltcbiiad an«s

FaBure to obey inairusilons of ftall lty peraonnat

Faflura to vaaa, appr<»7rlBte PPE

Unaafe driviitg practlcflB

Oltier (apocHy) .. :

Leaving trucic unattai>ded

Failure to diaplay ovefwaigM flag

improper tarping or detarpin

Ovetvwlght upon arrtvai

Security Guard Initials: . (fn^lcattng'reeaipt or Wasn Bay pass, ir necessary}

Ortnar^

wtiias tUKoiOi Cicen * Cuuiy. Aou ftce. " Pisic: EmweiiiiKnul '~T:';! CaideBnid:;Cdvcr

Rscaived Oec-31-ZOOl 13:25 ... F rom-tri 57540211" •?:;;r^.V To-ONYX ENVIRONkENTAl S Page 001

r

1 o

1=

3.V Generators Nams and Mailing Addiaas I

^ S f ^ R N ^ I E CÊR,PO QX 206S PRINCETON N J , 0 a | * a ^ . ^ . .

•-g"i5enemtci^TBlephonel6ftargg7-3l:97

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^^^ycM^^cT .%:^r/ i |s^;sFgs^!Ê - M^{Lil;Bt:rrSD IÂCILITY

Received Deo-31-200l 15:10 Frora-+715754021-1 •• Tb-ONYX ENVIRONMENTAL S Page 001

[— Dec-31-01 03:12pm From-CWM Chemical Services • r A » J S B R m -" " •—=^=«-«—••- • -g , . r-

^M.Mmu'TKSfli ^ CWM Chemical Services, Inc. Model Ciiy, NY

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White Reconli CRCD * Canmrji Aoas Res," Pink: EDwoniaeiilUl '^ '">' Goldmred: Q -

Received Dec-31-ZDDl 15:10 From-+n5754[iZl-l to-ONYX ENVIRONMENTAL S Page ODZ

Dec-31-01 03:12pm From-CWM Chemical Se rv i ces f - ^ ' i t e j ... J-716Z540211 1

. ,r 6 9 6 7 5 3 6 9 .;.. HAZARobuiWASTE ? IANIFEST fjeaaa^ or prinL Do not staple. I ' R-0; Bpx 12820^ Albany^gy rVbrk 122t2

T-268 P.007/027 F-999

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WASTE MANIFEST - W i j ,ff iiy a iB .a .3 i7 ifi .BT ? JQ, 3. Generator^ Nama and Mailing Address , . , F L E E T B A N K J 3 0 1 C A R N E 5 I E C E N T E R , P O ^ O X 2 0 6 6 P R I N C E T O N N J » 0 6 5 4 0 ;!

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HORWITH TRUCKS, INC

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2. Page 1 ol

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^ ^ ^ CCWM (lônowWuwMa^M sreo)

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NYB9675369 SEft SIRT NJ, 08750 J L l } ^

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CWM CHEMlCflL SERVICES, Li.L.C-1SS0 BRLMER ROAD HODEL CITY NY, 14107 ;

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N ,Y ,D ,0 ,» ,9 ,3,3Vst '£,7 ,9 H. FaciSlyToIephans ( ^ )

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MDC SRf 6a3SS2'^0R DELIVERY ON 12720/01 i - , - -> — .........

16. ( S E N E n A T O R ' S C E R T I R C A T I O N ^ - ^ noraisy daefâ Ihat-lhv esniiuitii of Ihis oocBign nent ara fully And:i>ccum<Bly doscrlbod abova biy pioper shippinp name and are dessined, packed, maikad and labeled, and oro In all respecta in proper coniHtlon lor tranEpdh b; highway accoruihg la appllcabla Intemallonal and national govemmant rogulaiions

' ana Btato lnv»s arm raguiauons. I I I am lame quantlly generator, I cartlly that I have a pingiam In piece to faducn the vdluma ai d tDxlelty of waste sonoraiod to tho degree I hava detamilned to ba economically praciicatila and thai I have selected the prectlcabla mstnod ot ireaimont, storage, or disposal curi iintly available to, me which minimizes the pmsont and future threat to human healtti atto tne environmani; tbn ir I am a smallor gonerator, I nava;,r7iBdc .a good blirL^rrort to minlmlso p y ^rracto gonamtlon and ooloat Uio boot vroolo monajonionl molhod Ihat 1* availabla tome and that I can afford- .. •

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19. Discrepancy indication Spaco

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20, Facility Owner or Operator: Cenlllcatjon of receipt of hazardous materials, covered Dy mis nar.iteal except as noted in Item 19,

. ^ 7;fc^ /J -06 f Signature,

cbt=y.ri:-mspa5ER;2TAT|:|:MMLED BTTSD FACILITY

^111: ; ) • 1

Received Dec-31-2001 15:10 Fron-+7167540211 To-ONYX ENVIRONMENTAL S Page 003

Deo-31-01 03i13pra From-CWM Charalca,riSS.erVices:.; . • \ : . ' .,.,; . . . ; + 7 1 6 7 5 4 0 2 1 1 " T-268 P . 0 0 8 / 0 2 7 F-999

%,J^yf!MSSI^M CWM Chemical Sertfteai. inc. , _ A - L \ cubsaybmo Model cay. NY

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smoking or aating In p«ahibltad araaa ^Leaving tnidk unanandad

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Faiiiir*tewMrappro(miirtaPPC Improper tarplng Of datarpin

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G WNte Rceanis G i m A. C U U I T : ACEU Rce, Pint-Ea»ironiDCTi»i;>S* Coldeaiod: D iver

Received Dec-31-2001 15:10 ' Frora-+7167540211 - :;.•;: To-ONYX ENVIRONMENTAL S Page 004

http://SarvicaReq.lt

NYB9675171 Please type or print Do not staple.

U C f A H I MCIN I U r t lWIMUMIVl t lN lAL OUNatzMVAl lUIN

iaiî6N':d;*soLW& HAZARDOUS MATERIALS

HAZARPOUf WASTE MANIFEST P.O. Box f^820,?Albany, New York 12212

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(Hazardota Waste Manifest S/DO)

UNIFORM HAZARDOUS , WASTE MANIFEST



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5. Jtansporter 1 (Company Name)

7. Transporter 2 (Company Namef


Dm CHEMlCm. SERVICES, L..L,C.

W^WL CITY MY, lAJt?

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I I I I I

I I I I I I ' I


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11, us DOT Description (Including Proper Shipping Name, Hazard Class and ID Number)

Information within heavy bold line Is not required by Federal Law.

NYB9675171

C. state Transporter's ID " i "f 3 i . ^ ^ ^ ^ j - - /

E. State Tfanspor/er's ID

D. Transpojter'pfq|ep^hpn> ( - , / . - ) - C i - ^ . . i ( L ' ^



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12. Containers

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K. Handling Codes for Wastes Usted Above'

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b. J, L 1_—JI L D n IS.Speeial Handling Instnjctions and Additional Information

.** CfLS&i^ ' l ;Pysy.^<y7y? 16; GENERATOR S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are

classified, packed, marited and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations.

If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if 1 am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Printed/Typed Name SIgnattjre Mo. Day Year

I ' P I ' I ' r ' I • 17. Transporter 1 Acknowledgemenfof Receipt of Materials

Printed/Typed Name Signature Mo. . Day Year

I I I I I 18. Transporter 2 Acknowledgement of Receipt of Materials


' I I I I I-19. Discrepancy Indication Space

;.Jc 7 . / b y / , y .,:d!£. yy yy , a /

^ \ ^.y^-. .a ~ .-7d / 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.

Printed/Typed Name Signature ./< Mp. .. Day Year

COPY 7-TRANSPORTER COPY - RETAINED BY TRANSPORTER

MVL Transporter Log *•-CWM Chemical Services, Inc. ModelCity.NY

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12/20/01 yf7y,(y / ^

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Date Time In Time Out

Arrived during Blacl<out? Y / N Notified DEC? Y / N

r~] Leaker Q ] Permit Violation [~| Placarding/Veh. I.O. Violation

[~| Other (apecify 2

m Bulk to Landfill , Q No wet line Q ] Flatbed Q Stabilization Q Druma Q Tanker Q Tranaformera

Laboratory ,

c TimeIn Time Out Initials Comments

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Landfill

Time In Time Out Initials Gross WL Comments


Other Time In TimeOut Initials Comments

CAqueous Treatment

TimeIn TimeOut Slgneture (NO Initials) Comments

FaciUty Personnel (pieese initial)

G

G

SmoUng or eating In prohibited areaa

Failure to obey inatructiona of facility peraonnai

Failure to vwear appropriate PPE

Unaafa driving practlcaa

other (apecify)

Laaving truck unattended

Failure to dlapiay ovenMeigtit flag



Secur i ty Guard Init ials: (Indicating receipt o f Wash Bay pass, i f necessary)

Diivai 'a Coninianta

White: Records Green A Canary: Acctt Rec Pink: Environmental Goldenrod: Driver

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Dec-31-01 03:15pm From-CWM Chemical Services +7167540211 wi..^ n i 1 • i,,i_ji I WI h.1^ V t( iwiîmi. i ' i I ' t i . V. .î<<OCr\VMi l U N

M V D Q C " 7 C : 0 - 7 0 " DIVISION OF SOUD & HAZARDOUS MATERIALS

T-288 P.009/027 F-999

Piesiso type or prinL Do not staple.

HAZARDOUS WASTE MANIFEST P.O. Box 12820. A lbany, New York 12212

CCWM


3, Generator's Nama and Mailing Addrass

FLEET BfiNK 3 0 1 CARNEGIE CENTER, PQ BOX SGI66 PRINCETON N J . 0 8 5 4 0 * . Gencratorâ Telephono if if l i f ibr 9 ^ 7 - 3 1 ^ 7 5. iransporl9ri (Company Nama] •

1. Gonaraloi's US EPA No. Manliest Doc. Na

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ITH TRUCKS. INC. 'tansponer 2 . (Company Name}

9. Designated Facility Name and Sita AOdresti

CUM CHEMICBL SERVICES. L.L-C. 1550 BflLMER ROflD MODEL' CITY NY. 14107 ^

S. u s EPA ID Number

P i B i D r l i 4 i f i . 7 l l . 4 ' i a i7 |f l & StateTtansportor's ID y L . - ^ 6 0 S * \ ( " ^

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J L L . I I I I I I I 10. US EPA'ID Numbe

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%lflZRRDaUS WASTE. SOLID, N. D. S, ' " '" " (TETRflCHLDROETHYLENE)(512157) 9 . N f l 3 a 7 7 . - E I I

2. Papa 1 of

J_ Information wcihin neavy bold line is not required by Pfedoral Uau,

NYB9675378 SEfl GIRT NJ, 08750 ^ '

0. Tianaport9f^ Tolnphon^HB £611 " E g g g

£ State Traimporter'te ID

R TraiKponar^ TelaphonB (

G. State Pacifiiy lO

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716754-8231 )

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K. Handling Codes lor Wasaog Ltetod Abovo

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IS.Speeial Handling Instrucdons and Additional Information

h o c SR* 623652 FOR DELIVERY DN 1 2 / 2 0 / 0 1

IB. GENERATOR'S CERTIFICATION; I nereby dedam that the contenis of this conslonrner classHlea padnd, marked and labeled, and are in all rospscts In properconaitlon br iranapori by hi; and stale laws and regulations.

; aro fully ond aeeuraiely doscribod aboro by proper snipping name and are iway according to applicable Intamational and national govemmant rooulallons

If I am larga cântliy genomtor. I certify that I have a program in placo to reduce iho volumeanct t> xidtj- r)\ wasn gengrutsd lo ths dogroo i hmo dsiermlned to oo sconomiesiiy ptqctfcaoia and ihat l.havo salacted the practicable memod of trDatmanl. sioraga, or disposaicuirentl • aiiaiilable to mo which minlmizaa tha present and tuluro threat to human heallh and ina enviranment: OR III am a smallar gonarMor, I fwvo madB a. gooa.falUi often lo minlmiaejiy » 15:3 gcncratisn and Boica the best waste management method Ihia Is available to me and thai I can aitord.

Printeonyped Nama

17. iiansporTBr 1 Aqltjôwledgeyont of Receipt o:." Matariala

i iSislnalu^

• v ^ < r w j / i ^

Ma Day Year

pnmeanvpeo Nami

'S'^gyc^^^'^,"!)^ / L / D £>igriaiure

IB.TI'ansponerZ Acknowledgemoni of Receipt ofMatarials

Mo. Day Year

\UZ\M.\aa PTimed/Typeo Name Signature Mo, Day Year

I I I I L_ 13. Discrepancy indlcalfonêasa

yJyy -y^^, -Kjyzyy^t^juSTj

so. Fadlity Ownar or opcraior: coniTicaTion of rccolpt of nazBTdoua maiedalaeovereo^y mis man fcst except, as noted in Item 19.

Prinlcsi/Typ"

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J^r^\£>Ay COPY 1-DISPOSER STATE - FACILITY

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Oec-31-01 03:22pra From-CWM ChemitJal- Services

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/ ^ improper tarping or dataipln

:•- Ovanwalght upon arrival

O H M T (apttei f r t

Security Guard Initials: {inaicating receipt o f Wash Bay pass, i f necassary)

wtiiieKxow4> Ciem A Caiuiy: Acax Rec Pink: EnviivniiKmai Tr^" Goidearod: D .ivcr

Received Dec-31-2001 15:21 FrQra-+71675402,1,1 To-ONYX ENVIRONMENTAL S Page 001

NYB96751,89 Please type or print. Do not staple.

o l / M C W r i N C W V i w n i \ j ;

4t^ . DEPABTMENT OF EIÎRCINMENTAL G"0NSERVATICN i ^ - -BftasiON OF SOLW & HAZARDOUS MATERIALS

HAZARDOuiwASTE MANIFEST P.O. Box 12820, Albany, New York 12212

IS^ff CChm

(Hazanjous Waste Manifest 5/00)

UNIFORM HAZARDOUS WASTE iVIANIFEST

1. Generator's U S EPA No. Manifest Doc. No.

IJ ^ iJS i 0 i @ i 8 | . 3 i ? i 6 i @ i 9 P i l i C i l if

2. Page 1 of

X Information within heavy bold line is not required by Federal Law.


FLfET ^SfMH M l VmH£Sm CHMT€:S,PO 8C5X S©&£ vniHCEim m; #854® _ ^ . 4. Generator's Telephone fyKmilr ^ ' ' ~ 3 » ^ /

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.NYB9675189

6. US EPA IBilêgbe^ # i? JT 7 Y

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B. Gg^to^sjlg^^ 1 ^ , 3875®


fi-C. state Transporter's ID ' ^ i ,» ' ^ i ^ ^ ' i ^

D. Transporter's Telephone ( 7. Transporter 2 (Company Name)^ 8. US EPA ID Number

. I I I I I I I I I


-1. . I F. Transporter's .Telephone ( 9. Designated Facility Name and Site Address

155® &ftL?«R SDJ^-HOSEL CITY M¥., i41®7


N |V ,5 ,S ,4 ,3 ^ 3 |& ,€» |7 ,'3


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71 & 75VSS31


Number Type

13. Total

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•Hfl:caf?DGy3 WASTE, SOL.r!>, M,£l, S. <TSTf¥S:iHU3?S3ETHYLeC)i'5.i2lS7> % W k m n , I I I

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• i s , ./ •"> ^ w •:ff;,f5DTi- • • ^ -,.;. ^ .\ : ... :s.r' .t/..::5>'7'^ GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and Sbcurately described above by proper shipping name and are classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according'to applicable international and national government regulations and state laws and regulations.

If I am large quantity generator. 1 certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method pf treatment, storage, or disposal cun-ently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Pnntgd /Typed N a m e » "t -• ( ."V L . . . -

Signature , , , /

•••,WMi*"> i J-'.îr ' H » , „ J Jt^JWKK

Mo. Day Year

I ' l"~l • I M •-! -17. Transporter 1 Acknowledgement of Redeipt of Materials 1 / • ; . /


G I ' " ' l ' ] ' ' \ ' I • 18. Transporter 2 Acknowledgement of Receipt of Materials


I I 1 I I I

19. Discrepancy Indication Space '

^ 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in Item 19.


I I I I I I

G-OPY 7-TRANSPORTER COPY - RETAINED BY TRANSPORTER

1A£^ Transporter Log '-^r '-- CWM Chemical Setvlces, Inc. Model City. NY

: 3 ± ^ O D n ^ X ' i a

Receipt ft Trailer Ucense Plate * and State

CutilcYards

12/20/01

774S0 LB G 2

Service Req. # P n O l e * Par rn^*

Transporter Name Tractor/Trailer/Rolt-off * .i.is31

Driver's Neme

Scheduled Arrival:

Actual Arrival:

GenerafDr

32120 LB 6 I

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Date Time ,«.

G

G

Date Tinie In Time Out

Arrived during Blacltout? Y / N Notified DEC? Y / N

n Lealcer Q PermH Violation Q Placarding/Veh. 1.0. Violation

I I Other (apecify ,_

} ./O

Receiving: J/i9 Initials Comments

f X j Bulic to Landfill Q No wet line ^ Flatt>ed [ ^ Stabilization Q Druma [ j ^ Tanlcar Q Tranaformera

Laboratory TimeIn TimeOut Initials Comments

Other

Aqueous Treatment

Time In TimeOut Initiels Comments

TimeIn TimeOut Signatum (NO Initials) Comments


Smoking or aating in prohibited areaa

Failure to obey Inatructiona of facility peraonnei


Unaafa driving practlcaa

Othar (apecify)

•.eaving trucic unattended




L Security Guard Initials: (Indicating receipt of Wash Bay pass, if necessary)

Stabilization

Landfill

Time In

TimeIn

Time Out

TimeOut

Initials

Initials

Gross Wt.

Comments

Comments

Ortvar'a Commants

White: Recordi Green A Canary: Accts Rec Pink Environmenul Goldenrod: Driver

Jan-D?-2D02 14.-53

Jan-I17-C2 IZHZpui

Froti-ONYX tXVIiJONMENTAL SERVICES +2155338758

FrsBi-CHW Chsffllcjl Se.-vlae: • +71S764BJI1 • i "''ciwSIONtJFSl3ClD4TVU>flDOUSMiTERWkUS

NYB9575225 ; HAZARDOUS WASTE M/.NIFEST Piea.owoeor5rint.DonotsiaDie. P-O. BoiC 12S20, Aibany, Nay fA jp r | 9^^2

T-902 ' OGZ/GO; F-55r

T-42; P.002/ -05 F-zea

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UNIIÔRM HAZ/,ROOUS V^'ASTE MANn=ÊST

; j T. Gencraw/^ US j

\ \ i ,riR ,<a ,e,e, , g , 3 , 7 i f e i a . , 9 | f ^ < ; i , ^ , ? , 4 3- Gen*raro?'B Name and MaB119 Aedreis FLEET BfiNK i ' 301 CflRNESIE CENTER, PO BO: 2eS6 PRINCETON N J . 9a;S40 * . Ganarzi-tQf'V T o , . p ^ n o . > f e g a r g < Q 7 - 3 I F

6. Transpor:ef 1 (Ccmpany N:im»)

IXEflN VENTURE. IWC. 7. Transoorter 2 (Comoany M imo)

S.- US ePA ID Numbar '

N.j:,(a..,g,a,eia 2,7,1,9,3 8, US EPA lO fJumCer

3. Oeslorâiad Faoli :y Name ana Sits AdSrasi

CUM CWEMICnL SERVICES, L. l i .C . i s 3 a Sf^LrtER fraoD MODEL CITY NY, J,4J87

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N Y D 0 * ,9 ,a 3 5 5 7 9 I L_t L

n . US DOT Ocscrlpton (incl joing Proper Shipping i^**na. Hajard aass ana IC Number)

"Â^f lRoous WOSTIE:. S D U I D , M. 0. S . (TETRaCHLORaETHYLENE) (5121571 9, Nfi387T, I I I

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K. Handling Coaeg lor w«. !«s Uiieo Above

D a IS.EpoclcJ H3ivti |ng tnct ruatont ana Jujdtiionul Inlorrri^non

MDC SR# u I FOR DELIVERY ON i 2 / g t i / - « l

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IC . G C N C F I A T O R ' S C E M T I H C A T I O t f ; i rujfotj,, aociara *>« i h^ ooptont: ot m^ rorijlsntiu rH aro ;ul)y snjJ accuraieiy d « « t * c d abovo By pi par shipping nama and are aaislrieo- pscliea. markati and '.ahabd. »nd are ip 311 r a i p o n : "Ji propor camiUon for Iranspon By h Btway iocord'ing to appUcaDlo Imarruiiional ana ra- anai gommmoni rBouoOonj aru3 itata lawa ana rsguiutlons. ;

i n 3m iars<9 qunnuiy gon j/oior. | can^r ">« I iha/o » p iopnm :« p lu ia » •cOuce ina vclurtfcand iDJtldiy al wBs;o gcnaatea to ttw fiapreo I have d. icrmined u> be wonot^ ia l ly PTac(.<3Dlo and ttni I ha«i. iolecied lhopr3c«aaWe^•»^ôao^^ra»DnBnLStO(3ge. orolBpasaleu;tBr ly evsUableio ma «hich tri-Mmues in« prasantan« luiuio uiraa;m ûm«n^5ol!^ and dig 9nvwonmof^t: OP I I vnacniaKwgonefazor, < ruua mac3««^Ddmiei.oHbrtta minfmixv*^ "A«ia co'ôfutlon and sokircnQ boct watieitânaoi nent mctnae inst to avajlaota lo mo y i q t ra l 1C3" oHet J. . ^ _ ^ ^ ^ ^ _ _ _ _

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RacBived Jan-or-;:ooz 12:41 From-tfl 57540211 To-ONYX ENVIRONMENTAL S ?aw ODZ

Jan-07-2D02 U:59 Fron-Om £NVIPONie-AL SEPVICES

.'an-or-OZ IZMZpj i From-CftM Cha i i cs l Jarv ices

+2155336-93

WIS T T ^ n s p o i j ^ r L n q CWM Chemical Senffoea, Inc.

Model C»f, NY

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\ I Leaker Q PermH Violat ion f ^ ) l>l«wrair>B/V«h. LD. vtol»t lon^

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TO] auiK i o i-^ntKiu r ~ j Mo wot Una Q Flaftwd • T~\ StabHtoalon" - [ ^ Drum* ' ' r n T«nk«r [ " ] Tra-«tormera

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TZmo frr 77me Out Iftittals ar»scM^ Common fs

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TIrrtam TlrrutOut tflfHaix ... t.;^ C'onrmv. tto

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Fail j r « t o obay immtnictha* o l racltny pa raomwi

Fal lura l o •!<»«# •piK'apriMta PVB

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RecelvBd Jan-07-2002 12;4i

S e c u r i t y G u a r d I n i t i a l s : _ ' (Indicating rtacaiptof Wash Say lass. ifnecessaty)

FnaB-+7IC7S4a211 '

Coidcen i : D<iMr '

'To-QNYX ENVIRONOTAL : Pag« 003


, STATE OF NEW YORK | 3 _ - , RgEAFITMENT OF ENVIRONMENTAL CONSERVATION

I^ IS ION OF SCUD & HAZARDOUS MATERIALS


nr^y' XXWi.

(Hazardous Waste Manifest S/00)

UNIFORiW HAZARDOUS WASTE iVIANIFEST

1. Generator's u s EPA No. Manifest Doc. No.

N|.J|l?i^|.f i@i@i3 |7 |S |0 |ÔiOi -2 . i5 i 2. Page 1 of

1 Information within heavy bold line is not required by Federal Law.


3St' CAfSCSIE CEMTES,i50 m t ' t Sfe

4. Generator's Telephone N § i § r f ^ ^ - ' - . S S ) ^ ?

A.

NYB9675729 «j3 m m « , ®a?5g

5. Transporter 1 (Company Name) 6. US EPA ID Number C. state Transporter's \D - ^ f { ^ f j 5 ^ j ^ V ^ .

D. Transporter's Telephone {'ici.-lQ )'^J"S^ •'"jnU 7. Transporter 2 (Company NanHeV 8. US EPA ID Number

I I I r I I I I I


F Transporter's Telephone ( 9. Designated Facility Name and Site Address

mt EL CITY m , Uiim


M|Y|5|i |4 |§. ,a |3,&|&,7|g


H/.A H. Facility Telephone ( )

7IB 7S4-SS3J

11. us DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 12. Containers

Number Type

13. Total

Quantity

14. Unit

Wt/Vol I. Waste No.

^•s«i8RS0i.,^ mmw., SQL 12, % B . % 77, I I !

EPA

I J,. B ,T 4.i4oiOic STATE

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b. EPA

STATE

J L I I I I EPA

STATE

I I I I I EPA

STATE

J_J. _L I I I I J. Additional Descriptions for Materials listed Above

a- Trr#i¥rrf-Q^CETi-fyt.£N£i • i i


B n ,1 U J . d. n n

IS.Speeial Handling Instructions and Additional Information , j *»» i

3€>

.y 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are


If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree 1 have determined to be economically practicable and that I have selected the practicable method oftreatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, 1 have made a good faith effort to minimize my waste generation and select the best waste management method that is availafale to me and that I can afford. # •••

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/\ f r

-Signature .'•' / 'A

''^•7 < ,. • Mo. Day Year

| . / | J | / | i \0 \ ! 18. Transporter 2 Acknowledgement of Receipt of Materials


I I ' I I I 19. Discrepancy Indication Spaca—


Printed/Typed Name Signature; ;

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Mo._ Day Year , / " / . - •, ,.-r <! .

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91486 êr 6 3

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f.-7î.tT^ yy / . Â37 T f f Q^ 9 ServicaRSq:-ft . . . - yRSqHf , ProBle* Permit*

T/ansporfsf Afavne p ^ 3 r ' Tractor/Tndler/Roll-off ft

5 ^ \ r X W 4 f ^ j^^lggj 5c^/iV.

12510

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76ISO IB .G 2

Driver's Name

Scheduled Arrival:

Actual Arrival:

Gem/afor

y'.yyyu/ Data Time ~

/ / / • s Dalte Time In Time Out

Arrived during Blacl<out? Y / N Notified DEC? Y / N

r~| Lealcer Q ] Permit Violation Q ] Placarding/Veh. LO. Violation

(~ | Other (apecify

O Bulic to Landfill Q No wet line Q Flatbed Q Stabilization Q Oruma Q Tanlcar Q Tranaformera

laboratory Time In Time Out Initials Comments

Stabilization

Landfill

Other

Aqueous Treatment

?'

Time In Time Out Initials Gross Wt. Comments


TimeIn TimeOut Initials 1

Comments

TimeIn TimeOut Signature (NO Initials) Comments


Smoking or eating In proitibitad areaa


Fallura to wear appropriate PPE

Unaafa driving pracHcea

other (apecify)

Laaving trucic unattended

Failure to diaplay overweigirt flag



Security Guard Initials: (Indicating receipt of Wash Bay pass, if necassary)

Ortvar'a ComflMM*

White: Reeardx Gicen A Canarv: Aesai Re P i n k - P f i u i r A n m M k f a l nnlA». .mA' rknv

Dao-al-Ol 03!44piii From-CW

,NYB9675234,. Plaaso typa or prinL Do not staple. ' '

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Chemical'Services'^ ' . f : : ! ! l ' l : .... -:'*^71B7S40^11 "« o n / i 5 i O N U l - S l u u u a nAÂnuuus i? M A T E R I A L S

..V- . . ..HAZARDGUS.WASTE-I\iIANIFEST : . I P.O. Box 12820, Albany, New York 12212

T-271 P.019/027 F-999


3 . Generator's Name sm4 Mail ing Address FLEET BANK • I 301 CfiRNEEIE CENTER,PO BOX £066 PRINCETON NJ» 08540

_•*• Cot^Qnite('sTolQphone(fe^r^fi^~-^^-9'^

1. G o n o i a i o i ' s U e e R A N o . . 7 . " Monifoal Doc. No,

N J ff 0 0 0 g i3 i7 i6 |g i5 lO td i f t i ' ^ Ifi

5. Tlansportarl (CompanyName)

CLEAN VENTURE, INC,

7. TiBnsponer2 (Company fvlamo)

9. Dealanated Faeinty N a m e a n d Site Address j

CWM CHEMlCflL SERUICES, L - L . C . 1550 BflLMER RIMD I MODEL CITY NY, 14107 I . - .

e.:.USERAlDNwmb8r

S. u s E m lONumbar

' I I ' ' ' I ' I ' 10. u s ER«k 10 Numbo:

N , Y , D , 0 , » g . J , 3 ^ ^ ; 7 ? 11, US DOT Description (Including Propar Shipping Nama, Hamid Class and 10 Number)

Ii Number

^HflZflRDQUS WASTE, SOLID; IN -O.S . - " ^^ (TETRACHLOROETHYLENE)(S12IS7); 9,Nf l30^7J I I I

t

MDC SR#

r J . Addillc r Moloriola Uôd AtTovc

2 . Pago 1 of

1 hrormation within haavy bold en»-s not roqulred by Fadaral Law.

NYB9675234 m m gi?^4»! <-/.

C. Stato Ttansponerl ID .--J>* L ; 6 t t y ^ ^ ^ ^ P. Transportei aTalepnenftJ^d .33 f» -Me i0

/ f F A

E. State •ftansportar'a ID F. TransponefsTelaphona ( ) Q. State FaclljN ID.

/A

M. i=aclllty Telephone ( 7 1 6 7 5 4 - 0 2 3 1

I S . Centa ins is

L

Typa

JL_i.

J_JL

I- '

15.Spacln l Handling Insrtruotions and Addlt ioncl InfotTnatlon

13. Ttoiai

Quantity

^V,c>pv

• 1 . I I

I I I

114. un iq

WtA/ol I. Wasto No. ES ^^0a STATE

EPA

STATE

EFA

STATE

EPA

STATE

K. HandCng Cooes Tor Wastes Uated ADova

I .

U^Û^ i . FOR-DELIVERY ON 15/20 01

^ / ^ J - ^ 7 ^ - 7 I S . Q E N E R A T O n ' 3 C C R T I F I C A T I O N : 1 herefiy.aoolaro that the coniBnls of:this conalgnmer! are. fully and accurately aeealBed above by propar ahippino nama and am

eiroalllad, packed, marioad and labolad. and are In all respscss in prxjper condition for transpon by hij nw»y fê«)^dlng le appllootile intemmlonsi ano riational govammeni roaulatlona and state laws and regulations.

« I am large quantiiy genaraloL I canity Ihat I have a program in piaea lo reduce Iho volume and l nirity ol wasje generaisd lo the degroo I have daterminsd to be economicaDv pracBcaBle and ihat I tofe aelected the oraetlcaDle method af trcatmnnl; siarsgs, or disoosal cuwend • avrdfeiii- ts mo which minlmizoa iho preoont and luiure inraatto human neaiin and tna anvironrnent; ORI f I am a smaller gene.-Btor, 1 have made a good laith effort to minimize my.w jstagenoral lon and select the best waste managcmont method thai la avanable lo ni& ano tnsi I ccin anord. \

Primed/Typed Wamo

^ ^ Mo IT.Tânsponar 1 AcKnyMedpemsmfefl

lama V

ledpemsm o f Heceipt df Kilaterials

rirjtiid/Typad Name »

1 8 . T i a n s p o n a t 2 AeXnowladgamant oT Rcesipt of Materials

Printed/Typed Name

Ma. Day Year

•>|2^f,7tg|f

MO, c & L -ffiar

Signature

19. Discrepancy IndlcationSpaSa a ( ^

Mo. Day "rear

I ' ' I ' 1

20 . Fadlify Owner o r OperatorJZanj f icat lon

Prime d/Typi tediTyped^NJIma f^^ t - ^ ~

of racaipt o l haizardeus maler la lycovered by,a»)irfB3J fes i except aa potsd In Hem i s . ( \

i ~ " . . I Signature/ T T " ^ y , j u ,u-^c^ YO„

COPY" 1-DISPOSER.STATE - ' ly iAILSD, BY TSO ' l tAC IL lTY

S^

Recaivad Dac-SI-ZOOl 15:42. Froin-+7167540211^ To-ONYX ENVIRONMENTAL S Paga 003

G

G

Dec-31-01 D3i44piii From-CINM Cheinioal Sarvioas +71B7540211

Raea ip tM

r^P'yJ-TianapeitarNfuna

Drivel 's Noma

Scheduled Arrival:

CWM Cheoilcal Service*. Inc. ModelCity.NY J .

^ ,_ . - Ttatlerjjtiepse P la te* and State

^ J r ^ A ^ ? 7 y - -.. ..-:.:.••.y--^ flroflfa # i : p a a n i t 0 , i

T-271 P.020/027 F-999

' ' 7 • 1 i ^ ' ^ •*• »>

nac tp r /T taUeaRd lhOf f

' Gdnotrafor 20/01 ^ ( i i

Actual Arrival: Oaiia

G Eji

/#> :/tô Time In . Time Oat:.^. •:•.••

.1 . , . , . . . . . " • ,.

A r r i v e d d u r i n g B lackou t? Y / N [ No t i f i ed D E C ? Y / N

P i Laakar F l P w i n l t Vte iat loq • j ^ P laeard lng/Voh. 1.0. Vto iat ian ' " .

I I Other (apecify^ i r^_

e.êceiving: ing: ^ Initials Gommants

B u i k t o L a n d f i n Q N o w e t l l n e H Q F l « f b « l [ f ] ~ j 5 i a b m a » t i o n ^ - ; ( 3 Druma £ [ ~ | Tanknr f ~ | Tran«<ormar»

Laboratory

Stabiii2ation

LantdfiU

.jr^^j-,.

I TimeIn TimeOai

I . Initials Cdrn.Tjen i

Other

Aqueous Treatment

Timain

j . - . • . „

1 .;,>

Twno Out?,-j, ,

j

• • - • • • • - : . • . ' . ' • ' •

Initials Grossjnt " Commerrts J

1 ' " • • • ; . - . -

Timain TimeOut 1

IniSalSr « , - Commeni f . . . • • - . . . ;

: ' • ' ' ' • • ' • • ' • i -

TTmefn nrnaCaf Initieis . .. Comrnanie

I

Timain Time Oat Signature (NOMtia ls) - Comments

Facilitv Personnel (piaase initial)

SiDofciiia or aadiig tn pitohiitttad araaa.

Failure to obay InatftKtiorM of l ^ i l i t y peraonnei

FaBure te w r a p p m p r i a t o P P E

Unaafa d r i v i ng pract lcaa

Ot t ia r (apaelfy) • :

Laaving trucit unattended

Fallura to dlapiay overwieigln flog

Imprepar toiplng or datarpin

Ovaiwalght upon arrtvai

Securi ty Guard ini t ials: (indlcatmg receipt of Wash Bay peas, if necessaiy)

•r SMvarî

Wbiie: Reearei Creen a CAnuy: Accu Rec | Iôk: Eavira^Qfiim''-

Racaivad Dee-31-2001 15:42 . •-• Froiii-+71-6754021 V

QaUcnrnd' D iwr



• | d 5 « — — •

STATE OF NEW YORK DEPAFTTMENT OF ENVIRONMENTAL CONSERVATION ;• DlVISlOfil OFSOUD & HAZARDOUS MATERIALS


[U^Z-€ X : M ^

(HazanJous Waste Manifest 5/00)


1. Generator's us EPA No.

j i i i i i j i j i i i i i i j i Z i l j J iS

Manifest Doc. No. 2. Page 1 of

sUiDi^^n 1' I 1 Information within heavy bold line is not required by FederalLaw.


FL.£i"T WS^.

4. Generator's Telephone N&iw'er ' " f^ ' " "^^

jtt'

A.

NYB9675765


f >* V f. 4__J . J L A

6. US EPA ID Number

. i i y p U {.{^ i6i^'f?? y C. state Transporter's ID . J . ,. •V

D. Transporter's Telephone p.ja, )^ '7 / ' - ./..ifA

7. Transporter 2 (Company Namg^,/ 8. "US EPA ID Number

I I I I I .y I I


I I I I F. Transporter's Telephone ( 9. Designated Facility Name and Site Address 10. yS EPA ID Number:

^ |V | I^ |V1 |4 | ' 5 |S |3 |& 6 ,? ,9.



,:, 71i& 734-323,^;


Number Type

13. Total

Quantity

14.-Unlt

WtA/ol J. Waste No.

Q [I

>•

oo

0

HAir RKC us iism'm.. ^ L I S . N . O , S . EPA

4 |4 V: I& lO STATE

EPA

STATE

I I I I EPA

STATE

I I EPA

STATE


a. x g - J ^ a A T R . n g S j g T I ' l Y l . g M ^ l ¥ I

K. Handling Codes for Wastes Usted Above n • b. J L D D IS.Speeial Handling Instructions and Additional Information

SM 4 , 2 . 3 4 ? , ^ - o t v€L.Fi.en¥ C*« l^lfZ^-iÂl ^ " i

/ 4&U, 16. GENERATOR'S CERTIFICATION: I hereby declare .thatths contents of thia consignment are fully and accurately described above by proper shipping name and are

classified, packed, marked and labeled;, and are in all respectsfjh proper condition for transport by higfnvay according to applicable-inteirnational and national government regulations and state laws and regulations. •'

If I am large quantity generator. I certify that I have a program iri place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best,waste management method that is available to me and that I can afford.

Printed/Typed Name

I^.-^. J ,-r....-;

Mo. . Day Year

1^ i 7 i J r i , / : 7 t f 17. Transporter 1 Acknowledgement ofîeceipt of Materials y -M^Vt / / Printed/Typed Name - ' • f'Signature '• Mo. Day Year

I - I I I / r h a / 18. Transporter 2 Acknowledgement of Receipt of Materials


I I I I I 19. Discrepancy Indication Space-


Printed/Typed Name Signature';•

...y^-'

Mo.-, Day .Year,'

r y ' r T' I'' /


G

G

G

G

G

G

G

G

y\EM T r a n s p o r t e r l -oq CWM Ctieflfilcal Services, Inc. Model City, NY

91503 .y^ • -V^/ f^^

yfJCMi:^ L^yy^y hJ Receipt*

Service Req. *

— .. TjailerUcBpsePlafe* and State

Permit*

yoo'<^ 7oo-o

Ckitilcy&rds

i3i02

12/20/0i

?2760 LB o 2

ii'V Transporter Name

Driver's Name •I

Scheduled Arrival:

Actual Arrival:

Tractor/Trailer/Roll-off* ^

f^/^l^4 /.ZÂrjk' Generator

y / Date .JJme

i ^ S ^ y Data TimeIn TimeOut


[~1 Leaker [ ^ PermH Violation Q ] Placardlng/Veh. 1.0. VIotation

(~ | Other (apecify


[ T i Bulic to Landfill [ ^ No wet line F l Flatbed Q Stabilization Q Druma Q Tanlcar Q Tranaformera


Stabilization

Landfill

TimeIn Time Out •.Initials Gross Wt. Comments

Time In Time Out Initials Comments

Other

Aqueous Treatment




Smoking or eating In prohibited areaa

Failure to obey inatructiona of-facility peraonnei


Unaafe driving practicea

GItier (specify) ..


Failure to diapiay. overweigirt flag

!mpro|>er tarping or detarpin

Oveiweight upon arrhral

Securi ty Guard Init ials: (Indicating receipt of Wash Bay pass, if necassary)

Orivar's CamnMiMB

White: Stecordi Green & Canary: Accts Rec Pinlr: Environmental Goldenrod: Driver

Deo-31-01 03:00piii From-CWM Cherai eal Seiv ices ^ Z ' ^ ^ Z ' '..i.J+^l.BJMOZIl

• i f l i u . o u / o / o o I HAZARDOUS WASTE M.\NIFEST Please eyp'a Of print OB not staple. !• P ^ ' B«»' 12820^ Albany, New' 'orK-12212 -

T-267 p.001/001 F-002

^ ^ CCWM IHizDfriouivwamMonlm Sue)


1. Seneraiofs US BPA lya ^ - . - > anlfest Doc Na

M 1J iR 10 10 fg-liB-i^ 1716-101 g - ..t - I I h .

2 . Page 1 o l

1 Horma i i on within heavy eoid line is not r e q u i r e by Federal Law.

a. Ganera ior^ N o m e and IMailing Address ,

FLEET BANK y 301 CARNE6IE CENTER, PO fiD;x 2066 PRINCETON N J , 08540 , -• .. : 4. oenarator'a-ftlephoneKI&^r^ST-aipT

:.;:i 'rim-'.- NYB9675738 y - r y ^ ' . ' -

^>:r^: 8. G | r |gg r^p g i p ^ p y g , ^

SEA GIRT NJ , 06750

I". 19

3. Ttaneportori (Company Name)

R-»Ce."T?4j«.i«iiê» C^ 7. TiBnsponer2 (Company nap:.

I L • 6, • tilS-€PA ID NUmbei! ^r C. State Transponei's 10 p / 0 2 A i ' ' h i ' j

9. U S E P A l O N u t t i b c r

I I 1.

P, Ttansponerl Telephone BfiOS^ZS^LjCOj E. State lyansponers ID

I - L R Trangporter'B TClepnona ( 9. Designaied Facility Name and Site Address ij —-• CWM CHEHICAL SERVICES, L.Lc. ISSO BALMER ROAD MODEL CITY NY, 14107

' 10 . US EPA ID NumtMr

N | Y i D | 0 | 4 , 9 - , B 3 , 6 : , 6 | 7 | 9

S. Slate Faciliu ID N/A

H. ftdrityTaleohone ( )

716 7S4-8231

E

c

1 1 . u s DOT Description (incUidlng Proper Shipeing Namf , Haaard C l a m ano lO Number) 12. Conlainers

NlumPer Type

13. Total

Quantity

14. Unil

Wi/vol I Waste No.

^HAZARDOUS WASTE. SOLID, N. O.S. -.:•-. . * = tTETRACHLDROETHYLfeNE) ( 5 1 ^ 1 5 7 ) 3 . Nf l3077;/ : i I !

SPA FB0S

*' '*-, i . . l ID T 4 4

STATE I o i g O

EPA

S l A I h

I I • J L SPA

STATB I . 1 - I I . L . . I

d. EPA

:oVh: STATE

I

J, Additional Descriptions tor Materials Ssted Above SOIL WITH TRACE

•^ T F T R f t C H I n R D F T H Y l I ^ N F I « : : i

K. Hanaling Cpogs lor Waarga Usled At iovc

D n • n

IS.Speeia l Handling Instructions and Addit ional irifermalion . . , ,_, . t_

HDC SR# C^TJ^LS::.') r FOR DELIVERY ON i s / i o / f i i fi\ VL:3= C?^3C^2

D C

/?/S5>/S'J i^ 16. G E N E R A T O R ' S C E H T I F I C A T I O N : I horsby aeelam tnai the eenianui:S( this eonaignincnt- rosTuDy «ne occuiaieiy descrtoea acDvs by proper shipping name and are

aassmaa, pscKed, marfcod end labeled, and oro in an reapacts in proper condition lor transport by highi ay according to appl iîUs international and nstiDnal governftiem regulations and stale laws and roauletlons.

I I1 em large quantity genaralor. 1 cenlly that I hava a program in place taredued tha volumoaha IOM aty o l waste gencralad l o tho degree 1 have deterrtAicd to be economically praelicaBle and Ihal I have salociod Ihe practicable method ol iraaimem, slotago, or disposal currenily; /ailable to me which:minimlzea the oreseniand luiuie thraal ro numan heallh and Iha envimnmeni: OR if I am a ernallef Bcncraior. i haua nu>«o a good taiih ehon lo minimize.oiy,was e-generaimn and aeleet the besi waste management method that is avallaoie to mo and that I can afford. i

pnnteonypaa Name ^ ^ \ ^ ^ \kfSlK

17. Transporter AcKtpviJEdgemenI c ^ i

SiStiali

iecoipl o l Materials ±a ^ . k

Mo. Year

^SesJL

Day

. f i - Z i / i - ^ i o i ;

primeoTiypesj Name Signatute Mo. Day Voar

, / i ^ ^ / i b , i : ^ . y IB.Transporter 2 Atdtnowledgement o l Receipt ol Materiala

PrintedHyped Nama Signature Mo. Day Year

_ ' . f i l l

-is.Discmpancy Indication S|

C ^ 20. Facility Ownor or Opora lon Oarttficailpn erf nsccipt oJ Kagarflous maierfals cDvereO b / this manite 3 excep ias noied in l lem I S .

Printad/rypird Namo

'^//.-ru J ^ ^ k M ^ l°Sl fe.x, A A - T I ^ - ^ M l C O P Y : | l - D r S P O S E R S T A T 5 - MAiL-E^ .BY TSD "FACILITY

Received Dec-31-2001 14:59 From-+715734621 r iV ' To-ONYX ENVlRONkENTAL S Page 001

Deo-31r01 03t48pn From-CWM Chemical Services " ' • ' - " "-:r,7t^

I l ia i i f f lBSSI CWM OMmlcal Swirlces, inc. McxlBlcay.NY ' i ^ '

•-+7167540211 T-271 p.025/027 F-OSO

C tMc Ya tds

765'rC- ^B 5 2

Tiauo'iJGense Plaam f a n d S t ^ B

Perrrtit*

G

Receip t a

TrapapeiterNama T t a ^ o t f t t a t t e i i R o l h a f r * .

Drivel 's Namm '<Gananiibr - -

scheduledAntval: JZ-2<9- ' f^} J Z i 3 0

Actiiai Arrival:

r2/20.'"C'l

Oote

B« "pi

id? 53

12/20/01

34420 LB G 1

^ -^ / ^ ' 5 ' .

G

C

VmelA \JlmeOut:-

Arrived during Blaokout? Y / N ••. Notif ied DEC? Y / N

r n l a a k a r Q Pwrmh V io la t ion [ ~ ] P lward lngATah. LO. Vio lat ion

• other (apecify _ _ ^

Receivihg: M Initials Commonts

^ Bu lK toLandf lU Q Mo w e t l ine l~\..^F\a!lbad . f 7 | j5iJjablli2Mllon (" "^ p t u m « Q Tankar f~ \ Traneformora

G

Laboratory

StatJilizalion

Landfill

Other

Aqueous liaatment

TimeIn TbtmOut

' S f ^ VJyn ^ / / - / ^ Comment -.

G

G

G

Timain

Timain

Tlma Out

• • :

Time Out

. - . . J e >

Initials "

• I I ' ' '

•- Mt ia lS:^ - :-T ,-rf C:jr. ••

_ ,.. QmssWt.

}..

Comment

. : • •

Comrrients

: • - - • • ' i n y

TimeIn

TimeIn

TimeOut

TimeOiJt

Initials . . .,_ Comment

..

-H SignaurafNOtiiitials} .•:. \

—•

^: .Commenia

Faci l i tv P e r s o n n e l (piaaaairtieai)

SmoUng or anting In pranibiled araaa

FWlur* to Obay inamietilona of facility peiMTOWl

Fal lura t o w e a r apprefr«tela PPE

Unaafa driving ptacHeaKt

Laaving truck unattended • i f

Fallura to diaptay ovatwalgm flag

impropar larptoig or dataipln

ovanwalght upon antval

Secur i ty Guard Ini t ia ls: ' (Indicaiing receiptor wasn Bay pass, IT necessary}

wutetXecnrtt Ci«eaaCuwy:AeettRec KalcEnvînmEBUir^ fiiilniml-n 1«T

Received D8C-31-2001 15:42 FTBm-+71B75iO?1V -;-, - " - - -TcreNVX ENVIRONMENTAL S Page 009

Deo-31-01 03:45pm From-CWM Cheraioa.l Serv ioes u^ ;-;..: ._.+I!67540211 _ w l v i a i w t T u r a U U U a t tAZARDOU ! M / K T E O I A L S '

T-271 P.021/027 F-999

NYB9675387 Please type or prInL Do not staplo.

HAZARDOUS WASTE MANIFEST PLO. Box 12820; Albafiy*Ni i /York 12212


I 1. tSonersuoi'B u s SPA No. . . . . „ Vanifoot Osft Nn.

Ir i,y p''i'a 10 I'a iia'ia i716 iq'i 3 iO|0 | 'o t -a i ? 2. Page 1 or

1 Information vitllhin heavy bold line la not required t y Federal Law

3, Generator's Nama and Mailing Address

FLEET BANK 301 CARNEGIE CENTER, PQ BOX 20&B PRINCETON N J , 0 6 5 4 0 4. 6flneraôrsTalepheno^6l8S^^7-31^7

NYB9675387 ej i SEl -- — ..^y

C. Slate Transporter's ID X g ^ ^ f e l * ^ C ^ A - )

' ^ gJ,' »§?irA; S. Transporter 1 (Comoany Name)

HQRWITH TRUCKS, INC.

S. u s EPA.II3 Munie« '

P '^ f l ^ rD , i : t 4 ,6 i r r l | 4 i 8 |7 ie p . Transponer'sT8laphondBl(0 2 6 j l " " S i 7, TiansporlerS (Company Name) 8. u s ERA ID Numbe -

' I I I ' '

E. Stale Ttsnsportar'a ID

J l - l F. Transporier's Telephono ( 9. Dealgnatad Fadlity Name and Site Address

CUH CHEMICAL SERVICES, L.L.C. 1550 BALMER ROAD MODEL CITY NY. 14107

10. u s EPA ID rUumbi r G. Stats l^clDiy ID N/fl

N,Y,D |0 |4 ,9 ,11 |3 iS-iS ,7 ,9 M, F=aclIUy Telephono ( )

716 734-eS31

11. u s DOT Dascnpnon (including Proper Snipping Name, Hazanl Claas and ID NumCierJ 12. Containers

NumtJsr Type

13. Total

Quantity

14. Unit

WtfVol L Waste Isia

HiOZflRDOUS WASTE, SOLID, • N. 0 . S," ; ' " . (TETHACHLOROETHYLEME) {512SS7) . .9i W»3077, t i l

• ' • - • > • 3 IT j^JiZîftiOD

EPA

Fa02 STOTE

EPA

STATE J L I I I

EPA

STATE 1 ,1 I I

EPA

STATE _L I I I I

K. Handling Codea forWasles Usted Above

Jm D n n

lS.Spaelai Handling Instructions and >lddtlionr,l Irrfomiatian

MDC SR# Sa3G5a FOR DEll ivERY ON 12/a iB/01

2^'^s^/c) 16. GEMRRATOR'S CSRTlPICATIONs i hsreoy aeiaare that tna^contema of mis consignme i. are fully and-aceurataly deseiibed atiove by proper shipDi'ng name and are

dassiileii, packed, marlted and lat>aled, and are In all resoeca In oropercandiiion lor transport By N ihu>i>y aesvrdlng la applicobio imamBiiorTai and nauonal govemmem ragulallona and araiB isws ana regulations. If I am larê quanlily ssneraton I certify Ihat \ have a program in place to reduce ma volume and l^xidty pf wests geneiqted to ins degree I have dDtamilned to be emnomleally piacticable and Ihal I hava seleetod Ihe practicable memod of irsatment sluiaae. or disoesal cuhem / auailnblp is me which mlnimicBa the piessnt ano future tnreat to human health ohd Ihe environment; QH it i am aamallor gensialar,.! have made a good iaiih.<:tfort to minimizs my.v.aste-genoiatlon and eelect Ihe baatvuaste management method that is svailaBie 10 me and ihat 1 can nlfcrd^ .

Priftaa/Jyped Nanje

^Pyy^C^'^^. IT.Transponer l Acknowlecdefnent of Rqcfipt of Ma'tofraia

jojjnied/Typed Name ^ _ . . .

j P ^ j g p 6 Clog î>. 18. Tianaponer 2 Acknowledgement of Receipt ot lirlalerials

Ma Day Vfear

Mo. Day _ Year

PrintaO/Typed Name Signature Ma Day Year

I I I T I l9,0iGcrepancy Indication Si

C ^ tyy fpy^ Vos of ^2:&.^('^'<^/ 20.FaciBty Ovmaror Operator; Ccrfilicalion ot receipt of hazanjoiis materials covofod by this- mar feat except aa nated In Hem ts .

Pnmed/Typ^d Ni ^ p d Name / signature

g ^ ^ dtAJ^p^zr-0 O P ; Y . : I ; - 0 1 S F O , S E R STATE - : M A l t E D BY TSX5 FACILITY

RecsiVBd D8C-31-2001 15:42 /..^Pl^'+^.^^^^'^Âlt -• ToÔNY-X ENVIRONMENTAL s' Pass 005

Dec-31-01 03!45piii From-CWM Chemical;S»fvlees I « - - <• - ' — -pi ."'.~ —

CWM Clwmlcal Sesvlces, Inc. ModelCity.NY "

•-..• :-fa •+7187546211 T-271 P.022/027 F-999

rcy Cubic V2in&

RpcaipiJt,. „ ^ ,. _ . TjBaierSJaaiisBPmBâ/MlStasa-- -

7Z,1^ LB J? 2

XSQtbX .^l^f^ ice Red, 0 .P ioOam

,JiatffpoiterNaiT>a ^ , _ .- Tm^pi/rr^lot/Rolt'%iif.*

j imef'sNama . Ganeiator .,,'|,,

Scheduled Arrival:

I4s31-

Oaii> Actual Arrtvai:

Oaia Timiiln - ^ ~ Timi-Out •

^m/2D/Ui ^ ^ ^ i ? / ^

- - A r r i v e d d u r i n g B lackou t? Y / N No t i f i ed DEC? Y / N

[~7 Leaker [ ^ Parmit Violation Q iiliMardlna/Vah. LO. VIoiailen

G I I Ottier (apecify ^ I _ _ _

[ t y S u i k to Landfill | | Nowatnner P ] FlatbeJi. r - j p ] ' Stahijizatlon [~] Oriima | ~ | Tankar Q Tran«*onn«r»

Labora to ry

Time In Time Oat Comrrieh s

G

SiabDization

Landfill

c other

Aqueous Treatment

Tima in Timo O i a .

' • • - " . '

Initials

• • • • - . ; : • -

Gnass Wt

; -i -

Comments

Timain Time Out: Initiais - CcmmerK 3

„ ,

, : . . - . . < TimeIn Time Cut liuSals , ,3 Cammem s

— - - - • ' • • ; • • •

TimeIn Time Cut SignatijiB flUO lniSals)f •-• C a m m e r ^

Faciifty Personnel {p/aas« *»•&/)

SmoUng or vadng m proMbRad araaa

Falliira to obay Inatrusifiona of facOKy peracinnel

Fallura to «war approf»iIatef>Pe

Unsafe driving pracdcsm

C M M T (apadfy) ;

Laaving tnicic unattandad

Fallura to diaplay owerweigbt flag

improper taiping or detarpin

Ovetwalgitt upon arrival

Secur i ty Guard I n i t i a l s : ; ^ dridicatSng receipt of Wasn Bay pass, ir necessary)

OilWl' jCoiiMiiewtt

whiiclKasnli I3<eea« Canwy: AceaKcc Piai: EmfifraOESUl finMrmiai-11 SWT

RacaivBd Dac-31-ZQDl 15:42 FrQiii-+71E754'DZlV . TD-QNYX ENVIRONMENTAL S Paga DQB

ug

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.an,-,0?-20J2 14:59 rrcTi-ONYX £,WIPOWfM.Al. SEPVICES _ -215533E73S

.'sn-07-02 !2U2pi!i Frsij-CWW Chsijlcal Services '-" '+7157540211 S T A T E O P . M E W V O B K

O G f V v R T U E N T O P E N V I H O N M C N T A L C o r S E R V A T I G N

OlViSlO.SI Q r S O U D i H A 2 A P 0 O U 8 M V T E B l A U S

NYB9S75153

T-9D2 ? 004/035 F-557

T-42! P.0M/.IO5 F-288

^B^, P j o a r A t y p o a ' p'-^'^c. OfS *<•[ £f=,ptc.

UNIFORM HAZA.RDOUS V\'ASTE MANIFEST

HAZARDOUS WASTE M;>NIFEST P.O. Box 12820. Albany, N9WI,>l^ftj2212 r —

1.- G c n e r s K c - c U 8 H ? A N o . Q C - . i ' a n J e s l D o e . N o . [ 2 , P i g a ' d I , nb rm£ i i o< -..t." n h , j w y bo ta Hn..

~ " I la not r e q v ec c y F t d e r a i L a w .

CCWh

M i.f Iff ici ip> .a 10 1.1 '7 rfc^ m ^ i f ' ^ . i |Q

PLEET BONK . ' • „ . ; . 3 0 : CARNEGIE CENTER, PO BOX 20b6 PRINCETON NJ , 88:340 t. Gendrsior's Telephons Ivfi^Sr 5^7 "31 p7 C. Tr3ntporT,ar l { C o m p ^ / i y H : .mo)

CL£«N t^NTURE. INC. 7. T r a n o p o r x r 2 [ C o m p a n y l^.fcmo)

5 ; U 5 SPA lO N o m o e r

N, j , e a , a . B i 0 g , ? . : ,9 .3

D. Oa : ]g r i , a toa fôalUry N a m o . i t d 5 i l c Ao<ln>cc

CWn CHEMICRL SERVICES, U U. C-l5Sa BALMER ROOD I MODEL CITY NY. 14107

a. u s SPA ID N u m o e r

1 0 . U S SPA 10 .vi iJmbef

|N ,Y ,D,B,4 |9 . ,8 S .6 ,6 ,7,9-

" NY896f^5153 e. Sgggiog^^.r, N .', 08750

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R T r a r t C e r t a r ' s T o l a p h Q r ; (

a. etaie Ricciy to t Y ' O -N/A

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716 7 5 A - a 2 n

t l . u s D O T O e s o f l p i l a n ( I n e i i d i n g P n p e r S h i p p i n B N t m e . M a i a r o t 3 a s 6 a n d l O N u m e e r )

HPZflRDQLiS WflSTb". SOLID, N-0. S. . ^.' . (TETRflCHLCROETHYLENE 1(512157) .9, Nfi3077v I H

3- iT I

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Feiaa STATE

EPA

STAT-E

EPA

STATE

a n „ n

IS.Speeial Handling Instrucdons and Aflflliionaj Infomiat.'orv

A\ r )o ^ f i : ^ " g r S g r t t ^ $ : ^ t^z>P^--^-.M y~<j X < 5 S ^ ^ 5 ^ I S , Q f f N E R A T O R ' S C g l - . T I R C A T I O N : I K e r t t x ' d 'adn/a i h p i i ha awuQOtT of this c o n t t g n m e i t arn^f^f ly ond ncc j ra t f l i y floscribea above hy pi , p w awpplng n a m o and arc

c(at i«i«ed. o»c)»7d. (TtsrluMi a n d tat ie iAd. ^ n a a;c*fc» -5^ n i W O S in Ofoocr condf t lof l fof c a n a p o f l fay rt* r i v t ^ accaro ing to appl icable intetTuironal ana PQ anal gowemtnflnt i^f lylacionff and 3L1W 'a»«:j ar»d regu-a.t iort i .

W I o t n l a r g e quan t i t y QBrwniiQr. \ csntJy l l i a i 1 haj;o •. p o g r a m in p tacs to r t c u c c m c v o t u m c a n ^ 1 m t d y crfLwaaiQ gofysfotoa ta trro degree 1 hove a ôrrrvooci to ao o-«ci«omlo.aiiv o o o b c s b l e ^ n d i n s x t h ^ v i f s e i d c t a a i n e D r v a i c i U d m i i m o d a f t r ^ a a n e n L s t o n ^ .Te wWldft m fn tm i i i ^V i cp r t acc rM t tnc .uiurQinfAat to h u m a n h e a u n a n d m « e n v i r o n m e n t ; O f t t I a m Ji a r w i e f y a n c o f w . J ftswe m a d e a gaccS a i m « n o a to r n r H r r s ^ ' " V " 3 S » Qonoracan orw3.r**lecr i f w so j c w3=ta marog t Tiont m e i n c a tnar )K j v ^ d a W c lo m t i arftf (ha j 1 c a n a M w r , '

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S i A i a

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t a . T > a n s p c n a r g A o i t n o w i a . ; 6 e m e n T of R e e e i o i of M l t e r l a B - • • ^ r - ' _

Mo. Day Vear

Ptiruad/Typafl N a m e Signature

- i g . r j l i - f i r o o a n c v lnaio.-Alioa

CJy32y^

Mo. Day Year

i _ _ i _ ! : I L

&. J(}V9(y>P. " z ^ZoZr ~ 7 / ^ ^

ZO.Fflcllliy OwiierorOpnn.lDrCBrtfiC3iicn o< nicelplolhaiartau: materials oovwad by this raEilfaat except as noted in Merr. IB.

Prlniid/iypei ^^.dOiicn^^ •'r '^.^^:(:: l4:2fcr dvd^f^ CORY. 1VDISPOSER STATE -.. W.'î-,tD-5T TSD FACILITY

Rocslveo Jan-ar-ZOCZ 12:41 From-I-715TE40Z1V : To-QNY)! ENVfRflNMENTAL S Paje 0D4

.an-07-2Gj2 14:59 rom-ONYA' ENVIRONMENT.AL SEPViCES •215533E79S

Jen-07-a2 I2:«pni FrM-CWM Chemlcil Sa-vioes

TânwKi r ter Log CWM CItmmlcal Service*, mc. Model Citst. NY

p a c B t p t ' TmHer Ucense P l a t e * and Slate

S t ru i co Poo. H Probla 0 - PooTtk »

Tnsrrxaoftar Noma ^-^ Tteet

1-m ? eOE/OOE F-557

T-421 P.CGS/iaS f - m

c

^ ^ u Z y yO. .^^?-AbA = ^ ^ f ^ 7 je^jÂj j^ Drivat's t iame

S c h e d u l e c l A r r r v a i :

TtaaatfTraHer/RdfS-ofT t

OenarsfiV

Uc

JJ;. 307 ' /O f^ Oeia

A a u a l Acr ivaJ: ^ / y-^ ^ -^ 4

/ ftectaSang n^

Mlrinis Oomman i

A r r i v e d d u r i n g B lac lcau t . ? Y / N N o t i f i e d D E C ? Y / N

j - Q Laoiwr Q P»cmlt Vk4««or» ^ PJjicardiBc/Veh. i lD. Vloletlon

Q Other (aisectfy - J

j : l ^ j Bulk to t-antffin | | Nswi«(l lBe J~] PUtD«<l | \ Sianmzatlon r n - O r t u n n ' Q T«nk»r [ ^ Trai v fo rm tm

f_. Laboratory Time I n Time Out Initials Cammen: •.

Stabilization

Landfill

Other

Aqueous Treatment

• ' . . ~ ' ' -Z-

TimtA i n Tlma Out ; .•, Initials Gross VW Commonts

' - . . , Tima in

Timain

Time In

fJme Oof " ...

TiflWQur .

-. -

77«no Our

Inia&ls .. . .

Init ial i .,;

CînmeAi s

• • • - * : -

Camrrraf la

"

Slgnatmv fNOInWals): _ "• • •

: •

Comments

Facilrty Personne l (p/owo/mte/j

FallvB'a t o o b * / Inat iurr to im of faoillTy peraonnai

Fal lura t o «««ar •pprcîrialla PPE

Unai i f * drMr iB pract iba*

o t r x i r (•pacify) . — ^ _ _ ^ _ _ _

Loavina t ruck unatie idad

Failure to <}I»piay nv. rvwigt i i flag

Improper tarp ing or lotarpln

0««r«Mlght upon an vat

S e c u r i t y G u a r d In i t i a l s :

tWiiio: Rnnnit Crmn i\ C»»ry Aaat Rec.

Received Jan-07--2Q02 I Z U t

' ' ( Indicat ing receipt o f Wash Bay p ss, i f necessary)

Pink: Eavironmcniil''

Froiii-+71S75402li

Goklenrod Driver

. .. Ts-OKVX ENVIROSMENTAL S Pa«e OOS


STATE OF NEW YORK-.r DEPARTMENT OF ENVIRONMENTAL CONSERVATION

• DIVISION OF SOUD & HAZARDOUS MATERIALS


e cxw.»^ (Hazardous Waste Manifest 5/00)

UNIFORM HAZARDOUS WASTE MANIFEST \

1.- Generator's US EPA No. „ Manifest Doc. No.

Mij i.Pi'j;iai6iiî3i?iaiiai-3k?iQioi.5 it 2. Page 1 of Information within heavy bold line

is not required by Federal Law.


R , E E T S P l * :

4. Generator's Telephone Ntiiffl)er 7 ' - ' ' ' ~ - ' f^- '^-—--__

NYB9675828 B. Gêiator's.JO-,, g | j , - j . piyj^f-j^-^^jr ^ y ; i


7. Transcprter 2 (Company Name)

6. US EPA ID Number

-ViViDr?ig'iî?iî?i--?î7 C. stale Transporter's IIJ .<^ t?y -^ f^3n~T*^

D. Transporter's Telephone (.ô j ) • ' i i 3 2 ) i


CWH CH£f1TC»L SERVICES. L . L . C . J5Si§ BfSi.. ?£fJ ??Oft& ffQ&EL CITY MY. 141»7

8. US EPA ID Number

I - I '1 I I I



w ¥ ri »j * 1 fl "J A

I I I I F. Transporter's Telephone (

G. State Facility ID N/f-1

11. US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 1


•;?,6 73-H-SE33 12. Containers

Number Type

13. Total

Quantity

14. Unil

WtA/ol I. Waste No.

D a ID

CM

-•5

^•HaraRiJOiiS (.IASTF:. S G L I O , W. O - S . EPA

"S^^c

?-• J STATE

'•« l '"i I •"'!'.:•• \ 0

EPA

STATE

I I I I I EPA

STATE I I I

EPA

STATE


• • • • ^ - - - 1


b. D a

0 15. Special Handling Instructions and Additional Information

•IDC SS# / -7 U 3SV iLfy-ZRy 0!^ l a r .i / Js 4-f | I : ^

/ -yyyHoil 16. GENERATOR'S CERTIFICATION: ! hereby declare that the contents of this consignment Care fully and accurately described above by proper shipping name and are


If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated lo the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal cunently available to me which minimizes the present and future threat to human health and the environment; OR if 1 am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Printed/Typed Name Signature

'7....

Mo. Day Year

• I ~ i j ; - i c i v : - ' i / I


g Printed/Typed Name Signature Mo. Day , Year

\wyy 18. Transporter 2 Acknowledgement of Receipt of Materials






Tranaporter Log -[AL IJSSSl CWM Chemlcai Services, iftc.

ModelCity.NY

9-1579 Cubidy^nJs^.

X ^•,y

G

G

C

Recmpt * Trailer Ucense Plate # and State

Service Req. * Pwflle* Pamtit*

Transporter Name Tractor/Trailer/Roll-off *

Driver's Name -

Scheduled Arrival:

Actual Arrival:

Generator

Date Time



I I leaker Q ] Permit Violation [ ] [ ] Placardlng/Veh. 1.0. Violation

I I Other (apecify


I I Built to Landfill Q No v»et line F l Flatbed Q Stabilization Q ] Druma Q Tanlcar F l Transformers

Laboratory • • Time In

Stabilization Time In

Time Out

Time Out

Initials Comments

Initials GmssWt. Comments

Landfill TimeIn Time Out Initials Comments

Other

C Aqueous Treatment

TimeIn

TimeIn

TimeOut

Time Out

inlb'als Comments


FaeJilty JPersonnei {pieasa initial)

SseeeldRg sr aating in prohibited areas

?at8ur3 -lo obay instructions sfuscility ^personnel

iraiSurs -lo tivear approjftrtate ?PS.

Unaafa driving âeticas

Othar i(8iis»e3fy) .

Lsavirtg irucit tunaitandsd

fal lura to diapiay svsnwei^tiit Siag

improper ^ rp ing or detarpin

Overweight m e n arrivai

Secur i ty Guard Init ials: (Indicating receipt of Wash Bay pass, if necassary)

^tii te: :SecanJa Giesn A Canawv. Accls ^tm. fttîAr.mrin.i. T>..i

i .o-~

^•mf^S9675837 ,^please type or print Do not staple.

DEPARTMENT OF ENVIRONMENTAL CONSERVATION DIVISUPN OF SCUD & HAZARDOUS MATERIALS


/j/^y (Hazardous WastB Uanltest 5/00)



\ u m m m is it i.31? i&i@i i i P r ' i^ 2. Page 1 of

?

Inlbrmation within heavy bold line is not required by Federal Law.


i LEFT mm/(

P¥eIM:£TDN m , ^ m ^ 4. Generator's Telephone Nu l ^^ r ^--^ -' " ~ -i p 7

A.

NYB9675837 . ^ 1 SIWT m% m r ^

S^ransporter I jpompany Name) 6. US EPA ID Number

fe/-i-yi0^^-îi5gi1>i¥ C. State Transporter's ID ' ^ < - . Ai p. Transporter's Telephone j ^ ^ ^ ! ^ S . T fey"

7. Transporter 2 (Company N a m e H ' 8.'US EPA ID'Number

I I I 1 I I I I I

E. State Transporter's ID ^ R Transporter's Telephone


cw»i osBticsi. ^mncESt L. L. c

?«je€L CITY vW, . i ^k$7

10. US EPA ID Number G. State Facility ID M/-3

t i J I J ^ J ^ ^ , ^ 1*^1-" I îlii H. Facility Telephone ( )

7i4 734-S53I

l:-^ 11. US DOT Description (Including Proper Shipping Name, Hazard Class and ID Number) 12. Containers

Number Type

13. Total

Quantity

14. Unit

Wl/Vol I. Waste No.

im7,-msmm W^TE, scs-i-e, M,.§.S. EPA

I I D ff 4 ^ o c>. r STATE

G CJ o CO CO

c

EPA

STATE

I I I I I I EPA

STATE

I I -J L _ L EPA

STATE

J—L I I I J. Additional Descriptions for Materials listed Above

aOI-L -U^TM T®SC£ ^-TgT?3-grM.ni?0£r?WL£:Mg| » i

K. Handling Codes for Wastes Usted Above n n I I d. _L b. D D

G

15. Special Handling Instructions and Additional Information JL

mr m ^ 6"2.MSS1 pm Mi„iwm QH i^/2.\./m ^* ' "^^ 6 / ^J ^/.} J i u •J /

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations.

If I am large quantity generator. I certify that i have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if i am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

c Printed/Typed Name

\. : • i .f

•Signature

yU Mo. Day Year

M I " I •- M " I r> I :•

17. Transporter 1 Acknowledgement ofT'eceiptof Materials

Printed/Typed Name

Ay f' ^ ty •^1

Mo. Day Year



I ' I- I I I 19. Discrepancy Indication Space

' ^ . ' r.<../ y y ^ I L

20. Facility Owner or Operator: Certification of receipt of hazartlous materials covered by this manifest except as noted in Item 19.

Printed/Typed Nacne,. Signature ;

/ ,y . . . -y . .y '

Mo, . Day ; Year

I ' " 7 - I M S / I


vmi Transporter Loo CWM Chemlcai Servlcies, inc. Model City, NY

k/s^yys7l Receipt*

.1

r ' -7 Service Req. * PmfUe* Permit*

Transporter Name

Driver's Name

Scheduled Arrival:

Actual Arrival:

Tractor/Traller/Roil-off #

. Generator

Data /

Time

C7-LOOO

Trailer Ucense Plate # and State'

Dete Time In Time Out


I I Lealcer Q Permit Violation • Q Placarding/Veh. I.D. Violation

I I Other (specify _-;

Cuta'cYards "

'739S0 LB & 2 10:54

12/21/01

Receiving: '"^y Initials Comments

[_]. Bulk to Landfill Q No wet line Q Flatbed Q Stabilization Q Druma Q Tanicor Q Transformers


Stabilization Time In Time Out Initials Gross Wt. Comments

Undfill Time In TimeOut Initials Comments

Other

Aqueous Treatment

TimeIn

Time In

Time Out

TimeOut

Initials Comments


G Facility Personnei (pieaseinitial)

SfflcUng or aating In prohibited areaa

Failure lo obey inatructiona of facility personnei


Unaafe thriving practicea

other (apecify)


Failure to diapiay overwelgiit flag


Overweigiit upon arrival

Securi ty Guard Initiais: -(Indicating receipt of Wash Bay pass, if necessary)

Orivar a OcaiiitMnta

White: Recoidt Green i . Canary: Accu Rec Pink: Environmenul Goidenrod: Driver

'J iz-vi c w r iNCVV i^-Tiiv

U •NYB9675846 Please type or print. Do not staple.

DEPARTMENT OF ENVIRONMENTAeCONSERVATION DIVISION OF SOUD & HAZARDOUS MATERIALS


/3fd (Hazardous Waste Manifest SOO)


1. Generator's u s EPA No.

N|J j lJ l iQi t | !a ia i3 |7 |£ | ia iq . | -> , >

Manifest Doc. No.

1*-. I ? i^.

2. Page 1 of

1 Information within heavy bold line Is not required by Federal Law...


4. Generator's Telephone HBmSir ' ^ ^ '•'' ^"^^^7

S. Transporter 1 (Company Name)

¥-i'i,- -i . . • C - U


,• O f 6 7 4 J t ? / - l f %

A.

NYB9675846 B. G ^ o r ' s ^ ^ .g.jg^ m M &

m.Pt SlffT NJ. ®87SS.

C. State Transporter's ID - S ° l J ' 3 . > ^ ' M ^j N?

D. Transporter's Telephone ( g^.^^, ) ' ^ i . *4 t . Transporter 2 (Company Najjig)''' 8. l i s EPXTD Number

I I I I I I I I I I I


F. Transporter's Telephone ( 9. Designated Facility Name and Site Address

'Cyw C'rCMIC:^, SCKVICES. L . L . C , 15S3 8ALI*£R J?0A3 .s«ODB. CTTY m , f.4.iia7

10. US EPA ID Number G. State Facility ID

f>J |V |S i® i» ,9 |8 | .3 | fe S ,7 ,'? H. Facility Telephone ( )

7.16 754V0S3I


Number Type

13. Total

Quantity

14. Unit

Wt/Vol I. Waste No.

IH.

J L [J ,T

EPA

STATE

'I '3 IO l o EPA

STATE

EPA

STATE

J L I I I EPA

STATE

.i—L J. Additional Descriptions for Materials listed Above

StifU, .mVA T-F!|iCE a. Tf:"Tl%ieHi.-.aSL€THVL£^£i » i


J . J L D D IS.Speeial Handling Instructions and Additional Information

S.??# LiA^ maiton k

F-Qt i£LJ¥ERV 0?* lZ.-%\ m i ^ U . ' ^ C

y/.>s~9y 7<: 7 X y

16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, rnarked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations.

If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal cunently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Printed/Typed Name

- \ u .Signature

. J—(,.., {,' V j

Mo- Day Year

I - I " I " I - 1 ^1 ' 17. Transporter 1 Acknowledgement of^Receipt of Materials ./? Printed/Typed Name Signature Mo. Day Year

I I 1 I I 18. Transporter 2 Acknowledgement of Receipt of Materials




Printed/Typed Name Signature Mo. Day. Year

' I I' I - • ^ ' '" 1 /


VIC» Transporter Loo CWM CtMmilcaJ Services, Inc. ModelCity.NY

3 ± 0 0 ^ / ^ / . ^ . ^

^yy-;\7!) Receipt* Trailer Ucense Plate * and State

-,' •" ,• i

CuijicYards

-12/21/01

•4640 LB 6 2

r" Service Req. if Profile * Pennit 0

i Transporter Name Tractot/Trailer/Roil-off *

G

Driver's Name

Scheduled Arrival:

Actual Arrival:

GenerafOr . . y

Date Time



[~~1 Leaker [ ^ PermH Violation Q Placarding/Veh. I.D. Violation

I I Other (specify

Receiving: '^ Initials Comments

|~1 Bulk to Landfill [ [ ] No vwet line Q Ftatbed [ ] ] SUbilization Q ] Druma ^ Tanker Q Transformers

Laboratory

G Time In Time Out Initios Comments

Stabilization

Landfill

Time in Time Out Initials Gross Wt. Comments

Time In TimeOut Initiais Comments

Other TimeIn Time Out Initials Comments

t- Aqueous

Treatment TimeIn TimeOut Signature (NO Initios) Comments


Smoking or eating In prohit>ited ereaa

Failure to obey inatrtictlona of facility peraonnei

Failure to twear appropriate PPE


othar (apecify)


Failure to display overweight flag

Improper tarping or detarpin -

Overwaiglit upon arrive

Secur i ty Guard Init ials: (Indicating receipt of Wash Bay pass, if necessary)

Drivar's CofiHiMnts

White: Reeordi Green A Canary: Acct> Ree. Pink: Enviranmental Goldenrod: Driver

NY.B 9^675855 Please type or print. Do not staple.

c o O

> z

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16. GENERATOR'S CERTIFICATION: 1 hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations.

If 1 am large quantity generator 1 certify that 1 have a program in place to reduce the volume and toxicity of waste generated to the degree 1 have determined to be economically practicable and that 1 have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if 1 am a smaller generator, 1 have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that 1 can afforel.

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STATE OF NEW YORK DEEARTMENT OF ENVIRONMENTAL CONSERVATION

DIVISION OF SOUD & HAZARDOUS MATHIIALS


HAZARDOUS wi^STE MANIFEST P.O. Box 12820, Albany, Ney York 12212 ^tezardous Waste Manifest 5/00)

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2f'^ryjol^ 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name and are

classified, packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations. If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practlcabis method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generajr, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

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NYB.9675774 Please type or print Do not staple.

DE.PARTMENTpi7.^NVIRONMENTAL CONSERVATION blVliiOT? OF SOUD & HAZARDOUS MATERIALS •

HAZARDOUS WASTE MANIFEST P.O. Box: 12820, Albany; New York 12212

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16.-,=:GENERAT0R'S CERTIFICATION: l hereby declare that the contents of this oonsignrrigflt are fully and accurately described above by proper shipping name and are classified, packed, marked and labeled, and are in ail respects in praper condition for transport bynighway according to applicable international and national government regulations and state laws and regulations.

If 1 am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available fo me which-minimizes the present and future threat to human health and the environment; OR if I am a smaller genp.rator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and Ihat I can afford. '-'•-:"•=-,- ' ^ i •

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f / b's^yf// 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are lully and accurately described above by proper shipping name and are

classified,,packed, marked and labeled, and are in all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations'. If 1 am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal cun'ently available to me which minimizes the present and luture threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I can afford.

Printed/Typed Name

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signature -• Mo. Day Year

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COPY 7-TRANSPORTER COPY - RETAINED BY^TRANSPORTER

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Model City, NY

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Securi ty Guard Init ials: ( Ind ica t ing rece ip t o f Wash Bay pass, i f necessary)

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BIVISION OF SOUD &H!l5apD131,«. MATERIALS "'•<-.^ ' \ \ , ^

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/ 5 T V ? / C P - / 16. GENERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described atxive by proper shipping name and are

classified, packed, marked and labeled, and are In all respects in proper condition for transport by highway according to applicable international and national government regulations and state laws and regulations. If I am large quantity generator. I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree I have determined to be economically practicable and that I have selected the practicable method of treatment, storage, or disposal currently available to me which minimizes the present and future threat to human health and the environment; OR if I am a smaller generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that Is available to me and that I can afforel.

Printed/Typed Nanjia,

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Mo. Day Year

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l_l I I L_ 19. Discrepancy Indication Space

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Receipt * jyji

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PmfUe* Pamtit*

± Transporter- flame

%yy...:,,:4\yy Tractor/Trailer/Roll-off *

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/ Driver's filame

Scheduled Arrival: J_ / Data

Actual Arrival:

Genaraior

1 Time

Data Time In- TimeOut


r n Leaker Q]] PermH Violation [ ] ] Placardlng/Veh. I.O. Violation

[~] Other (specify

CiMCffBids

7264-0 U 6 2

Receiving: / " W ^ ' Initials Comments

I I BuiktoLandfl l i [ ^ Nowet l lne Q Flatbed | ^ Stabilization Q Oruma | | Tanker [ | Transformera

Laboratory - , / • ^ r - y ,•--; TimeIn

Stabilization TimeIn

Time Out

TimeOut

Initials Comments

Initials. Gross Wt. Comments

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Landfill

Other

Time In

TimeIn

Aqueous Treatment

Time In

TimeOut

Time Out

TimeOut


Initials Comments

Initials Comments


Smoking or eating In prohibHed araaa



Unaafa driving practicea

Othar (specHy) -

Laaving truck unattended r



Overwaiglit upon arrival


Drivar's Commanta

Appendix 9

Certified Clean Fill Documentation


DEC-12-2001 09:35 LEUIIS ENUIROMENTflL -^ROn ; M. J. GRRUEL+SflNDCO, , I-NC. f-HX NIJ. :

6104956697 P.02 uec. Id ajwai iiiti:DyHn r^

NEW JERSEY GRAVEL & SAND CO.,INe. P.O.Boxl44J

WALL,N,a. 07719 j Fax 732938-4607 Phone 732-938-5252

To: Lewis Environmental Job: Rte 35 & Sea Girt Av. Wall, NJ 07719 0ate:12/Ol

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Dear Rob,

This is TO certify that the Sand Fill we delivered to the job site above is free of any contaminants or debris. It is considered environmentally sa.fe. We stockpile from a variety of locations, however, all samples are virgin material.

Revm C. Oraimpn Vice President'

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TOPSOIL - MULCH - DECORATIVE STONE - SAND YARD: Rte. 34 South, Wall T>vp. (2 Mi. No. of Rte. 195)

THTPlI P . 0 P

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NEW JERSEY GRAVEL & SAND CO.,INC. P.O. Box 1441

WALL,N.J. 07719 Phone 732-938-5252 Fax 732-938-4607

To: Lewis Environmental Job: Fleet National Bank, 1322 Sea Girt Av, Wall, N.J. 07719 Date:12/18/01-on

Dear Chris,

This is to certify that the Sand Fill we delivered to the job site above is free of any contaminants or debris. It is considered environmentally safe,

r . We stockpile from a variety of locations, however, all samples are virgin L material.

Kevin C. Gannon Vice President

TOPSOIL - MULCH - DECORATIVE STONE - SAND YARD: Rte. 34 South, Wall Twp. (2 Mi. No. of Rte. 195)

Appendix 10

Laboratory Analytical Report - Soil Samples Collected on December 17, 2001


<r Hill

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01/11/02

Technical Report for

Groundwater & Environmental Services

Fleet Bank, Wall, NJ

03-02046-02-03

Accutest Job Number: N4873

Report to:

Groundwater & Environmental Services P.O. Box 1750 1340 Campus Parkway Wall, NJ 07719

ATTN: Terri Evans

Total number of pages in report: 79

,»» A C C o ^

Test results contained within this data package meet tlie requirements of the National Environmental Laboratory Accreditation Conference and/or state specific certification programs as applicable.

încent J. Pugliese President

Certificatitjns: NJ(12129), NY(10983), CA, CT, DE, FL, MA, MD, NC, PA, RI, SCVA This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

New Jersey a 2235 Route 130 a Dayton, NJ 08810 a tel: 732-329-0200 a fax: 732-329-3499 a http://www.accutest.com

http://www.accutest.com

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Accutest Laboratories

Sample Summary

Groundwater & Environmental Services Job No: N4873

Fleet Bank, Wall, NJ Project No: 03-02046-02-03

Sample Collected Matrix Client Number Date Time By Received Code Type Sample H)

N4873-1 12/17/01 14:05 JHM 12/18/01 SO Soil SE-1 (17.5')

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

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Laboratory Beliverables

1- Cover Page, Title Page Lisfiitg Certification #, Facility Name and Adiiress, and Date of Report

- i . Table of Contents, C /

- 3. SuniniaiyShe^listkiganMytical results for alltaigeted and non-targeted compoun [. l/

4. Summary Table cross-refer«icing field nD#'s vs. lab ID #'s. r V

5. Dociiment bound, paginated and legible. '^L-^

^. Chain of Custody. \ ^

p 7. Methodology Siimmary f s ^

8. Laboratory Chronicle and Holding Time Check.

G V 91. Results submitted On a diy weight basis (if applicable) ' k J^

r ! 10. Method Detection Limits. \ ^

11. Lab certified by NJDEPE for parameters or appropriate categoty of parameters . . or a member of the USEPA CLPi f ^

12. Non-Conformance Stunmaiy. . [ l

Reviewer U . Date

N o r Jersey «ffesl) PtmdsCpqmateVillage « » i i M ^

TEST:-'-:

Percent Solids Detîmination

AaxiiestLalbofatories employs a rnoKJified ve determination of percent solids to calculate dry weight. AH data for solid matrices is reported on a dry weight basis by applying the percent solids data from this deteimination.

Aocufest labofatories. Docemtxa- 8.2000

IIS

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Table Of Contents Reduced Laboratory Data Deliverables

For Noa-USEPA/CLP Metliods

Tiaeft::oYer Page

Deliverable Chccidist

Table Of Contents

Section 1 General

A. Results Suoimary B. Chain of Custody C. Laboratoty Oironicles

Secfidw 2 GC/MS Suppor t Data grouped by fiactioa)

A. Mediotlology Review B. Coafonnanoe/Noa-coafiKinanccSafnniafy C. SiuTOgate Rcoove^ Resiitts Summaiy D. Matrix Spike/Matrix Spike Duplicate Suiamaiy E. Method Blank Suininaty F. Tune Results Stunmaiy G. Calibration Siunmaiy (sorted by faistnimeat)

Initial Calibration Check Summary Continuing Calibration Chedc Summary

H. Intemal Standatd Summaiy I. SainpteandBlaiikOiromalogianis, Quant Reports, Mass Spectra, and Library Search Data

Section 3 G C Suppor t Data

A. Methodology Review B. Conformance/Non-confotmance Summary C. Sturogate Recovery Results Stfflimaiy D. Matrix Spike/Matrix Spike Duplicate Summary E. Method Blank Suounaiy F. Calibration Summaiy (sorted by tnsttument)

Initial Calibration Check Summary Continuing Calibration Check Summaiy

G. Retention Time Shift Summaiy H. Sample Blank and Mutti-pedc Standard CSuomatograms and Quant Reports

Section 4 Metals Suppor t Data (sorted by InstiuntentType - ICP, Fuinacc, Flame, Mercuty)

A. Methodology Review B. Con&ananoc/Ndn-ooafiinnance Summaiy C Blank Rcsidts Sunimaiy

Initial and Continuing Calibration Blank Summary Mediod Blank Summaiy

D. Batch Quality Control Summaiy KfaAix Spike and Duplicate Results Summaiy Spike Blank and Lab Control Sample Summaiy

- Serial Dilution Results Summaiy E. - Calibration Summaiy

Calibration Check Standards Summaiy Intecfcfing Eleinents Check Standard Summaiy

Section S General Chemistry/Petroleum Hydrocarbon S u p p o r t Data

A. Methodology Review B. Confoimance/Non-Coofiiimance Summaiy C. Batch Quality Control Summaiy

Method Blank and Spike Blank Results Summaiy' Matrix Spike Results Summaiy Duplicate Results Summaiy ^

D. Raw Data and IR Spectra (Petroleum Hydiocaifaons) E. Raw Data and Run Record Clfexavalent Chromium)

New Jersey • FteshPoodsCotpoiateWHage • Buildiage • 223Sfioate 130 « Oayton. NJ 08810 • tel: 908-329-0200 • facSOB 329-3499 • Mlpy/www-accutestcom

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Report of Analysis Page 1 of 2

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Client Sample ID: SE-1 (17.5') Lab Sampl Matrix: Method: Project:

Run #1 a Run #2 b

elD: N4873-1 SO - Soil SW846 8260B Fleet Bank, Wall, NJ

File ID DF 150167.D 1 150255. D 1

VOA PPL List

CAS No.

107-02-8 107^13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 ' 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-5 10061-02-6 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Compomid

Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

Analyzed 12/29/01 01/01/02

Result

ND = ND<= ND<: ND^ ND"^ ND = NDt: ND^^ ND^ NDc NDi: NDt^ ND^ ND": ND<: ND": ND"^ ND<= ND<= ND-^ ND'= ND<= ND'^ ND<: ND-^ NDc ND'^ ND<^ NDc ND<= NDc ND": ND'^ ND^ ND^ ND'^

By RFY RFY

RL

3400 3400 67 340 340 340 340 340 340 1300 340 340 340 340 340 340 340 340 340 340 340 340 340 340 340 67 340 340 340 67 340 340 340 340 340 130

Date Sampled: 12/17/01 Date Received: 12/18/01 Percent Solids: 95.2

Prep Date Prep Batch Analytical Batch n/a n/a V12009 n/a n/a V12012

Units Q

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg^ ug/kg ug/kg ug/kg ug/kg Y

ND = Not detected RL = Reporting Limit E = Indicates value exceeds calibration range

J = Indicates an estimated value B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound

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Client Sample ID: Lab Sample ID: Matrix: Method: Project:

SE-1 (17.5') N4873-1 SO - Soil SW846 8260B Fleet Bank, Wall, NJ

Report of Analysis

Date Sampled: Date Received: Percent Solids:

12/17/01 12/18/01 95.2

Page 2 of 2

VOA PPL List

CAS No. Smrogate Recoveries Run#l Rmi#2 Limits

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1868-53-7 17060-07-0 2037-26-5 460-00-4

CAS No.

124-38-9

Dibromofluoromethane 92% l,2-Dichloroethane-D4 101% Toluene-D8 99% 4-Bromofluorobenzene 101 %

Tentatively Identified Compounds

Carbon dioxide Total TIC, Volatile

91% 96% 97% 106%

R.T.

2.73

55-132% 54-129% 65-133% 58-137%

Est. Cone.

4100 0

Units

ug/kg ug/kg

Q

JNB

(a) Methanol preservation/extraction. Confirmation run. Sample was reanalyzed due to carry-over. (b) Sample originally analyzed within the holding time. Methanol preservation/extraction. (c) Result is from Run# 2

s ND = Not detected RL = Reporting Limit E = Indicates value exceeds calibration range

J = Indicates an estimated value B = Indicates anialyte found in associated method blank N = Indicates presumptive evidence of a compound

y J CHAIN OF CUSTODY \ 2235 ROUTE 130, DA YTON, NJ 08810

732-329-0200 FAX: 732-329-3499/3480

ACCUTEST JOB »; * ^ ' ? j j i = f ' ^ ^

/ /V^3 TT

ACCUTEST QUOTE*:

I MATRIX COPik^

1 g CUENT INFORMATION FACILrrV INFORMATION ANALYTICAL INFORMATION M

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NAME Fl€£^

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NAME

ADDRESS M 5 077I9

PROJECT NAME

LOCATION

cmr. STATE ZIP PROJECT.NO.

SeHOnePORTTO: " T ^ G J O ^ r ^ FAx# 75Z- " j n - o ^ / b

ACCUTEST SAMPLE »

COUECTION

FIELD ID / POINT OF COLLECTION DATE TIME

SAMPLED BY:

PRESERVATION I

DW- DRINKING WATER

tSW • GROUND 1WATEB

WW- WASTE WATER

SO- SOIL SL- SLUDGE 01 - OIL LIQ - OTHER

UQUIO SOL - OTHER

SOLID

LAB USE ONLY

S£'\ Cn,s') l2^llj0L (H06 m . So 'X %^,yyi7

DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION mmm. HB" COMMENTS/REMARKS

APPROVED BY: K 21 DAYS STANDARD D 14 DAYS RUSH D T DAYS EMERGENCY D OTHER

21 DAY TURNAROUND HARDCOPY. EMERGENCY OR RUSH IS FAX DATA UNI^SS PREVIOUSLY APPROVED

^ NJ REDUCED D n NJFul l D D FULL CLP n a DISK DELIVERABLE n OTHER (SPECIFY) .

COMMERCIAL "A" COMMERCIAL "B" STATE FORMS

SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION, INCLUDINGCOURlEp DELIVER' PATE TIME: wyi) Ortr^ 1

(ffiUNOUISHEI^BY:

' A J Q f y ^ DATETIUE:

01 ^ylfO

/Poy REUNOUISHEO BV:

4. OATE-nua

SEAL! PRESERVE WHERE APPLICABLE D

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http://project.no

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GC/MS METHODOLGY SUMMARY

VOLATILE ORGANIC METHOD 8260

. Tilts mediod can be sununarizied as follows: For low levd contanunation. an irisott gas is bubbled through Sitil sample. The piirgeÎes are potently transferred fi-om tbe a<queous phase to the vapor phase. The vapor is swept tiirough a soibeat column where the purgeable arc trapped. When purging is complete, the soibent tube is heated and ba:ckflushed widi heltum to desod) trapped sample components. The analytes are desoibed dicecdy to a large bore capillary on capiUaiy precolunui before bd t^ flash evaporated to a narrow bore capillary for anal^ts.

l i ie coluoui is temperature programmed to sâcaute the analytes which are then delected with a mass spectrometer OM S) interfeced to the gas chromatogrs^h. Wide bore capillary columns requirea jet sâratot, whereas natrow bore capillary collumns can be direcdy interfeoed to the ion source:

Analytes duted from the cs^ttlary column are introduced into the mass spectrometer via a jet sq)arator or a direct connectioa Identification of target analytes is acGoaipli<êd by comparing th«r mass spectra witii the dectron impact spectra of

. autiieirtiG standard. Quantitation is accomplished by comparing the response of a ma/or (quantitation) on relative to internal standard with a five-îiit calibration curve.

1 1

N « c Jersey • fnSliPoiKbCoqioiateVaiagc -BuifcfeigB ^ 223SIV)ute 130 - Oayton.W08810 • lel.908 329 0200 • ««.9Q8 329 3499 - l«p/Aw«.'JOCUlcsl.com

T:

N O

G O M S Analysis <Jasc N^nra<iv<^Confoim

i . 0|ir<K«ta(o|;ran«s Lirftciod/Canipoumfs'fdcntificd (FicUi Samples aruf Aicffiod Dfaaks)

2. G C M S T W i c Meet Criteria

tuoimary

.YES

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-^. GGAwCSCaIAxati<>n-lA(tiatandCimtiauincCa(aHatioaM<xtMctlM>dR<i^

":{.' GCyMS Calibcatioa Reiquiicfacat;:

a . GaUKa(ioaCfKickGDai{ioun<ls

t>. System Pcrtbratanoc Otock GoiniKMtnds

6 . OlankGofilanuaation

i f yes, flic sample result i s qtiatijied vfifh a "D ".

'Sn.cfogfitc Rceovcrics lv<cct Criteria ^

i / t h e reqairemenf is not tttef. re/&- to iUui SurrogareSumrruiry-farcorruriettf.

I . Matrix Spikc/KCatrix 3p(icc Duplicate Iteoovcrics Meet Criteria

i f (fie requiremcnf is not met, refer lo kCS/MSO Summary f o r cornmcnf.

I I Intcntal Standard ArcaOlctcndon Time Siufl M e d Criteria

tftfie requirement is nolnicl , refer lo the Infernal Shutdm-d Surrunacy f o r comment.

Lil. Extraction ifoldioi;Time Met

I f l h c holding time is no i mel, refer lo Ihe Saritple Result page for comment.

I I . AnalysisIMdingiTiHtcMet

i f the holding lime i s noi met, refer lo A e Semtpfe Result page for commeal.

2.. Volatile Sample Prcse(vatiofi — pIIslMMildf>c< 2.' Us l any nortrcomptiant samples below.

ditional C<Kt%«K»ts:_ . -

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M

Kcv«c»r Sij;«atMfcr_ Date: yJ.J±l£_.^^. M n ' RG04 12

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- -Case f<a<-caGve - • : Obca<y Scacch Oata - ' .

ll»e«<kj4arg<^<xKnp6tK»dsdet<3KAe^^ teotattvsely ideaCfGed«sif»g a seareJi of the -HIST/BPA Mass Sp6ctcaJ Obcaty. HMS seardt sefecls cctlam uruguetiess dtacactedsfics from (tie sp<^<a of tlie aoa4a(gfd[ oompo<if»ds and compares U ocn lo ^^pecfra of conr^poutids that Itave been arclMvediaflwimasssptK^ffatlJajfaty: CotnpotitKlsiotltetJxatywftosesjTficftatnosic^

' reseoiblo Hue "specfta of Uve tiott-targei <xxnpot««Is are fist^ ja order of (Ctetr 'matdt fuaj Y" in Use search reswtts-

inte<pr€*k^ IJbtaty seardt data is sti*êcGve a<Kl <fc^pet*d^ Stihfecfivtly iticteases as spectral complexily ittoreases aod live fdc^diood of Itstttig a noa-<ar9e( cott^poond a s art ttoktioviAi beobotes greater.

Qtiia^tive idetiCfGKafioas of noaârgeted cootpociads must be evaluated cat^tilly lo detetm«ie if (h^r dieowcal atid pliysJcai propetties are ooti^sfeat *vft(t fiie ootnpoond classes Hva.t caa be detemKoed by ffie m^tod ia use. (f the cfietuical arid phywcaf ptoperSes of tbe suspect ootnpouod kvlicate that {MesetKe is possible, ihefibfafy seacdt data provides tlteba^s for foKtltertovestigaGoan. The iafocmaOoa generated via ftbtaty seardies of oon-taagdled tximpoucids ^Kxild be Seated as setni-

• quattaCve. ' -

OuanUtative values placed da lenlattvt^y idettfilied cotripouods (HGs) are calctjrfafed using aa assutnedf'^poase fadorof one (t). TI«s-asst«npfioa caa c a u ^ tbe calculated Coaoeafration to be gros^y esGtnated atvi may be l«gti by a s mudi as a factor of five (S) or tow by as mtidt as a factor of oae ttKKisatwl (1.000). Tlie acG«ta<y of gaaatitalcve data gettecated usio^fitxaryseardi procedures is unfaiown a<Kl SIKKIM be used guardedly: . , '

JUelfeca«ydseard^-may*ave'it*itea(ed^êp?essf«ce\jft>rgat>o?îcoa oompouods. cadxHi <iioi<id&, or aldol ooadeasates. Tlie organo-satooft cootpottrtds that f lave been identified in samples are found ia <)omponeats of ttie artalytical iasttumeataGoo. They are dassilied a s twairtal systeoi artjfads. Carfjoa dioxide, an afrndsfrfieric compoaenf is soluble in wafer aod capable of b< t»g detected in purge atKi tfap;systems. Its presettbe is iaooasequealta(t>eca<ise. of its tibtqoKlous nature. AkJol oondeasates are (>yprodktds of extradion/botvceatcalioo procedures that use aoetooe as a solvent. Tliey are prodtioed under certain pH conditions, vdwdt are a function of sample tnatdx dtaradetisUcs. None of ilusse compounds are of sample ongin and th«r appearance slKXtld be discounted for decision-making purposes.

Aooutca^CaOocjtortcs.AO'* 2«. <399 13

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Volatile Surrogate Recovery Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 1

Method: SW846 8260B Matrix: SO

Samples and QC shown here apply to the above method

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--

Lab Sample ID

N4873-1 N4873-1

, N4921-18MS N4921-18MSD N5247-4MS N5247-4MSD VI2009-BS VI2012-BS VI2012-MB1 V12009-MB1 V12009-MB2

Surrogate Compounds

Lab File ID

150167.D 150255. D I50162.D I50163.D I50262.D 150263. D I50150.D 15026 I.D 150253. D 150149.D I50160.D

SI = Dibromofluoromethane S2 = 1,2-Dichloroethane-D4 S3 = Toluene-DS ! S4 = 4-Bromofluorobenzene

SI

92.0 91.0 101.0 100.0 96.0 97.0 101.0 96.0 94.0 100.0 99.0

Recovery Limits

55-132% 54-129% 65-133% 58-137%

S2

101.0 96.0 107.0 107.0 103.0 104.0 110.0 -102.0 99.0 101.0 105.0

S3

99.0 97.0 100.0 lOO.O 97.0 97.0 102.0 98.0 94.0 98.0 102.0

S4

i 101.0 1 106.0 i 99.0 i 102.0 1 98.0 1100.0 1 100.0 1 96.0 1 109.0 1117.0 1 113.0

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Matrix Spike/Matrix Spike Duplicate Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 2

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Sample File ID N5247-4MS» I50262.D N5247-4MSD ^ 150263.D N5247-4 a 150259.D

DF 1 1 1

Analyzed 01/01/02 01/01/02 01/01/02

By RFY RFY RFY

Prep Date n/a n/a n/a

Prep Batch n/a n/a n/a

Analytical Batch VI2012 VI2012 VI2012

The QC reported here applies to the follovmig samples:

N4873-1

N5247-4 CAS No. Compoimd ug/kg '

107-02-8 Acrolein ND 71-43-2 Benzene ND 75-27-4 Bromodichloromethane ND 75-25-2 Bromoform ND 74-83-9 Bromomethane ND 56-23-5 Carbon tetrachloride ND 108-90-7 Chlorobenzene ND 75-00-3 Chloroethane ND 110-75-8 2-Chloroethyl vinyl ether ND 67-66-3 Chloroform ND 74-87-3 Chloromethane ND 124-48-1 Dibromochloromethane ND 95-50-1 1,2-Dichlorobenzene ND 541-73-1 1,3-Dichlorobenzene ND 106-46-7 1,4-Dichlorobenzene ND 75-71-8 Dichlorodifluoromethane ND 75-34-3 1,1-Dichloroethane ND 107-06-2 1,2-Dichloroethane ND 75-35-4 1, l-Dichloroethene ND 156-59-2 cis-1,2-Dichloroethene ND 156-60-5 trans-1,2-Dichloroethene ND 78-87-5 1,2-Dichloropropane ND 10061-01-5 cis-1,3-Dichloropropene ND 10061-02-6 trans-1,3-Dichloropropene ND 100-41-4 Ethylbenzene ND 75-09-2 Methylene chloride ND 79-34-5 1,1,2,2-Tetrachloroethane ND 127-18-4 Tetrachloroethene ND 108-88-3 Toluene ND 71-55-6 1,1,1-Trichloroethane ND 79-00-5 1,1,2-Trichloroethane ND 79-01-6 Trichloroethene ND 75-69-4 Trichlorofluoromethane ND 75-01-4 Vinyl chloride ND 1330-20-7 Xylene (total) ND

Method: SW846 8260B

Spike ug/kg

52500 5250 5250 5250 5250 5250 5250 5250 26300 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 5250 15800

MS ug/kg

66200 5400 5880 6400 5500 6130 5890 5090 28500 5350 4570 6050 5130 5310 5360 3990 5150 5920 5340 5320 5120 4910 5500 5880 5690 4880 4830 5680 5530 5860 5410 5590 5630 4890 17500

MS %

126 103 112 122 105 117 112 97 109 102 S7 115 98 101 102 76 98 113 102 101 98 94 105 112 108 93 92 108 105 112 103 106 107 93 111

MSD ug/kg

66700 5250 5700 6130 5200 6010 5660 4340 26700 5250 3890 5950 5460 5440 5460 4270 4990 5690 5220 5120 4900 4890 5300 5820 5630 4920 4850 5510 5330 5700 5200 5460 5340 4690 17000

MSD %

127 100 109 117 99 114 108 83 102 100 74 113 104 104 104 81 95 108 99 98 93 93 101 111 107 94 92 105 102 109 99 104 102 89 108

RPD

I 3 3 4 6 2 4 16 7 2 16 2 6 2 2 7 3 4 2 4 4 0 4 1 1 1 0 3 4 3 4 2 5 4 3

Limits Rec/RPD

1-199/35 64-132/15 64-134/15 53-147/19 45-132/19 54-143/19 56-137/17 33-140/22 29-166/19 66-130/14 46-137/22 61-138/15 46-139/18 44-143/19 44-143/20 43-139/25 67-131/15 61-135/14 60-130/19 63-132/16 63-131/18 64-132/14 58-133/16 53-138/18 49-143/20 57-130/15 41-135/23 27-207/27 48-145/16 60-136/19 62-131/15 59-146/18 27-140/24 49-142/20 45-146/17

15

G

G


Page 2 of 2

Sample File ID N5247-4MS» I50262.D N5247-4MSDa 150263. D N5247-4 a I50259.D

DF 1 1 1

Analyzed 01/01/02 01/01/02 01/01/02

By RFY RFY RFY



Analytical Batch .VI2012 VI2012 VI2012

The QC reported here applies to the following samples:

N4873-1

Method: SW846 8260B

G

G

G

G

G

CAS No. Smrogate Recoveries

1868-53-7 Dibromofluoromethane 17060-07-0 l,2-Dichloroethane-D4 2037-26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene

(a) Methanol preservation/extraction.

MS MSD N5247-4 Limits

96% 103% 97% 98%

97% 104% 97% 100%

92% 96% 97% 107%

55-132% 54-129% 65-133% 58-137%

IS

Blank Spike Summary Job Number: N4873 Account: GESNJ Groimdwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 2

Sample V12012-BS

File ID DF 150261.D 1

Analyzed By Prep Date Prep Batch Analytical Batch 01/01/02 RFY n/a n/a VI2012

The QC reported here applies to the follovnng-samples:

N4873-1'

£ j

G

J

'

:

__

_. ,

—

_

CAS No.

107-02-8 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-5 10061-02-6 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Compoimd

Acrolein Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1, l-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

Spike ug/kg

25000 2500 2500 2500 2500 2500 2500 2500 12500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 7500

BSP ug/kg

32900 2520 2740 3000 2580 2890 2690 2550 11000 2460 2210 2890 2460 2510 2510 1980 2390 2740 2480 2380 2330 2300 2450 2600 2590 2350 2370 2670 2560 2720 2580 2580 2890 2440 8140

BSP %

132 101 110 120 103 116 108 102 88 98 88 116 98 100 100 79 96 110 99 95 93 92 98 104 104 94 95 107 102 109 103 103 116 98 109

Limits

1-219 74-127 71-134 63-144 64-138 58-144 77-124 64-143 28-165 72-129 51-146 69-137 73-127 74-122 73-126 47-143 70-130 67-138 64-129 70-127 65-128 71-132 67-124 63-126 76-127 62-129 42-147 44-179 74-126 64-136 70-132 73-135 52-147 57-144 77-126

Method: SW846 8260B

17

G

G

G

G

G

Blank Spike Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 2 of 2

Sample V12012-BS

FUe ID DF 150261.D 1

Analyzed 01/01/02

By RFY

Prep Date n/a

Prep Batch n/a

Analytical Batch VI2012


N4873-1

Method: SW846 8260B

CAS No. Surrogate Recoveries


BSP Limits

96% 102% 98% 96%

55-132% 54-129% 65-133% 58-137%

G

G

18

Method Blank Summary Job Number: ' N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Pagel of 2

Sample VI2012-MB1

File ID 150253.D

DF 1

Analyzed 01/01/02

By RFY

Prep Date n/a

Prep Batch Analytical Batch n/a VI2012

(


N4873-1

Method: SW846 8260B

CAS No. Compound Result RL Units Q

^

J_

.

.-..

--

107-02-8 107-13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-f 10061-02-e 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1, l-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene

) trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

• iiii 2500 iiii 2500 iiii 50 iiiii 250 iiii: 250 iiii 250 iiii 250 iiiii 250 iiiiii 250 l i l 1000 iiiiii 250 iiiiiii 250 iiii 250 iiiiii i 250 iiiiiiiiii 250 iiiiiiiii 250 iiiiiiiiii 250 iiiiiiii 250 iiiii 250 iiiii 250 iiiii 250 iiiiii 250 iiiiiii 250 -iiiiii 250 iiiiiiiiii 250 iiiiiiiiiii 50 iiiiii 250 iiiiiiiii 250 iiiiii 250 iiiiiiiii 50 iiii 250 iiiiii 250 iiiiiii 250 iiiiiiiii 250 Iiiii 250 iiiiiiiii 100

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

19

G

G

C

G

G

Method Blank Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 2 of 2

Sample VI2012-MB1

File ID DF 150253. D 1

Analyzed 01/01/02

By RFY

Prep Date n/a

Prep Batch n/a

Analytical Batch VI2012


N4873-1

Method: SW846 8260B

G



CAS No. Tentatively Identified Compounds

124-38-9 Carbon dioxide Total TIC, Volatile

Limits

94% 99% 94% 109%

)unds

55-132% 54-129% 65-133% 58-137%

R.T.

2.75

Est. Cone.

2300 2300

Units Q

ug/kg JN ug/kg

20

G

G

G

G

G

G

G

G

Instrument Performance Check (BFB) Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 1

Sample: VI2008-BFB2 Lab File ID: I50138.D Instrument ID: GCMSI

Injection Date: Injection Time:

12/28/01 21:05

m/e Ion Abundance Criteria Raw Abundance

% Relative Abxmdance Pass/Fail

50 75 95 96 173 174 175 176 177

15.0-40.0% of mass 95 30.0-60.0% of mass 95 Base peak, 100% relative abundance 5.0-9.0% of mass 95 Less than 2.0% of mass 174 50.0- 120.0% of mass 95 5.0-9.0% of mass 174 95.0-101.0% of mass 174 5.0-9.0% of mass 176

7987 18919 31616 2116 67 23424 1720 23408 1596

25.3 59.8 100.0 6.7 0.21 74.1 5.4 74.0 5.0

(0.29) a

(7.3)a (99.9) a (6.8)b

Pass Pass Pass Pass Pass Pass Pass Pass Pass

(a) Value is % of mass 174 (b) Value is % of mass 176

This check applies to the following Samples, MS, MSD, Blanks, and Standards:

Lab Sample ID

V12008-CC1986 VI2008-MB2 V12008-BS ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ VI2009-MB1 VI2009-BS ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ

Lab File ID

I50139.D 150141.D I50142.D 150143. D I50144.D I50145.D I50146.D I50147.D I50148.D I50149.D I50150.D I50151.D I50152.D 150153.D I50154.D 150155.D I50156.D

Date Analyzed

12/28/01 12/28/01 12/28/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01

Time Analyzed

21:44 23:02 23:41 00:19 00:59 01:38 02:17 02:56 03:35 04:14 04:54 05:33 06:12 06:51 07:30 08:09 08:48

Hours Lapsed

00:39 01:57 02:36 03:14 03:54 04:33 05:12 05:51 06:30 07:09 07:49 08:28 09:07 09:46 10:25 11:04 11:43

Client Sample ID

Continuing eal 50 Method Blank Blank Spike (unrelated sample) (unrelated sample) (unrelated sample) (unrelated sample) (unrelated sample) (unrelated sample) Method Blank Blank Spike (unrelated sample) (unrelated sample) (unrelated sample) (unrelated sample) (unrelated sample) (unrelated sample)

21

G

G

G

G

G

G

G

Instrument Performance Check (BFB) Job Number: N4873 Account: GESNJ Groimdwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 1

Sample: VI2009-BFB1 Lab File ID: I50157.D Instrument ID: GCMSI

Injection Date: 12/29/01 Injection Time: 09:27

m/e Ion Abundance Criteria Raw % Relative Abundance Abundance Pass/Fail

50 75 95 96 173 174 175 176 177


7499 17464 29352 2073 0 21912 1595 21197 1338

25.5 59.5 100.0 7.1 0.0 74.7 5.4 72.2 4,6

(0.0) a

(7.3) a (96.7) " (6.3) b




Lab Sample ID

VI2009-CC1986 VI2009-MB2 N4921-18 N4921-18MS N4921-18MSD ZZZZZZ ZZZZZZ N4873-1

Lab File ID

I50158.D I50160.D I50161.D I50162.D 150163.D I50164.D I50165.D 150167.D

Date Analyzed

12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01 12/29/01

Time Analyzed

10:06 11:24 12:03 12:42 13:21 14:00 14:39 15:57

Hours Lapsed

00:39 01:57 02:36 03:15 03:54 04:33 05:12 06:30

Client Sample ID

Continuing eal 50 Method Blank (used for QC only; not part of job N4873) Matrix Spike Matrix Spike Duplicate (unrelated sample) (unrelated sample) SE-1 (17.5')

22

G

G

G

G


Page 1 of 1

Sample: VI2012-BFB Lab File ID: 150250.D Instrument ID: GCMSI


m/e Ion Abundance Criteria Raw Abundance

% Relative Abundance Pass/Fail

50 75 95 96 173 174 175 176 177

15.0-40.0% of mass 95 30.0-60.0% of mass 95 Base peak, 100% relative abimdance 5.0-9.0% of mass 95 Less than 2.0% of mass 174 50.0- 120.0% of mass 95 5.0-9.0% of mass 174 95.0-101.0% of mass 174 5.0-9.0% of mass 176

6704 16709 28051 2097 0 19819 1422 19499 1298

23.9 59.6 100.0 7.5 0.0 70.7 5.1 69.5 4.6

(0.0)a

(7.2) ^ (98.4) a (6.7)b




Lab Sample ID

VI2012-MB1 ZZZZZZ N4873-1 ZZZZZZ ZZZZZZ ZZZZZZ N5247-4 ZZZZZZ VI2012-BS N5247-4MS N5247-4MSD ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ

Lab File ID

150253. D 150254.D 150255. D I50256.D 150257. D 150258. D I50259.D 150260. D 15026 I.D I50262.D 150263.D I50264.D I50265.D 150266. D 150267. D

Date Analyzed

01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02 01/01/02

Time Analyzed

01:54 02:33 03:13 03:52 04:31 05:10 05:49 06:29 07:08 07:47 08:26 09:05 09:45 10:24 11:03

Hours Lapsed

01:57 02:36 03:16 03:55 04:34 05:13 05:52 06:32 07:11 07:50 08:29 09:08 09:48 10:27 11:06

Client Sample ID

Method Blank (unrelated sample) SE-1 (17.5') (unrelated sample) (unrelated sample) (unrelated sample) (used for QC only; not part of job N4873) (unrelated sample) Blank Spike Matrix Spike Matrix Spike Duplicate (unrelated sample) (unrelated sample) (tmrelated sample) (imrelated sample)

23

Initial Calibration Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI1986-ICC1986 I49372.D

Page 1 of 3

Method T i t l e L a s t Upda t e Response v i a

Response F a c t o r R e p o r t MSI

C:\HPCHEM\l\METHODS\MI1986.M (RTE I n t e g r a t o r ) SW-846 Method 8260 Mon Dec 10 1 4 : 2 7 : 4 6 2001 Initial Calibration

Calibration Files 400 =149379.D 50 =149372.D 20

100 =149375.D =149371.D 5

1 =149374.D =149370.D 10 =149373.D

G

G

G

G

G

G

1 2

3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43

44

Compound 400 100

I Tert Butyl Alcohol-d9 -M tertiary butyl al 1 428

I pentafluorobenzene M chlorodifluoromet M dichlorodifluorom M Dichlorotetrafluo M chloromethane M.vinyl chloride M 1,3-butadiene M bromomethane M chloroethane M trichlorofluorome M ethyl ether M acrolein M freon 113 M acetone M 1,1-dichloroethen M acetonitrile M iodomethane M methyl acetate M allyl chloride M methylene chlorid M carbon disulfide M acrylonitrile M methyl tert butyl M trans-1,2-dichlor M hexane M di-isopropyl ethe M 1,1-dichloroethan M vinyl acetate^ M chloroprene M ethyl tert-butyl M 2-butanone M 2,2-dichloropropa )M ethyl acetate M cis-1,2-dichloroe )M methacrylonitrile M chloroform M bromochloromethan )M tetrahydrofuran )M 1,1,1-trichloroet )S dihromofluorometh )S 1,2-dichloroethan

0 0 0 0 0 0 0 0 0 0

0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

482 321 310 209 176 054 251 117 801 106

432 078 302 009 833 136 341 283 702

786 337 257 042 633 054 529 064 088 427 .198 .350 .175 .898 .265 .043 .733 .714 .487

I 1,4-difluorobenzene

1

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

338

523 396 353 241 202 066 283 138 865 117 017 547 062 317 Oil 928 163 379 308 762

847 357 274 165 680 053 543 154 074 509 .225 .361 .182 .927 .272 .046 .864 .728 .573

1

0

0 0

0

0

0 0

0 0

0

0

0

0 0

0 0 0

382

081 013

215

844

327 607

960 335

656

480

302

925 150

.551 704 518

50

1

—

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

20

ISTD---379 1 287

ISTD---509 417 350 238 208 061 280 134 817 114 017 532 056 309 Oil 916 160 372 299 740

834 360 273 141 677 058 547 131 067 551 .215 .374 .175 .923 .269 .056 .886 .715 .526

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

[S^

463 413 342 231 228 061 310 142 817 116 020 497 060 293 009 918 158 366 307 721

860 353 278 079 669 052 477 092 070 536 .196 .356 .153 .910 .268 .057 .887 .709 .523

rr» .u —

5

1

—

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

035

470 466 316 226 220 029 251 128 668 100 019 512 072 280 007 907 117 388 316 717

886 351 261 102 689 032 448 119 039 523 218 357 079 931 255 .040 .863 .707 .509

10

1

—

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

360

532 471 367 274 221 058 292 134 721 114 018 550 099 319 012 966 178 385 327 757

886 374 318 236 719 056 545 219 090 593 210 .387 192 984 269 .047 .946 .716 .514

1

—

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

Avg

304

497 414 346 236 209 055 278 132 781 107 017 512 071 291 010 902 152 372 310 715 000 865 352 277 127 675 051 515 13 0 071 517 .210' .355 .159 .928 .250 .048 .8i9 .713 .521

%RSD

10

5 13 7 9 9

24 8 6 9

11 13 8

22 12 17 5

14 4 5 7

-1 6 3 7 6 3

18 8 4

25 10 5 7

25 2

17 14 16 1 5

_2

73

80 23 50 24 09 69 43 73 32 89 20 61 42 46 ' 21 22 18 59 04 34 00 22 84 93 11 95 50 15 77 81 28 .44 .48 .94 .92 .76 .67 .43-.11 .05

1

G

G

G

G

G

C

G

Initial Calibration Summary Job Number: N4873 Accoimt: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI1986-ICC1986 149372.D

Page 2 of 3

45) 46) 47) 48) 49) 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71

72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87

88 89 90 91 92 93 94 95 96 97 98 99

100 101 102

M M M M M M M M M M M M M M M M M M M M M S M M M M M

1,1-dichloroprope isopropyl acetate carbon tetrachlor cyclohexane tert-amyl methyl heptane 1,2-dichloroethan benzene Di-isobutylene ethyl acrylate trichloroethene methylcyclohexane 1,2-dichloropropa propyl acetate methyl methacryla bromodichlorometh 1,4-dioxane d i b romome thane 2-chloroethyl vin 4-methyl-2-pentan cis-1,3-dichlorop toluene-d8 (s) toluene trans-1,3-dichlor ethyl methacrylat 1,1,2-trichloroet 2-hexanone

0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

T /-till /-x-v-/-NK/=i>-.r»^£i*i/=i_/^ C J

M M M M M M )M )M )M )M )M )M )M ) )M

1,3-dichloropropa butyl acetate tetrachloroethene dibromochlorometh 1,2-dibromoethane chlorobenzene 1,1,1,2-tetrachlo ethylbenzene m,p-xylene o-xylene styrene butyl acrylate bromoform 1-chlorohexane cyclohexanone

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

573 598 932 339 887 427 647 765 644 475 512 353 362 395 197 024 001 487 163 097 653 938 591 608 431 305 229

704 203 791 185 764 024 .709 .524 .543 .547 .966 .962 .744 .321 .553

0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

) I 1,4-dichlorobenzene-d )S )M )M )M )M )M )M )M )M )M )M )M )M )M

4-bromofluorobenz isopropylbenzene 1,1,2,2-tetrachlo 1,2,3-trichloropr trans-1,4-dichlor n-propylbenzene bromobenzene 1,3,5-trimethyIbe 2 -chlorotoluene 4 -chlorotoluene tert-butylbenzene 1,2,4-trimethyIbe vinyl toluene pentachloroethane

1 2 0 0 0 2 0 2 2 2 1 1

0

.048

.248

.932

.660

.224

.708

.944

.012

.065

.362

.728

.972

.824

1 2 0 0 0 2 0 2 2 2 1 2

0

581 684 988 380 990 347 690 836 820 408 538 395 381 420 195 042 002 511 154 106 637 926 616 569 447 333 195

716 217 822 157 755 .067 .746 648 .573 .560 .961 .924 .757 .330 .117

.007

.455

.978

.680

.177

.911

.995

.199 :i87 .556 .905 .184

.857

0.

0 0

0 0

0 0 0

0

0

0 0 0 0 0 0

0

0 0 0 0 0 1 0 0 0 0 0 0 0

_ _

1

1

3 1 3 2 3

0

533

850 220

846 937

555 531 455

901

466

501 884 606 357 352 285

649

877 854 652 995 696 670 .593 .550 .713 .706 .522 .252 .495

.138

.261

.834

.191

.193

.827

.338

.912

0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 2 0 0 0 3 1 2 2 2 1 2

0

601 670 988 395 984 359 693 859 940 329 545 403 399 406 191 028 002 505 139 101 629 903 626 541 446 332 176

0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

589 566 953 392 924 317 694 852 125 292 540 377 402 387 198 014 001 495 110 101 578 902 600 471 426 326 192

. T C? 'TT^ J

730 213 899 157 764 .108 .780 725 .599 .613 .988 .854 .750 .327 .166

.013

.623

.992

.764

.151

.040

.041

.342

.505

.488

.997

.311

.887

0 0 0 0 0 0 0 1 0 0 0 0 0 0 0

Li.*

578 149 728 908 588 .883 .606 .353 .497 .483 .744 .560 .571 .252 .185

[STD--1 2 1 0 0 3 1 2 2 2 2 2

0

.037

.745

.051

.882

.120

.060

.057

.471

.509

.645

.018

.359

.863

0. 1. 0. 0 0. 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 0 0 1 0 1 0 0 0 0 0 0 0

1 2 1 1 0 3 1 2 2 2 2 2

0

564 641 882 351 949 261 733 861 866 230 534 372 413 357 187 954 001 512 089 091 525 897 623 433 398 328 174

686 152 828 960 641 .041 .682 .51 8 .551 .551 .753 .506 .576 .303 .234

.061

.909

.142

.263

.072

.130

.087

.660

.•387

.974

.202

.508

.860

0. 1. 1. 0. 1. 0 0 0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 3 1 0 0 3 1 2 2 2 2 2

0

636 813 002' 394 •053 350 717 905 454 261 567 406 424 476 192 012 001 509 115 107 615 893^ 64 2" 471 424 341 226

660 185 845 007 669 .033 .702 577 .583 .566 .832 .589 .625 .328 .597

.065

.044

.137

.911

.122

.342

.122

.669

.846

.805

.261

.561

.936

0 1. 0. 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 '0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 2 1 0 0 3 1 2 2 2 2 2 0 0

583 662 942 353 964 344 717 859 141 333 542 405 405 407 194 996 001 498 128 101 591 906 615 493 418 322 199

675 187 827 033 690 .022 .703 .574 .563 .553 .851 .729 .649 .302 .335

.053

.671

.071

.860

.144

.146

.062

.507

.475 -738 .019 .316 .000 .877

5. 5. 6.

17. 6.

15 8 6

39 27 3

14 7 9 2 5

29 3

22 6 9 2 2

17 8 6

11

7 16 6

12 10 6 7 7 6 6

-13 25 15 11 60

4 10 10 25 36 11

. 7 15 11 12. 9 9

-1

49 18 15 74 02 84 73 29 47 95 20 44 39 86 12 05 41 34 16 00 90 08 85 47 05 02 93

65 11 82 95 23 91 73 87 .29 .90 .96 .46 .29 .71 .94

.14

.97

.78

.83

.31

.44

.65

.36

.92

.17

.67

.35

.00 '

_25'°

.-4

n

r~

-.;

-

Initial Calibration Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

103)M s e c - b u t y l b e n z e n e 2 . 4 3 1 104)M p - i s o p r o p y l t o l u e n 2 . 0 5 2 105)M 1 , 3 - d i c h l o r o b e n z e 1 . 3 8 8 106)M 1 , 4 - d i c h l o r o b e n z e 1 . 4 7 9 107)M n - b u t y l b e n z e n e 1 . 9 7 0 108)M 1 , 2 - d i c h l o r o b e n z e 1 . 3 3 8 109)M h e x a c h l o r o e t h a n e 0 . 7 3 4 110)M l , 2 - d i b r o m o - 3 - c h l 0 . 3 0 1 111)M 1 , 2 , 4 - t r i c h l o r o b e 0 . 8 9 2 112)M h e x a c h l o r o b u t a d i e 0 . 6 2 8 113)M n a p h t h a l e n e 1 .2 03 114)M 1 , 2 , 3 - t r i c h l o r o b e 0 : 7 3 6

2 . 6 0 6 2 . 2 0 2 1 . 4 0 9 1 . 5 2 5 2 . 0 6 8 1 . 3 6 7 0 . 7 7 1 0 . 2 7 9 0 . 9 0 1 0 . 7 3 1 1 . 1 0 4 0 . 7 4 9

3 . 4 0 6 2 . 6 6 4 1 . 6 6 7 1 . 7 7 2 2 . 3 2 7 1 . 6 6 0 0 . 6 5 8

1 . 0 0 4 0 . 7 5 8 0 . 5 2 3

2 . 7 5 2 2 . 2 9 8 1 . 4 3 1 1 . 5 6 1 2 . 0 6 9 1 . 4 1 0 0 . 7 9 6 0 . 2 6 7 0 . 8 3 6 0 . 7 7 0 0 . 9 1 8 0 . 7 0 3

2 2 1 1 1 1 0 0 0 0 0 0

Sample: Lab FilelD:

732 2 6 6 4 4 0 584 939 4 1 6 7 5 3 254 6 9 9 697 8 3 5 654

2 . 6 7 9 2 . 3 3 0 1 . 4 1 7 1 . 6 6 2 1 . 8 0 0 1 . 5 6 9 0 . 7 2 1 0 . 2 4 2 0 . 4 6 4 0 . 6 9 1 0 . 6 2 6 0 . 4 4 1

A v e r a g e

Page 3 of 3 VI1986-1CC1986 I49372.D

2 . 9 9 6 2 . 3 8 4 1 . 4 9 9 1 . 5 9 0 2 . 0 1 3 1 . 4 9 0 0 . 8 1 5 0 . 2 8 4 0 . 7 4 2 0 . 8 7 0 0 . 8 6 5 0 . 7 1 4

2 . 8 0 0 2 . 3 1 4 1 . 4 6 4 1 . 5 9 6 2 . 0 2 7 1 . 4 6 4 0 . 7 5 0 0 . 2 7 1 0 . 7 5 6 0 . 7 7 0 0 . 9 0 1 0 . 6 4 6

% RSD = 1 1

1 1 . 3 0 8 . 1 2 6 . 5 5 6 . 0 2 7 . 9 6 7 . 9 1 6 . 9 7 7 . 7 8

2 1 . 6 9 1 6 . 6 1 2 1 . 9 5 1 8 . 3 0

. 7

G (#) = Out of Range ### Number of calibration levels exceeded format ###

MI1986.M Mon Dec 10 14:30:05 2001 GCMSI

G

G

G

G

S6.

.

—

—

1—

—

i -

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n

—

—

^

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—-

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Continuing Calibration Summary Job Number: N4873 Accoxmt: Project:

Data

GESNJ Groundwater & Environmental Services Fleet Bank, Wall, NJ

Page 1 of 3 Sample: VI2008-CC1986 Lab FilelD: I50139.D

Evaluate Continuing Calibration Report

File : C:\HPCHEM\1\DATA\I5013 9.D Acq On Sample Misc

28 Dec 2001 9:44 pm CC1986-50 MS58721,VI2008,10,,100

MS Integration Params: RTEIN2.P ,25,1

Method : C:\HPCHEM\l\METHODS\MI1986.M Title Last Update Response via

Min. Max.

1 2

3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41

I M

I M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M M

SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Multiple Level Calibration

RRF : 0.000 Min. Rel. RRF Dev : 20% Max. Rel.

Compound

Tert Butyl Alcohol-d9. tertiary butyl alcohol

pentafluorobenzene chlorodifluoromethane dichlorodifluoromethane Dichlorotetrafluoroethane chloromethane vinyl chloride 1,3-butadiene bromomethane chloroethane t ri chloro fluoromethane ethyl ether acrolein freon 113 acetone 1,1-dichloroethene acetonitrile iodomethane methyl acetate allyl chloride methylene chloride carbon disulfide acrylonitrile methyl tert butyl ether trans-1,2-dichloroethene hexane di-isopropyl ether 1,1-dichloroethane vinyl acetate chloroprene ethyl tert-butyl ether 2-butanone 2,2-dichloropropane ethyl acetate cis-1,2-dichloroethene methacrylonitrile chloroform bromochloromethane t e t rahydro furan 1,1,1-trichloroethane

Area : 5 0


(RTE Integrator)

% Max. Area : 150%

~ AvgRF

1.000 1.304

1.000 0.497 0.414 0.346 0.236 0.209 0.055 0.278 0.132 0.781 0.107 0.017 0.512 0.071 0.291 0.010 0.902 0.152 0.372 0.310 0.715 0.000 0.865 0.352 0.277 1.127 0.675 0.051 0.515 1.130 0.071 0.517 0.210 0.355 0.159 0.928 0.250 0.048 0.819

CCRF

1.000 1.168

1.000 0.504 0.307 0.298 0.203 0.196 0.049 0.281 0.136 0.924 0.104 0.013 0.413 0.064 0.293 0.010 0.911 0.187 0.344 0.284 0.672 0.031 0.857 0.338 0.236 1.058 0.654 0.050 0.547 1.145 0.067 0.500 0.195 0.354 0.157 0.951 0.263 0.050 0.943

R.T. Dev

10 RUIFENGY MSI I'.OC

0.50min

%Dev Area% Dev(min)

0.0 10.4

0.0 -1.4 25.8# 13.9 14.0 6.2

10.9 -1.1 -3.0

-18.3 2.8

23.5# 19.3 9.9

-0.7 0.0

-1.0 -23.Oft 7.5 8.4 6.0 0.0 0.9 4.0

14.8 6.1 3.1 2.0 -6.2 -1.3 5.6 3.3 7.1 0.3 1.3

-2.5 -5.2 -4.2

-15.1

81 68

77 76 57 65 66 72 61 77 78 87 70 58 60 88 73 71 76 90 71 73 70 Oft

79 72 67 71 74 66 77 78 77 70 70 73 69 79 75 68 82

0.00 -0.03

-0.04 -0.03 -0.02 -O.04 0.00

-0.02 -0.05 0.00

-0.04 -0.03 -0.06 0.00

-0.02 -0.02 -0.05 0.00

-0.03, -0.04 -0.03 -0.03 -0.05 -0.04 -0.03 -0.02 -0.03 -0.04 -0.05 -0.04 ; -0.03 -0.02 -0.04 -0.03 -0.02 -0.03 -0.05 -0.04 -0.04 -0.04

-0.04 2»J>

G

G

G

G

C

G

G

Continuing Cahbration Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI2008-CC1986 I50139.D

Page 2 of 3

42 S 43 S

44 I 45 M 46 M 47 M 48 M 49 M 50 M 51 M 52 M 53 M 54 M 55 M 56 M 57 M 58 M 59 M 60 M 61 M 62 M 63 M 64 M 65 M 66 S 67 M 68 M 69 M 70 M 71 M

72 I 73 M 74 M 75 M 76 M 77 M 78 M 79 M 80 M 81 M 82 M 83 M 84 M 85 M 86 87 M

88 I 89 S 90 M 91 M 92 M 93 M 94 M 95 M 96 M 97 M 98 M

dibromofluoromethane (s) 1,2-dichloroethane-d4 (s)

1,4-difluorobenzene 1,1-dichloropropene isopropyl acetate carbon tetrachloride cyclohexane tert-amyl methyl ether heptane 1,2-dichloroethane benzene Di-isobutylene ethyl acrylate trichloroethene methyleyelohexane 1,2-dichloropropane propyl acetate methyl methacrylate bromodichloromethane 1,4-dioxane dibromomethane 2-chloroethyl vinyl ether 4-methyl-2-pentanone cis-1,3-dichloropropene toluene-d8 (s) toluene trans-1,3 -di chloropropene ethyl methacrylate 1,1,2-trichloroethane 2-hexanone

chlorobenzene-d5 1,3-dichloropropane butyl acetate tetrachloroethene dibromochloromethane 1,2-dibromoethane chlorobenzene 1,1,1,2-tetrachloroethane ethylbenzene m,p-xylene o-xylene styrene butyl acrylate bromoform 1-chlorohexane eyelohexanone

l,4-dichlorobenzene-d4 4-bromofluorobenzene (s) isopropylbenzene 1,1,2,2-tetrachloroethane 1,2,3-triehloropropane trans-1,4-dichloro-2-butene n-propylbenzene bromobenz ene 1,3,5-trimethyIbenzene 2-chlorotoluene 4-chlorotoluene

0.713 0.521

1.000 0.583 1.662 0.942 0.353 0.964 0.344 0.717 0.859 1.141 0.333 0.542 0.405 0.405 0.407 0.194 0.996 0.001 0.498 0.128 0.101 0.591 0.906 0.615 0.493 0.418 0.322 0.199

1.000 0.675 0.187 0.827 1.033 0.690 1.022 0.703 1.574 0.563 0.553 0.851 0.729 0.649 0.302 0.335

1.000 1.053 2.671 1.071 0.860 0.144 3.146 1.062 2.507 2.475 2.738

0 0

1 0 1 1 0 1 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

1 0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 1 2 0 0 0 2 1 2 2 2

705 565

000 631 662 125 346 031 268 800 851 901 280 582 311 384 400 204 131 002 550 143 104 626 913 632 569 449 330 194

000 .736 .206 927 228 .782 .114 843 741 .618 .621 .965 .672 .825 .358 .108

.000

.059

.692

.990

.869

.157

.999 ,078 .415 .456 .525

1.1 -8.4

0.0 -8.2 0.0

-19.4 2.0 -7.0 22.1ft

-11.6 0.9

21. Oft 15.9 -7.4 23.2ft 5.2 1.7

-5.2 -13.6 -100.0ft -10.4 -11.7 -3.0 -5.9 -0.8 -2.8

-15.4 -7.4 -2.5 2.5

0.0 • -9.0

-10.2 -12.1 -18.9 -13.3 -9.0

-19.9 .-10.6 -9.8

-12.3 -13.4 7.8

-27.1# -18.5 67.8#

0.0 -0.6 -0.8 7.6

-1.0 -9.0 4.7

-1.5 3.7 0.8 7.8

76 83

72 76 72 82 63 76 54 83 71 69 61 77 56 69 71 77 79 68

79 75 74 72 73 73 76 73 72 79

75 75 72 77 79 77 75 81 76 77 76 73 59 82 82 49#

75 78 77 75 85 78. 74 78 77 74 76

-0.03 -0.03

-0.05 -0.03 -0.02 -0.04 -0.04 -0.03 -0.08 -0.04 -0.05 -0.03 -0.04 -0.03 -0.04 -0.04 -0.03 -0.02 -0.05 -0.05

-0.04 -0.03 -0.04 -0.05 -0.03 -0.04 -0.03 -0.03 -0.04 -0.03

-0.04 -0.04 -0.03 -0.03 -0.04 -0.04 -0.05 -0.04 -0.04 -0.03 -0.03 -0.04 -0.03 -0.04 -0.03 -0.05

-0.05 -0.04 -0.04 -0.04 -0.05 • -0.04 -0.03 -0.04 -0.03 -0.03

-0.04 2 8

G

C

Continuing Calibration Summary Job Number: N4873 Account: GESNJ Groundwater & Enviroimiental Services Project: Fleet Bank, Wall, NJ

Page 3 of 3

99 M tert-butylbenzene 100 M 1,2,4-trimethyIbenzene 101 M vinyl toluene 102 M pentachloroethane 103 M sec-butylbenzene 104 M p-isopropyltoluene'-105 M 1,3-dichlorobenzene 106 M 1,4-dichlorobenzene 107 M n-butylbenzene 10 8 M 1,2-dichlorobenzene 109 M hexachloroethane 110 M 1,2-dibromo-3-chloropropane 111 M 1,2,4-trichlorobenzene 112 M hexachlorobutadiene 113 M naphthalene 114 M 1,2,3-trichlorobenzene

Sei

2 2 0 0 2 2 1 1 2 1 0 0 0 0 0 0

-vices

019 316 000 877 800 3 1 4 464 596 027

. 4 6 4

. 7 5 0 2 7 1 756 770 9 0 1

. 6 4 6

2 2 0 0 2 2 1 1 2 1 0 0 0 0 0 0

Sample: Lab FilelD:

093 3 4 7 000 968 7 3 0 3 1 7 4 5 4 608 019

. 4 1 4 868

. 2 8 4 819 809 873

. 5 8 0

- 3 - 1

0 - 1 0

2 - 0

0 - 0

0 3

- 1 5 - 4 - 8 - 5

3 10

VI2008-CC1986 I50139.D

7 3 0 4 5 1 7 8 4 4 7

. 8 3 1 1

. 2

79 76

Oft 82 74 76 76 77 73 75 82 80 74 79 7 1 62

- 0 . 0 3 - 0 . 0 4 - 0 . 0 2 - 0 . 0 4 - 0 . 0 4 - 0 . 0 3 - 0 . 0 4 - 0 . 0 4 - 0 . 0 3 - 0 . 0 3 - 0 . 0 3 - 0 . 0 4 - 0 . 0 3 - 0 . 0 3 - 0 . 0 3 - 0 . 0 3

Average % D = 9.3

(ft) = Out of Range 149372.D MI1986.M

SPCC's out = 0 CCC's out = 0 Tue Jan 01 09:44:01 2002 GCMSI

G

29

G

G

G

G

G

G

G

Continuing Calibration Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI2009-CC1986 I50158.D

Page 1 of 3


Data File Acq On Sample Misc

C:\HPCHEM\1\DATA\I50158.D 29 Dec 2001 10:06 am CC1986-50 .MS58651,VI20 09,10,,100,25,1

Vial: 29 Operator: RUIFENGY Inst : MSI Multiplr: 1.00

MS Integration Params: RTEIN2.P


Min. RRF Max. RRF Dev

C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 ' Mon Dec 10 16:29:00 2001 Multiple Level Calibration

0.000 20%

Min. Max.

Rel, Rel.

Area Area

50% 150%

Max. R.T. Dev 0.50min

Compound AvgRF CCRF %Dev Area% Dev(min)

1 I Tert Butyl Alcohol-d9 2 M tertiary butyl alcohol

3 I pentafluorobenzene 4 M chlorodifluoromethane 5 M dichlorodifluoromethane 6 M Dichlorotetrafluoroethane 7 M chloromethane 8 M vinyl chloride 9 M 1,3-butadiene

10 M bromomethane 11 M chloroethane 12 M trichlorofluoromethane 13 M ^ ethyl ether 14 M acrolein 15 M freon 113 16 M acetone 17 M 1,1-dichloroethene 18 M acetonitrile 19 M iodomethane 20 M methyl acetate 21 M allyl chloride 22 M methylene chloride 23 M carbon disulfide 24 M acrylonitrile 25 M methyl tert butyl ether 26 M trans-1,2-dichloroethene 27 M hexane 28 M di-isopropyl ether 29 M 1,1-dichloroethane 30 M ' vinyl acetate 31 M chloroprene 32 M ethyl tert-butyl ether 33 M 2-butanone 34 M 2,2-dichloropropane 35 M ethyl acetate 36 M cis-1,2-dichloroethene 37 M methacrylonitrile 38 M chloroform 39 M bromochloromethane 40 M tetrahydrofuran 41 M 1,1,1-trichloroethane

1.000 1.304

1.000 0.497 0 .414 0.346 0.236 0.209 0.055 0.278 0.132 0.781 0.107 0.017 0.512 0.071 0.291 0.010 0.902 0.152 0.372 0.310 0.715 0.000 0.865 0.352 0.277 1.127 0.675 0.051 0.515 1.130 0.071 0.517 0.210 0.355 0.159 0.928 0.250 0.048 0.819

1.000 1.436

1.000 0.497 0.361 0.249 0.208 0.197 0.048 0.279 0.132 0.903 0.106 0.011 0.581 0.066 0.273 0.010 0.872 0.179 0.342 0.289 0.624 0.033 0.859 0.334 0.210 1.071 0.657 0.040 0.524 1.123 0.073 0.350 0.198 0.345 0.162 0.946 0.259 0.051 0.918

0.0 -10.1

0.0 0.0

12.8 28.Oft 11.9 5.7

12.7 -0.4 0.0

-15.6 0.9

35.3# -13.5

7.0 6.2 0.0 3.3

-17.8 8.1 6.8

12.7 0.0 0.7 5.1

24.2# 5.0 2.7

21.6ft -1.7 0.6

-2.8 32.3# 5.7 2.8 -1.9 -1.9 -3.6 -6.2

-12.1

76 79

74 72 64 53 65 71 59 74 73 82 69 49ft 81 87 66 69 71 83 68 72 63 Oft

76 69 57 70 72 51 71 74 80 47# 68 69 . 69 76 71 68 77

-0.02 -0.02

-0.04 0.00

-0.02 -0.05 0.02

-0.02 -0.02 -0.02 -0.02 -0.04 -0.05 0.00

-0.02 0.00 -0.02 0.00

-0.02 -0.02 -0.04 -0.03 -0.04 -0.03 -0.02 -0.02 -0.02 -0.03 -0.04 -0.07 -0.03 -0.02 -0.03 -0.03 -0.02 -0.04 -o;o5 -0.04 -0.05 -0.03

-0.033O

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Continuing Calibration Summary Job Number: N4873 Account: Project:

42 4 3

44 4 5 46 47 4 8 49 50-5 1 52 53 54 55 56 57 58 59

' 60 6 1 62 63 64 65 66 67 68 69 70 7 1

72 73 74 75 76 77 78 79 80 8 1 82 83 84 85 86 87

88 89 90 9 1 92 93 94 95 96 97 98

S S

I M M M M M M M M M M M M M M M M M M M M M S M M M M M

I M M M M M M M M M M M M M

M

I S M M M M M M M M M

GESNJ Groundwater & Environmental Services Fleet Bank, Wall, NJ

d i b r o m o f l u o r o m e t h a n e (s) 1 , 2 - d i c h l o r o e t h a n e - d 4 (s)

1 , 4 - d i f l u o r o b e n z e n e 1 , 1 - d i c h l o r o p r o p e n e i s o p r o p y l a c e t a t e c a r b o n t e t r a c h l o r i d e c y c l o h e x a n e t e r t - a m y l m e t h y l e t h e r h e p t a n e 1, 2 - d i c h l o r o e t h a n e b e n z e n e D i - i s o b u t y l e n e e t h y l a c r y l a t e t r i c h l o r o e t h e n e m e t h y 1 e y e l o h e x a n e 1 , 2 - d i c h l o r o p r o p a n e p r o p y l a c e t a t e m e t h y l m e t h a c r y l a t e b r o m o d i c h l o r o m e t h a n e 1 , 4 - d i o x a n e d ib romomethane 2 - c h l o r o e t h y l v i n y l e t h e r 4 - m e t h y l - 2 - p e n t a n o n e e i s - 1 , 3 - d i c h l o r o p r o p e n e t o l u e n e - d 8 (s) t o l u e n e

. t r a n s - 1 , 3 - d i c h l o r o p r o p e n e e t h y l m e t h a c r y l a t e 1 , 1 , 2 - t r i c h l o r o e t h a n e 2 - h e x a n o n e

c h l o r o b e n z e n e - d 5 1 , 3 - d i c h l o r o p r o p a n e b u t y l a c e t a t e t e t r a c h l o r o e t h e n e d i b r o m o c h l o r o m e t h a n e 1 , 2 - d i b r o m o e t h a n e c h l o r o b e n z e n e 1 , 1 , 1 , 2 - t e t r a c h l o r o e t h a n e e t h y l b e n z e n e m , p - x y l e n e o - x y l e n e s t y r e n e b u t y l a c r y l a t e bromoform 1 - c h l o r o h e x a n e e y e 1 o h e x a n o n e

l , 4 - d i e h l o r o b e n z e n e - d 4 4 - b r o m o f l u o r o b e n z e n e (s) i s o p r o p y l b e n z e n e 1 , 1 , 2 , 2 - t e t r a c h l o r o e t h a n e 1 , 2 , 3 - t r i c h l o r o p r o p a n e t r a n s - 1 , 4 - d i c h l o r o - 2 - b u t e n e n - p r o p y l b e n z e n e b romobenzene 1 , 3 , 5 - t r i m e t h y I b e n z e n e 2 - c h l o r o t o l u e n e 4 - c h l o r o t o l u e n e

/

0 .713 0 . 5 2 1

1.000 0 .583 1.662 0 .942 0 .353 0 .964 0 .344 0 .717 0 .859 1 .141 0 .333 0 .542 0 .405 0 .405 0 .407 0 .194 0 .996 0 . 0 0 1 0 .498 0 .128 0 . 1 0 1 0 . 5 9 1 0 .906 0 .615 0 .493 0 .418 0 .322 0 .199

1.000 0 .675

, 0 . 1 8 7 0 .827 1.033 0 .690 1.022 0 .703 1.574 0 .563 0 .553 0 . 8 5 1 0 .729 0 .649 0 .302 0 .335

1.000 1.053 2 . 6 7 1 1 .071 0 .860 0 .144 3 .146 1.062 2 .507 2 . 4 7 5 2 . 7 3 8

Sample: Page 2 of 3

VI2009-CC1986 Lab FilelD: I50158.D

0 . 7 1 1 0 .565

1.000 0 .609 1.517 1.084 0 .329 1.040 0 .175 0 . 7 9 1 0 .858 0 .829 0 .255 0 .562 0 .275 0 .395 0 .425 0 .204 1.115 0 . 0 0 1 0 .545 0 .135 0 .100 0 .587 0 .923 0 .628 0 .523 0 .447 0 .339 0 . 2 0 1

1.000 0 .735 0 . 2 0 1 0 .905 1.212 0 .772 1.099 0 .824 1.659 0 .604 0 .616 0 . 9 5 1 0 .636 0 .792 0 .348 0 .105

1.000 1.054 2 . 7 0 1 1.014 0 .852 0 . 1 4 1 3 .028 1 .091 2 . 4 3 1 2 . 3 8 7 2 . 8 1 9

0 . 3 - 8 . 4

0 . 0 - 4 . 5

8 . 7 - 1 5 . 1

6 . 8 - 7 . 9 49.1ft

- 1 0 . 3 0 . 1

27.3ft 23.4ft - 3 . 7 32.1ft

2 . 5 - 4 . 4 - 5 . 2

- 1 1 . 9 0 . 0

- 9 . 4 - 5 . 5

1 .0 0 . 7

- 1 . 9 - 2 . 1 - 6 . 1 - 6 . 9 - 5 . 3 - 1 . 0

0 . 0 - 8 . 9 - 7 . 5 - 9 . 4

- 1 7 . 3 - 1 1 . 9

- 7 . 5 - 1 7 . 2

- 5 . 4 - 7 . 3

- 1 1 . 4 , - 1 1 . 8

1 2 . 8 -22.Oft - 1 5 . 2

68 .7#

0 . 0 - 0 . 1 - 1 . 1

5 . 3 0 . 9 2 . 1 3 . 8

- 2 . 7 3 . 0 3 . 6

- 3 . 0

74 80

70 7 1 64 77 58 74 34ft 80 70 62 54 72 48ft 69 73 75 76 . 59 76 68 69 65 72 70 68 70 72 80

73 74 69 74 77 74 73 77 70 74 74 70 55 77 78 46ft

72 75 74 73 80 67 72 75 75 68 81

- 0 . 0 3 - 0 . 0 4

- 0 . 0 5 - 0 . 0 5 - 0 . 0 4 - 0 . 0 2 - 0 . 0 7 - 0 . 0 5 - 0 . 0 9 - 0 . 0 5 - 0 . 0 5 - 0 . 0 4 - 0 . 0 6 - 0 . 0 3 - 0 . 0 4 - 0 . 0 5 - 0 . 0 4 - 0 . 0 3 - 0 . 0 4 - 0 . 0 4 - 0 . 0 3 - 0 . 0 3 - 0 . 0 6 - 0 . 0 5 - 0 . 0 4 - 0 . 0 4 - 0 . 0 4 - 0 . 0 4 - 0 . 0 4 - 0 . 0 3

- 0 . 0 5 - 0 . 0 5 - 0 . 0 3 - 0 . 0 4 - 0 . 0 4 - 0 . 0 4 - 0 . 0 5 - 0 . 0 4 - 0 . 0 3 - 0 . 0 3 - 0 . 0 5 - 0 . 0 4 - 0 . 0 3 - 0 . 0 4 - 0 . 0 5 ' - 0 . 0 4

- 0 . 0 6 -0..04 - 0 . 0 4 - 0 . 0 3 - 0 . 0 5 - 0 . 0 4 - 0 . 0 4 - 0 . 0 4 - 0 . 0 3 - 0 . 0 4 -0.04 ' O X

G


Page 3 of 3

99 10 0 101 102 103 104 105 106 107 108 109 110

- Ill 112 113 114

M M M M M M M M M M M M M M M M

tert-butylbenzene 1,2,4 -trimethylbenzene vinyl toluene pentachloroethane sec-butylbenzene p-isopropyltoluene 1,3-dichlorobenzene 1,4-dichlorobenzene n-butylbenzene 1,2-dichlorobenzene hexachloroethane 1,2-dibromo-3-chloropropane 1,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1,2,3-trichlorobenzene

3ei

2 2 0 0 2 2 1 1 2 1 0 0 0 0 0 0

•vices

019 316 000 877 800 314 464 596 027 464 750 271 756 770 901 646

2 2 0 0 2 2 1 1 1 1 0 0 0 0 0 0

Sample: Lab FilelD:

102 367 000 972 688 248 450 562 869 439 842 274 716 737 787 537

-4 -2 0

-10 4 2 1 2 7 1

-12 -1 5 4 12 16

VI2009-CC1986 I50158.D

1 2 0 8 0 9 0 1 8 7 3 1 3 .3 .7 .9

76 74 Oft

79 70 70 73 72 65 73 76 74 61 69 62 55

-0.03 -0.04 -0.02 -0.05 -0.04 -0.04 -0.05 -0.04 -0.05 -0.03 -0.05 -0.04 -0.03 -0.02 -0.03 -0.02

Average % D = 8.9

G

G

G

(#) = Out of Range 149372.D MI1986.M


32

G

G

G

G

G

G

G

G

Continuing Calibration Summary Job Number: N4873 Accoimt: GESNJ Groundwater & Enviroimiental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FileH):

VI2012-CC1986 15025 I.D

Page 1 of 3


C:\HPCHEM\1\DATA\I50251.D 1 Jan 2002 12:36 am

CC1986-50 MS58809,VI2012,1,,100,25,1

Data File Acq On Sample Misc MS Integration Params: RTEIN2.P


14 RUIFENGY MSI 1.00


Min. RRF Max. RRF Dev

C:\HPCHEM\1\METHODS\MI1986.M SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Multiple Level Calibration

(RTE Integrator)

0.000 20%

Min. Max.

Rel. Rel.

Area Area

50% 150%

Max. R.T. Dev 0.50min

Compound AvgRF CCRF

1 I Tert Butyl Alcohol-d9 2 M tertiary butyl alcohol

3 I pentafluorobenzene 4 M chlorodifluoromethane 5 M dichlorodifluoromethane 6 M Dichlorotetrafluoroethane 7 M chloromethane 8 M vinyl chloride 9 M 1,3-butadiene

10 M bromomethane 11 M chloroethane 12 M trichlorofluoromethane 13 M ethyl ether 14 M acrolein 15 M freon 113 ' 16 M acetone 17 M 1,1-dichloroethene 18 M acetonitrile 19 M • iodomethane 20 M methyl acetate 21 M allyl chloride 22 M methylene chloride 23 M carbon disulfide 24 M acrylonitrile 25 M methyl tert butyl ether 26 M trans-1,2-dichloroethene 27 M hexane 28 M di-isopropyl ether 29 M 1,1-dichloroethane 30 M vinyl acetate 31 M chloroprene 32 M ethyl tert-butyl ether 33 M 2-butanone 34 M 2,2-dichloropropane 35 M ethyl acetate 36 M cis-1,2-dichloroethene 37 M methacrylonitrile 3 8 M chloroform 39 M bromochloromethane 40 M tetrahydrofuran 41 M 1,1,1-trichloroethane

%Dev Area% Dev(min)

1 1

1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0

000 304

000 497 414 346 236 209 055 278 132 781 107 017 512 071 291 010 902 152 372 310 715 000 865 352 277 127 675 .051 .515 .130 .071 .517 .210 .355 .159 .928 .250 .048 .819

1.000 1.442

1.000 0.486 0.407 0.277 0.227 0.223 0.051 0.318 0.150 1.020 0.110 0.014 0.422 0.062 0.285 0.010 0.918 0.189 0.346 0.301 0.683 0.033 0.854 0.344 0.228 1.074 0.654 0.050 0.538 1.101 0.056 0.490 0.201 0.358 0.158 0.949 0.259 0.050 0.949

0 -10

0 2 1

19 3

-6 7

-14 -13 -30 -2 17 17 12 2 0

-1 -24

7 2 4 0 1 2

17 4 3 2

-4 2

21 5 4 -0 0

-2 -3 -4

-15

0 6

0 2 7 9 8 7 3 4 6 6# 8 6 6 7 1 0 8 3# 0 9 5 0 3 3 7 7 1 .0 .5 .6 .1# .2 .3 .8 .6 .3 .6 .2 .9

65 68

71 68 70 56 68 77 59 81 79 89 68 56 56 78 66 64 71 84 66 72 66

Oft 73 68 59 67 69 61 70 69 59 63 66 68 64 . 73 69 63 76

-0.01 -0.03

-0.02 0.00

-0.01 -0.04 0.00 0.04

-0.05 -0.02 -0.01 -0.02 -0.05 -0.02 0.00

-0.04 -0.03 -0.01 -0.03 -0.02 -0.03 -0.02 -0.03 -0.03 -0.01 0.00

-0.03 -0.02 -0.05 -0.06 -0.02 -0.01 -0.02 -0.01 -0.03 -0.03 -0.03 -0.04 -0.04 -0..01 -0.03 33

G

G

G

G

G

G

G

Continuing Calibration Summary Job Number: N4873 Accoxmt: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI2012-CC1986 15025 I.D

Page 2 of 3

42 S 43 S

44 I 45 M 46 M 47 M 48 M 49 M 50 M 51 M 52 M 53 M 54 M 55 M 56 M 57 M 58 M 59 M 60 M 61 M 62 M 63 M 64 M 65 M 66 S 67 M 68 M 69 M 70 M 71 M


88 I 89 S 90 M 91 M 92 M 93 M 94 M 95 M 96 M 97 M 98 M

dibromofluoromethane (s) l,2-dichloroethane-d4 (s)

1,4-difluorobenzene 1,1-dichloropropene isopropyl acetate carbon tetrachloride cyclohexane tert-amyl methyl ether heptane 1,2-dichloroethane benzene Di-isobutylene ethyl acrylate trichloroethene methy1eyelohexane 1,2-dichloropropane propyl acetate methyl methacrylate

• bromodichloromethane 1,4-dioxane dibromomethane 2-ehloroethyl vinyl ether 4-methyl-2-pentanone cis-1,3-dichloropropene toluene-d8 (s) toluene trans-1,3-dichloropropene ethyl methacrylate 1,1,2-trichloroethane 2-hexanone

chlorobenzene-d5 1,3-dichloropropane butyl acetate tetrachloroethene dibromochloromethane 1,2-dibromoethane chlorobenzene 1,1,1,2-tetrachloroethane ethylbenzene m,p-xylene o-xylene styrene butyl acrylate bromoform 1-chlorohexane eyelohexanone

1,4-dichlorobenzene-d4 4-bromofluorobenzene (s) isopropylbenzene 1,1,2,2-tetrachloroethane 1,2,3-trichloropropane trans-1,4-dichloro-2-butene n-propylbenzene bromobenzene 1,3,5-trimethyIbenzene 2-chlorotoluene 4 -chlorotoluene

0.713 0.521

1.000 0.583 -1.662 0.942 0.353 0.964 0.344 0.717 0.859 1.141 0.3,33 0.542 0.405 0.405 0.407 0.194 0.996 0.001 0.498 0.128 0.101 0.591 0.906 0.615 0.493 0.418 0.322 0.199

1.000 0.675 0.187 0.827 1.033 0.690 1.022 0.703 1.574 0.563 0.553 0.851 0.729 0.649 0.302 0.335

1.000 1.053 2.671 1.071 0.860 0.144 3.146 1.062 2.507 2.475 2.738

0.689 0.546

1.000 0.648 1.583 1.139 0.385 1.065 0.188

• 0.821 0.893 0.889 0.281 0.590 0.293 0.389 0.417 0.206 1.144 0.001 0.565 0.127 0.101 0.642 0.896 0.651 0.557 0.465 0.346 0.203

1.000 0.740 0.204 0.939 1.209 0.791 1.154 0.849 1.745 0.628 0.646 0.985 0.661 0.817 0.360 0.094

1.000 0.996 2.700 1.000 0.830 0.147 3.013 1.107 2.419 2.597 2.579

3.4 -4.8

0.0 -11.1

4.8 -20.9ft -9.1

-10.5 45.3# -14.5 -4.0 22.1# 15.6 -8.9 27.7# 4.0

-2.5 -6.2

-14.9 0.0

-13.5 0.8 0.0

-8.6 1.1

-5.9 -13.0 •-11.2

-7.5 -2.0

0.0 -9.6 -9.1

-13.5 -17.0 -14.6 -12.9 -20.8# -10.9 -11.5 -16.8 -15.7

9.3 -25.9# -19.2 71. 9#

0.0 5.4

-1.1 6.6 3.5

-2.1 4.2 -4.2 3.5

-4.9 5.8

69 74

66 71 63 76 64 72 35ft 78 69 63 56 72 48# 64 68 71 74 57 74 60 66 68 66 69 68, 69 69 76

69 70 66 72 72 71 72 75 70 72 73 69 53 75 76 39ft

70 69 72 71 76 68 70 75 72 73 73

-0.03 -0.02

-0.06 -0.01 -0.01 -0.03 -0.03 -0.04 -0.09 -0.03 -0.03 -0.02 -0.05 -0.02 -0.05 -0.03 -0.02 -0.02 -0.03 -0.04 -0.03 -0.03 -0.02 -0.04 -0.04 -0.03' -0.03 -0.03 -0.03 -0.03

-0.02 -0.03 -0.02 -0.02 -0.03 -0.03 -0.02 -0.03 -0.03 -0.02 -0.03 -0.02 -0.02 -0.03 -0.02 -0.03

-0.03 -0.02 -0.02 -0.03 -0.03 • -0-..03 -0.01 -0.02 -0.01 -0.03

-0.02 3 4

G

G

G


Page 3 of 3

99 M tert-butylbenzene 100 M 1,2,4-trimethyIbenzene 101 M vinyl toluene 102 M pentachloroethane 103 M sec-butylbenzene 104 M p-isopropyltoluene 105 M 1,3-diehlorobenzene 106 M 1,4-dichlorobenzene 10 7 M n-butylbenzene 10 8 M 1,2-dichlorobenzene 10 9 M hexachloroethane 110 M 1,2-dibromo-3-chloropropane 111 M 1,2,4-trichlorobenzene 112 M hexachlorobutadiene 113 M naphthalene 114 M 1,2,3-trichlorobenzene

Sei

2 2 0 0 2 2 1 1 2 1 0 0 0 0 0 0

•vices

019 3 1 6 000 877 800 314 464 596 027 464 750

. 2 7 1

. 7 5 6

. 7 7 0

. 9 0 1

. 6 4 6

2. 2 0 0 2 2 1 1 1 1 0 0

- 0 0 0 0

Sample: Lab FilelD:

104 4 0 2 000 990 732 2 9 8 4 7 1 6 2 7 946 4 3 6 862 280 7 9 5

. 7 7 4

. 8 7 4 5 7 1

- 4 - 3

0 - 1 2

2 0

- 0 - 1

4 1

- 1 4 - 3 - 5 - 0

3 1 1

VI2012-CC1986 150251.D

2 7 0 9 4

. 7

. 5

. 9 0 9 9

. 3

.2

. 5

. 0

. 6

74 73

Oft 78 70 70 72 73 66 7 1 76 73 67 7 1 67 57

- 0 . 0 3 - 0 . 0 2

0 . 0 0 - 0 . 0 3 - 0 . 0 2 - 0 . 0 3 - 0 . 0 3 - 0 . 0 1 - 0 . 0 2 - 0 . 0 2 - 0 . 0 3 - 0 . 0 3 - 0 . 0 2 - 0 . 0 2 - 0 . 0 2 - 0 . 0 2

Average % D = 9.2

(ft) = Out of Range 149372.D MI1986.M


G

G

G

35

G

G

G

C

G

G


Page 1 of 1

Sample: ' VI1986-BFB1 Lab File ID: i49368.D Instrument ID: GCMSI


m/e Ion Abimdance Criteria Raw Abundance


50 75 95 96 173 174 175 176 177


9437 23187 39587 2726 81 28869 2145 28443 1828

23.8 58.6 100.0 6.9 0.2 72.9 5.4 71.8 4.6

(0.28) a

(7.4) a (98.5) a (6.4) b




Lab Sample ID

VI1986-1C1986 VI1986-IC1986 VI1986-1CC1986 VI1986-IC1986 VI1986-IC1986 VI1986-IC1986 VI1986-IC1986 VII 986-MB 1 ZZZZZZ ZZZZZZ

Lab FilelD

I49370.D 149371.D I49372.D 149373. D I49374.D I49375.D I49379.D 149383.D I49384.D I49385.D

Date Analyzed

12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01

Time Analyzed

11:12 11:52 12:31 13:10 13:50 14:29 17:08 19:46 20:25 21:04

Hours Lapsed

01:18 01:58 02:37 03:16 03:56 04:35 07:14 09:52 10:31 11:10

CUent Sample ID

Initial eal 5 Initial eal 20 Initial eal 50 Initial eal 10 Initial eal 1 Initial eal 100 Initial eal 400 Method Blank (unrelated sample) (unrelated sample)

36

G

G

G

G

G

G

G

Volatile Internal Standard Area Summary Job Number: N4873 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 1

Check Std: Lab File ID: Instrument ID:

Check Std Upper Limit ^ Lower Limit ^

VI2008-CC1986 I50139.D GCMSI

I S I AREA

63144 126288 31572

RT

5.87 6.37 5.37

IS 2 AREA

343119 686238 171560

Injection Date: 12/28/01 Injection Time: 21:44 Method: SW846 8260B

IS 3 RT AREA

9.62 305354 10.12 610708 9.12 152677

IS 4 RT AREA

11.61 238122 12.11 476244 11.11 119061

RT

17.72 18.22 17.22

IS 5 AREA

158873 317746 79437

RT

22.09 22.59 21.59

Lab Sample ID

VI2008-MB2 VI2008-BS ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ VI2009-MB1 VI2009-BS ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ

I S I IS 2 IS 3 IS 4 IS 5

I S I AREA

60570 65727 62854 62506 63098 64574 62068 60840 56578 59351 61501 57564 62012 59283 52715 59344

RT

5.83 5.84 5.88 5.88 5.91 5.84 5.90 5.88 5.82 5.86 5.88 5.89 5.93 5.88 5.91 5.89

Tert Butyl Alcohol-D9 Pentafluorobenzene 1,4-Difluorobenzene Chlorobenzene-D5

IS 2 AREA

345169 345780 353336 365887 362372 347678 351665 351895 329316 332453 343905 342788 348213 353287 355530 353379

1,4-Dichlorobenzene-d4

RT

9.62 9.63 9.61 9.62 9.62 9.60 9.61 9.62 9.61 9.63 9.63 9.63 9.61 9.62 9.63 9.63

IS 3 AREA

308729 303198 316617 321244 328036 318060 317092 313704 299996 298460 313489 311513 313872 315322 322376 316796

RT

11.60 11.61 11.61 11.60 11.60 11.60 11.60 11.59 11.60 11.60 11.61 11.61 11.60 11.60 11.62 11.62

IS 4 AREA

243116 237723 252531 254923 257764 248710 250119 250824 236583 232557 249728 245356 247561 255779 251149 249168

RT

17.72 17.73 17.72 17.72 17.71 17.72 17.72 17.72 17.72 17.71 17.72 17.72 17.72 17.72 17.73 17.72

IS 5 AREA

127739 159689 156004 145901 144128 136599 143635 142782 119021 155583 136075 130728 136321 142901 137766 138768

RT

22.10 22.09 22.10 22.09 22.10 22.09 22.09 22.09 22.09 22.09 22.09 22.09 22.09 22.09 22.09 22.09

(a) Upper Limit = +100% of check standard area; Retention time -1-0.5 minutes. (b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.

37

G

C

G

G


Page 1 of 1

—

— '

n

Check Std: Lab File ID: Instriunent ID:

Check Std Upper Limit ^ Lower Limit

VI2009-CC1986 150158.D GCMSI

I S I AREA

59723 119446 29862

RT

5.84 6.34 5.34

IS 2 AREA

331250 662500 165625

Iiyection Date: 12/29/01 Injection Time: 10:06 Method: SW846 8260B

IS 3 IS 4 IS 5 RT AREA RT AREA RT AREA

9.62 296704 11.61 232961 17.71 151926 10.12 593408 12.11 465922 18.21 303852 9.12 148352 11.11 116481 17.21 75963

RT

22.08 22.58 21.58

Lab IS 1 Sample ID AREA

VI2009-MB2 62317 N4921-18 51994 N4921-18MS c 61070 N4921-18MSD <: 59238 ZZZZZZ 61965 ZZZZZZ 62578 N4873-1d 39232

RT

5.84 5.88 5.88 5.88 5.91 5.88 6.02

IS 1 = Tert Butyl Alcohol-D9 IS 2 = Pentafluorobenzene IS 3 = 1,4-Difluorobenzene IS 4 = Chlorobenzene-D5

IS 2 AREA

320498 342241 344807 349856 355308 349421 382021

IS 5 =1,4-Dichlorobenzene-d4

RT

9.61 9.62 9.63 9.62 9.62 9.63 9.61

IS 3 AREA

289223 309789 310820 312070 321436 315524 329380

RT

11.61 11.60 11.61 11.61 11.61 11.61 11.62

IS 4 AREA

228542 244028 235543 242432 251025 247993 263548

RT

17.72 17.72 17.73 17.73 17.73 17.73 17.73

V

IS 5 AREA

119845 134974 161019 157411 144161 136389 166348

RT

22.10 22.10 22.09 22.10 22.10 22.10 22.10

(a) Upper Limit = -1-100% of check standard area; Retention time +0.5 minutes. (b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes. (c) Methanol preservation/extraction. (d) Methanol preservation/extraction. Confirmation run. Sample was reanalyzed due to carry-over.

38

G

G

G

G

G

G

G

G


Page 1 of 1


Check Std Upper Limit Lower Limit''

VI2012-CC1986 15025 I.D GCMSI

I S I AREA

51160 102320 25580

RT

5.86 6.36 5.36

IS 2 AREA

317562 635124 158781

Injection Date: 01/01/02 Injection Time: 00:36 Method: SW846 8260B

IS 3 RT AREA

9.64 279959 10.14 559918 9.14 139980

IS 4 RT AREA

11.61 218977 12.11 437954 11.11 109489

RT

17.74 18.24 17.24

IS 5 AREA

148421 296842 74211

RT

22.11 22.61 21.61

Lab Sample ID

VI2012-MB1 ZZZZZZ N4873-1= ZZZZZZ ZZZZZZ ZZZZZZ N5247-4 ZZZZZZ VI2012-BS N5247-4MS

I S I AREA

50178 51050 55853 54585 52909 55695 53493 54595 56944

d 55797 N5247-4MSD'* 51130 ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ

I S I IS 2 IS 3 IS 4 IS 5

53288 53447 54600 56522

RT

5.87 5.89 5.91 5.88 5.91 5.89 5.92 5.92 5.84 5.92 5.91 5.88 5.89 5.92 5.89

Tert Butyl Alcohol-D9 Pentafluorobenzene 1,4-Difluorobenzene Chlorobenzene-D5

IS 2 AREA

300284 323549 329675 327524 330042 332816 329165 329767 316414 326583 330699 330311 336601 333582 335204

1,4-Dichlorobenzene-d4

RT

9.64 9.64 9.63 9.64 9.63 9.64 9.64 9.64 9.63 9.63 9.63 9.64 9.64 9.63 9.63

IS 3 AREA

270204 290772 292461 290283 290149 293964 291718 296214 278138 289285 293475 291281 297315 297711 298515

RT

11.61 11.61 11.63 11.63 11.61 11.62 11.61 11.64 11.62 11.63 11.62 11.61 11.63 11.62 11.62

IS 4 AREA

212212 226210 228865 227669 233433 231627 230252 229992 219092 223453 231280 234019 232742 231541 232385

RT '

17.74 17.74 17.74 17.74 17.74 17.74 17.73 17.74 17.75 17.73 17.74 17.74 17.73 17.73 17.74

IS 5 AREA

108145 122846 125217 126519 127873 130627 124565 125770 142448 147334 146921 129009 125278 129218 126191

9

RT

22.11 22.11 22.11 22.11 22.11 22.10 22.10 22.12 22.11 22.11 22.10 22.10 22.10 22.11 22.11

(a) Upper Limit = -1-100% of check standard area; Retention time -1-0.5 minutes. (b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes. (c) Sample originally analyzed within the holding time. Methanol preservation/extraction. (d) Methanol preservation/extraction.

39

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50255.D Acq On- : 1 Jan 2002 3:13 am Sample : N4873-1 Misc : MS58 639,VI2012,3.9,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 8 13:33 2002

(QT Reviewed)




C:\HPCHEM\L\METHODS\MI1986, SW-846 Method 8260 Mon Dec 10 16:29:00 2001 , Initial Calibration MI1986

Quant Results File: MI1986.RES

M (RTE Integrator)

r- Internal Standards R.T. Qlon Response Cone Units Dev(Min)

G

G

G

G

G

G

G

1) Tert Butyl Alcohol-d9 5.91 3) pentafluorobenzene 9.63 44) 1,4-difluorobenzene 11.63 72) chlorobenzene-d5 17.74 88) 1,4-dichlorobenzene-d4 22.11

System Monitoring Compounds 42) dibromofluoromethane (s) Spiked Amount 50.000

43) l,2-dichloroethane-d4 (s; Spiked Amount 50.000 66) toluene-d8 (s) Spiked Amount 50.000 89) 4-bromofluorobenzene (s) Spiked Amount 50.000

Target Compounds

65 168 114 117 152

55853 329675 292461 228865 125217

500.00 PPb 50.00 PPb 50.00 PPb 50.00 PPb 50.00 PPb

0.04 -0.03 -0.03 -0.02 -0.03

9.89 113

10.86 65

14.76 98

20.00 174

213764 45.47 PPb -0.03 Recovery = 90.94%

164859 47.95 PPb -0.02 Recovery = 95.90%

256481 48.39 PPb -0.02 Recovery = 96.78%

139869 53.05 PPb -0.02 Recovery = 106.10%

Qvalue

^ / J l

'A $

(#) = qualifier out of range (m) = manual integration 150255.D MI1986.M Tue Jan 08 13:51:45 2002 GCMSI

40 Page 1

t:.

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50255.D Acq On : 1 Jan 2002 3:13 am Sample : N4873-1 Misc : MS58639,VI2012,3.9,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 8 13:33 2002

V i a l O p e r a t o r I n s t M u l t i p l r

18 RUIFENGY MSI 6 7 . 3 0



C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Initial Calibration

Abundance

190000

180000-

170000-

160000-

150000

140000

130000

120000

110000

100000

90000

80000

70000

60000

50000

40000

30000

20000-

10000-

U-' 1 •! 1

Time-> 2.00

,

7-rp""T 4.00

1 5

A • y - r i - i - T - i ' - r - i - t - r i -

6.00 8.00 1

(

0)' c 0)

^

^ tf "1? = am, a.

uoro

met

ha

,4-d

ifluo

rob

1^

ro

i n

CD C

^ Tp ^H

s- I L M . 1 1 1 '

0.00 12.00

TIC; I50255.D

m" T3

s •

u

CO

00 T3

L I I I I ' ' ' " ' • ! " ' • • ' ' • • ' ] ~ ^

14.00 16.00 18.00

U)

ene

(s)

e-d

4,1

NI C

! S

1

•

i. r*i—r^

20

j 1 i i > i •

L,

1 3

^ * * * * * - » - ' ' T . * r* —1—1 F^TM-T'-r*^—1—

00 22.00 24.00 26.00 . 28.00

150255.D MI1986.M Tue Jan 08 13:51:49 2002 GCMSI 41 . Page 2


LSC Area Percent Report

D C:\HPCHEM\1\DATA\I50255 1 Jan 2002 3:13 am

N4873-1 MS58 639,VI2012,3.9,,100,5,1



MS Integration Params: LSCINT.P

Method Title Smoothing Sampling Start Thrs Stop Thrs

C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator SW-846 Method 8260 ON . Filtering: 5 1 Min Area 0.1 Max Peaks 0.05 - Peak Location

1000 Area counts 100 TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal TIC

G

c

c

pea #

1 2 3 4 5

6 7 8 9

10

11 12 13 14 15

16 17 18 19 20

21 22 23 24 ; 25

26 27 28

k R.T. min

2.725 3.198 3.645 3.696 4.017

4.245 4.330 4.575 5.310 5.369

5.403 5.909 6.273 9.626 9.888

10.361 10.868 11.628 14.762 15.083

15.210 15.286 17.744 19.053 19.991

20.396 20.650 20.844

first scan

124 197 249 255 291

317 328 355 444 451

458 498 560 939 979

1044 1085 1178 1549 1605

1618 1628 1906 2068 2174

2232 2260 2285

max scan

143 199 252 258 296

323 333 362 449 456

460 520 563 960 991

1047 1107 1197 1568 1606

1621 1630 1921 2076 2187

2235 2265 2288

l^st scan

184 211 255 260 300

328 337 367 451 458

471 560 572 979

1026

1053 1144 1245 1605 1614

1628 1637 1962 2086 2228

2241 2268 2292

PK TY

rBV rVB rBV2 rVB2 rVB2

rVB rBV rBB rBV rVV2

rVB rBV5 rVB3 rBV2 rVB2

rVB rBV rBV3 rBV2 rVV2

rVV2 rVB2 rBV rBB rBV2

rVB3 rVB3 rVB3

peak height

143674 597 597 823 646

683 695 702 802

1055

1084 6825 809

117275 92985 .

621 50985

101429 99474 1218

524 449

128392 1049

162535

687 542 622

peak area

1285292 1726 1349 1064 1669

1390 1424 1838 18 91 3143

2982 97690 2872

1046504 790655

1348 402241 813414 755333

3795

2059 1075

824788 2321

954227

1444 1146 1290

peak % max.

100.00% 0.13% 0.10% 0.08% 0.13%

0.11% 0.11% 0.14% 0.15%. 0.24%

0.23% 7.60% 0.22%

81.42% 61.52%

0.10% 31.30% 63.29% 58.77% 0.30%

0.16% 0.08%

64.17% 0.18%

74.24%

0.11% 0.09% 0.10%

% of total

16 0 0 0 0

0 0 0 0 0

0 1 0

13 10

0 5

10 9 0

0 0 10 0

12

0 0 0

272% 022% 017% 013% 021%

018% 018% 023% 024% 040%

038% 237% 036% 249% 010%

017% 092% 298% 562% 048%

026% 014% 442% 029% 080%

018% 015% 016%

42

G

G

G

G

G

29 20.971 2301 2303 2307 rBV 780 1100 0..09% 0.014% 30 22.111 2425 2438 2471 rBV3 154470 872833 67.91% 11.050%

31 22.567 24-89 2492 2495 rBV3 563 1454 0.11% 0.018% 32 22.669 2499 2504 2506 rVV4 838 1545 0.12% 0.020% 33 22.728 2509 2511 2515 rVfi3 753 1254 0.10% 0.016% 34 22.838 2521 2524 2532 rVB3 529 1287 0.10% 0.016% 35 23.007 2537 2544 2548 rVB2 574 2049 0.16% 0.026%

36 .23.066 2548 2551 2555 rVB2 855 1506 0.12% 0.019% 37 23.142 2555 2560 2565 rBV3 683 2086 0.16% 0.026% 38 23.235 2568 2571 2574 rVB2 942 1546 0.12% 0.020% 39 23.294 2574 2578 2,582 rBV2 727 1535 0.12% 0.019% 40 24.003 2661 2662 2667 rVB 804 1040 0.08% 0.013%

41 25.051 2778 2786 2787 rBV2 587 1257 0.10% 0.016% 42 25.135 2792 2796 2800 rVB2 584 1452 0.11% 0.018% 43 27.610 3088 3089 3098 rVB 360 . 1037 0.08% 0.013%

Sum of corrected areas: 7898951

150255.D MI1986.M Tue Jan 08 13:59:00 2002 GCMSI

G

G

G

G

G

43

LSC Report - Integrated Chromatogram

File Operator Acquired Instrument Sample Name Misc Info Vial Number Quant File

C:\HPCHEM\1\DATA\I50255 . D RUIFENGY 1 Jan 2002 3:13 am using AcqMethod MI1986 MSI

N4873-1 MS58 639,VI2012,3.9,,100,5,1 18

MI1986.RES (RTE Integrator)

Abundance

150000

100000

TIC: I50255.D

50000

2.72

9.63

3.20 336H3 4.03^331.57 5 91

sasaro >-^6.27 ' I I ' ' ' ' I ' ' ' ' 1 ' ^ ' ' ' 1 ] ' ' I ' I I ' I ' I ' ' ' I I ' ' ' " ^ 1 ' I I ' I ' ~ ' ' ' ' I I I I I I I I i - i I ' I I I I I I I I I I I I M ' I ' ' I

2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7,50 8.00 8.50 9.00 9.50 10.00 Time~>

50000

' ' ' I I ' I ' I ' ' ' ' I ' • ' ' ' 1 " ^ ' ' ' I '

Time~> 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 Abundance

150000

100000

TIC: I50255.D

50000

19199 22.11

, vlp.'gD.gge<87 0 'i I I M I ' I M i ^ M ' I I I I I I

24,00 293D34 27.61 I I I I ' I I ' I I I ' ' I I I I ' I I I I ' ' ' I ' ' ' ' I I ' ' ' I ' ' ' ' I ' I I '

rime~> 19.50 20.00 20.50 21.00 21,50 22.00 22.50 23.00 23.50 24,00 24,50 25,00 25.50 26,00 26,50 27,00 27,50

44 150255.D MI1986.M Tue Jan 08 13:59:06 2002 GCMSI

Library Search Compound Report


N4873-1 MS58 639,VI2012,3.9, ,100,5,1

Data File Acq On Sample Misc MS Integration Params: LSCINT.P


C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 C:\DATABASE\NBS75K.L

Peak Number 1 Carbon dioxide Concentration Rank 1

Quant Method Title Library

R.T, EstConc Area Relative to ISTD R.T.

2.72 4132.82 PPb 1285290 pentafluorobenzene 9.63

G

c G

G

G

G

G

G

G

G

Hit# of Tentative ID MW Mo1Form CAS# Qual

1 Carbon dioxide 2 Carbon dioxide 3 Ethylene oxide 4 Ethylene oxide

4 4 C02 4 4 C02 44 C2H40 44 C2H40

0 0 0 1 2 4 - 3 8 - 9 4 0 0 0 1 2 4 - 3 8 - 9 4 0 0 0 0 7 5 - 2 1 - 8 3 0 0 0 0 7 5 - 2 1 - 8 3

(Abundance

5000

TjTTT rjT I I I I I I I I [I IT r p I I'l |T 1111 IT 1111111111111111111111 [ IT n p n I ] I n 1J111 r[TrTr[ n n ] ii 11 [ 1111 [ ii ii j i n 11111111 ii i -pn i j 11 ii ] n n

m/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

m/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Scan 143 (2,725 min): I50255,D (-) 44

40 46

#62263; Carbon dioxide 44

12 16 22 46

Abundance

5000-

#34: Carbon dioxide 44

16 22

m/z~>

46 | | " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " i " " l " " l " " l " " i " " l " " l " " l " " l " " i " " l " " l " " l " "

2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

#62267: Ethylene oxide 2|9

15

13 26

44

421

31 ,46 i | " " l " " l " " l " " l " l l | l l ' l | " " l ' l ' i | " i ' | i i " l " " l " " l " " l | i H l | l l M | i [ M | l l i l | i l i i | i i ' i i | i i ' i i | M i i | i n , | i i i i | n i i | i i i

m/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m / z 4 3 .9 , 100 .00%

I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' I I ' I 2,40 2.60 2,80 XOO

m/z 40. .05 2 .39%

2,40 2,60 2,80 3,00

m / z 4 5 . 0 ,

I ' ' ' ' I ' ' ' • I ' • ' ' I ' ' ' ' I 2.40 2,60 2,80 3,00

m / z 4 5 . 9 5 0.52%

I ' I I ' I ' I ' ' ' ' I ' I ' ' I

2,40 2.60 2,80 3,00


45 Page 1

Quantitation Report

Data File Acq On Sample Misc Quant Time

C:\HPCHEM\1\DATA\I50167.D 29 Dec 2001 3:57 pm N4873-1CF MS58 639,VI2009,3.9, ,100,5,1 Jan 8 14:29 2002


Quant Results File: temp.res


C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Multiple Level Calibration

Abundance 1400

1200

1000

800

600

400

200

0

Ion 65,00 (64.70 to 65,70); 150167,0 Ion 66.00 (65.70 to 66.70); 150167.D

I ' I ' ' • ' ' I I ' ' ' I ' ' ' ' I ' ' * ' I ' ' I 1' I I I ' I j I I 1 1 1 I I I M I I I I I I ' I ' I ' ' ' ' I ' I I ' I ' ' I I I I ' ' ' I I ' ' ' I ' ' ' I I I I I I I I ' I ' I I ' ' ' I 4,80 5,00 5,20 5,40 5,60 5,80 6,00 6,20 6,40 6,60 6,80 7,00 7,20 7,40 7,60 7.80 8,00 8,20 8.40 r ime->

Abundance

800

600

400

200

Scan 533 (6.023 min): 150167,D 615

46 44

42

35

91

' 5 5 " "6 'o"+l i f l 'd^^1^^-f^" ' I ' ' ' 75

" I I ' " I =1 " I ' -

85 Tl/Z-> 40 50 80 90 95 100

(1) Tert Butyl Alcohol-d9 (I)

6,02niin 500,00PPb m

response 39232

Ion Exp% Act%

65,00 100 100

66,00 25,00 0,00

0,00 0,00 0,00

0,00 0,00 0,00

150167.D MI1986.M Tue Jan 08 14:44:54 2002 GCMSI 46


Data File : C:\HPCHEM\1\DATA\I50167.D Acq On : 29 Dec 2001 3:57 pm Sample : N4873-1CF Misc : MS58639,VI2009,3.9,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 8 14:29 2002




C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Initial Calibration MI1986


c c

G

G

G

(s)

1) Tert Butyl Aleohol-d9 3) pentafluorobenzene

4'4) 1, 4-difluorobenzene 72) ehlorobenzene-d5 88) 1,4-diehlorobenzene-d4


43) 1,2-dichloroethane-d4 Spiked Tôunt 50.000

66) toluene-d8 (s) Spiked TVmount 50.000

89) 4-bromofluorobenzene Spiked Amount 50.000

Target Compounds 67) toluene 80) ethylbenzene 81) m,p-xylene 82) o-xylene

(s)

6.02 65 9.61 168

11.62 114 17.73 117 22.10 152

9.89 113

10.85 65

14.75 98

19.99 174

14.90 92 17.89 91 18.04 106 18.86 106

39232m 500.00 PPb 382021 , 50.00 PPb 329380 f' 50.00 PPb 263548 ' / r 50.00 PPb 166348 /r 50.00 PPb

0.16 -0.05 -0.05 -0.03 -0.04

250879 46.05 PPb. -0.02 Recovery = 92.10%

202200 50.75 PPb -0.03 Recovery = 101.50%

294430 49.33 PPb -0.03 Recovery = 98.66%

177252 50.60 PPb -0.03 Recovery = 101.20%

432087 17390. 23581 8046

7180.29 PPb 141.09 PPb 535.00 PPb 185.80 PPb

Qvalue 99 81 97

# 70

r

(#) = qualifier out of range (m) = 150167.D MI1986.M Tue Jan 08

manual integration 14:44:13 2002 GCMSI

47 Page 1

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50167.D Acq On : 29 Dee 2001 3:57 pm Sample : N4873-1CF Misc : MS58639,VI2009,3.9,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 8 14:29 2002





Abundance

2100000

2000000

1900000

1800000

1700000

1600000-

1500000-

1400000

1300000

1200000

1100000

1000000

900000

800000

700000

600000

500000

400000;

300000•

200000

100000-1

,A.

oca

i S C .Q

ceo •cE

TIC: 150167.D

Tlme-> 2.00 4.00 •I 'iS 'l ''I J—I I T

t-

P

^ t |N— -1 I 6.00 8.00 10,00 12,00 14,00 16,00 18,00 20,00 22,00 24.00 26.00 28,00

150167.D MI1986.M Tue Jan 08 14:44:18 2002 GCMSI Pag ge 2

#67 toluene Coneen: 7180.29 PPb RT: 14.90 min Seanft 1584 Delta R.T. -0.04 min Lab File: 150167.D Acq: 29 Dec 2001 3:57 pm

Tgt Ion: 92 Resp: •432087 Ion Ratio Lower Upper 92 100 91 172.9 142.7 202.7 65 28.6 0.0 54.2

Abundance Ion 92.00 (91.70 to 92,70); I50167,D 140000i|Q^ 91,00 (90,70 to 91,70): I50167,D

Ion 65.00 (64.70 to 65.70); 150167.D 120000-1

100000

20000

frime-> 14.60 14,80 15.00 15.20

Abundance

ReS)

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance

0

Scan 1943 (17,931 min); I49372.D (-) 9ll

39 47 65

l " l " l | ' " V | 78

53 5?|,| iT 84 , ' ' " I ' " I ' l " " ' l

131 106

•MrM

119

V ' I ' ' I ' I ' ' ' ' ' I l37 t T ' T I I 1 I

Raj(6

0

Scan 1938 (17,892 min); 150167,0 9|1

82

39 52 65

A1 I " ' ' I

117

106

T l

133 I ' ' ' ' I

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance

Sub 50

Scan 1938 (17,892 min): 150167,0 (-) 9|1

82

52 39 65

m J L

117

106

133

150b,/g.3>. D° • '3l^±']4^'8'^M' 60 ' ' 70 TBCe' • ^(^nic^8iii4 1^4 i^S' i^blf i i

#80 ethylbenzene Coneen: 141.09 PPb RT: 17.89 min Sean# 1938 Delta R.T. -0.04 min Lab File: 150167.D Acq: 29 Dee 2001 3:57 pm

Tgt Ion: 91 Resp: Ion Ratio Lower 91 100

106 15.6 0.0 65 6.9 0.0

17390 Upper

56 43

.5

.0

Abundance Ion 91,00 (90,70 to 91.70); 150167.0 Ion 106,00 (105,70 to 106,70); 150167. Ion 65.00 (64.70 to 65,70); 150167,0

12000

10000

0

ime~> 1 • — I — I — I — I — I — r - i — I — I — I — ] — I — I — I — 1 — I — I — I — r —

7.7gCM-6'.4o 17.90 i8.6tpge

n/z~> Abundance

30 40 50 60 70 80 90 100 110 120

Raî

Scan 1956 (18.044 min); 150167,0 9|1

39 51 65 77

l ,M ' | l J lM i l ' | l | l . 1 . " '

106

117

m/z~> I ' l '

30 40 50 60 70 80 90 100 110 120 Abundance

Subl 50

Scan 1956 (18,044 min); 150167,0 (-) 9|1

39 51 65

4 -m/z~> 30 40 50 60

77

- ^

106

117 I I

70 80 90 100 110 120

#81 m,p-xylene Coneen: 535.00 PPb RT: 18.04 min Scan# 1956 Delta R.T. -0.03 min Lab File: 150167.D Acq: 2 9 Dec 2001 3:57 pm

Tgt Ion:106 Resp: Ion Ratio Lower 106 100 91 234.7 201.0

105 46.1 19.2

23581 Upper

261.0 79.2

Abundancelon 106.00 (105.70 to 106,70); 150167.' Ion 91,00 (90.70 to 91,70); 150167,0 Ion 105.00 (104,70 to.105,70); 150167,'

12000- ^

Time-> 18.00 18-20 18.40

n/z~> ' l " " l ' i " l " " l " i i | | " ' | i i " l " " l " " l " " l " " l " ' ' l " " l " " l " " M " i | " " l

30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115

0 " " ' l " " l " ' i | " | | | | | " l " " l " " | i ' " l " " l " " l " i ' l " " l " ' M " " l " " l m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115

I 5 0 ^ y g . ^ . D j ^ ' i 3 ^ ' 9 a S 4 ^ 0 S's'eo teQ''-^lJiQ'(^^'9^ "I pieryi •i /V-«i-«intQ-

#82 o-xylene Coneen: 185.80 PPb RT: 18.86 min Scan# 2053 . Delta R.T. -0.03 min Lab File: 150167.D Acq: 29 Dec 2001 3:57 pm

Tgt Ion:106 Resp: 8046 Ion Ratio Lower Upper 106 100 91 215.4 242.4 302.4#

105 61.7 16.0 76.0

Abundancelon 106.00 (105.70 to 106.70); 150167,

5000

4000

3000

2000

1000-

Ion 91.00 (90,70 to 91,70); 150167,0 Ion 105.00 (104.70 to 105.70); 150167.i

'^ / .J.U-t '

I"' Tentatively Identified Compound (LSC) summary

Operator ID: RUIFENGY Date Acquired: 1 Jan 2002 3:13 am Data File: C:\HPCHEM\1\DATA\I50255.D Name: N4873-1 Misc: MS58639,VI2012,3.9,,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title: SW-846 Method 8260 Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Carbon dioxide 2.72 4132.8 PPb 1285290 ISTD02 9.63 1046500 50.0


G

G

51


C:\HPCHEM\1\DATA\I50149.D 29 Dec 2001 4:14 am MBl MS58651,VI2009,5,,100,5,1

MS Integration Params:. RTEIN2.P Quant Time: Jan 1 10:19 2002


Vial: Operator: Inst : Multiplr:




C:\HPCHEM\l\METHODS\MI1986.M SW-846 Method 8260 Mon Dee 10 16:29:00 2001 Initial Calibration MI1986

(RTE Integrator)

Internal Standards R

5 9

11 17 22

9

10

14

19

T.

82 61 60 72 09

88

84

72

97

Qlon

65 168 114 117 152

113

65

98

174

Response

56578 329316 299996 236583 119021

235531 Recove

172979

Cone Units

500. 50 50 50' 50.

50 ry

50 Recovery

265273 Recove

146819

48 ry

58

00 00 00 00 00

15 = 36 = 79 = 58

PPb PPb PPb PPb PPb

PPb 100. PPb 100. PPb 97.

PPb

Dev(Min)

-0.05 -0.05 -0.06 -0.04 -0.05

-0.03 30%.

-0.04 72%

-0.06 58%

-0.05

G

G

G

G

G

G

C


44) 1,4-difluorobenzene 72) chlorobenzene-d5

•88) 1,4-dichlorobenzene-d4


.43) l,2-diehloroethane-d4 (s) Spiked Amount 50.000 66) toluene-d8 (s) Spiked Amount 50.000

89). 4-bromof luorobenzene (s) Spiked Amount 50.000

Target Compounds

' ^X

Recovery = 117.16%

Qvalue

7

(#) = qualifier out of range (m) = manual integration 150149.D MI1986.M Mon Jan 07 11:17:11 2002 GCMSI

52 Page 1

Q u a n t i t a t i o n R e p o r t

Data F i l e : C:\HPCHEM\1\DATA\I50149.D Acq On : 29 Dee 2001 4:14 am Sample : MBl Mise : M S 5 8 6 5 1 , V I 2 0 0 9 , 5 , , 1 0 0 , 5 , 1 MS I n t e g r a t i o n Params: RTEIN2.P Quant Time: Jan 1 10 :19 2002

V i a l : 20 O p e r a t o r : RUIFENGY I n s t : MSI M u l t i p l r : 50 .00

Quant R e s u l t s F i l e : MI1986.RES

Method T i t l e L a s t Update R.esponse v i a

.C:\HPCHEM\l\METHODS\MI1986.M (RTE I n t e g r a t o r ) SW-846 Method 8260 Mon Dee 10 1 6 : 2 9 : 0 0 2001 I n i t i a l C a l i b r a t i o n

Abundance

190000

180000-

170000

160000

150000

140000

130000

120000

110000

100000

90000

80000

70000

60000

50000

40000

30000

20000

10000

r ime-> 2.00

3

L U L

TIC: 150149.0

4.00 6,00 n'"'"''"' I ; -T-T" "f—r^]—I—r* I I r r ' ! " ! '

8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00

150149.D MI1986.M Mon Jan 07 11:17:15 2002 GCMSI Ri 'e 2


Data File : C:\HPCHEM\1\DATA\I50149.D Acq On : 29 Dec 2001 4:14 am Sample : MBl Misc : MS58651,VI2009,5,,100,5,1 MS Integration Params: LSCINT.P

Vial: 20 Operator: RUIFENGY Inst : MSI . Multiplr: 50.00


C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 ON Filtering: 5 1 ^ Min Area: 0.1 Max Peaks: 0.05 Peak Location:



Signal TIC

pea u ^

• 1

^ 2 3 4

L 5

" 6 \-.. . 1

8 -' 9 ^10

pll .12 13 14 15

r.16 '17

^18 19 20

21 22

^23 24 '25

26 27

"28

k R.T. min

2.744 4.019 5.827 6.283 9.611

9.865-10.338 10.481 10.836 11.233

11.596 11.917 14.730 17.712 18.151

18.211 18.295 19'. 976 20.255 20.289

20.356 20.474 20.939 21.243 22.088

22.493 22.671 22.721

first scan

124 291 487 563 937

976 1043 1059 1083 114 9

1173 1229 154 7 1900 1966

1974 1983 2170 2216 2221

2229 2243 2298 2333 2421

2481 2501 2509

max scan

145 296 510 564 958

988 1044 1061 1103 1150

1193 1231 1564 1917 1969

1976 1986 2185 2218 2222

2230 2244 2299 2335 2435

2483 2504 2510

last scan

189 301 542 570 976

1031 1050 1067 1144 1161

1229 1236 1603 1962 1974

1983 1991 2216 2221 2229

2236 2250 2308 2343 2476

2487 2509 2514

PK TY

rBV2 rBB rBV3 rVB rBV3

rVB3 rVB2 rVB2 rBV rVB

rBV rVB2 rBV2 rBV2 rW 2

rVV2 rVB2 rBV2 rVV3 rVV3

rVB4 rVB3 rVB2 rVB rBV2

rVB3 rBV2 rVB3

peak height

31898 335 7986 504

117842

97 424 543 500

53325 587

100367 1142

102846 125945

945

599 742

161510 2074 1488

852 866 482 471

140140

760 616 777

peak area

317914 1021

108739 1255

1037400

871873 1209 1071

419404 1426

820505 1932

792179 850640 2916

1857 1404

980039 4045 4023

1461 1435 1417 1123

825230

1798 1324 1248

peak % max.

30.65% 0.10%

10.48% 0.12%

100.00%

84.04% 0.12% 0.10%

40.43% 0.14%

79.09% 0.19%

76.36% 82.00% 0.28%

0.18% 0.14% 94.47% 0.39% 0.39%

0.14% 0.14% 0.14% 0.11%

79.55%

0.17% 0.13% 0.12%

% of total

4.501% 0.014% 1.540% 0.018%

14.687%

12.344% 0.017% 0.015% 5.938% 0.020%

11.617% 0.027%

11.216% 12.043% 0.041%

0.026% 0.020%

13.875% 0.057% 0.057%

0.021% 0.020% 0.020% 0.016%

11.684%

0.025% 0.019% 0.018%

54

29 23.144 2554 2560 2566 rVB2 30 23.439 2591 2595 2601 rVB2

31 23.566 2609 2610 2615 rBV 32 23.659 2615 2621 2625 r W 2 33 27.748 3101 3105 3111 rBV

Sum of corrected areas: - 7063181

150149.D MI1986.M Mon Jan 07 11:17:36 2002 GCMSI

581 635

656 403 402

1886 1912

1010 1161 1324

0.18% 0.18%

0.10% 0.11% 0.13%

0.027% 0.027%

0.014% 0.016% 0.019%

G

G

G

G

G

G

G

G

G

55


File : C:\HPCHEM\1\DATA\I50149.D Operator .: RUIFENGY Acquired : 29 Dec 2001 4:14 am using AcqMethod MI1986 Instrument : MSI Sample Name: MBl Mise Info : MS58651,VI2009,5,,100,5,1 Vial Number: 20 Quant File :MI1986.RES (RTE Integrator)

rime->

50000

. 4,02 /'^•v^6.28 I MO. p r I I I I 1 I I 1 y I 1 1 I I I T T T'J 1 T T r J 1 t I 1 [ T 1 I I •[ 1 T I -I [ T ' T ' I 1 [• I T I ' l [ I I [ I | r i 1 I I I I I I I I T T I ) t I" I I ^[ I i ' l I |~

2.00 2.50 3-00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00

50000

„ 0.48/ \ii.23i \i:92 / v I vjatrao 0 h " \ I r I I I i T I I I I I I r ^ ' I T T 1 ] I > 1 1'[ I r r T [ r I I I [ 1 r I ' I [ "f I I I p i " ! ' i r | i i i i i i i i r - j i M i i [ i ~ r i i [ f r i ' i p T * t i i | i i i i | i

fnme-> 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 Abundance

150000

100000-

50000-

1 TIC; 150149.0

98 22.09

J720.941.24 I V . 2 2 2 e ^ 2 3 j a 2 a § B 6 1 1 ' ' • ' I ' ' ' ' f l ' ' ' T ' ' I ' I ' ' I ' l ' ' ' n 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 25.50 26.00 26.50 27.00 27.50

150149.D MI1986.M Mon Jan 07 11:17:42 2002 GCMSI 56

http://J720.941.24


C:\HPCHEM\1\DATA\I50149.D 29 Dec 2001 4:14 am MBl MS58 651,VI2009,5,,100,5,1





ic -k * * ir * * * -k -k * -k -k -k * * * * * -k -k -ir * * * * * -k -k -k -k -ir -k * -k -k -k -k -k -k -k * * * * * * * * * * -ic -k -k * * * * -k -k -k -k -k * -k -k -k * -k


R.T, EstConc Area Relative to ISTD R.T.

G G G G G

G

G

G

2.74 766.13 PPb 317914 pentafluorobenzene

H i t # o f 5 T e n t a t i v e ID MW Mo1Form

9 . 6 1

CAS# Q u a l

Abundance

5000

TT|iiii | i i i i | i i i i | i in]TiiT|TnrpTrTpiTipni|Tni|iT[i |nn[irrTjTTrr| 'nnjrnipTiTjnTr| 'nnjiiii | inipniprrr[iTii |n hl/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

Tni'[iiii[iiM[nii|Mrr|-nTTjTrTT]Trrr[iin|rrTT|TrrTyTTTTjnripTTi]TriTp'nTpiiT|7rrr|-nTrynnpiTr|iTrr

in/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54


44 C02 44 C02 44 C2H40 44 C2H40

000124-38-9 4 000124-38-9 4 000075-21-8 3 000075-21-8 3

Scan 145 (2.744 min); 150149.0 (-) 44

40 46


12 16 22 46

Abundance

5000


16 22 46 i i i i p i i i p M i p M i p i i i p t i i p i i i p i n p i i i p i i i p i i i p i n p i n p i i i p i i i p i i i p T i i p i i i p i i i p i i i p i i i p r M p i i i p i i i p i i i p i n p i i ' i

tr\lz-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000-

#62267; Ethylene oxide 2|g

15

13 J,

26

44

421

31 .46 'l""l""l""l""l""l""l""l""l""l"|||""l""l""l"'"l""l""l""l""l""l""l""l""l""l""l""l'"

b/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m / z 4 4 . 0 100 .00%

2.40 2.60 2.80 3.00

m / z 40. .00

I ' ' • ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I

2.40 2.60 2.80 3.00 m / z 4 5 . 0 5

I

1.35^

T i l I f I I I 1 r I I I I •T~r f\ 1

2.40 2.60 2.80 3.00 m / z 4 5 . 9 5 0 . 6 3 %

' ' I ' ' ' ' I ' ' ' '1 I ' ' ' ' I ' ' ' ' I

2.40 2.60 2.80 3.00

1 5 0 1 4 9 . D MI1986.M Mon J a n 07 1 1 : 1 7 : 4 8 2002 GCMSI 57 P a g e 1

Tentatively Identified Compound (LSC) summary

Operator ID: RUIFENGY Date Acquired: 29 Dec 2001 4:14 am Data File: C:\HPCHEM\1\DATA\I50149.D Name: MBl Mise: MS58651,VI2009,5,,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title: SW-846 Method 8260 Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISCone



G

G

G

G

G

G

58


Data File : C:\HPCHEM\l\DATA\l50160.D Acq On : 29 Dec 2001 11:24 am Sample : MB2 Mise : MS58651,VI2009,5,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 1 12:24 2002




C:\HPCHEM\l\METHODS\MI198 6.M (RTE Integrator) SW-84 6 Method 82 60 Mon Dec 10 16:29:00 2001 Initial Calibration MI1986

Internal Standards R.T. Qlon Response Gone Units Dev(Min)

G

G

G

G

G

G

1) Tert Butyl Aleohol-d9 5.84 65 62317 3) pentafluorobenzene 9.61 168 320498

44) 1,4-difluorobenzene 11.61 114 289223 72) chlorobenzene-d5 17.72 117 228542 88) l,4-diehlorobenzene-d4 22.10 152 119845

System Monitoring Compounds 42) dibromofluoromethane (s) Spiked Amount 50.000 43) l,2-dichloroethane-d4 (s) Spiked Amount 50.000 66) toluene-d8 (s) Spiked Amount 50.000 8 9) 4-bromofluorobenzene (s) Spiked Amount 50.000

Target Compounds

9.87 113

10.84 65

14.74 98

19.98 174


-0.02 -0.05 -0.06 -0.04 -0.04

226868 49.64 PPb -0.05 Recovery = 99.28%

175378 52.47 PPb -0.04 Recovery = 104.94%

266392 50.82 PPb -0.04 Recovery = 101.64%

143010 56.67 PPb -0.04 Recovery = 113.34%

Qvalue

'/7

(#) = qualifier out. of range (m) = manual integration 150160.D MI1986.M Mon Jan 07 11:38:08 2002 GCMSI Paai ge 1

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50160.D Acq On : 29 Dec 2001 11:24 am Sample : MB2 Mise : MS58651,VI2009,5,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 1 12:24 2002



Method T i t l e L a s t Update Response v i a

Abundance 190000

180000-

170000-

160000-

150000

140000

130000

120000

110000

100000

90000

80000

70000-

60000

50000

40000-

30000-

20000

10000

0.-rime->

V.

C:\HPCHEM\l\METHODS\MI1986. M SW-84 6 Method 8260 Mon Dee 10 1 6 : 2 9 : 0 0 2001 I n i t i a l C a l i b r a t i o n

TIC: I50160,D

_

5-o m

A

y

libro

mof

luor

omet

hane

(s)

, b

1,4-

diflu

orob

enze

ne,

1

tolu

ene-

d8 (

s).

S

CO

ca

?-

I I I V

i

l i

i

I i

3

L 'i 1 1 1 1 1 1 1 1 1 1 .1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

2.00 4,00 6,00 8.00 10.00 12.00 14,00 16.00 18.00

(RTE I n t

t o

e g r a t o r )

J I i 3

1 1

y •1 - 1 • !• 1 , , 1 1 1

20.00 22,

i

i . 3

:

l ^ . . _ > . .-, , r v 1 1 1 1 1 v ' l 1 ' I " ! " ' ' 1 '

00 24,00 26,00 28.00 .

150160.D MI198.6.M Mon Jan 07 11:38:12 2002 GCMSI

Data File Acq On Sample Mise


C:\HPCHEM\1\DATA\I50160.D Vial: 31 29 Dec 2001 11:24 am Operator: RUIFENGY MB2 Inst : MSI MS58651,VI2009,5,,100,5,1 - Multiplr: 50.00

G

G

G

G

G

G

G

G

G

G


•Method : C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title , : SW-846 Method 8260 Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 1000 Area counts Start Thrs: 0.1 Max Peaks: 100 Stop Thrs : 0.05 Peak Location: TOP

If leading or trailing edge < "100 prefer < Baseline drop else tangent > Peak separation: 5

Signal' : TIC

pea #

1 2 3 4 5

6 7 8 9

10

11 12 13 14 15

16 17 18 19 20

21 22 23 24

k R.T. min

2.744 3.732 5.844 6.157 9.612

9.865 10.473 10.845 11.166 11.360

11.614 11.935 14.731 17.721 18.574

19.976 20.770 22.097 22.485 22.646

22.730 23.034 23.195 23.296

first scan

118 257 487 546 937

977 1058 1086 1140 1162

1176 1232 1545 1900 2014

2170 2277 2421 2481 2499

2507 2545 2564 2574

max scan

145 262 512 549 958

988 1060 1104 1142 1165

1195 1233 1564 1918 2019

218.5 2279 2436 2482 2501

2511 2547 2566 2578

last scan

178 265 546 551 977

1044 1064 1140 1154 1171

1232 1246 1602 1962 2023

2229 2282 2472 2485 2507

2518 2553 2570 2582

PK TY

rBV2 rBV rBV3-rVB3 rBV2

rVB3 rVB rBV rVB2 rVB

rBV2 rVB3 rBV2 rBV3 rBB

rBV rVB2 rBV2 rVB3 rVB3

rBV4. rBV2 rVB2 rVB2

peak height

34770 507 7958 640

116690

95564 567

50284 1008 548

97640 1151

100648 123613

391

160045 708

135209 875 860

850 803 817 802

peak area

334909 1220

110773 1127

1024497

856125 1006

411348 3902 1196

810589 3329

775288 832349

1007

975203 1047

798946 1040 2183

2920 1834 1389 1709

peak % max.

32.69% 0.12%

10.81% 0.11%

100.00%,

83.57% 0.10%

40.15% 0.38% 0.12%

79.12% 0.32%

75.67% 81.24% 0.10%

95.19% 0.10%

77.98% 0.10% 0.21%

0.29% 0.18% 0.14% 0.17%

% of total

4 0 1 0 14

12 0 5 0 0

11 0 11 11 0

14 0 11 0 0

0 0 0 0

815% 018% 593% 016% 731%

310% 014% 914% 056% 017%

655% 048% 147% 968% 014%

022% 015% 487% 015% 031%

042% 026% 020% 025%



61


File : C:\HPCHEM\1\DATA\I50160.D Operator : RUIFENGY Acquired : 29 Dee 2001 11:24 am using AcqMethod MI1986 Instrument : MSI Sample Name: .MB2 Mise I n f o : M S 5 8 6 5 1 , V I 2 0 0 9 , 5 , , 1 0 0 , 5 , 1 V i a l Number: 31 Quant F i l e :MI1986.RES (RTE I n t e g r a t o r ) -

Abundance

150000

100000

50000-

TIC; I50160.D

9,61

2.74

3,73 5,84

' ' I ' ' ' ' I ' ' ' ' P ' I I I ' ' ' '. I ' ' ' I I ' ' ' ' I ' ' ' ' I I ' ' ' I ^ 1 ' ' I ' ' ' ' M ' ' ' I I ' ' ' I ' ' ' I I I ' ' ' I ' ' ' ' I ' ' I ' I ' I " rime-> 2,00 2,50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8,50 9,00 9.50 10,00 Abundance

150000

100000

TIC; 150160.0

50000

17.72

11.61 14.73

10.84

„ 0.47/ H^^J.2G % 9 3 0 '•11 I f ' I I I i T - i r ' l . I 11^-1 I I . I I I I I I I I I I I

.___ ^ _ - ^ 18.57

rime-> 10-50 11.00 11.50 12.00 12,50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18,00 18.50 19.00 undance

150000-

100000

50000

15 .98

k 1 ' ' ' 20.77

1 1 1 1 1 1 1 C 1 1

TIC: 150160.0

22

I ' l ' ' !

.10

Va2^5Ba32SU30

rime-> 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 25.50 26.00 26,50 27.00 27.50



C:\HPCHEM\1\DATA\I50160.D -29 Dec 2001 11:24 am MB2 MS58 651,VI2009,5,,100,5,1




Quant Method : C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title : SW-846 Method 8260 Library : C:\DATABASE\NBS7 5K.L

k - k k - k - k k k - k k k k k - k - k - k - k k - k - k - k - k k - k k - k - k k k k k k k k k k k - k - k - k - k - k - k k - k k - k - k k - k k - k k k k - k - k k - k - k - k k k - k k - k k k - k k

Peak Number 1 Carbon dioxide

R.T. EstConc Area

Concentration Rank 1'

Relative to ISTD R.T.

G

G

G

G

G

G

G


Hit# of 5 Tentative ID MW MolForm

9 . 6 1

CAS# Q u a l

Abundance

5000

rp 111 p 111 p 111 p nT| 1111 p 111 p i n p i n [TnT[ 111 T p 111 [ n 11 p 111 p n i p i T i p 111 p 111 JT i n p r r i prnrprni 'TrTTp 11 T | i r n j T i r r p r r j

fn/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

^ ^ l " " l " " l " " l " " l " i ' l " " l " " l " " l " " l " " l " " l " " l " " l " " | i i i ' l " " l " " l " " l " " l " " l " ' " | i " ' l " ! ' l " i i | " " l " " l m/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 424446 48 50 52 54


4 4 C02 4 4 C02 44 C2H40 44 C2H40

000124-38-9, 4 000124-38-9 4 000075-21-8 3 000075-21-8 3

Scan 145 (2.744 min); I50160.O (-) 44

40 46


12 16 22 46

Abundance

5000-


16 22 46 r| 111111111111111 n 111H H111 n 11111111111111111111111111111111111111 u 111111111111 n 1111 n 1111 n n 1111 n 111111111111111111H1111111

ir\lz-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

#62267; Ethylene oxide 2|9

15

13 26

44

42:

31 .46 ' l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " ' " l " " l " " l " " l " " l " " l |nM(iiii|ini|iMi|ini|iM.|

m/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m / z 4 4 . 0 5 100 .00%

m / z 39. .95 9.83%

I ' ' ' ^ I I ' ' ' I 2-40 2,60 2,80 3,00

m / z 4 5 . 0 5

2,40 2.60 2.80 3.00

m / z 4 6 . 1 5 0.53%

' ' 1 ' I ' ' I ' ' ' I I ' ' ' ' I ' I ' ' I '

2,40 2,60 2.80 3.00

1 5 0 1 6 0 . D MI1986.M Mon J a n 07 1 1 : 3 8 : 4 3 2002 GCMSI 63

P a g e 1

H Tentatively Identified Compound (LSC) summary

Operator ID: RUIFENGY Date Acquired: 29 Dec 2001 11:24 am Data File: C:\HPCHEM\1\DATA\I50160.D Name: MB2 Misc: MS58651,VI2009,5, ,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator)

t Title: SW-846 Method 8260 Library Searched: C:\DATABASE\NBS75K.L




G

G

G

G

G

G

64

Quantitation Report

G

Data File : C:\HPCHEM\1\DATA\I50253.D Acq On : : 1 Jan 2002 ,.1:54 am Sample : MBl . • Mise : MS58639,VI2012,5,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 8 13:30 2002

(QT Reviewed)



Quant Method : C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title : SW-846 Method 8260 Last Update : Mon Dec 10 16:29:00 2001 Response, via : Initial Calibration DataAcq Meth : MI1986

r- Internal Standards R.T. Qlon Response Cone Units Dev(Min)

G

G

G

G

G

G


4 4)- 1, 4-difluorobenzene 72) ehlorobenzene-d5 88) 1,4-dichlorobenzene-d4

System Monitoring Compounds s) 42) dibromofluoromethane

Spiked Amount 50.000 43) l,2-dichloroethane-d4 Spiked Amount 50.000 66) toluene-d8 (s) Spiked Amount 50.000 89) 4-bromofluorobenzene (s) Spiked 7\mount 50.000

Target Compounds

(s)

5 . 8 1 65 9.64 168

11.61 114 17.74 117 22.11 152

9.90 113

10.85 65

14.74 98

20.00 174

syCs 0 z

50178 300284 270204 212212 108145


0.00 -0.02 -0.05 -0.03 -0.03

201591 47.08 PPb -0.02 Recovery = 94.16%

154247 49.25 PPb -0.03 Recovery .= 98.50%

230090 46.99 PPb -0.03 Recovery = 93.98%

124115 54.50 PPb -0.02 Recovery = 109.00%

Qvalue

(#) = qualifier out of range (m) = manual integration 150253.D MI1986.M Tue Jan 08 13:50:22 2002 GCMSI Paq age 1

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50253.D Acq On : 1 Jan 2002 1:54 am Sample : MBl Mise : MS58639,VI2012,5,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 8 13:30 2002

Vial: 16 Operator:, RUIFENGY Inst : MSI Multiplr: 50.00



C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dee 10 16:29:00 2001 Initial Calibration

Abundance

160000

150000

140000

130000

120000

110000

100000

90000

80000

70000-

60000

50000-

40000

30000

20000-

10000

T I

5 5

k y

TIC; 150253.0

I r-i-i I I I I i S " T I I

rirrie-> 2.00 4.00 6.00 " T — [ " T " T""l I — p ^ " T — r * T — p T ' 'I—r—I 'I "T I — r ^ - ^ — I — I — I — I — I — I — I — I — I — ] — I — I — 1 — 1 — I — 1 — 1 — I — 1 — [ — I — I — I — I — I — I — 1 — 1 — I — [ -

8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 * r ^ r> fM; i~ I I I i " i ' - i - " f r '

1 5 0 2 5 3 . D MI1986.M Tue J a n 08 1 3 : 5 0 : 2 8 2002 GCMSI m 'ge 2


Data File Acq On Sample ) Misc


MBl MS58 639,VI2012,5,,100,5,1



Method : Title : Smoothing : Sampling : Start Thrs:

C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 ON Filtering: 5 1 Min Area 0.1 Max Peaks

1000 Area counts 100

Stop Thrs : 0.05 Peak Location: TOP


Signal TIC

peak R.T. L.. ^

1 1 rH

CM

3 4

... 5

": 6 7 8

r ^ _.10

pll 12 "13

p, 14 15.

16 '17

•-IS 19 20

21 22

__23 24

^25

"26 27 ;28

min

2.750 3.130 4.186 5.867 6.331

9.634 9.888

10.242 10.352 10.868

11.611 11.97 4 14.745 15.041 15.150

17.735 18.183 19.991 20.388 20.700

22.111 22.457 22.491 22.550 22.702

22.880 22.922 23.006

first scan

123 189 312 489 567

940 978 1032 1044 1089

1178 1236 1547 1600 1612

1905 1971 2171 2233 2269

2422 2477 2481 2488 2506

2524 2533 2543

max scan

146 191 316 515 570

961 991

1033 1046 1107

1195 1238 1566 1601 1614

1920 1973 2187 2234 2271

2438 2479 2483 2490 2508

2529 2534 2544

last scan

189 196 321 547 575

978 1032 1044 1055 1141

1236 1244 1600 1607 1625

1971 1979 2224 2244 2279

2471 2481 2488 2500 2515

2533 2538 2554

PK TY

rBV rVB rVB rBV4 rVB

rBV3 r W 3 rW3 rVB3 rBV2

rBV4 rVB rBV2 rVB2 rVB

rBV2 rVB2 rBV2 rVB3 rVB4

rBV rVB2 rVV2 rVB4 rVB2

rBV2 rVB2 rVB3

peak height

98776 474 318 6856 556

107720 88402 1642 740

43685

92337 679

87880 1016 693

114018 510

138253 607 480

126325 713 646 914 599

474 759 610

peak area

882531 1059 1024 92848 1310

949742 791448

5846 2129

357924

755155 1229

682278 1636 1873

763181 1202

851387 1955 1498

729910 1001 1373 2323 1506

1682 1403 1891

peak % max.

92.92% 0.11% 0.11% 9.78% 0.14%

100.00% 83.33% 0.62% 0.22%

37.69%

79.51% 0.13%

71.84% 0.17% 0.20%

80.36% 0.13%

89.64% 0.21% 0.16%

76.85% 0.11% 0.14% 0.24% 0.16%

0.18% 0.15% 0.20%

% of total

12.799% 0.015% 0.015% 1.347% 0.019%

13.774% 11.478% 0.085% 0.031% 5.191%

10.952% 0.018% 9.895% 0.024% 0.027%

11.068% 0.017% 12.348% 0.028% 0.022%

10.586% 0.015% 0.020% 0.034% 0.022%

0.024% 0.020% 0.027%

67

r L

-29 23.201 2566 2567 2571 rVB2 644 i30 23.277 2574 2576 2581 rVB2 640

_31 23.344 2581 2584 2588 rBV 580 '32 23.792 2634 2637 2641 rBV 422 33 23.995 2656 2661 2666 rBB 646 34 27.416 3063 3066 3074 rBB 317

1026 1406

1110 1132 1040 1036

•

0.11% 0.15%

0.12% 0.12% 0.11% 0.11%

6895094

0 0

0. 0. 0. 0

015% 020%

016% 016% 015% 015%

Sum of corrected areas;


G

G

G

G

G

68

G LSC Report - Integrated Chromatogram

File : C:\HPCHEM\1\DATA\I50253.D Operator : RUIFENGY Acquired : 1 Jan 2002 1:54 am using AcqMethod MI1986 Instrument : MSI Sample Name: MBl Misc Info : MS58639,VI2012,5,,100,5,1 Vial Number: 16 Quant File :MI1986.RES (RTE Integrator)

Abundance

120000

100000

80000

60000

40000

20000

I ' ' I I j ' ' ' ' I ' I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' I ' ' I ' ' ' ' I ' ' ' ' I lrime-> 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00

TIC; I50253.D

2.75

5.87 ^ . 3 4J9

I I I I I I I I I f I I I I r I ) I I I I I I I I J I I I I I I I I I I I I I I r I I I T' i i i I i J I i I I I I I I I I I I I I I i I I I J i I I

6.33

Abundance

120000

100000

80000

60000

40000

20000

TIC; I50253.D

17.74

11.61

10.87

35

14.74

1.97 .§45 I \ J8 .18 i*-i 1 1 r^y?< ' I I T-| I I' I I I r r I 1 ) I I I r-j-i i i i | . . . i | , , i i , , . . i | . . , i | i' i i . i i i - i J i | i . i . | . i i . | . . i i | i i . i | .' i . . | T T - i i | . i . i | i

Time-> 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14,00 14,50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 Abundance

120000

100000

80000

60000

40000-1

20000

0

TIC; 150253.0 19| 1999 22.11

rime~>

o.3ao.7o I sâa^tasaaa2B084 23.29.99 27.42-' ' M ' I ' I ' ' ~ ' I ' I ' I I ' I I ' I 1 ' ' ' I ' ' ' M ' ' ' ' ' M I ' I ' I 1 ' ' ' I ' i ' ' ' i I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25,00 25.50 26.00 26.50 27.00 27.50

150253.D MI1986.M Tue Jan 08 13:58:30 2002 GCMSI 69


C:\HPCHEM\1\DATA\I50253.D 1 Jan 2002 1:54-am

MBl MS58 639,VI2012,5,,100,5,1

Data File Acq On Sample Mise MS Integration Params: LSCINT.P



*-*••*--*-•*•*•*-•*•*•*••*••*• k - k k k k k k - k k - k k k k - k k - k - k k k k - k k - k k k k - k k k k k k k k - k k k k k k k k k k k k k - k k k k k k - k - k - k k



R.T. EstConc Area Relative to ISTD R.T,

G

G

G

G

G

G

G

G

G


Hit# of 5 Tentative ,ID MW MolForm CAS# Qual

1 Carbon dioxide 2 Carbon dioxide 3 Ethylene oxide 4 Nitrous Oxide

44 C02 4 4 C02 44 C2H40 44 N20

000124-38-9 4 000124-38-9 4 000075-21-8 3 010024-97-2 3

Abundance

5000-

m/z-> Abundance

5000

[ i i i p i i ip inp i [ ip i i ip i i ip i i ip i i ip i r ip i iT | iMip iMpr iTpnTpi iTp i i ip iT in i i ip r iTpr i r rn i i irtrpiTipinpiMpin'jTTrr]

in/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Scan 146 (2.750 min); I50253.O (-) 44

40 46 'I""I""I""I""I""I""I""I""I""I""I""I""I""I""I""I""||"'I""(""I""I""I"'||"|'I""I""1""I

2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 #62263; Carbon dioxide

44

12 16 22 46

Abundance

5000


16 22 46 | | " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " i " " l " " l " " l " " l " " l " " | | " ' l " " l " " l " " l " " l " " l " " l " " l

hi/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

'n/z->


15

13 26

44

421

31 .46 " ' l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " i " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l " " l

2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m/z 43.9,5 100.00%

I I I I 1 I 1 I 1 1 I I I I I I I I I I r I ]

2.40 2.60 2.80 3.00

m/z 40^05 2.78%

2.40 2.60 2.80 3.00

m/z 4 4 . 9 5 1.02%

2.40 2.60 2.80 3.00

m/z 4 6.0,5 0.50%

I I ' I ' I ' ' ' ' I ' ' ' ' I I ' ' ' I ' 2.40 2,60 2.80 3,00

150253.D MI1986.M Tue Jan 08 1 3 : 5 8 : 3 7 2002 GCMSI

70 Page 1


Operator ID: RUIFENGY Date Acquired: 1 Jan 2002 1:54 am ^ Data File: C:\HPCHEM\1\DATA\I50253.D Name: MBl Misc: MS58639,VI2012,5,,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title: SW-846 Method 8260 Library Searched: C:\DATABASE\NBS75K.L




G

G

G

G

G

G

G

G

G

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VOLATILE ANALYSIS LOG

Analyst Signature:_

Standard Data

Batch ID: yXiS%k

9/cA

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Status (Data)

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m-Jj-îl /uv-i^-4'^

Description npt ion

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169 74

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171 77

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Batch ro: Vi jOl^ '

Standard Data

Lot#

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79

Appendix 11

Laboratory Analytical Report - Soil Samples Collected on December 18,2001


- ^

Id 01/14/02

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Technical Report for


Fleet Bank, Wall, NJ

03-02046-02-03

Accutest Job Number: N4945

Report to:

Groundwater & Environmental Services P.O. Box 1750 1340 Campus Parkway Wall, NJ 07719

ATTN: Terri Evans

Total number of pages in report: 65

Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Conference

and/or state specific certification programs as applicable.

încent J. Pugliese President

Certifications: NJ(12129),.NY(10983), CA, CT, DE, FL, MA, MD, NC, PA, RI, SC, VA

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories,

New Jersey • 2235 Route 130 • Dayton, NJ 08810 • tel: 732-329-0200 • fax: 732-329-3499 • http://www.accutest.com

http://www.accutest.com


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Sample Summary


Fleet Bank, Wall, NJ Project No: 03-02046-02-03

Sample Collected Matrix Nuinber Date Time By Received Code Type

N4945-1 12/18/01 10:15 JHM 12/19/01 SO Soil

Job No: N4945

Client Sample ID

SE-2 #1

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N4945-2 12/18/01 13:00 JHM 12/19/01 SO Soil

N4945-3 12/18/01 13:15 JHM 12/19/01 SO Soil

SE-3 #2

SE-4 #3

G

G

G

G

G

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

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[

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Laboratoiy Beliverables

1. Cover Page, Tftle Page lisdng Certification #, Facility Name and Addtess, and Date of Report C V j /

2. TableofOmtente. g^jp^

3 . Suniotaty Sheete listing analytical results for all targeted and non-targeted compounds. I j f

4. SummaiyTable cross-referencing field ID #'s vs. lab ID #'s. f ^

5. Document bound, pagjuiated and legible. f j [

^. Chain of CXistody. \ ^

7. Mefliodolosr Sununaty f V

8. Laboratory Chronicle and Holding Time Check. C V

U 5*. Results submitted on a dry weight basis (if applicable) ' K f

r 10. M ^ o d Detection Liauts. 1 l /

11. Lab certified by NJDEPE for parameters or appropriate category of parameters or a member of the USEPA CU'i

12. Non-Conformance Stmmiary. .

.y^ff^ . JiMyiK^ ^ ^ ^ ^ ^ l u ^ l n < ^ \ / QCJReviewer \ \ Date I

New Jecsey « fiBshlVi«bCp«poraieVitege-»»ia(fiiig6<223^

Percent Solids Det^roihation

A<xaitest Lalboratories employs a iriodified Ve deteimtnation of percent solids to calculate dry weight. AW data for solid matiic^s is reported on a dry weight basis by applying the percent solids data froin this determination.

-w

^

Aocolest latjoratories. Ocoen»ber 8,2000

m

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Table Of Coafeats Reduced Laboratoiy Data Deliverables

For Non-USEPAKXP Methods

tltte/CoverPaye

Deliverable Checklist

T a b l e O f Contents

Secfion 1 General

A. Results SiMimaty B. Chatn of Custody C LaiioraliMyChfonictcs

Section 2 GC/MS Suppor t Data (grouped hy fiactioo)

A. Methodology Review B. OMifiMmanoe/Noft-coofixmaaccSuauiiaiy C. Sunogate Recorciy Results Summaiy D. Kfatrix Spike/Matrix Spifcc Duplicate Suaunaiy E. Method Blank Suaunaiy F. Tune Results Summaiy G. Calibration Sununaiy (sotted by bistnimcat)

Initial Calibcatioa Check Summaiy - Contiauing Calibcatioa Ched: Summaiy

H. {ateoialStandaixI Summaiy i. Sampte and BlaidcChiamatagiains, Quant Reports, Mass Spectra, and Libraiy Search Data

Section 3 G C Suppor t Data

A. Methodology Review B. Coa&cmance/Ndn-confonnancc Summaiy C. SuoogafieRccoveiy Results Summaiy D. Matrix Spikc/Mabix Spike Duplicate Summaiy E. Method Blank Summaiy F. Calibration Summaiy (sorted by lostnimeat)

Initial Calibcatioa Check Sununaty Continuing Calibration Check Summaiy

G. Rjitoitioa Time Shift Suaunaiy K Sampki Blank and Mutfi-pcakStandardCtuonutogranis and Quant Repocts

Section 4 Metals Suppor t Data (sortiedbylnstnimentType-ia', Fumdoe, Flame, Meromy)

A. Methodology Ricview B.' CocifiKnianoe/Nba-odnfixnunoe Suaunaiy C Blaidc Results Summaiy

Initial and Continuing Calibration Blank Summaiy McChod Blank Summaiy

O. Batch Quality Control Summaiy - ' M^rixS^%ie and Duplicaie Results Summaiy

. - Spike Blank and Lab Conliol Sample Summaiy Serial Dilution Residts Summaiy

E . ' - Calibration Summaiy ^ Calibia&m Check Standards Summaiy tntecfering EtemeirtsCSnck Standard Summaiy

Secfion S General Oiemlstry/PetroleHm Hydrocartton S u p p o r t Data

A. Methodology Review B. Confbcmaiioe/Nbn-OinfiKntaace Summaiy C. Batch Quality ContEQl Summaiy

Mediod Btaidc and SpScc Blank Results Simuoaiy-Matrix Spike Results Summaiy

- DupHcate Results Suaunaiy D. Raw Data andIR Spectra (Petroleum Hydrocarbons)

.E. Saw Data and Rim Record ^Hcxavaleat Chromium)

New Jecsey • fteshtHwdsCwpoateVinage • BuiWingB ^ 2235Rwde 130 • Oaytaa.NJ(M810 * M:908-323-0200 • 6ic908-329-3499 • WIpz/AimwaoateLcoro

— r


Report of Analysis Page 1 of 2'

CUent Sample ID: SE-2#1 Lab Sampl Matrix: Method: Project:

Run #1 Run #2

e ID: N4945-1 SO - Soil SW846 8260B Fleet Rank, Wall, NJ

FilelD DF 150185.D 1

VOA PPL List

CAS No.

107-02-8 107-13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-5 10061-02-6 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Compound

Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3 -Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1, l-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3 -Dichloropropene, Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichioroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

Analyzed 12/30/01

Result

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 234 ND ND ND ND ND ND ND

By RFY

RL

3200 3200 63 320 320 320 320 320 320 1300 320 320 320 320 320 320 320 320 320 320 320 320 320 320 320 63 320 320 320 63 320 320 320 320 320 130


Prep Date Prep Batch Analytical Batch n/a n/a VI2010

Units Q

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg J ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg


J = Indicates an estimated value ' - • " ' ^ B = Indicates analyte found in associated methxid blank N = Indicates presumptive evidence of a compound

G

G




SE-2 #1 N4945-1 SO - Soil SW846 8260B Fleet Bank, Wall, NJ


12/18/01 12/19/01 84.4

VOA PPL List

CAS No. Surrogate Recoveries Run#l Run#2 Limits

0 G G G

1868-53-7 Dibromofluoromethane 95% 17060-07-0 1,2-Dichloroethane-D4 101% 2037-26-5 Toluene-D8 ' 100% 460-00-4 4-Bromofluorobenzene 107%



R.T.

2.74

55-132% 54-129% 65-133% 58-137%

Est. Cone.

500 0

Units Q

ug/kg JNB ug/kg

8 ND = Not detected RL = Reporting Limit E = Indicates value exceeds calibration range




G

C

Client Sample ID: SE-3 #2 Lab Sampl Matrix: Method: Project:

Run#l Run #2

e ID: N4945-2 SO - Soil SW846 8260B Fleet Bank, Wall, NJ

File ID DF I50186.D 1

VOA PPL List

CAS No.

107-02-8 107-13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-5 10061-02-6 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Compoimd

Acrolein Acrylonitrile Benzene Bromodichloromethane

- Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vmyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

Analyzed 12/30/01

Result


By RFY

RL

2800 2800 56 280 280 280 280 280 280 1100 280 280 280 280 280 280 280 280 280 280 280 280 280 280 280 56 280 280 280 56 280 280 280 280 280 110



Units Q


ND = Not detected RL = Reportiiig Limit E = Indicates value exceeds calibration range

J = Indicates an estimated value ' ' ' i i B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound



SE-3 #2 N4945-2 SO - Soil SW846 8260B Fleet Bank, Wall, NJ

Report of Analysis


V

12/18/01 12/19/01 98.5

Page 2 of 2

/

VOA PPL List

CAS No. Surrogate Recoveries Run#l Run#2 Limits

G

G

G

G

G

G

G

C

1868-53-7 Dibromofluoromethane 95% 17060-07-0 l,2-Dichloroethane-D4 100% 2037-26-5 Toluene-D8 100% 460-00-4 4-Bromofluorobenzene 110%



R.T.

2.74

55-132% 54-129% 65-133% 58-137%

Est. Cone.

690 0

Units

ug/kg ug/kg

Q

JNB


J = Indicates an estimated value A fk B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound



G

G

G

G

G

Client Sample ID: SE-4 #3 Lab Sampl Matrix: Method: Project:

Run#l Run #2

e ID: N4945-3 SO - Soil SW846 8260B Fleet Bank, Wall, NJ

File ID DF I50187.D 1

VOA PPL List

CAS No.

107-02-8 107-13-1 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-5 10061-02-6 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Compound

Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1, l-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

Analyzed 12/30/01

Result


By RFY

RL

2800 2800 56 280 280 280 280 280 280 1100 280 280 280 280 280 280 280 280 280 280 280 280 280 280 280 56 280 280 280 56 280 280 280 280 280 110



'

Units Q


ND = Not detected RL = Reporting Lunit E = Indicates value exceeds calibration range



G

G

G

G

G

G


SE-4 #3 N4945-3 SO-Soil SW846 8260B Fleet Bank, Wall, NJ

Report of Analysis


12/18/01 12/19/01 97.1

Page 2 of 2

VOA PPL List

CAS No. Surrogate Recoveries Run#l Run# 2 Limits

1868-53-7 17060-07-0 2037-26-5 460-00-4

CAS No.

Dibromofluoromethane 95 % 1,2-Dichloroethane-D4 99 % Toluene-D8 99% 4-Bromofluorobenzene 111 %

Tentatively Identified Compounds

carbon dioxide Total TIC, Volatile

R.T.

2.72

55-132% 54-129% 65-133% 58-137%

Est. Cone.

430

, 0

Units

ug/kg ug/kg

Q

JNB

G

G


J = Indicates an estimated value ^ 2 B = Indicates analyte found in associated method blank N = Indicates presumptive evidence of a compound

Mm ..-. r !T~2 n-

CHAIN OF CUSTODY 2235 ROUTE 130, DAYTON. NJ 08810 732-329-0200 FAX: 732-329-3499/3480

l ^sss^ - - - • : S ^ ^

ACCUTEST JOB #:

M m r AcctiTEsr Quote «:

CUENT INFORMATION FACIUTY INFORMATION ANALYTICAL INFORMATION MATRIX CODES

:2h. NAME

^ ^ B c ^

ADDRESS Ccxi/ÔS, f(yrLiA)(-uj

cmr, bH. STATE

077/9 ZIP

PROJECT N A M E _

LOCATION

PROJECT NO.

SEND REPORT TO: T ^ Cl>*>*^5 PHONE # 73Z-Sr/q^Q/0Q FAX# 73^-9 /9 -0 '? / i>

ACCUTEST SAMPLE*

COLLECTION

FIELD ID / POINT OF COLLECTION DATE TIME

SAMPLED BY:

E 2^

PRESERVATION

00 5;

DW- DRINKING WATER

GW' GROUND WATER

WW- WASTE WATER

SO- SOIL SL- SLUDGE Ol - OIL LIO- OTHER

UQUID SOL - OTHER

SOLID

LAB USE ONLY

- ; <.&-2 # / I?//?}/ QL l O i ^ SkA 2D. i i - L Se-2> -UZ t2/ii^/Bi /300 Ji+M 5 0 -5 SB-H #3 /2/<s/ OL \JiS :TH/1 so

zv/c^ t 11

wimrfn. 5BS59WB* *S9 DATA TURNAROUND INFORMATION DATA DEUVERABLE INFORMATION COMMENTS/REMARKS

21 DAYS STANDARD APPROVED BY: 14 DAYS RUSH

D 7 DKfS EMERGENCY . D OTHER

21 DAY TURNAROUND HARDCOPY. EMERGENCY OR RUSH IS FAX DATA UNLESS PREVIOUSLY APPROVED

j a NJ REDUCED D NJFul l D F U a C L P D DISK DELIVERABLE D OTHER (SPECIFY) _

D COMMERCIAL "A" D COMMERCIAL'S' D STATE FORMS

SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION, INCLUDING COURIER DELIVERY | g | ;'.^':<^.^"^;--iv^M^

7 ^ DATETIME RECBVEO BY:

1 . ^ SJ rfXrrv/n 1 REUNaUISHEDBY:

•joanuzy) DATE 'HHE: )BY:

/ ^ V ^ ' C ^ / OK

\i^ r^'^^ b?' /^ -^ / REUNOUISHED BY:

4. DATE TIME:

ONICE^ RELINOlHSHEO BY:

5. ^ O A T E U M E : RECEIV^Kl BY:

5. SEALf PRESERVE WHERE APPUCABLE

D TEMPERATURE

f ^ ^

IF

? > "

[ GC/MS f VOLATILE

15

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G r-

VOLATILE ORGANIC METHOD 826Q

Tids method can be summarizied as fijHoiro: For low levd contafliiaafion, an insert jgas is bubbled through 5nil sample. The purgeables are efSdenlJy tiâos&iTed fi-om the aqueous phase to the vapor phase. The vapor is swq^t through a sorbent colurttn where the purgeable are trapped . When p u r g ^ is complete, the sotbent tube is heated andbackflushed with hdium to desotb trapped san: )le components. The analytes are desorbed directly to a large bore capillary on capillary prec(4umn before being flash evaporated to a narrow bore capillaiy for analysis.

The column is temperature programmed to separate the analytes which are then delected vnih. a mass spectrometer (MS) interfaced to the gas chromatograph. Wide bore capillaty columns requirea jet separator, whereas narrow bore capillary collumns can be directly interfaced to the ioix source.

Analytes eluted from the capillary column are introduced into the mass spectrometer via a jet sepjuator or a direct connection. Identification of target analytes is accompliched by comparing their mass spectra with the electron impact spectra of authîtic standard. Quantitation is accomplished by comparing the response of a major {quantitation) on rdative to internal standard with a five-point calibration curve.

New J e r s e y « FreSiPoTOJsCwpcwaeViMage • IBuildingB • 223SRoute 130 • Oayton.R)08810 • tel:908-329 OaW • lax: 908-329 3499 • WIp/Aw«acc«lesl,com

GC/MS Analysis Case Narrativc/Conformanccôn-Coniformancc Summary

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Fraction

1. Chromatograms Labeled/Compounds Identified {Field Samples and Method Blanks)

2 . GC/MS Tunc Meet Criteria

3 . G C / M S T\lIUngFrequcnqr--Paton«vedc»ay 24 l»uf3 foe 600 series are! 12 ho«« for 8000 s e t i ^

4. GC/MS Calibration - Initial and Continuing Calibration Meet Mctliod Requirements

5. GC/MS CalibraUon Requirements

a. Calibration Check Compounds

b . System Performance Check Compounds

6. Blank Contamination

I f yes, the sample result is qualified wilh a "D".

7. Surrogate Recoveries Meet Criteria

I f the requirement is not met, refer to the Surrogate Summary for commeni.

8. Matrix Spike/Matrix Spike Duplicate Recoveries Meet Criteria

I f the requirement is not met, refer to MS/MSD Summary for comment.

9. [ntemal Standard Area/Retention Time Shift Meet Criteria

I f the requirement is not met, refer to the Internal Standard Summary for comment.

10. Extraction Holding Time Met

I f the holding time is not met, refer lo the Sample Result page for comment.

\ 1. Analysis Holding Time Met

I f Ihe holding time is not mel, refer lo the Sample Result page for commeni.

12. Volatile Sample Preservation - pH should Ixi < 2. List any non-compliant samples below:

N O YES

t

Addilional Commcnis:

Q C Review Siynalt irc: ^ ^ ) " 7 ^ V. ylAji^lA Date: > / o ^ ^ 17 Form: RG04 Rev. Dale: 2/9/00

G

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Case Narrative . Library Search Oata

The non-target compounds detected in this sample were tentatively identified using a search of the NIST/EPA Mass Spectral library. This search selects certain uniqueness chara<êristics from the spectra of the nonârget compounds and compares them to spectra of compounds that have been archived in the mass specAral library. Ck>mpounds in the Library wliose spectra most dosely resemble the spectra of the non-target compoutKls are listed in order of (heir "match quality" in the search results.

Interpreting library search data is subjective and dependent upon (he analyst's jtidgement. Subjectivity increases as spectral complexity increases and the likelihood of listing a non-target compound as an unknown becomes greater.

Qualitative fcientifications of non-targeted compounds must be evaluated carefully to determine if their dtemical and physical properties are consistent with (he compound dasses ttiat can be determined by the method in use. If the chemical and physical properties of the susped compound indicate that presetK^ is possible, the library search data provides the basis for (urther investigation. The information generated via library searches of non-targeted compounds stiould be b-eated as semi-quafitative.

Quantitative values placed on tentatively klentified compounds (TICs) are calculated using an assumed response fador of one (1). This assumption can cause the calculated concentration to be grossly estimated and may be high by as much as a factor of five (5) or lowby as mudi as a fador of one thousand (1,000). The accuracy of quantitaUve data generated using library search procedures is unknown and should be used guardedly.

The library search may have indicated the presence of organo-silicon compounds, cartwn dioxide, or aldol cotKiensates. The organo-silicon compoutKls that have been identified in samples are found in components of the analytical instrumentation. They are dassified as notmal system artifads.. Carbon dioxide, an atmospheric component is soluble in water and capat)(e of beitig deteded in purge and trap systems. Its presence is inconsequential because of its ubiquitous nature. Aldol condensates are byproduds of extradion/concentration procedures that use acetone as a solvent They are produced ur>der certain pH conditions, which are a fundion of sample matrix charaderistics. None of these compounds are of sample origin and (heir appearance should be discounted for dedsion-making putiposes.

Accutest t.3boratories. April 28,1999 18

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Volatile Surrogate Recovery Summary Job Number: N4945 Accoimt; GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 1 of 1

Method: SW846 8260B Matrix: SO

Samples and QC shown here apply to the above method

Lab Sample ID

N4945-1 N4945-2 N4945-3 N5167-7MS , N5167-7MSD VI2010-BS VI2010-MB1

Surrogate Compounds

Lab FilelD

150185.D 150186.D 150187.D 150189.D I50190.D 150178.D 150177.D

SI = Dibromofluoromethane S2 = l,2-Dichloroethane-D4 S3 = Toluene-D8 S4 = 4-Bromofluorobenzene

SI

95.0 95.0 95,0 98.0 99.0 98.0 96.0

Recovery Limits

55-132% 54-129% 65-133% 58-137%

S2

101.0 100.0 99.0 106.0 106.0 108.0 103.0

S3

100,0 100.0 99,0 101.0 102.0 103.0 100.0

S4

107.0 110.0 in.o 103.0 103.0 107.0 110.0

G

G

19


Page 1 of 2

Sample File ID DF N5167-7MS a 150189.D 1 N5167-7MSD2 I50190.D 1 N5167-7a 150191.D 1

Analyzed 12/30/01 12/30/01 12/30/01

By RFY RFY RFY





N4945-1, N4945-2, N4945-3

Method: SW846 8260B

G

G

G

G

C

CAS No.

107-02-8 71-43-2 75-27-4 75-25-2 74-83-9 56-23-5 108-90-7 75-00-3 110-75-8 67-66-3 74-87-3 124-48-1 95-50-1 541-73-1 106-46-7 75-71-8 75-34-3 107-06-2 75-35-4 156-59-2 156-60-5 78-87-5 10061-01-5

Compound

Acrolein Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane Dibromochloromethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1 -Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene

10061-02-6 trans-1,3-Dichloropropene 100-41-4 75-09-2 79-34-5 127-18-4 108-88-3 71-55-6 79-00-5 79-01-6 75-69-4 75-01-4 1330-20-7

Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (total)

N5167-7 ug/kg Q

ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Spike ug/kg

63500 6350 6350 6350 6350 6350 6350 6350 31800 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 6350 19100

MS ug/kg

34500 6020 6750 7370 5880 7120 6780 5610 33900 6120 4870 7070 6090 6260 6280 5140 5760 6740 5750 5980 5590 5760 6230 6670 6610 5570 5350 7120 6520 6710 6140 6470 6340 5230 20100

MS %

54 95 106 116 93 112 107 88 107 96 77 111 96 99 99 81 91 106 91 94 88 91 98 105 104 88 84 112 103 106 97 102 100 82 106

MSD ug/kg

37600 5850 6750 7390 5870 6970 6600 5610 34500 6020 4850 7110 5960 6300 6110 4620 5680 6730 5520 5820 5590 5590 6200 6870 6510 5370 5500 6920 6480 6580 6090 6240 6250 4900 19900

MSD %

59 92 106 116 92 110 104 88 109 95 76 112 94 99 96 73 89 106 87 92 88 88 98 108 103 85 87 109 102 104 96 98 98 77 104

RPD

9 3 0 0 0 2 3 0 2 2 0 1 2 1 3 11 1 0 4 3 0 3 0 3 2 4 3 3 1 2 1 4 1 7 1

Limits Rec/RPD

1 1-199/35 1 64-132/15 i 64-134/15 1 53-147/19 1 45-132/19 1 54-143/19 1 56-137/17 1 33-140/22 1 29-166/19 1 66-130/14 1 46-137/22 1 61-138/15 1 46-139/18 1 44-143/19 1 44-143/20 1 43-139/25 1 67-131/15 1 61-135/14 1 60-130/19 1 63-132/16 1 63-131/18 I 64-132/14 ii 58-133/16 ii 53-138/18 ii 49-143/20 i; 57-130/15 i: 41-135/23 :i 27-207/27 ii 48-145/16 ii 60-136/19 i; 62-131/15 :i 59-146/18 1 27-140/24 ii 49-142/20 ii 45-146/17

20

Matrix Spike/Matrix Spike Duplicate Summary Job Number: N4945 Accoimt: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Page 2 of 2

Sample File ID DF N5167-7MSa 150189.D 1 N5167-7MSD ^ I50190.D 1 N5167-7a 150191.D 1

Analyzed 12/30/01 12/30/01 12/30/01

By RFY RFY RFY





N4945-1, N4945-2, N4945-3

Method: SW846 8260B

G

G

G

G

G

G

G

G



(a) Methanol preservation/extraction.

MS MSD N5167-7 Limits

98% 106% 101% 103%

99% 106% 102% 103%

96% 101% 100% 106%

55-132% 54-129% 65-133% 58-137%

21

Blank Spike Summary Job Number: N4945 Account: GESNJ Groundwater & Envirorunental Services Project: Fleet Bank, Wall, NJ

Page 1 of 2

Sample FilelD DF Analyzed By VI2010-BS 150178.D 1 12/29/01 RFY



N4945-1, N4945-2, N4945-3

Method: SW846 8260B

G

G

G

G

G

G

G

G

CAS No. Compound

107-02-8 Acrolein 71-43-2 Benzene 75-27-4 Bromodichloromethane 75-25-2 Bromoform 74-83-9 Bromomethane 56-23-5 Carbon tetrachloride 108-90-7 Chlorobenzene 75-00-3 Chloroethane 110-75-8 2-Chloroethyl vinyl ether 67-66-3 Chloroform 74-87-3 Chloromethane 124-48-1 Dibromochloromethane 95-50-1 1,2-Dichlorobenzene 541-73-1 1,3-Dichlorobenzene 106-46-7 1,4-Dichlorobenzene 75-71-8 Dichlorodifluoromethane 75-34-3 1,1-Dichloroethane 107-06-2 1,2-Dichloroethane 75-35-4 1,1-Dichloroethene 156-59-2 cis-1,2-Dichloroethene 156-60-5 trans-1,2-Dichloroethene 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 10061-02-6 trans-1,3-Dichloropropene 100-41-4 Ethylbenzene 75-09-2 Methylene chloride 79-34-5 1,1,2,2-Tetrachloroethane 127-18-4 Tetrachloroethene 108-88-3 Toluene 71-55-6 1,1,1-Trichloroethane 79-00-5 1,1,2-Trichloroethaiie 79-01-6 Trichloroethene 75-69-4 Trichlorofluoromethane 75-01-4 Vinyl chloride 1330-20-7 Xylene (total)

Spike ug/kg

25000 2500 2500 2500 2500 2500 2500 2500 12500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 2500 7500

BSP ug/kg

26600 2460 2880 3270 2340 3120 2750 2250 12600 2500 1880 3090 2480 2520 2590 1690 2320 2880 2250 2360 2210 2370 2640 2820 2820 2210 2280 2920 2680 2820 2610 2660 2780 2110 8400

BSP %

106 98 115 131 94 125 110 90 101 100 75 124 99 101 104 68 93 115 90 94 88 -95 106 113 113 88 91 117 107 113 104 106 111 84 112

Limits

1-219 74-127 71-134 63-144 64-138 58-144 77-124 64-143 28-165 72-129 51-146 69-137 73-127 74-122 73-126 47-143 70-130 67-138 64-129 70-127 65-128 71-132 67-124 63-126 76-127 62-129 42-147 44-179 74-126 64-136 70-132 73-135 52-147 57-144 77-126

Blank Spike Summary Job Number: N4945 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample FilelD DF Analyzed By VI2010-BS 150178.D 1 12/29/01 RFY


Prep Date n/a

Page 2 of 2


Method: SW846 8260B

N4945-1, N4945-2, N4945-3

G

G

G

G

G

G

G

G

G



BSP Limits

98% 108% 103% 107%

55-132% 54-129% 65-133% 58-137%

23


Page 1 of 2

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VI2010-MB1 150177.D 1 12/29/01 RFY n/a n/a VI2010


N4945-1, N4945-2, N4945-3

Method: SW846 8260B

G

G

G

G

G

CAS No. Compound Result RL Units Q

107-02-8 Acrolein ND 2500 ug/kg 107-13-1 Acrylonitrile ND 2500 ug/kg 71-43-2 Benzene ND 50 ug/kg 75-27-4 Bromodichloromethane ND 250 ug/kg 75-25-2 Bromoform ND 250 ug/kg 74-83-9 Bromomethane ND 250 ug/kg 56-23-5 Carbon tetrachloride ND 250 ug/kg 108-90-7 Chlorobenzene ND 250 ug/kg 75-00-3 Chloroethane ND 250 ug/kg 110-75-8 2-Chloroethyl vinyl ether ND 1000 ug/kg 67-66-3 Chloroform ND 250 ug/kg 74-87-3 Chloromethane ND 250 ug/kg 124-48-1 Dibromochloromethane ND 250 ug/kg 95-50-1 1,2-Dichlorobenzene ND 250 ug/kg 541-73-1 1,3-Dichlorobenzene ND 250 ug/kg 106-46-7 1,4-Dichlorobenzene ND 250 ug/kg 75-71-8 Dichlorodifluoromethane ND 250' ug/kg 75-34-3 1,1-Dichloroethane ND 250 ug/kg 107-06-2 1,2-Dichloroethane ND 250 ug/kg 75-35-4 1, l-Dichloroethene ND 250 ug/kg 156-59-2 cis-1,2TDichloroethene ND 250 ug/kg 156-60-5 trans-1,2-Dichloroethene ND 250 ug/kg 78-87-5 1,2-Dichloropropane ND 250 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 250 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 250 ug/kg 100-41-4 Ethylbenzene ND 50 ug/kg 75-09-2 Methylene chloride ND 250 ug/kg 79-34-5 . 1,1,2,2-Tetrachloroethane ND 250 ug/kg 127-18-4 Tetrachloroethene ND 250 ug/kg 108-88-3 Toluene ND 50 ug/kg 71-55-6 1,1,1-Trichloroethane ND 250 ug/kg 79-00-5 1,1,2-Trichloroethane ND 250 ug/kg 79-01-6 Trichloroethene ND 250 ug/kg 75-69-4 Trichlorofluoromethane ND 250 ug/kg 75-01-4 Vinyl chloride ND 250 ug/kg 1330-20-7 Xylene (total) ND 100 ug/kg

a4

H

r

r-

1—

r"

I - '

.-.

P


Sample FilelD DF Analyzed VI2010-MB1 150177.D 1 12/29/01

The QC reported here applies to the following samp

N4945-1, N4945-2, N4945-3


1868-53-7 Dibromofluoromethane 96% 17060-07-0 l,2-Dichloroethane-D4 103% 2037-26-5 Toluene-D8 100% 460-00-4 4-Bromofluorobenzene 110%



By Prep Date RFY n/a

les:

Limits

55-132% 54-129% 65-133% 58-137%

R.T. Est. Cone,

2.73 650 650

Page 2 of 2


Method: SW846 8260B

Units Q

ug/kg JN ug/kg

G

G

r

![

10

![

iC

IE

IG

[

iC

[


Page 1 of 1

Sample: VI1986-BFB1 Lab File ID: 149368.D Instrument ED: GCMSI


m/e Ion Abimdance Criteria Raw Abundance


50 75 95 96 173 174 175 176 177

15.0-40.0% of mass 95 30.0-60.0% of mass 95 Base peak, 100% relative abundance 5.0-9.0% of mass 95 Less than 2.0% of mass 174 50.0- 120.0% of mass 95 5.0-9.0% of mass 174 95.0- 101.0% of mass 174 5.0-9.0% of mass 176

9437 23187 39587 2726 81 28869 2145 28443 1828

23.8 58.6 100.0 6.9 0.2 72.9 5.4 71.8 4.6

(0.28) a

(7.4) a (98.5) a (6.4) b




Lab Sample ID

VI1986-1C1986 VI1986-1C1986 VI1986-ICC1986 VI1986-1C1986 VI1986-IC1986 VI1986-IC1986 VI1986-IC1986 VI1986-MB1 ZZZZZZ ZZZZZZ

Lab FileH)

149370. D 14937 I.D 149372. D 149373. D 149374. D 149375. D 149379. D 1493 83. D 1493 84. D 149385. D

Date Analyzed

12/07/01 • 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01 12/07/01

Time Analyzed

11:12 11:52 12:31 13:10 13:50 14:29 17:08 19:46 20:25 21:04

Hours Lapsed

01:18 01:58 02:37 03:16 03:56 04:35 07:14 09:52 10:31 11:10

Client Sample ID

Initial cal 5 ^ hiitial cal 20 Initial cal 50 Initial cal 10 Initial cal 1 Initial cal 100 Initial cal 400 Method Blank (unrelated sample) (uiurelated sample)

as

u

[

G

G

G

G

G

G

G

G

Initial Calibration Summary Job Number: N4945 Account: GESNJ Groundwater & Envirorunental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI1986-ICC1986 149372. D

Page 1 of 3

.Method T i t l e L a s t Upda te Response v i a

Response F a c t o r R e p o r t MSI

C:\HPCHEM\l\METHODS\MI1986.M (RTE I n t e g r a t o r ) SW-846 Method 8260 Mon Dec 10 1 4 : 2 7 : 4 6 2 0 0 1 Initial Calibration

Calibration Files 400 =149379.D 100 =149375.D 50 =149372.D 20 =149371.D 5

1 =149374.D =149370.D 10 =149373.D

1 2

3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35) 36] 37] 38) 39) 40) 41) 42] 43]

44)

Compound 100

) I Tert Butyl Alcohol-d9 )M tertiary butyl al 1 .428

) I pentafluorobenzene )M chlorodifluoromet M dichlorodifluorom M Dichlorotetrafluo )M chloromethane )M vinyl chloride )M 1,3-butadiene )M bromomethane M chloroethane M trichlorofluorome M ethyl ether M acrolein M freon 113 M acetone M 1,1-dichloroethen M acetonitrile )M iodomethane M methyl acetate M allyl chloride M methylene chlorid M carbon disulfide M acrylonitrile M methyl tert butyl M trans-1,2-dichlor M hexane M di-isopropyl ethe M 1,1-dichloroethan M vinyl acetate M chloroprene M ethyl tert-butyl M 2-butanone M 2,2-dichloropropa M ethyl acetate M cis-1,2-dichloroe M methacrylonitrile M chloroform M bromochloromethan M tetrahydrofuran M 1,1,1-trichloroet S dibromofluorometh S 1,2-dichloroethan

0 0 0 0 0 0 0 0 0 0

0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

.482 321 .310 .209 .176 .054 .251 117 801 106

432 078 302 009 .833 136 341 283 702

786 337 257 042 633 054 529 064 088 427 198 350 175 898 265 043 733 714 487

I 1,4-difluorobenzene

1

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

LOO

.338

.523

.396

.353

.241

.202

.066

.283 138 .865 .117 017 547 062 317 Oil .928 163 379 .308 762

847 357 274 165 680 053 543 154 074 509 225 361 182 927 272 046 864 728 573

0

0 0

0

0

0 0

0 0

0

0

0

0 0

0 0 0

--

L

.382

.081 013

.215

.844

.327 607

960 335

656

480

302

925 150

551 704 518

1

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0. 0 0 0 0 0 0

---

50

.379

.509

.417

.350

.238

.208

.061

.280

.134 817 114 017 532 056 309 .011 .916 .160 372 299 740

834 360 273 141 677 058 547 131 067 551 215 374 175 923 269 056 886 715 526

20

rSTD--1

[S^ 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

.287

rn .Lt — -

.463

.413

.342

.231

.228

.061

.310 142 .817 .116 020 497 060 293 009 .918 158 366 307 721

860 353 278 079 669 052 477 092 070 536 196 356 153 910 268 057 887 709 523

ISTD---

1

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

--

5

.035

.470 466 316 .226 220 029 .251 128 668 100 019 512 072 280 007 .907 117 388 316 717

886 351 261 102 689 032 448 119 039 523 218 357 079 931 255 040 863 707 509

1

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

---

LO

.360

.532 471 367 .274 .221 .058 .292 .134 .721 .114 018 550 099 319 012 .966 .178 385 .327 757

886 374 318 236 719 056 545 219 090 593 210 387 192 984 269 047 946 716 514

1

0 0 0 0 0 0 '0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1-0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

---

Avg

.304

497 414 346 .236 209 055 .278 132 781 107-017 512 071 291 010 .902 152 372 310 715 000 865 352 277 127 675 051 515 130 071 517 210 355 159 928 250 048 819 713 521

%RSD

10

5 13 7 9 9

24 8 6 9

11 13 8

22 12 17 5

14 4 5 7 -1 6 3 7 6 3

18 8 4

25 10 5 7

25 2

17 14 16 1 5

.73

80 23 50 .24 09 69 43 73 32 89 20 61 42 46 21 22 18 59 04 34 00 22 84 93 11 95 50 15 77 81 28 44 48, 94 92 76 67 43 11 05

z

Initial Cahbration Summary Page 2 of 3

r

G

G

G

G

G

G

G

Job Number: N4945 Account: GESNJ Groimdwater & Environmental Services Project

45)M 46)M 47)M 48)M 49)M 50)M 51)M 52)M 53)M 54)M 55)M 56)M 57)M 58)M 59)M 60)M •61)M 62)M 63)M 64)M 65)M 66)S 67)M 68)M 69)M 70)M 71)M

Fleet Bank, Wall

1,1-dichloroprope isopropyl acetate carbon tetrachlor cyclohexane tert-amyl methyl heptane 1,2-dichloroethan benzene Di-i sobutylene ethyl acrylate trichloroethene methylcyclohexane 1, 2 -dichloropropa propyl acetate methyl methacryla bromodichlorometh 1,4-dioxane dibromomethane 2-chloroethyl vin 4-methyl-2-pentan cis-1,3-dichlorop toluene-d8 (s) toluene trans-1,3-dichlor ethyl methacrylat 1,1, 2-trichloroet 2-hexanone

NJ

0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

72) I chlorobenzene-d5 73)M 74)M 75)M 76)M 77)M 78)M 79)M 80)M 81)M 82)M 83)M 84)M 85)M 86) 87)M

1, 3-dichloropropa butyl acetate tetrachloroethene dibromochlorometh 1,2-dibromoethane chlorobenzene 1,1,1,2-tetrachlo ethylbenzene m,p-xylene o-xylene styrene butyl acrylate bromoform 1-chlorohexane cyclohexanone

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

.573

.598

.932

.339

.887

.427

.647

.765

.644

.475

.512

.353 362 395 197 024 001 487 163 097 653 938 591 608 431 305 229

704 203 791 185 764 024 709 524 543 547 966 962 744 321 553

0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

88) I 1,4-dichlorobenzene-d -89)S 90)M 91)M 92)M 93)M 94)M 95)M 96)M 97)M 98)M 99)M

100)M 101)M 102)M

4-bromofluorobenz isopropylbenzene 1,1,2,2-tetrachlo 1,2,3-trichloropr trans-1,4-dichlor n-propylbenzene bromobenzene 1,3,5-trimethylbe 2 -chlorotoluene 4-chlorotoluene tert-butylbenzene 1,2,4 -trimethylbe vinyl toluene pentachloroethane

1 2 0 0 0 2 0 2 2 2 1 1

0

048 248 932 660 224 708 944 012 065 362 728 972

824

1 2 0 0 0 2 0 2 2 2 1 2

0

.581

.684

.988

.380

.990

.347

.690

.836

.820

.408

.538

.395 381 420 195 042 002 511 154 106 637 92 6 616 569 447 333 195

716 217 822 157 755 067 746 648 573 560 961 924 757 330 117

007 455 978 680 177 911 995 199 187 556 905 184

857

0

0 0

0 0

0 0 0

0

0

0 0 0 0 0 0

0

0 0 0 0 0 1 0 0 0 0 0 0 0

_ -

1

1

3 1 3 2 3

0

.533

.850

.220

.846

.937

.555

.531

.455

901

466

501 884 .606 357 352 285

649

877 854 652 995 696 670 593 550 713 706 522 252 495

138

261

834 191 193 827 338

912

0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 2 0 0 0 3 1 2 2 2 1 2

0

.601

.670

.988

.395

.984

.359

.693

.859

.940

.329

.545

.403 399 .406 .191 028 002 505 139 101 629 .903 .626 541 446 332 176

0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

Sample: Lab FilelD:

589 .566 .953 .392 .924 .317 694 852 .125 292 540 377 402 387 198 014 001 495 110 101 578 902 600 471 426 326 192

ISTD---730 213 899 157 764 108 780 725 599 613 988 854 750 327 166

0 0 0 0 0 0 0 1 0 0 0 0 0 0 0

578 149 >728 908 588 883 606 353 497 483 744 560 571 252 185

ISTD---013 623 992 764 151 040 041 342 505 488 997 311

887

1 2 1 0 0 3 1 2 2 2 2 2

0

037 745 051 882 120 060 057 471 509 645 018 359

863

0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 0 0 1 0 1 0 0 0 0 0 0 0

1 2 1 1 0 3 1 2 2 2 2 2

0

.564

.641

.882

.351'

.949

.261

.733

.861

.866

.230

.534

.372 413 .357 .187 954 .001 512 089 091 525 897 .623 433 398 328 174

686 152 828 960 641 041 682 518 551 551 753 506 576 303 234

061 909 142 263 072 130 087 660 387 974 202 508

860

0 1 1 0 1 0 0 0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 3 1 0 0 3 1 2 2 2 2 2

0

VI1986-ICC1986 [49372.D

636 .813 .002 .394 .053 .350 717 905 .454 261 567 406 424 476 192 012 001 509 115 107 615. 893 642 471 424 341 226

660 185 845 007 669 033 702 577 583 566 832 589 625 328 597

065 044 137 911 122 342 122 669 846 805 261 561

936

0 1 0 0 0 0 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 1 0 1 0 1 0 0 0 0 0 0 0

1 2 1 0 0 3 1 2 2 2 2 2 0 0

583 .662 .942 .353 .964 .344 717 859 141 333 542 405 405 407 194 996 001 498 128 101 591 906 615 493 418 322 199

675 187 827 033 690 022 703 574 563 553 851 729 649 302 335

053 671 071 860 144 146 062 507 475 738 019 316 000 877

5 5 6

17 6

15 8 6

39 27 3

14 7 9 2 5

29 3

22 6 9 2 2

17 8 6

11

7 16 6

12 10 6 7 7 6 6

13 25 15 11 60

4 10 10 25 36 11. 7

15 11 12 9 9

. -1 4

49 .18 .15 74 .02 .84 73 29 47 95 20 44 39 86 12 05 41 34 16 00 90 08 85 47 05 02 93

65 11 82 95 23 91 73 87 29 90 96 46 29 71 94

14 97 78 83 31 44 .65 36 . 92 17 67 35 00 .^

28 1

z:::

r ~

^

„ :

1 .

;.;

ii-i

Initial Cahbration Summary ^ Job Number: N4945 •

Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

103)M s e c - b u t y l b e n z e n e 2 . 4 3 1 104)M p - i s o p r o p y l t o l u e n 2 . 0 5 2 105)M 1 , 3 - d i c h l o r o b e n z e 1 . 3 8 8 106)M 1 , 4 - d i c h l o r o b e n z e 1 . 4 7 9 107)M n - b u t y l b e n z e n e 1 . 9 7 0 108)M 1 , 2 - d i c h l o r o b e n z e 1 . 3 3 8 109) M h e x a c h l o r o e t h a n e 0, .734 110)M l , 2 - d i b r o m o - 3 - c h l 0 . 3 0 1 111)M 1 , 2 , 4 - t r i c h l o r o b e 0 . 8 9 2 112)M h e x a c h l o r o b u t a d i e 0 . 6 2 8 113)M n a p h t h a l e n e 1 . 2 0 3 114)M 1 , 2 , 3 - t r i c h l o r o b e 0 . 7 3 6

2 . 6 0 6 2 . 2 0 2 1 . 4 0 9 1 . 5 2 5 2 . 0 6 8 1 . 3 6 7 0 . 7 7 1 0 . 2 7 9 0 . 9 0 1 0 . 7 3 1 1 . 1 0 4 0 . 7 4 9

(#) = O u t o f R a n g e # # # Number o f

3 . 4 0 6 2 . 6 6 4 1 . 6 6 7 1 . 7 7 2 2 . 3 2 7 1 . 6 6 0 0 . 6 5 8

1 . 0 0 4 0 . 7 5 8 0 . 5 2 3

2 . 7 5 2 2 . 2 9 8 1 . 4 3 1 1 . 5 6 1 2 . 0 6 9 1 . 4 1 0 0 . 7 9 6 0 . 2 6 7 0 . 8 3 6 0 . 7 7 0 0 . 9 1 8 0 . 7 0 3

c a l i b r a t i o n

2 2 1 1 1 1 0 0 0 0 0 0

\ Sample: Lab FilelD:

732 2 6 6 4 4 0 5 8 4 9 3 9 4 1 6 7 5 3 2 5 4 6 9 9 697 8 3 5 6 5 4

2 . 6 7 9 2 . 3 3 0 1 . 4 1 7 1 . 6 6 2 1 . 8 0 0 1 . 5 6 9 0 . 7 2 1 0 . 2 4 2 0 . 4 6 4 0 . 6 9 1 0 . 6 2 6 0 . 4 4 1

A v e r a g e

Page 3 of 3

VII986-ICC1986 I49372.D

2 . 9 9 6 2 . 3 8 4 1 . 4 9 9 1 . 5 9 0 2 . 0 1 3 1 . 4 9 0 0 . 8 1 5 0 . 2 8 4 0 . 7 4 2 0 . 8 7 0 0 . 8 6 5 0 . 7 1 4

2 . 8 0 0 2 . 3 1 4 1 . 4 6 4 1 . 5 9 6 2 . 0 2 7 1 . 4 6 4 0 . 7 5 0 0 . 2 7 1 0 . 7 5 6 0 . 7 7 0 0 . 9 0 1 0 . 6 4 6

% RSD = 11

l e v e l s e x c e e d e d f o r m a t

1 1 . 3 0 8 . 1 2 6 . 5 5 6 . 0 2 7 . 9 6 7 . 9 1 6 . 9 7 7 . 7 8

2 1 . 6 9 1 6 . 6 1 2 1 . 9 5 1 8 . 3 0

. 7

###

G

G

G

G

G

30

G

G

G

G

G

G

G

G

Continuing Cahbration Summary Job Number: N4945 Account: GESNJ Groundwater & Environmental Services Project: Fleet Bank, Wall, NJ

Sample: Lab FilelD:

VI2010-CC1986 150175.D

Page 1 of 3

Data Acq (

Evaluate Continui

File 3n

Sample Misc

ng Calibration Report

C:\HPCHEM\1\DATA\I50175.D 29 Dec 2001 9:26 pm CC1986-50 MS58670,VI2010,10,,10C

MS Integration Params: RTEIN2.P


Min. Max.

1 I 2 M

3 I 4 M 5 M 6 M 7 M 8 M 9 M

10 M 11 M 12 M 13 M 14 M 15 M 16 M 17 M 18 M 19 M 20 M 21 M 22 M 23 M 24 M 25 M 26 M 27 M 28 M 29 M 30 M 31 M 32 M 33 M 34 M 35 M 36 M 37 M 38 M 39 M 40 M 41 M

,25,1

C:\HPCHEM\l\METHODS\MI1986.M SW-846 Method 8260 Mon Dec 10 16:29:00 Multiple Level Cali

RRF : 0.000 Min. Rel. RRF Dev : 2 0% Max. Rel.

Compound

Tert Butyl Alcohol-d9 tertiary butyl alcohol

pentafluorobenzene chlorodi fluoromethane dichlorodifluoromethane Dichlorotetrafluoroethane chloromethane vinyl chloride 1,3-butadiene bromomethane chloroethane trichlorofluoromethane ethyl ether acrolein freon 113 acetone 1,1-dichloroethene acetonitrile iodomethane methyl acetate allyl chloride methylene chloride carbon disulfide acrylonitrile methyl tert butyl ether trans-1,2-dichloroethene hexane di-isopropyl ether 1,1-dichloroethane vinyl acetate chloroprene ethyl tert-butyl ether 2-butanone 2,2-dichloropropane ethyl acetate cis-1, 2-dichloroethene methacrylonitrile chloroform bromochloromethane tetrahydrofuran 1,1,1-trichloroethane

2001 bration

Area : 50 Area : 150

AvgRF

1.000 1.304

1.000 0 .497 0.414 0.346 0.236 0.209 0.055 0.278 0.132 0.781 0.107 0.017 0.512 0.071 0.291 0.010 0.902 0.152 0.372 0.310 0.715 0.000 0.865 0.352 0.277 1.127 0.67.5 0.051 0.515 1.130 0.071 0.517 0.210 0.355 0.159 0.928 -0.250 0.048 0.819

(RTE In

% Max. %

CCRF

1.000 1.244

1.000 0.465 0.308 0.261 0.204 0.171 0.051 0.253 0.111 0.859 0.100 0.019 0.434 0.060 0.265 0.008 0.868 0.174 0.309 0.272 0.576 0.029 0.838 0.313 0.197 0.993 0.621 0.040 0.524 1.069 0.060 0.430 0.187 0.332 0.132 0.907 0.252 0.047 0.905


tegrator)

R.T. Dev

2 RUIFENGY MSI, 1.00

1

0.50min

%Dev Area% Dev(min)

0.0 4.6

0 .0 6.4

25. 6# 24.6# 13 .6 18.2 7.3 9.0

15.9 -10.0 6.5

-11.8 15.2 15.5 8.9

20.0 3.8

-14.5 16.9 12.3 19.4 0.0 3.1

11.1 28.9# 11.9 8.0

21.6# -1.7 5.4

15.5 16.8 11.0 6.5

17.0 2.3

-0.8 2.1

-10.5

68 61

76 69 56 57 65 63 63 69 63 80 67 82 62 82 <. 65 60 72 83 63 69 59 0#

76 66 55 66 70 52 73 72 68 59 66 68 57 75 71 64 78

0 -0

-0 -0 -0 -0 0 0 0 -0 -0 -0 -0 0 0 0 -0 0 -0 -0 -0 -0 -0 -0 -0 -0 -0 -0 -0 -0 -0 0 -0 -0 -0 -0 -0 -0 -0 0 -0

00 03

03 02 03 04 00 00 00 03 03 03 04 00 00 00 04 00 03 02 03 03 03 03 02 03 02 05 03 03 02 00 02 02 02 03 03 03 03 00 03 ^ 3 1

G

G

G

G

G

G


Sample: Lab FilelD:

VI2010-CC1986 150175.D

Page 2 of 3

42 S 43 S

44 I 45 M 46 M 47 M 48 M 49 M 50 M . 51 M 52 M 53 M . 54 M 55 M 56 M 57 M 58 M 59 M 60 M 61 M 62 M 63 M 64 M 65 M 66 S 67 M 68 M 69 M 70 M 71 M


88 I 89 S 90 M 91 M 92 M 93 M 94 M 95 M 96 M 97 M 98 M

dibromofluoromethane (s) l,2-dichloroethane-d4 (s)

1,4-difluorobenzene 1,1-dichloropropene isopropyl acetate carbon tetrachloride cyclohexane tert-amyl methyl ether heptane 1,2-dichloroethane benzene Di-isobutylene ethyl acrylate trichloroethene methylcyclohexane 1,2-dichloropropane propyl acetate methyl methacrylate bromodichloromethane 1,4-dioxane dibromomethane 2-chloroethyl vinyl ether 4-methyl-2-pentanone cis-1,3-dichloropropene toluene-d8 (s) toluene trans-1,3-dichloropropene ethyl methacrylate 1,1,2-trichloroethane 2-hexanone

chlorobenzene-d5 1,3-dichloropropane butyl acetate tetrachloroethene dibromochloromethane 1,2-dibromoethane chlorobenzene 1,1,1,2 -tetrachloroethane ethylbenzene m,p-xylene o-xylene styrene butyl acrylate bromoform 1-chlorohexane cyclohexanone

1,4-dichlorobenzene-d4 4-bromofluorobenzene (s) isopropylbenzene 1,1,2,2 -tetrachloroethane 1,2,3-trichloropropane trans-1,4-dichloro-2-butene n-propylbenzene bromobenz ene 1,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene

0.713 0.521

1.000 0.583 1.662 0.942 0.353 0.964 0.344 0.717 0.859 1.141 0.333 0.542 0.405 0.405 0.407 0.194 0.996 0.001' 0.498 0.128 0.101 0.591 0.906 ,0.615 0.493 0.418 0.322 0.199

1.000 0.675 0.187 0.827 1.033 0.690 1.022 0.703 1.574 0.563 0.553 0.851 0.729 0.649 0.302 0.335

1.000 1.053 2.671 1.071 • 0.860 0.144 3.146 1.062 2.507 2.475 2.738

0.711 0.586

1.000 0.588 1.540 1.097 0.352 1.034 0.211 0.812 0.814 0.812 0.255 0.541 0.283 0.364 0.391 0.193 1.116 0.001 0.532 0.127 0.098 0.597 0.915 0.625 0.534 0.436 0.325 0.178

1.000 0.715 0.186 0.876 1.192 0.767 1.073 0.829 1.659 0.578 0.593 0.906 0.622 0.821 0.330 0.000

1.000 1.069 2.488 0.941 0.813 0.142 2.718 1.047 2.222 2.178 2.369

0 -12

0 -0 7

-16 0

-7 38

-13 5

28 23 0

30 10 3 0

-12 0

-6 0 3

-1 -1 -1 -8 -4 -0 10

0 -5 0

-5 -15 -11 -5

-17 -5 -2 -7 -6 14

-26 -9

100

0 -1 6

12 5 1

13 1

11 12 13

.3

.5

.0

.9

.3

.5

.3

.3

.7#

.2

.2

.8#

.4#

.2

.1#

.1

.9

.5

.0

.0

.8 8 0 0 0 6 3 3 9 6

0 9 5 9 4 . 2 0 9 4 7 2 5 7 5# 3

o#

0 5 9 1 5 4 6 4 4 0 5

76 85

71 69 65 78 63 74 41# 83 67 61 55 70 50# 64 68 71 77 60 74 65 68 67 71 71 70 69 69 71

73 72 64 72 76 74 71 78 71 71 71 67 54 80 74

o#

75 79 71 71 80 70 67 75 71 65 71

-0.03 •-0.02

-0.05 -0.03 -0.04 -0.03 -0.04 -0.03 -0.07 -0.03 -0.03 -0.04 -0.04 -0.03 -0.05 -0.03 -0.03 -0.03 -0.04 -0.03 -0.03 -0.03 -0.03 -0.05 -0.04 -0.04 -0.03 -0.03 -0.03 -0.03

-0.04 -0.03 ' -0.04 -0.03 -0.04 -0.03 -0.03 -0.04 -0.03 -0.03 -0.03 -0.03 -0.03 -0.03 -0.04 -19.65#

-0.03 -0.03 -0.03 -0.03 -0.04 -0.03 -0.03 -0.03 -0.03 -0.04 -0.03 32

G

G

G

G

G


Page 3 of 3

99 M 100 M 1 0 1 M 102 103 104 105 106 107 108 109 110 111 112 113 114

M M M M M M M M M M M M M

tert-butylbenzene 1,2,4-trimethylbenzene vinyl toluene pentachloroethane sec-butylbenzene p-i sopropyltoluene 1,3-dichlorobenzene 1,4-dichlorobenzene n-butylbenzene 1,2-dichlorobenzene hexachloroethane 1,2-dibromo-3-chloropropane 1,2,4-trichloroben2ene hexachlorobutadiene naphthalene 1,2,3 -trichlorobenzene

Se

2 2 0 0 2 2 1 1 2 1 0 0 0 0 0 0

rvices

019 .316 .000 877 .800 .314 .464 596 027 464 750 271 756 770 901 646

2 2 0 0 2 2 1 1 1 1 0 0 0 0 0 0

Sample: Lab FUelD:

009 195 .000 935 488 .099 .373 524 714 371 824 267 778 762 868 591

0 5 0

-6 11 9 6 4

15 6

-9 1

-2 1 3 8

VI2010-CC1986 I50175.D

5 2 .0 6 1 3 .2 5 4 4 9 5 9 0 7 5

75 71 0#

79 68 68 72 73 62 73 78 75 70 74 71 63

-0.03 -0.03 -0.03 -0.03 -0.03 -0.03 -0.03 -0.04 -0.04 -0.03 -0.03 -0.03 -0.03 -0.02 -0.02 -0.03

Average % D = 1.5

(#) = Out of Range 149372.D MI1986.M


33

G

G

G

G

G

G


Page 1 of 1


Check Std Upper Limit Lower Limit''

Lab Sample ID

VI2010-MB1 VI2010-BS ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ N4945-1 N4945-2 N4945-3 ZZZZZZ N5167-7MS " N5167-7MSD <" N5167-7 ZZZZZZ

VI2010-CC1986 150175.D GCMSI

I S I AREA

53110 106220 26555

I S I AREA

54499 54593 54657 54774 55120 58746 57766 59838 59097 56253 60093 57662 56235 59176 61892

• 54910

RT

5.86 6.36 5.36

RT

5.85 5.84 5.90 5.88 5.88 5.92 5.90 5.86 5.88 5.88 5.86 5.89 5.91 5.88 5.90 5.89

IS 1 = Tert Butyl Alcohol-D9 IS 2 = Pentafluorobenzene IS 3 =1,4-Difluorobenzene IS 4 = Chrorobenzene-D5

IS 2 AREA

339802 679604 169901

IS 2 AREA

338587 340617 350321 352623 349941 354286 349632 352696 355796 348224 352335 345987 348547 354821 351979 347537

IS 5 =1,4-Dichlorobenzene-d4

Inj ection Date: 12/29/01 Injection Time: 21:26 Method:

RT

9.63 10.13 9.13

RT

9.62 9.63 9.63 9.63 9.63 9.63 9.62 9.63 9.63 9.62 9.63 9.63 9.62 9.63 9.64 9.63

IS 3 AREA

298807 597614 149404

IS 3 AREA

293567 289077 304162 303783 302989 306219 306757 309240 308467 303044 308780 298560 303973 310725 308002 306502

SW846 8260B

RT

11.61 12.11 11.11

RT

11.61 11.60 11.60 11.60 11.61 11.62 11.61 11.61 11.61 11.62 11.61 11.60 11.60 11.61 11.61 11.62

IS 4 AREA

233764 467528 116882

IS 4 AREA

230033 224578 239864 243572 237361 242016 241187 238121 247528 239823 241542 238682 234600 240954 243207 240135

RT

17.72 18.22 17.22

RT

17.72 17.72 17.73 17.74 17.72 17.73 17.73 17.73 17.72 17.73 17.73 17.74 17.73 17.73 17.74 17.73

IS 5 AREA

158564 317128 79282

IS 5 AREA

129029 150947 140968 137225 140869 134448 135618 138939 139179 134381 136545 148511 156931 159909 140452 133647

RT

22.10 22.60 21.60

RT

22.10 22.09 22.10 22.10 22.10 22.10 22.10 22.10 22.10 22.10 22.11 22.11 22.10 22.10 22.10 22.10

(a) Upper Limit = -f 100% of check standard area; Retention time -1-0.5 minutes. (b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes. (c) Methanol preservation/extraction.

34

Quantitation Report (QT .Reviewed)

Data File : C:\HPCHEM\1\DATA\I50185.D Acq On : 30 Dec 2001 3:59 am Sample : N4945-1 Misc : MS58673,VI2010,4.7, ,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 1 13:01 2002



Quant Method : C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title : SW-846 Method 8260 Last Update : Mon Dec 10 16:29:00 2001 Response via : Initial Calibration DataAcq Meth : MI1986


c G

G

G

G

G

1) Tert Butyl Alcohol-d9 3) pentafluorobenzene

44) 1,4-difluorobenzene 72) chlorobenzene-d5 88) 1,4-dichlorobenzene-d4


43) l,2-dichloroethane-d4 (s) Spiked Amount 50.000

66) toluene-dS (s) Spiked Amount 50.000

89) 4-bromofluorobenzene (s) Spiked Amount 50.000

Target Compounds 75) tetrachloroethene

5.88 65 9.63 168

11.61 114 17.72 117 22.10 152

9.88 113

10.85 65

14.74 98

19.98 174

16.22 166

59097 355796 308467 247528 139179


0.02 -0.03 -0.05 -0.04 -0.03

240858 47.47 PPb -0.03 Recovery = 94.94%

188280 50.74 PPb -0.03 Recovery = 101.48%

280101 50.11 PPb -0.04 Recovery = 100.22%

156980 53.56 PPb -0.03 Recovery = 107.12%

Qvalue 15240 234.50 PPb 92

9<^

(#) = qualifier out of range (m) = manual integration 150185.D MI1986.M Mon Jan 07 12:49:04 2002 GCMSI Page 1

35

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50185.D Acq On : 30 Dec 2001 3:59 am Sample : N4945-1 Misc : MS58673,VI2010,4.7,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 1 13:01 2002

V i a l O p e r a t o r I n s t M u l t i p l r

12 RUIFENGY MSI 6 3 . 0 0



C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dec 10 1§:29:00 2001 Initial Calibration

Abundance J

210000-

200000-

190000-

180000-

170000

160000

150000

140000-

130000

120000

110000-

100000

90000

80000-

70000-

60000-

50000-

40000-

30000-

20000-

10000-

n

1 2

O i

• a

•o

5 2-CC

V.

. _

-

L A... U - I—1—1—1—1—p—]—1—1—1—1—1—1—1—1—1—[—1—1—1—

Time-> 2.00 4.00 6.00 8.00 1

s~

fluoro

me

oro

benzi

dib

rom

o

1,4

-diflu

« S ?

1 '-6

V, I L. 1 ^ • • ' ' ' • ' • ! 1 '

0.00 12.00

TIC: I50185.D

_ •a

1

w

s

2

0)' c

.c o

\ . I n—1—I—r-i—1—1—1—1—1—1—1—1—r~r

14.00 16.00 18.00

« s

a E

'

;

20

^ .a

: o

i 1 1 T3

1 ^.

i

v_

'

L. 00 22.00 24,00 26,00 28,00

150185.D MI1986.M Mon Jan 07 12:49:08 2002 GCMSI Page 336

G

G

G

G

#75 tetrachloroethene Coneen: 234.50 PPb RT: 16.22 min Scan# 1740 Delta R.T. -0.03 min Lab File: 150185.D Acq: 30 Dec 2001 3:59 am

Ion:166 Ratio 100 46.4 75.6 67.3

Resp: Lower

22.5 38.7 43.0

15240 Upper

82.5 98.7

103.0 ^bundancelon 166,00 (165,70 to 166,70); 150185.

Ion 168,00 (167,70 to 168.70): 150185.1 Ion 129,00 (128,70 to 129.70): 150185.: Ion 131,00 (130,70 to 131,70): 150185,

16,22

l " " l " " l " " T " " l " l l | l l M | M l l | l l l P | n > I | M I I ' | | M I I | M l l | l

]mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' I

rime~> 16,00 16,10 16.20 16.30 16.40

150185.D MI1986.M Mon Jan 07 12:49:13 2002 GCMSI Page 3*7

'- Data File Acq On Sample Misc

C:\HPCHEM\1\DATA\I50185.D Vial 30 Dec 2001 3:59 am Operator N4945-1 Inst MS58673,VI2010,4.7,,100,5,1 Multiplr



.-. Method Title

"~ Smoothing __. Sampling

Start Thrs - Stop Thrs

C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 ON Filtering: 5 1 Min Area: 1000 Area counts 0.1 Max Peaks: 100 0.05 Peak Location: TOP


Signal TIC

pea '- #

""i 1 ^ 2

3 r L 5

L 7 8

r^ 9 L 10

p 11 ; 12 13

r- 14 15

p. 16 ' 17

^ 18 19 20

21 22

^-23 24

- 25

26 ' 27 '.,28

k R.T. min

2.742 2.962 3.612 3.680 3.747

4.102 4.356 5.369 5.428 5.884

6.197 6.417 6.679 9.627 9.880

10.260 10.851 11.612 14.737 15.151

16.207 17.728 18.125 19.975 20.338

20.541 20.929 21.233

first scan

123 ' 168. 242 254 261

305 329 442 459 495

553 576 605 939 978

1032 1083 1174 1543 1613

1728 1903 1963 2171 2227

2249 2294 2331

max scan

145 171 248 256 264

306 336 456 463 517

554 580 611 960 990

1035 1105 1195 1565 1614

1739 1919 1966 2185 2228

2252 2298 2334

last scan

168 187 250 261 269

309 339 459 471 553

561 586 612 978

1025

1038 1147 1231 1613 1620

1758 1952 1970 2227 2235

2263 2299 2339

, PK TY

rBV2 rVB2 rBV2 rVB rBV2

rBV2 rBV2 rBV3 rVB2 rBV3

rVB2 rVB rBV rBV3 rVB3

rVB2 rBV4 rBV3 rBV rVB2

rBB8 rBV2 rVB2 rBV2 rVB2

rVV4 rVB rBB

peak height

17975 1781 761 604 952

645 533

1332 852

7192

1073 551 602

128249 104200

8 35 56715

105653 108326

556

14648' 136608

811 179555

877

254 678 605

peak area

176505 8723 1833 1380 1334

1011 1389 6284 2985

105780

1780 1288 1014

1121191 878811

1473 453650 854961 843389

1027

93567 869336

1001 1062618

1859

1455 1067 1003

peak % max.

15.74% 0.78% 0.16% 0.12% 0.12%

0.09% 0.12% 0.56% 0.27% 9.43%

0.16% 0.11% 0.09%

100.00% 78.38%

0.13% 40.46% 76.25% 75.22% 0.09%

8.35% 77.54% 0.09%

94.78% 0.17%

0.13% 0.10% 0.09%

% of total

2.365% 0.117% 0.025% 0.018% 0.018%

0.014% 0.019% 0.084% 0.040% 1.417%

0.024% 0.017% 0.014%

15.021% 11.774%

0.020% 6.078%

11.454% 11.299% 0.014%

1.254% 11.647% 0.013%

14.236% 0.025%

0.019% 0.014% 0.013%

38

29 30

31 32 33 34 35

36 37 38 39

22 22

22 22 23 23 23

23 23 23 23

103 576

754 923 016 117 235

430 531 607 995

2424 2490

2511 2528 2544 2555 2567

2591 2603 2610 2660

2437 24 93

2514 2534 2545 2557 2571

2594 2606 2615 2661

2475 2497

2517 2537 2552 2562 2575

2598 2610 2618 2667

Sum

rBV2 rVB3

rVB3 rVB3 rBV3 rVB rVB3

rVB2 rVB2 rBV2 rVB2

165252 934

1056 870 741 613 669

570 718 495

• 521

of corrected

952082 1441

1650 2038 1424 1193 1621

1280 1066 1293 1262

areas:

84.92% 0.13%

0.15% 0.18% 0.13% 0.11% 0.14%

0.11% 0.10% 0.12% 0.11%

7464064

12 0

0 0 0 0 0

0 0 0 0

756% 019%

022% 027% 019% 016% 022%

017% 014% 017% 017%


G

G

G

G

G


File Operator Acquired Instrument, Sample Name Misc Info Vial Number Quant File

C:\HPCHEM\1\DATA\I50185.D RUIFENGY 30 Dec 2001 3:59 am using AcqMethod MI1986 MSI

N4945-1 MS58 673,VI2010,4.7, ,100,5,1 12


Time~>

undance

150000

100000

50000

0-

2,74

/ \ l^ 1 1 1 1 1 1 , p , 1 f . , ?-|-i 1 1

33aaB5 4,101,36 1 1 r n 1 1 n i T - | 1 1 ,

TIC: I50185,D

-

9,63

•

553*3 ><!6.2e.42B,68 j 1 , , n - | 1 !•', , 1^-1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 , , 1 , , 1 , 1 , 1 1 i ' l

' 9,88

V M0,2

' 1 ' ' 1

2.00 2,50 3,00 3.50 4,00 4,50 5,00 5,50 6,00 6,50 7,00 -7.50 8,00 8.50 9.00 9,50 10,00 Abundance

150000

100000-

TIC: 150185,D

50000

17,73

11.61 14,74

10,85

15,15

16.21

J8.12

Tlme~> 10,50 11,00 11,50 12,00 12,50 13,00 13,50 14,00 14,50 15.00 15.50 16,00 16,50 17,00 17,50 18,00 18,50 19,00 Abundance

150000-

100000

50000

TIC: 150185,D

O-V

19,97 22,10 I

, ^gO.39,54 20,931.23 ' ^ " — p - ' - ' - n -

22^2223283581 24 00 - i - f I I I I I I I I ' I I I I I I I ' I ' I I ' I I ' I , , I I I I I I I I I I I I I 1-1 I I I I I I I 1 I I I I I I 1 I I , r-l I I , I , I I 1 , I , I 1 1-

rime-> 19.50 20,00 20,50 21,00 21,50 22,00 22,50 23,00 23,50 24,00 24,50 25,00 25,50 26,00 26,50 27,00 27,50



C:\HPCHEM\1\DATA\I50185.D 30 Dec 2001 3:59 am N4945-1 MS58 67 3vVI2010,4.7,,100,5,l




k k k k - k k k k k k k - k k k k k k k k k k k k k k k k k k k k k - k k k k k k k k k k k k k k k k - k - k k k k k k k k k k k k k k k k k k k k



G

G

G

G

G

G

G

R.T. EstConc Area Relative to ISTD



R.T,

9.63

CAS# Qual

1 Carbon dioxide 2 Carbon dioxide 3 Nitrous Oxide 4 Nitrous Oxide

4 4 C02 4 4 C02 44 N20 44 N20

0 0 0 1 2 4 - 3 8 - 9 3 0 0 0 1 2 4 - 3 8 - 9 3 0 1 0 0 2 4 - 9 7 - 2 3 0 1 0 0 2 4 - 9 7 - 2 3

Abundance

5000

i ] i i T i | i i i i [ i i i i | i i i i ] i i i i | iM i | i i i i | in i - jn i iHTrr | 'n i i | i iM|nu| i inn i i i [Tmj inn i i t i ]T i i i ]T in [ i ii i j 11 u] i n i ] 11 i i j i i i i [i i i i •n/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Abundance

5000

mlz-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Scan 145 (2,742 min): 150185,D (-)

44

40


16 22 • | | | | | ' | | | | | | | | ' | | ' | | " | | | " | | | ' | | | | | | | | | | | | | | | | | | " | | | " | | | ' | ' | | | | | " | | | | | | | | | | | | | | | " l " | | i " | | | | | ' | | | | " l " | | |

46

Abundance

5000


12 16 22 46

||'|||||||||"|||||'||||'||||||||||||||'||'||||"|||||'||||"||"|||||||'|"|||"||"'I""I'|'|||"||'"|||||'I"|||'||'||'|||'| mlz-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

| i i i i | i i i M ' i i i | i i i i | i i i i | i i i i | i i i i | i ' i ' | i " i | i i i i | " i i | i ' i i | ' i i i ! i i i ' | i " i | " " l " " l " " l " " l " " | i i i i | i ' i i | i i i i | i i i i | i m/z- i 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m/z 100.00%

' ' I I ' I I I I I I I I I ' ' ' I ' I I ' I

2.40 2.60 2.80 3.00

m/z 39..95 18.71%

2.40 2.60 2,80 3,00

m/z 44.95 1.34%

2.40 2.60 2.80 3.00


~-\ Tentatively Identified Compound (LSC) summary

,_ Operator ID: RUIFENGY Date Acquired: 30 Dec 2001 3:59 am 'Data File: C:\HPCHEM\1\DATA\I50185.D - Name: N4 94 5-1 Misc: MS58673,VI2010,4.7,,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title: SW-846 Method 8260 Library Searched: •C:\DATABASE\NBS75K.L




G

G

G

G

G

G

42


Data File : C:\HPCHEM\1\DATA\I50186.D Acq On : 30 Dec 2001 4:38 am Sample : N4945-2 Misc : MS58673,VI2010,4.5, ,100",5, 1 MS Integration Params: RTEIN2.P Quant Time: Jan 1 13:02 2002




C:\HPCHEM\l\METHODS\MI1986.M SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Initial Calibration MI1986

(RTE Integrator)

[— Internal Standards R.T. Qlon Response Cone Units Dev(Min)

G

G

G

G

G

G


44) 1,4-difluorobenzene 72) chlorobenzene-d5 88) 1,4-dichlorobenzene-d4


43) l,2-dichloroethane-d4 (s] Spiked Amount 50.000

66) toluene-d8 (s) Spiked Amount 50.000


Target Compounds

5 . 8 8 9 . 6 2

1 1 . 6 2 1 7 . 7 3 2 2 . 1 0

65 168 114 117 152

9.88 113

10.84 65

14.75 98

19.98 174

56253 348224 303044 239823 134381


0.02 -0.04 -0.04 -0.03 -0.03

236740 47.67 PPb -0.03 Recovery = 95.34%

182061 50.13 PPb -0.03 Recovery = 100.26%

274180 49.92 PPb -0.03 Recovery = 99.84%

156287, 55.23 PPb -0.03 Recovery = 110.46%

Qvalue

G

G 7


43

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50186.D Acq On : 30 Dec 2001 4:38 am Sample : N4945-2 Misc. : MS58673,VI2010,4.5,,100,5,1 MS Integration Params: RTEIN2.P Quant Time: Jan 1 13:02 2002




C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Initial' Calibration

Abundance 210000-

200000-

190000

180000

170000-

160000

150000-

140000-

130000-

120000-

110000-

100000-

90000

80000-

70000-

60000-

50000-

40000 -

30000-

20000

10000-

f\

u -

a c a c a

" (

1" = ,-c §^ CO) lUC —

hol-d

9.1

tylA

Ico

,

3 CD r 0) H

K I .A T-"T-T'-I—1—1—[—1—1— \—1—1—1—1—1—1—I—1—1—r—r

rime--> 2.00 4.00 6.00 8.00 1

1 1

dibr

omof

l

1,4-

diflu

o

CO

T3

1 cil.

-L I L |->'i -1 r 1 i-r

D.OO 12.00

TIC; 150186.D

c

1 u

CO

CO

I L 1 -1 1 -rJi 1 1 1 1 1 1 1 1 1 1

14.00 16,00 18,00

5:"

e (s

). S

enze

ne-d

nzen

loro

b

c

i 1 j 4

l^ -f 1 1 1 1 1 1 1 20,00 22,

L , 1 1 * ^ 'f

00 24,00 26,00 28,00

150186.D • MI1986.M Mon Jan 07 12:50:09 2002 GCMSI Page 2 44



D C:\HPCHEM\1\DATA\I50186 30 Dec 2001 4:38 am N4945-2 MS58 67 3,VI2010,4.5, ,100,5,1

• Vial: 13 Operator: RUIFENGY Inst : MSI Multiplr: 56.40



C:\HPCHEM\l\METHODS\MI1986.M SW-846 Method 8260 ON 1 0.1

(RTE Integrator)

Filtering: Min Area:

Max Peaks: 0.05 Peak Location;



Signal TIC

pea #

• 1

^ 2 ,3 4

L 5

r 6 - 7

8 ^ 9 J, 10

" 11

„, 12 13

r 14 15

pl6 17 18

, 19 20

.. 21 22

G-23 24

- 25

26 • 27 .'.28

k R.T. min

2.742 3.528 3.663 3.722 3.832

4.322 • 5.336 5.446 5.851 6.214

6.468 9.618 9.880

10.303 10.852

11.122 11.620 14.754 15.177 17.728

18.040 18.294 18.378 19.983 20.490

20.600 20.684 22.095

first scan

123 231 253 258 265

322 442 464 492 555

583 938 977

1038 1087

1136 1176 1548 1616 1905

1955 1983 1993 2172 2244

2255 2266 2421

max scan

145 238 254-261 274

332 452 465 513 556

586 959 990

1040 1105

1137 1196 1567 1617 1919

1956 1986 1996 2186 2246

2259 2269 2436

last scan

183 239 258 265 276

333 453 474 534 562

596 977

1038 1053 1136

1143 1224 1611 1624 1955

1960 1993 2002 2233 2255

2264 2282 2478

PK TY

rBV2 rVB rVB rBV rVB

rBB rBV rVB2 rBV4 rVB

rBB rBV rVV2 rVB2 rBV2

rVB2 rBV3 rBV3 rVB2 rBV2

rVB2 rVB2 rBB rBV rVB3

rVV2 rVB3 rBV2

peak-height

26822 700 753 605 420

383 1003 546

7535 702

474 123306 103089

853 54883

805 102967 105422

670 133909

1312 515 529

176171 728

694 734

158574

peak area

265464 1277 1138 1330 1806

1346 3087 1265

90813 1342

1328 1088796 901119

3448 431115

1733 831384 815832

1175 853458

1443 1642 1047

1038897 2420

1792 2534

900414

peak % max.

24.38% 0.12% 0.10% 0.12% 0.17%

0.12% 0.28% 0.12% 8.34% 0.12%

0.12% 100.00%i 82.76% 0.32%.

39.60%

0.16% 75.36% 74.93% 0.11%

^ 78.39%

0.13% 0.15% 0.10%

95.42% 0.22%

0.16% 0.23%

82.70%

% of total

3 0 0 0 0

0 0 0 1 0

0 14 12 0 5

0 11 11 0

11

0 0 0

14 0

0 0

12

652% 018% 016% 018% 025%

019% 042% 017% 249% 018%

018% 977% 395% 047% 930%

024% 436% 222% 016% 740%

020% 023% 014% 290% 033%

025% 035% 386%

45

29 30

31 32 33 34 35

36 37 38

22 22

22 22 22 22 22

23 23 23

467 585

729 796 872 931 991

083 633 954

2478 2493

2508 2516 2525 2533 2539

2552 2613 2653

2480 2494

2511 2519 2528 2535 2542

2553 2618 2656

2493 2502

2516 2525 2533 2539 2545

2563 2626 2660

rVV4 rVV4

rVB4 rVV5 rVB4 rBV rBV2

rVB4 rBV2 . rBB

1320 639

721 8,07 925 656 632

484 518 561

6930 2172

2043 2044 2063 1107 1070

1280 1651 1044

0 0

0 0 0 0 0

0 0 0

64% 20%

19% 19% 19% 10% 10%

12% 15% 10%

0 0

0 0 0 0 0

0 0 0

095% 030%

028% 028% 028% 015% 015%

018% 023% 014%

G

G

G

G

G

G

G

G

G

G



G 46



C:\HPCHEM\1\DATA\I50186. D RUIFENGY 30 Dec 2001 4:38 am using AcqMethod MI1986 MSI

N4945-2 MS58 67 3,VI2010,4.5, ,100,5,1 13


Abundance

150000

100000-

50000

rime~>

TIC; I50186,D

9,62

2,74

3,33^33 4.32 5.85

5,3,415 y~~^.2^.A7 I ' ' ' ' p ' ' I ' I ' ' I I I I I I I I I ' I I I I ' I ' I ' ' ' ' r ' ^ ' ' I ' I I ' I I ' I ' I I I ' I I ' I I I I I I I ' I I I

2.00 2.50 3,00 3,50 4.00 4,50 5,00 5.50 6,00 6,50 7,00 7,50 8,00 8,50 9.00 9.50 10,00

50000-

fTime~> 10,50 11,00 11,50 12,00 12.50 13,00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17,00 17,50 18,00 18,50 19.00 Abundance

150000

100000

TIC; I50186.D

50000

19 98 22,10

2C£BSa8 I I I ' 'i I ' ' " ^ ' I ' I ' I I ' '

8 23.623,95 r I I I M I I ' I I I I I I I I I I ' I ' ' I I i I I I I I I I I ' 1 1 I I I I ' I I I I I I I

Time~> 19,50 20,00 20,50 21,00 21,50 22,00 22,50 23,00 23,50 24,00 24,50 25,00 25,50 26,00 26,50 27,00 27,50

150186.D MI1986.M Mon Jan 07 12:50:36 2002 GCMSI 4t


C:\HPCHEM\1\DATA\I50186.D 30 Dec 2001 4:38 am N4945-2 MS58 67 3,VI2010,4.5,,100,5,1




C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 C:\DATABASE\NBS7 5K.L

k k k k k k k k k k k k k k k - k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k - k k k k k k k k k k k k k k k k k k k k



R.T, EstConc Area Relative to ISTD R.T,

G

G

G

G

G

G

G

G

G



9.62

CAS# Qual

1 Carbon dioxide 2 Carbon dioxide 3 Nitrous Oxide 4 Nitrous Oxide

4 4 C02 44 C02 44 N20 44 N20

000124-38-9 3 000124-38-9 3 010024-97-2 3 010024-97-2 3

Abundance

5000

m/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000-

||||||||||||||||||||||"|||'||'||||||"||||||||'"||"|'||"Miiii|""||"||||"||'|||"|'i"||||||||||"i""|ii"i"i'r"'i"'

fii/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Scan 145 (2,742 min); 150186.D (-) 44

40

' | | ' | | | | " | | " " l ' | | " | | | " " i " | | | " " l ' | " l " " l " " l " " l " " l I I I I I I I I I I I I I I I I I I I


16 22 46

Abundance

5000


12 16 22 46

|||||||||||||||||||'||||||||"|||'|||||||||||||"|'||"|||"||"|'I'||'I'|"I"|||||"I'||'|||"I""I""||"||""||"'I""|||' -n/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

|||||||||||"||||"||||"l""l""l""l"'||""||"'l""l""l""l""l""l""l""l"'|||"|||||||"|'l""l""l""l' •n/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m/z 4 4.0, 100.00%

2,40 2,60 2,80 3,00

m/z 39..95 11.20%

I ' ' ' M ' ' ' ' I 2,40 2,60 2,80 3,00

n"'" ' I

m/z 45.0 0.97%

2,40 2,60 2.80 3,00

48


"- Tentatively Identified Compound (LSC) summary

._, Operator ID: RUIFENGY Date Acquired: 30 Dec 2001 4:38 am Data File: C:\HPCHEM\1\DATA\I50186.D

- Name: N4945-2 Misc: MS58 673,VI2010,4.5,,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title: SW-846 Method 8260 Library Searched: C:\DATABASE\NBS7 5K.L




G

G

G

G

G

G

G

G

49






C:\HPCHEM\l\METHODS\MI1986, SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Initial Calibration MI1986


M (RTE Integrator)


G

G

G

G

G

G


44) 1,4-difluorobenzene 72) c h l o r o b e r i z e n e - d 5 88) 1,4-dichlorobenzene-d4

System Monitoring Compounds 42) dibromofluoromethane (s) Spiked 'Amount 50.000

43) l,2-dichloroethane-d4 (s) Spiked Amount 50.000

66) toluene-d8 (s) Spiked Amount 50.000


Target Compounds

5 . 8 6 9 . 6 3

1 1 . 6 1 1 7 . 7 3 2 2 . 1 1

65 168 114 117 152

9.90 113

10.85 65

14.75 98

19.99 174

60093 352335 308780 241542 136545


0.00 -0.04 -0.05 -0.04 -0.03

239733 47.71 PPb -0.02 Recovery = 95.42%

182415 49.64 PPb -0.03 Recovery = 99.28%

277459 49.58 PPb -0.03 Recovery ' = 99.16%

159115 55.34 PPb -0.03 Recovery = 110.68%

Qvalue

^

1


50

Quantitation Report


Vial: 14 Operator: RUIFENGY Inst- : MSI Multiplr: 56.00




Abundance

210000

200000•

190000

180000

170000-

160000-

150000

140000

130000

120000

110000

100000

90000

80000

70000

60000

50000 -

40000-

30000

20000

10000

0 X

 2,00 4,00 6,00 8,00 10,00 12,00 14,00 16,00 18,00 20,00 22.00 24,00 26.00 28,00

150187.D MI1986.M Mon Jan 07 12:51:07 2002 GCMSI Page



D C:\HPCHEM\1\DATA\I50187 30 Dec 2001 5:17 am N4945-3 MS58 673,VI2 010,4.6, ,100,5, 1


14 • RUIFENGY MSI 56.00



C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 ON Filtering: 5 1 0.1 0.05

Min Area: 1000 Area counts Max Peaks: 100

Peak Location: TOP


Signal TIC

pea ' #

1 - 2

3 4

- 5

6 -: 7

8 9

„ 10

- 11 _. 12 ' 13 - 14 15

- 16 , 17

- 18 _, 19 20

21 22

- 23 24

' 25

26 27 : 28

k R.T. min

2.724

3.619 3.763 5.317 5.410

5.596 5.866 6.196 9.625 9.887

10.386 10.850 11.129 11.213 11.264

11.627 14.753 15.040 15.277 15.319

17.726, 18.132 18.385 18.419 19.982

20.911 21.004 21.097

first scan

125 244 263 443 458

478 492 552 939 978

1043 1083 1137 1144 1151

1175 1548 1599

' 1627 1633

1904 1965 1992 2000 2172

2294 2305 2311

max scan

143 249 266 450 461

483 515 554 960 991

1050 1105 1138 1148 1154

1197 1567 1601 1629 1634

1919 1967 1997 2001 2186

2296 2307 2318

last scan

171 256 274 452 465

487 552 560 978

1036

1054 1137 1144 1151 1160

1244 1599 1611 1633 1641

1960 1970 1999 2009 2221

2301 2311 2322

PK TY

rBV2 rBV2 rVB rBV rVB

rVB rBV4 rVB2 rBV rVB3

rVB3 rBV2 rVV rVV rVB

rBV2 rBV4 rVB2 rVB2 rBB

rBV2 rVB2 rBB rBV rBV2

rBV3 rVV2 rVB4

peak height

17353 650 566 848 741

579 7851 674

126105 101746

722 55800 1588 763 514

104183 105971

1234 640 629

133586 923 537 521

178394

610 608 854

peak area

169140 2082 1276 2319 1035

1110 109659 1538

1104523 889237

2679 431616

3146 1823 1313

851984 816307 3274 1207 1193

870056 1314 1053 1157

1043008

1484 1227 2678

peak % max.

15 0 0 0 0

0 9 0

100 80

0 39 0 0 0

77 73 0 0 0

78 0 0 0 94

0 0 0

31% 19% 12% 21% 09%

10% 93% 14% 00% 51%

24% 08% 28% 17% 12%

14% 91% 30% 11% 11%

77% 12% 10% 10% 43%

13% 11% 24%

% of total

2 0 0 0 0

0 1 0 15 12

0 5 0 0 0

11 11 0 0 0

12 0 0 0

14

0 0 0

333% 029% 018% 032% 014%

015% 513% 021% 237% 267%

037% 954% 043% 025% 018%

753% 261% 045% 017% 016%

003% 018% 015% 016% 388%

020% 017% 037%

52

29 22.102 2423 2437 2484 rBV2 159085 909393 82.33% 12.545% 30 22.507 2484 2485 2495 rVB3 798 2842 0.26% 0.039%

31 22.693 2506 2507 2511 rBV 748 1104 0.10% 0.015% 32 22.744 2511 2513 2517 rVV3 791 1681 0.15% 0.023% 33 22.786 2517 2518 2524 rVB3 1095 1709 0.15% 0.024% 34 23.023 2543 2546 2550 rVB2 574 1238 0.11% 0.017% 35 23.099 2550 2555 2558 rVB2 937 2219 0.20% 0;031%

36 23.175 2558 2564 2565 rBV3 669 1431 0.13% 0.020% 37 23.200 2565 2567 2573 rVB3 586 1393 0.13% 0.019% 38 23.454 2594 2597 2600 rVB 561 1015 0.09% 0.014% 39 23.665 2619 2622 2627 rBV2 619 1611 0.15% 0.022% 40 23.918 2648 2652 2656 rBV 636 1672 0.15% 0.023%

41 24.020 2659 2664 2667 rBB 556 1027 0.09% 0.014% 42 24.214 2684 2687 2693 rBB 516 1168 0.11% 0.016% 43 27.812 3110 3113 3118 rVB2 363 1005 0.09% 0.014%

G

G

G

G

G

G

G

L



53



C:\HPCHEM\1\DATA\I50187.D RUIFENGY 30 Dec 2001 5:17 am using AcqMethod MI1986 MSI

N4945-3 MS58 673,VI2 010,4.6, ,100,5,1 14


50000

rime~> I I I I I I I I I I I I I I I I I I I I I I I I I I I I r - r I I C l I I T T i I I I I I I I I I I I I

2.00 2,50 3,00 3.50 4,00 4,50 5,00 5,50 6,00 6,50 7,00 7.50 I I I I I I ' I I ' I ' I I I I I ' I

8,00 8,50 9,00 9,50 10,00 Abundance

150000-

100000

50000

TIC; 150187,D

17,73

11,63 14,75

10,85

1,39 / \1J1ff l6 •GHte2gE 48,tff lB3ffi ' I I I I ' I I I r r I I ' I 1 1 I T - l I I 1 1 I I I I , I I I I , I I I I I I , I , I I I - I I I p I I I I I I I I I I , I I I I I I I I I I I I I I ' I I I i - T - 1 1 I I I I I I I ,

rime~> 10,50 11,00 11,50 12,00 12,50 13,00 13,50 14,00 14,50 15,00 15,50 16,00 16,50 17,00 17,50 18,00 18,50 19,00 undance

150000-

100000-

50000 -

0-

1£

I I I I I I I

98

L 2QB1D00 1 1 I ' T ' 1 '

TIC; I50187,D

22,10

- ^ V22^SBTOaEffianB.39.QSa.-€iM.21

1 1 1 i T f l 'i 1 1 1 1 1 1 1 I'M 1 r r r i ' i 1 1 1 1 1 I 1—1 TT—i-i i ' i l

y

27,81 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

rime~> 19,50 20,00 20,50 21,00 21,50 22.00 22.50 23,00 23,50 24,00 24.50 25,00 25,50 26,00 26,50 27.00 27,50



!F u.

if


C:\HPCHEM\1\DATA\I50187.D 30 Dec 2001 5:17 am N4945-3 MS58 67 3,VI2010,4.6,,100,5,1





k k - k k k k k k k - k k k k k k k k k - k k k k k k - k - k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k k - k k k k

Peak Number 1 Ethylene oxide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.



9.63

CAS# Qual

1 Ethylene oxide 2 Acetaldehyde 3 Acetaldehyde 4 Carbon dioxide

44 C2H40 44 C2H40 44 C2H40 4 4 C02

000075-21-8 3 000075-07-0 3 000075-07-0 3 000124-38-9 3

|[

[

Abundance

5000

T m T n n j T i n | T i T T n T T T p T T T p i i i | i i i i [ i i i i | i n i | i i n | i i npTTrpTTT[r iT i | ' i ' iT i | i i i r [Mi i j iTTr I I I I I I I 11 [ i n i | i i i i [ i n i | i i M ] i i i i [ i T i

m/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

h/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Scan 143 (2.724 min); 150187,0 (-) 44

40

46


15

26

44

31 42

46

Abundance

5000

#62265; Acetaldehyde 2l9

15

13| 26

44

42

' l " " l " " l " " l " " l " ' " l " ' " l " " l " " l " " l " " l " " l " " l TTT I 11 I I I I I I I I 11 I I I I I I I I I l " " l " " l " " l " " l " l kn/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000

#62264; Acetaldehyde 2|9

26

44

42 31 40,

'||||'|||||||'||'||||||'||||||'|||'|||''||||''||''|'||||||''||||'|||||"|||"||||||'|"|||||||"||""I""|||"I""||"|||||||"| hn/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m/z 44.0 100.00%

I ' I I I r

2.40 2.60 2.80 3,00

m/z 39.,95 29.34%

2,40 2.60 2,80 3,00

m/z 45.0; 2.20%

T^ T" 2.40 2,60 2,80 3,00

m/z 45.75 1.66%

I I I ' I ' ' I ' ' ' ' I ' I ' I I ' I

2,40 2,60 2,80 3,00

150187.D MI1986.M Mon Jan 07 12:51:41 2002 .55

GCMSI Page 1

G Quantitation Report

C:\HPCHEM\1\DATA\I50177.D 29 Dec 2001 10:44 pm MBl MS58 67 0,VT2010,5.0,,100,5,1

MS Integration Params: RTEIN2.P Quant Time: Jan 1 12:40 2002 Qui

(QT Reviewed)


Vial: Operator: Inst : Multiplr:

Its File:


MI1986.RES


C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 Mon Dec 10 16:29:00 2001 Initial Calibration MI1986


G

G

G

G

G

1) Tert Butyl Alcohol-d9 5.85 3) pentafluorobenzene 9.62

44) 1,4-difluorobenzene 11.61 72) chlorobenzene-d5 17.72 88) l,4-dichlorobenzene-d4 22.10


43) l,2-dichloroethane-d4 (s) Spiked Amount 50.000 66) toluene-d8 (s) Spiked Amount 50.000


Target Compounds

65 168 114 117 152

9.88 .113

10.85. 65

14.75 98

19.98 174

%

54499 338587 293567 230033 129029


-0.02 -0.04 -0.05 -0.04 -0.03

232500 48.15 PPb -0.03 Recovery = 96.30%

181710 51.46 PPb -0.03 Recovery = 102.92%

265777 49.96 PPb -0.03 Recovery = 99.92%

148885 54.80 PPb -0.03 Recovery = 109.60%

Qvalue


57

Quantitation Report

Data File : C:\HPCHEM\1\DATA\I50177.D Acq On : 29 Dec 2001 10:44 pm Sample : MBl Misc : MS58670,VI2010,5.0,,100,5,1 MS Integration Params: RTEIN2.. P Quant Time: Jan 1 12:40 2002




C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator] SW-846 Method 8260 Mon Dec 10 16:29:00 2001 I n i t i a l Cal ibrat ion

Abundance 200000

190000-

180000

170000

160000

150000-

140000-

130000

120000

110000

100000-

90000-

80000

70000

60000

'50000-

40000-

30000

20000

10000

0 ^ rime~> 2,00

5 5-

i 4,00

i

s §7J

XX Ll

TIC: 150177.D

U J "r

•5

4

w /T'^,^ Y'-r r I 'pr i i" J. 6.00 8,00 10.00 12.00 14.00 16,00 18.00 20,00 22.00 24.00 26.00 28.00

150177.D MI1986.M Mon Jan 07 12:41:48 2002 GCMSI Page 2 58



C:\HPCHEM\1\DATA\I50177.D 29 Dec 2001 10:44 pm MBl MS58 670,VI2010,5.0,,100,5,1




C:\HPCHEM\l\METHODS\MI198 6.M (RTE Integrator) SW-846 Method 8260 ON Filtering: 5 1 Min Area: 1000 Area counts 0.1 Max Peaks: 100 0.05 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak, separation: 5

Signal : TIC

[ pea #

1 • 2

r 4

•- 5

6 L. 7

8 . 9

Lio

rii _.12 13

"14 „15

pl6 17 18 19 20

21 22

•-23 .24 25

26 27

-^28

k R.T. min

2.733 5.834 6.112 9.626 9.880

10.311 10.429 10.843 11.611 11.966

12.220 12.279 14.754 15.261 17.727

19.983 20.456 20.7 60 21.013 22.095

22.500 22.813 22.863 22.956 23.041

23.252 23.446 23.564

first scan

125 490 542 938 978

1040 1050 1089 1178 1234

1263 1271 1545 1626 1903

2169 2240 2276 2303 2423

2483 2518 2526 2532 2546

2572 2588 2607

max scan

144 511 544 960 990

1041 1055 1104 1195 1237

1267 1274 1567 1627 1919

2186 2242 2278 2308 2436

2484 2521 2527 2538 2548

2573 2596 2610

last scan

201 537 554 977

1040

1050 1057 1154 1234 1241

1271 1278 1615 1632 1965

2215 2248 2282 2310 2477

2490 2526 2532 2540 2551

2580 2601 2616

PK TY

rBV2 rBV4 rVB rBV2 rVV2

rVB2 rBV2 rBV2 rBV3 rVB

rVB2 rVB2 rBV3 rVB2 rBV2

rBV2 rVB4 rBV2 rVB3 rBV2

rVB6 rVB3 rVB2 rBV3 rBV2

rVB rVB rVB2

peak height

28543 7329 981

118436 97420

877 629

51945 99294

879

433 511

99874 681

124589

168597 439 641 809

149257

1263 817 698 767 698

840 804 471

peak area

269828 90446 3038

1041747 890235

3045 1334

422628 817170

1447

1039 1026

818391 1407

836158

992077 1005 1032 1678

867831

2420 1823 1208 1572 1051

1602 2180 1195

peak % max.

25.90% 8.68% 0.29%

100.00% 85.46%

0.29% 0.13%

40.57% 78.44% 0.14%

0.10% 0.10%

78.56% 0.14%

80.26%

95.23% 0.10% 0.10% 0.16%

83.31%

0.23% 0.17% 0.12% 0.15% 0.10%

0.15% 0.21% 0.11%

% of total

3.810% 1.277% 0.043%

14.708% 12.569%

0.043% 0.019% 5.967%

11.537% 0.020%

0.015% 0.014%

11.555% 0.020% 11.805%

14.007% 0.014% 0.015% 0.024%

12.253%

0.034% 0.026% 0..017% 0.022% 0.015%

0.023% 0.031% 0.017%

59

G 29 23.801 2634 2638 2639 rBV2 •30 25.896 2883 2886 2895 rBB2

729 412

755 845 842

1176 1220

1192 1790 1850

0.11% 0.12%

0.11% 0.17% 0.18%

0.017% 0.017%

0.017% 0.025% 0.026%

31: 26.200 2918 2922 2924 rBV .32 26.242 2924 2927 2932 rVB '33 27.805 3105 3112 3117 rBB



G

G

G

G

G

G

G

G

G

G

G

G

G 60

LSC Report ^ Integrated Chromatogram

File :.C:\HPCHEM\1\DATA\I50177.D Operator : RUIFENGY Acquired : 29 Dec 2001 10:44 pm using AcqMethod MI1986 Instrument : MSI Sample Name: MBl Misc Info : MS58670,VI2010,5.0,,100,5,1 Vial Number: 4 Quant File :MI1986.RES (RTE Integrator)

Abundance

150000-

100000

50000

p i 1 I I I t I I I | ~ i ' r ' i " i " | I I I I [• I T T I [ r t I I ) " r r I I [ I I I T | - i r i i | i " r t i | i i i r ] r i i i [ i T I I ^[ -

Tlme~> 2.00 2.50 3.00 3.50 4^00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00

TIC; 150177.D

9.63

2.73

t I I p r I I I

Abundance

150000

100000

TIC; 150177.D

50000

17.73

11.61 14.75

15,26 I ' I I ' I ' I ' ' I 1^1 I ' I ' I I I I ' I ' ' I ' ' I I I I ' I ' 1 I" I ' ' | T ^ I I I I I I I I

rime~> 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 Abundance

150000

100000

50000-

1^ TIC: 150177.D

98 22.09

I

I V20.4e0.7g|.01 I I I T T I I I I I I I I I I I

v22j^fflBaa.2aaa3.80 25.9^2}} 27.80 I < y ^ ' I I I I I I I I I 1 I I I I I I I I I I I I I 1 I I I I I I I I n I I I I 1 I I I I I I I I I 1

rime-> 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23:50 24.00 24.50 25.00 25.50 26.00 26.50 27.00 27.50

61 150177.D MI1986.M Mon Jan 07 12:42:41 2002 GCMSI


G

G

G


C:\HPCHEM\1\DATA\I50177.D 29 Dec 2001 10:44 pm MBl MS58 670,VI2010,5.0,,100,5,1



Quant Method Title

C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) SW-846 Method 8260 .

Library : C:\DATABASE\NBS7 5K.L k - k k k k - k k k - k k k k k k - k k - k k k k k k k k k k k k k k - k k k k k k k - k - k k k k k - k k - k - k - k k - k - k k k k k k k r k k k k k - k k - k - k k k k

Peak Number 1 Carbon dioxide

R.T, EstConc Area

Concentration Rank 1

Relative to ISTD R.T,

G

G

G

C

G

G

C

G

G

G

G


Hit# of 5 Tentative ID' MW MolForm CAS# Qual

1 Carbon dioxide 2 Carbon dioxide 3 Acetaldehyde 4 Nitrous Oxide

4 4 C02 4 4 C02 44 C2H40 44 N20

0 0 0 1 2 4 - 3 8 - 9 3 0 0 0 1 2 4 - 3 8 - 9 3 0 0 0 0 7 5 - 0 7 - 0 3 0 1 0 0 2 4 - 9 7 - 2 ' 3

Abundance

5000

i [ n i i | i i i i ] i i i i | i i i i | i i i i [ i i i i [ n i i | i i i i [ M i i | n i t ] i i i i | i n i | i i i i | i i i i | r i i i n i r i i T i T i ] i i i i i n i i [ i i i i i i i i | i i ' M | i i i i | i i M | i M i | n i r

fn/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 Abundance

5000-

I ] 11MIMI n 111111111] 1 n 11111111111 ] 111111111 [ 111111111 [ 11M111111 n I n 111 [ 11111 [ n 1111111 [ 111 q i n r ] T r r r ] 11 n ] n ii ] 11 ri ] i ri 111111

l l /z -> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

Scan 144 (2.733 min): I50177.D (-)

44

40

#34: Carbon dioxide

44

16 22 46

Abundance

5000-

#62263: Carbon dioxide

44

12 16 22 46

•|||"i""i""i""l""i""|||||||"||||"|||"||||||||"i""r"'r"||"|||""i""i""i""l""i""i""i""i""r"

m/z-> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

i i i i | i i i i [ i i i i | i M i | i i i i ) i i i i j n i i [ i i i i ) i i i i ] i i i i ) i i i i | n ' i i | i r i i | i i ' i i | i i i i | i i i n i i i i ) i i i n H i i ] i r i i ( i r i i | i i ' i i | i i i i | i i i i [ t t i i | i i i i ] i i i i

hl/z~> 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

m / z 4 4 . 0

I ' ' ' ' I r I ' ' 11 ' ' ' I ' I ' ' 1

2.40 2.60 2.80 3.00

m / z 39 . ,95 13 .54%

I I I 1 t I v ' I I I I I I I T r f [""i I

2.40 2.60 2.80 3.00

m / z 44 .9 ,5 1.50%

I I I I I I I ' ' ' I I I ' • • ' I I " ' I I I I I I I I I

2.40 2.60 2.80 3.00

62 150177.D MI1986.M Mon Jan 07 12:42:46 2002 GCMSI Page 1


Operator ID: RUIFENGY Date Acquired: 29 Dec 2001 10:44 pm Data File: C:\HPCHEM\1\DATA\I50177.D Name: MBl

pMisc: MS58670,VI2010,5.0,,100,5,1 Method: C:\HPCHEM\l\METHODS\MI1986.M (RTE Integrator) Title: SW-846 Method 8260 Library Searched: C:\DATABASE\NBS75K.L



_ 150177.D MI1986.M Mon Jan 07 12:42:46 2002 GCMSI

G

G

G

G

G

63

\>hlo Standard Data


Analyst Signature:.

Standard Data

Batch ID: kx^-^^T yô/u

_ L o t #

- ; •

i -r ^ L

r

Description

- - •

Gone

- - • - - :

- •

— -

Lot# m''tU>'\ tM'WlT-M^4V-^ J g y ^ V i ^ -

hMJ'k^'*'^

Description

' ^ . v r f / ^

L £>

Cone 2r??M / jo^pfl

4L

Columns: Method Sea. File: Initial GaL: Date Archived:

QC Review:_

;?7xe^)-^^ M)^^

/« i . r \ / lH^6

• - • • ' - r . - . - . . . . , - . , .

••!

• ' . '

r.

i '

JUktittttc^ S a i i i ^ I t ) ' Test iMnqvui #

|A£S Samp. Amt ISolid

DU Multiplier t SUtiis (Data)

l ^ ^ ^S^ Cotiiiiieilts M

f-I t o i U ./yyrni-1 a Soo _^!2L ML

to in A / A - m - 1 1 ^ Z * ^ ' ^ ^ t?t/6i>

JIP/^J: /^4^^?- T A m f a II . ^ 1^

3-0//T .r_M. 4-0 /Ml

Li' /He? /] t? :4/^f4/- f iL ^

;H/^ <3?iy-*j f%,e^-„.'

XDi-7) 41 w -:ro/7x j i i 41 i > ^

^ m j ± _ ^ M: S^rf^? . ^ / 7 ^ /?/^n >fi T ^

J olA.

.â^ cc^ 1.9fy~.H y L . idi-ônC J^L. ft W i^^n

>-ffl( f-.? Vv/ _&£_

.<T)/7^ ^ 4 ^ ^ ^ ' ? ^ ^ V/J ^ C

^<D n ' j HA ? % ± raVH' , \ - t l 4-y/r r ^ 12 V 07c

C^PI^P M U f ] 

Jo^ll_ y f ^ ^ r - I IJ. ^Vs- s4. Uc vr < ? l ^

^ 4 ? 4 r - 7 T ' /r. 1U^ .J-/.4 yy e vib(3?7. r - I V

t - i U ^ ^ t ^

i r r X = Ma(rix

hl4.^cy- .2ff

1-i/sr iM sL^ J.

f.r ' V a"/-.; /^.2 V M^ & ^

Ti <r,C-j ~~rni Pmro iC '"Y, *r P -l - ^ ^ 1 &^

C" ' " . . . . : ; . " -n»J»ate W for water, S for soil, O for oiL I/f =Library Search. IS = Internal Sdrndard Area. SO = Sorrogate .

<«'P«'«^ r (P«w«e y5»lum«y(Sampfc Vo. (WT) x (% Solids) nple Amonat=Vot i ia ie (ML) or W d g h t (g)

PBJt 1 6 3 6 4

I nn: OR()01-02 Wv.l^te: 4/19/2001

»ite: It^li-^^ -


Analyst Signature:

Batch I P : 1/Z Vc"/o A / t z t . ; \

m-/. Standard Data Standard Data

L Lot#

L - I ;

'. ^ - ? ;

-:-; •sy- -k

Description

--.=".'....

Cone

..

m-¥i.'i)\

I jo t#

MV-4^ '3^ A1V-4-4-1J **v-<i.4-n^ AV'lH-Ui

Description

.W/M :np t

S^sLA <dpl (\ ^ / • / c

^tln.

Cone

•PTpph i<i^tf<^

lvo-^?m

fyof^l^

Mf^fVl

Columns: /JT/^ fa3 > Method Seq. File: Initial CaL:

^ / ^ O

, 1 2 ^ . < .

y.ii '^H

' -;

Date Archived:

OCReview:

Datafae Sample D) Test Ml vial ALS Samp. It

f l ^ io>4f-

SoGd DU Multiplier' Status'

(Data) Comments hi

y i h > i ? a / i-''Ai'

i l 2 i i u (Tji \ y t >g>p

i p / f / ^ • ^ f i f i - i l i ± 1 . / A . ^ ^ / p j t

J0±H-i^.t.i 2

- 2 H ^

i!dk i £ i 12. ^

Ct J K . . f a i ' f ] i a . J . Q K

W I f f ' M ^ • C ^ o \ L

hifi- f l /^ f^ ' 2 ^2 It h t > i i ^

•t^ i-fi: /< ^ / i i / ^ ^ ^ ^ : ^ - h . v^ _c2c j - v / f ] H .f-2f^ - ^ ^ i ^ 7?.^ a ^ ^v/ ^

i r j LL t i . i J V i ' ^ - t ^Vr m i£^ w dp;

ilEilt hfrîH--^-/^ H- yy/L m ax. J I qc. JTH^xni r/t:c)-/,f.-.l n- ^^/r ^ '.? 14 _£2 fci

rt>-></ ^ t ^ / ^ ->? ^ f ^•'/t- m Iii: / / ( ^

t h i ^ Z ^ Z . -r^^ fl»i"v vîiH

^ ^ \ H n i h i r?/ EIL ffo ?v i ^ V J3C. \ / l J C i I

i-ozo t -SS- fv / ^ o?C

c fT)2^>r H S 2 n - 1 f l t t ' o

id- ' - / r n y ^ y V J er^

j ^ io /C ^ / : t - 3 / ^ - 2 ii ^-'/r 2 i i i w M. in) >t"~l H )- /" - ^

H>ox ' H t ^ n - 4

f o ^ l ^ N r ^ i \ - r

LL i-7. ^ M JdLd. (9^C

if- 6 - } '/r IM 4 t/r- v ^ . . ( ^

I f i i . ^Vr t-T>gf0 Avr /? - f-

M A o ^ V J m^

fT>:?l| /y r / / 7 -t.i ^

i-yî 7 / ' 7 ^ A/V < ^ .

iL ilVii .'..*r. w < ^

t ^27<^

IT'^/S

13/^0 X oiC i h ? X f M

r c ^ y , ? / - h >

}r r X = M a t r i x Dcsigaate W for water , S for soil, O for o i l L+

tiplier == {^wgfi Volumey(Saimple Vo. (WT) x (% Solids) _ pie A m o a a t = V « l u n e (ML) o r Weight ^ )

I m: OROOl-02 iv. Date: 4/I9/2O01

V^ tH* =Library Search. IS = Internal S tandard Area . SU = Surrogate.

165

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