Download - CHEMICAL ANALYSIS REPORT 3x93 Eur,e tso~43 ~- ¢g S °F

n C f, , EAR2s~cy F to

TO : ,

FROM :

CHEMICAL ANALYSIS

REPORT

LOG NO .

S - 7,2 - g,3

, }SEAm 14 U DEP./GROUP S"99 Ss - I /

SSFL ANALYTICAL CHEMISTRY UNIT PHONE 3x93

REFERENCE : ` 4Droa4 /,r3

DATE ,

LOG NO .SAMPLE

IDENTIFICATION RESULTS

E--7.2-83 2t vTE,e/um 73 p M

CrL-3 .

SAv"k4 e Oo5 t' 4

y :;~Euj /do 1•uT JOE rl~er~ ~,vaPZB,~ 1

Eur,e tso~43 ~- ¢g S °F

~P_ECE / v€2 : S~IS'~43

/O/S' Mu -P- $7 o79 "7 tA7rz or--r MU

VA21 DES 4oo pp.~ hL p s y Vccvk" E

A s mi Z

COMMENTS :

APPROVE D

V . rrr 619-V

SSP A,l(ALITICAL CI 11STRY UNI T

BNA0147601 8

H D M S E00624292

ENGINEERING WORK REQUESTTITLE OF JO B

DINSPECTION REQUIRED

' cxJ 'I APPLICABLE DRAWING S

YES NO

GOING DEPT . LECCER ACCOUN T

REQU EESSTED 13Y

LAB SUPERVISION

GENERAL ORDER

(ATTACH I

DATE

REQUIRED ]

G .O ITEM & NCR INIT . GROUP I NOW OR TA 9

EXT . FACILITY SHIFT

ASSIGNED TO :

SHOP I I LAB I

INSTRUCTIONS ( BE SPECIFIC )

Z,

1119

ESTIMATO R

MECHANIC

DOI NC GROUP

No. R5n404 3REQUESTED COMPLETION DATE

ACTUAL COMPLETION DAT E

ESTIMATE

HOURS MATERIAL SREQ UIRED _ REQU IRED,_

NOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

m e I -s T L f

-4-T 1,_2 5.5 (A t_T "r0 LAJ - f T rt 1'/V

J72 /,ti.E l~ 1t2-r i7,~ f

46,4 No, f'- 7 2-eR'

i" , j2~z Dubs 1 a

l ht, -u _ '7 3 p n m

BNA0147601 9

REQ . SUPERVIS I

LEADMAN

LA N

HDMSE00624293

CHEMICAL ANALYSISREPORT

TO : T. /i4

FROM : SSFL ANALYTICAL CHEMISTRY UNIT P4ONE

DATE .

Ss-//

3 ,29 3

LOG NO .SAMPLE


S 7/ 83 iL{EUU•yl/~LE /-~2 4 ' 3 3 ~P v~

LrNE .

S~4mPCE,~ ~Lpi i t

~u1,e ~ ¢ 4 C~Ol~Sy ~Ew /~aivT ~EI JH W4 i 1AJ

-~/5 7 2 PS/(o

7 E -l1TCI,E/-77 J LEAF L OF f/z O

4r ° C 'I) 16-00 PStb t

46ot1T a-a PM RY I/oLUMt.

COMMENTS :

APPROVED

DEPT./GROUP __E1!

rr

6 9 . m mm u imi i iumm i iumiu ui i n i iu


TO : K , W,, 9 N ~e .

FROM : SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE : L 6 S 3 - so

PHONE s_/ It 7

DATE ,

LOG NO .SAMPLE


~- 66- 9 ; kF f kCt ^dJY '~ 33 K F = S. s 9 KCL = 0.5 3 3

k F t jCc An 'y r icf = 2 . L 7 fC ct = 0, oa fy

-k3 t~ F Y K Ct Y rOH tT F = f . 73 ;}C C1 0. 15 2

AAI' '`3S KOH 0 .6 4

- bh-g3 KF -t KCL t ftoN kF = I . 94 2 Kct = 0. 01 3

IV ." ) # 3t fi OF{ = ( .0 s y

S -7,0-f3 KF # KL1 t ti OH Kr = I. l y 7K ct = O, ot o

'r37 KoN = t,~~ 9

141c

5/ ;/s 3

COMMENTS :

APPROVED

~oFLrrno Flfjikau Manager

Corm 6 '9-V SS A4al tcar Chemon

LOG N0 •

,~- l~-Yt.

7o - Z 3

DEPT ./GROUP S 1 2

D4

~ ll~ ll 1~ 1~ III 1~~ ll~ ~11 1~

ENGINEERING WORK REQUESTTITLE OF JOB DATE

A. ,?u ) , I v ,A44Af7uie No. R49080 6INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED) REQUESTED COMPLETION DAT E

YES NO `J1rXIT

GOING DEPT . LEDGER ACCOUNT + CEMERAL ORDER G .O. (TEM 8 NCR INiT. GROUP HOW . OR TA6K DOING GROUP ACTUAL COMPLETION DATE

RESUESTED BY EXT, y^rI~ FAACIILIITY'i SHIFT REQ . SUPERVISIO N

TT

ESTIMATOR ESTIMATE

HOURS -MATERIAL 6REQUIRED REQU IRE D

SUPERVISIONASSIGNED TO :

LEADM MECHANI C

SHOP LA S

INSTRUCTIONS IBE SPECIFIC) NOTE: THIS FORM WILL BE USED FOR NON- DELIVERABLE ARTICLES ONLY .

~< .r0 tiroC. o/ dELiLI ~2UtiL /A-- G' ce -re-X' 7 o c I'de-;*' 44x?

A.~- : c --ic4' A 444? C O

/2) r// y w7Z/7 ate' ,e+~.r Ts

2jo 7,

rte i5O /G

I-O'k va - J- V 7/-p3

-F, )YJ I ~~ ,~~c E ` 335 Rpm 1-1,6 (- "g 2),

f,r/22ff

c=v c r 4 . .-_ C- MATER G c

BNA0147602 2

H D M S E00624296

TO: ,

FROM:

X . Nogg


DEPT./GROUP 564

SSTL ANALYTICAL C t 1ISTRY UNI T

2 UREFERENCE : Logbook ' S3 D .

LOSNO •

5.5',-83PHONE - 5447

DATE S /S 3

LOG NO .SAMPLE


5-5~-83 Wastewater, Canoga Copper - o, 9 0 mg/L

Site C, "Sea World " Nickel - 2 1, (p mg/L

Pa24 hr . Proportiona lSr -rlp tr 'K e"

S/q/83-5/5/830?3o

le received s sIB3

DSy ~

r

alyzed for copper, pEnd nicke l

COMMENTS : The L.A . City discharge limit for copper is 15 dig/I, for nickel the li.dt is

12 Mg/ I .Analyses per N . Mogg',f IL 81 1L-22 , 27 Oct . 1981

R .D. • lone deteete

APPROVEDSSFL ANALYTICAL Oi 1STtT UNIT

VBNA0147602 3

HDMSE00624297


to: II mama DllT./e IJF 5rvt

UTL AMLTT ICI L CKWISTIT UNI T

RE ,gRMNIX; Logbook '83 Pg . OU

LOS NO .

5-55-83

rFlONE 5447

DATE

i

LOS NO. IDENTIFICATION RESULTS

-55-5 Wastewater, Canoga Chromium 0 . ~ (p Mac /i

Site B , D/544 Process pH ! .Clari fie r

24 ar . Proportions l

sample

5/41B 3? 5/5/83O73 0

Sample received S'S 1

Analyzed for pH, an d

chromiu m

C:O ANW-NTS ; The L .A . city discharge lid/ for chromium is 10 mg/L

Analyses per Y . Kogg 's IL A1 PE-422, 27 Oct . 1981

V a►en $1e-V

JSUL A ALYTICAL Ot I3TIT IT

BNA01476024

HDMSE00624298

M. xogg

FROM :

CHEMICAL ANALYSIS

REPORT

DEPT./GROUP 564

SSFL ANALYTICAL CHEMISTRY UNIT

REFERENCE : Logbook 'Rpg• PO

LOG NO .

6-52-83

PHONE 5U ►7

DATE , y) 8

LOG NO .SAMPLE


5 -83 Wastewater, Canoga

Site L, D/5hh Scrubber Chromium - 5 2 rv (L

Sump PH ' -7 . 0Grab Sample taken

51 y 183 3

I Samle Received SA//$31130

Analysed for pH, an d

chromium

COMMENTS: The limit for Site L is 75 m]l .

APPROVED

form 619-V

SSFL ANALYTICAL CHBUSTRY UNIT

LOONO •

TO : M . Mogg

FROM


DEPT./9ROUP 64

SSFL ANALYTICAL QL ISTRY UNI T

REFERENCE : Logbook ' pt. eQ

S 51-83

PHONE 5"Z

DATE

LOG NO .SAMPLE


5j"'5 1 '8 xastevater, Canoga Copper • p, 5 L. mg/L

Site C, "Sea World " Nickel - IS . -7 mg/L

PE • ~~~24 hr . Prooortlona l~Sr-~L+1e taken

5/3/83-iP 5/' /s3

le received $~S~J

Analyzed for copper, pEnd nickel

i ■COMMENTS: The L.A. City discharge limit for copper is 15 mg/l, for nickel the limit

12 mg/ 1 .Analyses per M. Mogg 's 4 81 FT-422, 27 Oct . 1981

A.D. • done detected

APPROVEDSSFL AIIALYTII L QiSi1I41191 UKI?

BNA0147602 6

HDMSE00624300


LOG No .

5 -50-53TV M . worr OPT./OAOitijw S&4

p UYL ANALYTI CA L Ot i1STt? UNIT

Logbook 3 pg . '7 8

p9ONE 5447

DATE

LOG NO.$AMpti

IDENTIFICATION RE$ULT$

5- 5D-83,Wastewater, Canoga Chromium = N .D. <a .Q 5 nag /L

7Site B, D/544 Process . 1p8 =

Clarifier

24 hr . Proportional

sample

513183>51y~

Sample received S/Li 1

1130Analyzed for pH, andchrosl um

COr1ttOM NTS : The L .A . cit y discharge limit for chromium is 10 ag/L

Analyses per W . >iogg's IL ,11 FE-422, 27 Oct . 1981

APP OVER

V .srw+ $19-V

UFL AIMLYTIC& L QM [ISM OIIT

EEBNA0147602 7

HDMSE00624301

LOG NO .

CHEMICAL ANALYSIS

REPORT

Q UA LITY ASSURANCE

FROM : $SFL ANALYTICAL G®[ISTRY

REFERENCE:

DEPT. /GROUP

5-49,83

PHONE 5447

DATE

SAMPLELOG NO . IDENTIFICATION RESULTS

s_-$3 GAS . Cs NZREC'D : -5 / A / 83

SAMPLER : FL(

)OS2) 1PRESSURE 1q as W. P <. I (pp■ ) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED

SPECIAL : HYDROCARBONS

AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR ` TRACE ND = NONE DETECTED < = LESS THAN

ALFA BRAVO>J = GREATER THAN DNA = DOES MCI APPLY

COCA DELTA

CTL-3 C'TL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

OTHER : c'yp-

COMMENTS : *Kaximun ally.able limit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or 02 .

APPROVED

LOGBOOK PAGE

SSFL ANALYTICAL C1iEfIISTRY UNI T

Form 614-v

BNA0147602 8

D/556

HDMSE00624302

LOG NO .

CHEMICAL ANALYSIS

REPORT

QUALITY ASSURANCE DEPT./GROUP D/556

FROM : SSFL ANALYTICAL CHEMISTRY

REFERENCE : LOGBOOK (13 PAGE - C7

5 -yw? - 83

PHONE 544 7

DATE , 5 /9 lg 3


5-Lfl43 GAS : OL-L )'__

RECD : 5/L/ /83

SAMPLER : FGO (p32, o

PRESSURE lot 00 (1 , 0 . < (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED

COMPLETE

SPECIAL

: ,

14-C. GO

U fPE

4

FROM -

SSFL SUPPLY LINETR = TRACE ND = NONE DETECTED < = LESS THA N

ALFA BRAVO> = GREATER THAN DNA = DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

OTHER : SS P- Arl1

COMMENTS :

APPROVED /7/• SL - ~~sei 14j J

MA NAG SSFL OZAIVTTt'A1 . r4%'%4TSTRV ! TT

I IBNA0147602 9

HDMSE00624303

CHEMICAL ANALYSIS

REPORT

TO : G . BAUE R L E

FROM :SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE Loq~ook s3 PQ~ e 79

PHONE 514 7

DATE `'MAY- 83

LOG NO .SAMPLE


KINNEY A0/L 5A MPILES

FROM C w L L

5-9z-83 POST TEST-~. 5 9~ ; Y lo~~h e

q/3 083 3

5-43-33 POST r.E' ST z. 8 ~~I +~ l oGintS/i/ 83.

5-44-$3 / ST 71St g.5 9~),-}er ~oa~in t

3

5 /4 1P3

COMMENTS :

APPROVED ,

f arm 619-V

LOG NO .

5 - 4 2 -83To

5-44-83

DEPT./ GROUP 52 2 SS /

SSFL ANA IGL STRY UNIT


TO: M . Mogg

PRO" SSFL AMALYTIGL Oi ISTRY UNIT

REFERENCE : Logbook ' a3 DR. 7S

LOG NO .

5-41-83

PHONE 54h7

DATE

LOG NO.SAMPLE


Wastewater, Canoga Onnpper - 0 . 52. mg/L

Site C, "Sea World " Nickel - 16 .2 mg/L

P,-r- ti 7J.Z8

URAe, 5/3)93

.

sr-rle tPken (9 )315

ample received SI C

082.5Analyzed for copper, pa

nd nicke l

COMMENTS : The L.A . City discharge limit for copper is 15 mg/1, for nickel the licit i s

12 mu 1 .Analyses per M . Mogg 's ;K 81 ?E-, 27 Oct . 1981

T .D. • None detected

APPROVEDSSYL ANALYTICAL CWSTRY QIi

uiumuiuu i iBNA0147603 1

DEPT/61110UP 64

HDMSE00624305

LOG N O


TO. M . Nogg DEPT./GROUP 56k

FROM : , SSTL ANALYTICAL QLDIISTRY UNI T

REFERENCE.' Logbook ' SS DR,--7S

5-140 ,-83

PHONE h7

DATE 5,~L1 ~-' Z

LOG NO -SAMPLE


5-`'0$3 Wastewater , Canoga Copper - 0.53 ag/L

Site C, "Sea World" Rickel - 18 .9 mg/L

P'T #' 0E 8GRAB 53/83 .PSP-510 token ED 1 315

le received S/~-!

4QZ.5

przed for copper, pZ

nd nickel

COMMENTS : The L.A . City discharge limit for copper is 15 mg /l, for nickel the Bait is

1.2 n/ 1 .Analyses per M . Mogg • s IL 81 l2-J22, 2T Oct . 1981I.D. - lone detected /

APPROVED ySSFL ANALYTICAL CL{ 1 STRY UNI T

BNA0147603 2

HDMSE00624306

CHEMICAL ANALYSIS

REPORT

C . "e, cp.Q ,T DEPT/GROUP S~ b

fvorF&oo,ot' 0,330 , a. 46 -4-7

LOG NO .

PHONE 3 _ _

DATE , S 9 ~3

LOG NO .SAMPLE

IDENTIFICATION RESULTS IAJ EI(o /}7"

S- 3y-S3 meAZ,uE

9qg, ypAgk,NE

a t, W o -Z pb % c~ArE.eA u,t /,,if, 1,41-YS,S ,

~, r2 ,Ia 0 r3KA 906",&e /~✓d,E ~D7ES

c e co o/ -7 '

1, 64r0,,l r 8Y Tic E?•4cw 6 o 14J 3~1 /973

SSFL ANArY ICAL CKW.ISTRY UNIT

cc ; R . Yeaman, B . Beardsle y


TO:.

L . Forman

FROM : SSFL ANALYTICA L CHEMISTRY UNI T

REFERENCE : Notebook 0330, p . 44-45

DEPT./GROUP 631 SS 11

PHONE 3293

DATE 5/5/8 3

LOG NO .SAMPLE


Freon 14 samples fromCTL - III .

(% by volume)

Nitrogen Oxygen Wate r5-37-83 K bottle sample 0.17 0.36 5 ppm

FL 005927

650 psig

5-38-83 Run manifold sample 0.28 0.26 16 ppmFL 01954 1

500 psig

Nitrogen and oxygen were determined by ga schromatography using a Chromosorb 102 (80/100

Received : 5/3/83 mesh) column . The water values were obtained

by dew point determination .

Infrared spectra in the 3 to 4 micron rang eare attached . Complete spectra are available

for examination upon request .

COMMENTS :

APPROVED

c rm619-V

SSFL NALYTICA L CHSi1STBY UN I T

BNA01476034

HDMSE00624308

SPECTRUM NO .

DATE '~ /3z

SAMPL E

SOURCE

STRUCTURE

PATH /'"mm

cE&4SOLVENT

CONC.

PHASE _ G

COMMENTS 5y6l'g c

ANALYST

SPEED 3 -cm-1/min .

GAIN _----_-~~_D

PERIOD SEC .

S F WIDTH ___ m m

--%?cs O_ cm

GRAPHIC CONTROLS CORP .el rrn-r -)nr.$ I ll~ Tr'1h ACT-r

3

7o

O0 3200

4 WWAVELE.,JG PIf,/3 . 5

--I

3000 2803 2600

i

2400

uiumuuui i iBNA0147603 5

4

HDMSE00624309

SPECTRUM NO .

I DATE,'

1 3SAMPLE 5-' - 7

AEtc, A-) /¢ -

1 SOURCE

STRUCTURE

J

PATH r,45 m m

CEOSOLVEN T

CONC . _ -Vo_. tit

i .,AS E

COMMENTS ___.---_.--

6or7 iP

SPEED cm-1/min .

GAIN A U

PERIOD __I SEC.

S WIDTH mm

cu --3p 0 a cm- ,SPE&b s v,4 . = 2

3RAPHVC CONTROLS CORP .1PECTROPHOTOMETFR

U✓AVELEA47V l''I3 .5

i

4

3200 1000 2800 2600 2400

WAIlt4OW6771 1"k-13 .5 4

SPECTRUM NO

. DATE

SAMPLE 7

SOURC E

STRUCTUR E

PATH 104 m m

~''8?SOLVENT -

CONC .

F,,ASE

COMMENTS

/< &77z4

T-

>ANALYST

-F

SPEED J C_ cm-' / min .

GAIN I. FDERIOD -- -16-- SEC.

3 WIDTH '' 3 ,-_ m m

--

GRAPHIC CONTROLS CORP . 00 3200 3000Cv+~ ' IPR' r~ T M n0H ,lTnn.AFT7 a

IDID DBNA0147603 7

cm-1U a p

2300 2600 2400

flFHDMSE00624311

W,4 Vi c 3/5 ,AA- 1-14

T

-PECTRUM NO .

r

DATE 3-/3!f-3

SAMPLE S-fig 4-3

SOURCE

STRUCTURE

PATH ~rfmm_

ka r has Ct tSOLVEN T

CONC . /©v_

PHASE ------- ~ _. _ _- _

COMMENTS

YS TEPM two 41

ANALYS T

SPEED 300 cm-1/min .

GAIN ~~ - -

PERIOD SEC .

SL I T WIDTH mm

- 08 cm-' -- 1S "QEE j

CPAPH ;C CONTROLS CORP . )0

I IBNA0147603 8

HDMSE00624312

cc : R . Schmued

M . Francis 1)/564, PB 66

r . Mogg

CHEMICALANALYSI SREPORT

,u . PLJT SERVICES

FROM: SSFL ANALYTIGL C~f1STRY

REFER FI~IC lOG a 03 PAGE 73

DEPT./GROt1 P : D/031

LOG N O

5'- 33-?3

PHONE 544 7

DATE '?-MAY-&3

LOG NO.8I1N1P1 E

I aENTlfICATIO N © P08LB E TRAP © GC/!4S RffiULTS (PI )

Water aanple from the Using the concentration techniques and methods ap -Q

S -3 3 - 0)pd

S Pproved ~mder the guidelines stated in the curren t

epond a t, SS! L lNPDLS p rm t , the f of lowing VOLAT I LB ORGANI CGnt'IO0were f o~md :

Rock. t dyneAcetone (3C3) = 0 . O S

Freeboard = -0 it Bramodichloromethane (BrC8Cl2) _ <,Oo(

35 Carbon Tetrachloride (Cd11 ) _ NQ~,DO (sampled e 8 AH

00 1Chl f 0C C

S 3 83,oro orm ( .H 13 ) =

LW P'Methylene Chloride (c C12) _ ,VO~C,OD /

By : $.1,1,l-Trichloroethane (cH3CCl3 ) = 00 /

REC$IVffi3 Q IA

BB

: Trichloroethylene (C1 ( H :CCl2) _ .0 0

S / 3 / 1)3 Tetrachloroethylene (C12C :CC12 ) : /VD, Do (

1,2-Di chloroethylene (ClCS :CSC1 ) _Notation about appear-ance of the aample : Dibromochloromethane (C1CHBr2 ) _ /JD DOj

Isoprvpyl Alcohol ; also (CRSC80RCB3) _ /2~ (,0 1known as IPA ; 2-propanol

Preon TP (C12FCCF2C1 ) = D ~•oo /

1,1-Dichloroethane (C123) //O~, Doi

CObk1tHNTS : Tetrachloroethylene is also known ■ s perchloroethylene . ( 1) Monitoring specifi-cally required according to the Rocketdyne NPDBS permit, Order a 76-146, NP t)ES I CA0001309from the California Regional Water Quality Control Board, Los Angeles Region .(2) This supplementary information is provided in accordance with 40 CFR 122 .60.

P'A[ = PARTS PER MILLION

s LESS TEAN ND = !INE DETECTED / D4(A = DOffi NOT APPLY

APPROVE D

~rrn 6 1 9-V

TR = TRACE

SSFL AKAL IGL C~IISTRY UNI T

II0I m u imi i iumm i im iBNAOI 476039

I IHDMSE00624313

ENGINEE R ING WORK REQUESTTITLE OF JOB

J 11IF REWINGS IATTACH

INSPECTION REQ UfREDAPPLICABLE A

YES NO

DOING DEPT LEDGER ACCOUNT GENERAL ORDER G .O ITEM & MCR

UI RED)Q

DAT E

INIT . GROUP HOW OR TAS K

121 / U I(a // ~/ v' / cREQUESTED BY EXT . FACILITY I SHIFT REQ SUPERVISION ESTIMATO R

^r~1ti _LAB SUPERVISION

( ASSIGNED TO :

SHOP11 LAB j

INSTRUCTIONS BE SPECIFIC)

MECHANIC

DOING GROUP

No. 850017 8REQUESTED COMPLETION DAT E

ACT AL COMPLETION DAT E

ESTIMATE

HOURS MATERIALSREQUIRED REQUIRED

NOTE : THIS FORM WILL BE USED FOR NON- DELIVERABLE ARTICLES ONLY .

SuT-104-1A

No A/ 'y s-

LIST OF MATERIAL S1ORM R 94 .L REV 6 .57

ui uBNA0147604 0

--ADMAN

HDMSE00624314

CHEMICAL ANALYSIS

REPORT

D£PT.jGROUP 5

LOG N O

5'3D-.33

PHONE 5 14 47

DATE . 5I3)g 3

LOG NOSAMPLE


Wasteveter , Canoga

Site L, D/511J+ Scrubber chromium - fY'S /C.

Sup pH -a S

Grab Saaple taken

~3/g3@O O

Sa,irp1e S,ived 5J3,8 3

Analysed for pH, an dchromium

SSFL ANALYTICAL CHEMISTRY UNI T

IIDI m u imi i iumm i im i uiu U

X . Mogg

FROM :


DEPT./GROUP ~~55$

SSFL ANALYTICAL Q3E>r{ISTRY UNI T

REFERENCE : Logbook ' 03 DR .

LOG N O

5-29 .83

PHONE

DATE

~hb7

5/3 /a

LOG NO .SAMPLE

IDENTIFICATION RESULT S

S "G ► -S Wasteweter, Canoga Capper ' 0.22 mg/L

Site C, "Sea Hor1d" Rickel - 2 3 mg/L

~ O2L hr . Pronort,ional 'Sp-,le taken

qz /s3 -, 5 /3fi3

'.e received

uialyted for copper, pE

nd nicke l

.OMMENTS : The L.A . City discharge limit for copper is 15 mg ,'l, for nickel the 1t t i s

12 mg/1.Analyses per X . Mogg'e

M . D. - None detected

APPROVEDSSFL ANALYTICAL C tOtIS'TQY MI T

II0I m u imi i iumm i im i uiu 010 0BNA0147604 2

81 l!-422, 27 Oct . 1981

UHDMSE00624316

TO; M _ MoQe

r> o


DElp ' r j ePlou P 51%4

8STL AMLYTICAL O(I3TRY WI!?

REFERtNCE : Logbook ' 3 pg. 7 e

LOG PO .

5.28 -8a

P,lcNE 5447

DATE Sl3f__3

LOG NO

..

SAMPLEIOENTIfIGATION RESULT$

5~28-03 Wasterater , Canoga Chromium = 0 . 20 ✓ / .

Site H, D/544 Process p8 = 7

Clarifier

24 hr . Proportiona lsampl e

57W83 -~ 5/3/g;

Sample received S/3 /S3D8Analyzed for pH, an d

chromium

COMMENTS : The L .A . city discharge limit for chromium is 10 mg/LAnalyses per Y . Mogg ' s IL 81 FE-422, 27 Oct . 1981

APPRCVEp ____ ,_

r ,rm s t 9-V

5911 . AMLYrICAL QIDLIST1Y IT

II0I m u imi i iumm i im i ui uBNA0147604 3

HDMSE00624317

LOG N O

CHEMICAL ANALYSIS

REPORT

TO: LORIN BLEWETT

FROMSSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE :,LOGBOOK ' 83 ; page 78

PHONE 2095

DATE6 May 198 3

SAMPLELOG NO . IDENTIFICATION RESULT SGAS CHROMATOGRAPHIC R

SAMPLES FROM BAGGE DPOWERHEAD EXPERIMENT H2 02 Ar Helium H2OAT A-3 ppm ppm ppm ppm ppm

5-22-83 Cylinder #1 76 3400 58 61 75 0

5-23-83 Cylinder #2 4340 773 TrG 50 ND< 5 92 0

5-24-83 *Cylinder #3 EMPTY CYLINDER D UE TO ELECTRICAL SWIT CH AT A- 3

5-25-83 *Cylinder #4 EMPTY (CYLINDER DUE TO ELECTRICAL SWIT CH AT A 3

5-26-83 Cylinder #5 ND < 5 210,000 9100 ND < 5 * *

5-27-83 Cylinder #6 ND<5 3700 59 ND<5 45 0

The moisture analyses were performed by convertingthe moisture to acetylene by passing the va por

cc .Burr, M . D/584-155 AC58

through a calcium carbide packed tube, then to

Fox, U . D/584-155 AC58 the gas chromatograph . t

Grugoire, V . D/584-155 AC58 DETECTION LIMITS :

Hiroyasu, M . D/598-345 SS11 H2 - < 5ppm

LaRose, R . 0/584-154 SS 11 02 - .{ 200ppm

Monaghan, J . 0/598-345 SS11 Ar - .C 50ppmHelium - < 5ppm

H2O - < 5ppm

THE SAMPLE MANIFOLD CONTAINING COMMENTS :THE CALIBRATION GAS SAMPLES (#2,#6 )FROM 4/ 30 AND THE RUN SAMPLES 0/584 personnel reported that the oxygen and

FROM 5/2 ARRIVED IN THE LAB hydrogen calibrations were calculated to be

5/3/03• 5700ppm each according to the flow rates used

at A-3 .

COMMENTS :* Sample cylinders were empty .

** Moisture (H20) analysis was not performed on this sample Cylinder #5,This ratio is the compositional distribution for AIR .

APPROVEDNorma Fujikawa, ManagerSSFL Analytical Chemistry 7

,~ cti 1 ' u ySSFL ANALYTICAL CHEMISTRY UNIT

IIOI m u imi i iumm i im i ui uBNA01476044

5 - 22 - 83thru

5 - 27 - 83

DEPT./GROUP 584-155 AC58

HDMSE00624318

ENGINEERING WORK REQUESTTITLE OF C $

INSPECTION REQUIREDAPPLICABLE DRAWINGS (ATTACH IF REQ RED ,

YE S I I NO >( 1

DOING DEPT . I LEDGER ACCOUNT GENERAL ORDER G .O . ITEM B MGR INIT GROUP OR TASK

f310N ESTIMATORREQUESTED BY EXT. I FACILITY I SHIFT REQ . 6UPER V

LAB SUPERVISIONASSIGNED TO :

1LEADMAN

SHOP I LAB I

MECHANIC

HOURSREQUIRED

MATERIALSREQUIRE D

0

INSTRUCTIONS (BE SPECIFIC) NOTE: THIS FORM WILL BE USED FOR NON -DELIVERABLE ARTICLES ONLY .

N V 1 o- L o 1 o r - , ~ , -- z I. c t

.'" /S u 5' - C3 I-' 0, " 'L

L. -T

45-z / -g 3

RECEIVED @ LAB

MAY 2 193 3

SSSFL A N ALYTH ,i; CHEIv1i~TRYII :400,U,4- .

5_5 ' ;1 to

LIST OF MATERIAL S

FORM R G4 REV 6 .»

ui uBNA0147604 5

DATE

DOING GROU P

to

REQUESTED COMPLETION DATE

ti


ESTIMAT E

HDMSE00624319

1o x . Moe

!1K'~M=


564

SSIL AM LYTICA L OL61(ISTRT UlITT

NE?ERfT~CE; Logbook ' 33 pg .

LOes N O

5-20-83

PHONE 5447

DATE

LOG NO.SAMPLE

IDENTIFfCATloN RESULTS;

5-2&3Wastewater, Canoga Chromium = 1 .1 /'JL

Site L,, D/544 Process Pg = q, SClarifier

C~ 2A3sample

~. a 73 c)

Sample received

Analyzed for pH, and

chromium

COMME?(TS : The L .A . city discharge 1i .it for chromiu, is 10 mg/LAnalyses per ll . Yogg ' s IL 81 FE-422 , 27 Oct . 1961

APPROVED ✓ • 9!1 P

► ,„~ s i si--vSSTL AIMLYTIGL O;>OLISTRT US IT

IIDI m u imi i iumm i im i ui uBNA0147604 6

HDMSE00624320


TQ M _ o „S Q

!!l01rS

LOd HO

C 'T/OA+~Ij 58 t

537E AMLTTICAL o t5riT U1IT

RE !RLNCE Logbook '. pg .

SAMPLILOd 140 • I 0E14TiPICATIOI4

PHONE 5447

DATE S Q -3

RESULTS

"1 1r Wa5teiater, Canoga Chromium - Z 3 / 1 L

Site B, D/544 Process pS 7. 1Clarifier

G R ~. asample T"AKlp4

5/zl3D)30

Sp1. received

Analyzed for p8, andchromiua

COMMENTS: The L .A . city discharge licit for cbroe.ium is 10 mg,'LAnalyses per M . 1[ogg 's IL 81 PE-422, 2? Oct . 198 1

f•a OVtp -= .

its-VarnI

SUI. ANAL 7LCAL CttncI3TI @IIT

IIOI m u imi i iumm i im i ui uBNA01476047

i u I IHDMSE00624321

CHE\IICAL ANALYSIS

R E p()F~rr

TO _Q _ DEPT, CROUP 5~ , u

L N O

FROMSEA "IIS:TY - l~

PHON E

DATE s-/2 /gam,

LOG NO .SAMPLE

+ ~•3 m6iDENTIFI CAT}ON RESULTS -

~r,(D 3

-

'"RICH 3r NVR per

RL10001-F

E ?do . `~C7 ~ ~

BLANK : mg/500 ml

HARDWARE Q ,t~+ mg/500 ml

•EN o / ~ __ti..

BLANK: mg/500 ml

HARDWARE Cl 3 mg/500 ml

EWR No .

BLANK ° m€/500 ml

HARDWARE . mg/500 ml

Recd . _

MANAGERSSF ~ Analytical Chemistry

IIDI m u imi i iumm iiumimm i i I I


A' I/r Dar/ G/li~vr' i//L f 2 erTAD

INSPECTION REQUIRED IAPPLICABLE DRAWINGS (ATTACK IF REQUIRED)

YES NO

DOING DEPT . LEDGER AC OUNT GENERAL ORDER G .O ITEM

M&

lMC RORDER INIT . GROLP HDW . OR TAS K

REQUESTEDa

LAB SUPERVISION

EXT . 11ACILITY 6HIF T

ASSIGNED TO

SHOP I I LAB

INSTRUCTIONS ( BE SPECIFIC)

REQ . SUPERVISION

DOING GRCIU P

ESTIMATO R

LEADMAN MECHANIC

No. R49743 1REQUESTED COMPLETION DAT E


ESTIMATE

HOURS MATERIAL SREQUI RED REQUIRE D


l ! - f'/ ,~ f G 'A Asti ,4" , 4A/,4 / VT5 ~W

c'IA %E /N/l PCo (// 0174 y/) P1 AI /G~~/~~~ kr Sul r~ !7 / 1 A7r~1 -' A . M

f~Il ~ ~H/,~~~f rnJ

rrly U,y' {, 1

14W,44~~45-- [2 - ~, -3

RECEIVED Cal LAB

tIlA V9x3 3N

SSFL tlt'L LYT! .L CHEM ISTRY

/-Z ,"'.. ~-(„-

ui uBNA0147604 9

HDMSE00624323

ENGINEERING WORK REQUESTTITLE OF JOB

AA / /.<7 ` G/✓' C ,PD✓E A41T ~ f 1 ; /SAPPLICABLE DRAWINGS (ATTACH IF REQUIRED )

INSPECTION REQUIRED

YES N O

COING DEPT . LEDGER ACCOUN T

REQUESTED BY

LAB SUPERVISION

GENERAL ORDER O .O . ITEM B NCR INIT . GROUP

DATE

9 .1 7

DW OR T45K DO NI G 6 O l P

EXT . FACILITY SHIFT REQ . SUPERVISIO NI9g9 r/ /

.s~ 0/S

LEADMANASSIGNED TO ,

SHOP I I LAB

INSTRUCTIONS ( BE SPECIFIC )

/2 r,if N X "y

RECEIVED @ LAB

2 19E3

ESTIMATO R

MECHANIC



ESTIMATE

HOURS ! MATERIAL SREQUI RED _ i REQUIRED_

NOTE : THIS FORM WILL BE USED FOR NON DELIVERABLE ARTICLES ONLY .

,14' *0' AA44/ ys,TS Gi✓ 7? Z(// /< .l/

77/ (ii ~17,31 fl .1)3 r ,-

If

5- / (4O- 3

SSFL ANALYYII III AL CHtMIISTRY

MA-ER L _

BNA0147605 0

K/ /(i22//t <y/

HDMSE00624324

LOG NO .

TO:

FROM


R . Yeaman


REFERENCE : Ntbk . 0330, p . 88

DEPT./GOUP598

PHONE

DATE

5-1-83

ss 11

3293

6/28/83

LOG NO .SAMPLE


5-1-83 Unknown liquid from The sample consists of a clear , brown-colored

CTL-III . liquid with a small amount of fine particulat e

matter present . The sample is not flammable and8WR # 490698 not rater soluble . The infrared spectrum wa s

very similar to that of l,l , l-trichloroetbane ,with evidence of a small amount of rater present .

Based on the above information, the sample i s

probably 1,1,l-trichloroetbane (trick) With aReceived : 5/2/83 small amount of water present .

COMMENTS :

APPROVED

Jrr. 619-Y

IIOI m u imi i iumm i im iBNA01476051

UHDMSE00624325

iuu uuuiuiiuui mu mi uiuuuuiuu i iBNA0147605 2

HDMSE00624326

I APPLICABLE DRAWINGS (ATTACH IF REQUI RED 7INSPECTION REQUIRED

YES N O

~ DOING DEPT . LLU-R ACCOUN T

I REQUESTED By,

L/XB SUPERVISION

GENERAL ORDER G .O . ITEM R MC R

EXT . I FACILITY SHIFT

INIT . GRO U

REQ . SUPERVISIO N

ASSIGNED TO: LEADMAN

I

SHOP LA B


DATE

No . R50390 0REQUESTED COMPLETION DATE

Lf l-4 k_-DW OR TASK I DOING GRO U

ESTIMATOR

MECHANIC


ESTIMATE

HOURS MATERIALSREQUIRED REQUIRE D

NOTES THIS FORM WILL BE USED FOR NON DELIVERABLE ARTICLES ONLY .

No c

r ~.. 3 )3S 7S

RECEIVED @ LA B

SSFL ANALY1 cAL CHEMISTRYBY ~_

C MATER!

uiuuumui i iBNA0147605 3

U °

HDMSE00624327

cc : H . Francis, D/564, FB6 6

CHEMICAL ANALYSI S

S, Fr scf+E,R REPORT

TO: Paul Wolf DEPT/GROUP

FROM : SSFL ANALYTICAL Ct1MISTRY UNI T

REFERENCE

LOGNOj

4-183-83

Notebook. 0330, aaqe7 7

SAMPLEIDENTIFICATION

Unknown liould for

identification .From corroding

dru m

Receive :4/13/8 3

COMMENTS :

APPROVE D

► _- rr 6`9-V

SSFL 'AN LY T ICAL C;<iE3L3 STRY UNI T

BNA01476054

031, SSI 2

PHONE 329 3

DATE June 7, 198 3

RESULTS

The sample consists of a clear, color+

less liquid with some fine brown particulate

mater present . The sample is not flammable

and has a pH of about 4 . Emission spectro-

photometry revealed 310 ppm iron S 21ppmmanganese . Anion analyses showed no sign-ificant levels of sulfate, chloride or

fluoride . The infrared spectrum matched

that of water .

Based on the above information, thesample is probably water with rust presen t

CUU-CIL-111

HDMSE00624328

f FRANCi s D/561, FB 66

TO : P. WO L F

FROM :

CHEMICAL ANALYSIS

REPORT

LOG NO

4-183-83

DEPT. /GROUP 031 S S l 2


REFERENCE LO~Bo0K $3 FAoE 66

PHONE _ 7

DATE~5 -AffZ- 8 3

LOG NO .SAMPLE


4-183-83 WATER SAn1'L ErROM coRRODIaJ v

DRUM

S ~ ) -Fa e ND ' /D ' /

/3 Se ND '

C /o r" cIe TR /"/L

For,M S ~vow ►-. ~V CI f

made ba S I c l prvba6/y (o~+QJn S /Yre + '

c~ ~ 5 / i'Un } .S u

1CD ►'ITQ I n S Qr~ov~ a . o 1 e u i VQ Ie~4S

of acld p-v ' I i +er ir ~ . cc I ng only r

a s ) igh+ 'Y •

fQEC ID

/1-APR- 83

COMMENTS : A/D -

APPROVED

Jrrn 61g-V

IIOI iiiuiiuuimmmi i ii 0101 00 I IBNA0147605 5

NOAJ( DE TEC TE.C

7R = iRAc .

L~oC

SSFL A irP• CAL 1 TW UNI T

HDMSE00624329

CHEMICAL ANALYSIS

REPORT

LOG N O

cf-142- 8 3

DEPT /GROUP 7

PHONE c/4/ 7

DAT E

LOG NO .SAMPLE

IDENTIFICATION RESULTS b w~'

c~ -- 1 42 - $3 N10 s A AAp >~e

FK o M 5r1- 1

t .r l( 2'I tS NV K 2 a''`y~~Qe f N70

" f.''- M f N T O

Iq1 = £'.O M •~ /fy o f N To

a o- TAA c -~ G 0.0 !

'•l

q (13 1

.Uf?4'arma fuiik

4u Manage' SSFL ANAL 1CAL CHEa~ISTRY UNI Ti

IIDI iiiuiiuuimmmi muin iiiimiu

cc : M . Francls , t/56', FB6 6

CHEMICAL ANALYSISLOG NO .

FiscHREPORT

S.4-181-8 3

E .E . Shanks DEPT./4ROUP 5 9 8, S S 1 11

SSYL ANA LYf I GA L QiI STRY UNIT PHONE 329 3FRO M

REFERENCE Notebook 0330 . aaee 76 DATE June 7, 198 3


Unknown liquid fo ridentification . The sample consists of a clear, color

less liquid that burns with a blue flame .

The pH of the water soluble sample is 6 .Emission spectrophotometry showed n o

significant amounts of metals present .

4-181-83 Samples 26 Anion analyses revealed 90 ppm sulfate,

IEMR #3 6250 1.0 ppm chloride and 2ppm fluoride . Th e

infrared spectrum matched that of water4 with isopropyl alcohol .

R.eceivec' :4/13/8 3

I

cOMMEMT 5 :

A PPROYE D

. rer 619-V

Based on the above information,thesample is probably water and isopropylalcohol .

IIOI m u imi i iumm i im i IMMID DBNA01476057

I I IHDMSE00624331

cc : M . Francis , D/564, F86 6

T'O

CHEMICAL ANALYSIS. REPOR'T'5

F ~ sc K t.~2E . Shank s

SSFL A1ALYTFCAL Q1Jl 1IST1tY UKI T

REFEftEtrCE

LOG NO .

Notebook 0330, oane7 5


Unknown liquid for

identification .

4-i 80-83! Samp! a t25{1EwR t 34625 0

Rece ye :4/13/83

f

COMMENTS .

APPROVW

F~rm619-V

4-180-8 3

DEPT/$otP 598, SS1 1

LOG N O

PHONE 329 3

DATE June 7, 198 3

RESULTS

The sample consists of a clear, colorless liquid which burns momentarily whensubjected to a flame . The water solublesample has a pH of 8 and emission spectro-photometry revealed 36 ppm calcium . Anionanalyses showed 100 ppm sulfate . Theinfrared spectrum matched that of wate rwith isopropyl alcohol .

Based on the above information, thesample is probably a mixture of water andisopropyl alcohol containing some dissolvesalts .

IIDI m u imi i iumm i im iBNA01476058

UHDMSE00624332

cc : M . Francis , 4/564, FB6 6

CHEMICAL ANALYSIS

S F.t5cl+LE REPORT

4-179-8 3

E . ShanksDEPT/61loup 598, SS1 1

FROM : SSFL AM LYT I CA L CQi041 STRY UN I T

REFERENCE

LOG NO .

4-179- 8

COMMENTS

Notebook 0330 . pa ne 7 4


Unknown liquid for

identification .

Sample ! 24Ew'R 34625 0

Received : 4/13/83

PHON E 329 3

DATE June 7, 198 3

RESULTS

The sample consists of a ciear,ambercolored liquid with some fine brown part-iculates present . The sample was watersoluble with a pH of 5 . Emission spectro-photometry showed the presence of 100 pp m

iron . Anion analyses revealed the presenc eof 50 ppm chloride and 7 ppm fluoride .The sample was not flammable . The infrare dspectrum matched that of water with a smallamount of isopropyl alcohol .

The sample is probably water with

traces of rust, inorganic salts and iso-

propyl alcohol

SSFL I~LYTIOIL ( 1 1STRY 1II(I T

IIOI m u imi i iumm i im i 1 0100 I 0 IBNA01476059

I IHDMSE00624333

cc : M . Francis , P1564, FB6 6

CHEMICAL ANALYSIS

s , Fi sG+c..~R REPORT

RESULTS

Teo : E . Shanks T~ap 598, SS1 1

SSFL A1KALYTI CkL QE~ISTVY UNI T

REFERENCE

LOG N O

4-178-8 3

s

COMME NT S

APPROVED

V .>rrr 619-V

11 .ntebook 0330 . Da ae_7 3


Unknown liquid foridentification .

Sample t 23Eva 134625 0

Received : 4/13/83

LOG N O

4-178-8 3

Pl4ON E 329 3

DATE June 7, 198 3

The sample consists of a clear,colorless liquid which does not burn, Thesample is water soluble and has a neutralpH . Emission spectrophotometry revealed31 ppm calcium, 55 ppm sodium and 17 ppmmagnesium . Anion analyses revealed 300ppm chloride and 100 ppm sulfate . Theinfrared spectrum matched that of waterwith some evidence of isopropyl alcohol .

Based on the above information, thesample is probably water with small amountof some dissolved salts and isoproyl alco h


UHDMSE00624334

H . HO& ' D/5 42 F8 6 6


TO : P L/ 1J T SER V I c ES DEPT./GROUP 03 / _


REFERENCE : L oq ~OOOk S3 Page

LOG NO •

4-/77- 3

PHONE ,3'?7

DATE ___

HF

LOG NO .SAMPLE


9- 7 7-83 Wa-- 3 a ►~-, p/ ND -c Q.co/ pp, -j 7 E

Be 1 Ca yov,

~ / t 383

COMMENTS : PPN1 = Po.~s ~r- i►• i Dion = ~e--

jV d = N~wc DE 7s c rin

TC~ = TRicN~~ieo~T1 -A1E.

APPROVED

► o~m 619V

IIDI m u imi i iumm i im i I D ID DDI I iBNA0147606 1

HDMSE00624335

R . Schmued _ D/564, FB 6 6

J . Bowman

M. Mo~ CHEMICAL ANALYSIS

REPORTC . WINZER, D/031, SS 12

K . Johns, 01 031 ,SS 1 2

LOG NO

4 - 1?6- 8 3

TO: DEPT./GROUP


REFERENCE : T .nvhnnk 93 Pa 9' 66

PHONE 5447

DATE 14 -APR- B 3

LOG NO .SAMPLE


PPM FLUORIDE BY ELECTRODEWATER SAMPLES FOR

,

FLUORIDE ANALYSI S

BELL CANYO N

time= JD 25'AM D P

time=

time=

time=

time=

Received in the la band analyzed ASAP

4/ /3 / 83

DAY= WONESAAY = EPA distillation method

COMME NTS: The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride t o

be discharged from the property .

APPROVE D

~' crm 61c-vMANAGER 5Z: L ANAL1j1r-!, : . C:;E 13TRi i*4 '

BNA0147606 2

HDMSE00624336

CHEMICAL ANALYSIS

REPORT

TO : nUIRfEiT T,AB DEPT./GROUP 59'-31+14

FROM : SSFL-ANALYTICAL CHEMISTRY

REFERENCE : LB- 83 p. 's4p,L,83

LOG NO ,SAMPLE

IDENT{FICATION+ 3 mg

RESULTS -,

s{- i 5-93TRICH for NVR pe r

RL10001-F

EwR No . 437.25 O

BLANK mg/500 ml

HARDWARE D . ~ mg/5oo ml

EWR No .

BLANK mg/500 ml

HARDWARE • mg/500 ml

EWR No .

BLANK + mg/500 ml

HARDWARE . m,/500 ml

4COMMENTS :

APPROVED G2G4J"R.~.~

MANAGER

To

PHONE 5~ li_ 1~T

DATE

Recd . ____ 'R X83

SSF L Analytical Chemistr y

II0I m u imi i iumm i im i DI 01000 II


INSPECTIOI`~ .UIREDAPPLICABLE DRAWINGS ( ATTACH IF REQUIRED '

YES Jr N O

DOING DEPT . LEDGER ACGOU NT I GENERAL ORDER G O . ITEM 6 NCR I INIT . GROU P

REQUESTED BY EXT. I FACILITY! SHIFT I REQ . SUPERVISION


SHOP I LAB


L_

ti: I -L : Yv ( , t

r,33 1-1`

LEADM AN

DATE ^

HOW . OR TASK DOING GRO U

J 4'% I

ESTIMATO R

MECHANIC

No .R 43725 0REQUESTED COMPLETION DATE


ESTIMATE

HOURS MATERIAL SREQUIRED REQUIRED

S

NOTE ; THIS FORM WILL BE USED FOR NONDELIVERABLE ARTICLES ONLY .

'-: --T/

r-'

hn r /1 v - Ii t f~ I- c

RECEIVED @ LAB

lL ? 1 o" 19 3/o, sleo a „- ,

SSFL ANALYTICAL C''EMISTRYB Y

L. C ,:F /V C, .4,-' / 7 '- 83

c' rLIST OF MATERIALS

uiuiu i iuu i iBNA01476064

HDMSE00624338

TO: ,

FROM :

M. Mogg

CHEMICAL ANALYSIS

REPORT

DEPT./ GROUP


REFERENCE : Logbook '83pg• (e (o

LOG NO .

PHONE 5U 7

DATE

LOG NO .SAMPLE


Wastewater, Canoga

Site L, D/5J4 Scrubber Chromium

S,ucp pH 7.Grab Sample taken

4/I3/3 o 7 3D

R ivedS 1 ecea e


chromium

COMMENTS : The limit for Site L ie 75 z8/i •

APPROVED

F orrn 619-V

SSFL ANALYTICAL CHHiISTRY UNI T

II0I muim i iiu mmiiu mium mmu

To: k _ Yogic

lIK.~At


O!!'T. f aAOU~ 564

SSTL A1IALT ! IGL Oi. IST*T lffT

Logbook ' ~ , pg • (DC,

LOS NO

p,4014* 5447

DATE ___

LOG NO •SAMPLE

IDENTITICATION RESULTS

/ _ 3 Wastewater, Canoga Ghroaiua = Q D i ~ r ) L

Site BE D/544 Process pH a 7, 2Clarifie r


stapley/1211 ..p y)i3/s3

Staple received ./f13`

Aaalysed for pE, and

chromiua

COMMENTS: The L .A . city discharge halt for chromium is 10 ag/L

Analyses per L Wogg 's IL 81 PE-422, 27 Oct . 198 1

£PPf~OVW _I .arrn St9-V

rA rSUL AMALYTIGL OL ISTRY [JEI1 T


I IHDMSE00624340

CHEMICAL ANALYSI S

L, K V ~ A k

REPORT

DEPT./C3ROt3P +.~


REFERENCE L g g3 - 66

LOG N O

~t-l6Q-t3fJ

~- 17o -8 3

c 27_- 1t ?

PHONE S , _ 7

DATE ______-/-P 3

r

LOG NO .SAMPLE

IDENTIFICATION 6 Vs1 rte. cRESULTS

CoM~YSllTts N

/i {wow+ totSAIH

t~ TH Z = ! K. -€ ' d• c 04,

p

L{-l7o- :3 pawn ~esi~ $~twwa co ,~ = !r. g a/0

&eN f KA TbK

&f(( S 4 .',"32d

t, 2 o

.E/Jo t t'C stN S 1 . 3

Co 1.! %

N Ox s Ai t . O. O t 'b

Xt='~ c ok ~s so3 = o cyf X3/4 )

COMMENTS :

APPROVED r

Corm B1Q-V

Nona (kawa, ManagerSSPL Analytical CMmtslrv

SSFL ANAL ICAL CHEMISTRY UNI T

II0I m u imi i iumm i iumium i im U

R . Sch-.ued C D!564, F3 6 6

J . BonaniF ► an cH .

M . Mo CHEMICAL ANALYSISREPORT

C . WINZER, D/031, 55 1 2

TO: DEPT./GROUP


REFERENCE : 1 Q9'L 1(1k B 3 PQ'Je 66

K . Johns ,

[LOG NO •

S5 1 2

4-/67-83

PHONE 544 7

DATE 1-1 fa PR- 8 3

LOG NO .SAMPLE


PPM FLUORIDE, BY ELECTROD EWATER SAMPLES FORFLUORIDE ANALYSI S

BELL CANYO N

time=

4-167-83 / p .,~PPtime= 905A M

time-

time=

time=


4/ 13 / 8 3

DAY= WEDNESDAY EPA dist111 at ion metho d

COMMENTS : The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride t o

be discharged from the proper t

APPROVED

ForT 61a-v

A/

MANAGE

uiuiuuui iBNA0147606 8

S F '+i C F iEM IS TSTR\' U .A *AL',I~.'.iAL CHEIAR't LNIT

I IH D M S E00624342

K . Mogg D 54, FE c6 J . Monaghan D 598, SS 11.

F B . La :y D 596, 55 1


~: M . Francis

FROMSSFL ANALYTICAL CHEMISTRY UNIT

REFERENCE : Logbook '83 Page 64-66

LOG N O

PHONE 544 7

DATE19-May-83

LOG NO •SAMPLE

IDENTIFiCATION RESULTS

4-141-83 Soil Samples Twenty six soil samples were taken from 9 sitesto at ALFA retention pond at depths ranging from

4-166-83 to 2 feet . The samples were analyzed by GC/MSfor trichloroethylene (TCE) at a detection limi tof 20 pg of TCE per kg of soil . The attache d

sheets show the results and site locations .

SAMPLED & REC'D

12-Apr-83

COMMENTS :

APPROVED ~TRY UNITSSFL ANAL ICA

iimm u imi i iumm i im i 1 0100 I 0 I 0 IBNA0147606 9

4-141-83

to4-166-83

DEPT,/GROUP 564 FB 66

HDMSE00624343

LOG NO . SITE DEPTHS FT CONCENTRATIONS PPB

4-141-83 1 62 04-142-83 171 110

4-143-83 } 4804-144-83 2 1 2004-145-83 2 70

4-146-83 71 5504-147-83 3 1 3804-148-83 2 100

4-149-83 71 400

4-150-83 4 1 704-151-83 171 384-152-83 2 50

4-153-83 71 1504-154-83 5 1 80

4-155-83 2 24

4-156-83 71 2 24-157-83 6 1 2 2

4-158-83 2 90

4-159-83 33

4-160-83 7 1 21 04-161-83 2 51

4-165-83 9 ND<20

4-166-83 1} NDC20

1 PPB = 1 jag/kg

ND = None Detected

IIDI m u imi i iumm i im i uiu

ALFA poNO

N

r

~AMr'CF1>

SAM5 i7 )o I

P . Scb- eJ ~„ 0/56+, F9 6 6J . Bolan

aF ncr an ., CHEMICAL ANALYSISK

C . WINZER, 0/031, SS 12

K . Jobrs, D/C 3

LOG NO

SS 1 2

4- 13q-83- 1q o-g3

•

TO: DEPT./GROU P


REFERENCE : t .nahnnk 83 P4.t 64

PHONE 5947

DATE

LOG NO .SAMPL E


WATER SAMPLES FORPPM FLUORIDE, BY ELECTROD E

FLUORIDE ANALYSI S

BELL CANYO N

t i me

-/39-83 R 1. 0time= ~ ____'

q-t~ o- e3 PP O. 9 PPtime= ~sf

time=

times


4/12/B 3

DAY- Tv ESP A `r * EPA distillation metho d

COMMENTS : The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to

be discharged from the property . /

l~

APPROVED ~ -

MAhA R~ o,--n € c- J

5SFL LYTICAL CHEN I . TR'i TTA

II0I m u imi i iumm i im i ui uBNAOI 47607 2

H D M S E00624346

CHEMICAL ANALYSIS

REPORT

TO: QUALITY ASS URANCE

FROM : SSFL ANALYTICAL CHEMISTR Y

REFERENCE : LOGBOOK 83 PAGE !o

LOG NO .SAMPLE

IDENTIFICATION

x{•/37-83 GAS : EL /IJ44

e3RECD : /Z /A/ e3

SAMPLER : O/CZ BB

PRESSURE /95 D P //

A1'ALYSIS REQUESTED


AS ML HANE ONL Y

FROM :

SSFL SUPPLY LINE

ALFA BRAVO

COCA DELTA

Cl'L-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

4/ - /3 7- 3

DEPT/GROUP D/556

PHONE 5447

DATE 3 Q PR r l~' 3

ND < /

RESULTS

(ppm) TOTAL HYDROCARBONS AS CH 4

TR = TRACE ND = NONE DETECTED ( = LESS THAN

= GREATER THA N DNA = DOES NOT APPLY

COMMENTS ; *Maximum allowable limit. per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or C

APPROVED

///

. _ 4 1L ' _ i+ C EI _ _ . . .

IIOI m u imi i iumm i im i ui uBNA0147607 3

HDMSE00624347

CHEMICAL ANALYSIS

REPORT

TO ; QUALITY ASSURANCE

FROM : SSFL ANALYTICAL CHffivIISTRY

REFERENCE : LOGBOOK 93 PAGE 6

DEPT/GROUP D'556

/3 4. . 83

PHONE 5447

DATE

SAMPLELOG NO . IDENTIFICATION RESULTS 3

y-13~o"~3 GAS : /v/r1 4EA/

RECD : /2 /4p'! ./ B3E

SAMPLER : FLDOro3/J

PRESSURE 20~ '4 TR G d (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQ'ISTED

i


AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE ND = NONE DETECTED ( = LESS THAN

ALFA BRAVO= GREATER THAN DNA =DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANX NO .

TRAILER

OTHER • 55P- 3.4 ~pEft

COMMENTS : *Maximum allowable limit per RAO 615-072 for total hydrocarbons as methan eis 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or C

APPROVED

iimm u imi i iumm i im i uiu li m oBNA01476074

I IHDMSE00624348

M . Mv6C, O/564, F6b6 rx


To: P I Q h+ Se ►nr l C •~s

FROMSSFL ANALTICAL CHEMISTRY UNI T

REFERENCE : L09 6 0ok S 3 PA g c. I DATE ' 1-,'1A13

LOG NO .SAMPLE


1-/31-83 JcrFt Sdw.p leiW) <' D . OO / PPf1 TC E

l Ca n ~• o8e H

RF~~ D

COMMENTS : pp~ - PQr+s PCr ,. /lion = M ;l ljrt+*4s /ITer

ND _ NowE DCTEcTEo

7-~g TR/c_HL RDTrfY1-~'JE

APPROVED "' '1'(7 -

SSFL AN

i rm 619-V

IIDI m u imi i iumm i im i uiu I D IBNA0147607 5

LOG NO

' /31-83

DEPT./GROUP 0 3 I

PHONE 5417

I IHDMSE00624349

R . Schmued (. D/564, FB 66

J . BowmanFranM .

M . Mog CHEMICAL ANALYSI SREPORT

C . WIPZER, D,'031, SS 12

K . Johns, D/031,SS 1 2

TO: DEPT. /GROU P


REFERENCE : 1 nahr_rik 83 P49C 64

PHONE 544 7

DATE /4 - APR- 8 3

LOG NO .SAMPLE


PPM FLUORIDE, BY ELECTROD EWATER SAMPLES FO RFLUORIDE ANALYSI S

SELL CANYON O, 7

time= // 0°A14

time=

time=

time=

time=

Received in the la b

and analyzed ASAP

J1 12/ 8 3

DAY- TUESDAY EPA distillation metho d

COMMENTS : The NPDES permit for SSFL allows

be discharged fror, the property .

APPROVED

MA .'tA -Z EF.

a maximum of 1 .0 ppm fluoride t o

IIIIII I IIII III I I I III II I III I IIII I uiu MBNA0147607 6

HDMSE 00624350

ENGINEERING WORK REQUES TTITLE OF JOB DATE

y.-'z No . 8503 89 8INSPECTION REO UIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED ) REQUESTED COMPLETION DAT E

YE S NO

OOING DEPT. LEDGER ACCOUNT GENERAL ORDER G .O . ITEM 8 MCR INIT . GROUP HOW . OR TASK DOING GROUP ACTUAL COMPLETION DAT E

REQUESTED HY EXT . FACILITY SHIFT REQ . SUPERVISION ESTIMATOR ESTIMAT E

Uy/

HOURS MATERIAL S/ / _ __ REQUIRED REQUI R E D

B SUPERVISIONASSIGNED

TO ' LEADMAN:

MECHANIC 5

SHOP LA B

INSTRUCTIONS IRE SPECIFIC) NOTE' THIS FORM WILL BE USED FOR NON .DELIVERARLE ARTICLES ONLY .

RECEIVED @ LAB

rir't 12 1983,z

SS FL AN ,4LYTICAL CNEMIS,TRY

5s / 22 U

FORM R 04 .L REV . 6 .57

LIST OF MATERIALS

IIOI m u imi i iumm i im i uiu I I IBNA0147607 7

HDMSE00624351

LOG N O

CHEMICAL ANALYSIS

REPORT

TO :

FROM :

U ,Hogg

SSFL ANALYTICAL CHEMISTRY L NI T

REFERENCE :Logbook '3p . LI

PHONE 5~7

DAT E

LOG NO .SAMPLE


J o`Wastewater, Canoga

/Site L, D/5~+Ji Scrubber Chromi n - 8O /i'l~/&SWup pH - 7Grab Saapie taken

y z/ 3X30

S le Received

p37

zed for pH, and

chromium

COMMENTS : The Limit for Site L is 75 rig/i .

APPROVED

arm 619-V

/SSFL ANALYTICAL CHF]itISTRY UNI T

J- /31- 3DEPT./GROUP s

IIDI muim i iiu mmiiu mim nuuu


!'ROB SSFL AMLY ICAL O(Ei1 ISTAY U?4TT

REfEAENCS : Logbook '3

OEp rJ 3ROup 564

PHONE 5447

r DATE

LOG NO.SAMPtI

IOEMTu IcATiON RESULTS

`7 -/3D Wastewater, Canoga Chromium Odo7

Site B, D/544 Process pH =~Clarifier •

24 hr . Proportiona l

sample

Sample received L//i2.


chromium

COMMENTS: The L .A. city discharge limit for chromium is 10 mg/LAnalyses per M , Mogg 's JL 81 FE-422, 27 Oct . 198 1

APPU+sOVEQ __ GLW_.I

j.n, 61S-V

SSFL AMLY'TICAL aimISTu SIltI T

IIOI m u imi i iumm i im i ui uBNA0147607 9

HDMSE00624353

LOG N O

CHEMICAL ANALYSIS

REPORTLt -1t7- g

DEPT./GROUP c cg

PHONE S F '' 7

DATE Y 21 8 3

LOG NO .SAMPLE

IDENTIFICATION RESULTS L we+'ji ty

'_ !~7- is NTO s'Myte f, .A,

s rc -y c/12 A/ o = D . 6 2 /a

/? N r~ k /VV X= J t A^ } /J . f N Tt7

Fe = 1 .1 "/K, a f N T o

N?0= T,' .~e c 0 .CI °%

C i 0 .02.0 of N ro

Cu = 0.007 N► ,Ik, of A'TO

o . I 1 AA r /K , ,f NTo

't! 12143

Ica-(A- .--'Norma Fu% ManagerSSFL Anal cal Chemfttry

SSFL AMALY1ICAL CHE1dISTBY UNIT

IIDI m u imi i iumm i iumimmim u i

F" . 77c

CHEMICAL ANALYSIS

REPORT

DEPT./GROUP Saa-~

LOG N O

`f -// 2 -b 3To

PHONE 5' T

DATE APR/L. lZ ,198 3

LOG NO .SAMPLE

IDENT )F4CATION+ o . j !Il g

RESULTS

TRICH for NVR per

RU000L - F

EWR to. 490744

BLANK mg/500 ml

HARDWARE o • mg/500 ml

~AR75 Gp~ ~4-GrG C

plLor 72 v (Ga,~o y7ggc)

EWR No .

BLANK mg/500 ml

~•`~ ~ m8/ 5

EHR No .

BLANK mg/5

ARE mg/500 ml

,(/JT1,;NAGER

Rec'd. ~ _!/

SSFL Anaiytlcai GRsmistry

IIDI muim i iiu mmiiu mimmm u i

cc : P . tl .insaith 0/768, 14Oa. Sch.w.dM . traacis D/56 1i. , PH 66

s. vast

TO I u u PLAPT SEBVICaS

I . _ SSFL ABALTfICAL ('1 STBY

RETEtSfJ~C = LOG 8t '3 PAC$ 61

- CHEMICALANALYSI S

REPORT

OEPT./e'uP D/031

LOG NO .

4- !i4- 3

PMONE 5447

DATE 1-NAY-8 3

LOG NO . IDENT I~ f~ CATsoN D PG$tsi k TBAP GC/IS BESO 'LTS (PW )

114 - '1later sample frbe the Using the aanoeatrstian t.cbniques and ~ethoda ap -

-- Al Inl.t to the 1tZ pro+.d c 4.r the guidelines stated in the aurrec tretemtioo pond at 3L BPD~6 permit, the follo.ing VDLATII2 QB 1lIC

Rocketdyne . O 0[85 gars fo~snd :

Ao.tco. (c3 0oc3) - 0 .3 Z

8.spl .d a . /SPfrl sromodi (BrC~C12) - 0 .00 3

/! ~3 Carl~m T.trachlarid. (CC14) a ND ' .00 1

By : L Cc.//,, k Chloroform (CSC13 ) s 0 .O/5 i

B.thyla .Chloride (C82C12 ) = N~ < . 00/ j86CEIVED • LAB :

1,1,1-'rrichloroetban. (®3CC13) = ,* ' .04/ / ff3

Trichloroethylene (C1CH :CCIZ ) - 0. 004

Notatiou about appear- T.trmchloro.tbylene (C12C :CC12 ) - ND < .00 /

ante of the sample :1,2-Dicbloroethylene (Cl(S :GYIC1 ) = Nl) < .00 1

Dihroeochlosvm.thsne (C1CBBr2) a x .00 2

Isopropyl Alcohol ; also (CS3C80ECH3 ) = 7R . 0 /lmvarn as IPA ; 2-propanol

?r.on TY (C122C1 ) = ND ' . Oo /

1 ,1-Dichioroethan. (C12CHG$3) _ ,4/ 1, AD/

OD1i~lTS : htrschloroetbylsae is also >mo.a as perchloroethyl.ae . (1) Monitoring specifical-

ly r.quirsd according to the Bock.tdyns 1KPGLS permit, Ord.r W 76-146, NPDES P CAOOO1309 from

the California a.giooal Titer Quality Control Board, Loa Angeles Region . (2) This supple -

sientary 1nfor aticn is provided in accordance with 40 CFR 122 .60 .

a Lig$ THAN

APPROVED

~rrr 619-V

TR - TBAc$

SSFL A IGL YISTI:Y ID(IT

iimm u imi i iumm i im iBNA0147608 2

PAL - PASTS PSR MI LLI ONND s lQfB DSTACIZD QCA a DOLS 1117P APPLY

HDMSE00624356

cc : I . Scsassed

r . Frencis D/56k, Fa 66r .

CHEMICALANALYSI S

REPORT

TO: BOCSrry11E PLANT 5 VI(2S

SSTL AZALTICAL CBZfIISTVT

z $ 3 PAC3 6q

DEPT/SuP D/031

LOO NO

4-H3-83

PHONE 544 7

DATE 9 - MAY- 8 3

LOG NO.SAMPLE

IOEIYTt}'ICATION CD P J* Z • TRAP W) OC,4 6 ALTS ( PPM )

- ~~ 3 - $ 3later sastple frog the Osiag the easoentrstian techniques acid .ethoda ap-t2 rateatlm pond at proved vales the gvideliaes stated in the cure tloc>oetdyae . SSPL aPS1f8 pere>St, the following YOLATILa QANI C

CD[I+0 W6 ere found :Freeboard = ~ ft

1 30( Od f .ZS PMS l

®3C ®3) = .Acetoneaazp e

all chloron. thane (B rCaCl Z) = 0 .00 2

By : .L . Co /J"LsCarbon Tetrachloride (CCl4) = Mb < .00

C L1orofors (i C13) . VL < . 00 /UCETVE • LAB :

rethyleae Chloride (tS2C12) = No ~, OO /q // /! d3

1,1,1-?riahlosoethaae (CH30C13) _ NL < . I

Aotatioa about appear- Trlchloroathylaae (ClCS :CC12) _ ~.0/6once of the sal.:

etrachloroethyleae (C12C :CCl2) _ ' , DO

1,2-D1db.loroathylo. (ClC8 :C8C1) = 0.004

Dibrorochloroesthane (C1C~r2) _ 0 . 003

Isopropyl Alcohol ; also (C83C8D& 3) = ND < .01lmo.n as IPA ; 2-propenol

Freon TP (C12FccF2C1) = NO . Ca l

1,1-Dicbioroethane (C123) _ i ~. ~/

COMMENTS : Tetrschloroethylone is also kn n as perehloroethylene . (1) Monitoring specifical'.

required according to the locketdyne 1IPDls2i perait . Order # 76-146 , NPD*S * CA0001309 free the

California legiaoal later Quality Control Board, Los Angeles legion . (2) This supple-

mentary information is provided in accordance with bO QR 122 .50 .

PPM . PAS P** MILLIONDlIA - DES 157T APPLY TR = TRACE

APPROVED ,

1 .,rrr+ 619-V

SSFL ANAL ICAL STAY WILT


I IHDMSE00624357

cc : R. 8chs~ued. Franci 1)1564, TB 661[ s

1[ . Iloz

Tp I DfU Pldlrr SUYTCLS

BSFL AXALTfICAL CS14[1STIT

1lIVCE : LOG nc • 8 3 PAGE 64

CHEMICALANALYSISREPORT

DEPT./3I OuP 51031

LOS NO

4- 112 -83

PP• E 5447

DATE ~Q - _ Y- 83

LOA NO. IDENT I~fICATION Q~ k p © o s us (PP i )

- 112-g3Vats saeple frog the Bsiag the ece trstian t.chaiquws sad a~etbods ap-PP rsteotiCn pond at prov.d under the guidelia.s stated la the currentRochtdyas . S. L AR1~5 per 1t, the folloving Y~ATIIZ OBGU!I C

(0004P0 were found :

Freeboard s ft

d 1:35 pti3 1

//Acsteoe (c23cx 3) - 0 .1b

asp .

s1~" sro.odicbloro.ethan. csr~C12) s ND ' .00 /dh

By : Collinscarbon Tetrachloride (CC14) D . oo /

Chlorofora (C8C13) = d, dG

RECEIVED 0 IA : ll.thyl.ne Chloride (2c12) . ND' . Ob i

4 / B / 8-3 1,1,i- &ioroethane ((S3CC13) a 1VD< .00/

Trichloroethylaae (C1CS :CCIZ)• 0,0/ 1

$otatioa about appear-ance of the aa upl. : . T.trac2tloroethy 1.ne (C12C : CL12) = ND' ,I)0/

# p .OD B1,2-Dichloroethylene (Q® :C8C1) _

Mbr~ocb1oro.ethane (C1C88r2) s f} < .00 /

Ieoproyyl Alcohol ; also ((3;3C OHCH3 ) = ND L . 0 1known as IPA ; 2-propanol

Freon TY (C12FCcF2C1) = Np •C .oO I

1,1-Dicbioro .thane (c12G8{$3) = Mo <, 00 /

C~0[IIQTS : Tetrschloroethyl .ne is also imown as perchloroethylene . (1) Youitoring specificai-

ly r.Guired according to the Rock. tdyne 2fPDE8 permit, Order p 76-146, I0?DES a CA0001309 from

the California Regional later quality Control Board , Los Angeles Region . (2) This supple-

mentary information is provided in accordance with O CFR 122 .60.

• I~SS T8A1V 1®s lIQ1Q

APPROVED

I ~rrn 619-VMANAGER

SSPL AKAL ICAL STAY UIi:T

TA =TRACE


P P B = P A R T S P E R P41 L L I O N9 I><iA = DOES tar APPLY

I IHDMSE00624358

TITLE OF JOB DATE

No 849974 4Nyii' AAMJ y_sUs N,/ PJI P7 e✓ - 4- i/- .I P T ON R IRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED ) REQUESTED COMPLETION DAT ENS EC I EQ U

YES

I

NO X 4GOING DEPT . LEDGER ACCOUNT I GENERAL ORDER 0 .0 . ITEM S MCR INIT . GROUP HOW . OR TASK DOING GROIJP ACTUAL COMPLETION DAT E

REQUESTED BY EXT . FACILITY I SHIFT REQ . SUPER VIB N ESTIMATOR ESTIMAT E

l/J . I

A~ .I U f ` s r? HOURS MATERIAL S

/Y/~~/l

ry(, REQUIRED RE Q UIRE DLAB SUPERVISION ADM N

ASSIGNED TO :MECHANIC $

SHOP LAB

INSTRUCTIONS (BE SPECIFIC I

ENGINEERING WORK REQUEST


1 CAS A71 PfA'~Grl~t A~/ ,t/j' ' ,442 YsIS gW 7X71 fL' A'

OF P,4K7__( /~E' 16(G Ph i l'VIIL h 7/,) Plw ' l

_si~1i✓ 2e N4zz~~,Al 0,-// 7c

7~7AL J/~~ '

#AKP 4/A k'E my

NZ ANk 3 m

my = , 9/ 71/ 1 = r~~~~

4- //- 8 3

RECEIVED @ LAB

LP ; 11199 3

SS FL ANALYTiCACHEnJTRy

.41/_ - 116 - cg.

L_.- OF MATER'ALE

uiuuuuu iBNA0147608 5

HDMSE00624359

EFFLUEN T DISCHARGE REPOR T

CHE CAL ANALYSIS RESULT S

TO : INDUSTRIAL ENGINEERING D/031 SS1 2

FROM : SSFL ANALYTICAL CHEMISTRY D/539 SS1 1

REFERENCE : LOG BK ' g 3 PAGE

lSAMPLED FROM : At 1Y1k+ +o R2 C : I S

LOG N O

4-II I- 83

DATE : 1-APR-6 3

PHONE : 5447

ON f I- APR-8 3

corrSTrr(rErrr RESULTSJl

CONCENTRATIO NTIT, Jl

pH at 25° C 8,1 pH unit to units

Total Dissolved Solids on Drying at 180° C 5 1 5 950Teraperatu.re of Water 16.0 37.8 ° CChloride 53 150

Suspended Solids r 150

Settleable Solids 0.1 m1J1 0.3 rn1J1BCD at 2O ° C I 60

Grease and Oil <,1

5

Residual Chlorine 0 .59 0. 1

Surfactants as MBAS 0, 01 0. 5

Sulfate 140 300Total Chnror¢itmm 0.001 0.01Fluoride 0. 6 1. 0

Boron 0,6 1.0

Turbidity 38 NT(J (5 )

Phenols 0.013 (4 )

Mercaptans 0./ (4 )

C ya ~,d~ 0.00 2

(1) Filtered with Whatrnan GF/C paper .

(2) Filtered with Whatman GF/C paper and dried at 103° to 105° C .

(3) Limitation not required to be met during rainfall .

(4) Wastes discharged shall not contain phenols, mercaptans, or other substances is

concentrations which would impart taste, color, odors, foaming or other object-

ionable characteristics to receiving waters, .,or any substance in concentratiox

toxic to human, an :imal, plant or fish life .

(5) Wastes discharged shall not increase the natural turbidity of the receiving

water. at the time of discharge .

A.ppro,ea

AFL Ah"iXMCAi . CflF:!t1~T1tY '1 T


I IHDMSE00624360

EFFLUENT DISCHARGE REPORT

(5 )

APPROVES • S.tfANA G

Form &'5-vSSFL A LYTICAL CHMISTRY UNIT

EDBNA0147608 7

CHEM ICAL ANALYSIS RESULTS

LOO NO

-4- 1O6- 63TO

4-110-8 3

TO : _ Industrial Er aineering w DEPT ./Group 031

fl04 : SEEFL ADIALYTICAtC_[IS'rRY . IEPT . S3 . PHDNE 5L67

Formom •- LB-83 -o . 64 DATE : Z 1 - A PR - 83SAMM IIE rrIFICATIQN : SA aW Flit R 2 Q I :25 PM ON_)I-APR-93_.. .._..

RESULTS/1

NCENTRATIONL=j /1

pH at 25• C 9.z pH taut to 9 units

Total Dissolved Solids on Drying at 180' a 511 950

Temperature of Water 17.0 37.8' C

Chloride 45 150

Suspended Solids 6 150

Settleable Solids < 0.1 mail 0 .3 mail

BOD at 20 ' C 4 60

Grease and Oil < I 15

Residual Chlorine 0 .0s 0 .1

Surfactants as KBAS 0 .01 0 . 5

Sulfate 164 300Total cnraaium (0, OC' 0 .01

Fluoride 0.5 1 . 0

Boron O . 1.0

Turbidity 2 z NTU (5)Sewage Treatment Plant Influent BDD at 20• C 37'4 (4)

Sewage Treatment Plant Effluent BOD at 20• C 3 (4 )

Sewage Treatment Plant Influent Suspended Solids -4 1 54 (4)

Sewage Treatment Plant Effluent Suspended Solids z(4) -MMMJ

Filtered with Whetmen GF/C paper .

Filtered with What-an GF/C paper and dried at 103°to 105° C .

Limitation not required to be not during rainfall.

The average final effluent concentrations shall not exceed 15$ by weight ofthe average sewage treatment plant influent concentrations of HOD 20 0C andsuspended sclids during periods of discharge .

5

Wastes discharged shall not increase the natural turbidity of the receiving:raters at the time of discharge .

HDMSE00624361

cc : R . Schmued, Y . Francis , M . Mogg : D-'564, FB 66

CHEMICAL ANALYSIS

REPORT

LOG NO

1-106-8 3

Tp ; ROCKETDYNE PLANT S ERVICES OEPT~GROUP D/031

FROMSSFL ANALYTICAL CH8I4ISTRY UNI T

REFERENCE : Logbook $ 3 Page 69

PHONE 5447

DATE Sf 310 3

LOG NO-SAMPLE


4-/06-63 MATER SAMPLE

from

R zAnalyses required :

CYAI4 1DESJQ, o o b ''9/ l ; {ter C V,4 ,4J (DES

PBENOLS 0 . 0/ 3

DATE SAMPLED :

// 8.3

SAMPLED BY :

1 . coil/ ,

COMMENTS: This supplementary information is provided in accordance

.itb 40 CFR 122 .60 .

APPROVED

f .) rrn 619-VMAY AGER

SSFL ANAL CAL TRY UNI T

IIOI m u imi i iumm i im iBNA0147608 8

H D M S E00624362


CHEM i CAL ANALYSIS RESULTS

LOG N O

4- 103-83TO

4- 105-83

TO : _ Industrial Ehaineerinb DEPT./GUP 031

F!Dt : S. R?LALYTSCAL CE~tIST ~Y . . sg PS1HE 447

isc :_ L8- 83 -c.61 DATS : 2L"'APR-$3SAMPLE IIQrTIF ICAT "ION : PROM PP O ! : 35 PM ON 11- A PR -83

RESULTS/l

N ENTRATIONir_mg/i

pFI at 25• C 8.0 pH Wait to t

Total Dissolved Solids on Eaying at 180' C 525 950

Deeratte of dater j 5, q 37.8' CQ]loride 59 150


Settleable Solids < O. 1 m2J1 0.3BOD at 20 C 7 60Grrase and Oil < I 15

Residual Chlorine <0.04 0. 1

Surfactants as MBAS 0.02 0. 5Sulfate I73 300

Total Chrnnimm <0. 001 0.01

7Lmride 0 .8 1. 0Boron 0 .4 1.0

tyT 3 1 N T U (5)_ _ __

Sewage Treatment Plant Influent BOD at 20 ' C 1 80 (h)

Sewage Treatment Plant Effluent BD at 20' C 2 (b)

Sewage Treatment Plant Influent Suspended Solids 37 39 (4)

Sewage Treatment Plant Effluent Suspended Solids 3 (4)

Filtered with Whatman GF'/C paper .

Filtered with Whatmaa GF/C paper and dried at 103° to 2050 C .

Limitation not required to be meet during rainfall .

The average final effluent concentrations shall not exceed 15¢ by weight ofthe average sewage trey ent plant influent concentrations of ~D5 20'C ensuspended solids d'„nring periods of discharge .

(5) Wastes discharged shall not increase the natural turbidity of the receivingwaters at the tine of discharge .

APPRQvW

Form 615-1!A NAG

/

4~

444 ..~

SSPL MkLrrI CA L iEE[ 1 S'i'RY U1 I T


HDMSE00624363

~e?T. 55o


TO: EQUTPr4ET LAB DEPT /GROUP

fLOG N O

L -/o z - 8.3To

P}iONE 5 kL7

DATE A PRIG /z , ! 9 &

LOG NO .SAMPLE

IOENTIFICATION+ Q .3 ru g

RESULTS -

FREON or NVR per

RU0001-F

4-107 -83

EWR No . '-1- 9074 0

BLANK mg/500 a L

HARDWARE Z .1 / 50O n> i

F-BQN 5M4Lt. v4[.v5aR G,4

EWR No .

BLA.'vK m50O ml

RARE IDa/ 5

EHR No . _____

~ANtc @gl 5

uaRE mg/5oo ~

COMMENTS :

APPROVED

MA .YAGER

Recd . g-,/ .-& 3

5 . N. Q a

St. Analytical CR.mistry

II0I m u imi i iumm i iumimm i nm i

ENGINEERING WORK REQUESTTITLE OF JOB n 1/ E

No . 8 4 9 0 7 4 0INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED) REQUESTED COMPLETION DAT EI

DOING DEPT LEDGER ACCOUNT GENERAL ORDER G .O ITEM & MCR 1HIT . GROUP I HOW OR TASK DOING GROUP ACTUAL COMPLETION DAT E

REQUESTED BY EXT . FACILITY i SHI FTY EQ . SUPERV N ESTIMATOR ESTIMAT E

,9 ~lu,~~/ _ 9~~ El 1 V /S

HOURS MATERIALS

RE Q UIRED REQUIR E D


ADM MECHANIC_

SHOP I LAB

INSTRUCTIONS ( BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON - DELIVERABLE ARTICLES ONLY .

lief/_ ,t-le *490,7,79]

hf/iE ,4,V /lW AA~4I r f; e' r{i,y

l'1L~7 ,PI/ (fi 'I771/) PEA' ,L / D̀42/SL ,Vv SL's u! 75 ~~ C2 . 1 14 z W - A. 4' '

P2-I ~, 7 A?V MA"7-J gJvf~ 5tf4'M4I- A107Z/ / Ii, _r Af) 'le f ~ `

Tv TAI 9 ' / f

NAxpw~A~LJ31 ~iA/K

my

RECEIVED @ LAB

11D ; 11198 3

SS FL ANALYTICAL CHEKSTR Y

L_. /D2 -93

FL * ST12 2 sy_I H7 C) = NAATt=RIALS

uiuiuuiuu i iBNA0147609 1

HDMSE00624365

CHEMICAL ANALYSIS

REPORT

M, Mogg


Logbook ' • pg. ~1

PHONE ___

DATE _ '/"/ 3

LOG NO .SAMPLE

IDENTIFICATtON RESULT S

y ld 1- ~3Waetewater, Canog a

Site L, D/5kh Scrubber Chromiur - 5~ /vt /LSump pH 7. ~7

Grab Sample taken

/,'/g3 (2d'? 3 )

Sample Received

(5for pH, and

chromium

SSFL ANALYTICAL' CHEMISTRY UNIT

LOG N O

-/D/- 83

DEPT./GROUP 561t

II0I muim i iiu mmiiu mimmuiim u

~IoQQTa: v .

rROSG


OEPt/OIlOUP 56~_

931L AMLYTICAL O( I3Til! UET

!!EnRENCE: Logbook fj pg.

LOO MO .

/-/ O-~ 3

P♦IOMS 5447

DATE ____

LOG NO .SAMPLs

IDENTiFIGAT$ON RESULT!

Y-r~- Waatmter, Canoga Chromium - N4 2. < d,o 5 MS,/t_

Site B, D/544 Process pH : 7 /Clarifier (p

G a .•asea le f4K!i. s

11 130',/i 3 @,03i

Seaple received

Analyzed for pH . andchroaiua

COMMENT!: The L .A . city diaekarse lieit for cbromiua ie 10 md/LAnalyses per Y. Yogg 's IL s; PE-422 , 27 Oct . 198 1

APPROVED ,

I S1 -V

SUL ANALYTICAL. Ot. 1ST Y UNIT


I IHDMSE00624367

_ r_a-' . 5 ;Q LO(~ N O

CHEMICAL ANALYSIS `f -

REPORT _

To: EQUTWINT LAH DEPT fGROUP 59-3!4

To

PHONE5! 7

DATE ,4P1 u /2 ,/983

LOG NO .SAMPLE

IDENTIFICATION RESULTS ± ~' 3 ~B

TRZCH for NVR per

RLL0001-F

4 -95-&3EWR no . 503893

BLANK 0 .3 mg/ 50O sI

HARDWARE mg/5OO m1

-i&µ L45TC 4&i TA N k

EWR Yo.

BLANK ~/5OO ml

EWR No.

BLAMC m8I5OO

WARE "_, mg/500 ml

COMMENTS :

APPROVED

MANAGER

Re' d . ' _

SL Ana ytlcal Ch.mI .try

IIDI muim i iiu mmiiu mimmi iimu


3 No.R5n389 :jINSPECTION REQUIRED

APPLICABLE DRAWINGS ( ATTACH IF REQUIRED ) REQ UEBTED COMPLETION DAT E

, /YES 1 1 NO Y NDOING. I LEDGER ACCOUNT GENERAL ORDER G .O . ITEM 6 MCR INIT . GROUP HOW . OR TASK DOING GROUP ACTUAL COMPLETION DAT E

REQUESTED BY FACILITY SHIRT REQ . SUPERVISION ESTIMATOR ESTIMAT E

l'7" ~f Asp'

_~-----

HOUR SREQI1IRED

MATERIAL SREQUIRE D

PE ISIONASSI6'NFD TO :

LEADMAN MECHANIC III

SHOP I LAB

INSTRUCTIONS ( BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

4::151 &,~~ -4~ L~~'6;~~

~5vA>-- /~~ ~?671 -

RECEIVED 0 LAB

A 111983

BY LL ANALYT1CAISTR Y

- 9 .5'- s3

FORM R 94 .L REV 4.57

uiuiuuui iBNA0147609 5

LIST OF MATERIALS

I IHDMSE00624369


TO:

FROM :

F. pA ~o f a.


REFERENCE :, LK Y3- 62DATE

LOG NO.SAMPLE

IDENTIFICATION RESULTS by W.9rh t

--- s s N Tv s A ~.r /'f f1 OM u p 0. t 2 %

ST t - w ft i6

N d X= .2 N ► Y/j .f Ntor

'M 14NR

Fe = I. ( ^^ '/1C 7 .f NTO

,y t 0. 0 c of NTo

111 0 = r~ 4 « o. o, •,,Cx 4, olo&„, /A .f NT o

C t4 = p, 0/I ""Yll~g a NTJ

0 . oo ~

x< <'/ i i f ~ 3

COMMENTS :

APPROVED

Form 619-V

LOO NO

~- q'f-- s 3

DEPT. /GROUP Se,

PHONE S _ y' 7

SSFL ANALYTI CAL Q ISTRY UNI T

II0I muim i iiu mmiiu mimmimm u

. J ~

Q'ROM

~ BoD~Me .~EQ Z ~R- 33CHEMICAL ANALYSI S

K . Francis

REPORT

- DEFT,/GROUP

BSFL ANAL?UCPI L CiiEM1STRY UNI T

REFLREIVCE : I,8-83-page 62 ; NB 329, p . 152

PHONE 544 7

DATE APRTL 18 . 1983

LOCI NO .SAMPLE

IDENTIFICATION RESULTS (OC REVISION B)

4-93-83 RIGIDAX, 26-22, Total PCB's as Aroclor 1260 25 mg!kg

WI-NF, Lot 3201

Detection Limit = 25 mg/k g

Total 1"CT's as Aroclor 5460 < 50 mg 'kg

Detection Limit = 50 mg 'k g

® Results were obtained using a gas chroaatograph

equipped with an electron capture detector. A six

foot glass coluan packed with 3% SP -2100 on 100.'120

RECEIVE 11 A 83 aesh Supelcoport was utilized under the following

conditions :

(Wl TBIPERATURE P8 )FIL8 :

Initial value = 200°C

Initial tine = 1 . 00 ainute

Level 1

Progra■ ratb = 8 .00 °C

Final value = 335 QC

+

x 1 Th e ckrowatgraa did not coapare with known Aroclo rI1260 or Aroclor 5460 .~-

COMMENTS: G = Less than

N .A . = Not availabl e

APPROVED

I orn+ 519-V

AG

LOGNO •

4 - 93 - 8 3

564 FB66

e/d 7Ssn. AJMLTTIGL ai~ISTR Y LWI T

IIOI m u imi i iumm i im i IDIM DBNAOI 47609 7

HDMSE00624371


r

!FROM

L Franci s

SSFL ANALYTICAL CIinIISTRY UNIT

LOG NO •

4-92-83

DEPT./GROUP 564 FB66

REFERENCE :LB-83-page 62 ; NB 329 , p . 151

PHONE 5447

DATE APRIL 18, 198 3

LOG NO .SAMPLE

4DENT4FICAT{ ON RESULTS (GC REVISION B)

4-92-83 Bennet Products Co . ,

Inc ., Yellow, Electr Total PCB's as Aroclor 1260 25 mg'kg

forming Filler

Replacement Detection Limit = 25 mg'kg

Total PCP's as Aroclor 5460 t 50 mg 'kg

Detection Limit = 50 mg'kg

® Results were obtained using a gaa chroestograph

equipped with an electron capture detector . A si x

foot glass column packed with 3% SP-2100 on 100 '12 0

RECEIVF) 11 APR ' 83 mesh Supelcoport was utilized under the following

conditions :

0V~Q TPSRATDRE PROFI LE :


Initial time = 1 .00 minuteLevel 1

Program ratb = 8 .00 °C

Final value = 335 QC

QThe chrosatograa did not compare with !mown Aroclor

1260 or known Aroclor 5460 .

gr LTf ICA L C~LI SfY @t TI

i orrn 619-V


HDMSE00624372

. O~

PROM :

CHEMICAL ANALYSIS

REPORT

1[ . Franci s

BSFL ANALYTICAL Ctin[ISTRY UNIT

DEFT./GROUP

REFERENCE :LB-83-page 62 ; NB 329, p. 150

PHONE 544 7

DATEAPRIL 18, 1983

LOG NO .SAMPLE

IDENTIFICATION RESULTS (OC REVISION B )

4-91-83 Bennet Products Co ., Total PCB' s as Aroclor 1260 L 25 mg'kgInc ., Blue, Replace-

ment Electroforming Detection Limit = 25 mg'k g

Filler

Total PCB's as Aroclor 5460 < 50 mg'kg

Detection Limit = 50 mg'k g

Q Results were obtained using a gas chromatograph

equipped with an electron capture detector . A si x

foot glass coluan packed with 3% SP-2100 on 100'120

RECEIVED 11 APR ' 8 awesh Supelcopo rt was utilized under the followin g

-- oonditions :p. _. TBaI1PHiATVRE PROFILE :


Initial Lila 1 .00 ainut e

Level 1Ptograa ratb = 8 .00 °C

Final value = 335 °C

A1 Tbt cbrosatograa did not coapare with lmown AroclorL

1260 or known Aroclor 5460 .

COMMENTS :

APPROVE

Form 619-V

LOG

4 - 91 - 83

564 FB66

$STL ANALTTICAL QinLISTRY IT

IIOI m u imi i iumm i im i I D I DID D IBNA0147609 9

= Less than

LA . = Not available

HDMSE00624373

7:

FROM


Y . Franci s

BSFL ANALYTICAL QiD[ISTRY UNIT

DEPT/3ROUP

REFERENCELB-83-page 62 ; NB 329, p . 1 49

LOG NO

4 - 90 - 83

564 FB66

PHONE 5447

DATEAPRIL 18, 8 3

LOG NO .SAMPLE

{pENTIFICA TION RESULTS (OC REVISION B )

4-90-83 Bennet Products Co ., Total PCB's as Aroclor 1260 < 25 mg/kgInc ., Pink, Replace

ment Electroforming Detection Limit = 25 mg/kgFiller

Total PCT's as Aroclor 5460 50 mg'kg

Detection Limit = 50 mg 'k g

® Results were obtained using a gas chromatograph

equipped with an electron capture detector . A siz

foot glass coluam pscked with 3% SP-2100 on 100'120

RECEIVED 11 APR ' 83 mesh Supelcoport was utilized under the following

conditions :0Vlfli T~ RRATURE PROFI LE :

Initial value 200°C

Initial time = 1 .00 minute

Level 1

Program ratb 8 .00 °CFinal value = 335 oC

Q The ckromatogram did not compare with {mown Aroclor

1260 or known Aroclor 5460.

4wtci -

SSrL AEALTTICAL QITSlIsnY D I T


HDMSE00624374

CHEMICAL ANALYSI SREPORT

TO : J7M W/L. SO/V DEPT./GROUP


LOG N O

`f _8 9 _83

PHONE 5e/ i '?

DATE 1/ 9,O/2 ' g

LOG NO .SAMPLE


4-8g -83 FLU/„j~ 7~) =a OM A-3 4i' i' . PPMF,~EaN TF ~C/~ AC C a C /,2E TLJ .N $ y ✓oW#t1

Ec'I No, y9</8i5

FOR FIeEO ,V CCNTS N

ER ,€I. /o/ 2

SR MPG E 7~t C !~

// A PR i L 83


Form 619-V

IIDI m u imi i iumm iiuumimmiu


To : Av2? Y V4 )G Hit/

FROM : SSFL ANALYTICAL CHEMISTRY UNIT

LOG NO -

DEPT/GROUP5

/ 8- 3 4' 5

REFERENCE : O'/( /83

PHONE 5 yy

DATE c/ A P12 X83

LOG NO .SAMPLE


4L-87- 83 RP-f rgoM2 ' 9 N/ T _

~2R v0 3T4Nd BaCo

aA Tc d /aJ

it /C D j,V / TC

Co iv TEN T

SRIt4PLE fet C O

COMMENTS :

APPROVE D

Form 619-V

A/fSSFL ANALYTICAL CHEMISTRY UNI T

II0I m u imi i iumm i iuumimiiii U


To: F. pA T o T 4


REFERENCE

DEPT/ GROUPP

LOCI N O

£1.- 47- Q 3

c4'

PHONE SI ' 7

DATE 'f- 2 Y 3

LOCI NO.SAMPLE

IDENTIFICATIONf

RESULTS ~y f

q- - ; N TO S" /,r M NO - 0. 2 '4

STl-it ct[l 29dNVK = ,~'~/k of NTc~

I~ UA/ T4 ,l k~

Fe = O. s .? M yak a NTo

AL = d. 0 ` '~ ► y /f~ I f N TO

({2 o _ Trwcc L 0.0/'1.

C, D. 0 + 0 .N TO

(j = 0 .0!, Mfit Ky of IY7tJ

M = 0 070 . y/K of HTo

KY ~

COMMENTS :

APPROVED

Form 619-V

SSFL ANALYT ICAL CHEMISTRY UNI T

IIOI muimiiiummiiuumiuuiuiu

TO :

FROM :



REFERENCE : Logbook 'g3pg' l02

PHONE 5447

DATE

LOG NC .SAMPLE


-~-~3Wastewater, Canog a

Site L, D/5114 Scrubber Chromium - G~Sump pH 7.Grab Sample take n

71,$'1 g3 , 0 '? )

ivedy/W~3S mp~(~

Analysed for pH, and

chromium

COMMENTS: The limit for Site L is 75 rtg/1 .

APPROVED

I .)rm 619-V

ILIZLV _______

53FL ANALYTICAL CHEMISTRY LNL T

IIOI muim i iiu mmiiuu mim i iu

LOG NO .

D£PT./GROUP 564

U


TO: M' Mogg DEPT./GROU P

FROM : SSFL ANALYTICAL CHEbtISTRY UNI T

REFERENCE : Logbook ' 3 ca• (, +2

PHONE ~1L1 7

DATE __L(___

LOG NO .SAMPLE

IDENTIF$CAT ) ON RESULTS

Wastewater , Canoga Copper - Q , 1 Z_ mg/L

Site C, "Sea World" Nickel - L/, 8 rng/ L

p~ - g O2L hr. Proportiona l4p--'~tsa tokp n

y/~/S 3 --~ yft/

ample received

thaLyed for copper, pEnd nickel

COMMENTS : The L.A . City discharge Limit for copper is 15 ng/l, for nickel, the Limit is12 ng/ 1 .

AaaLyaes per M . Mogg's IL,81 F!4i22, 27 Oct . 1981N .D. - None detecte d

APPROVED

S . FL ANALYTrCAL CHF7(ISTRY UNI T


UHDMSE00624379


To: . ova

lR01~ SSTL A :UUTICAL Qf 1ST1LY WI2T

RfPERENGE : Logbook ' 3 pg . ~o ~-

L06 NO .

DEFT./GOP 564

PHONE 544 7

DATE 8 8 3

L03 340.SAMPLE


Wastewater , Canoga Chromium = Q /' fytg/L

ISite B, D/544 Process px = 7. 0Clari fier

24 hr . Proportiona lsample

yl7ffr3--~ /c/g3

t

Sample received

Analyzed for pH, andchromiua

COMMENTS: The L .A. city discharge limit for chromium is 10 mg/L

Analyses per M . Sogg 's IJi 81 FE-422, 27 Oct . 1981

APPROVEDS WL A!M LY! I CA L OiftX ST*Y IJ (LT

r 619-V

IIOI m u imi i iumm i im iB NA0147610 6

HDMSE00624380

CHEMICAL ANALYSIS

REPORT

TO 0. BAUERLE

FROM SSFL ANALYTICAL CHEMISTRY

REFERENCE: LOGBOOK r S 3 PAGE r0 Z

LOG NO

4-70-g~r~ Igo Li ( (.E

4r, - g 3

DEPT./GROUP D/522

PHONE 4824

DATE

LOG NO •SAMPLE


I .D . # _ '? ^g3 MEASURED PRESSURE _ (o / ms

SAMPLE # = C L S i b , 02 = s' 7 N2 = 2 I- Z m m4-7o-3 - N~

FLASK # =pr He = _ 0 am Cl2 = N) Ld. ol mm (' of )

PRESSURE = - _ psia H2O = Q ~n_ NOTE :WASCCEgk.tiFr.as+c 6

------ ------- 4r rimi

I .D . 7 - 3 MEASURED PRESSURE _ > /CC as

-

'SAMPLE # _ / O2

=- / (Q O mm N a = S$ O-

FLASK W = !O He = formmD C12 = 00 mm (0.Q )

PRESSURE _

__

sia

_____

^- 2NorE : Sro/NoCK O G

_ p H2O = . mm FtgSk u,qs f £AKrN(tl

----- - - - -

A r -r rt1L 0 F AN 14'Sis.

-- ------ -- -I .D. # = 4-7-~ 3 MEASURED P .ESSURE= mmbZ-

SAMPLE # = ~- 02 = /7. _ mm N2 = I. Z mm

FLASK # = He = 41 . S mm cl2 = 0 . 0 3 mm ( 0 03 )

PRESSURE = - psia H2O = 0. 0 mm

- - - - - - - - - - -

I .D. # =

- - - - - - - - - - - - - - - - -

MEASURED PRESSURE =

- - - - - - - - - - - - - - - -

mm

SAMPLE # = 02 = mm N2 = mm

FLASK # = _ He = mm C12 = mm ( )

PRESSURE = - psis H20 = mm

COMMENTS :

APPROVE D

Form 614-V

SS ANALYTICAL CHEMISTRY UNI T


CHLORINE VALUES IN PARENTHESES ARE NOT CORRECTED FOR MANIFOLD SAMPLING LOSSES

AND ASSUME CONVERSION TO CHLORIDE PRICE TO THE CHLORIDE DETERMINATION . ALL

OTHER VALUES ARE CORRECTED FOR THESE LOSSES . WATER IS DETERMINED BY REACTION

CHFIOMATOGRAPHY .1 ,~Er5u,.rS Q~ /i Pl e0 kI /t/7 .

HDMSE00624381

51,7PHON E

DATE 41/. 23

LOG NO .SAMPL E


LOX

ALFA I

7YuRrry7183

oxYa i BY VOLZXE

# 0/9

@ 2O() PSIG

RECEIVED :

`7 / 7 f

SSfL Analytical Ch .rnistry

IIDI m u imi i iumm i im i i ii

-- aT c~ LOG NOi~.1. CHEMICAL ANALYSIS

REPORT _To

-

rO : EQUIPMENT LAB

FROM : SSFL-ANALYTICAL CHEMI STRY

REFERENCE : LB' P. 62.

DEPT /GROUP 598-3h

PHONE 5 14 1+7

DATE A ~JP/L Q , I ~I ~j

LOG NO.SAMPLE

IDENTIFICATION+ p, 3

RESULTS - nig

TRICH for NVR pe r

RL10001-F

-68 -834EWR No .

BLANK mg/500 ml

aRnwaPE / • 3 mg/ 50O m1.

$4f/€D : 74P4J$

EWR No .

BLANK mg/5OO ml

HARDY • mg/

EWR No .

BLANK mg/5

ARE . mg/500 ml

COMMENTS :

APPROVED

MANAGER

Rec'd. ~f

N 0Ua 11~ 47SSFL An lytlcal Chemistr y

II0I muimiiiummiiuumim i iim i

. .,iNEERING WORK REQUES TITLE OF JCR DATE

No. 850389 0INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED) REQUESTED OMPLETION DAT EC

"61YES I NIO /.

_.. . ..._

DOING DEPT . LEDGER AC U NT GENER AL ORDER G .O . ITEM 9 MGR IN IT GROUP HDW OR TASK DOING GROUP--

ACTUAL COMPLETION DATE

QUESTED EXT . FACILITY SHIFT REQ . SUPERVISION ESTIMATOR ESTIMAT E

B

_HOURS MATERIAL S

REQUIRED REQUIRE D

-ul

ERISION LEA DM AN MECHANIC $

/

ASSIGNED T

SHOP LAB

INSTRUCTIONS BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

e:~~ "-/~

2- 2

RECEWED @ LA B

APR 7 ;93 3/ 4-' .5 Z#-I _

SS FL ANALY T iCA CH ISTRYBy -4~4~

'8 3

FORM R 94-L REV 6 .57

= /226

LIST OF MATERIAL S

BNA0147611 0

HDMSE00624384


LOG N O

~ - 63 - b 3To

DEPT./GROUP 598-3l

PHONE 547

DATE APR'L b ,1`783

LOG NO .SAMPLE

IDENTIFICATIONt 0 .3 m8RESULTS

Freon for NVR per

RL10001-F

sL43 -83 EWR No .

` 'Freon Ppm

F r o rr+ / ✓5. _ m8 ml✓ o /i'.e - fo'c k

EWR No .

BLANK • mi5OO m1

HARD'.! • sgf

EWR No .

BLANx mg/5

.ARDWARE m8/5~ ~-

COMMENTS :

APPROVED

M A.'V ACER

Recd .

5 o11 ,SSFL Ac✓alytieal 'Cham(stry

IIDI muim i iiu mmiiumiu iiiuu i


INSPECTION REQUIREDA LICABL RAWINN" (ATTACH IF REQUIRED)

YES NO

DATE

No.R50936 4__REQUESTED COMPLETION DAT E

DOING DEPT LEDGER ACCOUNT GENERAL ORDER G .O . ITEM & MCR INIT . GROUP HDW . OR TASK DOING GROUP ACTUAL COMPLETION DAT E

' REOU STED BY EXT . FAtJL17Y SHIFT REQ. SUPERVISION ESTIMATOR ESTIMAT E

y v~ _

- -- -

HOURS MATER]AL BRE Q U1RED R EQU IRED

LAB SUPERVISIO N---

_ ___ASSIGNED

TO :LEADMAN MECHANIC

$ _-

SHOP I I LAS

INSTRUCTIONS IBE SPECIFIC) NOTE: THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

Y-- S If C 7 Y/~ 'I 1' 6 G- ✓ ~I 1 P-' ~.,1 r .r. ; ' / =-,'" .

I vZ

S e 0- e "

A,' 7 c? J )

G-. ., vT P -y " 'h .

r. se, rf 0rSa oJ Z

~-Or ,,/ , ., 1

Die s

-y -/ r, °/ /0

.r/c O, , o"c- c /,P//

,z . , ,

-s, p

y v S .. ,/ , .- 0 ,#

r-r

Y 'e

-. / Gi / P CSI` ,

't- - 3F -3

LIS OF MATERIAL S

BNA0147611 2

HDMSE00624386

r'

G l/G 11

Internal Letter Rockwe H Internat cnai

26 April 1983 MFR 83-031 9

c : BUT IO N

, SS i 1J . Kwa n

E59c-346,SS11S,Yscc ie r

0539, SS11N . Fujikawa

.G, Shanks S . 3 . Evan s

.D/598-346 SSFL Analytical ChemistrySS12 0539/ 169, SS1 I

Glove Compatibility Test s

Samples of three brands of cloves, uranet 2002, Edmont 29-865, andPioneer NS-35, were exposed to NTO, '1MH, IPA, Freon, and Tricn asper instructions in EWR No . R50364 . All three gloves seem to beunaffected by Freon and IPA . On exposure to trich, all threeglove materials swelled on contact with the worst swelling beingencountered in the Pioneer NS-35, and the least being observed inthe Granet 2002, Even with the swelling of the glove material,there was no noticeable loss of strength and pliability in thegloves . On contact with MMH, the Pioneer NS-35 and Graret 2002were unaffected and the Edmont 29-865 seemed to dissolve veryslightly (noticeable only because he hMH became yellow), and allthree gloves retained their strengtn and pliability . None of thegloves lasted for more than 4 minutes in NTO (two 2-minute soakingsas per EWR) . The glove materials became hard and blistered on airdrying and the deterioration was accelerated by flushing the materialwith water after the two-minute NTO immersion .

Based on the results of these tests , none of the gloves tested cansafely be used when handling NTO and they are questionable whenhandling trich because of the swelling .

J - 2 ( -Steve Evan sMember of the Technical StaffSSFL Analytical ChemistryMaterials and Producibility

SE/jbApproved :

N . S . ugi aw , ManagerSSFL Analyti al ChemistryMaterials and Producibility


~v

UHDMSE00624387

cc : R . Schmued D/541, FB12

M . Francis D/541, FB12M . Mogg D/541, FB12

TO: ROCKETDINE PLANT SERVICES


CHEMICALANALYSI S

REPORT

DEPT./ GROU P D/031

REFERENCE : LOG BK ' 83 PAGE 6 2 NOTEBOOK

LOG N O

4 - 5C - 83

PHONE 5447

DATE $ -APR-e 3

LOG NO .SAMPLE

IDENTIFICATION j PURGE & TRAP ✓ GC/MS RESULTS (PPB )

water sample from the Using the concentration techniques and methods ap -4-56-83 PP retention pond at proved under the guidelines stated in the curren t

Rocketdyne . SSFL NPDES permit , the following VOLATILE ORGANI C

6 5CONFOUNDS were found :

.Freeboard = f t

4SA

Acetone (CH3000B3) = D < IDSampled @ g M

/-4/7/d3

Bromodichloromethane (BrcBCl2 ) =

B £To /4Carbon Tetrachloride (CC14) _ ND' I

y : i 115.Chl f (oro orm (~C13) =

RECEIVED @ LAB : Methylene Chloride (CH2C12) _ D< I

4 / 7 / P3 1,1,1-Trichloroethane (CH3CC13) = NZ< I

T 3Trichloroethylene (C1CR:CC12)Notation about appear-ance of the sample : Tetrachloroethylene* (C12C :CC12) = AID .( /

= - -1,2-Dichloroethylene (C1CII :CHC1) 1 I

Dibromochloromethane (ClCHBr2) =

Isopropyl Alcohol ; also (CR3c OHCR3) = _ t _

known as IPA ; 2-propanol

Freon TF (C12FCCF2C1) = ND~ /

1,1-Dichloroethane (C12CHC113) = /IIQ C /

COMMENTS : * Tetrachloroethylene is also knows as perchloroethylene . (1) Monitoring specifical-

ly required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES # CA0001309 from

the California Regional Water Quality Control Board, Los Angeles Region . (2) per (1) "Wastes

discharged shall not contain phenols, mercaptans, or other substances in concentrations which

would impart taste, color, odors, foaming or other objectionable characteristics to receiving

waters . . .", "or any substance in concentrations toxic to human, animal, plant, or fish life . "

PPB = PARTS PER BILLION= LESS THAN ND = NONE DETECTED DNA = DOES NOT APPLY TR = TRAC E

APPROVE D

r arm E'9 V

4//f. .SSFL ANALYTICAL C I TRY UNI T

II0I m u imi i iumm i im i ID ID DID DBNA01476114

UHDMSE00624388


M . Francis D/541, FB12

M . MOgg D/541, FB1 2

TO: ROCKETDYNE PLANT SERVICES

FROM: SSFL ANALYTICAL CHEMISTRY

CHEMICALANALYSI S

REPORT

DEPT./GROU P

REFERENCE : LOG BK '3 PAGE 6 2. NOTEBOOK -

LOG NO .

4q - 55 - ?3

D/031

PHONE 5447

DATE ____ - _

LOG NO .SAMPLE

IDENTIFICATION PURGE & TRAP GC/MS RESULTS (PPB)

Water sample from the Using the concentration techniques and methods ap -

.ss _ ems? R2 retention pond at proved under the guidelines stated in the curren tRocketdyne . SSFL NPDES permit , the following VOLATILE ORGANI C

f tFreeboard = /COMPOUNDS were found :

_

q'Acetone ( CH3000H3) =

Sampled @ AM84/ / Bromodichloromethane (BrCHC12 ) = /(/Q (7 Pj

Carbon Tetrachloride (CC14) =

By : L ./

C o //MJChloroform (CHC13) = O

RECEIVED @ LAB :(C C1 TI?'H2 2 ) =Methylene Chloride

1,1,1-Trichloroethane ( CH3CC13 ) = ND .

6Notation about appear- Trichloroethylene (Cl® :CC12) =

ance of the sample : nnTetrachloroethylene* ( C12C :CC12 ) =

1,2-Dichloroethylene (Cla :aC1) =

Dibromochloromethane (C1CHBr2) = ND /

Isopropyl Alcohol ; also (CH3CHOHCH3 ) = ,VD/ 2known as IPA ; 2-propanol

Freon TF (C12FCCF2C1 ) = /IIQL

1,1-Dichloroethane (C12CHCH3 ) = ND' !

COhLti4ENTS : * Tetrachloroethylene is also known as perchioroethylene . (1) Monitoring specificall

required according to the Rocketdyne NPDES permit, Order W 76-146 , NPDES # CA0001309 from the

California Regional Water Quality Control Board , Los Angeles Region . (2) per (1) "Wastes dis-

charged shall not contain phenols, mercaptans, or other substances in concentrations which

would impart taste, color , odors, foaming or other objectionable characteristics to receivin g


PPB = PARTS PER BILLION

= LESS THAN ND = NONE DETECTED DNA = DOES NOT APPLY TR = TRACE

APPROVE D

1 ~rrrn 519-V

SSFL ANAL CAL C ?TRY UNI T


HDMSE00624389

cc : P . Kleinsmith D/768, T040

R . Schmued D/541, FB12


M . Mogg D/541, FB12

CHEMICALANALYSI S

REPORT

TO ROCKETDYNE PLANT SERVICES DEPT./ GROUP

FROM SSFL ANALYTICAL CHEMISTR Y

REFERENCE : LOG BK ' $3 PACE 62 NOTEBOOK

D/031

LOG NO .

PHONE 5447

DATE 8-, 4PR - 8 .3

LOG NO .SAMPLE

IDENTIFICATION & TRAP © GC/MS RESULTS (PPB )PURGE

Water sample from the Using the concentration techniques and methods ap-

4-59 'B3 Al inlet to the R2 proved under the guidelines stated in the curren t

retention pond at SSFL NPDES permit , the following , VOIATILE ORGANIC

Rocketdyne . COMPOUNDS were found :

Acetone ( CIi3000H3 ) = ND< /D

Sampled S Bromodichloromethane (BrCHC12) = I'Q~ I

7 f'j Carbon Tetrachloride (CC14) = I

By : L . Ca~/riifr Chloroform (CHC13) = 2Methylene Chloride (CH2C12)

RECEIVED @ LAB :Cli CC1 = TR < I3 3)1,1,1-Trichloroethane (

-4/ 7 /?33Trichloroethylene (C1CJ : CC12) =

Notation about appear- Tetrachloroethylene* (C12C:CC12) - N 1ante of the sample :

1,2-Dichloroethylene ( C1CH :CfiC1) = ND<

Dibromochloromethane (C1CHBr2) = N d /

Isopropyl Alcohol ; also ( CB3CIIOBCH3 )


Freon TF (C12FCCF2C1) = N< /

1,1-Dichloroethane (C12Q1Ci3) = N11. /

COMMITS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifical-


the California Regional Water Quality Control Board, Los Angeles Region . (2) per U) "Wastes

discharged shall not contain phenols, mercaptans, or other substances in concentrations which

would impart taste, color, odors, foaming or .other objectionable characteristics to receiving



= LESS THAN ND = NONE DETECTED DNA = DOES NOT APPLY TR = TRAC E

APPROVED

t ~rrn 619-V

N.J '. 97's •ISSFL ANAL ICAL STRY UNIT

IIOI m u imi i iumm i im i ID ID DI D D I IBNA0147611 6

HDMSE00624390

CHEMICAL ANALYSISREPOPT

LOG No .

L1-y8-8 3TO : M . Mogg DEPT./GROUP 56+

SSFL ANALYTICAL CHEMISTRY UNIT PHONE 544T

DAT E

LOG NO .SAMPLE


1718-33 Weetevater , Canoga

Site L, D/54l Scrubber Chromium - 43 MJ/LSump pH 7

Grab Sample taken

q/'71V3 0'730

Sample Rtceived .117Af

D ?11;0Analyzed for pH, andchromium

S ziFL ANALYTICAL CHEMISTRY UNIT


To. M . Mogg

FROM:-SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE : Logbook ' iR 3 DR. ~o V

rLOG NO .

y-y7-g3

PHONE [41i7

DATE , 7193

LOG NO

.

SAMPLEIDENTIFICATION RESULTS

y~y7-Ll7 Wastewater , Canoga Copper - 0.2.7 Ong/ L

Site C, "See World" Nickel - 4, 2. rng/ L

24 hr. ProportionalPM 7.

Sp^rtp f'-'We n1 / / / c 3 - >-

d yb/637 5c~

lyzed for copper, pA

and nickel

COMMENTS: The L .A. City discharge limit for copper is L5 rg/1, for nickel the limit i s1.2 mg/ 1 .

Analyses per M. Mogg 's IL 81 PL-422, 27 Oct . 1981X .D. • None detected /

APPROVED

.- - 92 . %-%A

DEPT./GROUP '; 1

aF~ LYTICAL CHEMISTRY L1 41 T

BNA0147611 8

HDMSE00624392


7=

SSlL A!ULYTICAL CHMISTIIY UNIT

REFERENCE : Logbook ' £s3 pg.

DEPT./GROUP 564

PI• OP4E 5447

DATE g'3

LOA NO .SAMPLI


Wastewater, Canoga Chromium =0. 13 Mg

Site B , D/544 Process PH =

Clarifier


'//G/83 -.a y~~~f3

Sample received y/7/53

Analyzed for pH, andchromium

COMMENTS . The L .A . city discharge limit for chromium is 10 mg/LAnalyses per V . Mogg ' s 1jL 81 FE-422, 27 Oct . 1981

APPROVED

I .arm 619-V

S31L ANALYTICA L CHMISTItY UNIT

I IBNA0147611 9

HDMSE00624393

CHEMICAL ANALYSIS

REPORT

To: EQUIPMENT LAB

LOG NO'

To

DEPT/GROUP 599-344

PHONE 5447

DATE A ?R!L 8 1983

LOG NO .SAMPLE

IDENTIFICATION0 .3 mgRESULTS

Freon for NVR per

RL10001-F

EWR No .

Freon T, 3 m g/500 Ml

m/cN& mg/5O0 ml

EWR No .

BLANK m8/5o0 ml

HARUw • ag/

EWR No .

BLANK; mg/5

HARE mg/500 ml

COMMENTS :

APPROVED

MANAGER

Aec'd . 4 17 /f(3

SSF L Analytical Chemistry

CHEMICAL ANALYSIS

REPORT

DEPT./GROUP 599

LOGNO •

`1- qL]- X5 3

P "ONE544 T

DATE q 7

LOG NO .SAMPLE


q- 4y-83 Lox

ALFA I

PURITY ONLY OXY= BY VOLUME

TEST IzuN ~# 013

SAMPLER #

FL r106AQ 672

@ 9LM PSIG

RECEIVED :

SSCI Analytical ChemistryLABORATORY A WAGER

iimmuimiiiummiimi uunuuiu

CHEMICAL ANALYSIS

REPORT-0: EQUIPMEYf LAB

LOGNO -

43 -83To

598-;4 4DEPT./GROUP

PHONE 5447

DATE MAY /6 , /98j

LOG NO .SAMPLE

IDENTIFICATION+ 0 .3 mgRESULTS

TRICH for NVR per

RL10001- F

8~ ~ 3f3-4 -E'dR No . 5O3 B8 7

BLANK mg/500 ml

HARDWARE . O mg/50O ml

oL 3ro-XdC.A

r.4AJ k

EWR No .

BLANK m8/500 ml

HARM • ma/

EWR No .

BLANK mg/5

ARE mg/50o ml

COMMENTS :

kvl'APPROVED

!4X4A ER

Rec'd. 4 - 6 - 83

-~ . aG( 4SSFL Anal tlcol sml.try

IIDI muim i iiu mmiiuuuuiuiu u i


; - c a~ vr2. _ y ~ No. R5^388 7INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED( REQUESTED COMPLETION DAT E

YES NO

DOING D PT . LEDGER ACCOUNT C6NERAL ORDER G .O . ITEM & MCR INIT. GROUP HDW . OR TASK DOING GROUP ACTUAL COMPLETION DAT EE

REQUESTED BY EXT . FACILITY I SHIFT REQ . SUPERVISION ESTIMATOR ESTIMAT E

'~ fl2x

' I _ __ -_HOURS MATERIALSILs REQUIRED R EQUIRED

L P RVISION LEADMA NASSIGNED TO :

_MECHANIC

~

S

SHOP I I LAB

INSTRUCTIONS ( BE SPECIFIC) NOTE: THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

RECEIVED © LAB

APR 6198 3

SSFL ANALYTICAJ.. C4EMISTRYY .,_ "

FORM R R4 . L REV 6 .37

DATE

rc ik 6

LIST OF MATERIALS

II0I m u imi i iumm i im iBNA0147612 3

HDMSE00624397

LOG NO .

TO: QUALITY ASSURANCE

FROM : SSFL ANALYTICAL CMISTRY

REFERENCE : LOGBOOK PAGE h O

CHEMICAL ANALYSIS

REPORT- 'Vi-8.3

DEPT ./GROUP D/556

PHONE 5447

DATE;DR f 3

SAMPLELOG NO - IDENTIFICATION RESULTS

141+3 GAS : HEL /U"

REC'D :

SAMPLER : /=LOD G3d O

PRESSURE Pl1DO T/Q < I (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE ND = NONE DETECTED < = LESS THAN


COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

SS P-' IOTHER :

ARE -

COMMENTS : *Maximum allowable limit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2 , and 26 .3 ppm in N2 or 0

APPROVED AZI111

For- F,c_„

SSFL ANALYTICAL CHEMISTRY UK 'MANAGER

B NA01476124

HDMSE00624398

CHEMICAL ANALYSIS

REPORTTO : QUALITY ASSURANCE DEPT./ GROUP D/556

FROM : SSFL ANALYTICAL CHWISTRY

REFERENCE : LOGBOOK j ~3 PAGE 60

LOG NO .

y _ Z/o - 003

4

PHONE 544 7

DATE 0 4R a'3


GAS : N/'?ie0(~'E4/

RECD :

SAMPLER : /=1-4 O5 ' 9

PRESSURE GU00 ?5' ( ppm) TOTAL HYDROCARBONS AS CH4

ANALYSIS REQUESTED


AS METHANE ONLY

FROM :


A LFA BRAVO> = GREATER THAN DNA = DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

OTHER : 5 5 P~ .314 e :4 a


is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or 0

/ YAPPROVED

SSFL ANALYTICAL CHEY I ST R'!

BNA0147612 5

HDMSE00624399

CHEMICAL ANALYSIS

REPORT

LOG NO

y-38- 8,S

DEPT./GROUP 564

PHONE 5447

Logbook '853 pg. _ (Pb DATE 6 83

LOG NO-SAMPLE


H.3g 3 Westeveter, Canoga

Site L, D/544 Scrubber Chromixn - r4 g ~~ I LSump pH 7. qGrab Sample taken

yl(l833 0

Sample Receive d

) C -0 1Analyzed for pH, andchromium

SSFL ANALYTICAL CHEKISTRY UNIT

CHEMICAL ANALYSIS

REPORT

To. M . Mog g

FROM: SSFL ANALYTICAL CHEt( ISTRY UNI T

REFERENCE : Logbook ' -'~ pa, (o(D

LOG NO .

Y-3 -7 -83


Wastewater, Canoga

Site C, "Sea World "

24 nr . ProaortionRl

12P-01P o' n

y 15 I$3 -~ ~ lG fg~`X1

30 C% is

Sample received C(l1-/g-3

~--o SsSalyzed for copper, pnd nickel

RESULT S

Ccpper - D . i (p mg /L

Nickel - 3 . 2 rog/L

pN- ? . 2

COMMENTS : The L.A . City discharge limit for copper is 15 mg/l, for nickel the limit is12 mg/l .

Analyses per M .,Mogg 's_IL 81 F!4.22, 27 Oct . L98 1N .D. - None detected

APPROVED

rDL)f-J,A~

y~iFL ANALYTICAL CHIINISTRY UNIT

4BNA0147612 7

LOG N O

y- 3 -7 -83

DEPT./GROUP '4

PHONE sh1t7

DATE 618

HDMSE00624401

TO: =:


DElR/QilOl,iP 56`1

FIRIC F 3SVL AIMALYTICAL CIt 13T1<T UNI T

•f IVjMNCE : Logbook ' S3 pg . (,O

L.OONO-

y -3(o- ~;3

p}NONyE 5447

OATS

LOS NO-SAMPLS


y-3 {o 's Wastewater, Canoga Chromium = () .1 /'M5 ISite B , D/544 Process pH = "7, L/

Cla ri fier


sample

y/s/s3 -' 4IV73p 8/S

Sample received '1/6163

08 5Analyzed for pH, and

chromium

COMMENTS: The L.A . city discharge limit for chromium is 10 mg/L

Analyses per v . Ilogg's IL 81 FE-422, 27 Oct . 198 1

APPROVED

farm 619-V

SSTL ANALYTI CA L 0t 1ST1lY UNIT

I IBNA0147612 8

H D M S E00624402

CHEMICAL ANALYSI S

TO: EQTYrPMENT LAB

FROM : SSFL- ANALYTICAL CHx..''4ISTRY

REFERENCE : LB-a3 : P. C- C

REPORT

DEPT./C,ROUP

7 0

-3S -83

c ,14 ]y7PHON E

DATE APRIL (p 17 .53

LOG NO .SAMPL E

IDENTIFICATION

+ 0 .3 mgRESULTS -

TRICH for NM pe r

FL10001-F

E'dR No . 503 88 5

CaLANDl(

5 .3 9/500 ml

HARDWA.°E mg/5o0 ml

N/GrN BA Y

E'dR No . o388S

BLANK 2 . mg/500 ml

4-35-83 HARlYWAIRE mg/500 ml

ACl2 VAy

0 .

BLANK M-1

HARDWARE mg 500 ml

COMMENTS :

APPROVED ;~~i J-&XA,~

;MANAGER

598-34 4

Rec'd . 3

Anal)lticai Chemistr y

iimmuim i iiu mmiiuuuuiumiu

E NGINEERING WORK REQUES T

INSPECTION REQUIRE D

YES NO1 .`.'.

APPLICABLE DRAWINGS (AT7ACH IF RE Q

GENERAL ORDER G .O . ITEM S MCR I INIT . GROU PDOING UEPT LtDGER ACCOUN T

X12REQUESTED BY _

SUPERVISION

EXT . FACILITY SHIFT REQ . SUPERVISIO N

ASSIGNED TO :

SHOP 1 I LAB


LEADMAN

DAT E

HOW . OR TASK DOING GROUP

ESTIMATO R

MECHANIC

No . R5^388 5REQUESTED COMPLETION DAT E

/ /i/2 .ACTUAL COMPLETION DAT E

ESTIMATE

HOURS MATERIAL SREQUIRED REQUIRED

INOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

G J~O,4, G 2l d:k

~ _3~-g~9 cep

RECEIVED c LAB

6i 9- 3 ?

SSFL ANAL I L Ctit iSTR Y[ ?,y~~'~`~ a . wt

FORM R 9 4.L REV R .57

LIST OF MATERIAL S

BNA0147613 0

H D M S E00624404

CHEMICAL ANALYSI S

TO:

FROM :

A, /BORN

REPORTq-33-8 3

DEPT./GROUP 'S9g - 3 5~S


REFERENCE : L C4800t" 8-3 'p . <o C

PHONE

DATE /2 4PRIL 83

LOG NO .SAMPLE


4-33 -93 (;Ref' SvaSr'4AvCE / ~-r /V / A/FRq RE: O SCAN W45 MADE

OA/ D/APHRAfrM fRo 1

Rove REG ULAro ffl 01-' A SME4/Q OF THE I' G REE,V

vsi'rD Ar A- 3 A~' aR suasr,'wcE'; T1-IE M4J0 R 4,vscRpr/ON

1-lEL /UM SE'Pv /GE, BANZ75( 9Sc - /'400 CM-) AG, REED

FWR 49&1733WELL w/rH THOSE oG KRY7,rX AND

W/rH SPECr'RA SHOWiV IN R50/44O-022 ,

54MPLE REc/D

SAPRB~THE . /A PHf►'g4 M #n .O REM4/N/N4

/ lqREE/V SUBSTANGE~ WERE FaRwARDE D

ANALYSIS R~Q SIE C HEm /S rR Y AND 1 Y0N-ME7-A4LI C

~To

4REE NI~ENr/~y L.aaORaroR /ES~ .D/s39-/69, C4A'd 4

S'UBSTANC E ~~ ~FoR FLuoRESC~NT X-RAY SP~cTR -

G4APN/C AtVAi-Ys/s w/rM 57W 1-7-5

TO 8E RE PoRTE D , Y THAT LABORATORY ,

COMMENTS :

APPROVED

i or rn 619-V

SSFLANA TICAL CHEMISTRY UNI T

BNA0147613 1

LOG NO

HDMSE00624405

11% FockaWyne DIViBIOTTDATE Luni ., 4 .v ,

` c

REP! RENC E

k -REPORT NO

iRockwell International

1 9 i.: 7 ij14 9 f 2 4

PART NAME & NUMIE I

A 3 IS ',~+-'c iA ?n ZAC NlGUAM ITY

JMATERIALS & PROCESSES MATERIAL FICTION

ccAf'- i R ~lTEST REPORT i cWIMITTED By DEPAETMENT LOCATION PION !

A . HcRZti tom.

PURPOSE OF TEST

iJ7 > CA7-1 e ti ?✓ G C 1 M J /V

CHEMI CAL ANALYSISELEMENT

REQ'D.

OITAINED

TENSILE TESTS

LABORATORY TESTS AND RESULT S

SAM►t ENO .

YIRDSTRENGTH

Iat

ULTIMATELOAD

UII.

ULT%MAT!ST m4irM

ra

ELONGA-TION

7L

REDUCTIONOF AREA

R:

HARDNESSREMARK S

REQ'D.

OITAINED

OTHER TESTS

T r N c, cnTAn Ati' AS r,rv Alc °1'H 2 A H

vZ 2MA7cn (Ft-

, b,- rtr cal:

A5 -~ 5"F' G 4 J+(' 1) 1:5 L An'T

GF 5 v + + VJPiCH CC C 4 '5 Act C~ c ~7nil- [5 S~ x c.

NTH l gi-r ' ' fc 1~r t, )PAcY~~ N GK~ _ Fo~`rti i i

-7;41

cif 7_.r i

17j o951 3/c o

FORM R 70-U-1 REV . 3-73ul-d Doi.

B NA0147613 2

H D M S !00624406

ENGINEERING WORK REQUES TT T_E C F -C 0


YES NO

GS .A --APPLCA6LE DRAWI_NGS I

AT TA CH IF REQUIREDE

DOING DEPT . LEDGER ACCOUN T

REQUESTED B Y

LAB SUPERVISION

EXT . FACILIT Y

f/ASSIGNED TO :

SHOP 1 I LAB j


E DMA MECHANIC

No. R19173 3REQUESTED COMPLETION DATE

FACTUAL COMPLETION DAT E

ESTIMATE


S

NOTES THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

ILL E~ ~~ ANAL YZE SyeJ74,4/17 O 'V D1A~'i/k'A G M F ~~'!

A G A7 2 2 17,7-

14-3, 1-'1j" L j t (/Z- ~uG'r7,rr, r 10f41"

LSE ,ey~TO (K o 14v-) AAIV Uc%<< , /~~

R[ !'D k' 7 /l'C I ~L 75 i0 f L . j 4A14'1 h'/,C-W

Z- 0G No, `7/- 39 3m 619

LIST OF MATERIAL S

FORM R 94 .L REV 6-57

BNA0147613 3

GENERAL ORDER G .O . ITEM & MCR NIT GROUP

DATE

HOW OR TASK DOING GROU P

SHIFT RED. SUPERVISION ESTIMATOR

HDMSE00624407

SP TRUM NO .

~ . 4G g3

\MP 1 .E___ 4 -3 3 -Y -S

SPEED __..cm-' / min .

Dw~'; 2- SEC

TH

3 000

7 0

30

20

1 OCR

I III IIII II III I

ENGINEERING WORK REQUES T1 TITLE Or _OE I

INSPECTION REQUIREDAPPLICABLE DRAWINGS (ATTACH IF REOU'RED ,

YES ! NO KDOING DEPT I LEDGER ACCOUNT

5

REQUESTED BY ! EXT .

~iZ C,oC-LAB SUPERVISION

GENERAL ORDE R

06 az

G .O . ITEM & MCR INIT (;ROUP MOW . OR TAS K

FACILITY SHIFT

55ÀSSIGNED TO :

SHOP . i LAB

RED . SUPERVISIO N

LEADMAN

ESTIMATOR

MECHANIC

GATE

DOING GROUP

No.R 4LOo4 bREQUESTED COMPLETION DAT E

L -ig-x`3 3ACTUAL COMPLETION DAT E

ESTIMATE

HOURS MATERIALSREQU IRED REQUIRED

S

INSTRUCTIONS BE SPECIFIC ) NOTE : THIS FORM WILL BE USED FOR NON - DELIVERABLE ARTICLES ONLY .

AC--;?LI C A [3 LL i rc ~12~(o y 7

C~•`TC L ( . .-t2 (l~ V fZ ti.~ < .. ` - L (0 v c.~ tl ©C - "C I Lc - -j} . a c- c-!

Iv,~L ca T~+r- 'J F= G=`v5!_I ~~ Co IL 5L2A L

cL 77A = , I Lt 3 ~+Z

C 14 -•~ L C?~ ~7 C- s p£

P13 Soo- C

4- 7-13

RECEIVED @ LA B

SSFL ANALYi I L L c- i-L : 4; yEy

551Z .JoLIST OF MATERIAL S

FORM R 94-L REV . •-57

I III II I I I I I III IBNA0147613 5

HDMSE00624409

LOG NO .


TO : QUALITY ASSURANCE DEPT / GROUP D%6

FROM : SSFL ANALYTICAL CH ..ISTRY

REFERENCE : LOGBOOK )k3 PAGE

4/ - -'7- 0':2 -8 3

PHONE 544 7

DATE JS ,4P C 2 3


GAS : //EL/ 1)4

RECD : /y

SAMPLER : F Lb0632o

PRESSURE 1 950 PS/(~ TiQ / (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

FRO&' :

SSFL SUPPLY LINETR = TRACE ND = NONE DETECTED ( = LESS THA N


COCA DELTA

CPL-3 CTL-4

CPL-5 DELIVERY

TANK NO .

TRAILE R

OTHER : S P -/ ZE". L


is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or O2

APPROVED

Fr"' F Ic-u

/ k

SSFL ANALYTICAL CHEMISTRY UN I

B NA0147613 6

H D M S E00624410

LOG NO .


o: QUALITY ASSURANCE DEPT. (GROUP D/556

FROM : SSFL ANALYTICAL CRII~iISTRY

REFERENCE : LOGBOOK , PAGE G8

LOG NO .

COMMENTS :

APPROVED


GAS : N/T/QCGE N

RECD : /4 /4,Ie,/SAMPLER : Ftb05_fr_1

PRESSURE /5'50 RS/C,

ANALYSIS REQUESTED


AS METHANE ONLY

FROM :

SSFL SUPPLY LINE

ALFA BRAVO

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER _

-OTHER :________

RESULTS

N.]). < / (ppm) TOTAL HYDROCARBONS AS CH 4

TR = TRACE ND = NONE DETECTED < = LESS THAN

= GREATER THAN DNA = DOES NOT APPLY

*Maximum allowable limit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume , for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or 0

Form 619-U

/G L%SSFL ANALYTICAL CHEMISTRY UN

IIOI m u imi i iumm i im i ID ID DBNA0147613 7

PHONE 594 7

DATE' '4f', 8

i u I IH D M S E00624411

CHEMICAL ANALYSIS

REPORTQualm Assurance DEPT . /GROtW :

FA+GE : SSFL A3 LYTICAL CeEMISTRY L+80RATORY

REFERENCE : Logbook - 1 3 Page - 1 1

LDC Nt7 1ER :

PHO11E • 5447

DATE : t\ lay 2. , 118 3

SAMPLELOG 110 . IDSIQTIFICATIO1 R 1JLTS

~QAS : (r 4i. PURITY = D.N.A . % D .N.A . By Difference

4-4r4-83 RECKIYSD : $!sif83 PARR s D.N.A . %

SA1lp'LaR : ~ ~ 0 0 s~Z$TMPURITLB 9

PRESSURE : t 1 o o I02 = D.N .A. S O2 • 4. G PPm

ANALYSIS REQQESTED : N2 = D .N .A. % s f _ pps

Of11[PL TE Ar = D.N .A. 5 Ar s D .N .A . PPm

PRCIAL For AD ND .N.A . S Co .. . PP+aO~ and N2 Only . :00 D N A a% C0 D.N .A . PPm2 . . . 2

t4 - D .N .A . 5 t54 • D .N .A . PPm

FROM : C2H2 = D .N .A . % 0282 = D.N .A . PPm

SSFL SUPPLY LINE 82 • D .N.A . S H2 = D.N .A . ppm

ALFA

BRAVO D .N . A . (pppm) Total Hydrocarbons as C84

DELTA

COCA $0ISTURE = D.N.A . ppm H2O ( D .N.A . of DEW POINT)

CTL #3

CTL #4

CTL #5

TANK 110 .

DELIVERY

TRAILERTr - Trace

OTfLER

c - Less Than- Greater Than

A' 3 dN .D . - None Detecte

ZK e.'

. D .N .A, - Does Not Apply

LABORATORY IIMI4GER SSFL ANALYTI CA L a MlSTRY


556

I IH D M S E00624412

LOO NO

CHEMICAL ANALYSIS k - y t2-S3 =REPORT y - L 13 - g 3

To: R L E 0 N !R_._D_ DEPT. /eROUP S b/ i y y

FROM SSFL ANALYTICAL CIiD[ISTRY WIlT PHON E

REFERENCE : = O~ S~ P Ln DATE - - O 1

LOG NO.SAMPLE


4 _ Lr i 2- g Well Water from E .L.~7

pH 1 , S Fluoride _ mg/L

L{ - 3' Well Water after pH 7. (c Fluoride__________ mg/ L

flushing tank

E .W .R .# 504160

Received SSF L

y / 29/x.3

COMMENTS :

APPROVED

corm 619-V

SSFL AM ► LYTIGL cH ISTRY UNI T

II0I m u imi i iumm i im i ID IDD I D IBNA01476139

UH D M S E00624413


TO ~

FROM :

L . k


REFERENCE 1.S 43- 7G

PHONE s ~~ 7

DATE

LOG NO •SAMPLE

IDENTIFICATION RESULTS jy V,1 '4c

4- yO~ - QS (. °M~ lSf O N

YS f'k o,►1 t L ~s~~,ri Nz - Tk .ct r7. Sw- ~roq-g3

t- itf0 U

J!POWN h , 1"! S 1e

CUz

RUN . 3 ! A~~o = J ,

Tcx ~co S*wf,+; x

M 'A N2~l zY~ Y3

-+- c o = 1 . 9

IVD~ ~ s NO, = Tw-e L o, Oo r '/o

V6,

SOx ~$ 5O3

R c s !~

y/~yjS2

1 tCOMMENTS : Icet L Se f04 ~u~ f< K

APPROVED

Cn . ~1O-v

Norma Fdikdw. ManagerSSFL Aili1utkal Ckerni ?ru

LOGNO •

4- sic?-

t- 9-10- t

L SDEPT./GROUP 32f -/

c* R t s {I (f s w -t ~* N e w fn n (1 : cs

i 1 . c ./i

SSFL ANALYTICAL CHE1dISTRY UNI T

IIOI m Ii l u i I i Iumm i Iuumm II u U

LOG NO .



FROM : SSFL ANALYTICAL CESI~!ISTRY

REFERENCE : LOGBOOK ~.~ PAGE 7

4 . 4//-8 3DEPT.JGROUP D/556

PHONE 5447

DATE


y-yll-~s3 GAS : C____

RECD : / 2.S / 83

sA~ PLSR : F~.[~1528g

PRESSURE / 6S0 N . .() 1 (ppm) TOTAL HYDROCARBONS AS C;I1 4

AAIALYSIS REQUESTED


AS METHANE ONLY

FRC* :

SSFL SUPPLY LINETR = TRACE ND = M)NE DETECTED < = LESS THAN

ALFA BRAVO= GREATER THAN DNA = DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER __________

OTHER : PC cig ►4, l;3

COMMENTS : *Yaximu:. allowable limit per HAD 615-072 for total hydrocarbons as methan e

is 5 ppm by volume , for moisture is 9 ppm in He or H2 , and 26 .3 ppm in N2 or 02 .

APPROVED

FCrr' 614-vSSFL ANALYTICAL CHD ISTRY LNI T

IIOI m u imi i iumm i im i ID 0BNA01476141

UH D M S E00624415

CHEMICAL ANALYSIS

REPORT598

DEPT./GROUP

LOG N O

4-407-83

PHONE 3293

DATE5'2'83

LOG NO.SAMPLE


4-407-83 Hydrogen peroxide H2O2 = 89 .4% by weight

sample fro*i CWLL

Received ; 4/29/83

SSF)G Ji ALyTICM OJ 1STBY tJlI IT

IIDI muim i iiu mmiiuu m m mi iu

SS 11

LOG NO •

T,O : M. Mogg

FROM

CHEMICAL ANALYSIS

REPORT

DEPT./ GROUP 56Ii


REFERENCE : Logbook "$~ )g• -1

PHONE __

DATE di' ~` S~

LOG NO .SAMPLE


Waatevater, Canoga

Site L, D/544 Scrubber M 9 /LCTiromium • 1 $OSump !

I

pH ~.to

Grab Sample taken

ylzg f 3O ?3c '

Sanplee Received t1~z4//~~alysed

for pH, andA nchroni t

COMMENTS : The limit for Site L is 75 ~g/1 .

APPROVED

r ~ . .w F,iQ-V

k'fSSFL ANALYTICAL CHEMISTRY UNI T

IIOI m u imi i iumm iiuumi III DIDI i

LOO N0 •


X. Hogg DEPT./oROUP 5 6

SSFL ANALYTICAL QIAQSTRY UNI T

R'EFERENGf Logbook ' g3 D . ) "

LOCI NO .SAMPLE


3-L{Q53 Waeteveter , Canoga Dapper - 0 . yS a.g/L

Site C, "Sea World" Nickel - 2 . 2 mg/L

~- 8 . ILL ur . Provort <.cnal!-l. t" '

y/zgf~ 3 - 9jzqf073~

ecpLe re ce i vea è/~~y/& 3r

ria1yed for copper, pEnd nickel

COMMENTS : The L.A . City diecharge lisp for copper is 15 mg/1, for nickel the licit i s

12 / 1 .Arelyeea per H . Hogg'a1I .t. - lone detecte d

APPROVED

PHONE _ bh7

SSFL ANALYTI CAL C2i8lISTYY ai r

II0I m u imi i iumm i im i 001000 I IB NA01476144

H D M S E00624418

LOe NO


V nag70 M .

____ UFL AMLTTIC►L QL ISTIT UNIT

• Logbook ' ~3 pg .- tP

ovTlo+~oua'

g-vov-s3r►40NE 5447

DATE ___ 3__Z

/ NO •!

LO

•AMPLZIDENTIFICATION

'NE$ULTS

,~,3-1O 'Cano aJa tewater Chromium s 0 . /5 nn cJ /Lg,s

Site B , D/544 Process pH = ~p 5

Clarifier


sample

y/~~83

SaRple received " i1 Z

Analysed for p$, and

chroa1 tsm

CO$4MENTS: The L .A . city disctarge lisp for chromiua 1s 10 .g/L

Analyses per 11 . Yogg's IL 81 PE-422, 27 Oct . 198 1

Ada Q.GtrA.~w-L LMIZTICAL Q4 TSTRT IT


H D M S E00624419

:t:S . c P+t. . /sq s, ss I i)MICALcc : R . Schmued

M . Francis

M . Mogg

D/564, FB 66

CHEANALYSISREPORT

TO : (t A N T J E R V 1 C ES DEPT./ GROUP: D703 1

FROM : S S FL ANALYT ICAL CBRi[I STRtY

REFERENCE we BiC '83 PAGZ 70

LAG NO

4 ..402-8 3

PHONE 544 7

DATE 9 -M4 Y-d'3

LOG NO .S.MFPLE

IDENTIFICATION © PURLR; & TRAP O GC/1R3 RffiULTS (PPl1 )

Water sample fro, the Using the concentration techniques and methods ap-

_ proved under the guidelines stated in the currentpond at SSTL NPDRS permit , the f of losing VOIAT I Li ORGAAI C

CCiD"OUNDSS were f amd :RocketdTne .

A D 2cetone (C83COC83) = .

Freeboard = / • S ft Broaiodichloromethane (BrC8G12 ) = D <, Dof

S l d ! 84S AMCarbon Tetrachloride (CCl4) = IV!)4 1

amp eChloroform (CHC13) = 0.00! ,

IB ! f ;L

Methylene Chloride (CE2C12) = ND<, D Oy : . l 0 1S

1,1,l-Trichloroethane (c . l3) = 0 0

R2CEIV A IAB : Trichloroethylene (cl( :Cc12) fp.0734 / 29 / 8 3 Tetrschloroethylene (C12C:CC12) _ _ < Qp

1,2-Dichloroethylene (C1( :CBC1) = 0.02.Notation about appear-

OO r7~ance of the sam ple : .Dibromochloromethane ( Cl4 r2 ) =

Isopropyl Alcohol ; also (CR3C8 )HCR3) = 0 . / 8known as IPA ; 2-propanol

Freon TF (C12FCCF2C1) = Q. I q

l,l-Dichloroethane (C12CEC83) _ 0. 00 !

CObMENTS : Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifi-

cally required according to the Rocketdyne NPDES permit, Order W 76-146 , NPDBS 0 CA0001309

from the California Regional Water Quality Control Board, Los Angeles Region .

(2) This supplementary information is provided in accordance with 40 CFR 122 .60.

IIOI m u imi i iumm i im i DI DB NA01476146

I IH D M S E00624420

~. Fi5C K Pe r/ 5, 8 ._ .., 1cc : I . S chaued

M . FrancisK . Mogg

D/564, TB 66

CHEMICALANALYSI S

REPORTo: PLANT SER\ICES

FROM: S S FL ANALYTICAL CH 1 STBY

REFERENCE : LOG Bg _' S 3 PAGE 6

DEPT /GROUP: D/031

4-1o1-g3

PHONE 544 7

DATE 9-HA Y- r3

LOG NO-SAMPLE

I DENT IfICAT10N PflRfa$ a TBAP O GC/118 RBSOLTS (p )

Water sample frog the Using the concentration techniques and .ethods ap-

'4-4a1'83SI -

proved under the guidelines stated in the currentpond at SSFL RPDES permit, the following VOLATILE ORGANI C

were found :Rocket dyne

A 0 3 1cetone (CB3C~3) = .

Freeboard = _0 ft Bro dichloroeethane (BrC Cl2 ) = N)< .c),

QSaapled 0 04SAM

Carbon Tetrachloride (CC14 ) = ND< .D0 (

4/2 9 /8 3Chloroform (C8cl3 ) = 0 .00 I

// ))B L ~v ~~

Kethylene Chloride (C82 C12) = ND< .Do /y : . tTSl

1,1,1-Trichloroethaae (CB3CCl3) = 0. / 0

RECEIVE 0 LAB : Trichloroethylena (C1( :CC12 ) = ~. 038

4 / 1 / S3 Tetrachloroethylena (C1 C :a 12 ) _ NL)4 Gel

1,2-Dichloroethylene (C1 CB :®Cl) = Q . 0 16Notation about appear-

ance of the sample : Dlbrosochloromethane (C1CBBr2 ) = 0.00 1

Isopropyl Alcohol ; also ( C83CBC►6( 3) = o. 2 5known as IPA ; 2-propanol

Freon TI (C1 .2FCCF2C1) = 0. 6 71,1-Dichloroethana (C123) 0.00 3

CO6WSTTfS : Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifi-

cally required according to the Rocket dyne NPDES permit, Order # 76-146, KPDES $ CA 0001309

from the California Regional Rater Quality Control Board, Los Angeles Region .

(2) This supplementary information is provided in accordance with 40 CFR 122.60 .

= LESS THAN

PPS[ = PARTS PER MILLION

ND = BONE DETECTED / DRiA = DOES NOT APPLY TR = TRACE


I I IH D M S E00624421

55h

CHEMICAL ANALYSIS

REPORT

UG N O

DEPT. /GROUP 5 0-3-344

?ih7PHONE ~._._.

DATE 1 2' L 8~

LOG NO .SAMPLE

IDENTIFICATION+ 0 .3 mgRESULTS

TRICH for NVR pe r

RL10001-F

EWR No . q1242 7

BLANK mg/500 ml

ARDWA I0• 65 mg/500 ml

1 .t~t fT' L

E! ,TR No .

BLANK • mg/500 ml


EWR No .

BLANK • m /500 ml

HARDWARE mr;/500 ml

Recd .

1g05

SSF L Analytical Chemistry

E

c . 'L-k~LOGNO


Po-rD k DEPT./4i1lO P

S$?L ANALYTIa+ 1L OiDQ$TRY UItI T

REFERENCE : IOG BB{ PA,

U

4- 3q- g 3

PHONE 3447

DATE I~ atn 5; 19 8

LOG NOsAMPt.E

IDfNT~F1CAT10N RESULTS (by •eight )

1rTO lroa STL - 4, DENSITY . . . . . . . . . . . . ~ga/mi at 60° P

N O4 . . . . . . . . . . . . . . .

B20 . . . . . . . . . . . . . . . . ~.a , ai_ SC1 . . . . . . . . . . . . . . . . . OO 7

AAALYSIS PSR Fe4 _ 1 . 1^~'SPECIFICATION :

Yi1-P-265390Al*

" '. . . . O, 1 2. . . . . . . ~m~l~

?ZCE IVED ! LAtB :

y i .2g ,~3

COMMENTS : Ia A DOES JOT APPLY &= LpS S rl~an

* This analysis la not tscluded is 1tiI-P-26 533C .

APPROVED

iimm u imi i iumm i im i 0 I DI I IBNA0147614 9

H D M S E00624423

ENGINEERING WORK REQUESTr--TI T~E OF

M D ENo R 4 9 7 4 2 7IC

U' • AV C G A/ _-....._....__._ 1~ .INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED) REQUESTED COMPLETION DAT E

YES NO

DOING DEPT LED ;ER ACCOU NT GENERAL ORDER GO ITEM 6 MCR INIT . GROUP HDW OR TASK DOING GROUP ACTUAL COMPLETION DAT E

E ST E DB YR EQU FACILITY SHIFT REQ . SUPERVISIO NEXT . ESTIMATOR ESTIMAT E

AJ ///'

/II /

REQ UIRED REQUIRE DLAB SUPERVISION

ASSIGNED TOLEADMAN MECHANIC $

SHOP li I LA B

INSTRUCTIONS IBE SPECIFIC ) NOTE ' THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLE S

[r~✓;~ # 4 97167ONL Y

of A( r& 7V (Fl U/l. /Z 9tl2

T ~s~L /, l 4 1' 7

NARoWA 47[G'L A,i

my

RECEIVED @ LA B

2 819 3

SSFL ANALYTIC A CHEMISTRYBY

1/ r__"/

2

FDFV P

T C= O4TtRIALS

2

BNA0147615 0

H D M S E00624424

TO

FROM


DEPT. /GROUP ~.. 5

SSFL ANALYTICAL ChEMISTRY UNI T

-1 LiREFERENCELogbook ' pg•

LOG N O

y 3 Y-83

PHONE __

DATE _ __ s ~LOG NO .


Neateveter , Canoga

I9 OSite L, D/5 ► Scrubber Qiroeiium -Sump pH - (p .7

Grab Sample taken

RcceisedSample ,Q~l ~ Ilyred for pH, and

chroainm

COMMENTS :

APPROVED

1 orrr 619-V

The LLmit for Site L is 7j r~g/1 .

SSFL ANALYTICAL QiEISTRY UNI T

IIOI m u imi i iumm iimi immiiu

CLOG NO .

M_Mo~gg

Fll'OM~


DEPT/GROUP

SSFL ANAL'(TIGL QL IISTRY UNI T

REFERENCf~ Logbook ' g)3oar.

LOG NO .SAMPLE


-3- Waetevater , Canoga copper N, a~~•~~- mg/L

Site C, "Sea World" Rickel J,tp rug/L

- 8 .cam21 ~r . Provortione 1

s pLe re ceived L1/f /'L1 (

alyzed for copper, pEnd nickel

COMMENTS : '"Fe L.A . City discharge 1 :Q.it for per !s 15 mJ1, for nickel the halt is

12 mg/1 .Aria lysea per M. Mogg's IL E1 R422, 27 Oct . 1981

N .D. - lone tested

APQROVED

y 383 -&~

PHONE 57

DATE '-3

SSFL ANALYTICAL o{WSTYY LIT

IIOI m u imi i iumm i im i ID OVID O I IB NA0147615 2

H D M S E00624426

r


ro: uep~ OtRT./dwou~ 564.

P"OA~ SSFL AULYTIGAL Q1ifIISTH ZA 1T

REPEREWCE : Logbook ' p3 pg

V • 382•&3

~lCawc 544?

DATE __` yL~ _

r

Loa NO .$AMPL*


Wa9tewater , Canoga chromi i = 0, 3, r&/(.. ..

Site B, D/544 Process pH =Clarifier


sampl e

.//?/s3 ? /2 S/

ceivedam le rep


chromium

COMMENTSc The L .A . city discharge 11$t for chraaium is 10 sg,Z

Analyses per W . Nogg 's L Si PE-422, 27 Oct . 1981

PPyeOvCD

r,rrr ate-v

$SlL AJA LyTIcAL OiDlI$TRT Q>!tI T

II0I m u imi i iumm i im i ID 101000 I IBNA0147615 3

H D M S E00624427

cc : 1 . Sch~ue d. Franci D/56, FB 66Y s

Y . Yoe;

TO: ilOC~TDYNE PLAT s V1 Cu

FilC)M SSFL AIiALYT I CAL CS ~ I STR Y

LOG 8 3 p 74


DEPT /GROUP D/031

LOG NO .

4-375-83

PHONE 5447

DATE - MAY-83

L06 MO.8~►b1PLE

DENTliIC: ATlOfJii Q pt k TRAP O Gc, s RESULTS (PPM )

Water sassple fros the aline the concentration techniques and aethods ap -

q- 375- 83 PP retaantion pond at proved smdar the eui6eliaea stated in the curran tRockatdyDe . 857I. 1fPDbS permit , the Soilowtng V0 AT1LB OICA1(I C

Freeboard = ftOCKP~Ot1 1 D6 were f oamd :

_ ____

Sp Acetone (C$3CDC83 ) _ C, CS 2s::pl.d e $ AN

2 $ f 8 3Rroaodichloroaethane (Brt~C12) = ND' . 00 /

~

fn sB !

Carbon Tetrachloride (CCl4) _ j .W '.00/

y : r • _chiorofor► ( 2C13 ) _ 0 .00 1

RE EIV~ 0 LAB : ttethylane chloride (CIIZCI2 ) ND'. DO H

4 / Zg / S~ 1,1,1-firi ch1oroethane (CS3C13 ) = N~' .0O I

Trichioroethylene (CIC~ : CC12) U. f)D 1

Notation about appear-

ance of the sasiple : Tetrachloroethylene (C12C : CC12 ) = N~ x .00

1,2-Dichloroethy lane (Cl (8 :C$C1) _ 0.002

Dlbromochloronethane (C1r2) = ND ( 0o f

Isopropyl Alcohol ; also ( CS3C~OHC~3 ) = TR .O/known as IPA ; 2-propanol

Freon TF (C12?ccP2C1 ) ND'.00/

1,1-Dichioroethene (C12(BC83 ) a _1D<,CJO/

O ENTS : Tetrachioroethylene is also kturwa as perchloroethylene . ( 1) Monitoring specifical-

ly required according to the Rocketdyne NPDES permit , Order a~ 76-146, NPDES a CA0001309 from

the California Regional water Quality Control Board, Los Angeles Region . (2) This supple-

mentary information is provided in aecordence with L40 CFR 122 .60 .

- LESS THAN

APPROVE D

f . r,, 619-V

P'PB = PARTS PER M I L L I ON

ND = !NE DETECT') rzA = DOES ) T APPLY

MANAGE

TR = TRA C3

1LILSTRY T

IIOI m u imi i iumm i im i ID I VOID D I IB NA01476154

H D M S E00624428

cc : _ . SchstuedY . Francis D/56k, TB 66

>r . jogs

CHEMICALANALYSIS

REPORT

TC1 : iEOCSETDY2 Z PLA?FT S VI CPS

l4lOw- S S F1. A1(AL7? I CAL Cffi1[I STRT

► : loc BIS S 3 PAGE 71

DEPT./GROUP D/031

LOG NO

4-374-8 3

~~~ONE 5447

CATS - H14 83

LOG NO .S.AA4P'LE

I 'CENT I } IC ATIQ~IV P[fBGL i TRAP O GC i S RESULTS ( PPM)~

eater saaple froe the Using the cancaestration techniques and methods ap-

_374-83 R2 retention pond at proved corder the guidelines stated in the curren tSocketdyne . SSPL aPil!!8 permit, t1 following VOLATIIL OBGAI'I C

5CC~OiTiG16 wr. fo®d :

ftFreeboerd = 1.Acetone (Cfl3COCH3) _ 0 . 0 g0

Saepl.d o S API/2 _ / Broeodichloroeetlune ( BrC~C12 ) _ D', 00 !

C o 1I I1 sLCarbm Tetrachloride (CCl4) = /JD . OD /

.By :Chlorofora (®C13) = 0, OD 1

BEC~YID • LAB :Illethyl.ne Chloride (CH3Cl2) ND <, DD /

4 ,2g / 83l,l,l- riahloroethan. (CS3CC13 ) j1 < DO /

Notations about appear- Trichloroethyleae (C1CS:CC12) _ 0. 0 / /

anee of the sasple :

Tetr.chloroethylene ( C12C :CC12 ) = ND' . 00 /

1 ,2-Di chloroethyl.ae (ClCS :®Cl) - 0.02 0

Dibroeochlorowethane (ClCBBr2) _ TR <.00 /

Isopropyl Alcohol ; also (C83C~8CB3 ) = 0 .01 0losovn as IPA ; 2-propanol

Freon TP (C12FCCF2C1) = ND < . OO lN

1,1-Dichloroethane ( C22CHC83 ) _ ID ( 00 /

Cfl10~NTS : Tetrachloroethylene is also known as perchloroethylene . ( 1) Monitoring speciiical_

required according to the Rockstdyne NPDFS permit , Order W 76-146, NPDSS # CA0001309 from the

Californi ■ Regional Water Quality Control Board , Los Angeles Region . (2) This supple-

mentary infornetion is provided in accordance with ho CYR 122 .60 .

PPM - PASTS P86 MI LLI ON

- 1 S THAN xD - t DrTsCTSq 18IA - DOffi' POT APPLY

APPflovED

F ,arm (=1 $-VNorwa Fu wa , Ma' ape ►SSPL .4na of CAemutry

TR - TRACE

~ •

SSPL A ICAAL~ STRY UNIT


I IH D M S E00624429

cc : P. L 1 .inaaith D/768, 1040

1 . Schauwd

M . Prancia D/564, TD 66M . MOR

PPM = PARTS PSR MILLION

ND = 1(Z aSrBf'TZD , t (A = DOES 1IOT APPLY

Tc BaC DYza PLANT 3EYwICS8

-r SSFL ANALYTI CAL Th13T1Y

L4G S 3 PACE 79

DEPT./GROUP D/03 1

06 NO .LSAMPLE

1DENT ) fICA1T10N ESULTS ( PPM )Paso s. TAP O GC/NS

later ample frog the Vaj g the coao.atratiao tedxaiques and aethoda ap-

•373-83 AI Inlet to the BZ proved s~ader the guidelines stated In the current Jrrtention pond at 98FL P perch, the follv.ing VOLATILZ A. IC

socketdya. . Cd6~dIDm5 rare Sound :

Aostaa. ((S3CaC83) = 0,1 2p

saapl .d . D °A M Braodiehloraethsa. (8r12) = 0 1

28 g3 Carbm Tetrachloride (CC14) 0<, DD

By: L Chlorofos'a (CHC13 ) _ 0. 037 LMethylea. Q1orids (C$~CiZ ) = ND~ .OO I

BECSIVTSD • LAB :/U

i8

~T

l,l,l-rrirbloroethaae ( CS3CC13) _ 0.00

Trichloroethylene (C1CS : CC12) _ 0, d / Z

Notation abort appear- T.trachloroethylsne ( C12C:Ct12) _ /10'.00 1ante of the sample :

1,2-Dih1oro.tby1.n. (C1Q :CSC1 ) = A1L . DO l

Dibro.oc .loroa.th.n. (c1c Br2) = D. P46

Isopropyl Alcohol ; also (CS3CA38CS3) _ ND 1 . 0 lkaowa as IPA ; 2-propaao1

Fran TF (C12FCCF2C1) _ / 10 '.00 1

1,1-Dichloroethane (d12CHC83) = N ~ ~ ~'

C010iKNTS : Tetrachloro.thyl.a. is also kaowa as perchloroethyleae . ( 1) Monitoring specifical-

ly r.quir.d according to the Bocketdyae IzFDES p .rmit , Order t 76-146, NPQLS # CA0001309 fros

the Ca lifornia 8egioa.al later Quality Control Board , Los Angeles Region . (2) This supple-

mentary information is provided in accordance with 40 CFR 122 .60 .

= LS THAN

APPROVED

CHEMICALANALYSIS

REPORT

GLc.I't7~--'~'~Manager

SSFL Awaytal CAsm4h yNor+wo

PHONE 5441

DATE 6 - _ Y-_ 3

TR = TRACE

SSFL ANAL ICAAL- STRY @(IT

IIOI m u imi i iumm i im iB NA01476156

I IHDMSE00624430


TO : R . L E O N A R DEPT ~aROU P

FROM SSFL ANALYTICAL Q{BYISTRY UNI T

REFERENCE : Lo Q 1? k

PHONE 5 y y 7

DATE

LOG NO.SAMPLE


4-3(~~- 83 D .I . Water from E .L . pH L . O Fluoride~~ e < 0 1 mg/L

4 3b'7 - D .I . Water after flush pH L4 Fluoride_________ mg/ L

tank

E .W,R .# 504160

Date Received A SSF L

COMMENTS :

S ; ±SSFL ANALYTICAL O1STHY UM T

IIDI m u imi i iumm iimi ini i im U


/ 5~TE

No R50416 0/~~~ ~g - - .INSPECTION Rr061RED

APPLICABLE RAW ] NGS (ATTACH IF REQUIRED) REQUESTED COMPLETI N DATE

YES NO

V Nloq-

O

3

DOING DEPT LEDGEft ACGO NT GENERAL ORDER G .O . tTEM S MGR yl I T . GROU P

55c ►_ 34OR TASK GROUP ACTUAL COMPLETION DATE

REQUESTED BY EXT . FACILITY SHIFT RE SUPERV ION I ESTIMATOR ESTIMAT E

M I C I 'j

HOURS MATERIALS_

(„934 REQUIRE DREQUIRE D

vLAB SUPERVISION

ASSIGNED TO :LEA A MECHANIC

$

SHOP I LA B

INSTRUCTIONS ( BE SPECIFIC) NOTE: THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

F4 r G <9~e'►,r(` p p ~,..

u coc ecC6 3 °1) (x q lqy cl

LIST OP MATERIALS

I IBNA0147615 8

H D M S E00624432

LOG NO

CHEMICAL ANALYS IS £t- 3 ct - g3

REPORT Y - 3! - P 3

J. 0 3 t w K~ DEPT.~GROUP S 1,-6

SSFL ANALYTICAL CH®MISTRY 'NI T

L IS '3-7C

PF$ON E c / 't 7

DATE 2 7 : 3

LOG NO .SAMPLE


4-3t-41 NTu s*up/r f. . .,

GRI,, ..,< «/tloYa ~o- ~ Sa,-gz Al ~ .~ ;,~ •~. = 0,0 3

(.«lV$ ;M ~oT s. st

/Sc*t{N ANN

622 i h 14 ( I)A4, 4v•' ,-a

q, s c

Nro srL( fh•M _

G, (,(*H.'' e I t

"_ D. ! c A.ylky

toy ii-/ S~f -Q z

/ i A, y '309( s . Ste t

{ C Ir t<N Ass! T;-,4 C- V 't r; A ~► l - s/: sc

/27/4 3

Norma Fuj' wa. Manage rSSFL Anat cal Chemistry

SSFL A LITIIAL CHEMISTRY UNI T

IIDI m u imi i iumm iimi iniuuuu

LOG NO .

CHEMICAL ANALYSIS

REPORT

QUALITY ASSLTRANCE

FROM ; SSFL ANALYTICAL C.Etl~'~.ISTRY

REFERENCE : WGHOOR c~3; PAGE

DEPT./GROUP D/556

y• 3 ;e3

PRONE 5447

3DATE g /Z , )&


GAS : G N zIl X03-

REC ' D : 'i /S3

SAMPLER : E.. Oo ~27 l

PRESSURE t °IDO (~~ D (pp.) TOTAL HYDROCARBONS AS CH 4

ANALYSI S RE~UESTEI)


AS METHANE ONLY

FROAS :

SSFL SUPPLY LINETR = TRACE ND = W)NE DETECTED G = LESS THAN

ALFA BRAVO \=GREATER THAN DNA =DOES NOT APPLY

COCA DELTA

CTL-3 CTL- 4

CTL-5 DELIVERY

TANK NC .

T RA I LER

OTHER : ~ P_~

COMMENTS *Waximu~ allowable limit per MO 615-072 for total hydrocarbons as methan e

is 5 ppe b} volume, for moisture is 9 pp. in He or H21 and 26 . 3 ppm in N2 or O2 .

APPROVED

SSFL ANLYT ICAL CKDIS':RY L

II0I m u imi i iumm i im i ID 01001 DD I IBNA0147616 0

H D M S E00624434

LOG NO .

CHEMICAL ANALYSIS

REPORT

TO : QUALITY ASSURANCE

FROM : SSFL ANALYTICAL CH~SISTRY

REFERENCE : LOGBOOK PAGE 7 L11

`l -362 ~3

DEPT./GROUP D!556

PHONE 5447

DATE ~ z 7 _


1' 3 02-D3GAS : ___ ltl M

RECD : LI ' t) ' 3

SAMPLER : FL Ord Z8 7

PRESSURE ZCX N (~, 1 (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

II

FROM :

S S FL SUPPLY U NETR = TRACE ND = NONE DETECTED G = LESS TRA M


COCA DELTA

CTL-3 CTL-4

4 CTL-5 DELIVER Y

iTANK NO .

TRAILER

`̀OTHER : SSP- t A QEA }

COMMEN?S *Maximum allowable limit per RAO 615-072 for total hydrocarbons as methan eis S ppr by volume, for moisture is 9 ppm in Be or H2 , and 26 .3 ppm in N2 or O2 .

APPR'=D

SS-L AMLYTICAL CfEIISTR 'i L :

IIOI m u imi i iumm i im i ID DI D ID D I IBNA0147616 1

HDMSE00624435


DEPT./GROI.JP 5b4

LOG NO .

y-3io-83

PHONE 5+14 7

Logbook ' $~pg. ? DATE _ S 3

LOG NO .SAMPLE


Westeweter, Canoga

U .. 3O 53 Site L, D/51►k Scrubber rOmium - / ,Q "is /i...Sump pH

,Grab Seaple taken

`/fr1/s3 O?3a

d 5/! L 783R il veecee

~y5

Ana d for pH, andchromium

LiSSFL AIiALYTIGL O{1STRY UNI T

r L Lk'.Y.~C .J~

7IIDI muim i iiu mmiiuuumum u i

TO~

l1~OM~

N. Nogg


DEPT / GROUP

SSFL ANALYTICAL OiDIISTRY UNIT

REFERENCE : - Logbook ' g 3 oR.

-359-83

E

DATE Q 7 1$3

LOCI NO .SAMPLE


L/ .. 359..3 Wastewater , Canoga Copper 0 . .) mg/L

Site C, " Sea World " .1--1 mg/LR1cke1 - 2

,Qpa ' V. 221. tr . p-~ovo-tonal .

!"-clP tpkt~

q/2 c / 7 v/Z7/83

~o?3c)

Le received y (2~~W S

aly .ed for copper, pE

nd nicke l

C:OMMEN(TS : The L.A . C ty dischargr t for capper is 15 m&/1,

12 mg/I .Ane .yses per N . Nagg 'I II. 61 7!422, 27 Oct . 1981

X.D. - )oae detected

APPROVED

for nickel the Itait i s

SSFL ANALYTICAL CStF .ISTRY tfhIT

IIOI m u imi i iumm i im i ID DI D IDD I IBNA0147616 3

HDMSE00624437

10: Y _ Woa e

!KONG


SSTL AMLYTIGL OL 1STIT U$1 T

REptRtNCE : Logbook '3 pg • 7 T

OLO

y-358 .83

P4ONE 5447

DATE

LOG HO.$AMPLZ

IDENTIFICATION RESU LTs

-3 3 Wastewater , Canoga Chromium - Q . 2.?. r3'~/L

7Site B, D/544 process p13 =

Clari fier

24 hr . proportiaoa l

sasple

L1/L24f /2?C3

Sasple received ~fZ~1

Analyted for p8, an d

chromium

COMMENTS. The L .A . city discharge liadt for chromium is 10 ag/L

Analcses per Y . Ko68 's IL 81 PE-422, 27 Oct . 198 1

APP Vta-

SS.TL AMLYTIC&L Q4.O 1ST*Y Q (I T

II0I m u imi i iumm i im i ID DIDDI DB NA01476164

I IHDMSE00624438


f &elDATE

z6 _,f, No. R49069 6INSPECTION REQUIRED

APPLIdABLE DRAWINGS ( ATTACH IF REQUIRED ) RFO STED COMPLETION DAT E

YES N C

DOING DEPT LEDGER ACCOUNT I GENERAL ORDER I G .O . ITEM S MCR INIT . GROUP HOW . OR TASK DOING GROUP ACTUAL COMPLETION DAT E

RE UESTEDD BY EXT . FACILITY SHIFT REQ. 1 N ESTIMATOR ESTIMAT EY€ ',i~.

, 17/~~L HOURS MATERIAL S

REQUIRED REQUIRE DLAB SUPERVLS ION

ASSIGNED TO :L M I MECHANIC S

SHOP I I LAB

INSTRUCTIONS ( BE SPECIFIC ) NOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

I A-'/f /_ / P_ ie /-It A./ / [f /", y/V L Ef ,

/ti .rraC_v cr'/a A.6r v r-= 4-+,0erZ y ~c~.t~+.tr✓ X ~/ 76 ,

S~~O /2 L-rU L-7T 7 a H// / I Z

c

F/ O /U2 8 ? /l ~5 /fir

At

~_3S1-g3A

4

=ORS/ F 4G _ F . 6 .!'

RECEWED @ LAB

V83

BY L A~~HEMiSTR Y

a

LIST OF MATERIALS

I IBNA0147616 5

HDMSE00624439

CI-IEMICAL ANALYSIS

REPORTTO : Quality .4ssurance DEPT . /GROUP :

YROM! : SSFL ANALYTICAL CHEMISTRY LABORATORY

REFERENCE : Logbook - 83 Page - 75

LOG NUMBER :

4L -357 -b'3

PHONE : M4 7

DATE : MAY 183

SAM PLELOG NO . IDEWTIFICATION RESULTS

9-35783 GS : HEL./VM PURITY = > 5 9 . __ % HEL1vM By Difference

RECEIVED :~77 ApR X83 PARA = -DN4

SAMPLER : FL4J0 R1' 7

PRESSURE : /900- pS/G-#IMPURITIE S

02 = P .)4 % Ar t02 r 5. a, ppmANALYSIS REQUESTED : N2 = N~ = 3o ppm

COMPLETE A r = °k Ar = W4 pp mSPECIAL :

CO = , co = tt.I>. f 5 Ppm

CO = °b CO ~ '= N• Oa g p m2 2 . P

CH = CH = )NA ppm4 4

FROM : C2H2 =% C2H2 =, ppm

SSFL SUPPLY LINE H2 = HZ = PPm

A LFA

BRAVO /(~• D, < / (ppm) Total Hydrocarbons as CH4

DELTA

COCA MOISTURE = C .5 ppm H2O ( _ °F DEti' 1 )INT )

CTL #3

CTL # 4

CFL #5

TANK NO .

DELIVERY

TRAILER Tr Trace

OgR ~"~vrcl2 ~/OCtrc = Less Tha n> = Greater Tha n

R4NEL 7'LF N .D . = None DetectedCELL- 1 D .N.A . = Does Not Apply

COl MENTS :

APP4tO~ED :-

DA TOY

556

SSF'_ ANALX.IC.AL C'YL'•' .=-R Y

II0I m u imi i iumm i im i ID DIDD I IB NA01476166

UH D M S E00624440

TO:

FROM :


L . Forman


REFERENCE Logbook ' 83, p . 74 5/2/8 3

LOG NO.SAMPLE


4-351-83 Freon 14 sample . See infrared spectra attached .

EWR # 490696Entire spectrum from 2 .5 to 15 microns i s

Sampler # FL 010288available upon request . The portion included

850 psig with this report is consistant with the reques t

submitted .

Received : 4,27 / 8 3

COMMENTS :

APPROVED

form 619-V

4-351-83

r

DEPT. /GROUP631 SS 11

LOG N0 •

PHONE 3293

DAT E

SSFL(AIILYTIGL C IISTRY UNI T

IIDI m u imi i iumm i im i lID DID DBNA0147616 7

This report supplements the one issued on 4/28/83 .

I I IH D M S E00624441

3

SPECTRUM NO .

DAT E

SAMPLE

I¢ CFA

SOURCE _ _

STRUCTURE100

PATHK6r (ms CE C .

SOLVENT

CONC . _ I_~_ ►titwt _-tt

PHASE (S _

COMMENTS

47- so r-k

ANALYST

SPEED 0O --cm-1/min.

GAIN

PERIO D

'T WIDTH ______~•_ ___ mm

4 3ooo cm_,

Sego sup. 2

I'D

}

I

U GRAPHIC CONTROLS CORP . 00 3200 3000 2800 2600 2400CP (`TC?nDWnTnNA CTCrl

BNA0147616 8

H D M S E00624442

SPECTRUM NO .

DATE

SAMPL E

SOURCE

STRUCTUR E00

PATH -4x=*w'mm

<190-

SOLVENT _---_ _

CONC. O_IPAA SSUAS

PHASE a/!-

&ECK k21o 7 •

ANALYST_

SPEED 3DO _ cm-' / min .

GAIN W4

PERIOD _ SEC .

T WIDTH _0 -3

c m-'

3 . 5I

4

gEns SAP. . 2. ;{ t

2 GRAPHIC CONTROLS CORP. )0 3200 3000 2800 2600 %no

BNA0147616 9

H D M S E00624443

Cc : L .2 inA~

LOG N0 •


4-351-83

TO : R . Yea man DEP T./GROUP598 SS 1 1

FROMSSFL A NA LYTI CAL C HEM I STRY UN I T

REFERENCE

PHONE 3293

Logbook X83, p . 74DATE

4/28/83

LOG NO .SAMPLE


4-351-83 Freon 14 sample . Water was determined on the sample by dew point ,

EWR # 490696 and was found to he 200 ppm by volume .

Sampler # FL 010288 (dew point of -Dc-} fr8850 psig - 32°F.

The sample was analyzed by gas chromatograph yon a Chromosorb 102 column and found to contai n0 .22% oxygen, 0.28% nitrogen, and the balanc e

tetrafluoromethane .

Received : 4/27/83 The sample was scanned in the region 2 .5 to 1 2

microns by infrared spectroscopy . The path lengt h

was 1 .25 meters and sample pressure 10 mm Hg .

(see attached spectra )

COMMENTS :

APPROVEDSSFL A2CAIGYTICAL CHEMISTRY QNI T

► orm 619-V

IIDI m u imi i iumm i im iBNA0147617 0

H D M S E00624444

.1 0

u .20Z

C .300J) .40Cu

< .50.60.70

1 .01 .5cc4000 3000

WAVELENGTH (MICRONS)5 6 7 8

2000 1500

9 10 11 12 13 14 1 51 I I

1200CM-'

1000 900 800 700

SPECTRUM NO .

SAMPLEAk " a

ORIGIN__ _

VACUUM - BLANK SCAN

LEGEND_ REMARKS__

P . E . model 137 IR

PURITY 2 .

PHASE--- 4/28/83DATE

- 1 .25 metersTH ICKNE SS - OPERATOR

U .t

0. 0

.1 0

u.ju . 2 0

co .30

uD .40mQ .50

.60

.70

1 .0

A

4000 3000 2000 1500 1200CM- 1

SPECTRUM NO .

a) i

N)

WAVELENGTH (MICRONS)4 5 6 7 8 9 10 11 12 13 14

SAMPLEJJ')

i

(_ /I

ORIGIN_cTL-II I

__ _ Log# 4-351-83

PURITY

PHASE gas ` 10 _ mm press

LT HICKNE SS 1 .25 meters

3( )

1 .40

.50I . 6 t )

1000 900 800 700

LEGEND---- _

OPERATOR

P. E . model 137 1R

TNF PFP (IN(FI MFR CC PPfPATI(-lN N(-1QWA1 K (-()Nh i

REMARKS

GAS ES

AN D

VAPO R S

A SPECIAL COLLECTION OF INFRARED SPECTRA

from

THE COBLENTZ SOCIETY, INC .

with partial support fro m

THE JOINT COMMITTEE ON ATOMIC & MOLECULAR PHYSICAL DATA

and

THE OFFICE OF STANDARD REFERENCE DAT A

CLARA D . CRAVER, EDITO R

Copyright 1980, THE COBLENTZ SOCIETY, Inc .FOB 9952, Kirkwood, MO 6312 2

All rights reserved Printed in U .S .A .

Libro ry of Congress Catalog No . 80- 23347

R V V i L : .Yyr 1 ~ E T Lit riRT

IIDI m u imi i iumm i im i IDI I IBNA0147617 3

H D M S E00624447

Tetrafluoromethane(Freon 141

- T

C,A . #75 - 73-O 8850SAMPLE 7REO - - - fii added COBLENT Z

CF4 'total pressure 600 mm'PATH STRUCTURE

C1 VERIFIED

STATE gas

F-C-F MP B PF SPEC TROMErER MAKE+ MODEL CONTRIBUTING LA B

Dow KBr forepgrTB .inRQ, Dow Chemical Company

Changed 5 .0 ,7 .5, l5 .O DATE RECORDED 1964

W'aven •na :,er ca- 1

Carbon tetrachloride Methane , tetrachioro- C .A . 056-23-5

SAMPLE added COBLEKf2CC 14 total pressure 600 mm

pt- STRUCTUR E

5 c m VE RIFIED

CN S ATE gas

CI-C-CI M P B PI Z.°EC-RDMETER MAKE + MODEL CQNTRIEUTNG LAB

8821

CI Dow Or foreprIssTl Dow Chemical Company

Changed 5 . 0,7$5, 5 . /,!DATE RECORDED 1964

;... ?- ry, :-l .-- b -

E li m oB NA01476174

I IH D M S E0062444 8

ravanvat,*x o-1


FROM

J" x o srNT='~SSFL ANALYTICAL Q1SNISTRY UNI T

REFERENCE:, L8$3-7

PHONE S i f 7

DATE

LOG NO .SAMPLE


ct _3sa -sS M( , 7 o 'tlst! TLt s .i # pI.i c w 'c lot+~ iM .MfRst d

CAA / N~SIN NW fo .• 33d~y s . QNr s~ mp /Y w4 f

2 S~MP 1' S I11 farir ~ lr •J~l~ ; 12- /heM '

wws ~vo No 1.C edl L( ch 4Nst ,•M Y4Ir .t

s q ' fre t A A, s4' I. it J4~ . r n 3 t t ✓ r .vr&l'

f il t ly . rte SA P ,Ir. wer<

t~ , • S1N AY~'f •

dI~fC~

t

4 / 2 7/c 3

COMMENTS :

APPROVED

Form 619-V

SSFL ANAL CAL LISTRY U IT


LOG N O

4#- 33"0- 8 3

DEPT./GROUP S j- "

UH D M S E00624449

CHEMICAL ANALYSIS

REPORT

LOG N O

w- 349'- 8 2

r P .ttw EAU.( DEPT/GROUP S 1 ti - / (


$ 0- 72

PHONE S/

DATE 2/ C

LOG NO .SAMPLE


A s tNO !oy s~~.~+Gs TL . s R ..r>•.s %)I 4( 4 l M M ~ . s 1N ,A,

N TO Alr &4' M,uH {oa 3o L s. No

No f i c .e A 1 f.1 (i A# ' W a. s o~ sue .. . . r~

£4 ,#/e . Sa i vlam s ' '-t,, c~tL .< k/

/• (T /te a S~N'yM~~( •

iM

't/27/1 i

SSFL A CAW

SSFL ANALYTICAL (34 1STRY UNI T

IIDI m u imi i iumm iimimnuu I I

CHEMICAL ANALYSIS

REPORT

TO: EQUIRQ IT LA B

FROM : SSFL-ANALYTICAL CHEMISTR Y

REFERENCE : LB-&3 P.72.

DEPT./GROUP 599-job

`f -3-e~8 -83

PHONE544T

DATE APRIL- 2.7 , / 1̀63

LOG NO .SAMPLE

IDENTIFICATION0 .3 mgRESULTS ±

TRICH for NVR per

RL10001-F

EWR No . 504,Z (03

BLANK mg/500 ml

HARDWARE d • 1 mg/ 500 ml

1 .US * OL 1POBB,NS

V44t'

EWR No. X942.9

- 3 5E 8 -Pz3 BLINK mg/500 ml

HARDwARB 0-& mg/50o ml

GLu1N- oG G~d+fKET

-Am

No .

BLANK A ml


COMMENTS :

APPROVED

ANAGER

flm

Rec'd .

U..Ve

SSFL Ana tlcal N .mistry

cc : R . Schaued

Y . Francis D/564, ?B 66

K . Mogg

To: PLANT -SERVICES

FRO" SSTL ANALYTICAL CBEMISTRY

REFEpEWCE : LOG BK ' S 3 PACs 7 2

DEFT/GR X P :

LOG NO .

-4 - 345- ?3

PHONE 5447

OATE 6-/IAY-83

LOS NO.SAMPLE

IDENTIFICATION © PURLM & TRAP GC-/W RESULTS (PPM )


~} 39 C5 A8 sproved under the guidelines stated in the curren t

- I poOd at SSFL MRS permit , the following VOLATIIA ORGANI CO[POMS were sandC

Rocketdyne .A t (08 0008 / ~0ce one 3 3) _ .

Freeboard = - ft Bromodichlorosethane (BrCBC12) t)' . 0U !

Carbon Tetrachloride (CC14 ) Do I

Sampled

q 26 /Chloroform (CHCl3 )

F3 _

By : h. • CO /finsMethylene Chloride (CR2C12 ) = ND , 00 1

1,1,l-Trichloroethane (CS3CCl3) _ D~.00/

RECEIVRD 0 LAB : Trichloroethylene ( C1CE :OC12 ) 0.00 1

/ 2-41 83 Tetrachloroethylene (C12C :0012 ) - 7R 00 1

1,2-Dichloroethylene ( C1CE .C81C1 ) _ 0.D01Notation about appear-

ance of the sample : Dibromochloromethane (C1CEBr2) = 00 1Isopropyl Alcohol ; also (CE3C80HC83) = 0-02on as IPA ; 2-propanol

From TF (C12FCCF2C1 ) = D~ 00 I

1,l-Dichloroethane (C12 3) < . 00 I

CCNN12 TS : Tetrachloroethylene is also known as perchloroetbylene . ( 1) Monitoring specifi-

cally required according to the Rocket dyne NPDES permit , Order 176-146, NPDES 0 CA0001309


(2) This supplementary information is provided in accordance with 40 CFR 122 .60 .

PPM a PARTS PER MILLION

EBNA0147617 8


D/031

H D M S E00624452

ENGINEERING WORK REQUESTTITLE OF JOB I DATE

No 849942 9~, Ic ~- w~Ax I scL~ ~ ~~ ;zc,

.INSPECTION REQUIRED

APPLICABLE DRAWINGS ( ATTACH IF REQUIRED) REQUESTED COMPLETION DAT E

YES NO -2(p -j 3 5

DOING DEPT . I LEbGER ACCOUNT GENERAL ORDER GO . ITEM 8 MCR INIT. GROUP HOW . OR TARN DOINGG GROUP ACTUAL COMPLE T

I

-

I I {Y -_- _ _E U ST

U E5 ED B YREQ EXT . FACILITY SHIFT REQ . SUPERVISION ESTIMATOR ESTIM AT Ec_{^

'L ~ SCHOURS MATERIAL S

l 1` ✓ _ ___ REQUIRED _ REQUIR EDLAB SUPERVISION

ASSIGNED TO :LEADMAN MECHANIC $

SHOP LAB

INSTRUCTIONS (BE SPECIFIC ) NOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

JCL rn I -~/ ~L N) v 1 ~ P GL. L- 1 a o ~ cP= Tom,'` - ~ c ; -4

zn; rA , T /~ -I r1/~-r ("" n- , ] , 1 -i „ Li 5, ij

r~ ---, ;L. G3 t -.r <;,~ P 27 , C~- y °► 9 42 7

- P11 / s 1

Ct+~ L4(1 c~ +t

rv~~ ~s~ v r . .~ - ~3 ~- ► .

4, 3 CkT- o

RECEIVED @ LAB

APR 26198 3

SSFL ANALYTICAL CHEMISTR YBY 3 : 10 . ~~

ccp M

Z- -c cx,LIST OF MATERIALS

:ORM R 4 '. - [.S?

EBNA0147617 9

HDMSE00624453

ENGINEERING WORK REQUESTTITLE OF JOB DAT E

NV GA.-,.1.~ om a 'l t -~ N OP R 5 n 4 2 6 3A LICABLE DRAWINGS (ATTACH IF REQUIRED) REQUESTED COMPLETION DAT E

INSPECTIO EQUIR E

YES jff NO +"f - lc~ C7 _

DOING DEO'F LEDGER A NT GENERAL ORDER G .O . ITEM a MCR INIT . GROUP HDW . OR TASK DOING GROUP ACTUAL COMPLETION DAT EI

-REQUESTED BY EXT . FACILITY I SHIFT REQ . SUPER I ION ESTIMATOR ESTIMAT EI

HOUR MATERIAL SDREQUIRED REQUIRE D

LAS SUPERVISION EADMAN MECHANIC_

ISASSIGNED TO :

SHOP I LAB

INSTRUCTIONS ( BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON • DELIVERABLE ARTICLES ONLY .

RA~

Ewe Soy~6'~

&~ RL 1 0 0 c2 I . S .v.-A~~

RECEIVED @ LAB

APR 26198 3

SS FL ANALYTICAL CHEMISTRY 7.14

t-o_2sLIST O~ '.MATERIAL S

=0kw P .4'L P>~ P .!-

BNA0147618 0

H D M S E00624454

CHEMICAL ANALYSIS

REPORTT0 ; Quality Assurance DEPT . /GROUP :

Ti : SSFL ANALYTICAL CHEMISTRY LABORATORY

REFERENCE : Logbook - #83 Page - 73

LOG NUMBER :

/ - 3 / -83

PHONE : 5447

DATE : - a- MA y '83


GAS : _ __ 6GEi1/ PURITY = ' * % DUA By Difference

RECEI VED : .2 4r APR '&3 PARA = DA1A %

SAMPLER : FL00529 St

PRESSURE : 1950 #ia5/GIMPURITIE S

02 = DN f► % Arl-02 T,Q < / . O ppm

ANALYS IS REQUESTED : N2 = y, Na _ .3, 4PPM

A r Ar = IV f}PP m

SPECIAL : CO = % 00 = ~• 7~. < S PP m

CO = =% C0 N lj < O . S m2 2 . . pp

CH = CH = . )A) ft pp m4 4

FROM : C2H2 = q0 C2H2 = PPm

SSFL SUPPLY LINE H2 = % H2 = ppm

A LFA

BRAVO ~K .(ppm) Total Hydrocarbons as CH4

DELTA

COCA MOISTURE ppm H2 ( of DEW POINT )

CTL #3

CTL #4

CTL #5

TANK NO .

DELIVERY

TRAILER Tr - Trace

c = Less Than

OTHEF. (J/cam > = Greater Than

RECEIVES 4oO N .D . = None Detected

L A - HL/DR-G,FU D .N .A . = Does Not Apply

C MMENTS : *Maximum allowable limit per RAO 615 -072 for N2 is 15 ppm ; for 02 + Ar, it is 5ppm,4' * SNSV#'P~"dGj )7 S*AJj 0LE ro Y~EAE~DIG"

LABORATORY' ER

556

SSFL A. ALYTICAL C'riMISTR Y

BNA0147618 1

HDMSE00624455

[LOG NO •

CHEMICAL ANALYSIS

REPORT 4- 341- 83TO . M . Mogg DEPT.7GROUP 56 &


gbook ' 3P€. -7 Z

PHONE 5 ►7

DATE :'r° /g3

LOG NO .SAMPLE


_3q) _

J

Wastewater, Canoga

Site L, D/51411 Scrubber Chromium - 1 L(Q ✓►'tra /L

S ,.=P pH

Grab Sample taken

/IZ C./83 @ O)3O

ived [ 1 j2L tleJ- y7C ~

Analysed for pH, andchromium

COMMENTS : The limit for Site L is 75 mg/1 .

APPROVED

F arm 619-V


iimmuim i iiu mmiiumi muiim u

CHEMICAL ANALYSISREPORT y-3'lo•833

To. M . Mogg DEPT./GROUP 564


REFERENCE Logbook ' 8 3 oR . -72-

PHONE 5447

DATE 4/2('/9 3

LOG NO .SAMPLE


24-3,to-G 3 Wastewater, Canoga Copper - mg/L

Site C, "Sea World " Nickel - £' g/L

pE- I . ~24 Gr . PrODOrtionelsp-rlP rokpn

' /Zs~3 -74 /u 1'3~a~3a

Sample received 1412G

l yzed for copper, pHand nicke l

COMMENTS : the L.A. City discharge limit for copper is 15 mg/l,12 gag,/l .

An alyses per M . Mogg ' s II. 81 7E-422, 27 Oct . 1981N.D. - None detected /

APPROVED

for nickel the limit i s

SSFL ANALYTI CA L CHEMISTRY UNIT

I IBNAO147618 3

HDMSE00624457

TO:

Me"


C E I•/OIIONP 561

SSFL AXALYTICAL CHJUISTItY UNI T

REtEREMCE : Logbook ' $3 Pg . 72

LOG P40 .

4.339 -83

PHONE 5447

OATS 83

LOS N0.SAMPLE

1DENTIPICATION RESULTS

Y 339 8Wastewater , Canoga Chromium 20 .~✓1Q /L

`JSite B, D/544 Process PH = -7, (OCla ri fier


sample

y/25/83 7IZ~I~ 30-7 30

Sample received

Analyzed for pa, and

chromium

COMMENTS. The L .A . city discharge licit for chromium is 10 mg/LAnalyses per K . Yogg 's IL 81 FE-422, 27 Oct . 1981

r1 A.t It 1/ (21L 1Ld

SsFL AIiALYTI CA L Ctt 1ST[ L

I .xM 319-V

VB NA01476184

HDMSE00624458

S)hn, ks of 51 8 5T7 - .LOG NO .


FROM SSFL ANALYTICAL CHEMISTRY UNIT

DEPT./GROUP n8

PHONE 5447

REFERENCE : LOG BE ' 93 PA (Z 72 DATE

LOG NO .SAMPLE

IDENTIFICATION RESULTS ( by weight )

ST L - 4 ,MdH fromm DE?zSITY . . . . . . . . . . . . . . . 7C) gm/ml at 77o F

g ~jCELL _I- Lam!

44 - S3 -f 3 . . . . . . . . . . . . . . . . . . . 9q

ANALYSIS PER H O . . . . . . . . . . . . . . . . . . .

SPECIFICATION :2

Mil-P-27404B

Other Soluble Impurities = + . %

Color At Time Of Submittal ~,-~- Cp /QrlesS

RECEIVED E LAB :

COMMENTS : L A = DOES NOT APPLY

I IBNA0147618 5

HDMSE00624459

CHEMICAL ANALYSIS

REPORTTO : Quality Assuranc e

FROM : SSFL ANALYT ICAL CHEMISTRY LABORATORY

REFERENCE : Lrogbook - Jp 3 Page - 73

LOG NUMBER :

4 - 33y -23

DEPT . /GROUP: 556

PHONE: 5447

LATE : oZ ~~~ '83w~


GAS : yY_le6t_EEA) PURITY = > 7 9 . f % By Difference

RECEI VED : .?,S 2[ R PA RA = p N i4

SAMPLER : F4. o05a9-3IMPURITIE S

PRESSURE : /954l~j #t`X+ 4rt 02 s ppm02 = J NA

ANALYSIS REQUESTED : N2 % N2 = 7-,0- G / . y ppm

A r = % A r A- ppm,

SPECIAL :CO - % CO = u•D --, S ppm

= N .J1 , . 0 .5 pp mC0 = % Co2 t

CH4 CH4 = .P N 14 ppm.

FROM . PPC2H2 % CZH2

SSFL SUPPLY LINE

^

H2 = % H2 PPM

ALFA

BRAVO ~fo (ppm) Total Hydrocarbons as CH4

DELTA

COCA MOISTURE = G S ppm H2O of DEW POINT )

CTL #3

CTL #4

CTL # 5

TANK NO .

DELIVERY

TRAILERTr = Trace

C = Less Than

OTHER 5IC SUPPLY > = Greater Tha n

CHUMP. ST47 N.D . = None Detecte dD.N .A . : Does Not Apply

COMME NTS : *"aximu:n o__ovable limit per Rp( 615-072 for N2 is 15 ppm for 02 + Ar, it is 5ppm .

_2APPRD\7ED :

:ABO :ti.= ;0R . N.-GER

B NA0147618 6

H D M S E00624460

CI-I EMiCAL ANALYSIS

REPORTTO : Quality Assurance

FROM : SSFL ANALYTICAL CHEM!ISTFY LABORATOR Y

REFERENCE : Logbook - F3 Page - 73

DEPT . IGROL'P . 556

LOG NUMBER :

~' - 333 - S3

PHDNE : 5447

DATE : a2 A iA 5' F3SAM PL.E

LOG NO . IDENTIFICATION RESULTS

'/-333-83 GAS : NlT1e0 (:;EN PURITY = 7 ~1~• / % All ;-e06f;WBy Difference

RECEIVED : .25 APIA '83 PARA = -PV A %

SAMPLER : AZI- D p(, 3J2IMPURITIES

PRESSURE : /$&)02 = --D N 4 % Ar+-02 ,r 7 0 ppm

ANALYSIS REQUESTED : N 2 NZ ppm

PLETE Ar = % Ar = ppm

SPECIAL :CO = o CO = N. ~ . < $ ppm

CO C0 = /V, -D . < O, 5 pp m2 2

CH4 = ro CH = .DN 4 ppm

FROM : C2H2 =

4

% C2H2 = ppm

SSFL SUPPLY LINE H2 - ro H2 = ppm

A LFA

BRAVO (ppm ) Total Hydrocarbons as CH4

DELTA

COCA MOISTURE < 5 pp:n H2O 21g, of DEW POINT )

CTL ;3

CTL #4

CTL # 5

TANK NO ,

DELIVERY

TRAILERTr = Trace

OTRER

c>

= Less T= Greate

ha nr Tha n

TL- I N .D . = None DetectedD.N .A . = Does Not Apply

CSC MMENTS :

A PPR OVED: _ - - f '

o .B ~Rr T Or.'r N X CLE

~i~ C~sZ-S SFL A \AL 7T I CA L 4l iL,~S1+} 1

B NA0147618 7

H D M S E00624461

CHEMICAL ANALYSIS

REPORTO : Quality Assurance DEPT. !GRpi P: 556

FROM : SSFL ANALYTICAL CHLMU STRY LABORATOR Y

REFERENCE : Logbook - '93 Page - /3

ILO NUMBER :

-1/- 3,3 . - 93

PHONE : 544 7

DATE :,(-1 y '9-3


SJ` 33.2 43 C~,S : ,q.6-4141,4-1 PURITY = 7 //kL/04 By Difference

RECEIVED : 45 /4)Ok e3 PA RA = y/VA °s

sAMPLSR ; FLoo6 32JIMPURITIE S

PRESSURE : # r~202 = __ % 02 - . - 7 PPM

ANALYSIS REQUESTED : _ °l, NN PPM2 2

COMP*-LITE Ar = % Ar = PPM

IE

SPECIAL :CO = % CO = N, ~, l+ S ppm

=co % co pp mn tCH4 = 7o CH4 = PPM

FRCiM :-

C2, = o C2B2 = PPM

SSFL SUPPLY LINEdHy o H2 = PP M

A LFA

BRAVO (ppm) Total Hydrocarbons as CH 4

DELTA

COCA MOISTURE ppm R2 (C gG °F DEW POINT )

CI'L =3

CTL =4

CTL F 5

TANK NO .

DELIVERY

TRAILER Tr = Trace= Less Than

OR /g~H _ f a = Greater Tha n

.TI. N.D . = None Detected

D .N .A . a Does Not Apply

ca NTS :

F' kNAi"'IC.+L =r'-

BNA0147618 8

H D M S E00624462

LOG NO-

CHEMICAL ANALYSIS

REPORTr

DEPT./GROUP 5611

DATE

LOG NO .SAMPLE


83 Wastewater, Canoga

! £ 'S ILSite L, D/5J Scrubber C)Chromium -toH (Sump o •p

Grab Sample taken

Y12-5A-3 @073u

caple Received4ZA j

Iffi-a-lyzed for pH, and

chromium

TO- Mo

rpc"


DQR /*stoup 564

$STL AIIALYTICAL CH>el[ISTItT =1 ?

RE!'EREAiCE : Logbook ' 83 P` • 7 ,..

L0• P40 .

9-32183p'} ; 5447

OATS e.7- -S/T-5

MMONEWMEN~

1 .048 MO•SAJAPLE

IoENT1FICATIOM RESULTS

7 322--83 Wastewater, Canoga Chromiu m

Site B, D/544 Process pHs ~. OClarifier

Cr AAasample TAcccrw

y125/93 9030

a le receivedmp

4-7


chromium

CC►MM KT S : The L .A . city discharge limit for chromium is 10 ag/L

Analyses per V . Kou's IL 81 FE-422, 27 Oct . 1981

A P ACVEO ,

f it nl S19-V

SS7L ANALYTI CA L CMQLIST1i U391T

BNA0147619 0

H D M S E00624464

LOG NO .SAMPLE


4- Lox

ALFA III_

PURITY ONLYQ-( 9• OZ7(m BY OOLila

TEST # DO

SAMPIZR

AA '

B PSIG

RBC€IYSD :

2 S

SSFL Analytical Chemistry

I I

CHEMICAL ANALYSIS

REPORT

To: G'. SG A IV r{ s

FROM : SSFL ANALYTICAL CHENUSTRY UNIT

REFERENCE : t .--h nk 9 ;- 72

DEPT. /GROUP r 9 8 - 3 41

PHONE 5447

DATE T s / g„~ 3 _

LOG NO . DTU MIDENTIFICATION RESULTS V.1u,~~~ rtr(i . 7

- a3-4 N - 4L AAMH n 99.0 N o- d S S O.-3o4-s - 8130 M

-30 - p - - - 0.10.6 05 1sv(-sr 3-'it a 2 It14 -A& 11 q 1 . 3 0= 01 a

- o -f3.

3000.

ham A 171, 3 AX 0= 0, 3

COMMENTS :

APPROVED

Form 619-V


iimm u imi i iumm i iuummuu mu

cc . D . Bowiran , D/539, 055, SS1 2


1O : Quality A ssurano.

FAl : SSPL ANALYTICAL CEIDQSTRY L A BORATORY

Logbook - g , Page - 7 .3

4-3oF 3

per: 5447

fl TS : ~h;Q 2$ , 19 8 3

SAMPLEwG NO . IDENTIFICATIOW RESULTS*

CAB : G H 2. PURITY - 17 N A S Dr1 A B, Difference

4-301-53 R YY3D : 4/2zft 3 PARA - ANA s0t9 z6

ntPORI TI&9PRESSURE : (q 0 o p

03 - Dot A x t+02 - > I . o pp:ANALYSIS RBQUBSTffi1 :

N2 s 3; * Na _ > 6 5 WIN

Ar 1 Ar 'Dr, F1 PDaSPECIAL :

M x CD

00 =2 WINCH C8 = non

rocae ntelFROM :

E

4

c

4

C232 pp.

Ct

s Leb.

SSFL SUPPLY LINE H2 - X H2 P'Pa

ALGA

BRAVO-;> ('l1) (pp■ ) Total Hydrocarbons as Ca4

DELTA

COCA WISTURE = V N p ppa a2o 1'7 N q or DEv Pei1rT

CTL #3

CTL #4

CTL #5

TAM NO .

DELIVERY

TRAILER Mfr - Trace= Less Than

OTHER - Greater ThanX .D. - None Detected

D .R .A . - Doss Not Appl y

*Martmum allowable limit per Mil Spec . 27201B for 02 + Ar is 1 ppm ; for acombined nitrogen, moisture and hydrocarbons is 9 ppa . TnItR

1F THE LE,E(s or CeNCEMTRATrow of Ant 01 AAM r4 - .s our of CAUikAli o,4 RA.cr,

THE RtMAuriip , A*4NLOES w ►sRE CAr4C%L0E D .

APPROM : -~ .J

LABORATORY MGEH

55i

C' . . fj,.,857L ANALYTICAL CHEMISTR Y

BNA0147619 3

H D M S E00624467

t

ihw

CHEMICAL ANALYSIS

REPORT

TO: EQ P'd ^T? 'SAE

FROM :SSFL-ANALYTI CAL C}{ 1STRY

REFERENCE : LB- S3 P. -7

PHONE 544?

DATE Y 2 (a 1 CO _~

LOG NO .SAMPL E

iDENTIFiCATiON+ 0 .3 mgRESULTS

ncl

TRICH for I per

RLID001-F

Yw? No . .149 C, L-4 tCf

M:TL'4!s mg/coo ml

HARD ARE mg/500 mI

F I usk cf rod

n9 4o r E W R

!' ~qg4 o .\L4r _4- 3oo•83i

' L; No . -~3 9 4 2.1500 ml

mg~5 ~1?i R `~Acr ! 11! _Fl usti of Z' bocceto book per EWR

d7 499 L4 ?_0 0 .95 &.J

s

COMMENTS :

APPROVED X/f

LVG NU •

To

LA - 300- $ 3DEPT. /GROUP 598-34 4

,y?, , / , S!, ~ . 't-A -SSF L Analytical Chemistry

I IB NA01476194

H D M S E00624468

ENGINEERING WORK REQUES TTITLE OF JOB DATE

II No R49942 1tO 32 11 PA. C-,c:~- .APPLICA LE DRAWINGS IATTAC IF REQUIRED ) REQUESTED COMPLETION DAT E


YES NO 3DOING DEPT . LEDGER ACCOUNT GENERAL ORDER 1,1 - ITEM 8 MCR !-T- GROUP HOW . OR TASK DOING GROUP ACTUAL COMPLETION DATE

FACILIT Y ILITY SHIFT REQ . SUPERVISION I ESTIMATO RREQUESfED BY ESTIMAT E-'" ,{

I _ I _L~16Z5----- -----

HOURS I MATERIAL SREQUIRED j REQUIRE D


LEADM AN MECHANIC $

SHOP ( LAO


-D?-T~ Z ~7 r~~ v Y' G i-- I l_ Oc' 0 Z F~ cam= TI-~_ ~-~

-r+r - L C J S A ~. L G? L.

rzz ; '4 a".-` - . 9S ;- Z

C -4-- .- I.- AI-~ 1-o c' I

r^~ /S v '-' ,. . -- QL (-';I n.I L

A LC Q

-- P as Re, -.,

LIST OF MATERIAL S

BNA0147619 5

RECEIVED @ LAB

APR 221983

SSFL L CHEMISTRY

3 0 0 -

H D M S E00624469


ND . R4 9 9 41 9INSPECTION REQUIRED APPLICABLE DRAWINGS

( ATTACH IF REQUIRED )

YES I I NO

REQUESTED COMPLETION DAT E

41 `2 ( - g 3DOING DEPT . LEDGER ACCOUNT GENERAL ORDER G .O . ITEM & NCR INIT . GROUP (DW . OR TASK DOING GROUP ACTUAL COMPLETION DAT E

REQUESTED BY EXT . FACILITY SHIFT RED, SUPERVISION ESTIMATOR ESTIMAT E

HOURS MATERIAL S\ I REQUIRED RE Q UIRE DS S CIN

LAB SUPERVISION

ASSIGNED TO :LEA DM AN MECHANIC $

SHOP I I LAB

INSTRUCTIONS ( BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON -DELIVERABLE ARTICLES ONLY .

j TC~ZL ir'- J (U ✓GL P rL r .L 1Oc)O ! 7Vt T1'-

3 t-- (C c .4 A r~--t P +! D 7'c v J F--('-t -s `v5 r_1 O r

_ EZ. A4 c( 9

- - -r /-', > _ alb ; c -r~ : . r L( P + Z

#-3 /SPO -

1, 6 k-Q C-1 &~

"~ L /~ S L ✓~s~ `T I -i G. or CL C - ,c cz 210 Z w . -r-~-1

RECEIVED @ LAB

AP R 2 J98 3

BYSSFL ANALYji ,cHEMJSTR Y

44

LIST O~MATER '

c-OPV F 64- .. P . 6',

B NA0147619 6

HDMSE00624470

CHEMICAL ANALYSIS

REPORT

LOG NO .

LI - 2q8-

PHONE 5Ja 7

DATE y 2 Z

LOG NO .SAMPLE


4 -2~ia'83 Waetevater , Canog a

Site L, D/54b Scrubber Chromium a O ," /LSump ~pH ~. /

Grab Saaple taken

th - /3~- p73o

Sgmp1e Besc~eire d

Ana]3rzed for pH, andchromium

-SSFL ANALYTICAL CNfUSTRY UNI T

IIDI m u imi i iumm i iuumm i imiiu


-; M . Mogg DEPT./GROUP

FROM : SSFL ANALYTICAL CHE~ ( ISTRY UNI T

REFERENCE : ~pLogbook ' Q3 D .

PHONE cl~L?

DATE `mss

LOG NO .SAMPLE


Wastewater, Canoga Copper - O, 13 Ong/L

Site C, "Sea World" Nickel - d.9 5 mg/L

2A nr . Proportional b

`/(v/ ;- ~ /,/z / ;0730

enp1e received 4(ZZ~

Lnalyzed for copper, pEnd nicke l

COMMENTS: The L.A . City discharge limit for copper is 15 mg/l,12 mg/1 .

Analyses per H . )4ogg 'e IL 81. n-422, 27 Oct . 1981U .D. - None detected

APPROVED ______~ -_


. .,, . .,~1~3SFL ANALYTICAL Cf~IISTRY UNI T

IIOI m u imi i iumm i im i ID 0 I 0 010 0 IBNA0147619 8

H D M S E00624472


TO: -- M _ 1[oQ¢ D T./ 3 OUP 564

lROAAC SSTL AMLYTICAL O(afISTIY U IIT

IIEPERENCE : Logbook ' ' 3 pg . o

Pt1ONE 544 7

DATE r Z/ z /c3

LOO NO.SAMPtA


~J-24 '•Qaetewater , Canoga chromium Q.lbrn5 / LSite B , D/544 Process pH = 7Clarifier /


sample )-

~ c 7 3O

M

Sample received

Analyzed for pR, an dchromium

COMMENTS : The L .A . city discharge limit for chromium is 10 mgtLAnalyses per M . Mogg 's IL 81 FE-422, 27 Oct . 1981

APPROVED _ _ ~

V .em $19-V

a ,,,Q Ste, J-43ANALYTI CA L Oi~t1STWf @(I T

IIOI m u imi i iumm i im i ID 0 I 0 I DID 0 IBNA0147619 9

HDMSE00624473

cc :• 556 ' Bob Wilson D/ 588 u. 138, HC 8 6

CHEMICAL ANALYSIS

REPORTN . E . TOH E

8SFL 1NIALYTICAL C87lt4I8TRYFROM :

3 0REFERENCE : t 2

LOG NO •

4-253-~s3

PHONE

DATE ~L /zL/g

LOG NO .SAMPLE


-2~3 453 wx

ALFA III

G I_PURITY [LY T `• ~D % ort B'I OOLI1Z

SAMPI$R # r

FL A,I Co3 `C ~

5 gD PSIGe

RRCEIVBD :

/2'z/F3

COMMENTS :

APPROVED6SFL Analytical Ch.mlatry

b._ 1 a .IIDI muimiiiummiiuuu i

DEPT./GROUP 598

CHEMICAL ANALYSIS

REPORT

To : g .

FROM : SSPL ANALYTICAL ai®tISTRY UNI T

REFERENCE : L a 4 3 10

't - scg- s a

DEPT./GROUP c02.

P!•iON E s / ~ 7

DATE44./ 21/' 4 3

LOG NO•SAMPLE

1DENTW ICAT{ON RESULTS

y .y_p3 NTO Sc~•+ilteKH - D c

SD~V I , O/V TOM

y .~

PL F. (vI)ti

lY ; f 11 = 7't M Y/ C E

P

y- /1 / 3

COMMENTS :

APPROVED

Form 619-V

Nornw fLj' w , ManagerSSPL A rtal heal Chenwlr~

SoFL ANALY ICAL CHEMISTRY UNI T

IIDI muim i iiu mmiiu uui iim iii U


DEPT./GROUP ;Z ? -/ `S

PHONE Itf 7

L $1- 70DATE ,

LOG NO .SAMPLE

IDENTIFICATION RESULTS {i ~e~ue, C

2ti4-" ICa,al. s

24t- 4; s,~~rl<s f~•~ t!~ N~ Tit sy- F7-t3 7~ .~ ,v~i ./.r s1e*t .

/fr1A.{ jc471 +`

COz 1 3

R u" 2 3 7

T e v A t o "A' N2 = k l . l

M . .., ; CM-.de

AN Of s N 02 0. 00 S' '/o

As50 = 0, 3S %soy 3 r

tt/ ~ //I l

f-cl,ji s

Norma Fug' wa, 'ManagerSSFL Anaty cal Chematry

SJFL ANAL?- AL CHEMISTRY U.NIT

E


TO

FROM

M . Mogg


REFERENCE : Lcgbook '3 pg•- O

PHONE __

DATE

LOG NO .SAMPLE


LI-2

Weetewater , Canoga

~Site L, D/5Ui. Scrubber ( iromium - • -Sump

7

Grab Sample taken

7~Z `~a3 ~o ~3v

d q/-!: P*3R iece ve'~2~~

Analysed for pH, and

chrosium

COMMENTS : The limit for Site L is 75 mg/l •

APPROVED

arm

LOG NO

Y-2b'Y-83DEPT./GROUP 56I

SSFL ANALYTICAL O[1STRY UNIT

IIOI muim i iiu mmiiu uui iiu uu U

~: M . Mogg

FROM


~.DEPT./C3ROUP

S5FL ANALYTICAL Cti!°.IUSTRY UNI T

REFERENCE : Logbook

OLO G

q-283-$3

PHONE SLLr

DAT E

LOG NO .SAMPLE


~_ Z$~j• 3 wastewater , Canoga Copper 0.i 5 mg/L

Sate C, "Sea World " Nickel • ~•~ mg/ L

~s

pr2 hr . Proportional

! -r1p t,nk.on

emple reeeiard 41~Z~f630927

alyzed for copper, pfnd nickel

COMMENTS : The L.A . City discharge limit for copper is 15 tig/1, for nickel the limit i s

12 ragJL .Analyses per M . 14ogg 's TL 81 P!-1 .22, 27 Oct . 1981

N .D . - Fore detecte d

APPROVED>j1L A?iAjSTICAL L TRY [TI T

IIOI m u imi i iumm i im i DI D OBNA01476204

UHDMSE00624478

LO4 NO •


ro: >a . Mo a OEPT./311ouP

lROAE SSTL AMLTTICAL CiiIBTAT UXIT

REfERENCi Logbook ' g3 pg .

4'- 22Z- 3

Pf1ONE 5447

OATS

LOO NO •5AMPLS

IDENTIFICATION 1! ES U LTi

~-Z6Z-S7~ Wastewater , Canoga Chromic = N . D. O515/

Site B, D/544 Process pR =Clarifier


sample received 51/Z~ l

O'Z 7Analysed for pH, and

chromius

COMMENTS : The L .A . city discharge listit for chra J.us is 10 mg/LAnalyses per L Yogg's IL 81 PE-422 , 27 Oct . 1981

APPROVED iti •,~~,G

V .rT $19 ►-V

5971. AIN►LYrIGL CfiDLISTRY t 1 T


HDMSE00624479

r

CHEMICAL ANALYSIS

REPORTTo

TO: EQ` - . L AB DEPT. /GROUP 593-34 4

FROM : SSFL-ANALYTICAL CHE(ISTRYPHONE 5447

REFERENCE : L° `'A3 ` . "TL1 DATE L1 - L 10 1 R 3

LOG NO .SAMPLE

IDENTIFICATION RESULTS + 0 .3 m g

y - 2B 1-$3 ;TRICH for N71 pe r

RL10001- F

E'w'R No . LC[R 41 .5

mg/500 ml

HARD 'APE Q • 'S mg/500 mlF" I us 1, of E,L . IL%r,e Assembl y

o .L'4 ++ z

F-,7 No .

C"L'

m :,/5!)0 ml

HAK AF . mgl5 _

E No .

mar rr ~5 k

''r,!,RE mg'5)J ml

C

COMMENT S

APPROVED

Recd . aC) r o

\~2, ,/ (', .A -v-vn A'

CSF L Ana ;ytieal Chemistry

m


INSPECTION REQUIRED IAPPLICABLE DRAWINGS ATTACH IF REQUIRED I

YES NODOING DEPT . LEDGER ACCOUNT J GENERAL OR D

y d

REQSTS Y

L

LAB SUPERVISION

EXT . FACILIT Y

ASSIGNED TO :

SHIF T

SHOP LAB


RECEIVED @ LAB

(( 4C71Lf

? ;-7__ t~- L l o c c~ { Qcz- - --1--1! I ~I_r

-Yv T7 L

13

MECHANI C

ESTIMATO R

DATE

DOING GROU P

'_ L/Cl



ESTIMAT E


S


4-t

SSFL ANALYT1CAt CHE STRY

I4PR 20 1983x ;77

-L!E Cis MATER AS E


O . ITEM & MCR INIT . GROUP HOW . DR TAR

REQ. SUPERVISIO N

LEADMAN

HDMSE00624481

LOG NO .

CHEMICAL ANALYSIS

REPORT

~-O : QUALITY ASSURANCE

FROM : SSFL ANALYTICAL USTRY

REFERENCE : LOGBOOK X83 PAGE

9 -a 7?-83

DEPT./GROUP D/556

P1iONE 5447

DATE 4/ AP2 i4

SAMPLELOG NO . IDENTIFICATfON RESULTS

9-83 GAS : HEL /i1i4

RECD : ao %APfi',~ 83

SAMPLER :

PRESSURE ,2V )O P5/(, /Vj.). G I (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

FRO'x1 :

SSFL SuIPPLY LINETR = TRACE ND = NONE DETECTED C = LESS THAN


COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

OTHER : 55P /A

COMMENTS : *Maximum allowable limit per MO 615-072 for total bydrocarboas as methan eis 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or 02 .

APPROVED

SSFL ANALYTICAL CND I5TR1 UNI T


H D M S E00624482

i;

CHEMICAL ANALYSIS

REPORT

1O ; QUALITY ASSURANCE

FROM : SSFL ANALYTICAL CEIs~1ISTR Y

REFERENCE : LOGBOOK 13 PAGE vi

LOG NO .

'f - 7 V g

DEPT./GROUP D/556

PHONE 5447

DATE .2/ ,4I1 D

-3

SAMPLELOG NO . IDENTIFICATION RESULT S

- o? 9t 3 GAS : NI 7OG 6T4J

RECD : /4P '/ !3

SAMPLER : FL U05, ~S9

PRESSURE /go P5/Ci TIC < / (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE NIT = NONE DETECTED C = LESS THAN


COCA DELTA

CFL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

T RA I LE R

OTHER : 55P - 3

COMMENTS : *Maximum allocable limit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2 , and 26 .3 ppm in N2 or 02 ,

APPROVED

SSFL ANALYTICAL CHD ISTRY UNI T

IIOI m u imi i iumm i im i I Di I IBNA0147620 9

HDMSE00624483

CHEMICAL ANALYSIS

REPORT

LOG N O

L/- 2T?-~3

TO : M . Mogg DEPT/GROUP 5 6)+

FROM SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE :Logbook '83pg • )b

PHONE __

DATE

LOG NO .SAMPLE


Weatevater, Canoga

Site L, D/5i4 Scrubber ,V /LChromium - 3A'Q&imp QP H

Grab Sample taken

7'/w/€3

R di1 veeces~p e

elyzed for pH, andchromium

COMMENTS : The limit for Site L is 75 mg/1 .

APPROVEDSSFL ANALYTICAL CKDiISTRUNI T

~ . 619-V

IIDI m u imi i iumm i im i U

TO :

FROM :

CHEMICAL ANALYSIS

REPORT

r. . nogg

SSFL ANALYTICAL O3 (ISTRY UNI T

REFERENCE : Logbook ' pR . ? C)

LOG NO .SAMPLE


Wastewater , Canoga Copper - O4 ! mg/L

Site C, "Sea World " Nickel - 1 . to rng/L

2w hr . ProuartionA 1! A -r1P tQkC"

f ~`?is3 3+ qf2 f 3

aaple received y~S3

~0~30slyzed for copper, p!nd nicke l

COMMENTS: The L .A . City discharge limit for copper is t5 xg/1,12 mg/1 .

Analyses per K . Hogg'a IL 81 FE - .22, 27 Oct . 1981

X. D. - none detecte I

APPROVED

DEPT./GROUP 5

LOG N O

4-27~ - 3

PHONE 51► h 7

DATE 1 20 3


FL .A ALY:ICAL cHE3tI~TRY UNI T

IIDI m u imi i iumm i im i ID ID ID D IB NAO 147621 I

HDMSE00624485


TO: - M Y o¢Q O!!'T./DAQUP 54

P"OA~ SSYL ANALYTICAL OLDIIS TIT WI!?

REPEJIENcE : Logbook ' I)2)P8• 1 C)

LOS NO

~- 275 -S3

PHONE 5447

OATS ' ?O `t

LOG NO .SAMPLE

IDENTIFICATION RESULT:

q-2 5£3 Nastesater , Canoga Chromium . C). V 8 a4 9/ L

Site B , D/544 Process p8 =

Clari fier


sampl e

'///q/,3 --' q)w/1

Sample received


chromium

COA~IMENTS : The L.A . city discharge lilt for chromium is 10 mg/L

Analyses per L Uogg ' s IL Sl TE-422, 27 Oct . 1981

SSZL AMALYrICAL O{n .I$TSY @tIT


UH D M S E00624486

cc : Dir . 55b LOG N O

CHEMICAL ANALYSIS `tTo

REPORT

DEPT. / G ROU P 599-?bb

PHONE5! .1 7

DATE A P'/'- 2 / 983

LOG NO .SAMPL E

IOENTIFICATION RESULTS ~•3 mg

TRZCH For NV'd pe r

RU000i -F

L Z 7443

Ho . #q_-BLAI+RC _ ___ __,_„ mg/ 500 m l

HARDWARE °:L._ mg/5o0 ml

G(U/SN oL C„d5K67

EiiR No. ____________

BiA21lC 5OO ml

HARD4! ~_ erg/

EWR 3o .

ffirA1fK m8/5

ARE _____50O m 1

Rec' d . 4 / 9 -3

MJ .'IAGER SSFL Ana tlcal h.mistry

IIDI m u imi i iumm i iuuui i III ui u i

ENGINEERING WORK REQUES TTITLE OF JOE DATE

(U vfZ No. 849941 2INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIRED ) REQUESTED COMPLETION DATE

YES I I NO kDOING DEPT . LEDGER ACCOUNT I GENERAL ORDER ITEM 6 MGR INIT . GROUP HOW OR TASK ❑ OING GROUP ACTUAL COMPLETION DATE

OO7O

! --_BY,REQUESTED EXT . FACILITY SHIFT RED . SUPERVISION ESTIMATOR ESTIMA T E

HOURS MATERIAL S

--_-._-_-___ .._............__ REQUIRED REQUIR E D

LAB SUPERVISIONASSIGNED TO

, MECHANI CLEADMAN

__

$

SHOP I I LAB

INSTRUCTIONS ! BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

f (4~ 9 L-1 c /-I '~-, L 4 -TID (2--~ . . 'L- 44 1 1 I

-T Wit, •-~T 1 /'l./ v A .) ~/2 ~' ~R. . 6L L. (v ? v~ p 7 1^ ~-~e. l C r

/c c1 T c~5A Q 4 D ~3 -r, , , v ~= 6'L-t, --~ 5 _1 o(Z C-,4-5

-Tza -r-, f -IL -44 . ° • 5 3 -c r 2-

L- uR (L~j Tr ~~ c.~,l cL, ÈQ O c`

~Klf- 195,~t - Z' 74- s~3

RECEIVED 9 LAB

APB 19198 3

SSFL ANALY-KC CHEMISTRY-~ 3BY

S 2LIST OFMATERIAL S

GORT R. 64 . Ri

B NA0147621 4

HDMSE00624488


TO : F. Pa T o to


REFERENCE LOG BK ' 4 3 PAGE 70

LOG NO

DEPT/GROUP ;- 9 S

PHONE 5447

..~~~ DATE __*, g?

LOG NO .SAMPLE

IDENTIFICATION RESULTS (by weight )

?.B from STL - 4, DENSITY . . . . . . . . . . . . . . . Q , p 7 :Z., gm/ml s t 770 F't 27I-

CELL 2 1 8

MMR . . . . . . . . . . . . . . . . . . . fl .C4 %

ANALYSIS PER H2O . . . . . . . . . . . . . . . . . . . L 0

SPECIFICATION :

Mil-P-27404BOther Soluble Impurities = O.

Color At Time Of Submittal C(«M 4 (

C i7 I v Nl-t ~ SRECEIVED C LAB :

./ 11/ s ?

COMMENTS : tP(A = DOES NOT APPLY

APPROVED

l,~rm 619-v

4/i £L4 L-SSFL ANAL TICAL CHFitISTRY UNI T

IIOI m u imi i iumm i im i ID ID D D I IB NA0147621 5

HDMSE00624489

LOG ) ER :

CHEMICAL ANALYSIS

REPORTTO : Quality Assurance DEPT . (GROUP :

FROIS : SSFL ANALYTICAL CHEIIUSTRY ORATORY

REFERENCE : Logbook - $ 3 Page -11

4-2 a -8 3

PRONE : 5447

DA TE : /~ prt i Q 9 , 9 3

SAMPLELOG NO . ZDENTIfCATION RFsSULTS

GAS: _ PURITV = D.N.A . S D .N .A . By Differenc e

4-21D-83 RECBIVffi? : 4/19 3 PAR. = D.N.A . 5

SAJ&PLMR : T L 0 0 S 19 3

PRESSURE (81 #IMPURITIES

:02 = D .N.A . x Og • f~~~ ppa

ANALYSIS REQDFSTED : N2 = D .N.A . 5 NE _ +t•4 ppm

OOIID'LSTE Ar = D .N.A . S Ar = D .N .A . pp m

SPECIAL ForACO = D .N .A . 5 QO = D .N . . ppm

02 and N2 Only . =GO AD N 5 CO = D N A ppm2 ., . 2 . . .

CE4 = D .N .A . S CH4 = D . N .A . ppm

YRAI[ : C2H2 = D .N .A . S C2H2 = D .N .A . pp m

SSFL SUPPLY LINE H2 = DNA . S H2 = D . N .A . ppm

AIPA

BRAVO D .N .A . (ppm) Total Hydrocarbons as Cfi4

DELTA

COCA MOISTURE D .N.A . ppm H2O ( D .N.A, of DEW POINT )

CTL #3

CL #4

CTL #5

TANK NO.

DELIVERY

TRAILER Tr . Tracec Less Than

OTHER tj Str~pLl• > = Greater Thaa

CAMP STN .N .D ,

As None Detected

t A lN.D .N . _ Does pp yo

COMMENTS : Maximum allowable limit per RAO 615-072 for N2 is 15 ppm ; for 02 + Ar, it

is 5 ppm . ,

APPROVED : / ✓

LABORATORY NA ER

556

SSFL ANALYTICAL C} h(1STRY

II0I m u imi i iumm i im i ID ID 01000 I IB NA0147621 6

HDMSE00624490

TO:

FROM :

CHEMICAL ANALYSIS

REPORT

M. Mogg


REFERENCE : Logbook ' pg•70

PHONE 5' 7

DATE ____ 3

LOG NO .SAMPLE


I -2~c ~3

` !

Haeteweter, Canog a

T Site L, D/544 Scrubber Chromium - 320 v►^5 (L

Sump PH 7L/

Grab Sample taken

'-1 /19/S3 730

Sale Received


COMMENTS : The limit for Site L is 75 rng/1 .

APPROVED

► .)rm6'9-V

r.LOG N O

LI -29 -DEPT./GROUP 5614

c5SFL ANALYTICAL CHEMISTRY UNI T

IIOI m u imi i iumm i im i


To ; M . Mogg


REFERENCE Logbook ' :2) DR .

LOG NOSAMP1f


_Z~o$ _t53 Wastewater, Canoga Copper - ()455 mg/ L

Site C, "Sea World" Nickel - 3.2

. jog/L

0ly - a Vp .

214 hr . Pratiortioaa l! rlP ±o1rpfl

'i/i 193 -L( /1' 1E3

maple received L1~9I43

C_~25alyzed for copper, pE

nd nickel

COMMENTS : The L.A . City diacharge limit for copper is 15 mg/1,12 mg/l .

Analyses per M . Mogg ' a IL 81. 12-1422, 27 Oct . 1981K .D . - None detected /

APPROVED

LOG NO-

-2-83DEPT./GROUP SFlt

PHONE 4h7

DATE ______~ - ~


S~FL A!ULzTLCAL Cft TRY JSi T


I IH D M S E00624492

TO: M . oa¢

rRow~


OQ*T.~OIlOtIIA' 564

UTL AMLYTI CAL QIEItIrr Y uxlT

RErERE gIcE : Logbook 'B3 p g • 7

LOS NO

q ;L 7-8 .3

P't10N! 5447

DATE _______

e

LOA NO.SAMPLE

IDENTIFICATION R E'.i U LTs

Wastewater, Canoga Chromium s

Site B, D/544 Process pH = ( •Clarifier


sample

y~ ► g 1g; ~ ~ ~(9 ~~3

Sample received


chromium

COMMENTS : The L .A . city discharge sit for chromium is 10 mg/LAnalyses per M . Mogg 's4L 81 FE-422, 27 Oct . 198 1

A►plepvEp

r ern, eli ►-v

SSIL AMALYTICAL OtC .IST1IY @(IT

IIOI m u imi i iumm i im i ID ID D I D IB NA01476219

I IHDMSE00624493

CHEMICAL ANALYSI S

TO : 306 AI/ ft

REPORT

LOG NO

4-Z5B-83

DEPT./GROUP 598-3~ 3

FROM :SSFL A NA LYTICAL CHBMISTRY UNI T

REFERENCE :bk . 83 -p .70

PHONE _ 7

DATE L}P7~/L Z (o, /Q83

LOG NO .SAMPLE


SUS PECTE1~

-Z58-83 CGfl1c , i . CL1F CIL

72 r/N L1 Y1. y &a iLetdr ,nk inc~ c() a/~ Y h Jrocar6c~c 0 .35 ►ng /Iitek

5a P PJ( re ce r v e of

4I53 ®3 : 3Sp'

COMMENTS :

SSFL ANA LYTI L CtL ISTRY UNIT

f arm 619-V

IIDI muimiiiummiiuuu iui i i iuiu

N)N

4000 3000

SPECTRUM NO .

2000

SAMPLE q- zs zf - X1,3

1500

7 EWAVELENGT H

ORIGI N

PURITY

PHASE L/Qu%2

THICKNESS -GM

' rv-%r

(MICRONS )

LEGEND

9(-)0

5a-t7C tv!

lam ,i rt-9 cJ ¢~r ~ ' 5

R E

r .rri

(C L

v~d 6

u se

~v po

/- /c

fio• v

r a,ti _

11 12 13 14 1 5

DATE Ap~z~

OPERATORS.,

REMARKS s ,,,/ ~tc-

wF d`{ Gc-G ti 4,v11

3G,6/V N/_<D a C TW GL t

3- <f AAIC, 9-4N J

c : a[ '.lN! rI!nU" .;

I,-

z0

LOG NO

CHEMICAL ANALYSIS

REPORT

TO : ~E ► 0.1lSL E


REFERENCE - Li? 83- 7/

~ - x.57- 83

DATE P2 par L 83

LOG NO.SAMPLE

IDENTIFICATION RESULTS ~Y VOL ,

NF 3 SA.PLe37. r ;' NF 3

- ~•B3 FR~~ crL ]Ia, NZ

~cc IJ 18 ~Pw 3 Y O Z

O,o8 (

COMMENTS :

A

APPROVED

t ,rm 619-V

A

r

DEPT. /GROUP 5~ 8^3 ''~)

PHONE 5 4 _

0SSFL ANALYTICAL C D ISTEY UNIT

IIDI muimiiiummiiuuu iuiuu u i

c c'


!'1lOM :

f

387L ANA LYTI CA L QfI18ThY UNIT

REfERENCt : WC BE ' f ; PAfE 7 0

PHONE M47

DATE 3

LOG NO •$AMPLi

IClENTIiiCI1T10N USULTS (by .eight )

fro. STL - 4 LtiL11S ITT . . . . . . . . . . . . _ gL a1 at 60° !

crU •,. » 11204 . . . . . . . . . . . . . . . ' Q. 9! xK 'AI T4 V k !

H2O . . . . . . . . . . . . . . . . . d! %

Cl- . . . . . . . . . . . . . . . . o, o ,o x

. . . . . . . . . . . . . . . . . 0.9 2 s

AIIALTEIS P!S P.s. . . . . . . . . . . . . . . . . I. 8 A49 /K1 .faro6PECIfI CATI011 :

1►Alt, . . . . . . . . . O. Z Y 11~r0/K

1tl-P-2653907

. T~

w V 1t . "' "''?~,~ ,f NTo

RECEIVED S LAS :

t / q j

COMMENTS : nfA = V$ WT APPLY

* This taelysie is Dot

$D ru I.. ®n $fY IT

. f ,fir n+ ~1 o-V


LOO NO

L/.i 256-8 3

o+~PT~swoul' s g

clud.d is If 4-2U3 C.

£L/ W~

HDMSE00624497

ro:

FROM :

M. Mfg

CHEMICAL ANALYSIS

REPORT

DEPT/GROuP


REFERENCE : . Logbook ' )pg. ?C)

t-~LOG N O

L/ - 253-83

PHONE 54 1&7

DATE S

LOG NO .SAMPLE


1-253-S3 We etevater , CanogaSite L, D/51ai ► Scrubber Chromium - 23C) n"gfLSump pH

,Grab Samp a taken

Sample Receive d

X052Analyzed for pH, and

chromium

COMMENTS: The limit for Site L ie 75 mg/1 .

APPROVED

/ orm 519-V

A

SSFL ANALYTICAL a(M ISTRY UNIT

IIDI m u imi i iumm i iuuuiui i iim u i

rim

!'flO 3377. AMLYTICAL O4. IS IY Wfl!

REfRENc[~ Lotbooh ' .4 pg . 70

'r+0Ng 5447

t24TE y / ` g

LOS NO.SAAt IA

IpE1rITIfIG1~T10N ~ESULT$

y- 2s2-$3 Wastewater , Canoga Cbromiua - N. D. 4 p,o M5 /L

Site B, D/544 Process pH - VClarifier

G R .•a■aaple TAK0i.3

y~ ►~1g3~~~~~ s

Saap1 . rec.iv.d y I

ib S ZAnalyzed for pH, ■adchrosl ua

coMMwTs; The L.A . city discharge liait for chroaiua is 10 a;/L

Aaalyses per L• flogg 's IL 31 PE-422, 27 Oct . 1981

1.M1lOVla ~.---

I ari .1*-V

II0I m u imi i iumm i im i 10010 0 I IBNA0147622 5

Los P40 •

y- ~.SZ -8 3CHEMICAL ANALYSIS

REPORT

D 'T/owou• 56t

HDMSE00624499

cc : P. tl.ins.i th D1768 , 1040 _ CHEMI CALR . ed ANALYSISY . aaia J D/5~► ,

REPORT

To: EOOO.Tui 1 P1MR' SEHVIC><S

l110M ssFI . AEALTI"ItYL C® rSTRT

REPERENGE : InG s • 8 3 PAGE 6 8

LOS NO . IDENT $ P I CAT/ON

q-zso-s3Water sample fro. the

t2Al Inlet to theretention peed atfocketdyns .

Bs.pl.d • .'/0 _ H

.4/':/ 3By : L . Co //ins

RBC6IY®• LAB :

/d / .3

Rotation abet appsar-save of the sa.pl. :

OEPt/aNQUP D/03 1

© PU1tt8 a TIAP O GC/YS

LOG NO

~{-250-8 3

rh10NE 5447

DATE _____ 8 3

R3svhaS (PI' A)

Using the oonoantratie techniques and srtbods ap-

pru,r.d oadsr the guidelines stated is the current88TL >1PlaS psrait , the folloering VOL&?ILX QSCrIBIC

.ere ford :

Aoetoos (cu3oocs3) - 0 .13

Bzo~. .df (Bri9c19) - 0.002

Carbm Tetrachloride (CC14) - NI)' . 00 1

Oslorofora (cHC1 ) 0.0083

Bethylens Chlarida ( 2c12) -

1,1,1 4ricb].wu. than. (Oi3ac1 ) - DO I

Trichloro.thylsae (c

3

l~ :CC12) 0 .00 '-

Tetrachloroethyl .n. (C2.2C : CC12 ) _ ND . 00/

1 ,2-Mchloroethy1sae (C1 :C1)

Dibroawchloroesthan . cc1®r2) _ .00 1

Isopropyl Alcohol; also (C83ClI~CH3 ) - A'D ' . 0 1imam as IPA ; 2-propaaol

Tryon TY tcl2rcc~2c1) - D < . 00 /

1,1-Dichloroethaae CC12C8Cg3 ) = D < , 00/

COIOmiTS : Tetrachloroethylaas is also Iusoen as psrchloroethylsns . (1) Monitoring specifical-

ly required according to the Bockstdyas IBS psr.it, Order X 76-146, *1S IIr GOOO1308 fro.

the California Rsgioaal Water Quality Control Board , Los Angels. Region . (2) This supple-

.entary information is provided in accordance with 1t0 CYR 122 .60 .

PPI[ - PAAT9 PiR li I LLIO 1

- LIES TBAi! Im = 11CR!B nsracrm DIU ► DO 11D2 APPLY =TRACETi

STRY fl(I T

II0I m u imi i iumm i im i IDDIDDI I IBNA0147622 6

HDMSE00624500

cc : R . Schaued

I . Francis JD/56, ?D 66■ . rioa

CHEMICA LANALYSI S

REPORT

TO: >DOC83;TDuII PLA1 T SUVICI;S bElaT./AlI10iJP

1'Pe0u SSTL ANALYTICAL (SaL'T TR

reErrrc LOG IhIC $3 PAG; 6 B

D/031

LOG NO .

~-249-8 3

PHONE 5447

DATE -9 -MAY- 83

LOO NO. I DE NT 11t I C AT10M © PUNS Jk TRAP L OC/KS RESULTS (PPV )

F3later saupie fre■ th. Using the es .oentratioa technique . and sarthoda sp-R2 retantim pond at pro'.d under the guidsliaes stated in the curren t

Socketdyne . BSTL ar psr.lt, the following VOLATILZ OiICaAAI C

,,~~{{ COIII 6 wrs found:lr.eboard = Sv St de[]

1 qO(C X ,3 ) =83cXAoetaise8aspled f 9 . 20 H

00 '0

--

.Eresndi chlorot~ e thaae (flrQC13 ) =

'//h) I

Carbon Tetr.chloridr ( CCl4) = NO < . 00 1,. Cr0y :

c:h1orofor: (CHc13 ) _ 0 . 005k VI LAh1 :

Hethyleae Caloride (C132c12 ) _ 0 . 00

1,1,1-Triob3 o=oetbaae (ClI30C13 ) _ 0 . 00 /

Notation sbont appsar- Trich .oroethylene (C1~ :CC12 ) ci . Q O 6

inc. of the sal. :Tetrschloroethylne (c12C :OC12) = NO < . 00/

1,2-Dichloroethyleae (ClCE :®Cl ) 0 .002 .

Dibra.ochlorasethane (C1C®r2) _ C) 00 /

Isopropyl Alcohol ; also (CH3CHDHC 3 ) = 7R O•D I

In as IAA ; 2-prop.nol

ITrean TT (Cl2PCCF2c1 ) = ND . Do f

1,1-Dichloroet nne (CIZCBCi[3) = ND' . DO !

COhOtERPS : T.trschloro.thylen. is also hno.n as p.rchloro.thylene . (1) Qonitoring specificall

required according to the Rockatdyns NPDffi p.rait, Order # 76-146, NPDffi AI CA0001309 fro. the

California Regional later Quality Control Hoard , Lou Angeles Region . (2) This supple-

mentary information is provided in accordance with IO C!`R 122 .60 .

ppll = PARTS Plot MI LLION

~~rn 61P-V

TR = TRACE

SSYL AIIAL ICA L

IIOI m u imi i iumm i im i IDDID DBNA0147622 7

DhU1 = DOhL9 NDT APPLY


cc : K . schanL.a D/564, FB 66

Y . Pranci sK . Koa

TD: X ETDYl1 pt rr 9>I3tvICLS

lROI 98FL AML!TICAL CBA' TBY

' 8 3 PALE 6 8

CHEMICALANALYSIS

REPORT

DEPT./tis0up D/031

l Oe NO

■

4- 2i6 -8 3

P 4ONE 5447

DATE - MAY- 83

LO® NO . IDENTIIPIICATfON a p Q GC/S BESVLTS (PPM)

4- 24&LWater saapl. frog thepp

Using the eonc.mtratian tecbaiques and sethoda ap -retention pond at proved imd.r the guidelines stated Lu Lb. cur t

Bocbtdyne . SL ! S psrait, the folloring VOLATILE ORGARI C

Fr..board - itCOLPOtilWS eere fond :

______A 15ODf3 0(CS

Saaipl.d • 9 :30A,-1aetc7ne ~ 33) _ .

4l/f// 3 8x O'Odi chlorosethans C BrCSC12> - ND'. oo r

Co //~~ rB LCarbon Tetrachlorid. (CC14) _ /NQt, OD I

y : .Q.1orofors (CHC13) - 0 .00

BSCSIVKD S LAB : K.tbylass. Chloride (CIlZC12 ) - ND .DO

-! / /0° / 13 1,1,1-►rri.h1oroetban. (Ol CC13 ) - /J t, co l

Trichloroethylette (Cl :CCi2 ) - D .0 4Jot.tim about appear-ance of the sasple : Tetracbloro .thyl.oe (C12C :CC12 ) - ,VD <,DO I

1,2-Did .loro.thyl .a. (Cl®:~Ci) - 0 .003

Dlbrosochlororetban. (C1C®r2 ) = D ' .Do

Isopropyl Alcohol ; also (CB3QOHC83 ) NI) ~. 00?knoen as IPA ; 2-propano l

Precn TP ( CIZPCC.F2C1) - /JD . 00!

1-Dichloroethace (C12®«3 ) _ ND ' . DD/

-COjiiffiPI'S : T.trachloro.thyl.ne is also Imoeu as perchloro.thyl.u. . (1) Monitoring sPecifica1

17 required according to the Boch.tdyne NPDb9 permit, Order p 76-146 , IiPDES P CA0001309 from

the California Regional Water Quality Control Board , Los Angeles Region . (2) This supple-

mentary iuformstion is provided in accordance with 40 CTR 122.60 .

■ LESS THAN ND s J)NI DETEWE - PARTS PER M I I. L I O ND LEA : DOES IIDT APPLY TB s TRA M

AP'VltOVED A'VT ~

MANAGE RI JrT 61~-V

SSFL ANA ICA STAY 7fl T

II0I m u imi i iumm i im iBNA01476228

I IHDMSE00624502

EFFLUENT- D i SCHARBE REPOR T

CHEM i C AL AN AL YS IS RESULT

INDUSTRIAL ENGINEERING D/031 SS1 2

FROM : SSFL ANALYTICAL CHEMISTRY 0/539 SS11

REFERENCE : LOG BK ' S3 PAGE 68

LOG N O

~4- 297-8 3

DATE : /3-HA Y

PHONE : 544 7

SAMPLED FROM : Al. IuLET To R2 C 9/0 All AM /P . ON : lff - A?R-83

CONSTITUENT RESULTSmg/1

CONCENTRATION

mg/1p}1 at 25° C 7,5 pH unit 6 to 9 unit s

Total Dissolved Solids on Drying at 180° C 107 950

Temperature of Water /2 . 37 .6 ° C

Chloride l'~} 150

Suspended Solids S 7 150

Settleable Solids 0.3 m1/1 0.3 ml~l o

HOD at 20 ° C 4 60Grease and Oil < / 15

Residual Chlorine o . z$ 0 . 1

Surfactants as MBAS (0.0/ 0 . 5

Sulfate 30 300

Total Onrorait n 0. 007 0 .01

Fluoride 0.2 1. 0

Boron 1.0

Turbidity 35 NT(/ (5)

Phenols < 0.00 1 (4 )

Mercaptans 0. S (4 )

4 n t~t 0, 00 /

(1) Filtered with Whatman GF/C paper .

(2) Filtered with Whatman GF/C paper and dried at 103° to 105° C .

(3) Limitation not. required to to met during rainfall .

(4) Wastes discharged shall not contain phenols, mercaptans, or other substances i

concentrations which would impart taste, color, odors, foaming or other object-

ionable characteristics to receiving waters . . .or any sdbstence in concentration

toxic to human, animal, plant or fish life .

(5) Wastes discharged shall n increase the natural turbidity of the receiving

waters at the time of di harge .

Approved : ~ ,

MANAGE SSFL Ah:^•l,A

- vG1L CHEM TRH' UNI T

II0I m u imi i iumm i im i 100100 I D IBNA01476229

UHDMSE00624503

EFFLU EPT D I SCHARGE REPOR T

CHEMICAL ANALYSIS RESULTS

O :_ ndustrial F'nrrineerin¢

F:gCM : SSFL MIALY .̂'ICAL CftEMISTRY . IEPT . 534

rP2 : t-3_- .o 6 BSAMPLE IT.QriIFICATION : SAZ4PLE FE I~ Z

LOG NO

TOI - z 46-s3

DEPT ./GFcup 031

P UE 41 .7

DA TE :13 -MAY-J3I q 0x 1 8 -APR-13

~,,J, RESULTS/1

NCENTRATIONIT /1

pH at 25' C $„ $' pH unit to units

Total Dissolved Solids on Darying at 180 ' C 2.63 950Temperature of Water /2 , 7 37.8' CChloride 24 150Suspended Solida /0/ 150

Settleable Solids D ./ ml/1 0.3 m1/1

3)D at 20' C 4 60Grasse and Oil z 15

Residual Chlorine .04 0. 1

Surfactants as HBAS (O. Of 0.5

Sulfate 75 300

Total Gnrum < O.OO I 0.01

Fluoride 0 .3 1.0

Boron 0, Z 1 .0Turbidity 25 N7t1 (5)

Sewage Treatment Plant Influent BOD at 20 C 656 (k )Sewage Treatment Plant Effluent BOD at 20' C 4 (1~)

Sewage Treatment Plant Influent Suspended Solids 334g (1 ► )

Sewage Treatment Plan Effluent Suspended Solids 6 (4 )

(5)

~1vSSFL A LY'TICAL cE,1ISTRY UNIT

APPROVED

Form 619-V


Filtered with Whetman GF/C paper .

Filtered with Whetman cF/C paper and dried at 103°to 105° C .

Limitation not required to be met during rainfall .

The average final effluent eonoentrations shall not exceed 156 by weight ofthe average sewage treatment plant influent concentrations of HODS 2O'C sadsuspended solids during periods of discharge . ,

Wastes discharged shall not increase the natural turbidity of the raeeivingwaters at the tine of dis arge .

UHDMSE00624504

EFFLUENT D !CHAR GE REPOR T


LOG N O

-4- z39- a3TO

'1- Z1 - 83

(5 )

1 :Industriel Enaineeriinr

FffiM : SSFL MALYTICAL CHD4ISTRY . IEPT. s.q

P: LB-83-p .68

SIDLE IDEtrTI YICATION : SAMPLE FFCN_PP

mo./Gaup 031

PzNE 5ia ►7

Dq~: /3/1A'-B3Q.'30 4y ON /8-APR- : 3

CO~rr RESULTS/1

NCrNTRATIONIfi /l

pH at 25• C 7.6 pH unit to units

Total Dissolved Solids on Drying at 180 C j .q $ 950

Tecaperature of Water 12 .0 37.8' C

Chloride 20 150


Settleable Solids <0 . 1 ml/1 0 .3 ot]./1

BOD at 20' C $ 60

Grease and Oil < ( 15

Residual Chlorine < 0.04 0 . 1

Surfactants as MBAS < 0.01 0. 5

Sulfate 38 300

Total Chromium 0 . 0O z 0.01

Fluoride 0 .4 1.0

Boron 40.2. 1.0

Turbidity /5 N rv (5 )

Sewage Treatment Plant Influent BOD at 20 ' C 4/0 (4 )

Sewage Treatment Plant Effluent BOD at 20' C 3 (4)

Sewage Treatment Plant Influent Suspended Solids Z5 Z (1 )

Sewage Treatment Plant Effluent Suspended Solids 1 (1k )

Filtered with Whattman GF/C paper .

Filtered with Whatman GF/C paper and dried at 103 ° to 105° C .


The average final effluent concentrations shall not exceed 15~ by weight ofthe average sewage treatment plant influent concentrations of BODS 20'C andsuspended solids during periods of discharge .

Wastes discharged shall not increase the natural turbidity of the receivingwaters at the time of discharge .

APPROVED

Form 619-V

.J .MANAGEIy 95FL A GLY:ICAL IDII9iA Y UNSSFL A LYTICAL ISTRY TJNI T


UHDMSE00624505

cc ; R . Schmued, M . Francis , M, MOgg ; D/564, FE 66


LOG N O

4-2q2-8 3

TO : ROCKETDYNE PLANT SERVICESDEPT,/GRC► UP D ."03 1


REFERENCE : Logbook 23 Page 6$

PHONE 5447

DATE S 3 3

LOG NO •SAMPLE


WATER SAMPLE

from

Je 2

Analyses required :

CYANIDES 0 .003 '/i.- (b ~SPfISNOLS 0 .001 // , t*r /~{ lV OL_ S

DATE SAMPLED :

q /8 i3

SAMPLED BY :

2 . Co//mss

COMMENTS : This supplementary information is provided in accordancewith 40 CFR 122 .60.

APPROVED 1t2f Jrrn 619-V

MANAGER SSFL ANAL TICAL QiElr[ISTRY UNI T


HDMSE00624506

ENSINEERIN WORK REQUESTTITLE Of JO B

ti~ v fz~ ~cL OL, " -TDAT E

a - , 3 -s3 42864 6No . AINSPECTION REQUIRED

APPLICABLE DRAWINGS ( ATTACH IF REQUIRED )

F

REQUESTED COMPLETION DATE

-1N - 73YES I I NO ~~%

DOING DEPT . LEDGER ACCOU NT GENERAL ORDER G .O . ITEM a NCR INIT . GROUP NEW . OR TASK OING GROU PD ACTUAL COMPLETION DAT E

O

REQUESTED BY EXT . FACILIT YFA FTSHIFT REQ . SUPERVISION ESTIMATOR ESTIMAT E

i t - c c ZI T` HOURS MATERIAL S`h I REgU1RED REQUIRE D

LAB SUPERVISIONASSIGNED TO

LEADMAN MECHANIC_ _

$

SHOP LAB


,4 PG' L- I C ,443 L' To a-, EL. y 2 3 G Li S

~~ -[ ~_~L-+-►-► n> v 2 P• Z 6L- t... 1© 00 1 ©c r~L, -rk c +v ; d - ; c'~ Cam/ ILA -r

pc r a~ w C.. L9 4 S

- TIC L- A-VZ _'c =' * 2 !.. f 4.

C L, Aa C-

V"Z J5a v X

'^^ ~l / Jr0 2 - Q i. x4 1. /C.

4 dt v-

I'I O Tt r---l w R, L TTZTL

-(3 RECEIVED Cap LAB

APR 14 198 3

SSFL ANALYTI L CHEMISTRY,3 Y

55 `LIST OF MATERIALS

FORM R G<-' RE" 6 .31

BNA0147623 3

HDMSE00624507

CHEMICAL ANALYSISREPORT L- 3S-g3

. Hir7&!u DEFT /GROUP 598-345TO:

FROMSSYL ANA LYTICA L CH I STRY LIMIT

REFERENCE : Logboolt ' pg . (og

PHONE 5447

DATE ~4 83

LOG NO .SAAB


L~_23g'~3Argon K bottl e

Fros A-3 Coca\

H2O = 5ppQ \ r ' - g(o °F F' -Serial # w3 Ig 2 l J/LRecd.

y ~1~ (s3

Analyze for Moiatureonly

COMMENTS :

APPROVE D

rr~ 619-V

AU iLikaj»FL ANALYTICAL CHH[ISTRY UNI T

llDl muim i iiu mmiiu uu III DD i im u i

LOG NO

CHEMICAL ANALYSI SREPORT L/ 23~-g3

TO K . H1rovasu DEPT-/GROUP 598-34 5

FROM SSFL ANALYTI CA L CHB1tISTRY UNIT

REFERENICE : t4 boot '3 pg.

PHONE 5447

DATE

LOG NO .SAMPLE


Argon B bottl eFrota A-3 Coca ~

H 0n('

?-~ 5 wf rSerial # w i 7ag 2Rec'd .

yl~~183

Analyze for Moistur e

only

COMMENTS :

APPROVED 41 ~~aw _..-'

Jrm 519-V

»FL ANALYTICAL C}{ISTRY UNIT

IIDI m u imi i iumm i im i ID ID I DD II


TO: K_ Hiropaeu

FROMSFL ANALYTI CA L C}L (ISTRY UNI T

R£FERENCE~ Logbook '

LOCI NO .SAMPLE

tOENTIFICATION RESULTS

Argon H bottle

Fro. A-3 CocaSerial N W 2.3(0(0 2~]

H 0 = .2

Recd.

/,~Js3 ArvA L4'S lS C An~G~Tc - __ D

* h I LxD B L? QA. oN _

PART' Cu

Analyze for 1[o1ature

only

COMMENTS :

APPROVED ,41 •

m 619-V

LOG N O

DEPT. /GROUP 598-345

PHONE 5447

DATEl ~Ct lg3

FL ANALYTICAL CHH[ISTWI UNI '

II0I m u imi i iumm i im i I I


TO : K_ Rj rovaau

FROMSSFL ANALYTICAL C& (ISTRY UNI T

REFERENCE Logbook ' 3 pg .

LOG NO .SAMPLE


Argon K bottle~ !LI .235'S3 Prove A-3 Coca e~H2O =~ 5 Ppry+ ( -+ r OSw FLv i}

Serial # w 8 g 22~Recd . ylb~/9

3

Analyze for Moisture

only

a

COMMENTS:

APPROVED

l~rm.619-V

LOG P40 .

DEPT /GROUP 598-345

PHONE 5447

____ DATE y 3

5SFL ANALYTICAL cl-L 4ISTRY GT( I

iimm u imi i iumm i im i IMIDD I I I

LOG NO

CHEMICAL ANALYSI SREPORT y "~3c,~~g3

TO: K . Hirovasu

SSFL ANALYTICAL QL ISTRY UNIT

REFERENCE : Logbook' 3 pg . ~o O

LOG NO-

COMMENTS :

APPROVED

..arm 619-V

SAMPLEIDENTIFICATIO N

Argon B bottle

From A-3 Coca

Serial FW sis coRecd ,

Analyze for Moistureonly

DEPT./GROUP 598-345

PHONE 5447

DATE 3

RESULTS

H2O ~ .

ANr4C.'r'S ►S CA,VG ~L~ 'TO

/ L Lr D 8 Q.R . Okl

PA 27i CU L1q 7- -3

j . FL A!lALYTICAL CHEMISTRY U!1T T

IIDI m u imi i iumm i im i IDiu ii um U

LOO NO • --

CHEMICAL ANALYSIS-~REPORT q-33 3

TO: K . Hirovaau DEPT,/C3R01.IP 34 5

FROM : SSFL ANALYTICAL CHSIIISTRY UNITPHONE 5447

REFERENCE : Logbook '3 pg . (~► ~DATE ! ~`7 g

LOG NO .SAMPLE


4-X33-53 Argon 8 bottleFroa A-3 CocaS i l #

H p =~ S pPm /,~_~ o%2er a w 365 . c•Rec'a . 4/(,j~3

_ ___! _~o t3 C . F . a Al

pARTic.uL -r

Analyze for Noiature

only

A/ii AGW/7L. -p. GND/-SSFL ANALYTICAL C {Fi [ISTRY UNI T

IIDI muimiiiummiiuuu III DDI mu


TO: K . Hirovasu

FROMSSFL ANALYTICAL O1 1STRY UNI T

REF'ERENC>< : Logboot ' g3 pg .

PHONE 8447

DATE

LOG NO .SAMPLE


y-232'g3Argon H bottleFro. A-3 Coca

"

H O2 fp.r,4J ~}Seri al #/57 7

Rec'd, y ~' 83

Analyse for Moisture

only

COMMENTS:

APPROVED

I Drrr 619-V

LOONO-

y-a3a- ~ 3


SSFL A?ALYTICAL OfldISTRY UN1 :

IIOI m u imi i iumm i im i u ii DDi 0 U

CC : FL Aeg~ r

TO G . BAUERLE

-D~63~-ffE7 FA ~4:


FROM SSFL ANALYTICAL CHII~ISTRY

REFERENCE LOGBOOK PAGE ( D

PHONE

DATE

4824

LOG NO .SAMPLE


I .D . 4-- MEASURED PRESSURE = mm

4-2 2 ! -o 3jSAMPLE # = I 02 = / L 4 - N2 = Q. 1 mm

FLASK # _ 2-- He = l 5' ( mm C22 = Z mm (D Z )

PRESSURE _ ~_ o 520 =//f0 mm

----- ----- -I .D. ~+ =

----- -4--I S- C_

---- -MEASURED

----- -PRESSURE =

------ -3 S.

--- -t1e

---- -

;2 3o -g3SAMPLE # = 2 0z = /04 mm N2 = (2/ mm

FLASK # = /0 He = .24c mm C12 = (2/ mm (Of))

PRESSURE = 38, fc g20 = 0. 3 mm

I .D . # = MEASURED PRESSURE = mm

~'EfUf : SAMPLE # = 02 = em N2 = mm

¢/IS/83 FLASK # = He = tie C12 = mm ( )

- - - - -

PRESSURE =

- - - - - -

psis

- - - - - - - - - - -

820 =

- - - - - -

mm

- - - - - - - - - - - - - - - -


SAMPLE # = 02 = a N2 = mm

FLASK # = He = em Cl2 = em ( )

PRESSURE = psis 820 = mm

COMMENTS :

APPROVED -// A QAAT Lh LSSTL'ANALYTIOAL CHEMI STRY U

IIOI m u imi i iumm i im iB NA0147624 1

CHRONIA TOGRA PRY .

CHLORINE VALUES IF PARENTHESES ARE NOT CORRECTED FOR MANIFOLD SAMPLING LASSES

AND ASSUME CONVERSION TO CHLORIDE PRIOR TO THE CiLORIDE DETERMINATION . ALL

OTHER VALUES ARE CORRECTED FOR THESE LOSSES . EATER IS DETERMINED BY REACTION

LOG NO

44-'34-3o3o -8 3

DEPT /GROUP D/522

HDMSE00624515


TO : Quality Assurance DB~P .fapOUP: 556

FROM : SSFL AMLTTICAL CHEMISTRY LABORATORY

REFERENCE : Logbook - ' 3 Page -69

LOG N BER :

PHONE : 5447

DATE : (~pR . 19, 198 3

SAMPLELOG ' ) . ID~ITIFICATION RffiQLTS

&'S :____________ PURITY >-q .8 % NQ By Difference

RECEIVED : 4f'/g~ PARA a 4F %

SAMPLER:__________

PRESSURE : f 9 15 #IMPURITIES

02 =___________% 02 + 4. g ppn

ANALYSIS REQUESTED : N2 % N~ _ 1•$ pP=

Ar % Ar

-

DN Fl ppmSPECIAL :

CO = 00 = Na < S ppm

= _ D < O . _ ppmC0 = % CO2 2

CH4 e % CH = ~N Fj ppm4

FROM :C _ % c2i2 = - ---ppm


ALFA 3 K 6/6

BRAVONt < I (ppm) Total Hydrocarbons as CH4

DELTA

COCA MOISTURE ppm H2O ( <.-$(, °F DEW MINT )

CTL #3

CTL #4

CTL # 5

TANK NO .

DELIVERY

TRAILER Tr - Trace

c a Less Than

OTFIER > a Greater Tha n

N.D . - None Detected

D .N.A . - Does Not Apply

COMMENTS : *Maximum allowable limit per LAO 615-072 for N2 is 15 ppm ; for 02 + Are it is 5ppm.

APPROVED : GZ.I.v u

LABORATORY MA "GER SSFL ANALSTICAL CHEMISTRY

II0I m u imi i iumm i im iB NA0147624 2

HDMSE00624516

CHEMICAL ANALYSIS

REPORTT0 : Quality Assurance

FROM : SSFL ANALYTICAL CHEMISTRY LABORATORY

REFERENCE : Logbook - $ 3 Page - 6 9

DEPT. /GWUP :

LQG NUMBER :

PHONE : 5447

DtTE: APR . 19, 198 5

SAMPLEIAG N0 . IDENTIFICATION RESULTS

GAS : GNZ PURITY = > ICS •$ % N~ By Difference

~-{--226$ 3 RECEIVED : 4.f(5[3 PARA = •Tj r_ R

SAMPLER : F L o o 51-7 IIMPURITIES

PRESSURE : 18 S o #021-fix= < ©• ( % 02 . `_ _ NI PPm

ANALYSIS REQUESTED : N2 = %Na= Ppm

Ar = ro Ar ppm

SPECIAL :CO CO = !~ PPm

CO 5 ppmCO = 410., 2 .

CH4 CH4 = D N 11 ppm

FROM : C2S2. = o C2H2 = ppm


ALFA 3 K el eBRAVO T(t < ( (ppm) Total Hydrocarbons as CH4

DELTA

COCA MOISTURE _ •C _ Ppm H2 (L-$ 6 OF DEW POINT )

CTL #3

CTL #4

CTL # 5

TANK NO .

DELIVERY

TRAILER Tr a Tracec = Less Than

OTHER > = Greater Than

N.D . a None DetectedD .N.A . = Does Not Apply

COMMENTS : *Maximum allowable limit per RAO 615-072 for N2 is 15 ppm ; for 02 + Ar, it is 5ppm.

APPROVED-C .

LABORATORY NAGER SSFL ANALYTICAL CHEMISTRY

I D IBNA0147624 3

556

HDMSE00624517


FROM :

M . Hogg


REFERENCE :. Logbook ' t $

`~"

PHONE 54+7

DATE

LOG NO .SAMPLE


Westevater, Canoga

Site L, D/ 5i Scrubber Chromium r ) LSump P - '7. LGrab Sample take n

1lS /S3 @ c 73c

Sample Received Jjlj0 1 6


COMMENTS : The limit for Site L is 75 mg/l .

APPROVED

EB NA01476244

LOGNO-

Li-22q-83DEPT./ GROUP 561

SSFL ANALYTI CA L { HWQSTRY UNI T

HDMSE00624518

CHEMICAL ANALYSIS

REPORTTO: Quality Assurance ~p~OQp; SS6

F1 f : SSFL ANAL?TICAL CFZMZSTRY IABORATOR Y

REFERENCE : Logbook - 8 3 Page - 69

LO NUMBER :

4-z -

PRONE :: 5447

IMTE : ('~ (3p. • I `1 , 19$ 3

SAMPLELOG N0 . IDENTIFICATION RESULTS

GAS : LoX PURITY = 9 9• 4' x o;REC~ZVED : 4 r 15 ! 8 3 PA RA = ,___ N xSAMPI.ER : F L o 3 E 6 q ,

PRESSURE : #60 #IMPURITIES

02 = I7N x 02 s N Fj PPsANALYSIS REQUffi"PED : N2 = x Na = PP■

V=im Ar x Ar PpmSP&CIAL :

CO = % CO ND~ S ppm

00 = x 00 = N D < 0 52 2 . ppm

CH = % CH = N 14 PPm4 4 __

FRCP : c2H., x c2H2 = rtn < O . t PPm

SSFL SUPPLY LINE H2 x H2 = ppm

ALFA Tra N K 6 oBRAVO a23 (ppm) Total Hydrocarbons as GH 4

DELTA

COCA MOISTURE = < S PPm H2O ( < °F DEW PC3INT )

CTL :3

CTL #4

CTL :5

TANK 2i D .

DELIVERY

TRAILER Tr :Trace

t = Less Than

OAR > : Greater ThanN .D . = None Detected

D .N .A . . Does Not Appl y

0 JIQ~T5 : *Max:aum allowable limit per RAO 615-072 for N2 is 15 ppm ; for 02 . Ar , it is 5ppm .

A PHtOVED

SSFL ANALYTICAL CHESd1STRY


I IHDMSE00624519


TO : Quality Assurance DEPT . /GROETP :

FROG[ : SSFL ANALYTICAL CHEMISTRY LABORATORY

REFERENCE : Logbook -3 3 Pa ge - 6~

WC Na BER :

4-~ z z --~ 3

PHONE : 5447

SAMPLBLOG !À . IDENTIFICATION RE5DLTS

GS : Lox PURITY = 4 9 • , % Oa,'~--22Z-$3 RECEIVED : 4(,S f$ 3 PARA = PNA ~•

SAIPLER : 5 ~ _ ~ 3 a

PRESSVRE : 37o xIMPGRITIES

02 a D N % 02 - t rY A PPsANALYSIS RSQII~Sr FsD : N2 - S NZ = PP'

A' _ S Ar = PPmSPECIAL : _ CO ND < S PPm

00 = S CO = ND< O $2 2 . PPm

CS = % CH = 'DNA PPm4 4

FR : f-3 T-RNK I G$ C2H2 = - °~. C2H2 = < C. PPa

SSFL suPPLY LI!1E H2 = S H2 = ANA pp m

ALF A

BRAVO.~.3 (ppm) Total Hydrocarbons as CH ;

DELTA

COCA 5&OISTURfi = _ _ PPm H2O ( <. 6 of DEW P3INT )

CTL 3

CTL 4

CfL =5

TAME y0 .

DELIVERY

ICI LER Tr = Trace= Less Than

OT liE R >, a Greater Tha aN .D . = None Detected

D .N .A . . Does Not Apply

CI ENTS : ~Maa_zuc allowable 1imit per RAG 615-772 for N ., is 15 ppm ; for 02 + Ar, it is Sppc.

i ~

APPRdI' ED: ' ~LABORATORY MA .ZR'

556

_ ~T A ti) C . (-jSSFL ANALYTICAL CHEMISTR Y

IIOI m u imi i iumm i im i DI D IB NA01476246

I IHDMSE00624520

cc : K. Scn.aed

V . Francis D/564, FB 66

U . NeuANALYSI S

REPORT

To: P .AMT SERVICE S

FRO" SSFL ANALYTICAL CHS![ISTRY

R : IAG BK ' p 3 PAGE 6 8

DEPT./ GROUP : D/031

LOSNO-

4- 216-83

PHONE 5447

DATE 6-MAY-3 3

LOG NO.SAMPLE

IDENTIFICATION PQRCB L TRAP GC/ BBSULTS (PPM)

Water sample fro, the Using the oonoentrstian techniques and method, ap-proved under the guidelines stated in the current

pond at SSFL XPDES Permit, the following VOIATILE ORGANI CCCR[POUMS were fatmd :

Rocket dyne .170Acetone (CB30D 3) _ .

Freeboard = 3 it Sromodichloromethane (BrCHC12) = ND< .00

d 0 0Q4514

MlSCarbon Tetrachloride (OC14) = NP<.DO 1

amp e4//5/8 3

--

Chloroform (CBCI3) _ 0,00 2. ,

'CD W0LB

Methylene Chloride (C%C12) = ND-1 , 60 /. 5y :

1,1,1-Trich.loroethane (C83OC13) = 0 023

RECEIVED 0 LAB : Trichloroethylene (Cl( 0.059

4 / 15 / 9 3 Tetrachloroethylene (C12C :C7C12) _ 00/

1,2-Dichloroethylene (C1CS :CRC1) _ C).OZ ONotation about appear-

D b 0 001ance of the sample : roeochloromethane (ClCBBr2) = .i

Isopropyl Alcohol ; also (CE3CWHC83) = 0.14'known as IPA ; 2-propanol

Freon TY (CI2FCCF2C1) = 0 . 1 7

l,1-Dich2oroethane (Cl2CVM3) 1) <, 00 !

CCI M3DTS : Tatrachloroethylene is also known as perchloroethylene . (1) Monitoring specifi-

cally required according to the Rocketdyne NPDZS permit , Order $ 76-146, NPDES 0 CAD001309from the California Regional Water Quality Control Board, Los Angeles Region .

( 2) This supplementary information is provided in accordance with 40 CFR 122 .60.

PPM - PARTS PER MILLION

. Lass THAN ND = NOPr DETECTED DNA = DOES NOT APPLY TR s TRACE

APPROVED

Form 619-V

EB NA0147624 7

IV~To CHEMICAL

i awo~~ d.No Fli/ wo Manager SSFL ANAL CTRL CAM-ffSTRY UNITSSFL Anatw ' Cho wft

4 V

HDMSE00624521

F/55CK•f (.F , 4/5

cc : A. Scharue dY . Francis D/564, TB 66

M . Mogg

To: PLANT SERVICES

FRO" SSYL ANALYTICAL ' flSTRY

REFERENCE : LOG Bag ' S 3 PAGE 6 8

DEPT. J G RO0JP :

PHONE 5447

DATE 6 - MAY-8 3

LOG NO .SAMPLE

IDENTtfICATION PURR & TRAP © GUNS RESULTS (PPM )

Water sample frog the Using the concentration techniques and methods ap-

9 21 51 -provedproved under the guidelines stated in the curren t

5 - g3- pond at SSPL 1IPQ35 perui t , the following VOLATILE ORGANI COOMPOQk® s were found :

Rocketdyne .A t ( CE 000k3 0 2 1ce one 3 3) = .

Freeboard a 0 ft//

Bromodichlorome thane (BrCBC1.2) = V .00 3

d O $45ANS lCarbon Tetrachloride (CC14) = ND /- .00 1

amp eChloroform (Cacl3) _ , 005

LLB 1(inCMethylene Chloride (CK2Cl2 ) = NV 00 f

y : . so1,1,1-Trichloroethane (cCC13) = 0 .r/3

RECEIVED Q LAB : Trichloroethylene (C1CB :OC12) - . Oq

15' / $3 Tetra chloroethylone (C12C :CC12) = ND< .~O !

1,2-Dlchloroethylene (ClCz :CBCl) zNotation about appear-

ance of the sample : Dibromochloromethane (C1CBBr2) = 0. 003

Isopropyl Alcohol ; also (C83Cg3HCR3) = 0.28known as IPA ; 2-propanol

From TF (C12FCCF2C1) = 0. 6,1

1,1-Dichloroethane (C12CWC93) _ .00.1

COMMENTS : Tetrachloroethylene is also known as perchloroetbylene . (1) Monitoring specifi-

cally required according to the Rocket dyne NPDkS permit, Order # 76-146, NPDES # CA0001309


(2) This supplementary information is provided in accordance with 40 CFR 122 .60.

PPA = PARTS Pk B MILLION

DKA ■ DO ES 1* )T APPLY TR a TRACE

SSFL AML ICAL Ct ISTRY UNI T

I . rm619-V

EMBNA0147624 8

ss rlCHEMICALANALYSISREPORT

LOGNO-

- z1 -5 -83

D/031

I IHDMSE00624522

LOG NO .

CHEMICAL ANALYSIS

REPORT



REFERENCE : LOGBOOK '03 PAGE Gg'

3- .2 ic - 8 3

DEPT/GROUP D/556

PHONE 5447

DATE /5 4P,€ J~• ~


GAS : .'IEL / L) M

REC'D : / / APki k3

SAMPLER : _FLO%aZ_ _

PRESSURE /' 95 P510 T G / (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

FRONT :



COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILER

OTHER : 1-A E - / 3

63- 3COMMENTS : *Maximum allowable limit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or 02

APPROVED

Fore 61a-y

EBNA0147624 9

SSFL ANALYTICAL CHEY.ISTRY UNI '

HDMSE00624523

LOG NO .


TO : QUALITY ASSURANC E


DREFERENCE : I 10GBOOE 83 PAGE G'O

PHONE 544 7

DATE /5 AP'e 'P3


GAS : N/ 7 /C O (:~5A/

RECD : 4P,el 83

SAMPLER : FL-00431 9

PRESSURE 1750 PS/4 7 G / (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED


AS METHANE ONLY

FROM :

SSFL SUPPLY LINETat = TRACE ND = NONE DETECTED < = LESS THA N

ALFA BRAVO > = GREATER THAN DNA = DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILE R

OTHER : NL-l3 /

COMMENTS : * Maximum allowable limit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2 , and 26,3 ppm in N2 or o ;

APPROVED

Form 619-V

SSFL ANALYTICAL CHEMISTRY UN I

BNA0147625 0

- a2i/-d'3

DEPT/GROUP D/556

HDMSE00624524

CHEMICAL ANALYSIS

REPORT

LOGNO •

z/-2/0-b-3

DEPT./GROUP 03 1

L oq book '63-p 68

PHONE S4 4. 7

DATE A p rd 16,1163

LOG NO .SAMPLE


4 -210-83 Hazardous Grease 13 47')aster

CLUkG - er ✓e d

4-I~-83 B.7ca .M .

SSFL APIA ICAL 6UNISTRY UNIT

rG : u+ air ,o/ ,i- ,, o FA 2'f


TO G . SAUERLE

FROM SSFL ANALYTICAL CI3D6ISTRY

REFERENCE : LOGBOOK ' 83 PAGE 6 S

PHONE 4824

DATE I s .r 3

LOG NO .SAMPLE


4-207-S3 I .D. #= tH MEASURED PRESSURE = Q• 1 :m

SAMPLE #'_ 02= O.O( N2= 0.07 am

FLASK N = y' He = 4 .2 C12 = 112 am (1 .1 )

PRESSURE _ '. 7 To k,~ H2O = 0. 0 am

- - - - -

_ x 0 f - 3

- - - - - - - - - - - -

I . D . 4+ = -# 1

- - - - - - - - - - - - - - - - - - - - - - - - - - -

MEASURED PRESSURE = 11. IJ Q

SAMPLE 02 - R2 = r.♦ a< < o l~mm

FLASK 0 He = '. mm Cl2 = /~ ( mm (j. 0 )

PRESSURE = I >f . 3 TO (4 H2O = 0. 0 3 am

- - - - - -

q- - 2 V t- 97

- - - - - - - - - - - -

I . D . # _ -03

- - - - - - - - - - - - - - - - - - - - - - - - - - -

MEASURED PRESSURE = 17 .0 mm

SAMPLE #r = *3 02 = _s, I mm N2 = ! ma

FLASK 0 = It He = !0. '*C12 = z• mm

PRESSURE _ Tct:A. a20 = Q, 07 mm

- - - - -

p et v

----------- -I .D . 0 =

-------------------------- -MEASURED PRESSURE = mm

LO It/13 SAMPLED = 02 = N2 = mm

FLASK= He= mm C12= am ( )

PRESSURE = psia 020 = mm

;.OMMENT5 :

APPROVED

S5FL AKALYTICAL CF.D!IS7FY' UNI T

BNA0147625 2

CHLORINE VALUES IN PARENTHESES ARE NOT CORRECTED FOR MANIFOLD SAMPLING LOSSES

AND ASSUME CON'VERSI0N TO CHLORIDE PRIOR TO TEE CHLORIDE DETERMINATION . ALL


CHROMATOGRA PliY .

A/.it ; I •) M 4 . 1 o+l -k~Jt 1iw J, c to S In A& #,q O tV+I -.al: :a

st4r-

LOGNO-

L~! *4t - 207- Y 3t.,J•7- s a

DEPT.%6ROUP D/522

HDMSE00624526

CHEMICAL ANALYSIS

REPORT


PHONE 5 44T

DATE APRIL- J5 . 1 943

LOG NO .SAMPLE

IDENTIF CATION0 .3 mg+RESULTS

TRICH for NYR per

RL10001-F

--203-83

E'aRi No . `1372 7

BLANK • mg/ 500 ml

RAAD5IAP~Iii) ~o= mg/ 500 ml

PROM FGNSlt ofF~ 77 /N4-5

EWR N1o . !f 2.8( j(e

BiAm ma/5o0 ml~--2 04 f$

\RAFtD4fARS ' • 3 m/500 ml

o~tn ~-u7yG G Q► 4S kiT

EWA No . 9Z Ff(w

BI.A .YIC mg/500 mly-2

\HARDSJARE ' O~~- mg/ 500 ml

y' RvM GLcl'J~

e 4 Fc - s~4~

Ree' d . __i~hf

SSFL Analy Ical Gnsm!stry


43724 7INSPECTION UIRE D

'

A PPLICABLE DRAWINGS (ATTACH IF REQUIRED, REQUESTED COMPLETION DAT E

YE S Z NO A - 7 -jDOING DEPT . LEDGER ACC UNT GENERAL OACER G .O . ITEM & MCR INIT . GROUP NDW . OR TASK DOING GROUP ACTUAL COMPLETION DAT E

REQUESTED BY EXT. FACILITY SHIFT REQ . SUPERVISION ESTIMATOR ESTIMAT E

LHOURS MATERIAL S

REQUIRED REQUIRE DLAB SUPERVISION

ASSIGNED TO: LEADMAN MECHANIC S

SHOP I LAB i

INST13.7CTIONS ! BE SPECIFIC)

(l L c / ~,v t r'~~;

NOTE- THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY

Z37 2L Cv

mar= r- < < ',\-C- P.-~ L u3~

r

RECEIVED @ LAB

APR 1=U 1983

SSFL ANALYTiCA CHEMISTRY(/"

z4 , Z, () --~ - ~ ~

FORM R 94.L REV . 6 .57

LIST OF MATERIALS

I IBNA01476254

C'+ZT I ' r1' G L-Qc'

HDMSE00624528

CHEMICAL ANALYSIS

REPORT

r-mmmumm"u-LOG NO .

4/-3/-4p3

DEPT /GROUP SSA;.

PHONE S4 1

DATE gP/ty l- 'a3

LOG NO .SAMPLE


F40LO FQEOAJ Tic (C/y Fee, F d/) = 7. 5 PpAlA 40A4 .43 £Al ~JIA4 6 y v41- u u

S vPPL y

ICo K Pe 4F6 A)

Ca A-Jr5AJ T P--)t

leL /00/2

SAMpGE .EEd~o

5 APi'it. '&

SSFL ANALYTI L CHEMISTRY UNIT

iimm u imi i iumm iimmmmmu


LOGNO-

'0 -83

To

-30 -63


PHONE 5447

DATE APRIL 60

LOG NO .SAMPLE

IDENTIFICATION0 .3 mgRESULTS

TRICH for NVR pe r

RL10001-F

E'WR No . 50-368y

BLANK 8 • 0 mg/500 ml

HARDWARE mg/500 ml

EWR No . 5R3 884

BLANK mg/ 500 ml- .3 0 - 83

xARDWARE 8 . 3 mg/500 ml

A MM"N

0 .

BLANK mi

HARDWARE mg/500 ml

MANAGER

Rec'd . s 8.j

SSFL Analytl al Ch mistr y

iimm u imi i iumm iimmniiumu

R . Schmued . D/564, FB 6 6

J . Bowma n

n CHEMICAL ANALYSISM

. MoaREPORT

C . WINZER, D/031, SS 12

K . Johns, D/031 ,

LOG NO

SS 1 2

-4 - 2 6 - 83

TO: DEPT./GROUP


REFERENCE : I-nv"innk 83 Page 60

PHONE 544 7

DATE 14- APR-6 3

LOG NO .SAMPL E


PPM FLUORIDE , BY ELECTRODEWATER SAMPLES FORFLUORIDE ANALYSI S

BELL CANYON

time=

L£TF DRA/NA6E O. 3 pp P-,time` //2O .1

time=

time=

time-


41 S / 8 3

DAY= TUESDAY EPA distillation method



APPROVE D

F1c

M1BNA0147625 7

S-SFL A .' -',`T1CAL CHZMI-STR'~ ','NIT

I I IHDMSE00624531




To: C . W1uZE R


DEPT./GROUP :

REFERENCE : LOG BK ' 83 PAGE 60 NOTEBOOK -

LOGNO •

4-14-83

D/031

PHONE 544 7

DATE 6 -APR- 63

LOG NO .SAMPLE

IDENTIFICATION PURGE & TRAP O GC/MS RESULTS (PPB )


Bproved under the guidelines stated in the curren t

4 - 14 - S3 S P pond atA SSFL NPDES permit , the following VOLATILE ORGANIC

COMPOUNDS were found :Rocketdyne .

Acetone (CH3COCH3 ) = AID .4 0

Freeboard = ft Broaiodichlo romethane (BrCHC12 ) = N1 /

45Carbon Tetrachloride (CC14) = ND . /

Sampled @ 8 A/'1Chloroform (CHC13) _ N < I

I . Co//ins .By :

Methylene Chloride (CH2C12) = N~ < /l,l,l-Trichloroethane (CH3CC13) = NQ< /

RECEIVED @ LAB : Trichloroethylene (ClCH :CC12) _ 3

63 Tetrachloroethylene* (C12C :CC12) = ND -

1,2-Dichioroethylene (C1CH : CHC1) _ NO ,< /

Notation about appear-(C1CHB )hance of the sample : r2Dibromoc loromethane

Isopropyl Alcohol ; also (CH3CHOHCS3 ) = ND' /Oknown as IPA ; 2-propanol

Freon TF (C12FCCF2C1) = N

)

( /

1,1-Dichloroethane (Cl2CHCH3) =

CO? ENTS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifi-

cally required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES # CA0001309

from the California Regional Water Quality Control Board, Los Angeles Region . (2) per (1)

"Wastes discharged shall not contain phenols, mercaptans, or other substances in concentratior

which would impart taste, color, odors, foaming or other objectionable characteristics to re-

ceiving waters . . .", "or any substance in concentrations toxic to human, animal , plant, or fist

life ."B = PARTS PER BILLION

1< = LESS THAN ND = NONE DErECT2 DNA = DOES NOT APPLY TR = TRACE

APPROVE D

firm 619-V


Qx,~SSFL ANALYTICAL CHEM STAY UNI T

BNAO147625 8

HDMSE00624532

ENGINEERING WORK REQUES TTITLE OF JC S

INSPECTION REQUIREDAPPLICABLE DRAWINGS (ATTACH IF REQUIRED)

DAT E

YES NO Ul

DOING DEPT. ~ LEDGER ACC UN T

REQUESTED B Y

YY11 - A,A

SUPERVISION

GENERAL ORDER G .O . ITEM 8 MCR 1N11 GROUP ~ HOW . OR TASK DOING GROU P

EXT . I FACILITY

LysASSI ON ED TO :

SHIFT

SHOP I I LAB

REQ. SUPERVISIO N

IESTIMATOR



ESTIMATE


$EADMAN 1 MECHANIC

INSTRUCTIONS IBE SPECIFIC) NOTE: THIS FOR M

g 563 Spa- A9.e -clLZ,

ti`- S"-83

WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

RECEIVED @ LAB

RPR 51983

SS FL ANALYTICAL CHEMISTRY

s3__I ,2 , (o 0

FORM R 94 .L REV 5 .57

LIST OF MATERIAL S

BNA0147625 9

HDMSE00624533

EQVTP! -VW LAB

FROM : SSFL-ANALYTICAL CRf]HISTR Y

REFERENCE : LB-" -' P. too

PFIONE 544T

DATE M,4 ' / 6 . 19 83

LOG NO .SAMPLE

IDENTIFICATION+ 0 .3

mgRESULT S

TRICH for NVR per

`5 rs3 RL10001- F

FWR 1o. 5 b3 88a

BLPNK mA/500 a1

HARDWARE 11Y • 3 mg/ 500 mi

z A/V /N

!W No. $b388a

HLA:tx 71-3 mg/ 500 m1Bj

HARDWARE 2d500 ml

No.

ffi,ANic m].

HARDWARE mg/500 ml

COMMENTS .

APPROVED

KJOAC.ER


Ree' d . 4 - 4 -83

SSFL Anal tlcal 04qmtatry


R50388 0N oI,3--30 _g3 -INSPECTION REQUIRED

APPLICABLE DRAWINGS ( ATTACH IF REQUIRED ) REQUESTED COMPLETION DATE

S NY „F _ JSOE I

DOING DEPT LEDGER ACCOUNT GENERAL ORDEP --- . ITEM B NCR INIT . GROUP HDW . OR TASK DOING GROUP ACTUAL COMPLETION DATE

3 q I--I

I _ ---REQUESTED BY EXT . FACILITY SHIFT REQ . BUPERV ISION ESTIMATOR ESTIMAT E

/ /c

HOURS MATERIALS•CYII LLL_-J REQUIRED REQUIRE DLAB SUPERVISION

ASS I GNED TO: LEADMAN MECHANIC $

SHOP ! I LAB I I

INSTRUCTIONS ( BE SPECIFIC) NOTE: THIS FORM WILL REUSED FOR NON-DELIVERABLE ARTICLES ONLY .

~lw k 563 99 o'~{- 4J t J_~/ - 5 " 83

,2

3 3o -B 3

RECEIVED @ LAB

w- 2 ,, 1983

SSFL ANALYTICAL CHEMISTRY

LIST 0I MATERI AILS_~.

BNA0147626 1

HDMSE00624535

/JF

R . Sch,7ued1D/564, FB 66 K. Johns, D/031 ,

SS 1 2J . Bowa n

FranMog

,CHEMICAL ANALYSI S

,REPORTC . WINZER, D/031, SS 12

LOG N O

9 -9 -83AM D

-4-10-e 3TO: DEPT./GROUP


REFERENCE : 1,nvhnnk 83 P4 13 G 60

PHONE 534 7

DATE 5 -APR- 8 3


WATER SAMPLES FORPPM FLUORIDE , BY ELECTROD E

FLUORIDE ANALYSI S

BELL CANYON

time=

-9- 83 R i 3.1xlD69al /, Q /o/vrn

time= 9qS

A/f

I-/D-83 /NL%T TO R l Q, ~Pr>r1

time=-

t ime =

time=


and analyzed ASA P

4/5/83

DAY= Tu ESDAY tillation metho dEPA di s

r"OM ME NT S : The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVED

SSFL AN=,LYTI AL Ci

BNA0147626 2

HDMSE00624536

cc : DEPT . 556 D. C . Akeson , D/594, DA 86

CHEMICAL ANALYSIS

REPORT

TO: 5 . T . YOHE

FROM: SSFL ANALYTICAL CH ISTRY

REFERENCE : LB- ,R . P. ~ C

LOG NO .

'- ?-&3


LOX

ALFA I

PURITY ONLY

TEST # o / Q

SAMPLER # N& 3 7,3,1(0

FL

/ 9 o PSIG

0^

COMMENTS :

APPROVED

RECEIVED :

"7'/ / 3

L

DEPT./GROUP 598

LOGNO •

4/- :-8 ,5

PHONE5 1+ T

as

DATE lv o 0 ~~ 4

RESULTS

9 OXYGEN By VOIA}

LABORATORY/MANAGER SSFL Anatytlcal Chemistry

I IBNA0147626 3

HDMSE00624537


LOG N O

PHON E 544T

LOG NO .SAMPLE


Wastewater, Canog a

2~$3 Site L, D/514 Scrubber Chromiu.L-n 2 7 pi, / zSump P H

Grab Sample taken

o-73O

S

ZWZceived


iimm u imi i iumm i iuuumi i iu mu

CHEMICAL ANALYSISREPORT l---93

TO: M_ uoea DEPT./<3 O1JP 56. 4

PROD SST[. AMLYfICAL CHMISTILT UNIT plOt4E 5447

REFERENCE : Logbook ' 83 pg . (o(] DATE 7 y /

LOG NO .SAMPLE


1-S3 Wastewater , Canoga Chromium N~~. O . (~ vYt9 /G

Site B , D/544 Process pHCla ri fier

G QAsample

S110 41)u l

Ca, 030

Sample received


chromium

COMMENTS : The L .A . city discharge limit for chromium is 10 mg/LAnalyses per N . Nogg ' s IL 81 FE-422, 27 Oct . 1981

APPROVED ,

V . rm419-V

S3TL AKALYTICAL MWSTlY UNI T

BNA0147626 5

:A C1A

HDMSE00624539

IIDI muimiiiummiiuuumiiumu

TO G . BAUERLE


DEPT./GROUP D/522


REFERENCE : LOGBOOK 23 3 PAGE S 0

LOSNO •

3- S73-g33 -S7~ _ g 3

PHONE 4824

DATE .

GNSAMPLE


I .D. # = 3 - 31 - l A MEASURED PRESSURE = 5-~ mm

SAMPLE # 02 = /. ( .. N2 = DI mm

F

FLASK # He = am C12 = 0 . 3 7 mm 0.33j

PRESSURE psis H2O am

3- - - - - - - - - - - -

I . D. # ,3 - 3 I - / 2)

- - - - - - - - - - -

MEASURED PRESS URE =

- - - - -- - - - - - - -

as

- - -

SAMPLE # = 2- 02 = /o. 7 am N2 = mm

FLASK # _ He = C2 mm Cl2 = /U7) GD•O I mm (N~ )coo l

PRESSURE = psis B2 0 = 0 3 mm

I .D. # = MEASURED PRESSURE = mm

SAMPLE # = 02 = an N2 = mm

FLASK # = He = am CI2 = mm ( )

- - - - -

PRESSURE = psis

- - - - - - - - - - - - - -

H2O =

- - - - - - - - -

mm

- - - - - - - - - - - - - - - -


SAMPLE # = 02 = ma N2 = mm

FLASK # = He = ma Cl2 = mm ( ) '

PRESSURE = psia g 0 =2

mm

COMMENTS :

APPROVED

rc E,c_`,

I-- _ aMA NA --, ER

MEBNA0147626 7

CHLORINE VALUES IN PARENTHESES ARE NOT CORRECTED FOR MANIFOLD SAMPLING LASSES

AND ASSUME CONVERSION TO CHLORIDE PRIOR TO THE C HLARIDE DETERMINATION . ALL


CHROMATOGRAPHY .

LQ 0

sSF L'! 1 ICAL CNEY ISTRY LN :"

flmHDMSE00624541

R . Schmued D/564, FB 66 W . Baisley , R . Knight, D /598, SS 1 1

J . Bowman1Franc

CHEMICAL ANALYSIS

REPORTC . WINZER, 0/031, SS 1 2

TO DEPT./GROUP


REFERENCE : Lnahnnk 83 Pnae 56

K . Johns, 0/031 ,

LOG NO

ES 1 2

3-57c- 3

PHONE ___

DATE 4-APR-93

LOG NO .SAMPLE



3-57 g3 BELL CANYON O. 7 mPtime

~s= z PM

P

time=

time=

time=

time=


3,3(1 8 3

DAY= THVRSDAY *s EPA distillation metho d



APPROVED

MANAGER

i i

cc~I ANA? VTTr~

iimm u imi i iumm i im i IDOl 0 I DI D IBNA0147626 8

H D M S E00624542

CHEMICAL ANALYSIS

REPORT

To:

FROM

: aA ~o f ,►


REFERENCE :

PHONE s 7

DAT E

LOG NO .SAMPLE

IDENT{FICATIQN RESULTS .L Y We i f b f

3- S~9-ss N TO s~ .Mr i~ f.~eM`'t'/oNO O,

cc[L 21 a ~~N

TAW k NV : 2 .2. Ma ~~

F. = 0. 3 1 ^~~ /ky NTO

A C = 0. o s M r/k' AlT O

/-o = TK .~ o. O /

~R D; o .!!M 9/ NW .

CM = o. 0 U' g/h y N TO

0, 0 9 2 //c N W3 3r )~ 3

COMMENT 5 :

APPROVE D

Form E1y--V

Norma FuuA Manage'SSFL Anai ,ca/ Chernutry

LOG NO

~- S(' - ( 3

DEPT./GROUP S 9 E - d

SSFL AML'TICAL C)-IEM ISTRY URI T

IIDI muim i iiu mmiiu uum iumiu

cc : 1? . Franci s

G . ShanksTO DEPT./GROUP


REFERENCENotebook 0330, p . 31

LOG NO .

PHONE 3293

DATE1!4!84

LOG NO .SAMPLE


3-568-83 Unknown liquid from The sample was found to be a clear, colorles sNAKA, Drum # 22, liquid with a very pungent odor . The liquid

burns with a yellow flame, producing white smoke .

Received : 3/31/83 The sample is miscible with water, and shows a p H

of about 3 when tested with pH paper . The infrare dspectrum is very similar to that of trimethyl

phos phi t:e .

The sample was sent out to IT Analytical Service sfor GC/MS analysis . The following was reported :

Trimethyl phosphite 540

Dimethyl phosphonate 310Trimethyl phosphate 20Not identified 13%

Emission spectrochemical analysis showed 2100 pp m

silicon, 290 ppm aluminum, 61 ppm tin, and 16 pp mtitanium .* No other heavy metals were found to b epresent in significant quantities . Fluoride i s

present at the 1 mg/1 level .

Elemental analysis showed ; 26% carbon, 7% hydrogen ,

24 .5% phosphorus, and 340 oxygen, with less tha n

0.005% nitrogen .


most likely composed of those compounds identifie d

by GC/MS and listed above, along with othe r

unidentified similar compounds .

* Emission spec, performed on ignited residue

volrtile components may not have been reco ered .

COMMENTS :


Fprrr F~s-v


CHEMICAL ANALYSIS

REPORT3-568-83

598 SS 11

H D M S E00624544

cc : H . Francis , D/564, F 3 6 6

CHEMICAL ANALYSI S

. Fi SCM-VEQTD E . Shank s

FRaM

REPORT

SSA L ANA LYT I CAL C3W STRY UNI T

REFERENCE :

LOG NO

Notebook 0330 . case 2 9


Unknown liquid foridentification .

3-566- 83! Sa'.pie '20EWE. c 34625 0

Received : 3/31 /8 3

COMMENTS :

APPROYEB

LOG NO

3-566-8 3

DEPT./G *JP 59B, 5511

PHONE 329 3

DATE June ], 1 98 3

RESULTS

The sample consists of a clear, ambercolored liquid which burns only while aflame is applied . Emission spectrophoto-metry revealed no significant levels ofmetals present . The infrared spectrum wasvery similar to trichloroethylene . Thesample was not water soluble .

Based on the above information, thesample is probably trichloroethylene .

SSFL A)(ALYTICAL CSEi1S" RY WI T

1 .rm fi'~JV


HDMSE00624545

CHEMICAL ANALYSIS

REPORT

TO ~

FROM

J . Rosengard

SSFL ANALYTICAL C1iEMISTRY UNI T

REFERENCELogbook '83, p . 58-59

539DEPT./GROUP

LOGNO •

3-564-83

PHONE 3293

DATE4/20/83

LOG NO .SAMPLE


3-564-83 Freon TF used for 200 ml of the sample was evaporated , and the

flushing ACE FUEL residue analyzed by infrared spectroscopy .

line(s) on Peace - The residue was found to contain 0.11 mg of

keeper Stage FPT-2, hydrocarbon (as Nujol, the reference std .), and

less than 0 .2 mg of paraffin ( as the std, pro-

Serial Number : vided) .

4877068The residue was not colored .

Results are corrected for the blank reading ,

which was obtained on "clean " Freon TF submitted

with the sample .

Received : 3/31/83

COMMENTS :

APPROVED

V orrn 619-V

s sF~L N4 I .,rT ICA L a 1 STRY WIT

IIDI m u imi i iumm i im i V I DBNA0147627 2

EB 37

I IH D M S E00624546


TO: J . Rosengard

FROM SSFL ANALYTICAL CS811ISTRY UNI T

REFERENCE :Logbook ' 83, p. 58

DEPT. /GROUP

LOG NO-

3-562-8 3

539 EB 37

PHONE 3293

DATE4/22/83

LOG NO .SAMPLE


3-562-83 Freon TF submitted on 200 ml of the sample was concentrated and analyze d

3/31'83 for use as by infrared spectroscopy. It was found to contai n

blank in the analysis 0 .059 mg of hydrocarbon as Nujol, the referenc e

of samples 3-545-83 standard . No paraffin was detected (less than

through 3-564-83 . 0 .2 mg/200 ml, as the reference std, submitted) .

The hydrocarbon value was subtracted from the

hydrocarbon values obtained on the samples .

COMMENTS :

s

APPROVED ,SSFL LYTIGLL CHL[ISTRY UNI T

IIOI m u imi i iumm i im i ID IBNA01476273

I IHDMSE00624547

TO :

FROM

M . Mogg

CHEMICAL ANALYSIS

REPORT

DEPT./ GROUP 5 +

SSFL ANALYTICAL CHEMISTRY LI T

REFERENCE: Logbook ' a~ pg. c R

LOG NO -

PHONE 5Z 'T

DATE

LOG NO .SAMPt.E


C!3Wastewater, Canog a

Site L, D/54 Scrubber Chromium - 282 ivVC/L

Sutap pR (~ C}

Grab Sample taken

3/3//83

Sample Received 3 /3'JIOas

Analyzed or pH, and

chromium

COMMENTS : The limit for Site L is T5 ~g/1 •

APPROVED

orrn 619-V

SSFL ANALYTICAL CHF]HISTRY UNI T

IIDI m Ii l u i I i Iumm i Iumuu i III I U


4. "4ogg

LOG N O

3-5(o--g3

DEPT./GROUP

FROM SSFL ANALYTICAL CHELIISTRYUNIT Pt-BONE

REFERENCE= Logbook • Fs3 ci . g DATEl7/f /g3

LOG NO.SAMPLE


3-5o-3 Wastewater, Canoga Copper - Q, 07 ng/ L

Site C, "See t~orld" Nickel - O . 53 mg/L

- ' 221 hr . Prooortioaal ,Sa-rte token

3/ q43- 3/3'/ 3

le received

102.Salyzed for copper, pR

nd nickel

COMMENTS: The L.A. City discharge Limit for copper is 1.5 c&'l, for nickel the Limit is12 cng/l .

APPROVED

Analyaea per N . Mogg 's IL 81 ?!-L22, 27 Oct . 1981R.D. • lions detected

Q4SSFL ANALYTICAL C{ .4ISTRY UNI T

IIOI m u imi i iumm i im i I D IBNAOI 476275

I IHDMSE00624549


TO:

SS?L AMLYT I CAL QtAtI STRY WiI T

RErwRENCE ' Logbook ' $3 pg . 5

LO3 hO .

3-559-R3

OEPT./ 3RUljp 564

PI1OIVE 5447

DATE

LO NO.SAMPLI

IOENTIfiCATioN RESULTS

-~3 Wastewater , Canoga chrome+~ N Q

Site B, D/544 Process pH = -z 2

Clarifier

24 hr. Proportiona lsample

3f3g23 -- 3 f3/lg.

Sample received 3/3/~0 2S


GOMM~-`MS: The L .A . city discharge limit for chromium is 10 mg/L

Anslysea per 11. Mogg's IL Si FE-422 , 27 Oct . 1981.

A /APpROVED _ r QLQ_) -I ,.~ _ t •

SSIL AMLYTIGL OtOL1STU I3MI T


HDMSE00624550

CHEMICAL ANALYSIS

REPORTJ . Rosengard


REFERENCE : Logbook '83, p . 56-59

DEPT/GROUP 539

LOG NO •

3-531-83through

3-558-83

EB 37

PHONE 3293

DATE4/20/83

LOG NO .SAMPLE


Freon TF used for 200 ml of each sample was evaporated , and theflushing ACE residue analyzed by infrared spectroscopy for th epropellant lines on following constituents :Peacekeeper Stage

FPT-2 . (OXIDIZER

SIDE) mg Hydrocarbon(l) mg Paraffin(2 )Serial Number per 200 ml per 200 ml Notes

3-551-83 4877069 0 .15 ND L 0.2 -

3-552-83 4877071 0.06 ND G 0.2 -

3-553-83 4877068 0.09 ND < 0.2 -

3-554-83 4877073 0.02 ND < 0.2 -

3-555-83 4107338 0.13 ND < 0.2 yellow residue

3-556-83 4877075 0.04 ND < 0.2 -

3-557-83 4107335 0.05 ND 4 0.2 -

3-558-83 4877076 0.06 ND < 0.2 -

Received : 3/31/83 (1) as Nujol , the reference standar d

(2) as paraffin, the reference standard provided

All results are corrected for the blank reading ,

which was obtained on "clean" Freon TF submitte d

with these samples .

less than

COMMENTS :

APPROVED

Vorm619-V

,4

E RBNA0147627 7

SSFL Jl LYTICAL CUMSTQY UNI T

HDMSE00624551


FROM

J . Rosenga rd

SSFL ANALYTICA L CHEMISTRY UNI T

REFERENCE : Logbook '83, p. 56-59

PHONE 3293

DATE ,4/20/83

LOG NO .SAMPLE


Freon TF used for 200 ml of each sample was evaporated , and theflushing ACE pro- residue analyzed by infrared spectroscopy fo rpellant lines on the following constituents :Peacekeeper Stag e

FPT-2 . (FUEL SIDE) .mg Hydrocarbon( l) mg Paraffin(2 )

Serial Number per 200 ml per 200 ml Notes

3-545-83 4877075 0.06 ND < 0.2 -


3-547-83 4107338 0.07 ND ( 0.2 yellow residu e


3-549-83 4877073 0.22 ND L 0.2 yellow residue

3-550-83 4877069 0.56 ND C. 0 .2 yellow residue

Received : 3/31/83 (1) as Nujol, the reference standard

(2) as paraffin, the reference standard provided

All results are corrected for the blank reading ,

which was obtained on "clean" Freon TF submitted

with these samples .

less than

COMMENTS .

APPROVED

!Jrm 619-V

EBNA0147627 8

LOG NO .

3-545-83

through3-550-8 3

DEPT./GROUP 539 EB 37

SSFL Ali iYTICAL CH MY UNI T

HDMSE00624552

R . Schmued I D/564, FB 66 W . Baisley, R . Knight, D/598, SS 1 1

owma n

M

:a


K . Johns, D/031,SS 1 2

LOGNO •

3- 5-i 0 -e 3TO

3-54Z-8 3C . WINZER, D/031, SS 1 2

TO: DEPT./ GROUP

FROM : SSFL ANALYTICAL CHEMISTRY UNIT PHONE 544 7

REFERENCE : I -hnrk O 3 rA4(? DATE 4- APR -8 3

LOG NO.SAMPLE



FLUORIDE ANALYSI S

BELL CANYON

time=

3 -5-40- 83 PP 98'oooya lt

1, / p prvitime= 92 A M

3_54 r- $3 SPRAY RuaoFF/ z PPS''

time= $ uA N!

3 -572'83'Z•5 ~w ;1~ro.~ galR1 / 2 ~p~pm

time= S '_____

time=


3131 / 8 3

DAY= THURSDAY= EPA distillation method

COMMENTS : The NPDES permit òr SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVED C ~~ M

u i iBNA0147627 9

HDMSE00624553

cc : M . Mogg D/564 FB 66

R . Schmued

M Francis'

K . Johns D/031 SS 1 2

LOG NO .■

J . Bowman CHEMICAL ANALYSI SREPORT

TO :

FROM :

nzer DEPT./GROU P


REFERENCE :Logbook '83, p . 56

PHONE 544 7

DATE

3 *-538-83

SS 12

3/31/8 3

LOG NO .SAMPLE


3-538-83 Water sample from Trichloroethylene = none detected, less than 1 ppbBell Canyon, sampled

at 1 :00 pm, 3/30/8 3

Received : 3/30/83

COMMENTS :

APPROVED ,

0 -~ rm 619-V

SSF11 LYTICAL CHEMISTR I' UNI T

BNA0147628 0

HDMSE00624554


LOG NO .

3- c73- 1 37N '*-

3- S7r - a ?

TO : A. VA j, N KbtDEPT./GROUP 52 1


REFERENCE :, L L 3

PHONE S 17 7

DATE ,

LOG NO .SAMPLE

IDENTIFICATIONl

RESULTS G W•I'~g o f

kJA OH t NA t l

NA, S 0~ t '42'k

AA X foot-(

3-533-x3 ' 3! /VA OH = 0, lc 2

NA cc = 0. 't77 -NA soY = 0 . 0 S4~►

1, 't- Its A 0.

S-10 # A'A O N = 0. /q 3 %

N A Cl = 0,6 0 11,

1VAA 50'~' 0 . V 9ff

3-53 43 32 14 82 01 D. 3 2

i C

3) io/s 7

COMMENTS :

APPROVED

A o,rrw Fuj aw ManagerS.S .!

S~EL ANA-'f-,ILA . CHEMISTR Y U --.T

I IBNA0147628 1

HDMSE00624555

CHEMICAL ANALYSIS

REPORT

L 883-

LOG N O3 -Tj'2',-$ ?

DEPT/GROUP 5, A

PHONE S I ~f 7

DATE '/ ?/ f .3

LOG NO .SAMPLE

IDENTIFICATION RESULTS Js 1-e, , A ty

NA OR-► Kntt i

A/ A2 SOY t N, 02

Mtx tvk-(

3 - 511-`61 X 2 11 N A ON = o. 2 Off

N Ct = 0, 6 S

NA 2 5D, D, ll ! r

3-~3o 3 ~yA 92 ox 0. S 3 2

. .531-4330 NA ON y

NA ct - 0 . 6 2 q ;.

NA2 50~ 0. 103 I'

3 _ 53, -43 30" N2 02 = 0 . 6 1~ y

JQec /

Nf917:tiOr!Ifu i ;ipiculu Mu'tJQQ'

SiFL ANALI"IiCA C EW1 T}tl L T

I I

R . Schmued ~ D/564, FB 66 W . Baisley, R . Knight, D/598, SS 1 1

J . Bowma n

M. Mog


C . WINZER, D/031, SS 1 2

TO: DEPT./ GROUP


REFERENCE : TQZhr..r r 83 Pagge 56

K . Johns, 0/031 ,

LOG NO-

55 1 2

3-523 -e3TO

3-525- 8 3

PHONE 544 7

DATE ^q-APR-8 3

LOG NO .SAMPLE


WATER SAMPLES FORPPM FLUORIDE, BY ELECTRODE

FLUORIDE ANALYSI S

BELL CANYON

time=

3-5Z3-83 R I~s

x It' #a'Pp v

time= /O A M

3-524-83pp 213'fftvl~al

0. 9 Pp&Itime= /020A M

3-525-83 SPRAY RvooFF / . z PPmtime= J02/4

time=


and analyzed ASAP

3 / 3o / 8 3

DAY = WEDNESDAY EPA distillation method



~ -1

APPROVED

M;~ v EE --

S 5 F L A. 'U'TICA'. CHEM. ;STF'- LNi

VBNA0147628 3

HDMSE00624557

CHEMICAL ANALYSI S

F. A 1a tR

REPORT

DEPT./GROUP

3 - X22- 8 3

1)8 - 3It!

PHONE !711t 7

tl _Y 3 - S 6 DATE

LOG NO .SAMPLE

IDENTIFICATION RESULTS by we %f~ t

AI TO f• e" Sr l-9Sl?%3 cell Aga N0 = D.

I, OW t,- A-Al v x S. g M 'I fl,vT o

rf = o. so M y/k~ N Tt2

Ac = V. 00 7 AA 7 /K ,v T O

H 0 = TRACE [ 0. 0

O S~ AA 7Ag N TO

[ = 0. 016 AA yJ ,,i(, NTO

M s= 0. 1 0 ~+ §~K N 70

11/ K,~aNorma FuiL t w . Manage, SSFL At,AL] IICAL CHEWISTI Y 17N!7

I I


TO : M . Kogg DEPT./ GROUP 564

FROM:SSFL A?IALYTICAL QLISTRY UNI T

REFERENCE :Logbook '83Pg. S6

LOG NO

3-521-8 3

PION E 7

GATE

MENEWONOWNW~

LOG NO .SAMPL E

IDENTIFICATIONRESULT S

Cc3"~2r~o3

Wastewater , Canoga

Site L, D/54 Sez bber chromiii - Z ~Q "t 99., ILSuap pff (p~

Grab Sale takeug0

3/30/S3


chromium

COMMENTS: The licit for Site L is 75 mg/l.

M . Mogg Notified by phone

APPROVED

.Farm+619-V

3SFL ANALYTICAL CHMISTRY UNI T

iimm u imi i iumm i iuuui i ummu


TO: M . Mogg


REFERENCE : LaQbook ' $ O . .s6

LOG NO ,

3-520 - 83

PHONE c447

DATE 30/

LOG NO .SAMPLE


3--52043 Wastewater, Canoga Copper - O .2 8 mg/L

Site C, "Sea World" Nickel - 1, 2 mg/ L

pE211 hr . Proportiona l2Fa-ob A kp 1 1

1-93 --9- 3/V73/2

u C~3/~g3~ ~

lyzed for copper, pHad nicke l

COMMENTS : The L.A . City discharge limit for capper is12 mg/l .

15 mg/ L ,

DEPT/GROUP c...1~

Analyses per M . Mogg ' e}/ IL 81 PL-122, 27 Oct . 1981

APPROVED

N.D. - none detected


sSFL ANALYTICAL CHEMISTRY 'J`( T

BNA0147628 6

HDMSE00624560

CHEMICAL ANALYSISREPORT 3-5/s-g 3

TO: _ Mo¢¢ DElr/C3ROUP 564

NlOA~C 3$IL AlIALYTICAL OtDI9f8Z UIR T

RFERENC Logbook pg• •Slp

PHOPdE 5447

DATE 3O

LOA NO .3AMPLa

IOENTIl~ICATION RE5ULTS

-35I S3 Wastewater, Canoga Chromium : v, 09 1Y 5 /L

Site B, D/544 Process pH =7

Clarifie r

24 hr . Proportionalsample

3/z~ /83 }0 3/a%3

s

r

Samp receivedleep~~

~1 3Oo

Analyzed for $, andchromium

COMttENTS: The L .A . city discharge limit for chromium is 10 mg/L

Analyses per L Mogg ' a IL 81 FE-422, 27 Oct . 1981

APPROVED

I arm •19-V

SSlL AI(ALYTIGIL atZki TIT ((I T

IIOI m u imi i iumm i im i IDBNA01476287

ID mHDMSE00624561

CHEMICAL ANALYSIS

REPORT

LOG NO .

-- s,'- g 2to

s - s/f - f s

DEPT. /GROUP 2- I t S

PHONE S~ ~ 7

L5 43- S6 DATE '3/i SI Q 3

LOG NO .SAMPLE

IDENTIFICATION RESULTS Jo Ve "A^ r

2- Sli;-Q3 Co AS "StfeN -{'! /SAC f L O. S CIO_Hs~1A4rks fRc, f1< 2

3 - ~17-4J

3 _ 51 - 4 3

/f1 o w~.

4o l. e s tt nt, 19'. S 04

{N { i A I c H

I I °/a

23c N2 = $ I r 7

1' '21/43CO =

N0~ s N~2 - O. 4 o / '4

SOr As 54, = 0. 0~ 6

J/ 3o/8 7

Norma Fujika~'a , ManagesSSFL Analytical Che iLshy

SSFL ANA ICAL CHEMISTRY UNI T

IIDI muimiiiummiiuuu i imuiu

cc : M . Mogg D/564 FB66

R . Schmued

K . Johns D/031 SS1 2

LOG NOM . FrancisJ . Bowman CHEMICAL ANALYSIS

REPORT'-S W__ ._ iri

■

TO : DEPT ./GROU P

A ALYTICAL CHEM S R YSSFL N I T UNITFROM PHONE

REFERENCELogbook 83, p . 56

DATE

SS 1 2

544 7

3/31/83

LOG NO .SAMPLE


3-515-83 Water Sample from Trichloroethylene = none detected, less than 1 ppb

Bell Canyon, sample d

at 3 :00 pm on 3/29/83

Received : 3/29/83

COMMENTS :

APPROVE D

/Jrrn 619-V

/r SSFL ANAyL ICAL CHEMISTRY UNI T

IIOI m u imi i iumm i im i ID D I DID D IBNA0147628 9

3-515-83

HDMSE00624563

R . Schmued D/564, FB 66 W . Baisley, R . Knight, D/598, SS 1 1

J . Bowma n

M;9 CHEMICAL ANALYSIS

REPORTC . WINZER , 0/031, SS 12

TO:

FROM: SSFL ANALYTICAL CHEMISTRY UNIT

REFERENCE - 1.mchmmk D3 P€ SQ

s!q- B 3

K . Johns, 5/031,SS 1 2

LOG NO

3

DEPT. (GROUP

PHONE 5447

DATE 4-APR- e 3

LOG NO .SAMPLE



3-483 BELL CANYON .0, 5 ~OD~►-~

time 3°°PM

time =

time=

time=

time=

Received in the la band analyzed ASA P

3 / Z9 / 8 3

DAY=TVESDA'( EPA distillation method

COMM ENTS : The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to


JAPPROVED F

a:-.NASE

d1SSFi

II0I m u imi i iumm i im i 100 i Dlv iBNA0147629 0

2E

I IH D M S E00624564

R . Schmued ~ FB 66 W . Baisley , R . Knight, 0/598, SS 1 1

J . Bowman'F rancH .

CHEMICAL ANALYSIS. Mo

REPORT

To:

FROM SZS Z ANALYTICA L CHEMI STRY UNI T

REFERENCE : 7--h -k S3 Paq r- 56

SAMPLELOG NO . IDENTIFICATION

WATER SAMPLES FORFLUORIDE ANALYSI S

f BELL CANYO N

3-512-83 SPAY g u,vo'r

F

: i me= /2 40,'-W

R / ~3 . 3 x /o 69e ~)3-513 -83

me= 12 4 A~-'

k e:eived in the lab

analyzed ASAP

3 / 2 f / 83

. :,av= TUESDAY

RESULTS

PPM FLUORIDE , BY ELECTROD E

0.7pp-i

* - EPA distillation metho d

COMMENTS. The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to

be disc~.arged from the property .

APPROVED

Form 61q-V

BNA0147629 1

C . WI%ZER, D/031, SS 12

K . Johns , D/331,SS 1 2

LOG NO

3-512-S 3APO

3 - 513 - 8 3

DEPT./ GROUP

PHONE 5447

DATE 24 MA R

SSFL A. LYTIC..L C:H NISTRY UNIT

I IHDMSE00624565

•



FROM : SSFL ANALYTICAL CHEMISTR Y

REFERENCE : LOGBOOK 1~3 PAGE S(o

LOG NO .

3-// -83

DEPT./GROUP D/556

PHONE 5447

____ DATE 83


GAS : A/ZGD/1~

RECD : ay i MAff 93.K io7fl

SAMPLER :

PRESSURE .'VA < / (ppm) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTEDG/

< i of DEW POINT )MOISTURE = .5 ppm H2O ( %


AS METHANE & MOISTURE

j FROM :

iSSFL SUPPLY LINE

TR = TRACE ND = NONE DETECTED 4( = LESS THAN


COCA DELTA

CTL-3 CTL- 4

CTL-5 DELIVERY

TANK NO .

TRAILER

OTHER :

COMMENTS : *Maximum allowable limit per MO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in N2 or O 2

APPROVED

Forr* 619-vSSFL ANALYTICAL CHEMISTRY L I

II0I m u imi i iumm i im i IDD I DID IBNA01476292

UH D M S E00624566

M. Mogg

SSFL A!dALYTICAL CHEMISTRY UNI T

CHEMICAL ANALYSIS

REPORT

DEPT/GROUP 56

3-5/0 -S 3

PHONE 5__ 7DATE

LOG NO .SAMPLE


3'5JO_b3

~7

Wastewater, Canoga

Site L, D/51411 Scrubber Chromi'i • Z 46 'S IL

S .unp pH ~O.

Grab Sample taken

3/z4 /~3D~ ~S

Sample Received 3/v I

a- Iof oAnalyzed for pH, and

chromium

APPROVED

F)rm 619-V

SSFL MIAL?rICAL CHEMISTRY UNI T

IIDI muimiiiummiiuuuiuuumu


15 Tg/1 ,

TO: M . Mogg DEPT./GROUP 5

FROM : SSFL AMAL? ICAL CHEMISTRY UNIT

REFERENCE : Loghook ' >3

PHONE chh7

DATE ~~,~/

LOG NO .SAMPLE


3^ $ Wastewater, Canoga Copper Q, / S ng/L

Site C, "Sea Wor1d" Nickel - / , 2 cg/L

p~ - 8 224 nr. Prooortionel .'-t,1 1 ken

3 /zf 3

ample received 3/29/

alyzed for copper, pand nicke l

COMMENTS: The L .A . City discharge limit for copper is12 itg/l .

Analyses per K . Mog$'e IL 81 F!-l22, 27 Oct . 1981N .D. - Xone detect

APPROVED

. ._, ~ .~,_ . .

3-5D9 -8 3

for nickel the Unit i s

S~FL ANALYTICAL O{4ISTRY UNI T

II0I m u imi i iumm i im i 100 I DID I D IBNA01476294

HDMSE00624568

10 M . Maff


oePT/QilQNP 5 6,x..4. ,.,

SSTL A)IALYTIGL O4. tST1lT Wit ?

Rf1ERENCE : Logbook ' S3 pg • .S (o

LO N O

~-sog-8 3

P . pdI 5447

DATE 3/2/S'3

LOd NC . IDENTIFICATION R E S U LTJ

3 583 Wastewater , Canoga Chromium = N . 7.> <0.0 .5 fii, h.

Site B, Il/544 Process pH = / 2Clarifier

.24 hr . Proportional

aarple

3/2 /83

mple receivedSA

Analyzed for pf, andchromium

COMMENTS : The L .A . city discharge lieit for chromium is 10 mg. L

Analyses per Y . Mogg ' s IL 81 FE-422 , 27 Oct . 198 1

•PPIROVED -~ •~,

t ~~T 61~V

Q Q$UL ANALYTICAL OtWSTRT III (Lt

II0I m u imi i iumm i im i 100 I VIOl 0 IBNAOI 47629 5

HDMSE00624569

CHEMICAL ANALYSIS

REPORT

LOG NO .

. 5 , 01-- S 3

3- Sot- -4 3

TO: X . WAS Al t K DEPT./GROUP S-2 2


REFERENCE : 19 83 - cPHONE _ 3-l 9- 7

DATE *11 K I/ g 3

LOG NO .SAMPLE

IDENTIFICATION RESULTS w-t r hY t

r(F t kOH Un i x

3-~o3-ss w 27 K DH = 3 . `tl ~

KF = 2 .11 1

(0et-gs # 2 !t O 14 = 3 . 73 9

KF = 2 . 0

K( C

1xy18 3

COMMENTS :

APPROVE D

C c o - 17, -1

Nornw Fujikariua ManagerSSFL ? na ) , ;i, : ! C.P re,,

L .̂ : TSSFL ANALYTICAL CHEMISTR Y

BNA0147629 6

HDMSE00624570

(1 7

CHEMICAL ANALYSIS

REPORT

TO : F. DEPT/GROUP


LOGNO •

3 - X97- 83

PHONE 5447

DATE &K 3Q A05

LOG NO .SAMPLE

IDENTIFICATION ►4*RESULTS (IX,

NTO M -4 N 4. ~` @3-'' 7-83 Ce" 29 Q

N V R= to g /t; I-e,

ptl

1-Iz~ = O. D

w - 0 . 07 AA rAnd = 0. 17 AA ;

reed

SSFL A ?t41 .Y'TIC L CHFVI~TF',~ I TI "N'

iimmuimiiiummiiuuu iumiiu iu

R . Schmued L D/564, FB 66 W . Baisley, R . Knight , D/598, SS 1 1

J . BormaniM . Franc

CHEMICAL ANALYSISM . Mo


TO :

FROM' SSFL AXAL1TICAL CHEMISTRY UNI T

REFERENCE : T .nrhankg 3 Page 57'4

K . Johns, D/031,SS 1 2

LOGNO •

3 --q96 - 83

DEPT./GROUP

PHONE 544 7

DATE 2 _ MAR- 8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYON

time=

3-qq6 -83 MOUiTAI ►J RvNoFF 8 P~,,►-,Vtime= 2 °°PM

,

time-

time=

time=


3/28 / 8 3

DAY= MON DA`(= EPA distillation metho d


be discharged fron the prope r

APPROVED

L A! LITIC L CHD ISTF I T

BNA0147629 8

HDMSE00624572

CHEMICAL ANALYSIS

REPORT

DEPT/GROUP SZ 1

ct3'~S~-g3

LOG NO .

?' ~qy~-83

3_ yqS- t 3

PHONE _ S I y 7

DATE 4 3

LOG NO .SAMPLE

IDENTIFICATION RESULTS ;y W .(t S lt t

NA 0 1 t NA et t

NAz 50w t 1I O:

/VI t v fvi -f

3-~1y-~3 # ~L Nw O N = 0. 13~ y

N~ ct = 1 .

NAB SOY 0. 3 8 0 y

g-'i93-43 *2c Ha 02 0. Sol ?

NAOH = 0 .16 7

Nit! = 0 .6 1 x -

3 / 2 8/83

SSFL ANALI" CAL CHEM'_TPY L^<I T

iimmuimiiiummiiuuu ium iuuu

M . Mo(& D/5 4 F8 66

D. C L ARKS oIS98 , SS//

J . MONA G HA X) 0w596 Z11 CHEMICAL ANALYSISr, REPORT

TO : C W /NZE'K


REFERENCE : L0gboat 63 rage.54 DATE 28 -AW--6 3

LOG NO .SAMPLE


WATER SAMPLE TRiCHL-OROETHYLENE (TC E

3993 .83 L FA lam! r~P

3128/93

COMMENTS :

APPROVE D

I orm 619-V

IIBNA0147630 0

LOGNO •

3-9R3 -8 3 ~~

DEPT./GROUP 03 / SS/ .z

PHONE 5447

HDMSE00624574

R . Sc~nue '~ ~ C/554, FS 6 6

j . Sownan

n CHEMICAL ANALYSISM . Mog

REPORTC . WINZER, D/031, S5 12

K . Johns, D/031,SS 1 2

LOG NO

3-' 12-83

TO: DEPT./ G FiOU P

FROM : SSFL ANALYTICAL CMISTRY UNI T

REFERENCE : T•nPtu,nk 8 3 Past 54

PHONE 5447

DATE Z 8 - MAR-8 3

LOG NO .SAMPLE


PPM FLUORIDE , BY ELECTROD EWATER SAMPLES FORFLUORIDE ANALYSI S

BELL CANYON

time=

3-492-83 FCL - 2- /. 7 ppvtime-

time=

time=

time=


and analyzed ASAP

3128/ 8 3

DAY= H D J •MY `* EPA distillation method



APPROVED

SSFL ANALYTICAL C}i1;]IISTR1 UNIT

BNA0147630 1

HDMSE00624575


TO : M . Molrg DEPT/GROUP 56+

LOG NO.SAMPLE


3-motIgo

`+~~~3Waetevater, Canoga

Site L, D/54 Scrubber Chromium 550 /LSump pH - (per (D

Grab Saap taken

3/z8 1 3~ 0-)3 o

R ived3/~t~St_ ~nA alyzed for pH, andchromium

FROM :

REFERENCE : Logbook ' mpg. Sy

SSFL ANALYTICAL CHEMISTRY UNITPHONE 54T

DATE

COMMENTS : The limit for Site L is T5 mg/l .

APPROVED NfLfjF arm 619-V


HE


FRO" 3s1L ANALYTICAL CRUIST!Y UNI T

REFERENCE : Logbook ' ~3 pg - S~

PPIONL 5447

DATE

LOS NO -SAMPLE


Wastewater , Canoga Chromium = A/.,~ . 0. 05Site B , D/544 Process pH

fClarifier I

GRAS 1sample TQKt Aa

3/25/' 3

0736

ample received 3 'S` 8


L

COMMENTS : The L .A . city discharge hut for chromium is 10 mg/LAnalyses per M . Mogg7s IL 81 FE-422, 27 Oct . 1981

APP QVEDSUL AMLYTICAL Cl(S1STAY UNI '

i,rn, 6 19-V

flEBNA0147630 3

LOG NO

3-g9o -83OEI•T./GROUID 564

HDMSE00624577

R, Sc`-.ued ~ D/564, FB 66 W . Baisley, R . Knig't, D/598, SS 1 1

J . Bowma n

M : ran,CHEMICAL ANALYSIS


TO:

FROM : SSFL ANALYTICAL QiEMISTRY UNIT

REFERENCE Lnchnnk 8 *3- Page s`f

K . Johns, D/031,SS 1 2

LOGNO-

3-488-83pup

3-489-83DEPT./GROUP

PHONE 5447

DATE 28 -/YA9- 8 3

LOG NO .LOGSAMPLE



FLUORIDE ANALYSI S

BELL CANYON

time=

3-4g8-83 MoonrAt v RuuoFF 0 . 8 Ptime= 7 OBA H

3-489-83 R 1 (2-'7`06 ~a ~) I . / ppri~o

time= A"

time=

time=


and analyzed ASA P

3/28 / 8 3

DAY= MONDAY EPA distillation method



APPROVED

CC,,-- C1J_v

SSFL ANALYPI L CHEKISSTRY UNI T

BNA01476304

HDMSE00624578

cc : M . Francis , D1564, FB6 6


S .R $C*L.ERTo: E . Shank s

SSFL ANALYTICAL MUMSTRY UNI T

REFERENCE : Notebook 0330, page 25

PHONE 329 3

DATE June 7, 198 3

LOG NO .SAMPLE


Unknown liquid fo ridentification . The sample consists of a clear liqui d

with a large amount of suspended fin e

orange -brown particulates . Emission spec -trophometry showed the sample contain sabout 110 ppm iron . The infrared spectru m

3-487-83 Sample t 16 matched that of water . Analyses reveale d

EWR 0 346244it to have a pH of 6 and a fluoride leve l

of 5 ppm .

Received : 3/28/83Based on the above information, th e

sample is probably water with rust part -

iculates and a small amount of dissolve d

salts .

{

COMMENTS .

APPROVED

F arts 619-V

BNA0147630 5

L06 NO

3-487-8 3

oePr./49%WP598, ss1 1

HDMSE00624579

cc! V . Francis 564 FB 66

TO:

PROM :

CHEMICAL ANALYSIS

S . Fisuttr~2 REPORTE . Shanks

SSn ANALYTICAL OiURI8ThY UNI T

REFERENCE Notebook 0330, p . 24

LOGNO •

3-486-83

3293

DATE 6/6/83

L06 NO .SAMPLE


Unknown liquid for

identification .

3-486-83 # 15 The sample consists of a clear, colorless liq-EWR # 346244

uid which does not burn . Emission spectrophotometr i

analysis showed the sample to contain about 25 ppm

iron, 15 ppm phosphorus , 9 ppm manganese and 34 ppm

nickel . Anion analysis revealed 140 ppm sulfate ,

350 ppm chloride and 3 ppm fluoride . The infrared

spectrum matched that of water . The sample pH is

about 4 .

Received : 3128/83 Based on the information above , the sample i s

probably water with a small amount of acid and dis -

solved salts present .

COMMENTS:

SSFL YTICAL C>aAiIST'RY UNI T

Iorrn619-V

BNA0147630 6

598OEPT./SIP

PHONE

SS 12

HDMSE00624580

cc : M . Francis 564 FE 66


E . Shanks

SSFL ANALYTICAL QiO[ISTRY UNIT

REFERENCE: Notebook 0330, p . 23

LOO NO .SAMPLE

IDENTIFICATION

Unknown liquid for

identification .

PHONE 3293

DA5/31/83

TE

RESULTS

3-485-83 # 14 The sample consists of a clear, pale yellow liquid

EWR # 346244 with a gasoline-like odor . The sample burns with

a yellow, sooty flame . Spectrophotometri c

analysis showed no significant amounts of metalspresent . The infrared spectrum was similar to

that of normal alkanes .

Based on the above information, the sample isprobably a mixture of hydrocarbons similar togasoline or kerosene .

Received : 3/28/83

COMMENTS :

APPROVED

V wren 619-V

SSFL IGL QiA[ISTRY UNI T


LOG NO

3-485-8 3

5 89 SS 12DEPT /!ROUP

HDMSE00624581

.c Y . Francis 584 TB 66

1Q

l~glif


I • Shanks DIP-T./SOUP .. 8

U?L AMLTr2CAL C1iO 18TRT WIT T

Notebook 0330, P•_22

LOS N O •

r!lONE ,

3-484-83

88 12

3393

DATE 6/6/83

LOG NO.SAMPLZ

IDENTIffcAT10N REfULTS

Unknown liquid fo r

identification .

3-484-83 # 13 The sample consists of two phases . The top

EWR # 346244 layer ( about 80% ) consists of a clear, pinkliquid which burns with a yellow , sooty flame .

emission spectrophotometric analysis shored no

significant amounts of trace metals present .

The infrared spectrum was typical of that ofnormal alkaaes .

Based on the above information , the sample

is probably kerosene or a similar hydrocarbo n

mixture .

The lower phase ( about 20% ) is a clear ,

orange-brown liquid which does not burn . The

p~H is about 4, and emission spectrophotometri cReceived : 3'28 /83 analysis showed only low levels ( about 6ppm

each ) of manganese and nickel . The infrared

spectrum matched that of water . The sample con-

tains about 20 ppm chloride .

Based on the above information , the lower phase

is probably water with a small amount of acid an d

dissolved salts present .

OOMMENT 5 :

iimm u imi i iumm i im i 0 D iBNA01476308

I IHDMSE00624582

cc : M . Francis, DI56k, F866LOG NO

CHEMICAL ANALYSIS

S .~scffi►~Q, REPORT3-483-8 3

TOE E . Shanks DEPT/$ iOuP598, S S 1 1

rtet~~ SSFL ANALYTIOkL ,l ISTRT UNIT

REFERENCE

LOO NO .

Metebook 0330 . DaOC 2 J


PHONE 329 3

DATE June 7 . 198 3

Unknown liquid for The sample consists of two phases .identification . The top layer ( 90%) is a clear, pink liqui d

with a few dark-colored flakes present . Itburns with a yellow , sooty flame . Emissionspectrophotometry revealed no significantamounts of metals present . The infrare d

3-183-83 Sanple?12 spectrum was typical of normal alkanes .

ER t 346244 Based on the above information, the

top layerof the sample is probabaly kerosenor similar hydrocarbon . The lower phas e

Received : 3/28/83 is not flammable with 110 ppm iron and 12ppm manganese present . The infrared spectr

matched that of water . The pH is about 3and the sample contained 10 ppm chloride .The sample is probably water with tracesof acid and metal oxides .

COMMENT S

APPROVED

V .arm 619-V

SSFL .YTIcA L t rW1 STRY UN I T

IIDI m u imi i iumm i im i I D IBNA01476309

I IHDMSE00624583

CCt M . Franci ■ 564 FB 66

lfiaOM=


s . shank .O'T/MOIVP ~.

59:

$SPL AIIALYTICAL "1D[ISTEY CAR T

1lEF~flEAICE Notebook 0330, P. 20

LOd NO

PHONE

3-482-83

3293

DATE 6/6/83

SS 12

LOO NO.$AMPLE

IDENTIFfCAT10N RESULTS

Unknown liquid for

identification .

3-482-83 # 11 The sample consists of a clear, pale amber

EWR # 346244 colored liquid which does not burn . Emission

spectrophotometric analysis showed 380 ppm iron ,

30 ppm magnesium and 14 ppm strontium. Anion

analysis revealed 120 ppm sulfate, 90 ppm chlor -

ide and 20 ppm fluoride . The sample p8 is about

2 .5 . The infrared spectrum matched that of water .

Received : 3,'28/83 Based on the above information, the sample i s

■ost likely water with small amounts of dissolve d

salts .

COMMENTS

form e19-V

II0I m u imi i iumm i im i I0 ID DIDD 1 IBNA0147631 0

HDMSE00624584

cc ; Y . Francis 564 TB 66

LOG NO

l190~A~

CHEMICAL ANALYSIS

S . FsC~ c. REPORT

DEPT /SOUPP sbanka

UPL AM LTTi d1 I. f3E• 18TRT UIU T

wEF~eENCE : Notebook 0330, p . 19

P OP4E

3-481-83

3293

DATE 6/6/83

LOG NO .GAMPLE

IDENTIFICATION RE5ULT6

Unknown liquid for

identification .

3-481-83 #► 10 The sample consists of a clear, pale yellowEWR # 346244

liquid which does not burn . Emission spectro-

photometric analysis showed the sample to contai n

about 110 ppm iron , 80 ppm magnesium and 200 ppm

potassium . The infrared spectrum matched that of

water , while the pI3 is approximately 8 . The sampl e

was found to contain about 150 ppm sulfate and

12 ppm fluoride .

Received 3'28'83Based on the above information, the sampl e

is probably water with some minor as+oimts of dis -

solved salts .

COir+ MEMT5 :

F or 619-V

IIOI m u imi i iumm i im iBNA0147631 I

598 88 12

UHDMSE00624585

cc ; M . Francis, 0/564, F36 6

CHEMICAL ANALYSIS

i s cif-c.QREPORT

E . Sha n ks DEPT./GROUP 598, SS1 1

FROM : SSFL ANALYTICAL CKS141STRY UNITPHONE 329 3

REFERENCE Notebook 0 3 3 0, oa o e 18 DATE June 7, 198 3

LOG NO .SAMPLE


Unknown i i qu i d for The sample consists of two phases . The top laye ridentification . consists of a clear , colorless liquid with some

fine brown particulate matter . The sample burnswith a blue flame . Emission spectrophotometri canalysis showed 310 ppm iron and 31 ppm magnesium .the infrared spectrum was very similar to that o f

3-480-83 Sample S 9 isopropyl alcohol with evidence of water . Ga s

EWR # 346244 - chromatographic analysis suggested water with alesser amount of isopropyl alcohol .

Based on the above information, the top layer (whichReceived : 32883 represents about 60% of the sample ) is probably

water with isopropyl alcohol and rust particles . *

iii The lower phase is also a clear, colorless liquid

which is flammable . Emission spectrophotometricanalysis showed no significant amounts of metal spresent . The infrared spectrum indicated Freon TFwith isopropyl alcohol . Gas chromatography

revealed Freon TF with a lesser amount of isopropylalcohol .

Based on the above information, the lower phase is

probably Freon TF with isopropyl alcohol . *

* Subsequent analysis by gas chromatography showe d

that the top layer is about 80% water with abou t

20% isopropyl alcohol, while the lower layeris about 88% Freon TF, 10% isopropyl alcoho l

and 2% water .

COMMENTS :

APPROVED

c orm 619-V

SSFL AH L YTICAL C1iiHIISTBY UNI T

II0I m u imi i iumm i im i ID ID DID DBNA01476312

UHDMSE00624586

cc' M . Francis 564 Fn 66

lROM~ ,


E . Shank s

SS?L ANALYTICAL QiniISTRY UNI T

REFERENCENotebook 0330, p . 17

DEPT /SROUP598

LOG NO

PMONE

DATE

3-479-8 3

329 3

5/31/83

SS 1 2

LOG NO .SAMPLE


Unknown liquid for

identification .

3-479-83 # 8 The sample consists of a clear, colorless liqui d

EWR # 346244 with a viscosity similar to that of water . The

sample burns with a clean yellow flame . Spectro-

photometric analysis showed no significant amount s

of metals present . The infrared spectrum of

the sample was nearly identical to that of iso -

propyl alcohol (IPA) .


probably IPA or a similar alcohol .

Received : 3%28/83

COMMENTS :

APPROVED

F orm 6'19-V

SSFL AMLYPIGL (LDtISTRY UNI T

II0I m u imi i iumm i im i ID ID IDDD I IBNA0147631 3

HDMSE00624587

cc Y . Frac.cis 554 FB 65

LOd N O •

CHEMICAL ANALYSIS

S . Fi sc µ ~s2 REPORTE. Sbanka DtPT/~Iwoup 59

8

l4~OM~

Notebook 0330, p . 16

PI ZONE

DATE

3-478-83

98 12

3293

6/6/83

LOO NO.SAMPLE


Unknown liquid for

identification .

3-478-83 7 The sample consists of two phases . The upperEWR n 346244

layer is a clear, colorless liquid that burn s

with a yellow sooty flame . Emission spectropho-

tometric analysis showed no significant level s

of metals present . The infrared spectrum wa s

typical of normal alkanes .

Based on the above information, the uppe r

phase ( about 98% of the sample ) is probabl y

Received : 3'28'83kerosene or a similar mixture of hydrocarbons .

The lower phase is water-based according t o

infrared data, with a pH of about 2 .

c0MMENTS

A ff

iimm u imi i iumm i im i ID ID DID D I IBNA0147631 4

IZS?L ANA LYT I O L OI 18TRY CThU T

HDMSE00624588

cc M . Francis 564 FE 66

IeROM


E . Shanks

SSFL ANALYTICAL Q1EMISTRY UNI T

REFERENCE : Notebook 0330, p . 15

598DEPT /GROUP

PHONE

DATE

3-477-83

329 3

5/31/8 3

LOO NO .SAMPLE


Unknown liquid fo r

identification .

3/477/83 # 6 The sample consists of a clear, amber liqui dEWR # 346244 with a viscosity similar to that of motor oil .

When hot, the sample burns with a yellow, soot yflame . Spectrophotometric analysis showed th esample to contain about 95 ppm phosphorus, 9 6

ppm zinc, and 8 ppm barium . The infrared spectrumwas very similar to that of normal alkanes .

Based on the above information, the sample i sprobably a lubricating oil .

Received ; 3/28/83

COMMENTS :

SSFL A AkTTICAL CS~iISTRY UNI T

orrn 619-V

IIOI m u imi i iumm i im i ID ID DOD I IBNA0147631 5

LOG P40•

SS 1 2

HDMSE00624589

cc' Il . Frs.r is 564 TB 66

CHEMICAL ANALYSI S

y

sF Isc

j* . Shanks Ot'PT./sAcuP

____ . $SFL AM LY'TI04 L I 1 1 8'PSY UlUT

REF>:llElrCY Notebook 0330, p . 14

588

LOS NO .

PHONE ,

3-476-83

3293

DATE 66/6/83

88 12

LOO NO .SAMPLE


Unknown liquid fo r

identification .

3-476-83 # 5 The sample consists of a slightly viscous ,

EWR # 346244blue-green water soluble liquid which burns wit h

a clean yellow and green flame . Emission spectro -

photometric analysis showed about 5000 ppm sodium ,

220 ppm boron and 160 ppm phosphorus . Sulfate

was found to be 160 mg1L, and chloride 35 mg/L .

The infrared spectrum was very similar to ethyl-

ene glycol .

Received 3!28/83


probably ethylene glycol with some minor impur -

ities .

GOMME IYT S :

APPROVED 4/! LTTIGL ~t1ST8Y ISIIT

IIOI m u imi i iumm i im i ID ID DI DD I IBNA0147631 6

REPORTt+~R

HDMSE00624590

cc . Y . Fra^c'_.s 564 FF3 66

TO:

FROM:


E . Shanks

SSFL ANALYTICAL QisYIISTRY UNIT

REFERENCE:Notebook 0330, p . 13

DEPT. /GROUP598

LOSNO •

PHONE

DATE

3-475-83

SS 1 2

3293

5/31/83

LOG NO .SAMPLE


Unknown liquid for

identification .

3-475-83 # 4C The sample consists of a clear, pink liquid wit h

EWR # 346244 a viscosity similar to that of water . The

sample burns with a yellow, sooty flame . The

spectrophotometric analysis showed no significan t

amounts of metals present . The infrared spectrum

was very similar to that of normal alkanes .


probably a hydrocarbon mixture such as kerosene .

Received : 3/28/8 3

COMMENTS :

APPROVED ,

F arm 619-V

RA I IBNA0147631 7

S C.~

SSFL AN4L*I CA L CKWISPRY UNI T

HDMSE00624591

cc : M . Francis 564 FB 56

FROM:


B . Shank s

SSPL ANALYTICAL O1Sf[ISTRY UNI T

REFERENCE : Notebook 0330, p . 12

DEPT./GROUP

3-474-83

598 SS 12

PHONE

DATE

3293

5/31/8 3

LOG NO .SAMPLE


Unknown liquid for

identification .

3-474-83 # 4B The sample consists of a clear, pink liquid wit h

EWR # 346244 a viscosity similar to that of water . Thesample burns with a yellow, sooty flame . The

spectrophotometric analysis showed no significan t

amounts of metals present . The infrared spectrum

was very similar to that of normal alkanes .



Received : 3/28/8 3

COMMENTS :

APPROVED

fornn619-V

I IBNA0147631 8

JLOG

HDMSE00624592

cc, V . Fra__cis 564 Fr. 5 6


E . Shanks

SSFL ANALYTICAL QLO1ISTRY UNI T

REFERENCE Notebook 0330, p .11

DEPT. /GROUP598

LOGNO-

3-473-8 3

P4ONE

DATE

SS 1 2

3293

5/31/83

LOG NO .SAMPLE


Unknown liquid fo r

identification .

3-473-83 # 4A The sample consists of two phases . The top layer

EWR # 346244 (about 70%% of the sample) is a clear, pink liqui d

that burns with a yellow, sooty flame . Thespectrophotometric results showed no significan t

amounts of metals present . The infrared spectru m

is very similar to that of normal alkanes .



The bottom layer is a clear, colorless liqui d

which does not burn and contains some rust-colore d

residue . The spectrophotometric analysis showed

about 24 ppm iron present with no other significan t

Received :3 /28/83 amounts of metals . The infrared spectrum indicated

water as the predominant material present, and a

pH test showed a reading of about 5 .

Based on the above information, the lower phase i s

probably water with a small amount of rus t

particulates .

COMMENTS :

APPROVED ,

I arm 61%-V

SSFL L*{TIGL STRY UNIT

VBNA0147631 9

HDMSE00624593

cc- N . Franc!= 564 FB


PROM

E . Shanks

8SFL ANALYTICAL QL ISTRY UNI T

REFERENCE: Notebook 0330, p . 10

LOG NO .

3-472-83

DATE

3293

5/31/8 3

LOG NO .SAMPLE


Unknown liquid for

identification .

3-472-83 # 3 The sample consists of a clear, amber liqui d

EWR # 346244 with a viscosity similar to that of water .

The sample burns with a sooty, yellow flame .

Spectrophotometric analysis showed no significan t

amounts of metals present . The infrared spectru m

of the sample was very similar to that of a norma l

alkane .


probably a hydrocarbon such as kerosene .

Received: 3/28/83

COMMENTS :

APPROVED

Iornn619-V

SSFL YTICAL QIW STRY UNI T


598DEPT./34%OÙP

PMONE ,

SS 12

HDMSE00624594

cc V . Francis 564 7S 6 :

FROM :

CHEMICAL ANALYSIS

REPORTE . Shanks

SSFL ANALYTICAL Q{ ISTRY UNI T

REFERENCE :Notebook 0330, p . 9

LOGNO •

DATE

3-471-83

3293

5'31 `8 3

LOG NO .SAMPL E


Unknown liquid fo r

identification .

3-471-83 #2 The sample consists of a clear, colorless liqui d

EWR # 346244 with a viscosity similar to that of water .

The sample burns with a clean flame similar to tha t

of an alcohol . Spectrophotometric analysi sshowed no significant amounts of metals present .

The infrared spectrum of the sample appeare d

almost identical to that of methanol .


probably methanol .

Received : 3/28/83

COMMENTS :

APPROVED ,

form619-V

598DEPT./GROUP

PHONE

SSFL I CA L CE1H ISTRY UNI T

BNA0147632 1

SS 12

HDMSE00624595

cc- V . Fra:cis 564 FB 66

CHEMICAL ANALYSI S

f S - F15CHL.E

TO= 9 . Shank,

REPORT

ovR /Savour :_

USTL ANALYTICAL OMtIST 'RT UNIT

1lEFEJlENm :Notebook 0330, p . 8

L0dNO-

PHONE ,

DATE

3-470-8 3

3293

6/6/83

88 12

LOS NO .SAMPLE

IDENTIFICATION

--

RESULTS

Unknown liquid for

identification .

3-470-83 , 1 The sample consists of a clear, viscous liq -

EWR # 346244 uid, slightly yellow in color, which burns onl y

when heated . The sample is water soluble and

has a slightly basic pH . Emission spectrophoto -

metric analysis showed no significant amount s

of metals presents . The infrared spectrum i s

Received- 328'83 most similar to propylene glycol and glycerol ,

with water .

Based on the above information, the sampl e

is probably a polyhvdric alcohol such as pro-

pylene glycol or glycerol, with some water pre-

sent .

COi4ME NT S .

AFP/ip1/ED '

apron 019-V

ICAL CENIQSTIY WI T

BNA0147632 2

HDMSE00624596

CHEMICAL ANALYSI S

Quality Assurance

REPORTDEPT . /GROUP :

FROk : SSFL ANALYTICAL CB SISTRY LABORATOR Y

REFERENCE : Logbook - 8 3 Page - 54

LOG F.N(B ER :

3 - `~~ 3 - 83

PBOKE: 5447

DATE : ? 1t?14, 83


3- ,3 ^ '3 GAS : HYDROGEN PURITY = D .N.A . % D .N .A . By Difference

RECEIVED : Q5 M4 . PARA = D .N.A . %

SAYPIZR : FL() o59A G

PRESSURE : /FCC p5/( NIMPURITIES

02 = D.N.A . % 02 r~ N, .D. < / ppa

ANALYSIS REQUESTED : N2 D .N.A . % N2 _ 7,q < / ppm

CO!KPLETE Ar = D .N . A . % Ar = D .N.A . pp mSPECIAL : For

CO D.N .A . % CO s D .N .A . Ppm02 and N2 Only . =CO AD N CO =`r AD N m2 .. . 2s ., . pp

CE = D .N.A . 4. CH = D . N .A . PPM4 4

FROM : C2H2 = D .N.A . % C2H2 = D .N .A . ppm

SSFL SUPPLY LINE H2 = D .N.A . X. H2 = D .N .A . ppm

ALFA

BRAVO D .N .A . (ppm) Total Hydrocarbons as ®4

DELTA

COCA MOISTURE = D.N .A . ppm Hp ( D .N .A . of DEK POINT)

CTL #3

CTL #4

CTL #5

TANK NO .

DELIVERY

TRAILER Tr - Trace

= Less Than

OTHER 5 K SUPPLY > - Greater Than

COMP, 5-"A j N .D . - None Detected

L -1 D .N.A . - Does Not Apply

COMMENTS : Maximum allowable limit per RAO 615-072 for N2 is 15 ppm ; for 02 + Ar, itis 5 ppm .

APPROVED: -/• &,44,v /Ll~.

LABORATORY )MANAGER

556

SSFL ANALYTICAL CHEMISTR Y

BNA0147632 3

HDMSE00624597

66 w . Baisley, R . Knight, D/598, SS 1 1

J . Bowman

iF ranc s,M .C H E M I C A L A N A LYS I SM . Mogc /

F . B . LARY , D / 596, SS 11 REPORTC . WINZER , D/031, SS 1 2

TO: DEPT./ GROU P


REFERENCE : T .nahnnk 93 Pn94 54

K . Johns, D/031,SS 1 2

LOG NO '

3-16o-8 3T O

3 - -4(-2.- 8 3

PHONE 5447

DATE 25 - MA R -8 3

LOG NO.SAMPLE



FLUORIDE ANALYSI S

BELL CANYON

time=

3 -46O -83 S`1- z 0. / P? Ftime= OS_ AM

3-96/-83 c~-z 1 . pp,Y, Ftime= // °°A M

3-462-83 APT Ftime= ____ _

time=


and analyzed ASAP

3 / 25 / 8 3

DAY= F RI DAY 1 EPA distillation metho dA =



APPROVED

Form 619-V

SSFL A LYTICA L CHEMISTRY UN IT

BNA01476324

HDMSE00624598

I r". _. ~1CC ^ 5 R K n S 11 K . Jo-'s ,

ncisF raM .CHEMICAL ANALYSISM . Mo

F . B . LARY, D/596, SS 11 REPORTC . WINZER, D/031, 55 1 2

TO :


REFERENCE : T .nabnnk 3 F e 54

LOG NO

55 1 2

3-458-8 3

PHONE 5447

DATE 25- MAk- 18 3



3-4c &3 BELL CANYO N

time= /0 A M

time=

time=

time-

time=


3/ 25 / 8 3

DAY= FR i DAYEPA distillation metho d



APPROVED

Form 619 -VSSFL A LYTICAL CHEMISTRY UNI T

BNA0147632 5

DEPT./ GROUP

4L'4 e~- ~~-'

HDMSE00624599

TO :

FROM :

M. Mogg

CHEMICAL ANALYSIS

REPORT

DEPT/GROUP 561


REFERENCE : Logbook '; pg. j -

LOGNO-

3- 57-8

PHONE 5447

DATE 3 /.-I's [.Z 3

LOG NO .SAMPLE


Wastewater , Canoga

3'57-~3 Site L, D/544 Scrubber Chromium - 3? 0Sump pH - 74v

Grab Sample taken

S l$3

@0745

Stern 6cre~Uived 3/25/S3

Analyzed for pH, an dchromium

COMMENTS : Tl e limit for Site L is 75 rag/1 .

,#. f 11~ -, . Z.,2jd -,4,oo0ei .,L,-LI I - z~~,oAPPROVED

SSFL ANALYTICAL CHEMISTRY UT IT

form 619-V

I IBNA0147632 6

HDMSE00624600


TO. M . '!ogg DEPT./GROUP 5

FROM : SSFL ANALYTICAL CND(ISTRY UNI T

REFERENCE : Logbook ' 22 DQ . J' '7

LOG NO . ~-~

PHONE s 1 7

LOG NO .SAMPLE


3- y 5~ -€3 wastewater , Car oga copper - Q . ! 3 ing/L

Site C, "Sea world" Nickel - , ag/L/ 2~

21 hr . Proportional S • l°a-ple take

n

3fZ t/ /83

Le received 3~3

alyzed for copper, pHnd nickel

COMMENTS : The L.A. City discharge limit for copper is L5 n$/1, for nickeL tre Liait is12 mg/l.

Analyses per M . Kogg ' e IL 81 !'!-i22, 27 Oct . 1981R.D. - None detected

APPROVEDFL ANALYTICAL C2{E6tI iTRY U N

IIOI m u imi i iumm i im i ID I DBNA01476327

I I IHDMSE00624601


TO M . Mo¢¢ DQ►T./d#IOtJP 56 t

f1lOl~t ss1L ANALYTICAL CFtm ( 13T1!! L7(I!

RErERENCS Logbook '3 pg . c [..~

PtiOprE 5447

DATE a'Z

LOG NO .SAMPLE

IOElVTIFICATION RESULTS

3-455- Wastewater, Canoga Chromium = O, O S f fL

Site B, D/544 Process pH =

Cla ri fier !


sanple

3fzLl f 3

Sanple received j/7,5,

cOcIgOAnalyzed for pH, andchromium

COMMENTS : The LA . city discharge llait for chromium is 10 !ng/LAnalyses per M . Mogg ' s IL 81 PE-422, 27 Oct . 198 1

APPR~Vf ,t?iV a~rr 619-V

5911. AMLYTICAL. C t. 1STRY LIMI T

II0I m u imi i iumm i im iBNA01476328

UH D M S E00624602

R . Sc~-uec ~, n/5~+, F5 W . Ra .sley , R . Krit, D/58, SE 1 1

J . BowmaniM . Franc s

CHEMICAL ANALYSISM . Mo g g/

F . B . LARY , D/596 , 55 11 R E P O RTC . WINZER, D/031, SS 1 2

TO . DEPT./GROUP


REFERENCE : Lnahnnk g3 P~g~ 54

K . Jor's, J ;'n + ,

SS 1 2

LOG N O

3-952- 83TO

3 - 454- 8 3

PHONE 5__

DATE ZS-/-1A1-8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYON

time =

3-4s2-s3 PP ($74,0°0 9aI) 0 . 6 PPStime=_____________

3-153-83 Mo~Nm,~v RoMoFF //f,/7 /S/time=_____________

3-459-83 I (3iM ;II ;e .. gal) / s ff,,,- ,time= 9 BOAM

time=


and analyzed ASA P

3/R5/ 8 3

DAY= FR I DAY y= EPA distillation metho dA



APPROVED

Form 619-V

SSFL NALYTICAL CHEMISTRY UNI T

II0I m u imi i iumm i im i 100100 I D IBNA01476329

I IHDMSE00624603

ENGINEERING WORK REQUES T-ITLE CF :CB

APPLICABLE DRAWINGS (ATTACH IF REQUIR EINSPECTION REQUIRE D

YES NO

DOING DEPT LEDGER ACCOUNT GENERAL ORDE R

EXT .REQUESTED B Y

SUPERVISION

FACILITY

9gV4I L-ZSASSIGNED TO :

No . R5 ~387 j

G .O . ITEM & MCR INIT . GROUP HOW . OR TASK I DOING GROU P

SHIFT

I

SHOP) I LAB

INSTRUCTIONS lBE SPECIFIC )

tie 5c3 ~~3

REQUESTED COMPLETION DAT E

ACTUAL COMPLETION LAT E

ESTIMAT E


s

NOTE : THIS FORM WILL BE USED FOR NON .DELfVERABLE ARTICLES ONLY .

C)

S#tfL 6

RECEIVED @ LAB

SSFL ANNALYTIu' :AL CHEMISTR YBY

FORM R 94 .L REV E-57

TLI

LIST OF MATERIAL S

BNA0147633 0

REQ . SUPERVISION ESTIMATOR

LEADM AN MECHANICII

H D M S E00624604

CHEMICAL ANALYSIS

REPORT 3 1950- 93

DEPT.!GROUP __-

PHONE -

DATE z 9 ti1A f b' 3

LOG NO .SAMPLE

IDENTiFiCATION

+ .0 .3 19RESULTS -

3-y1/ 9-83TRHc for T oe r

RL10001-F

FwR No . 503 871

BT .A,v-' mg/500 ml

=114RDWARE mg/ 500 m1

3-X50 -$3 EwR No . 5O -3 8'7/

mg/500 ml


EWR No .

BLANK mg/507 ml

A.ARDWARE . mg/500 ml

fI

MANAGER

Recd . ;2 5 /-14e 183

SS : L Analytical Chemistry

. 9o,-,c

CHEMICAL ANALYSIS

F . B . LARY , D/596 , ss 11 REPORTC . WINZER, D/031, SS 12

TO

FROM SSFL ANALYTICAL CRI)GSTR'i UNI T

REFERENCE : T .nohnn4- 8 3 Pte. 5 1

LOS N O

3-4~1-8 3

DEPT./GROUP

PHONE 5447

DATE 2,1-MA R-8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

3-44 1-63 BELL CANYON0. 3 ppM v .4; pp ~

time= /O'5A

M

'3-~ ~~ -83 PP d~ :, .,g C sct6E 0 3P~~t i rte= 7

,oAPI

3 - A Z3 -s 3 R 1. J v r-1 n9 b 15. c A96F O. 3 pp n^

ire= 6ss,g M

3-428-91 Al dvr. ^! DucwILf6 E

+ t ir+e= 645A P

ire=

Rece ve- i - t'e ' a `

aid ara I .ze :: AS .

324/ F 3

1 '-,AY= T HUPSt ' = EPA distillation method

COMME NTS T,. NODS for SSFL allows a ,:axir"ur' of 1 .C pp' fluoride to

d•Sc`•a-Cs_ frDc

APPROVEDSSFL 'iAL1TICAL CHD ISTR1 LN'1 7

BNA0147633 2

H D M S E00624606

CHEMICAL ANALYSIS

REPORT

TO : M• KogB DEPT./3R01~P `,~►

SSFL ANALYTIGL Qf~IISTRY UNIT

LOG N O

3-L~0 -g3

P1-iON E _T

LOG NO .SAMPLE


3-qo-a3 Weftevater, Canog a

Site L, D/5 ► Serabber throml m • (h7 ✓K9 /L.S ;mp pH 7* b

~jGrab Sasple taken

3 li.y ( c 3~073O

Fred 3/Z/3

aAn lysed for pH, andchroaiua

jjFL AML'[TIC:AL QC IiTgY 1 4L T

IIDI muim i iiu mmiiumi ii uim i

CHEMICAL ANALYSIS

REPORTM . "oag DEPT/GROUP ^ h

FROM: SSFL AMALYTICM CHEMISTRY UNI T

REFERENCE : Logbook ' b3 va . .~

BOG N O

3 - y39 -83

P4- NE ;4h'

DATE °~

LOG NO .SAMPLE


3L3 Wastewater, Canoga Ccpper - Q~ O C.c g/L

Site C, "Sea world" Nickel - O. 2 cO Tg/L

p~ - 8 221 hr . Proportional .Q.°^,l° lakpn

3 .3/&3

aple received 3/Zc f~

lo3oalyzed for copper, pE

nd nicke l

COMMENTS : The L .A . City discharge Lisit for copper is .5 Tg/i, for nickel tte .i~it La12 ugh .

Analyses per M . Mogg 'a t 81 F!4.22, 2? Oct . 1981B .D. - None detecte d

APPROVEDS .iFL ANALYTICAL CN.EMIiTRY NI T

II0I m u imi i iumm i im i ID 10010 I IBNA01476334

HDMSE00624608

r


To _ OT./3j 56 4

f>lOMr SSTL AML. TIGL C7(l~rI3? T UNIT

RcPERENCE : Logbook ' 83 pg .

L O C3 H Q

3L/3 a

p*yp~E 5447

DATE

LOG NO.SAMP .Z

IOENTffiCAT1QIV ReSULTS

3-4? -g Wastewater, Canoga I~romiurn = , VV yv19

Site B, D/544 Process yH =

Clarifie r


sample

3J3/g3

r

Sarple received 3/4310 3


chromic

COMMENTS : The L .A . city discharge licit for chromium is 10 sg,'LAnalyses per M . Mogg ' s IL 81 FE-422 , 27 Oct . 1951

APVf~OVEO

r,rm 619-V

5311.. ANALYTICAL QtDl19TWY ;MIT


I IHDMSE00624609

CHEMICAL ANALYSIS

REPORT

To: L, K u s k


REFERENCE : 1_3 g3- .2

PHONE _ S I ~I7

DATE 3 2 3

LOG NO .SAMPLE

IDENTIFICATION RESULTS ly Volvn. ie

3 -43c- '3 Co *1 Lvs f,'o #'/

f = ~iZHC~ o. r °%U-~3c-Y5 KOnn5~► Mr/ts 2

-3-#37-fl ~ewNh i (( SRA M

S i ll 5e1 .'°'1 .1 °%A-A D

#2 C K ✓ /'r 0,lZ

J~l~ = 81,6 cy,

C D

NO AS NOz =0,003%

t/

~~41~( ✓ ~~ its S(~ = 0.79 %

325/

COMMENTS :

APPROVED

aormv Fwikccvc McnagerSQL Anolrhfa! ~trem~s! ~.

SSF'L ANALI TiCAL CSiElfZSTi) UN T

II0I m u imi i iumm i im i ID 100 I D IBNA0147633 6

LOG NO3-~t3c- S 3

td

1-'137-

S2 - 6 SDEPT./GROUP

I IH D M S E00624610

cc : P . Kleinsmith D/768, T040R . Schmued D/541, FB12




TO: ROCkE`TDYNE PLANT SERVICES DEPT./ GROUP

FROM : SSFL ANALYTICAL i~LEMISTR Y

REFERENCE : LOG BK ' '3 PAGE 5 2 NOTEBOOK -

D/031

LOG NO

3~g31 -g.3

PHONE 544 7

DATE 2~ - NIAR - 8 3

LOG NO .SAMPLE


Water sample from the Using the concentration techniques and methods ap-3 .'3/-8 3 Al Inlet to the R2 proved emder the guidelines stated in the current

retention pond at SSFL NPDES permit , the following VOLATILE ORC:AJiICRocketdyne . CClIPOUNDS Were found :

Acetone (CH3COCH3) f~

/Sampled 6 ___ H

qBromodichloromethane (BrCHC12) = I

3 1 83 Carbon Tetrachloride (CC14) _

By : L . ('//,n Chloroform (C 1013) _ ✓

Methylene Chloride (CH2C12) = 7RECEIVED LAB :

3 /2'9 pp3

1,1,11rrichloroethane (dH3CC13) = TR

Trichioroethylene (ClC$ :CC12) = S

Notation about appear- Tetrachloroethylene* (C12C :0C12) _ /Vi9ance of the sample :

1,2-Dichloroethylene (ClCH :CHC1) _

Dibromochloromethane (C1O1Br2) _ D

~1Isopropyl Alcohol ; also (CH3CHOHCH3) = TDlmown as IPA ; 2-propano 1

Freon TF (C12FCCF C1) = ND2

1,1-Dichloroethane (C12ECH3) _ /(/?' /

COMMEYTS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifical-

ly required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES # CA0001309 fromthe California Regional Water Quality Control Board, Los Angeles Region . (2) per (1) "Wastesdischarged shall not contain phenols, mercaptans , or other substances in concentrations which

would impart taste, color, odors, foaming or other objectionable characteristics to receivingwaters ., .", "or any substance in concentrations toxic to human, animal, plant, or fish life . "

PPB = PARTS PER BILLION= LESS THAN ND = NONE DETECTED DNA = DOES NOT APPLY TB = TRACE

APPROVED _ f l,Lt(A ~I• ~ T

F .rrr E'9-V

SSFL AI~ALY?.CA:. CHr.✓_ . Ar. : U'vI .

IIOI m u imi i iumm i im i IDID DBNA01476337

i u UH D M S E00624611


M . Francis D/541, FB12M . Mogg D'541, FB12

CHEMICALANALYSI S

REPORT

TO : ROCKETDYNE PLANT SERVICES DEPT./ GROUP D/031

FROM : SSFL ANALYTICAL CSEMISTRY

REFERENCE LOG BK '3 PAGE 5 2 NOTEBOOK -

LOG NO

3 -130 -83

PHONE 5447

DATE 24-MAR-P3

LOG NO .SAMPLE

IDENTIFtCAT1ON PURGE & TRAP GC/MS RESULTS (PPB )

Water sample from the Using the concentration techniques and methods ap -3-i30 -$ 3 R2 retention pond at proved under the guidelines stated in the curren t

Rocketdyne . SSFL NPT)ES permit , the following VOLATILE ORGANICCOMPOUNDS were found :

Freeboard = -- ft50Acetone ( CH3 O00B3) =

Sampled @

3~Bromodichloromethane (BrcHC12) = NL <

2~ 83_T

'

By :Carbon Tetrachloride ( CC14 ) = fV~ < /

Chloroform (CHC13 ) = Tip I

RECEIVED ® LAB :CH C1 3

3 /2'/232 2) =Methylene Chloride (

1,1,l-Trichloroethane (CH3CC13) = TR ' I

Notation about appear- Trichloroethylene (Cl( :CCl2) = 4ance of the sample :

* (C1 C CC12 : 2 )Tetrachloroethylen e

1,2-Dichloroethylene (Cl i :C8C1) = 3Dibromochloromethane (ClCHBr2) = NL 4 I

Isopropyl Alcohol ; also (CH3CHOHC133) = 43known as IPA ; 2-propanol

Freon TF (C12FCCF2C1) = 8

1,1-Dichloroethane ( C12CHCH3) = __ L

CObCv1ENTS : ' Tetrachloroethylene is also known as perchloroethylene . ( 1) Monitoring specificall

required according to the Rocketdyne N'DES permit, Order # 76-146, NPDES # CA0001309 from the

California Regional Water Quality Control Board, Los Angeles Region . (2) per (1) "Wastes dis-

charged shall not contain phenols, mercaptans , or other substances in concentrations which


waters . . .", "or any substance in concentrations toxic to human, animal, plant, or fish life . `


= LESS THAN ND NONE DETECIEI) DNA = DOES NOT APPLY TR = TRACE

APPROVED rf ~

SSFL ANALYTICAL STAY UNI T

_r-r 6'9-V


I IH D M S E00624612

cc : R, Schmued D/541, FB12M, Francis D/541, FB12


TO : ROCKETDYNE PINT SERVICES


CHEMICALANALYSI S

REPORT

DEPT. /GROU P D/031

REFERENCE : LOG BK ' K3 PAGE S 2 NOTEBOOK

LOG NO .

3-12c 8 3

PHONE 5447

DATE 29 -MAR- 8 3

LOG NO .SAMPLE


Water sample from the Using the concentration techniques and methods ap-3-9 29-8 3 PP retention pond at proved under the guidelines stated in the curren t

Rochetdyne . SSFL NPDES permit , the following VOLATILE ORGANICCds[POUNDS were found :

Freeboard = ft

/ pSampled @ 7 Ak

Acetone (CB3COCB3) = Z

312/g3 Bromodichloromethane (BrC~C12 ) = Q~/ < /

C IICarbon Tetrachloride (CC14 ) = /VQL /

By : L . O ~JChloroform (CBC13) = ,V~ < /

RECEIVED @ LAB : Kethylene Chloride (CH2C12 ) = 7< /

3 / 29 / 83 l,l,l-Trichloroethane (CH3CC13) = 7Z? < j

Trichloroethylene (C1CB :CC12) =Notation about appear-

ance of the sample : Tetrachloroethylene* (C12C :CC12) = N' 1

1,2-Dichloroethylene (ClCH :CRCl) = !

Dibromochloromethane (C1CBBr2) = NI)' /

Isopropyl Alcohol ; also (CB3CHOBC 13) = /70known as IPA ; 2-propanol

Freon TF (C12FCCF2C1) = ND' I

1,1-Dichloroethane ( C12CBCB3 ) = /VD < /

OOmtENTS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifical-ly required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES # CA0001309 from


discharged shall not contain phenols, mercaptans, or other substances in concentrations whichwould impart taste, color, odors, foaming or other objectionable characteristics to receiving

waters . . ., nor any substance in concentrations toxic to human, animal, plant, or fish life . '


= LESS TBAT ND = NONE DETF~trED DNA =DOES NOT APPLY TR = TRAC E

APPROVED

' rm 619-V

/ V J~ _SSFL ANA&rICAL CHEMISTRY NI T

II0I m u imi i iumm i im i ID 100 I 0 I 0 IBNA0147633 9

H D M S E00624613

LOG N O

FROM : SSFL ANAL17ICAL CHEMISTRY D/539 SS11 PHONE : 5447

CHE CAL l AL YS i S RE SU LT S

T' : INDUSTRIAL ENGINEERING D/031 SS12 DATE :

A.ppro\ e .i

4-APR-83

REFERENCE- LOG BK ' 83 PAGE 5 2

CONST=NT 77SULTSrr /1

CONCENTRATIO NLIMIT /l

p11 at 25° C 7 .9 pH unit 6 to unit s

Total Dissolved Solids on Drying at 180° C 521 950

Ter,; ereture of water 11 .8 37.8 ° C

Chloride 46 150


Settleable Solids < 0 .1 ml/1 0.3 rnl/1

ROD at 20'C <1 60Grease and Oil < 1 15

Residual Chlorine 0.29 0 . 1

Surfactants as MBAS C 0.01 C. 5

Sulfate 147 300

Total Cnrornim 0 .002 0.01

Fluoride 0 .3 1.0

Boron 0 .2 1 . 0

Turbidity 6 (5 )

Phenols 0 .001 (4 )

Mercaptans 0 .6 (4 )

Cyanide 0 .003

SAMPLED FROM : AI inlet to R2 C 6 :45 AM AM/PM ON: 24-MAR-83


(2) Filtered with Whatman GF/C paper and dried at 1030 to 1 .05° C .

(3) Limitation not required to be met during rainfall .

(4) Wastes discharged shall not contain phenols, mercaptans, or other substances it

concentrations which would impart taste, color, odors, foaming or other oh .ieci

ionable characteristics to receiving waters . . .or any substance in concentration-

toxic to human, animal, plant or fish life .

(3) bastes discharged shall not increase the natural turbidity of the receiving

waters at the time of discharge .

BNA0147634 0

3-428-83

H D M S E00624614

EFFLUENT D ! SCHARGE REPORT

CHEM1 CAL. ANALYSIS RESULTS

10 :_ Industrial Eneerincr

LOG NO .

3-423-83to

3-427-83

1i T./GHOtJP 031

FROM :_ SSSL MALYTICAL Cf E ISTRY . DEPT . 539 P ! _4I 7

LB.83 -p, 52 DATE : 4-APR-83 .

SgMPI,E IIEtrI'zFICAZ'ION; gpTg'LE yF~NS R2 Q 6:55 AMon 24-MAR-8 3

RESULTS/1

NCENTRATIONy /1

pH at 25• C 7 .7 pH unit to t

Total Dissolved Solids on Drying at 180 • C 210 950

Tefapemtue of Water 11 .4 37.8' C

Chloride 18 150


Settleable Solids <0 .1 ml/1 0.3 ml/1

BOD at 20' C 4 60

Grease and Oil 2 15

Residual Chlorine (0 .04 0.1

Surfactants as MSAS { 0 .01 0. 5Sulfate 48 300

Total Cn - njura 0 .006 0.01

Fluoride 0 .3 1.0

3oron C 0.2 1.0

Turbidity 29 (5 )

Sewage Treatrtient Plant 7ni'1uent BOD at 20 ' C 684 (h)


Sewage Treatment Plant Influent Suspended Solids 4368 (1+ )

Sewage Treatment Plant Effluent Suspended Solids 9 (2i )

(5)

Filtered with Whatman GF/C paper.

Filtered with Khatman GF/C paper and dried at 103°to 105° C .


The average final effluent concentrations shall not exceed 15$ by weight ofthe average sewage treatment plant influent concentrations of BDDc 20'C andsisperided solids during periods of discharge .

Wastes discharged shall not increase the natural turbidity of the receiving

waters at the time of discharge .

SSFL A?IALIC~L CHEMISTRY UNI T


H D M S E00624615

EFFLUENT" DISCHARGE REPORT "

(5 )

APPROVED

Form 619-V

CHEMI CAL. ANALYSIS RESULTS

T 4 : S,SFI, ANALYTICAL C' MISTRY . DEPT . 539

REFEKENCE :_ LB- 83-0 . 5 2

SAMPLE IIENTIFTCA'TION: SAME F" E_P

LOGNO-

3-420-83t o

3-422-83

TO :_ Industrial Encrineerinrz DEPT ./GFCUP- - 031

?W19E 5447

. DATE : 44-A -8'i

0 77 10 AM ON 24-MAR-83

CONSTITUENT RESULTS/1

CONCENTRATIONL3HTT /1

pH at 25' C 8 .1 pH unit to 9 unit s

Total Dissolved Solids on Drying at 1800 C 118 950

Temperature of Water 10.1 3T-8* C

Chloride < 5 150


Settleable Solids < 0 .1 ml/l 0.3 ml/1

3DD at 20' C 3 60

Grease and Oil 2 15Residual Chlorine 0 .05 0.1

Surfactants as MBAS < 0 .01 0 . 5

Sulfate 18 300

Total Chromium 0 .010 0 .01

Fluoride 0 .3 1.0

Boron < 0 .2 1.0

Turbidity 29 (5 )

Sewage Treatment Plant Influent BOD at 20' C 168 (24 )

Sewage Treatment Plant Effluent 30D at 20' C 3 (4 )

Sewage Treatment Plant Influent Suspended Solids 1639 (b )

Sewage Treatment Plant Effluent Suspended Solids 10 (4 )

Filtered with Whatman GF/C paper.

Filtered with Whhatman CF/C paper and dried at 1030 to 105° C .

Limitation not required to be met during rainfall.

The average final effluent concentrations shall not exceed 15% by weight of

the average sewage treatment plant influent concentrations of BDDS 200C andsuspended solids during periods of discharge .

Wastes discharged shall not increase the natural turbidity of the recet wingwaters at the time of discharge .

MANAG

BNA0147634 2

H D M S E00624616

cc ; M . Mog~ D/564, 055, FB66


TO: D . Grie p


LOG NO

3 - 416 - 83

to3 - 419 - 8 3

DEPT./GROUP 546

REFERENCE: LB 83- page . 53

PHONE 5343

Mar . 28, 1983DATE

LOG NO .SAMPLE

IDENTIFICATION*

RESULT S

Waste Solvent ,

Unidentified, Drum #

3-416- 83 1 The major constituent of all four samples, ove r

99 area percent , was identified as 1,1,l -Trichloro-

3-417-83 2 ethane based on the Retention Time of an external

standard . No perchloroethyleie (C2C14 ) was detected3-418-83 3

3-419-83 4

For qualitative identi -

fication of the majo r

constituents .

Received on Mar . 24,'83 * Results were obtained using a gas chromatograph

equipped with a thermal conductivity detector . An

eight foot stainless steel column packed with 1%

SP-1000 on 80/100 mesh Carbopak was utilized unde rthe following conditions :

Oven Temperature Profile :

Initial value= 120° C

Initial time= 1 .00 minute

Level 1Program rate= 8 .00°C

Final value= 220 °C

COMMENTS :

APPROVE D

~rrn 6`9-'

CSSFL ANALYTICAL CHEMISTRY NI T


H D M S E00624617


-- 14INSPECTION REQUIRED I CABLE DRRf

Ay4INGS (ATTACH IF EQ U~.RED

YES N O

ZOING DEPT LEDGER ACCOUNT GENERAL ORDER G 0 ITEM 6 MCR INIT . GROU P

REGU ESTE D

LAG SUPERVISIONI ASSIGNED TO

: LEADMA N

SHOP LAB

INSTRUCTIONS BE SPECIFIC) NOTETHIS FORM

I DATE

NDW OR TASK DOING GROU P

ESTIMATO R

MECHANIC



ESTIMATE


S

WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

t // /:F ' !C 7% .r 1

_- F F mt . E.~T

3'- / / 7- 83

II im uBNA01476344

L_ ! _- O~ MATERIALS

I IH D M S E00624618

;c S 55 ii . C3'SS 1 2

LOG N O

ra CHEMICAL ANALYSIS

F . E . LA °Y, D/596 , S S 11 REPORTC . WINZER, D / 031, SS 1 2

To :

FROM

DEPT./GROUP

3-d~ 33-8 3AIJ D

3-434-8 3


REFERENCE : r k Pd~G 5 2

LOG NO .SAMPLE

IDENTIFICATION

WATER SAMPLES FORFL'U RISE ANALYSI S

SELL CANYO N

3433 Mot,NTA r ?'J Ru r~OF~

~ time= ~ 2oA rii

~-434-83 ~ ;~ 1ti -~_ 7~SAN

i1

tI

GALLON S3.3 M E~~tIO N

It i

s~Rece ve= in the 1aE

ian'_ a-~al~zed ASAP

i3 i 24 .'

Tr4URSDAYi EPA distillation metho d

COMMENTS pert for SSFL al lows a maxinur of 1 .0 ppr fhcr ide to

~e s :3 `nor the c-ert y

APPROVE D

c-- • '_-,

I D IBNA0147634 5

PHONE 5__

DATE 24 - HAR- 8 3

RESULTS

PPM FLUORIDE, BY ELECTROD E

1 . / pp,n

1 . Ypom

~1:G/Ls~4C ~ E~iClfs~_Z-

SSFL A1 .ALYTIG+L CRDIISTR.1

I IH D M S E00624619

Ea s'e ., R . Knit Sj 1 1

5 cw-•o

Mac -.,;Y CHEMICAL ANALYSI S

B . LARY, D /5~6, Ss 11 REPORTC . WINZER, D/031, 55 12

TO:

FROM : SSFL A LYTICAL CHEMISTRY UNI T

REFERENCE : Lnrhnnk 2S Page. 52.

J=,^ s

LOG N O

3-q +3 -83TO

3-915-6 3

PHONE 544 7

DATE 23- MAK- 8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

EELL CANYON

time=

3-q 13 -S3 PP (7oo,ov "Q 0, 8 pp m

t ime= 3 00 P M

3-4 44 -F3 J M Ou NTAIN RUIJ OFF mpp

i me- 3 °S PM

~- 15-83~~ PH

on 9a1~ 2 . I ppmt ~,e= 3

Received in t~:e la b

and anal yzed ASAF

1 3/ 23/ Q 3

2At= WEDNESDAY' EPA distillation method

COMMENTS T, .e N"-ES per-it for SSFL allows a maximur of 1 .0 ppr fluoride to

:e ' :s :he -ced fro- the property .

APPROVEDSSFL ANALYTICAL"CHEMISTRY L'!~ :-

MBNA0147634 6

DEPT/GROUP

H D M S E00624620

CHEMICAL ANALYSIS

REPORT

TO : M . ucgg

FROM: SSFL ANALYTICAL CHEJ(ISTRY LIMIT

LO3

~34GL 83c E1DEPT. /GROUP

PHONE `11i 7

DATE 3/-//8 3

LOG NO .SAMPLE


3.401 -$3 Wastewater, Canoga Copper • ©, 13 T, g/ L

Site C, "Sea WorLd" Nickel - C) . Co 9

2 1o. hr . Propart ioaal p~ ~a'a^~1o f&(P n

3 Jz 2. /'3

srp1e received 3/z3, 31 3) b~

alyted for copper, pEnd nickel

COMMENTS : ".è L .A . City discharge li~1t for copper is 15 -gJl, for nickel the linit Isi2 rig/ 1 .

Analysee per M. Mogg ' e I81. -L22, 27 Oct . 198111 .D. • None detected

APPROVED

~3FL ANALYTICAL CK~t23TRY +JNL T


I I IH D M S E00624621

A LOG NO.

CHMICAL ANALYSIS

REPORT

TO: QUALITY ASSURANC E

FROM : SSFL ANALYTICAL

C

HFS'.ISTRY

REFERENCE : LOGBOOK O PAGE S

DEPT /GROUP D,'556

PHONE 544 7

DATE


GAS : N4L,Ut 1

RECD : 3 / :2..3 '83SAMPLER : r-L OQ(

PRESSURE , 1> / (ppm) TOTAL HYDROCARBONS AS CR 4

ANALYSIS REQUESTED

SPECIAL : HYDROCARBON S

AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE ND = NONE DETECTED ( = LESS THAN

ALFA BRAVOJ =GREATER THAN D<va = DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRAILE R

OTHER : S 1 /

COMMENTS : *Maxinum allowable limir per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for moisture is 9 ppm in He or H2, and 26 .3 ppm in No or 02 .

APPROVEDSSFL ANALYTICAL CHE7~SISTRY UNI T


H D M S E00624622

LOG NO .


TO : QUALITY ASSURANCE DEPT.fC3ROUP D/556

FROM : SSFL ANALYTICAL C~[ISTRY

REFERENCE : LOGBOOK 83 PAGE 5 °Z

3L 7/O3 3~g3

PHONE 5447

DATE

SAMPLELOG NO. IDENTIFICATION RESULTS

GAS : ~'

4/L3 f~s_

REC'D 3 /Z /Ps3

SAMPLER : _ l

PRESSURE 9 srt, fy, C). `, I (ppo) TOTAL HYDROCARBONS AS CH 4

ANALYSIS REQUESTED

COMPLETE


AS METHANE ONL Y

IFROM

SSFL SUPPLY LINETB = TRACE ND 2A)NE DETECTED < = LESS TBAX

ALFA BRAVO \=GREATER THAN DNA =DOES NOT APPLY

(X)CA DELTA

CPL-3 CTL-4

CPL-5 DELIVERY

TANK NO .

TRAILER

rr : SS P /~ 2COMMENTS :

APPROVED


SSFL ANALYTICAL CHD ISTRY 2'

H D M S E00624623

c : 3, S c3cr 539 _^:1 71

_ . Patota 598 58 1 2

CHEMICAL ANALYSIS

REPORT

TO

FROM :

J . Rosengard


LOG NO-

PHONE 329 3

REFERENCELogbook °83, p . 50-52 DATE 3/25/83

LOG NO .SAMPLE


3-400-83 Residue from NTO The residues were analyzed for the metals liste dsupply filter, found below by atomic absorption spectroscopy. Allon fitting joint results are in percent by weight .external surface

inside insulation . Joint Surface Filter ElementMetal Residue Residue

3-401-83 Residue from NTO

conditioner supply Aluminum 6.4 5. 7

filter elementbetween run tank and Calcium TRACE f~0.01 0.01

chiller .Chromium 0.02 0.23

Copper TRACE <0.01 0.03

Received ; 3/23/83

Iron 0.16 1. 4

Magnesium TRACE < 0.01 0.01

tZinc TRACE <0,01 0.03 i

The joint surface residue was found to contai n

11% nitrate by weight, while the sample from th e

filter element was found to contain 10% nitrate b y

weight .

COMMENTS :

APPROVED

t orm 619-V

= less than


3-400-83

3-401-83

DEPT./GROUP 539-166 EB 37

H D M S E00624624

SSS 1 1

CHEMICAL ANALYSI S

F . B . LARY, D/596, SS 11R E P URT

C . WINZER, 0/031, SS 12

K

LOG N O

3- 396- 3Tb

3- 399 -S 3

T0= DEPT/GROUP


REFERENCE i•n~h ,.~tc g 3 Pa ge 50

PHONE 5__

DATE z 3 - MAR- 83

LOG NO .SAMPLE



FLUORIDE ANALYSI S

33%3 MT rN RU OFF I . I pp ►, ntime= 32°PH3/22/83 TUESDAY

3-397-83 p PSD

O.9 pp.nt i r,e= 7 A M

3/23/3 ►"~ C D u >:5 DAY

3-39e-$3 F1oL TAl~ RQNoFFQ

mPPtime= 7 5 5AM

3/23/Q3 WEDNESA4 Y

3- 399 -83 R I 3 .1 Ppri,time= A M

3/23J3 WEDNESDA T

time=


and analyzed ASA D

-/ -I R 3

D~vm

= EPA distillation method

COMMENTS . The NPD=_S pe--it for SSFL allows a maximun of 1 .0 ppm fluoride to

be G :Sc'Zreec frog the property .

APPROVED

Orr Etc_~

.r

SSFL A L1TICAL CHEMISTRY U'U T

IIOI m u imi i iumm i im i ID 10 I0 00 I IBNA0147635 1

H D M S E00624625

CHEMICAL ANALYSI S

REPORT

TO: EQUT? NT LAB

PHONE 54l 7

DATE M'4R' Z3 ~ q

LOG NO .SAMPLE

IDENTIFICATION RESULTS O . j mg

TRICH for NVR per

FL10001-F

3-39'-t

raR Ho . 5 0387 0

BLANK mg/500 m].

xARDwAt 4 .1 m/500 ml

e'-, 5N1,4LL. VAL ✓~

EWR No . S 03 F'7 O

3 '3 9 S- j BLANK mg/ 500 ml

I1III' • o mW500 m~

SE L. I4/C' CA /

No .

BLANK mI

HARDWARE . mg/500 ml

APPROVED

M NAGER

LOG N O

3 -3 y~ - S 3

3 -3 95 -g3

DEPT/GROUP 598-31 x+

5 ~.a aSSF L Analy ical C emistry

IIDI muimiiiummiim i inmmm i

cc, W)B BUSH D/551 13A11 M . Mogg, 0/564, FB 66 Dr . R . P . Jewett , 01 539 . AC 1 0

JOEL LIEB D/539 AC1O M . Francis, D/564, FB 6 6

FRED SCHULER D/5513HEMICAL ANALYSIS

REPORT

T0= JOE @UAGLINO

LOG NO-

3 - 393 - 83

DEPT./GROUP D/539 BA33

FROM SSFL AKALYTICA L CHEMI STRY UNIT PHONE ___

REFERENCE LOGBOOK '83 . page 50 DATE 22 MARCH 1983

LOG NO .SAMPLE


3-393-83 RIGIDAX WAX RESULTS ATTACHED TO THIS REPORT FORM

i

COMMENTS ;

APPROVE D

t~-rr6?9 V


~- P L : al~ural t bemi 5FL ANALYTICAL CHEM:ISTRV UF :T

I IH D M S E00624627

SSFL ANALYTICAL CHEMISTRY 2 METHOD - GC Revision B

DATE MARCH 22 . 79R3 . ~ PHONE 5447

PAGE 1 of

RIGIDAX WAX SAMPLES SHOWING POLYCHLORINATED BIPHENYL (PCB) CONTENT AND%OR POLYCHWRINA'rED TERPHENYL (PCT )

GOO NUMI3ER SAMPLE IDENTIFICATION PCB CONTEPIT AS PCB CONTENT

AROCWR 1260 ( mg/kg ) OTHER THAN

AROCIA)R 1260(mg'kg )

PQLYCNIARINATEII

TERPHENYL (PCT )

CONTENT AS AMO-

CZAR 5460

2-51-83 Terphenyl Lot 5615 1620 ** N .A .

2-52-83 Terphenyl Lot 618, WI-LB 270 N .A .

2-170-83 WI-NF , Yellow, Lot 5356, Box#I 248 NA .

2-171-83 WI-NF, Yellow, Lot 5356, Box #11 785 NA .

2-172-83 WI-NF, Yellow, Lot 5356, Box #III 96 NA .

2-173-83 WI-NF, Yellow, Lot 5356, Box #IV 284 NA .

2-174-83 WI-NF, Yellow, Lot 5356, Box #V 376

2-175-83 WI-NF, Yellow, Lot 5356, Box #VI 893 NA .

2-179-83 WI-LB-NAT, Lot #L-4833, Box #I 290 NA ,

2-180-83 WI-LB-NAT, Lot #L-4933, Box #II 88 N .A .

2-181-83 WI-Light Blue, Lot #L-4436, Box lit 170 NA ,

rOMMF.NTS : • N . D . none detecte d

** NSA . = not available (These samples were not anniyzed for PCT cont:ont . No quantitetive

or qualitative data is presently available . )

DETECTION LIMITS : AROCLOR 1260 = 25 mg/ku

AROCLOR 546p = 50 mg/k g

Norma Fujikawa, ManagerSSFL Analytical Chemistry

SSFL ANALYT CAT . (`HEMISTRY UNIT

DATEv MARCH 22, 1983 PHONE 5447

PAGE 2 of 3

RIGIDAX WAX SAMPLES SHOWING POLYCHLORINATED BIPHENYL (PCB) CONTENT AND/OR POLYCHLORINATED TERPHENYL (PCT )

SSFL ANALYTICAL CHEMISTRY METHOD - GC Revision B

InG NUMBER SAMPLE IDENTIFICATION PCIl CONTENT AS PC © CONTEN T

AROCLOR 1260 (mg/kg ) OTHER THA N

AROCLOR 12G 0

(mg/kg )

POLYCHI (*IMATE!)

TF.RPIIFNYL (PCT )

CONTENT AS ARO-

CIA( 5460

2-182-83 WI-Light Blue, Lot #L-4436, Box #II 131 ** N .A.

2-183-83 WI-Light Blue, Lot #L-4436, Box #III 127 N .A .

2-184-83 WI-Light Blue, Lot #L-4436, Box #IV 184 N .A .

2-185-83 WI-Light Blue, Lot #L-4570, Box #I 150 N .A .

2-186-83 Type unknown , Lot unknown, No Label 2800 N,A ,

2-187-83 WI-Light Blue, Lot #3308 2700 N .A .

2-188-83 WI-Light Blue, Lot #618, Box #I 240 N .A .

2-189-83 WI-Light Blue, Lot #618 240 N .A .

2-190-83 WI-Light Blue, Lot #618, Box #I 210 N .A ,

2-191-83 WI Light Blue, Lot #(318, Box $11 150 N,A ,

2-192-83 WI-Light Blue, Lot #618, Box #III 230 N,A ,

CflIME:NTS : + N .D. = none detected

* *

APPROVED '.J !CAL (91FM(54THY UNTTNorma Fu/(kawa , Manager

l391rT, ANAt,YT

ScR 4/J Chernlsfry

N .A . = not available (These sumpl ©s were not unulyaed ['or PC'!' eontant . No IuunhlLuLlve

or qualitative data is presently uvulluble . )

DETECTION LIMITS : AROCWR 1260 = 25 mg/kgAROCLOR 3460 = 50 mg/kg

1 ~

DATE MARCH 22, 1983

RIGIDAX WAX SAMPLES SHOWING POLYCHLORINATED BIPHENYL (PCB) CONTENT AND/OR POLYCHLORINATED TERPHENYL (PCT )

IL)G NUMBER

SSFL ANALYTICAL CHEMISTR Y

SAMPLE IDENTIFICATION

METHOD - CC Revision 9

PC II CONTENT AS * PCB CONTENT AS

AROCIAR 1290 ( mK/kg ) AROGLOIt 12 60

PAGE 3 o f

PHONE 5447

2-269-83 WI886D, Lot #0.01, 28 4100

2-270-83 WI886D , Lot #0 .02, (~) 3300

2-271-83 WI886D , Lot #0.005, 29 91

2-357-83 Blue wax in glasa beaker 2766

2-358-83 Gray-blue in plastic bag 2308

2-359-83 Blue wax in plastic bag 1409

* 3-39-83 WI-LB, Lot 4436, PCB Storage Area 147, 159, 120

* 3-40-83 WI-LB, Lot 618(BoxIII ), PCB Storage 226,218, 130

* 3-41-83 WI-LB, Lot 3308, PCB Storage Area 2003,2667, 238 4

DETECTION LIMITS : AROCLOR 1260 =

AROCLHt 5460 =

25 mg/kg

50 mg/kg

COMMENTS : * Theee samples were analyzed in triplicnto and ull three eamplescould be sent to the EPA National Enforcement and Investigation

** N .A . = not available (Those samplo8 wore not analyzed Tor PC Tor qualitative data ie pro8ently availablo . )

APPROVE D

Norma Fajlkuma, Ma nCcc, Arnalulknl Ch„irl

rml/k0

POLYCli InN t NATFI )

TFRtiiENYI . (PCT)

CONTENT AS

AROCLOR 546 0

** N .A .

N.A .

N .A .

N .A .

N .A .

N .A .

N .A .

N .A .

N .A .

were split eo that portions

Center in Dunvor, Colorado .

content . No (luantitatlvu

1

- / {.c . ~9SFL ANALYTICAL . CHEMISTRY t1NI'C

LOG NO .

CHEN11CAL ANALYSIS

REPORT

TO : B . BEAROSLE Y

FROM SSFL ANALYTICAL CKLV .'!_7nY UNI T

REFERENCE : L o56ook 83 Pa ge S O

3-3'2- 3

DEPT./GROUP 5 9 e/3, -7511

PHONE 54,47

DATE 23-MAR-& 3

LOG NO,SAMPLE


('AS SAMPLE NITROGEN TRIFLVDRiDE (NF3 )

m o l e

3-392-83 NF3 CTL -3 36 .9 °D NF3

2 t7Ak -

COMMENTS :

APRROVE Z^SSFL AkALY:'1CAL CKDi!STRS UNI

CHEMICAL ANALYSIS

REPORT

TO: VV . Mce Q

SSFL AMLYTICAL OLI4( ISTlIY UIII T

REl pENCE: Logbook ' 8 -~ pg . 7l_J

L1.3 PiQ .

3- 3~ I - 8DEFT J oRauP 564,

p*E 5447

,~.~.~.. OATE 2, ._-

LOCI 4O•SAMPLE


3"3Ì'$3 Wastewater , Canoga Chromium = NJ. U. O,O ~j ► /L

Site B , D/544 Process pH = 7 . 9'Clarifie r


sample

Sample received 31-Z2A

6-) oci 3S


chromium

COMMENTS : The L .A . city discharge limit for chromium Is 10 '59,'L

Analyses per M . Mogg's IL 81 FE-422 , 27 Oct . 193 1

APP"OVED , urT \ v~-~4 f -tic

S3FL AKALYTI CA L Q Dt. T*Y -:.NI T

BNA0147635 8

H D M S E00624632

CHEMICAL ANALYSIS

REPORT

TO : M . Kogg DEPT/GROU P


REFERENCE : Logbook ' 83 DR . SO

LOG N Q

3-3D- 3

PHONE c4L7

DATE /Z3

LOG NO .SAMPLE


3'3!L}$3 Waetewater, Canoga Copper - 0 .1 C~ Tg/ L

Site C, "Sea World" Rickel ~, 9 =3/L

PH ! . g24 nr . Pronort'_oielsP--D1P takwn

ample received 311463

(7 011 .5

Analyzed for copper, pHand nickel

COMMENTS . The L .A. City discharge limit for copper is 15 r.gJ 1, for nickel the 11-nit is12 m4V1 .

Analyses per M. Mogg 's t . 81 P!-422, 27 Oct . 1991R .D . • None detected

APPROVED N. fSSt'L AÀLfTLCAL C(. i4ISTRY :L'+L T

BNA0147635 9

HDMSE00624633


a1-03 NO -

3 -388- 8

Pt-ION E 5"7

DATE --3J2-3 /83

LOG NO .SAMPLE


1 _ 26~-63 Wastewater, Canoga

Site L, D/544 Scrubber Ciromi ia - 2 (o o ,,. / LSump

..

PH (o

Grab Saaple take n

3/22-/ 3,0-7q5

5 eived,3/' ✓6


SaFL ANALYTICAL (H ISTAY 'S'IT

SS 1 1

Bowman-

gcis

CHEMICAL ANALYSISM . Mog

F . B . LARY , D/596 , SS 11 REPORTC . WINZER, D/031, SS 1 2

TO:


REFERENCE : Lnghnnk 83 P43t 50

K . Jor-s,S S

LOG NO .

3- 385-E 3To

3-387-83DEPT./ GROUP

PHONE 5447

DATE 22- MAR -8 3

LOG NO .SAMPLE

ID ENTIFICATI ON RESULTS


FLUORIDE ANALYSI S

BELL CANYO N

time=

3-385-g3

~

R I HG LIONS -T .s Pf1 i

time= $ 3S/`j M

3-386-83 P P l 5GLAW J , 2 PP M3 o

time= g AM

3-387-93 MOUNTA/N RUNOFF

/time= g SAM

time=


and analyzed ASA P

3 1 22 / 8 3

DAY= TU E SDAY EPA distillation metho d



APPROVED

Form 614-U

SSFL 14ALYTICAL CHEMISTRY :?\I T

BNA0147636 1

HDMSE00624635

cc! J . Becker 539 BA 71

F . Patota 598 SS 1 2

TO:

FROM


J . Rosengard


REFERENCE :Logbook '83, p . 50

539-166DEPT/GROUP

LOG N O

PHONE 3293

DATE

3-384-8 3

3/25/83

LOG NO .SAMPLE


3-384-83 Residue from 2-inch The sample was analyzed by atomic absorptio n

NTO run line filter, spectroscopy for the metals listed below . Result s

STL-4, cell 29B . shown are percent by weight .

Aluminum 6 .7 %

Calcium 0 .02 %Chromium 0 .19 %

Received 3/21/83 Copper 0 .02 %

Iron 1 .2 %

Magnesium 0 .07 %

Zinc 0.01 %

The sample was also found to contain 11% nitrat e

by weight .

COMMENTS :

APPROVE D

I Drrrn 61G-V

SSFL'AJ4ALY7TICAL CHEMISTRY' T NIT_

I IBNAO147636 2

EB 37

H D M S E00624636

c .c


TO : i-Ye ,n k o '~+D DEPT./GROUP

S SFL ANA LYTICA L C IUMI STRY UNI T

/t1E.MRENCE : I By S3 PACE 5t

LOG NO

3-381-$ 3

PHONE 544

DATE rrg. (q Q

LOG NO-SAMPLE


1FP0 from STL - 4, DENSITY . . . . . . . . . . . . . 1,

(

59ga/Kl at 60° F

CELL _ N204 . . . . . . . . . . . . . . . 200 %a)

H2O . . . . . . . . . . . . . . . . 6.2$ % LJ

CI- . . . . . . . . . . . . . . . . _ o. 01 0

ANALYSIS PER Fe* . . . . . . . . . . . . . . . . . Q .7 PPm 1tiq ! K 9SPECIFICATION :

Nil-P-265390NVR*"""""""" mg/liter

RECEIVED IAB :

3/21rt

1~1i~-t-~CS3g GL1 --S rEi1

N2 o,t . - N O rrur k vr. urr+ = g 9 . 5Wad.'r eq~lvala~3' maat.IMfl = O . 1 77%,

0 M E NT 5 : mA = DOES ) T APPLY 4 : L.,55 t h0

* This analysis is not included in Vil -P-265390 .

A.ctRO vE D'-~ ~1 II

` IDt T'TIGL C z[ 1 STY .SSFL AlaLY

I IBNA0147636 3

HDMSE00624637

Rocketdyne Division01% Rockwell International

DATE CONT., G .D

3 ```'4

REFERENCE REPORT NO .

PART NAME & NUMBER QUANTIT Y

Po>A`` ~c1M 1..ot? «

MATERIALS & PROCESSES MATERIAL SPECIFICATION

/n1 A ijTEST REPORTSUBMITTED B Y

111 .5 1•'tJ i r a<rilnltADEPARTMENT LOCATIO N

S5 )el-PHON E

PURPOSE OF TESTCN ' cl o s , o Co x r

CHEMICAL ANALYSI SELEMENT

REO'D .

OBTAINED

TENSILE TESTS

LABORATORY TESTS AND RESULT S

SAMPLENO.

YIELDSTRENGT H

Kai

ULTIMATELOAD

LBL

ULTIMAT ESTRENGTH

KSI

ELONGA •TION

'R

REDUCTIO NOF AREA

SS

HARDNESSREMARK S

REO'D .

OBTAINE D

OTHER TEST S

rT< E tit ATzE r',1, !_ A 5 11 LYL 1: / x ) AL . o X1M r b

n , L - A ) 7 J 1,! H M C a SCo SoM a ~~ , Y ,

=~` ~1 J~' ~A ~' "T"6 A5~ ?r ^~'k_D ~l r_ U ran r4Rr?, L

AmuLtil7 O~ C-Ai-Liu NIC . i Ci]UL~ YAO/14 'x11 !~1 b

C-r

}~l 77,a .fio'LC v G 'T CI O r-?

FORM R 70-U-1 REV . 3 .73

jai -2'.2 -1S 3Slplnd Date Appray*d Date

VBNA01476364

HDMSE00624638

ENGINEE RIN G "WORK REQUEST

No. R 37121 7INSPECTION REQUIRE D

YE S NO

DOING DEPT LEDGER ACCOUN T

2447STEP B Y

rLAB SUPERVISION I LEADMAN

+Q'I EHOW OR TASK ', DOING ODOUR

ESTIMATO R

MECHANIC

REOLEST, ED COMPLETION DATE


ESTIMATE

HOURS MATERIALSREQUIRED R EQUI RED

S

INSTRUCTIONS ( BE SPECIFICI NOTE- THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

The attached sample is from the insulation on the potassium loop at

SSFL . Michael Francis, the environmental specialist, will ne taking

contr3ttors out to the loop on 3/23/83 to see about disposal, an d

he needs to know whether or not the insulation is ( JALITATIVELY, 110T )UANT . )

asbestos . ?lease call N .S . Fujikawa at5448 wit h

APPLICABLE DRAWINGS ATTACH 'F 0F01 .' RE D

GENERAL ORDER G O TEN A CC R

EXT .

5448

4 0206 nl-)20FACILITY SHIFT REQ . SUPERVISIO N

SS 1 1 . S . Fug Iawa

ASSIGNED T O

SHOP j I LAB

"arty ~obertson , 3'--147,

the results, o r

OVERTIME IS AUTHORIZED IF IT IS `4ECESSARY . 4/'f ; ,

sc F L Lo Cs - 3 --'3 S0 - 33

-OpR R $4-,. FE'J 5-57

LIST OF MATERIALS

I IBNA0147636 5

HDMSE00624639

CHEMICAL ANALYSISREPORT 3 -3 -93

TO: W moQQ OW!!T./eROUR 564,

!ROSS S3FL A :MLYTI CA L O4. I3TIIT UNIT

RE.pERENCE: Logbook ' 19 3 pg. SO

P*lE 5447

DATE

L048 NO-SAMP


3-37i-g-; wastewater, Canoga Chromium • Jy 'p . Q 05

/Site B, D/544 Process~

pH /, 7Clari fier

G a ..asample TA Kai ► s

3 /2/ /'2 3o-73S

Sample received


COMME! TS: The L .A . city discharge licit for chromium is 10 mg/'L

Analyses per Y . Yogg 's IL 81 FE-422, 27 Oct . 1981

APPROVEDSUL ANALYTICAL ChXbUMT MILT

BNA0147636 6H D M S E00624640

J .


- DEPT./OROsJP .~.~.~

£SFL AA LYf 1 CAL i1 STRY UNI T

: LDG sx ' 83 PA 6 C)

LOO N O

3 - 3~g-g3

PHONE 5447

DATE 2S . ~g 3

'~- WO .SAMPLE


!PO from STL - 4 , DENSITY . . . . . . . . . . . . 1 .J35 gn/al ■t 60° F

DELL '37 N204 . . . . . . . . . . . . . . . _ x

HO . . . . . . . . . . . . . . . . OHO 2 %

:- '9

C1 . . . . . . . . . . . . . . . . 0 . DPI x

IID . . . . . . . . . . . . . . . . . e_g~_ x

ANALYSIS PER Fey . . . . . . . . . . . . . . .. , PPmSF'ECIFICATIOir :

=i1-P-265390 NVB* . . . . . . . . . . . . . . . . _________ mg/lite r

)>Z£CE I VED F LAB :

3,%:3

C.+7a~AeiENT 5 : Df.A =DOES ) 0T APPLY

m This analysis is Dot, included in 1il -f-26539C

SSF1. LMLT WA L fl{ tI STkY I T

IIOI m u imi i iumm i im i IDO ID DBNA0147636 7

H D M S E00624641

CHEMICAL ANALYSIS

REPORT

To: C . Wt ►JzE R

FROM :SSFL ANALYTICAL CHEMISTRY UNIT

REFERENCE :Lo]oook 83 PgQ- co

LOG NO

3-377-83

DEPT/GROUP 231 SS/ 2

PHONE __

DATE 21 - MA R ' 8 3

LOG NO .SAMPLE


WATER SA r1 PL E TR l ( LO RO E TH ' L E ►~ E (T )

3-377-83 S E LL CANy'ON NIA < l pP ~

pE-c v3/2/4 3

oND~ Y

COMMENTS:

APPROVE D

"`_ ° iivi m u imi i iumm iimiiiunmiu

J ?., FB L_ 6a s e~, . Kr ', S:/ coR, SS 1 1

Bowman

r'ciF raM .CHEMICAL ANALYSIS

F . B . 1.ARY , D/596 , ss „ R EPORTC . WINZER, D/031, 55 12

K . Johns,SS 1 2

LOG N O

3-3%-8 3

TO DEPT. /GROUP

FROM SSFL ANALYTICAL ( iEMISTRY UNI T

REFERENCE : Lnvhnnk S3 P gc)

PHONE 5447

DATE _____ - S 3

LOG NO .SAMPLE


BY ELECTROD EPPM FLUORIDEWATER SAMPLES FOR

,

FLUORIDE AfiALYS f S

'3-376-83 BELL CANYON pr. 1O, S 1time= I0

30AH

,

time=

time=

time=

t i e=

eceived in the 1a 6

land analyzed ASA P

3/2I/E 3

DAY= _____ EPA distillation method

________ jCOMMENTS : The NPD_5 per-it for SSFL allows a maximum of t .0 ppm fluoride to

be discharged frog t he prorertY .

APPROVEDSSFL ANLYTTICAL CHE41ISTRY UNI T

II0I m u imi i iumm i im i 100 I D I DID D IBNA0147636 9

H D M S E00624643

CHEMICAL ANALYSIS

REPORT3-375-~3

TO : M. Mogg DEPT./GROUP 5

SSFL ANALYTICAL CHEMISTRY UNI TFROM: PHONE 5!a?

REFERENCE : Logbook 'SP . Sd DATE `__

LOG NO •SAMPLE


337c3 Wastewater, Canog aSite L, D/54b Scrubber Cttromiu ..n • 2710Su¢p pH - 7 7Grab Sanp1e take n

3 /zi / c 3

le Received /ifgAnalyzed for pH, andchromiua

COMMENTS: The licit for Site L is 75 rngf 1.

APPROVED

.,rm 619-V

SSFL ANALYTICAL C L USTRY UNI

iimm u imi i iumm iiumiu i iiim i

J :.C . ..

CHEMICAL ANALYSIS

REPORT

EQt TTPMENT LAB

FROM : SSFL -ANALYTICAL CHEMI STR Y

REFERENCE : -8-3 P•

LOG N O

3 -373 - 63To

3 -37i/-83

DEPT./GROUP 598-31

PHONE S~~ T

DATE MAR . 2 2 , 1 983

LOG NO .SAMPLE

IDENTIFICATION± 0 .3 m8RESULTS

TRICH for NVR per

RL10001-F

3-373 " EriRR No . '3722 7

BLANK mg1500 ml

A°.E 3. 4- mg/500 mI

r-'8oor *

EWR No . '1 3722 7

BLANK ma/500 ml3-37µ-

5 NI,►t,L V4L ✓E

No .

ffi•AP(!C m1

HARI7iJARB mg/500 ml

COMMENTS :

APPROVED

Recd . _ 2I

SSF L Ana tic.I C tmistry

IIDI m u imi i iumm iiumi i III DII I I

Sc~^ D r' S~ W . Basle , R . K-'q' t, D,5°8, 55 1 1

. Bo•ira nFM . ranc ,

CHEMICAL ANALYSISM . Mo

F . B . LARY, 0 /596 , Ss 11 REPORTC . WINZER, 0/031 , SS 1 2

TO. DEPT./GROU P

FROM : SSFL ANALYTICAL (EMISTRY UNIT

REFERENCE : t nahnnk 83 TQ~1G S)

K . Johns, D!'31SS 1 2

LOG N0 •

3-368-83TD

3- 3?2 -8 3

PHONE 5447

DATE z l - /'9A R - $3

LOG NO.SAMPLE



FLUORIDE ANALYSI S

3-368-3 PP ~• 6 pp'

time= 9 'API

3-3-63 ,QZ 0 . 3 pptime= 9 °S~M

3-370-83 MDufJ TA,AJ RuNoFF

t i ae= 9 ____

3- 371- 83 RI 4.0 Ppii

time 9~ lA /-i

3- 372- 8 3 EC[ -2 2 .0 p,°t i " Se= 9 4 SAM

Received in the la ba-C analyzed ASAP

31 21 / 8 3

t f C JDA Y- , EPA distillation metho d

COMMENTS : The NRDES permit for SSFL alloys a raximur of 1 .0 ppm fluoride to

be disc-a-ged frocr the property .

APPROVED

SSFL ANALY-TICA CH!'ISTRY UNI T

IIOI m u imi i iumm i im i DID IBNA01476372

I IH D M S E00624646

C1-I EN-11CAL ANALYSIS

REPORT

I TOQUALITY ASSURANC E

FROM:SSFl-ANAXY11CA . XMISIRY

REFERENCE :

LOG NO .

t

3-36~-8 3

L .B .83 : P. s I

SAMPLE

IDENTIFICATION

GAS : L Hz

DEPT./GROUP556

LOGNO-

3-3(7-83

PHONE 5447 Y

DATE MAR - 12 1 19`t 3

RESULT S

PURITY = > a9 .9g9 Ha _ By Difference

RECEIVED : PARA = 'DMA % 1

SAMPLER : FL oo532 .1

PRESSURE : 400 # IMPURITIES

02 = DN A 1 02 = NIA < 1 ppmANALYSIS REQUESTED :

N 2 N 2 = ND < I ppm

Ar = Ar = ri3> < 1 ppmSPECIAL : CO CO = ND<5 ppm

C0 = = NDCO S2 2 pprr,<O.

CH = % CH =4 . 4 t7rc~ PPMMFR :O

C2H2 =16 C2H2 = -P p m

SSFL SUPPLY LINE H2 = % H2 pmALFA

ERAVO 7R< (ppm) Total Hydrocarbons as CH 4

DELTAMOISTURE = O ( < $6 °F DEW POINT )/, _ ppm H

A-3 TANK j00 - 2

CTL 3

CTL 4

CTLS

TANK NO .

DELIVERY

TRAILER

OTHE R

1

COMMENTS :

APPROVED

Tr = Trace< = Less Tha n> = Grcoter Than

N .D . = None DetectedD .N .A . = Does Not Appl y

~► Maxim= allowable limit per RAC 615-072 for NG is 15 ppm ; for 02 + Ar it

is 5 pp©•

rid rL Arn • f - ..I

MBNA0147637 3

H D M S E00624647

CHEMICAL ANALYSIS

REPORT

TO : T'/M U)/~-SDN DEPT./GROU P


REFERENCE L'OG ScOK '93 , p,4GE 50

r

PHONE `cy7

DATE d/ MA/` X83

LOG NO .SAMPLE


3-366-NS~DkAuL1G PLvLD

C!) _ /3 PPM ~ YF7eEON rF (ci FCC FF,CoM 1QE 5E'EJvv rlt? a aVOLUM E

/¢T A-3

COMMENTS :

APPROVED

)r r' 679-V

LOG NO .

.3- 3G~ - ~3

IIOI m u imi i iumm i im i II I IBNA01476374


H D M S E00624648

LOG NO


TO . W!Aiz£R


REFERENCE ~- Oq~ao{c S 3 Page 5-0

DEPT./GROUP 03

3-3q-83

SS/ 2

PHONE 3447

8DATE

2'- 5

LOG NO .SAMPLE


WATER SAHPLE TRICF+ LOROETHYIEQE (7zE )

3-364-83 &EL& CAiv}'oA/ 41/) .< / p, 6

/eel IQ

3/i 9183S ATvR04 Y

COMMENTS :

APPROVEDSSFL ANA ICA L

_` 9 ° iii muim i iiu mmiium i

R . Schmued ?. 0/564, FB 66 W . Baisley , R . Knight , 0 /598, SS 1 1

J . BowmaniF ranc s.M .

CHEMICAL ANALYSI SM . Moga/

F . B . LARY , 0 /596 , SS 11 REPQRTC . WINZER, 0 /031, 55 12

K . Johns, 0/031 ,SS 1 2

LOG N O

3- 360-83ra

3 -363- 3

TO DEPT/GROUP

FROM : SSFL MIALYTICAL QiEMISTRY UNI T

REFERENCE : Ln .hnnk 8 3 Pa gc. S C)

PHONE 544 7

DATE 2I-HA,--e 3

LOG NO .SAMPLE



FLUORIDE ANALYSIS

m3-360 .83 BELL CANYON o. 6 P'time= / D 45 A !'?

3/i/73 s r

3-3/-8 3 /-83 Jt'Iou,urAi,v ~Pv~vo~F / . 9 pp rvi/ti=__________

3 ii/t3 sAT

3-362-83 BEL L W'rD/v ~. Piontime= 95 H_

3/Z/ e3 S~M.~

3-363-53 MouNrtiN A uo;F I. ~p/ MI

time (1 A MSL AI .

time=

Received in the la band analyzed ASA?

-/-/83

OAY== EPA distillation method

COMMENTS . The NPDES perrit for SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVED/ J4c(/ a91

EFL ANALYTICAL CHE~:iS:'F.L? i '


HDMSE00624650

cc : J . Becker 539 BA ;1

F . Patota 598 SS 12

CHEMICAL ANALYSIS

REPORT

LOG NO -

3-357-833-358-83

TO : J . RosengardDEPT. /GROUP

539-166 EB 37

FROM : SSFL ANALYTICAL CHEMISTRY UNITPHONE 3293

REFERENCE Logbook '83, p . 50 3/25/83DATE

LOG NO .SAMPLE


SST-8-3/17/83

Both samples we re analyzed by atomic absorptio n3-357-83 Residue from STL-4, spectroscopy for the following metals . Results

cell 29B . are listed in percent by weight .Orifice plate

Metal Plate Residue Inlet Residue

3-358-83 Residue from STL-4,i

Aluminum 7.4 7. 8cell 29B .

Valve inlet, oxidizer Calcium 0.02 0.01side .

Chromium 0.03 0.04

Copper 0.01 0.02

Received : 3/18/83 Iron 0.14 0.1 6

Magnesium 0.04 0.07

Zinc 0.04 0.04

The plate residue was found to contain 10%a nitrat e

by weight, while the inlet residue analyzed a t11% nitrate by weight .

COMMENTS :

APPROVED 4Lform 619-V

SSFL €tALYTICAL CHEMISTRY UNI T

IIOI m u imi i iumm i im iIIBNA0147637 7

HDMSE00624651

c t


DEPT./ OUP .2,8.

SSFL ANALYTICAL OiDiI STRY UNIT

LOG NO

3 - 3,-'3

PHONE 5447

DATE tK 1qR'~

LOG NO .SAMPLE

IDENTIFICATION USULTS (by weight )

!FO f roa STL - 4, Li 5' ga/=1 at 60° FDENS ITY . . . . . . . . . . . . . •

CELL ~ g(

N204 . . . . . . . . . . . . . . . l.11. _ %

0 . . . . . . . . . . . . . . . . O ' a (4 xH3-35r~-83 2

C1- . . . . . . . . . . . . . . . . O .oz S

ro . . . . . . . . . . . . . . . . . 0,45 xpA,u i. sIs P1yR Fe*. . . . . . . . . . . . . . . . . _,_ PPa . tN3'~

3SPECIFICATION :

NVR*.. . " °""""" I D ag/lite r

Mi1-P-265390

RECBIVED LAB :

3 / I, / ~3

LI r pE R. M (L -rQj ►Jo con}ems' M ► n . ' o. b2~ MA ' { .O Z

I M E NT 5 : IliA = DOES NOT APPLY

• Thia analysis 16 not iacluded in Yi1-P-265390 .

APPROVE D

rERLNcE : LOG Hx ' a3 PA(~ 5 0

_- .- F•o-v

SSFL A1IALTTIoAL Isiw UNIT


H D M S E00624652


FROM: SSFL A NA LYTICAL CHEMISTRY UNI T

REFERENCE

LOG NO .

- 3 S7- Y 3

3-353- 77

3 - 3S4-Y3

g- 3S S -YS

COMMENTS :

APPROVE D

Fcr . .' F1Q-V

L t $3- So


M M H '1 e/

9 . c

r4 1 s ,, . /,, .e ,~Ay << tow t '.' los s

fo .~ MMN

S ►" s

w S

LOG NO •

3 - i11 - Y Z

t.

3 - a ss - $ 3

DEPT./GROUP Sy Q -

PHONE 5f Y- 7

DATE ___f~______~RESULTS ►,v M .~cl / 9bAt, %

I Cl~L, wctC~Isr

..ay

13

o/ s .'1 .t 1r '

''? //LJ -

No r, na ManagesSSFL Analy ! Chenltslrg

SSFL ANALYTICAL CHEMISTRY IJNI T

IIOI muim i iiu mmiium imi i uu

vv ; y IFa m ; -4 . E cts .f-- 42 Sr4.4-M (J ED,GFS 6

S9gI/564,

F Qy~ ~' CHEMICAL ANALYSISSS t

REPORT

LOG NO •

3 - 3~ 8 -8 3

TO: W ► IJ Z E R. DEPT. /GROUP 03 / SS / 2


REFERENCE : Lo.g~oo)< S3 Page 98

PriON E 541 7

DATE / ?- MA R - 8 3

LOG NO•SAMPLE


y,rArFR SAHPLE TR(CNLOWETNYLENE (TC E

3-398-83 BELL 14NYo/v TA /

o5

Ft~1D" 1

REVD If tiM-83

bVR,?Jb DISCHARG E

I-FR M ITrE lT

/ EAV YS owE 5

COMMENTS :

APPROVE D

V yrT F~q-~,~


SSFL ANAL _ UNIT

I IH D M S E00624654

R ~- -Je~ ^!>~~ F R 56 W, Baisley , R . Krisht D/598, SS 11

J . isormar V .S .~✓~'C~-~f5981 3S Il)M . Franc

CHEMICAL ANALYSISM . Mao

F . B . LARY , 0/596 , SS 11 REPORTC . /INZER, 0/031, SS 12

TO:


REFERENCE : i .r, hnnk 8 3 I'etgc

PHONE 5447

DATE l ' -MAR - S3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

3-395-8 3 BELL CANYON O

1time= ~ySPH

3-36-S3 M OVNTAiPJ RUN O FF 1 L P Pt i rtie= ____

3-347-83 A PIF 3 .0 ppriPt-itime= !

t irfe =

time=


and analyzed ASA P

3 / /8 / a 3

DAY= FR DAB= EPA distillation method

lur>~QM 1'tiFNTE v 5


be discharged from the propert y

APPROVE D

tor-- f t c_

SSFL ?IALYTIGIL CHF1►~ISTA~' L"~Z T

iimm u imi i iumm i im iBNA0147638 1

K . Jo'-rs, 0/331 ,SS 1 2

LOG N O

3-395-8 3TO

3-317 -8 3DEPT./GROUP

I IHDMSE00624655

1- S ca+U LE2 Q U I4G-t I AJO , f S 39 -16 ~~ 3/4 33

CHEMICAL ANALYSI S

TC1 : M . ?ranci s

IFROM~

REPORT

LOG N O

3 - 344 - 83

(re-sample o f

2-353-83 )

DEPT /GROUP 564 FB66

PHONE 544?

DATE Mar . 22, 1983

SSFL ANALYTICAL CEiAIISTRY UNI T

REFERENCE LB-83-page 49, NB329 p . 146

LOG NO•SAMPLE

IDENTIFICATION RESULTS (OC REVISION B )

3-344-83 RIGIDAX, WI-NF 25-9 Total PCB's as Aroclor 1260 < 25 mg/kgLot 3125, Light

Brown Lump . Detection Limit = 25 mg/kg

This was a cleanl y

taken sample ofTotal PCT's as Aroclor 5460 ( 50 mg/k g

material from theDetection Limit = 50 mg!kg

same WI-NF 25- 9

that was identifie d

as SSFL log #

2-353-83 ,

believed to have L =J Results were obtained using a gas chroaatograph

been contaminated .equipped with an electron capture detector . A sixfoot glass coluam packed with 3% SP-2100 on 100/120

during the sampling ,esh Supelcoport was utilised under the following

cn di t i ons :proces s . O'P>eQI TI RATURE PROFI IB :

Initial value = 200°CInitial time = 1 .00 ainuteLevel 1

This sample Progras rata = 8 .00 °C

was received]rind value = 335 °C

18 March 1983 . Q The cbraaatograa did not ooepare with known Aroclor

1260 . gowever , there are a nu.ber of peaks present

in the area where KB's would be expected to beeluted .

COMMENTS : G = Less thanN .A . = Not available

APPROVED

1 orm 619-VMA! AG


n C t

SSFL AISA LYf 1 CAL CBAiI 9TRY LDI I T

UH D M S E00624656

SUtV t j2 4 ~ . Q U IEcru NO / ` !69 33

CHEMICAL ANALYSI S

M . Franci s

FROM

REPORT

SSFL ANALYTICAL OiE1[ISTRY UNI T

REFERENCE : LB-83-page 49, NB 329 p . 145

3 - 343 - 83(re-sample o f

2-354-83 )

DEPT/GROUP 564 FB66

PHONE -- 544 7

DATEMar . 22, 198 3

LOG NO•SAMPLE

IDENTIFICATION RESULTS ( OC REVISIOE4 B )

3-343-83 RIGIDAX, WI-LB 25-9 Total PCB's as Aroclor 1260 < 25 mg/kg

Lot 3124, Blue LumpDetection Limit = 25 mg/kg

This is acleanly takensample of material

50'from the same mg!kgs as Aroclor 5460Total PCT

WI-LB 25-9 Rigidaxthat had been Detection Limit = 50 mg/kg

previously submitt eand was identifiedas SSFL log #2-354-83 . It i sbelieved tha t2-354-83 wa scontaminated durin gthe samplingprocess . Results were obtained using a gas chrovatograph

equipped with an electron capture detector . A sixfoot glass coluan packed with 3% SP-2100 on 100/120

RECEIVED 18 Mar . 198 mesh Supelcopo rt vas utilized under the following

conditions :O r T1~IF'EPATURE PROFI1Z

Initial valve = 200°C

Initial tine = 1 .00 sinute

Level 1Progra ■ rath = 8 .00 °CFinal value = 335 °C

The ehroeatogras did not coapare with known Aroclor

1260 . Rowever, there are a number of peaks presen t

in the area where PCB's would be expected to b e

eluted .

COMMENTS: • = Less thanN .A . = Not available

APPROVED

/vrm619-V

MAN AGE

C .SSFL AMLYr 1GL C3iSI1 9TRY tWI T


I IHDMSE00624657

~. ScHOL 1. t ~- QuaGLuJO '/53 q -16Q 1 ~A 33

CHEMICAL ANALYSI S

M • Mo&G-TO : L . Franci s

SSFL ANALYTICAL Cfi>d[ISTRY UNIT

3-342-83(re-sample of

2-354-83 )

DEPT/GROUP 564 FB66

REFERENCELB-83-page 49, NB 329 p . 144

PP$ONE 544 ?

DATEMar . 22, 1983

LOG NO .SAMPLE

IDENTIFICATION RESULTS (GC REVISIOI+1 8)

3-342-83 RIGIDAX, WI-LB 25-9 Total PCB's as Aroclor 1260 < 25 mg/kg

Lot 3121, Slue LumpDetection Limit = 25 mg/k g

This is a cleanl ytaken sample o fmaterial from thesame WI-LB 25-gthat had previously

Total PCB's as Aroclor 5460 G 50 mg/kg

been submitteddd i

Detection Limit = 50 mg/k geand was i enti f

as SSFL log #2-354-83, It i sbelieved tha t2-354-83 wa scontaminated durin gthe samplin gprocess .

0 Results were obtained using a gas chroeatographequipped with an electron capture detector. A six

foot `lass coluam packed with 3% SP-2100 on 100/120

each Supelcoport wan utilized under the followingconditions :

OV>~I TBit3'RRATURE P 1)FILI3 :prC ~7~ Initial value = 200°C

/~ G y Initial tiee = 1,00 ainute

D I PMAR iLevel 1

°. CProgn■ rata = 8 .00Final value = 335 4C

~ The ckroeatograa did not coapare with known Aroclo r~ .--

1260. however, there are a nuaber of peaks resen t

in the area where PCB's would be expected to be

eluted .

COMMENTS: G = Less thanN .A . = Not availabl e

APPROVED

I orrn 619-V

REPORT 1

MA'\ AGE SSFL AKALYTICAL (I1STllY UII(IT

IIOI m u imi i iumm i im i ID DI 0 I 0 IBNA01476384

HDMSE00624658

'{~~Icc . D . Bowman, D/539, 055, SS12


ILK: if kBER :

?O: Qu• 11 t7 Aaaareane 7el~r.llioloP:

PWW : SSFL AMLYTICAL Ft T IAWLMV Y

RSFSRENCB :

pgq fg : 5,447

Logbook - page -4 nrlTE : Mi4R . 24, f 98 3

LOG 110 .BAICFiB

ZDrrlFLcATICl1

GAS : s ![JRIT7 = > c19 , 4 cc1 H 2 By vi ritrsaoe

3-34 -a3 ESCSTV : r e 3 vN A s8AYPizR : FL oQ529 3

PESSSURE : r95 o prSs

O2• _ D N R S Ant 02 . rJ D < I pp.AW LYSIS RBQD85TSD : =Z = S s ND < t pp.

Ar = S Ar G DNA ppeSPECIAL: ao S ao Nn < 5 pp.

tS~ = S L _ 1A ppelrkt[ :n J tel C R2 =

4

S CsH2 : pp.Effects Leh . 2

SSYL SUPPLY LIRE = S = pp.

ALFA

BRAVOTR < I (pp.) Total Hydrocarbons as CSC

DELTA

COCA YOISTCBE _ . pp. B20 { < -$ > °P DEW lGIWT)

CTL #r3

C"TL #4

CTL # 5

TANE SO .

DELI VERY

TRAILER ~'r s Trs Oec = Less Than

OTHER > s Greeter Tb as1!.D. = Saar Detected

D .F.A . s Does *ot Apply

OOILID;NTS : *Maximum allowable limit per Yil Spec . 27201E for 02 + Ar is 1 ppm ; for acombined nitrogen, moisture std hydrocarbons is 9 ppm .

6 S F L &L A L I A` C i!T -~ •;

IIOI m u imi i iumm i im i ID 0 I 0I 0 IBNA0147638 5

HDMSE00624659

M. !toga


OEPT./GROU P

SSFL AXALYTIGL CK ISTRY UNI T

REFERENCE : Logbook ~3pg' i4 8

PHONE 5ii 7

DAT E

LOO NO .SAMPLE

IpENTIFiCATION RESULT S

Waatevater , Canoga

3 33-3 Site L, D/51►1► Serubber (hroaiua - 3(OO ' 5 /L .Sump 7

pg /. S

Grab Saaple taken

3 igfS3

i~R3Sired ,3f/$/$3

Anayysed for p8, andebroni ta

COMMENTS: The Bait for Site L is 75 ag/1.M . Mogg Notified by phone

APPROVED

r ~rrr 619-V

SSFL .ANALYTICAL C&I 1STRY UNIT

IIOI m u imi i iumm i im i


TO : !4• MoggDEPt./GROUP s ^

FROM : SSFL ANALYTICAL CH EM I STRY UNI T

REFERENCE : Logbook ' ~3 oa . '7 U

LOG NO

3-33g-g3

PHONE 4L7

DATE 3 /fig/S

LOG NO .SAMPI_H


3_ g_S Wastewater, Canoga Copper - 0. 12 g/L

Site C, "Sea World" Nickel - 3, d mg/ L

pH2h hr . Prcnortion .~ lS~' DLp ' k Pn

ample recived 3/if/ 3~d 3

alyzed for copper, pHnd nicke l

COMMENTS: The L.A . City discharge limit for copper is 15 mg/l, for nickel the limit is12 r .g/l .

AnaLyses per M . Mogg 's IL 81 F!-L22, 27 Oct . 198111 . 1) . • None detecte d

APPROVED AUSSFL ANALYTICAL C}{EISTRE' ']NL T

IIOI m u imi i iumm i im i ID ID D IBNA0147638 7

H D M S E00624661

To : M .. Mo


O T.JGROu' 564

rROA~ 9SlL A P(A LYTICAL 04. I3TRY U1RT

REFERENCE = Logbook ' g3 pg . 4g

LO3 NO .

3 -33 T7 -83

P*lOt~iE 5447

DATE 3

1.04 NO .SA MP1.E


3-337-83 Wastewater , Canoga Osromium = ~. 2 5 ►'Y15~(-

Site 8, 0/544 Process pH = T.Clarifier


sample

1

3 f 1 kjs ple received ,. qc)e 3


COMMENTS: The L .A . city discharge licit for chromium is 10 mg/LAnalyses per M . Mogg ' s IL Ni PE-422 , 27 Oct . 1981

APPROVED

I ., r Ai i19-V

SFL AML.rrIGL Q4L'i13TRY Ul4I T

IIOI m u imi i iumm i im i ID V DID D IBNA0147638 8

H D M S E00624662

; M, . ANA 5 * R . S CHM LJ .~ /5 4, F666

~.- LoG NO .. . P Ry )SS 1 1

CHEMICAL ANALYSIS 3- 333-83

To : C Wi JZER

REPORT To3 - 3 3S- 8 3

DEPT. /GROUP 03 / SS) Z

PHONE _ 7FROM : SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE : L O= 83 R?q t 9 O DATE / o - /~~R S 3

LOG NO .SAMPLE


WATER s.A 1 LE$ TR 1-HLOROETVLENE (TGE)

3-333 8 PP

3-339-83 R 2 6 ,I7p

3-335-93 A Z

RE 'D 18- 1AR- 3 3

DQR ► ~C, D ►scy~R(~ E

err PJi ITtE4rr,

W EAV'SF OWE .5

COMMENTS :

APPROVED

1 )r .r. F1Q-"

-

SSFL ASAL ICA L STRY UNI T


H D M S E00624663

LOG NO .


.7/M Wi'-5°"J

FROM= SSFL ANALYTICAL CHEMISTRY UNIT

DEPT./GROUP 55(r,

PHON E

REFERENCE : ~-OG ~mK ,,y 3 PIi G c '~ 9 DATE

LOG NO .SAMPLE


~-3~9'8~ l1Y1~KAvuCr- ~t1/Ij}lr'GG, F C/) r .2 /DD

,/ ,y/V °M RE ✓1/

A r+ 4-3 ~Y vacv'

fdR Fie,Eu/►/CON7 1VT lgER

R

s,*Mfb *I L ±

COMMENTS :

APPROVED

arm 619-V

A%f

II0I muim i iiu mmiiu u IDD I DI DI I I

cc :

3-3~8-83

To : Ii . Lr . YORE

SSFL ANALYTICAL Cfff~ISI'RYFROM :

REFERENCE : 'aa r- 4~

LOG NO•-

3-3 l 8-e

COMMENTS :

SAMPLE(DENT 1F 1CATION

LOx

ALFA I

FjrrY ONLY&J6. ZZyoo5TZsr # d0 c 1SAMPLER #

FL

® 3 -h') PSIG

RECEIVED :

3/17 /$~c L EO

DEPT./GROUP 599

LOG NO

5U47PHONE

DATE

RESULT S

Q9. S OIY~ BY VOL.U E

APPROVED / V ~ 1 ,

L BORATORY 4.C AR SStL Ar .Iytlc .I Ct ern tr y

/ F$

r

IIDI muim i iiu mmiium ium imu



FROM : SSFL ANALYTICAL C LISTBY

REFERENCE : LOGBOOE ''3 PAGE 1

3-3/7-83

DEPT. /GROUP D/556

PHONE 544 7

_____ DATE4 ./7,/t793


GAS : C Nz

RECD : 3 / /7 /S 3

SAMPLER : PL. 2 a 52 7 /"f7-,3

PRESSURE Z ODp 75/Cr N ~. G / (PPa) TOTAL HYDROCARBONS AS CE 4

ANALYSIS REQUBSTE )

C Th PIST E

{ SPECIAL : HYDROCARBONS

AS METHANE ONLY

FRO! f

SSFL SUPPLY LINETR = TRACE ND = M)NE DETECTED ( = LESS THA N

ALFA BRAVO2> = GREATER THAN DNA = DOES NOT APPLY

OOCA DELTA

CTL-3 TL-4

CTL-5 DELIVERY

TAN}; NO .

TRAILER

OTHER : $ 8 N - 1, G TL - 1

COMMENTS :

APPROVED

SSFL ANALYTICAL C}D!ISTRY U '

II0I m u imi i iumm i im i 11001 101 DI 1BNA01476392

I IH D M S E00624666


Qu4LITY ASSURANCE

FROM SSFL ANALYTICAL CSffi1ISTRY

REFERENCE : _ LOGBOOE g3 PAGE

DEPT./SROUP D/556

3 -3 / 6 - S'3

PHONE 5447

DATE M,4 . /7, / 9 S~3

SAMPLELOG NO. {DENT IF iCATION RESULTS

GAS : NEL/CIM

REC'D : 3 1/7 / 3

3-3/ ' 3 SAMPLER : 4oo .32 0

PRESSURE f 97S PS/4 /~. D . </ Dam ~PPo) TOTAL HYDROCARBONS AS CH 4

ANALYSIS RFQLTSTEL

CO !PLF E


AS IfETPANE ONLY

FRO :



COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TAN NO .

TRAILE R

OTHER : &&/1-/,c7?.. -J

COMMEPJTS .

APPROVEDE-CE ~ S S F L LYT I L CHD! I STRY LJN

II0I m u imi i iumm i im i 100 I 0 ID I 0 IBNA0147639 3

H D M S E00624667

cc : J . Becker 539 BA 7 1

TO :

FROM :

CHEMICAL ANALYSIS

REPORT

J . Rosengard


REFERENCE :Logbook '83, p. 48

LOG N O

PHONE 3293

DATE

3-314-83

3-315-83

3/23/83

LOG NO .SAMPLE


Stage 5 R2

3-314-83 31-propellant valve A colorless gel-like material was removed fro mfrom axial engine the oxidizer inlet of the bi-propellant valve .

The neutral pH material was heated to 107°C . for3-315-83 NTO line from axial one hour and experienced a 60% weight loss .

engine

A light-colored powdery material was removed fro mboth the valve oxidizer inlet and oxidizer lin eoutlet . Both residues were analyzed by atomic

Received : 3/15/83 absorption spectroscopy for the metals listed below .Results in percent by weight :

Metal Valve Residue Line Residue

Aluminum 29 29

Calcium 0.04 0.08

Chromium 0.03 0.06

Copper 0.05 0.02

Iron 0.10 0.24

Magnesium 0.07 0.18

Zinc 0.06 0.05

In addition, a black, rubber-like material was

obtained from the oxidizer inlet plate of th e

valve . The amount of sample was insufficien t

to generate a meaningful infrared spectrum .

The valve residue was found to contain 0 .35%

nitrate, while the line residue analyzed a t

2 .2% nitrate .

COMMENTS :

APPROVED

F orm 619-V

a,ui mac.,SSFL ANj&LITICAL ~HEMISTRT .UNIT

IIDI m u imi i iumm i im i IDD I DID 1 D IBNA01476394

539DEPT./GROUPEB 37

H D M S E00624668

iJJ J . Da n S I !• .G[ / O[ (, to 5 "7 3~Zb'd c) ,

•RT MO

9i___ 6 -E . dC .lCM ICMT01AE Aa WiriaL Lr OMt , T .U ITONEI

o -Evc _S2 -c t.Fit r V( 7. ITTY•UMT LCC JUMI 00100 ft. am .*CCl NO. WERE LITM rK S. Rw

TYPE

..ANN[D Y2

. . .,~Q -

,e A.: 1'EG

//-~o • !z

~J

ONT . MIME no, 4fTg11 iA qw

X913~TGT

" / l-/am a. .$S1 / REIT AEET.

_txR t .

*TV. P" tMff7lMA CL► "/ I tM

T1 COPT US ON TMR PART Ef T Op

SDooSR2 w r\1

JT MECM . MD/ CWR L .OC$ . UP C MO C .O .

UNIT OTY .

~ OEA

MG LTR -cc* Z

DPI NATION

MO

MATERIAL

OAT' .

OTT A CGL PT ED TOO L ' CAT MOit DATE MECM /L.DM

~Li1. 14 RTI OAT [ Iwf► .E~- U DWG SEW

I -MO M I L~I.E •TOTI[ EEO CURE ECMI O .

:RE9

a . ~

-1 1/s I.S L

i5,0 ORS 70 a 20

YER/FY//!cCD~P' O _7 IT- _ ~-

((~ SJ G ~iII~EC7 "/l ' ~.CD~~,.

N7Y 1 1 x ` )_ _ ~~

.572-D8~ + PRD EL'T .~ ✓I `l ;9

- - -: . DEL I ►~E/c T

_ Ti

o f 9 73 -, . . ; # M 44

r~Av 7-o s U /

-t-

~e ' ltrECT~IaE~ z, e~ -~

i_--L-

TLM!N IRn ~v 1t OClROOM MO [SSE S R[RIAL MO

aWN tCM /Lp~

fEEO MTC COOL'T

OAT [

BNA0147639 5

H D M S E00624669

R . Schmued ~,. D/56~, FB 66 W . Baisley, R . Knight , 0/598, SS 1 1

J . BowmaniFrancM .

M . CHEMICAL ANALYSISMo

F . B . LARY , D 1 596, SS 11 R E P O R TC . WINZER, D/031, SS 1 2

TO DEPT./ GROUP


REFERENCE : T .twhnnk 83 Pane ' 8

K . Johns, 0/031,SS 1 2

LOG N0 •

3-3iz- 8 3A All)

3-313-83

PHONE 5447

DATE 17-/-/AR-8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time-

3-312-83 PP / .time= /2 So p,1

3- 313-83 MOUNTA /N R VNOFF 1. SPP^'1time- /2 ss PM

time=

time=


3/17/ 8 3

DAY= THURSDAY_ EPA distillation method



APPROVED

Form 619-vMANAGER SSFL ANALYTICAL HEMISTRY UNI T

II0I m u imi i iumm i im i 100 I DID ID D IBNA0147639 6

HDMSE00624670



aura/Norma Fujika , ManagerSSFL Arnai,t I Chcrnutry

LOG NO

3- 3/C-4 3

DEPT./GROUP

PHONE S7'-7

DATE ~f _, _ __

RESULTS L y w~ • S t

L .~ CL = S. y z


IIDI muim i iiu mmiium iumiu uu


F:


L 1S ~ 3 - 'f

PITON E 5 / 13fr 7

DATE 3/F7/ 3

LOG NO .SAMPLE


3 -Soy- " N T o £ i . 4 f,~ oM ~~ - ~. `1 D ~• y F/ST[ 't f( j k? ofNTo

o A / ~ ► NrCy 5e 5f pa t

/(SAF,I•!a f N A~YMN/A.

cy

NSF: . AAALY CAL CHEMISTRY LT~I T

LOG NO

3-Soy-g 3

DEPT./GROUP y

IIDI muim i iiu mmiium iumuuu


TO M . 'or Dt/Gaj 564.

SSTL A NALY!ICAL OIDI 3 T1lY W(I T

RE RENCE : Logbook "3 pg •

PHOkE 5447

DATE

LO4 NO .SA MP'LE

IDENTI / ICATIOM RESULTS

3-30'7-33 Wastewater , Canoga Chromium = 0.07 '3 IL_Site B, D/544 Process PH = 7, 1Clarifier

GRp asample

3/i7/S'aa(()7' )

Sanple received 3 /i7

c~ U91 p


COMMENTS : The LA . city discharge Bait for chromium is 10 mg/LAnalyses per M . Mogg ' s it B1 FE-422, 27 Oct . 198 1

APP,OVED _ __S37L ANALYTtGL O4. 1STIT t3(1 f

arT sia-v

II0I m u imi i iumm i im i IDD I 0 I Di UBNAOI 47639 9

HDMSE00624673


DEPT./GROUP S~

PHOW E 5 r

DATE - u ~ i1c

LOG NO .SAMPLE


Siestevater , Csnoga3 - 3C&a3 Site L, DI5b Serubber c~roaium - 5(0 IJ

Sump pa- 77

Greb Sample taken

3/ :7/3 °c, D)LQ

Sample ReceiiedO~} ! D

Analyzed for pay andchroaiua

t'J53FL AMALrrLGL C.M. zsTBY UNI T

IIDI muimiiiummiiummim i iuiu

R . Schmue! ~, D/561+, FB 66 W . Baisley, R . Knight, 0/598, SS 1 1

J . Bowman

F irancM.z,CHEMICAL AN LYSI SAM . Moga/

F . B . LARY, 0 /596 , SS 11 R E P O R TC . WINZER, 0 / 031, SS 1 2

TO:


REFERENCE : i .nQhnnk 83 Pagel $

K . Johns, 0/031,SS 1 2

LOG N O

3- 309 - 8 3AP. J D

3- 305-8 3

DEPT./GROUP

PHONE 5447

____ DATE __ 8 3

LOG NO.SAMPLE



BELL CANYO N

time=

3-3o4-83 1fOV PJT4/^1 R VNOFF I . SP,P,n-~

time=_________

3-3o5-83 PP /. 2 pp vi

time 8'°,4H

time=

time=


3/ /7 / 83

DAY= THURSDAY EPA distillation method

COMMENTS: The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVED

Form 619-v


IIOI m u imi i iumm i im i uui 0 I DBNA01476401

UHDMSE00624675


TO : QUALITY ASSURANCE

FROM : SSPL ANALYTICAL C13mEI5TRY

REFERENCE : LCIGB X ~3 PAGE '4 $'

DEPT. /SROUP D/556

LOG NO .

3-302-63

PHONE 5447

3DATE ,7,/qt

LOO NO . IDENTIFICATtON RESULTS

GAS : M5L/UM

R.C' D : 3 / 14' /(3

3 3i2Z- 3 SAMPLER : FLO/OZ K'

PRESSURE 2 DOO P5/C- N ~/ (pp.) TOTAL HYDROCARBONS AS CR4

AN LVSIS RLTSTED

CXNM! PLiEI' E


AS 1[SPHANE ONLY

FROS! :

j SSFL SUPPLY LINETR =TRACE ND = l~C)NE DETECTED t; = LESS TfiA K


QOGa DELT A

CTL-3 CTL-4

CTL-5 DELIVERY

TAKE NO .

T R4I LSF

OTHER : S 5 P-/ , AREA - J

COMMENTS .

APPROVED~. N. Q.

SSFL A LYTICA CHEWISTRY US' '

II0I m u imi i iumm i im i uui 010 0BNA01476402

UH D M S E00624676

LOG NO .


QUALITY ASSURANCE o€p7 ,,aROup D

Fes: SSFL ANALYTICAL CS~CISmY

REFERENCE : LOGBOOK B3 AAGH q g

3-3°/-83

PHONE 5447

DATE MA ./7 , 1 3

SAMPLELOG NO • IDENTIFICATION RESULTS

GAS : (.i N2

RECD : 3 // ' /S'3

3-3o/ "B3SAMPLER : FG aa5y8'9

PRESSURE / 9 5a P5/( N • D. < f (pp. ) TOTAL HYDROCARBONS AS C8 4

ArALYSIS REQ ESTID

COMPLETE

SPECIAL : EYDROCARBONS

AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE ND = Ii )NE DETECTED C = LESS TAN

ALFA BRAVO > = GREATER THAN DNA = DOES NOf APPLY

COCA DELTA

CTL-3 CTL- 4

Ci L- 5 DELIVERY

TANK N0 .

TRAILER

OTI.O;R : SS P-3, 4 A2

COMMENTS :

APPROVED

II0I m u imi i iumm i im i uu iBNAOI 47640 3

4

SSFL A LYTIGL CHD .̀ISTRY UN F

HDMSE00624677


LOG NO .

3 -3cc 3

Pf4ONE __

DATE :_L

■

LOG NO .SAMPL E


westeveter, Canoge

-3cO - s3 Site L, D/5k1 ► CRRiF,~a c roai - N. f . ~~.05 ✓NS~L- 7 9Grab Sap1e taken

3//t, 83

~,, 04 0

Sample Received)C33

AEIIy7ed for pH, andchraaiiua

3F

IIDI muim i iiu mmiiu mmim i imui


Tp; M . Moog DEPT./GROU P

SSFL ANALYTICAL (i{»iISTRY UNITPRONE __

DATE ~1Ia~~S -

LOG NO .SAMPLI


~2 ~53Waetevater, Canoga

Site L, D/5ik Scrubber (~roniua S/4 ,i5/LSup p5 7. 8Gra takenk

b~33 /

C?~~o

Analyzed for pH, andchrott t

AlL3SFL ANALYTICAL Gi1~lISTRY UNI T

IIDI muim i iiu mmiiu mmiu uim i


LOG N O

3-298-83TO: uO¢g DEPT/GROUP


REFERENCE : Logbook p&. £ L

PHONE 5l 7

DATE 3/i/ 3

LOG NO .SAMPLE


32s3 Wastewater, Canoga Copper N.1~ .~D .QSg/ L

Site C, "Sea ~or1d" Nickel - 1. 5 ^~g/L

QpN u .

2'I ~, .. PQ, 14SAwm pt.

preceived 3/1h/83

(E933nalyzed for copper, p8nd nicke l

COMMENTS : The L .A . City discharge Limit for copper is 15 mg/I, for nickel the Limit is12 mg/l .

Analyses per M . Mogg's IL 81 FE-y22, 27 Oct . L981N .D. - None detecte d

APPROVED

farm 619-V

53FL ANALYTICAL CHEMISTRY UNI T

IIOI m u imi i iumm i im i uu iBNA0147640 6

HDMSE00624680

, LOq MO .

r CHEMICAL ANALYSIS _REPORT 3 ~9 7-~ ~

OEtT.,O+40NP 564.

lallOlr~ SSPL AMLYT2GiL O 4.lOtt3T*T UT?

1l1:fERENCE : Logbook ' g3 pg . Y~

PtIONE 5447

DATE G

LOG NO .SAMPL E

tDENTiFICAT1ON RES~ILTS

3&.?? 83 Raste.ster, Canoga Chromium = O. /3Site B, D/544 Process pH = 7 .2Clarifier


1

mple received 3/I/3

r~33Analyzed for pH, and

chromium

GOMMEMTS: The L.A . city discharge lilt for chromium is 10 rng .IL

Analyses per M . Mogg'a/IL 81 PE-422, 27 Oct . 198 1

APP,OVED ,

Harm 61St-V

GtwavSUL AIiAL1 7IGL QLDl.L3Tll7 111Ir

IIOI m u imi i iumm i im i uu iBNAOI 476407


R, Schmuec ~, D!564, FB 66 W.3alsLey , R. Knight, D/598, SS 1 1

J . Bowma n

n C HEMI CAL ANALYSISM . Mog

REPORTC . WINZER, 0/031, SS 1 2

TO' DEPT./GROUP


REFERENCE : Lncrhnnk g3 ~a9e 9

K . Johns, / :31 ,SS 1 2

LOG NO .

3- 295 -8 3/~ N p

3-296-8 3

PHONE 5447

DATE / c-MAR-e 3

LOG NO .SAMPL E



FLUORIDE ANALYSI S

BELL CANYON

time =

3-295-e3 R I 3. 6 ~' ► `~'

time _____

3-296-83 Mou JrA!N RuJOFSC / . 3 Ppr-1

it me=

time=

time=


and analyzed ASAP

3//6/83____DAY= VtJEDtJESOA' _ EPA distillation metho d



APPROVED

Form 619-v

SSFL ANALYTICAL CHEMISTRY U1 I T

IIDI m u imi i iumm i im i uui V D IBNA01476408

I IH D M S E00624682


TO:

FROM :

1, .j ILSO N


REFERENCE :, L 'a3 p41

LOG NO .

3 -Zq4-8 3

DEPT./ GROUP SS (p

PHONE 5441

DATE MAR . 1 6 195 3

LOG NO .SAMPLE


34.33 I-(' ( A UL, C O I L

Ntl - H- 83282J REo 4 TF (c F C CF3(Q)_ PP ...'

FROM f $€RvasR (3'1 voIUH E

11 A- 3REF . R L reot 2

f-OR FRFo 's C .oNTSNT

RE C'D

16 MAR . Iq83

COMMENTS :

APPROVED ___IL_L

F orm 619-V

4 C . Y -

SSFL ANALYTICAL Q1El1STRY UNI T

IIDI m u imi i iumm i im i uui I D IBNA01476409

UHDMSE00624683


LOG NO .

DEPT./GROUP y Q

PHONE S~

DATE _.T/l3

LOG NO.SAMPLE

IOENTIFICATION RESULTS

-2)- Y N To s~ ~.y4 f. .,► ,N V K = 1I f NT OQy/

57(-4- ce/! xgh.•

fok N V .

31 ► ~/~3

SSFL AM ICAL CHEMISTRY UNIT

IIDI m u imi i iumm iiumumm u i


TO: M oof

PRo 9SFL AIIALYTI CA L QLE!(ISTAY U (1 T

RE~EREp& : _ Logbook "3 pg • '.(0

3_z~ ZDiPT.~O~lOIJr 564

PHONE 5447

DATE ,. 3/4S/'31

LOO NO.SAMPLE

tDENT1fICAT1ON RESULTS

3 -~92- Fs3Wastewater , Canoga faromium = O,0 ,`.

Site 8, D/544 Process pB =

Clarifier

Grz e 3/i5) 3sample °C $ 2.0

f

Sarple received

~. ► 30a

Analyzed for pa, an d

chromium

COMMENTS : The L .A . city discharge licit for chro'niun is 10 mg/L

Analyses per 1 4 . Mogg ' 3,IL 81 FE-422, 27 Oct . 198 1

SIT s»-v

r

591L AMALYTI L Ocn l$T~Y UIIT

IIDI m u imi i iumm i im iB NA0147641 I

UHDMSE00624685

R . Schnued D/564, FB 66 W . Sais 'ey, R . Knight, 0/598, SS 1 1

J . Borma n

M . Mogn CHEMICAL ANALYSIS

F . B . LARY, 0/596, SS it R E P O RTC . WINZER, 0 /031, SS 1 2

TO DEPT/GROU P

FROM: SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE : T .nuhn k ~3 Pa €. 4 6

K . Johns, 0/031,SS 1 2

LOG NO .

3-2R1-8 3

PHONE 5__

DATE

SAMPLELOG NO , IDENTIFICATION RESULTS

PPM FLUORIDE, BY ELECTROD EWATER SAMPLES FO RFLUORIDE ANALYSIS

I291-83 BELL CANYON 0. 8 ~~rh

time=

time=

time=

time=

time=


and analyzed ASA P

3/ /S/ 8 3

DAY= TU E3DAY EPA distillation metho d



APPROVED

Form 619-V


II0I m u imi i iumm i im i ID ID D ID DD I IB NA0147641 2

H D M S E00624686

CHEMICAL ANALYSIS

REPORT

TO EQUIP! N LAS

FROM : SSF'L-ANALYTICAL CHII4ISTRY

REFERENCE : LB-S3 P.' L('

LOG NO

3 -,Z 89 -~ 3To

DEPT./GROUP 598-3Ia

PHONE 5b47

DATE MAR ' /, . 1963

LOG NO .SAMPLE

IDENTIFICATION4, 3 mgRESULTS -

TRICK for NVR per

RL10001-F

3z~B3EWR No . ,137Z22 _

BLA+'C mg/500 ml

xA.tts^,v:t~; O,7 /500m].

GL a SH oC G-45,tC7

E'WR No .

BLANK mg/500 ml

HA,ItDW • mg/

EwR No .

BLANK mg/504

WAF.E • mg/500 m1

COMMENTS :

APPROVED

Recd .

~GT o or•'~

SL Anal Ical C emistry

IIDI m u imi i iumm i im i V ID ID D I IB NA0147641 3

HDMSE00624687

ENGINEERING WORK REQUES TTITLE OF JOB I DATE

I, No R 437222INSPECTION REQUIRED

APPLICABLE DRAWINGS (ATTACH IF REQUIREDI REQUESTED COMPLETION DATE

YES NO

DOING DEPT . LEDGER ACCOUNT GENERAL ORDER G .O . ITEM 11 MCR INIT . GROUP NDW . OR TASK DOING GROUP ACTUAL COMPLETION DATE

C- -2

CPREQUESTED BY EXT . FACILITY S}IIFI' REQ . SUPERVISION ESTIMATORESTIMAT E

-~. -.L

IHOURS MATERIALS

- _ _-_ REQUIRED REQUIREDLAB SUPERVISION

ASSIGNED TO1LEADMAN MECHANI C

SHOP I LAS

INSTRUCTIONS ( BE SPECIFIC) NOTE : THIS FORM WILL BE USED FOR NON - DELIVERABLE ARTICLES ONLY .

C L C7i'a /1! I rL (,t lw

DC -, zz~:' - ~-'-' ' &)V IZ, ~' fL RL ti QoO< <7~= (mil

J~ ,-3 - 1 Pik L ~~. 43722' _

&_c i (~-~,1 (_R JC12.-1 rc r,., vG £ L s v L-r 3I4 ! QL a ny )t„_

A-, L ` /1,

3- - T-'3

RECEIVED 0 LAB

MAR 14 198 3- f/ /1H,

BY L ANALYTICAL CC MI TRY


LIST OFMATERIAL S

B NA0147641 4

HDMSE00624688


M . Mogg DEPT./GROI~P _

FROM: SSFL AMALYTIGL CH® tISTBT UNI T

REFERENCE : Lflgbook 'p . `7 l0

fLOG NO •

3-Z88-8 3

PtHCN E __

GATE

LOG NO .SAMPLE


3_Z8~Waeteveter, Canoga

8 Site L, D/5 Serubber Chromium - 4/ 4!6 rh g /LSup pH

•Grab Sample taken

3/i 5/83

iced 3/'5/8e

S

0 d for pH, andchrrAiut

COMMENTS : The limit for Sit. L to 75!4 . Mogg Pfotified by phone

APPROVED

SSFL ANALYTICAL c iiraY LNL T

II0I muim i iiu mmiiu m mi mim i

REFERENCE :Lagboak 3p$

. ` ID DATE iLOO NO .

SAMPLEIDENTIFICATION RESULT S

3-87

-g3rtewater , Canog a

site L, D/5 Scrubber c~rao<isa - 7QQ I1 /L_Smp p1 - 7 3

,Crab Sn~p1e taken

3)I 3JD

3l6k~ 4 g

nAnai. zed for pif, aridchromiua

COMMENTS : The ].trait for 31te L is 75 r *Ji.M . Mogg ! tified by phone

FL ANALYTI CA L CHE>tIISTAY U?II T

IIDI m u imi i iumm i iumummmu


TO~

FROM

M . Ko3g

SSFL ANALYTICAL CSEMISTRY UI4I T

REFERENCE Loghook ' 3 rR . L) ~p

LOG NO

-3-Z8(-8 3

DEPT./GROUP ^

PHONE ShL1

DATE _ ____

LOG IVO •SAMPLE


3-286-83 Wastewater , Canoga copper - 0. / / rng/L

Site C, "Sea WorLd" Rickel • /, y 'ng/L

8 ' 224 hr. Proportional .SAô1P tpke n

amp Le rece ived 3/► S/'43

0948alyzed for copper, pl i

ad nickel

COMMENTS : The L .A . City discharge Limit for copper is L5 mg/1, or nickel the limit is

L2 -g/l .AnaLyes per M. Xogg ' s 11/81 FL-L22, 27 Oct . L981

N . D. - None detecte d

APPROVED

ern. 619-V

,v rSSFL ANALYTICAL Q ISTRY UNIT

IIOI m u imi i iumm i im i 0 ID I I IB NA0147641 7

HDMSE00624691

To: . M oc e

fRO~


DEFT./ GROIJJ• 564

SSTL ANALYTI CA L CHEltI3TAT LNY T

REPERSNCE = Logbook t'S3 pg • i..L (p

3-285 83

P lOP4e 544 7

DATA ________

LOG NO .SAMPLE

Ioci4TIFiCATIOW RESULT S

'2gS 1Yastevater , Canoga Chroxium = O . 5 3 (>'1 /L...Site B, 1)/544 Process pB = / !Clarifier


sample

1

Saaple received

~S


chromium

CGMMEMS: The L .A . city discharge halt for chromium is 10 mg/L

Aaalyses per M . Mogg ' s I). 81 FE-422, 27 Oct . 1981

APP~eCVEO ,531L ANALYTICAL Qt 13T*Y tI?!I T


UH D M S E00624692

LOG NOD . 556cc :3 -2&'-&3CHEMICAL ANALYSI S

REPORT

DEPT./GROUP 543-31

To

PHONE 5~7

DATEM4R. / I '

LOG NO .SAMPLE

IDENTIFICATIONt m gRESULTS 0 . 3

TRICH for NVR per

RL10001-F

ENR No . 4 3 72 / 5

ELANK mg/500 ml

xARDFIp .°,~' 0 .5 m/500 ml

Fc d5N c F 3 Hoses

EWR No .

BLANK mg/500 ml

xaRnw ma/5

EXR No .

ffi~ANK mg/5

WARE a mg/500 m1

Rec'd . __ f~3

SSF L Ar 1Iytlcal Chemistry

IIDI m u imi i iumm iiumummiu


APPLICABLE DRAWINGS (ATTACH IF REQUIRED IINSPECTION REQUIRED I

YES I NO

DOING DEPT I LEDGER ACCOUN T

IREQUESTED BY EXT

LAB SUPERVISION

GENERAL ORDE R

FACILIT Y

ASSIGNED TO :

G .O . ITEM S MCR I INIT . GROUP HOW

DATE

OR TASK I DOING GROU P

SHIF T

SHOP I i LAS I

REQ. SUPERVISION ESTIMATO R

LEA DM AN I MECHANIC

No.R 43721 5REQUESTED COMPLETION DATE


ESTIMATE

HOURS I MATERIALSREQUIRED ~ REQ UI RED

INSTRUCTIONS ( BE SPECIFIC) NOTE' THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

C;L.~, rn `

1*

-7 -/ ` -83

1 . 1

Lc-# 3-zFJ-T 3

I -v , ma _ ae,

LIS- OF MATERIAL S

BNA0147642 0

RECEIVED @ LAB

MAR 19198 3

SS FL ANALY" CHEMISTRY

H D M S E00624694


L1 83- y-G

LOGNO-

3_ IY3- ts 3

DEPT./GROUP 5 9 Q

PHONE 5-/If 7

DATE 3 11 / 7 0

LOG NO .SAMPLE


NtO 5,, A-ttlle fa 'k F-F -f J . i A g {

se's & OAA1 A0 PJ AAt ~~ey of Nrn

f ^ y

STL -4- ce(l 24 L

-~ c

3~rc) 3

A/f.'v orma FL' llh a Manaye- S~FL A':AL.1IGAL CHt:N.1- F\ J ;T


M, Francis D/541, 1312M . Mogg D/541, 131 2

TO ROCKETDYNE PLANT SERVICES



DEPT./ GROUP D/031

REFERENCE : LOG BK ' S3 PAGE 9 NOTEBOOK -"

LOG N O

3- 28C- g3

PHONE 5447

DATE/J-/ 14, -g 5

LOG NO .SAMPI..E



3-28 0-8 3 PP retention pond at proved under the guidelines stated in the currentRocketdyne . SSFL NPD85 permit, the following VOLATILE ORGANIC

CC6(POUNDS were found :Freeboard = ft

Sampled @ 2rf

?tlAcetone (CH3COCH3)

-30O

Bromodichloromethane (BrcBC12) _ N~G f _

B L C o I /iCarbon Tetrachloride (CC14) = ND<

y : . r,Sq

Chloroform (CHC13) = (

RECEIVED @ LAB : -TDMethylene Chloride (CH2C12) = //< <

3 / /1 / `3 l,l,l--Trichloroethane (CE3CC13) = /VQ< /

Trichloroethylene (C1CH :CC12) _Notation about appear-ance of the sample : Tetrachloroethylene* (C12C :CC12)

1,2-Dichloroethylene (C1CFi :CHC1) =

Dibromochloromethane (C1CHBr2) = N D L I

Isopropyl Alcohol ; also (CE3Qi0HCE3) = 4300known as IPA ; 2-propanol

Freon TI (C12FCCF2C1) = ~< /

1,1-Dichloroethane (C12CH (S3) = 53OOQiL1TS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifical•ly required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES CA0001309 fromthe California Regional Water Quality Control Board, Los Angeles Region . (2) per (1) "wastes

discharged shall not contain phenols , mercaptans , or other substances in concentrations which

would impart taste, color , odors, foaming or other objectionable characteristics to receiving

waters . . .`, "or any substance in concentrations toxic to human, animal , plant, or fish life . "

PPB = PARTS PER BILLION= LESS THAN YD = DRONE DETECTED DNA = DOES DCT APPLY TR = TRACE

f- t. res~i~s t'vcnsn,~f4e~ j-, C . WiMrxr aNJ H . I-tob6 3//5/93•

APPROVED

f arm 619-V

SSFL ANAL ICAL~• ISTRY UYI T

IIoI m u imi i iumm i im i 10010010 I IBNA0147642 2

H D M S E00624696

R . Schmued . D/56 FB E 6 W . Baisley , R . Knight, D / 596, SS 1 1

J . BowmaniF s,rancM .

CHEMICAL ANALYSI SM . Moga

F . B . LARY , D/596, s 5 11 R E P O I TC . WINZER., D/031, SS 1 2

TO :


REFERENCE : T .nuhc r k 33 ~a9c 46

K . Johns, D/031,SS 1 2

LOG NO

3-27~-8 3

DEPT./ GROUP

PHONE 5__

DATE /5-H//-'3

LOG NO .SAMPLE



BELL CANYO N

time=

*3- 279-83 PP ri1 0 pp.time= 2 '5 Pr!

time=

time=

time=


and analyzed ASA P

3i 14 /s 3

DAY= M N ~Y EPA distillation metho d



PER!M IER POND/ K>ATdS iROM TAE ppop TF2Ty FoLLow/ N

,OO771cAPPROVED

Form 619-V

031 ~ L 5€D -rrF

SSFL A LYTICAL CHEMISTRY UNI T

II0I m u imi i iumm i im i 100101000 I IBNA0147642 3

HDMSE00624697

< < s no s! ti ~„~,~~ /c- i« e 3

LOG NO .

CHEMICAL ANALYSI S

REPORT ~' $ &

To: F 1A I O 7 .


REFERENCE tiS 83- wL

DEPT. /GROUP S9 $

PHONE ~ r _ 7

DATE

LOG NO .SAMPLE


3- 274-43 NT a 'A i' r fa a 1/ k NTO

STL -

c r (t 2' IS K u,u

. (5 9 A ///Pd'1AN k

`

cyLr w s/ew )

(, I

COMMENTS :

APPROVED ~t,i' LAf,,aAA,z '

Form 614-v

Norma Fajihawa, anagerSSFL Anahihcat hem Lc Ma

SSFL ANAL ICAL CHEMISTRY UNI T

II0I m u imi i iumm i im i 10010010 I IB NA01476424

HDMSE00624698

F . Schmued . 0/56+, F5 66 W . Baisley , R . Knight, 0 / 598, SS 1 1

J . Bowman

iF srancM .CHEMICAL ANALYSI SM . MogQ/

F . B . LAP.?, D1 596, 5 5 11 I E P O RTC . WINZER, 0 /031, 5 5 12

K . Johns, 0/031,SS 1 2

LOG N O

3- Z 75 -83T O

3- Z77 -83

IMF

■

TO: DEPT. /GROUP


REFERENCE : T .nahnnk Pa t 46

PHONE 5__

DATE /4-M--8 3

LOG NO .SAMPLE


WATER SAMPLES FORPPM FLUORIDE , BY ELECTRODE

FLUORIDE ANALYSI S

BELL CANYO N

time=

3-275-83 PP . NORr i to f'P~-►time= /°//1

3-276-83,D1 SO)T,/ /. O~°f'r` i

time /O°/2M

3-217-93 pp, wesr /0 Apr-,

time=

time=


and analyzed ASAP

3/Ll/8 3

DAY=________________ ► = EPA distillation method



APPROVED

Form 619-V

SSFL ANALYTI(ÀL CHEMISTRY UNI T


I IHDMSE00624699

R . Schmued .. D/561', FB 66 W . Baisley, R . Knight , D/598, SS 1 1

J . B owrna ni

M .Franc

` CHEMICAL ANALYSIS

F . B . LARY, b/ 596 , 55 11 R E PORTC . VINZER, 0 / 031, SS 12

K. Johns, 0/031, f1FSS 1 2

LOG NO •

3-V72-8 3APD

3-z7 3 -s3

TO: DEPT :/GROUP


REFERENCE : T .nv ii n1 83 Pate q6

PHONE 5447

DATE 14 - MA_-8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

3- 273 -83 BELL CANYON Q.' p1,m A O. 4ppmtime=

3-272-83 MOJNTAUJ RvaoFF/ . /

I

pv,l

time 1r__ _

time=

time=

time=


3//q / 8 3

DAY = h OrJ DAY s* EPA distillation method



APPROVED

Farm E'Q-V


II0I m u imi i iumm i im i 1001001 IBNA01476426

I IHDMSE00624700

cc : ;i 61-41 s '34 -IfC CS 27

LOG NO .

TO :

FROM

CHEMICAL ANALYSIS

REPORT

F. p . fo fq


REFERENCE : Gg f3 - w6

PHONE !9'/ It 7

DATE 3 r33

LOG NO .SAMPLE


3 - 2 71- 83 N TO SA * i. 4 f o KIc

_ o6 2 ^^ ~ F

Ir

,'AoN {AGAR s Tl -5~ 9 of N rokC .c fl 2'I$ x VAi

Tor k ( (A. ,.y lard

I'A/ A [ ✓ M 1'044, AA

ywclfA.

-''~`f 4 3

COMMENTS :

APPROVED /t/fZ&4~ -

rorm619-V

Normc Fujik )a, ManagerSSFL Analyt I Chernistry

B NA0147642 7

3- 27 1 - 8 3

DEPT./GROUP £ 2 1

SSFL ANA 1"TICAL CHEMISTRY UNIT

i uHDMSE00624701

cc : P . Kleinsmith D/768, T040R . Schrnued D/541, FB12M . Francis D/541, FB12M . Mogg D/541, FB12


FROM : SSFL ANALYTICAL CHMISTRY


DEPT/GROUP D/031

REFERENCE : LOG BIC ' 93 PAGE 44 NOTEBOOK -

LOG N O

3- 26q-e 3

PHONE 5447

DATE /5-M4'-83

LOG NO . iDENTiFICATION PURGE & TRAP lO GC/1s RESULTS (PPB )

Water sample from the Using the concentration techniques and methods ap-AI Inlet to the R2 proved under the guidelines stated in the currentretention pond at SSFL NPDES permit, the following VOLATILE ORGANICRocketdyne . COMPOUNDS were found :

Acetone (CH3000H3) = 1 ZSampled E ____/__ Bromodichloromethane (BrCHC12) = 37

311-11-63 Carbon Tetrachloride (CC14) _ )

'By: LL . Co //j ? S

^̂Chloroform (CHC13) = J 8Methylene Chloride (CH2C12) N,041I

RECEIVED @ LAB :

1 1 1-T h li h YR'3/,W /83

, , r c oroet ane (CH3CC13) _ 1.Trichloroethylene (C1CH :CC12) = S

Notation about appear- Tetrachloroethylene* (C12C•CC12) = ND <ante of the sample :

1,2-Dichloroethylene (C1CH :CHC1) _ L <

qDi.bromochloromethane (C1CHBr2) = / /

Isopropyl Alcohol ; also (CH3CHOHCH3) = NQ <known as IPA ; 2-propanol

Freon TF (C12FCCF C1) _2

1,1-Dichloroethane (C12CHCH3) = ND<

COMMENTS : * Tetrachioroethylene is also known as perchloroethylene . ( 1) Monitoring specifical-ly required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES # CA0001309 from

the California Regional Water Quality Control Board, Los Angeles Region . ( 2) per (1) "Wastes

discharged shall not contain phenols , mercaptans , or other substances in concentrations which

would impart taste, color, odors , foaming or other objectionable characteristics to receiving


PPS = PARTS PER BILLION


Hi k ees ,~ !-&s frsH,i••,,ifet }'a C . W,nt - dnal M HaG(, 3/, /P3 .

APPROVED / / • "` ~~

f arm 619-V

&a~SSFL ANAL 'ICAL CHEMISTRY UNIT

I IBNA0147642 8

HDMSE00624702



M . Hogg 0/541, FB12



DEPT./GROUP D/03 1

REFERENCE : LOG BK ' S3 PAGE '16 NOTEBOOK -

PHONE 5447

DATE

LOG NOSAMPLE

PURGE & TRAP © GC/MS RESULTS (PPB. IDENTIFICATION )


3-268-83 R2 retention pond at proved under the guidelines stated in the currentRocketdyne . SSFL NPDES permit, the following VOLATILE ORGANIC

COMPOUNDS were found :Freeboard = -'-- ft

z 8S d @l 9 °pAfrf

Acetone ( CH3COCH3) =amp e

383/Bromodichloromethane (BrCf1C12) = N~ r _

/ - 9~o //":,7By : L . C ~

Carbon Tetrachloride (CC14) = 0~ t

Chloroform (CBC1 ) _RECEIVED @ LAB :

3

3 / ! Q $ 3

/

Methylene Chloride (CH2C12)

1,1,1-Trichloroethane (CH3CC13) = NO < f

Notation about appear- Trichloroethylene (C1CH :CC12) = I (ance of the sample :

AID < j*Tetrachloroethylene (C12C :CC12) =

1,2-Dichioroethylene (ClCH :CHC1) = 2 2.

Dibromochloromethane (CICRSr2) = ND < I

Isopropyl Alcohol ; also (CH3CHOHCS3) = /I


/Freon TF (C12FCCF2C1) _ /VV

1,1-Dichloroethane (C12CHCE3) = N1) <

COti0ENTS : * Tetrachloroethylene is also known as perchloroethylene . ( 1) Monitoring specificall

required according to the Rocketdyne NPDES permit , Order T 76-146, NPDES # CA0001309 from theCalifornia Regional Water Quality Control Board , Los Angeles Region . ( 2) per ( 1) "Wastes dis-

charged shall not contain phenols , mercaptans , or other substances in concentrations whichwould impart taste , color , odors, foaming or other objectionable characteristics to receivingwaters . . . ", "or any substance in concentrations toxic to human , animal, plant , or fish life . "


= NONE DETECTED DNA = DOES NOT APPLY TR = TRACE= LESS THAN ND~i

H igk rejvl+s 4YdnS ,,+ ~Ti4 fO . W ihzcr QNd H. nab& 311Wf3 .

APPROVED NZ

LOG NO .

3 -269 -8 3

SSFL ANA ICAL CAMdSTRY UNI T

BNA0147642 9

CHEMICALANALYSI S

REPORT

HDMSE00624703

EF FLU ENT DISCHARGE REPO RT

CAEEST C AL AN AL YS I S RESULT S

TO : INDUSTRIAL ENGINEERING D/031 SS12

3-266-8 3

DATE : 22-Mar-8 3

FROM : SSFL ANALYTICAL CHEMISTRY D/539 SS11 PHONE : 544 7

REFERENCE : LOG BK '83 PAGE 46

SAMPLED FROM : AI inlet to R2 @ 8 :45 AM AM/Phi ON : 14-Mar-83

CONSTITUENTRESULTS

/1CONCENTRATIONIM IT mg/1

pH at 25 ° C 7 .6 pH limit to units

Total Dissolved Solids on Drying at 180 ° C 677 950Temperature of Water 14 .4 37.8 ° C

Chloride 111 150

Suspended Solids < 5 150

Settleable Solids < 0 .1 ml/1 0 .3 ml/1

BCD at 20 ° C 60

Grease and Oil 1 15

Residual Chlorine 26 .7 0 . 1

Surfactants as MBAS < 0 .01 0 . 5Sulfate 178 300


Fluoride 0.4 1. 0

Boron 0 .3 1 . 0

Turbidity 2 (5 )

Phenols < 0 .001 (4 )

Mercaptans 0 .8 (4 )

Cyanide 0 .001


(2) Filt.ere,1 with Whatman GF/C paper and dried at 103° to 1050 C .

(3) Limitation not required to be mrt during rainfall .

(4) Wastes discharged shall not contain phenols, mercaptans, or other substances ir,

concentrations which would impart taste, color, odors, loanung or other object-

ionable characteristics to receiving waters . . .or any substance in concentration :

toxic to human, animal , plant or fish life .

(5) Wastes discharged shall not increase the natural turbidity of the receiving

waters at the time of dis9harge .

Approved :

SSFL, AN,^1, TiC A1 . ClI .111]TRY 1'NT T

BNA0147643 0

HDMSE00624704


(5 )

APPROVED

Form 619-VEA SSFL A LY':ICAL ISTRY U N

BNA0147643 1


LOG NO-

3-261-8 3to

3-265-83

DEPT./GFCUP 031

F4 : SSTL nNAM CA, MMISTRY . DEFT. 5 n9 P3DNE 5447

LB-83 -y . 46 DATE: 22-Mar-83,

SAMPIZ 1101M ICATION: SAMPIZ FR~4 ~ R2 A 9 . 00 AM ON 14-Mar-83

TO Industrial Encrineerinn

00N5Tri'fJENT RESULTS/1

CONCENTRATIONLIKIT /1

pH at 25 ' C 7 .7 pH =Its to units

Total Dissolved Solids on Drying at 180' C 358 950

Temperature of Water 14 .8 378 CChloride 30 150


Settleable Solids 0 .4 ml/l 0.3 ml/1

BOD at 20' C 4 60

Grease and Oil 2 15

Residual Chlorine < 0 .04 0 .1

Surfactants as MBAS 0 .01 0.5

Sulfate 92 300


Fluoride 0 .4 1 . 0

Boron 0 .2 1.0

Turbidity 11 (5)

Sewage Treatment Plant Influent BOD at 20 C 510 (4 )


Sewage Treatment Plant Influent Suspended Solids 1316 (4 )


Filtered with Whatman GF/C paper .

Filtered with Whatman GF/C paper and dried at 103°to 105° C.


The average final effluent concentrations shall not exceed 15% by weight ofthe average sewage treatment plant influent concentrations of BOD5 20'C andsuspended solids during periods of discharge .

Wastes discharged shall not increase the natural turbidity of the receivingwaters at the time of scharge .

lll .t _

MANAG

HDMSE00624705


CHEM ICAL ANALYSIS RESULTS3-258-83

to

3-260-83

I

TO : Industrial Engineering - DEPT./GNOUP 031

T 1 : SSFL ANALYTICAL CfIA{IS*TRY_ M'? r . 539 PM _W47LB- 83 -p . 46 DATE :_ 22-Mar-84

SAMPLE ZDEta'TI>'ICATION : SAMPIE FROM PP 0 9:15 An ON 14-Mar-8 3

(5 )

APPROVED

Form 619-VSSFL ANALY T ICAL EMISTRY UN !

BNA0147643 2

CONSZ'IT[lENT RESULTS/1

CONCENTRATIONLIMIT /1

pH at 250 C 7 .7 pH unit to unit s

Total Dissolved Solids on Drying at 180' C 238 950

Temperature of Water 13 .0 37.8' C

Chloride 24 150


Settleable Solids <o .1 el/l 0.3 m1/1

BOD at 20' C 25 60

Grease and Oil ( 1 15

Residual Chlorine < 0 .04 0.1

Surfactants as MBAS 0 .01 0.5

Sulfate 56 300

Total Cnromium 0 .002 0 .01

Fluoride 0 .8 1. 0

Boron < 0 .2 1. 0

Turbidity 3 (5 )

Sewage Treatment Plant Influent BOD at 20 ' C 177 ( 4)

Sewage Treatment Plant Effluent BOD at 20' C 2 (4 )

Sewage Treatment Plant Influent Suspended Solids 1870 (4 )


Filtered with Whatmen GF/C paper .

Filtered with Whatman GF/ C paper and dried at 103°to 105° C .

Limitation not required to be met during rainfall.

The average final effluent concentrations shall not exceed 15 % by weight ofthe average sewage treatment plant influent concentrations of H0D5 20'C andsuspended solids during periods of discharge .

Wastes discharged shall not increase the natural turbidity of the receivingwaters at the time of discharge .

NJ

HDMSE00624706


TO : M. 4ogg DEPT./GROUP 5 64

SSFL ANALYTICAL C}4D ISTRY UNIT

LOGNO-

3-25 7-8 3

PF4ON E 5 +'

DATE / " /

LOG NO .SAMPLE


?-2,57-83 'Matevater , Canoge

Site L, D/54h Scrubber Chromium 370 rviJr.Sup pH

Grab Sample taken

311/83

Received 31,e//R


SSFL ANALYTI CA L CHEMISTRY UNIT

R . Sc'?n ed . Di56~, FB 66 W . Baisley, R . Knight, D/598, 5S 1 1

J . Bownanr 0 1

CHEMICAL ANALYSISN

.

F . B . LARY , D/596 , ss 11 REPORTC . WINZER, D / 031, SS 1 2

TO :


REFERENCE : nIhnnk 93 PA9G '16

K . Johns, D/031,55 1 2

LOG NO .

3-255-83AN D

L 3- 256-83DEPT./GROUP

PHONE 5447

DATE /4-MA- 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time-

3-255-83 MovNTAI J RvJos~ F 1 . 2 PP'"'

time- 2 00 PP-I3//2/S3 SATiiDA Y

3-256-83 HOVNTA IAJ ,1VA OFF I .2 ppwi00

time= 2 PM3113183 SWNDA Y

time=

time=


and analyzed ASAP

-/ -/ 8 3

DAY=EPA distillation metho d



APPROVEDSSFL ANALYTICA L CHEMISTRY UNIT

I IBNA01476434

HDMSE00624708

CHEMICAL ANALYSIS

REPORT

LOG MOLOG NO

3-zsy-g3To: M . Magg DEPT./GROUP 56k

SSFL, ANALYTICAL CHWISTRY MI T

REFERENCE : Lcgboot '8 Dg . qPt 4ON E 547

DATE /a

LOG NO.SAMPL E


Waetevater, Canoga

Site L, n/5b. Scrubber Chromium 2 9 Q 106 ILSump p$ - '

Grab Sample taken

3--11-83

Sample Received 311A3( O,7dOAnalyzed for pH, andchromium

COMMENTS: Th* limit for Site L is 75 :ag/I .M. Mogg Kotified by phone

APPROVED / ✓•/~/JdfX~

SSFL ANALYTICAL OL dISTAY LNIT

R . Sc'',rjed ~ .̂!564, `5 66 U . Baisley, R . Knight, D/599, 55 1 1

J . Bowmann isN F cr a.

M . Mo CHEMICAL ANALYSI S

F . B . LARY , D/ 596 , SS , REPORTC . WINZER, D / 031, SS 1 2

TO: DEPT/GROU P


REFERENCE : T .nahnnk ~3 P'C-5r 4

K . Johns, D% ?1,SS 1 2

LOGNO-

3-253- 83

PHONE 5447

DATE /,-MAR-

"3

LOG NO .SAMPLE



BELL CANYON

time=

3-253-83 rf OuN T .) RW,JOFF / 2 pp1,,,~

time= 3°SPM

time=

time=

time=


and analyzed ASA P

3/// /s 3

DAY= FRIDA`( EPA distillation metho d



APPROVED

Form 619-V


VBNA0147643 6

HDMSE00624710

CI- EMICAL ANALYSIS

REPORTQUALITY ASSURANCE 556

.O : DEPT./GROUP

LOGNO •

3-z5z-? 3

544 7FROM :

SSF t - ANAMY11CAl . CHEMISTRYPHONE

REFERENCE :

LOG NO .

3-i52-83

L .B .91 A. P. 4 1


GAS : HA

RECEIVED : Bit 1 18 3

I

1

SAMPLER : FL QI0Z% 1

PRESSURE : 2 IMPURITIE S.0 toDNA % At t, 02 = pp m

ANALYSIS REQUESTED : N2 =

__

% N2 = 24 ppmCC`'OLETE Ar = % Ar = -D N Fj pp mSPECIAL : Co = Co = AR < 5 ppmC

=CO % CO =2 ND < 0 . ppm2

CH = % CH =4 4FRCS' : :

'C2 H2

= =% C2H2 ppm

-FL SUPPLY LINES -H2 = % H2 = ppm

ALF A

BFAVO 1 < < (ppm) Total Hydrocarbons as CH 4

DELTAMOISTURE = 4 5 ppm H O ( 'F DEW POINT )COCA

2

CTL 3

C " L 4

CTL 5

TA'4K NO .

CELIVERY

TRAILER

G` ER f'L F

I+MTERFIR Lr= FA. i

DATE MAR • 2 1 , 198 3

RESULT S

PURITY = > 89 .996 % FJre By Difference

PARA = AN A %

Tr = Trace< = Less Tha n> = Greater Than

N .0 . = Noire DetectedD .N .A . = Coes Not Appl y

COMMENTS . * Y.azi.== allowable limit per RAC 615 -072 for N2 is 15 pram ; for 02 + Ar. itis 5 ppm .

I

AP' ROVED

C

M1BNA01476437

I I IHDMSE0062471 1

t,

TO; M . Mogg


DEPT./GROUP 5_+

FROM SSFL A NALYTICAL CHEMISTRY UNIT PHONE ~hh7

REFERENCE : Logbook ' 3 os . ~+1D DATE /i/83

LOG NO .SAMPLE

IDENTIFICATION R SULTS

3 2 5h S3 Weatevater , Canoga

E

copper - 0 . / t' Ong/L

Site C, "Sea World" Nickel 2 . 5 mg/L

pE-24 ar . Prooortioaal

s~!ôte tpke+ ±

le received 3/11/83(c3o1yzed for copper, pE

nd nicke l

COMMENTS : The L.A . City discharge limit for copper is 15 mg/1, for nickel the limit is1.2

cg/l.

Analyses per K . Mogg ' a IL Si F!-1422, 27 Oct . 1981N . ). - None detecte d

APPROVEDSSFL ANALYTICAL CHEMISTRY UNIT

t arm 619-V

IIOI m u imi i iumm i im i 0 I0 I 0 I 0 IBNA0147643 8

HDMSE00624712


TQ: M Moz¢

!1l01~3S?1. AMA LYr 2 CA L O{Dilx 3TAT LMI T

REp FEp : Logbook '83 pg . L . L,i

LG0 MO

3-25 -83

Pp/OpiE 5447

DATE v ..~

LOG N .SAMPLE

Iov rafic*T10N RESULTS

-25 C Ch i D O 'B M /1anog aWastewater, rom um = . ._

Site B, D1544 Proce ss pH = 7,Clarifier


sample

rsple received 3fIt

30Analyzed for pH, an d

chromei im

COMMENTS: The L .A . city discharge halt for chromium is 10 rsg/L

Analyses per M. MOU ' a U. 81 Ft-422, 27 Oct . 1981

APPROVED ,

~rrr S19-V

SSIL ANALYTI CA L Ot 13T*Y cIIr1T

II0I m u imi i iumm i im i 10100 I DI 0 IBNA0147643 9

o~vT /aweou~ 564.

HDMSE00624713

CHEMICAL ANALYSIS

REPORT

LOG NO .

3_ 2cfI- s 3

DEPT./GROUP sg

PHONE S/'t 7

DATE II 4 _

LOG NO . IDENT FICATION RESULT S

N TO SAP. fo ilc.'it yM f'~

~ ., . fK~~ Sri- `f o{ N Ty

CeI1 b /r .. N

T,, N r . (s•...,. 4a(

~I 4 1 1/ AllfyVA!

c y I :..~1 .~ .. }

1 C G[

3IIo/83

SSFL AKA ' TICAL C}1 ISTRY UNI T

IIDI m u imi i iumm i iummmim u i


TO :

FROM :

A . W A 5c ►vIf


REFERENCE : It _9 3 - Lt4

PHONE s / 7

DATE , -3111711 3

LOG NO .SAMPLE


L ; 0 04 •tL :C(tf1,,01M, Xtw {

-two-83 M .r f/*f !ry L ; 0H = 0 i47y L ; CL= O.S1~1

H101= 0.35 f

3-2t1-Y3 AA ,x tuKr '~20 L ; of = 0 . 2317 L, C L

H2O = 0. 307 1

3 _ 2't2 -~s 3 M . tuw-t , l L ; OH = 0. 39 3 . L ; fL = O. 5'96 yI4 02 = 0. 214• }

3-243-91 M ;x f--< 422 L . OH = 0.OSY~ L ;CL = 0.7a`t g

}1z Oz = 0 .3~•p ~

3- ~wt-Y3 ~^ Y t ✓ ~~ ~z 3 Li OH = 0 . 02 -C' L ► CL = 0. 7 1 9

H ., 0, = 0.0s19.

3- .~rf ;'Y3 IVl~X1uJ #?4 Li 0H = 0, ill s- L .'CL = (. 1l-2,-

H 02 = 0.060 1

31j0/ ~ 3

COMMENTS :

APPROVED

Lcrm C19-V

N orma Fujik )a lHcnagerSSFL .Analy ca! Che, .,r-L

hB NA0147644 1

LOG NO .

3 - 2't0 - a 3to

3- 2'tC-8 3

DEPT./GROUP 5,2 2

SSFL ANALYTICAL CHEMISTRY LT*:I T

HDMSE00624715

LOG IIO .

CHEMICAL ANALYSIS

REPORT

TO~ Q UA LITY ASSURANCE DEPT /GROUP D/556

~rpp E : IAGH00[ 83 PAGE ,f

LOG NO •

3-239-83


GAS : & Nz

RECD : 3 //o /83

SM[PI R : FGOO5Z,/

rsES SURE / 90 o P5/ ,

ANALYSIS REQUESTED


AS METHANE ONLY

SSFL SUPPLY LINE

ALGA SBAVO

COCJ1 IIELTA

CTL-3 CTL-4

CTL -5 IZLI VY

TA>)I< * .

TRAILR$

OTI B : Nc - I j/, 4 -3

a

3-Z .39&3

PHONE 5447

DATE /IA412 . I/ , 198 3

RESULTS

MD, <i (pps) TOTAL HYDROCARBo AS CH 4

= TRACE ND = JAMB DETWrED < = LESS THAN 1

= GREATER THAN LE1A = DOffi IIZ7f APPLY

COMMENTS: •Maaiaeda allousble liait pes LW 615-072 for total byd.r carbons as eethaneis S ppa by volua~e~ fu sjoisture is 9 p~ in Be or H2 , and 26 . 3 ppa in N2 or ` .

APP7lpWED'S a

•A)! ___________MANAGER BSPL AM LIT! CBEYISTRY UNIT

II0I m u imi i iumm i im i uu iB NA0147644 2

HDMSE00624716

LOG NO .


Tp; QUALITY ASS1YMNC8

FROM : SSFL AALTTICAL DI STRY

plEFERENCE : 1DGHOOE 3

LOA NO.SAMPLE

IDENTIFICATION

GAS : /dELIWM

BEC'D : 3 f /C / 8

r SAIiPLZIR : Ft,O/0z68

DEPT./GROUP D/556

3-Z38-83

,PHONE 5447

DATE M4z. /1.198 3

RESULTS

3-238-83 , PRESSURE / 87S P5/i. I 7"R ( / (ppa) TOTAL HYDROCARBONS AS CH4

ANALYSIS REQU$STED

SPECIAL : BT)CARBONS

AS 1 K1 ANE ONLY

SSFL SUPPLY LIFE

ALFA HI;AYO

Q CA !LTA

CrL-3 CPL-4

crL-5 I*LI~Y

TANS NO .

TIAl Lit

yr zK : Nf-73, 3

TR = TRACE ND = 1Q!IB DETSCrXD < = LESS THAN

= GREATER THAN IA = DOffi NOT APPLY

''.4MMENTS: xiao~a sU *ble limit per *AO 615-072 for total hydrocarbons as ,ethane

is 5 pp, by •olone , for ,oiature is 9 }pa is He OT HZ, and 26 .3 pp, in 112 or L` .

a$SYL LTTI L CH34[ISTRY UNI T

iimm u imi i iumm i im i uui ID IBNA01476443

I IHDMSE00624717

CHEMICAL ANALYSIS

REPORTQuality Assurance DEFT ./GRDIIP :

FA01~ : SSFL ANALYTICAL C4 I LABORATORY

REFERENCE : Logbook - 83 Page -

LOG )fl BER :

3-237- 83

PH Z : 5447

DATE : '. Af4q.83

SA7iPL8LOG 1K) . IDENTIFICATION RESULTS

GAS : F/rdRA f~V PURITY = D .N.A . % D.N.A . By Differenceg..27'3 R8(3Iiy u : /d Mw j,' . ~3 PARR = D .N .A . %

BAYPLIR : _CL Z70IMPtRI TIES

PRESSURE : /$C, p$IiNC /02 = D .N.A . S OZ • ppa

ANALYSIS REQDESTED : N2 D .N.A . 5 N~ = ppm

c, SEPIE1'B Ar = D .N.A . S Ar D.N.A . ppmSPECIAL: For

CO = D .N.A . 5 00 = D.N.A . ppm02 and N2 Only . =C0 AD N K 00 = D N A m2 .. . 2 . . . pp

054 = D .N.A . S C9 = D.N.A . ppm4

1rB01[ : C2M2 = D .N.A . S C282 o D.N .A . ppm

SSFL SUPPLY LINE H2 = D .N.A . S H2 = D.N .A . ppm

ALFA

BRAVO D .N.A . (ppm) Total Hydrocarbons as C84

DELTA

cocA MOISTURE = D.N.A . ppm 520 ( D .N .A . of DEW TNT )

CTL N3

CTL #4

CTL #5

TANK f ) .

DELIVERY

TRAILER Tr =Tract< = Less Than

OER 2 K 875 > = Greater Than.-3

N.D . None Detected

D .N.A . = Does Not Apply

00b44EI4T8 : Maximum allowable limit per MO 615-072 for N2 is 15 ppm ; for 02 + Ar, it

is 5 ppm .

Q.c.srvt .APPROVED: , ! 'L,;LABORATORY MA GER

556

SSFL AN& YTICAL CHEMISTRY

IIOI m u imi i iumm i im i uui DID IB NA01476444

I IHDMSE00624718

R . Schmued ~. D/56, FB 66 W . Baisley, R . Knight, 0 /598, SS 1 1

J . BowmaninF„ . c „ra

CHEMICAL ANALYSIS

K . Johns, 0/031 ,

LOG NO •SS 1 2

3-239 -8 3F . B . LARY , 0/596, SS 11 R E PORTC . w U ZE R, 0/031, 5 5 1 2

TO DEPT. /GROUP

FROM SSFL ANALYTICAL CHEMISTRY UNIT PHONE 5447

REFERENCE : T .nahnnk 83 Page 44 DATE /o 'N^R-83

MF

LOG NO .SAMPLE



FLUORIDE ANALYSI S

3_231 -83 BELL CANYON 0.5 prii pp - ,

time= ?°°A14

time=

time=

time =

time=


and analyzed ASA P

3 / /D / 8 3

OAY = THURSDAY= EPA distillation metho d

COMMENTS : The NPDES permit for SSFL allows a maximum of LO ppm fluoride t o


APPROVED

SSFL A!ALYTIG+ L CEi~4!ISTR ~y : :

IIOI m u imi i iumm i im i uu iBNA01476445

UHDMSE00624719

TO:

FROM :

4. !nogg


OEPT./GROUP 5 67►

SSFL AN(ALYTIGL OtS1[ISTRY UNI T

REFERENCE : Logbook '3 pg. 1.i y

LOG N

3-23383

PHONE 5 ►T

DAT E

LOO NO .SAMPLE


_233_83 liastevater, CanogaSite L, W5A Scrubber N+g /~Cbraai~aSup

Op$ •

Grab ° ale taken

3/10/8 3

930ived 3110$3

Analyied for a, an d

chroa►i ust

COMMENTS: The Limit for Site L is 15M. Kogg Notified by phoae

APPROVED

~rrn 619-V

1.

SSFL •1PWLYTIGL CH . ISTRY UNI T

IIOI m u imi i iumm i im i uui DI D IB NA01476446

I IHDMSE00624720

TO : M . Mogg

FROM:


DEPT./GROUP S51


REFERENCE : Logbook ' 83 os . Ay

LOG P10 .

3-232-83

PHONE ckh7

DATE 10! S 3

LOG NO .SAMPLE


3-232-83 Wasteveter , Canoga Copper - 0 .87 rng/L

Site C, "Sea World" Nickel - 3 . 5 mg/L

P11 -24 hr . Provorticnsl JFpôie $ kP '

lample received 6 //V 1 83( 0930knalyzed for copper, pEnd nickel

COMMENTS ; The L.A . City discharge limit for copper is 15 mg/1, for nickel the limit i s12 mg /1 .

Analyses per M. Wogg 's 1% 81 FLP-e22, 27 Oct . 1981N.D . - None detected


hB NA0147644 7

HDMSE00624721

CHEMICAL ANALYSISREPORT 3-23)-83

TO: M _ Mo¢z OLrPT./©ROup 564

PRO" SSFL ANALYTICAL GF( I3TR1 UM T

REFERENCE: Logbook ' 83 pg . 14q

Pt1Of4E 544 7

DATE ---I /to /A3

LOG NO .SAMPLE


3-231-83 Wastewater , Canoga Chromium = 3 . ►' ►'9 /LSite B, D/544 Process PH = 7 2Clarifier .24 hr . Proportiona lsample

Sample received 3/ .,o/

0930


chromium

COMMENTS ; The L .A . city discharge li t for chromium is 10 %g .2Analyses per 14 . Mogg 's 1% FE-422, 27 Oct . 198 1

APPROVED

F , . r ., e»-v

hBNA0147644 8

SSFL AKALY?ICAL Qt I3TRY LIMI T

HDMSE00624722

LOG NO .


-m ; F P.

REFERENCE :, L6 73-'t't

1- '2 30 - 8 3

DEPT./GROUP Sq 9

PHONE S / 7

DATE , 3 0 3

LOG NO,SAMPLE


3 - 2 30 43 N TO S A ^% p /Y AA

1 i1 0 A , STl-c'«luKa of NTO

20

1 6 a v t • ► .•, k

f v#% ;PL Ow/

r(5AA4p/e

X .e

31to~8 3

COMMENTS :

APP4OVED

Form 619-V

kL C.,SSFL kML ICAL CHEMISTRY 1J N'IT

h

R . Schmued L. D/564, FB 66 W . Baisley, R . Knight, D/598, SS 1 1

J . Boyar

MCHEMICAL ANALYSIS

F . B . LARY , D/596 , 5S 11 REPORTC . WINZER , D/031, 5S 12

K . Johns, D/031,SS 1 2

LOG NO

3- 228-83ArU D

3- 229-83

■

TO: DEPT./GROU P

FROM : SSFL ANALYTICAL CHEMISTRY WIT

REFERENCE : 1 . 0rhank 83 Pag e- 44

PHONE 544 7

DATE 10-HAR-8 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYON

time=

3-228-83 PP 1YPA-~ 3 / . /~°f''h , •time-

714SArf

3-229-83 ?1O"rA/N RVU oFF / / pptime= SWA M

time=

time=


and analyzed ASA P

3//0/8 3

DAY- TNVQSLAY * EPA distillation method

COMMENTS : The NPDES permit for SScL allows a maximum of 1 .0 ppm fluoride to

be discharged frog the property .

APPROVED

,or

S=rL A N A L. Y rICAL CF Ì T

BNA0147645 0

HDMSE00624724


FROM:

K . WA y a*.#

SSFL ANALYTICAL CH]ZMISTRY UNI T

REFERENCE : 1_ g S 3 - It- DATE ,

LOG NO .SAMPLE


[ .op . t ;Ct>#so2

3-X20-83 #r /9. L ; OH = 0. 2 ') 'ry L . Cl = 0. 2 7')

H1 02 = I . 0

5-22I-Y3 '~ IS L ; ON = l1. 3 X49 L ; Cl = 0. 2 737,

20 7 0. 14 -3 1

3-222-13 # 16 C ; ON = 0 .3792 L,' (j = 0 . 2 U

223-g# )8 L~ off = 0 .("'t7 Cl = 0•0 0Sg

N,, 0} = 0. 14 22,

1 iv-43 Hs OZ t fl ~0 14 N t- 02

Ns so,~ = 1 . g << y

a r t d

3~y~8 3

COMMENTS :

APPROVEDNora F awa 1NanavsrCC F! dK ~, . .~ . ,~ /Y-L .- .

LOGNO •

3- Z20- s3to

3- .2? - S 3

DEPT./GROUP .5--22-

jJam.. 4 _

SSFL ANALYTICAL C 1Ef[ISTRY UNIT

uuuiuuiuu i iBNA0147645 1

HDMSE00624725

R . Schmued S. D/564, FB 66 W . Baisley, R. Knight, D /598, SS 1 1

J . Bowman

CHEMICAL AN LYSI SAM . Moa cc1/

F . B . LARY , D/596, SS 11 REPORTC . WINZER, D / 031, SS 1 2

TO: DEPT./ GROUP

FROM : SSFL ANALYTICAL CEiEMISTRY UNI T

REFERENCE : T .nohnnk g3 PA9 . -74

K . Johns, D/031 ,SS 1 2

LOG N O

3- 2z 3- 8 3TO

3-227-s3

PHONE 5447

DATE 9- HAP "g 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time=

3- 225- F 3 S . ) . 0. 3 j)p#itime= 3O°PM

3-224-93 P P BYPAs3 /. 0 ~oPwl

time= 3°-r PH

3-227 -g3 HoVNT'"J Rwu#FF1 .2 pp M

time=-3/Opl

time=


and analyzed ASA P

3/ 9 / 8 3

DAY--WEDN E5 DAY EPA distillation method



APPROVED&~~ OZ .- 64e42

C", Ile

MF

YATNAGEF / SSFL ANALYTICAL CF.D''.STh1 UNIT

I IBNAO147645 2

HDMSE00624726

cc . BOB B"SH D '551 E .A1 iBOB SETT D/539 AC1 0FRED SCHULER D/5

5% EMICAL ANALYSI S

REPORT

TO : ~Tne Oumrlinn

FROM: SSFL ANALYTICAL CHEMISTRY UNIT

REFERENCE : LOGBOOK '83, page 44

PHONE 209 5

DATE 9 MARCH 1983

LOG NO.SAMPLE


3-219-83 NEW WAX RESULTS ATTACHED TO THIS REPORT FORM

COMMENTS :

APPROVED

Form 619-V

L~~& q5h~~~SSFL ANALYTICAL CHEMISTRY UNIT

I IBNA0147645 3

LOG NO "

3 - 219 - 83

DEPT./GROUP D/539 BA33

HDMSE00624727

SSFL ANALYTICAL CHEMISTRY METHOD - GC Revision B

NEW WAX SAMPLES SHOWING POLYCHLORINATED BIPHENYL (PCB) RESULTS LESS THAN 25 mg/kg 0LOG NUMBER SAMPLE IDENTIFICATION PCB CONTENT AS

AROCLOR 1260 ( mg/kg )

PCB CONTENT

OTHER THAN

POLYCHLORINATED

TERPHENYL (PCI' )

AROCLOR 1260 CONTENT AS ARO-

(mg/kg) CLOR 5460

2-53-83 Lot 25-9 * N .D . ** t 25

2-54-83 Red Dye N .D . 25

2-155-83 WI-NFL 24-12 N .D. * ** 52, C 25 p mw V

2-156-83 WI-LB, 23-8 N. D . . 25N C

d

2-157-83 WI-NF, 23-8 N . D . . 25 ~$3 OcC r

-4- 1

2-158-83 WI-LB, 24-12 N . D . 25> 4) oo

mLot#1519 a +~+ - H

aCCd

2-159-83 WI-LB, NAT-24-12 N .D . < 25e q `

~

06 4 -1

2-194-83 WI-LB, I.ot#2896, Box#I N .D . 25 cCa a aU) ( U

o N

2-195-83 WI-LB, Lot# 2896 , Box#I I N .1) . t++ .

1-196-83 WI-LB, LAt# 2896, Box#I II N .D . .4 25 o a 14o f

w +-' m

2-197-83 Box#IVLot# 2896WI-LB N .D . t 25 D o m,,x U

2-198-83 WI-LB, Lot# 2896, Box#V N .D. .i 2 5

00 N--z COMMENTS = none detected ** <D* N = less than: ..

* ** LOG NUMBER 2-155-83 was analyzed twice using two separate sample aliquots .

Both results are listed in the table .

DETECTION LIMITS : AROCLOR 1260 = 25 mg/k g

M -00rnN

4NOD

SSFL ANALYTICAL CHEMISTRY : METHOD - GC Revision B

NEW WAX SAMPLES SHOWING POLYCHLORINATED BIPHENYL (PCB) RESULTS LESS THAN 25 mg/kg

LOG NUMBER SAMPLE IDENTIFICATION PCB CONTENT AS PCB CONTENTAROCLOR 1260 (mg/kg) OTHER THAN

AROCLOR1260

(mg/kg)

POLYCHLORINATE D

TERPHENYL (PCr )

CONTENT AS ARO-

CIOR 546 0

2-267-83 WINFY , 23-8, 1304 * N .D . ** < 25ti

2-268-83 WINFY, 24-12, L 395 N .D . 25 al 4)

a + m2-350-83 26-18 NF N . D . 2 5

2-351-83 26-19 N .D. 25a~ 0 0

0

2-352-83 26-15 N .D. < 25a) O O q0o a

2-353-83 25-9 NF N.D . 25 ? 4)

41 a2-354-83 25-9 N . D . 25 w 0 0 m

O 'H •ri • H

a b 5 02-355-83 26-15 NF N .D . 25 a s ca N

O N Wz h U' 10

2-356-83 26-18 N . D . . . 2 5

COMMENTS : *N.D. = none detected

= less than

DETECTION LIMITS : AROCLOR 1260 = 25 mg/kg

MLOG NO .

CHEMICAL ANALYSI S

TO : QUALI TY ASSURANCE

FROM. BSYL ANALYTICAL C IDU STRY

REFERENCE:

L0 43 NO.

3-z / 7- 83

REPORT

DEPT./GROUP

LOGBiOCS 83 PAGE 'r


GAS : HELIUM

RBC'D : 3 / q /63

SAItPLBR : PLOO(s32-0

PRESSURE Z000 PS/6-

ANALYSIS REQUESTED

SPECIAL : HYDROCARBCW

AS IEIHANE ONLY

FROM :

SSFL SUPPLY LIMB

ALFA BRAVO

COCA DELTA

CTL-3 CTL-4

CrL-5 DELIVERY

TANK ID .

TRA I LI6t

urHmt : 537-/ ARAA-1

D/556

.3 - z 1 ~7- B3

PPION E

TR <l

5447

DATE MAR , 1/g/90#3

RESULTS

(PPS) TOTAL HYDROCARBONS AS CH 4

TR = TRACE ND = JAMS DETECTED < = LESS THAN

= GREATER 'IRAN IIRA = DOES IKir APPLY

70MMENTS_ *I1ari2 allowable licit per RAO 615-072 for total hydrocarbons as methane

is 5 papa by volcse, for moisture is 9 rpm in He or H2, and 26 .3 on in A2 or -2 .

~Q P

RIFT a 1 .1rrT rA, C7tmi T STRY U '

BNA0147645 6

HDMSE00624730

LX NO.

CHEMICAL ANALYSI S

TO; QUALITY ASSURANCE

REPORT

DEPT. f9ROUP

FROM I ANALYTICAL CHEI[IST>rY

REFEI~JVC~ = I.ocaoac ~3 ~ 4

3-2/(,& 3

PHONE S447

DATE M,4~. //. l9B i

SAMPLELOG NO. tOENTIFICATION RESULTS

GAS : __

REC'D : J / 9 I &

SAMP1 R : too-23 T

321483 PRESSURE /950 Psi& M . C / (pp.) TOTAL H1DftXARBONS AS C84

ANA LYS IS REQUXST®

SPECIAL : HDCI.RBO

AS METHANE ONLY

FRCL :

SSFL StTh LY LIREm = TRACE ND = NONE DETECTED < = LESS THAN .

ALFA SBAVO= GItSATER THAN DNA = DOSS NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 I LIVESY

TANS NO .

TRAILER

OTH~ : SS A

COMMENTS : +Maxi ua allowable limit per RAO 615-072 for total hydrocarbona as methane

is 5 ppa► by vole, for moisture is 9 p. in He or H2, and 26 .3 ppa in N2 or 0 2

SSFL AMLYTIGL C®IISTAY UNI'

r--- ! . ..

IIOI m u imi i iumm i im i IDMID DBNA0147645 7

D/556

D IHDMSE00624731

CHEMICALANALYSI S

REPORT

To: M . M OrCr


REFERENCE : LOG BK '5' PAGE

LOG NO .

3-2)5-8 3

PHONE 5447

DATE /

LOG NO.SAMPLE

IDENTIFICATION Q PURGE I TRAP © GC/M2 RESULTS (PPB )

Water sample from the

3 Zi5 J3 No! Ac,s~ RaoM TOLUEAJ E (CbH5 CH3) = N_ b ►UN 1D (GU N D CApr 1g.,N Dcsv~~~or +r~gZ) _ < 1-t,4 N K 8L1 . Qz [

~J

Acetone (CH3000H3) ~ j

Bromodichloromethane (BrCHCl2) = C. J_Carbon Tetrachloride (CCl4) = ND. < 1Chloroform (CHC13) _ . L . < 1

Iltetllylene Chloride ( CS2Cla) = N •D. < 11,1,1-Trtchloroethana (CR3CC13) = 2020

RECEIVED ® LAB : Trichloroethylene ( C1CH : CC12) _ ,b, < )

3 / 9 / 33 Tetrachloroethylene* (C12C : CC12) = I

1,2-Dichloroethylene (C1CR : CHC1 ) =Notation about appear-

ance of the sample : Dibromochloromethane (C1CHBr2) = N. ( f

Isopropyl Alcohol ; also (CR3CIDHCH3) = ( IImoen as IPA ; 2-propanol

Freon TF (C12FCCF2C2) =

1,l-Dichloroethane (C12CHCR3) =2_

CObQ "NTS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifi-cally required according to the Rocketdyne NPDES permit, Order 76-146, YPDES CA0001309

from the California Regional Water Quality Control Board , Los Angeles Region. ( 2) per (1 )Wastea discharged shall not contain phenols, mercaptans , or other substances in concentratiot

which Would impart taste , color, odors , foaming or other objectionable characteristics to re-ceiving waters . . .", "or any substance in concentrations toxic to human , animal, plant, or fist

life ."PPS = PARTS PER BILLION

= LESS THAN ND = 370ME DETECTED) DNA DOFS NOT APPLY

/2,t' /74? a44/APPROVED .F arm 619-V

i_SSFL ANALYTICAL QIEISTRY L 1 T


DEPT./GROUP : .5 7

TR = TRACE

HDMSE00624732



REFERENCE : LOG BK ' $~ PAGE

LOG N O

3-21-83

PHONE 344 7

DATE 3/'/8/$

LOG NO .SAMPLE

IDENTIFICATiON a PURGE & TRAP © GC/`SS RESULTS (PPB )

3-2"-/-&3Water sample from the

No t ACID RcO r TA E {c~, ►{ScNa) N . l~ I

UNDEk G ROUND CALec .~ DiSv p 'oi (cS) - N. D < I .~ANiC 13L_LXT. Ca3S Acetone (CH3 QDCH 3) =~

Bromodichloronethane (BrCRC12) = N. D.< f

Carbon Tetrachloride (CC14) = N. D,< 1

Chloroform (CHC13) = /L4

Methylene Chloride (CR2C22) = 11/. D . 1

1,1,1-2rtchloroethane (CH3CC13) = Z 1 (O

RECEIVED A LAB : Trichloroethylene (C1CH :CC12) = C I3 / 9 / ~3 Tetrachloroethylene* (C12C :CC12) = 1 Z O

1,2-Dichloroethylene (C1CE:CHC1) = t~ .D . < 1Notation about appear-

ance of the sample : Dibromochloromethane (C1CBBr2) = ND . <jIsopropyl Alcohol ; also (CH3CHORCH3) = N .D . < iknown as IPA ; 2-propano l

Freon TF (C12FCCF2C1) = J ,D, <l,l-Dichloroethane (C12CRCR3) = _3

COh44ENTS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring Specifi-cally required according to the Rocketdyne NPDES permit, Order 76-146, NPDES * CA0001309Iron the California Regional Water Quality Control Board, Los Angeles Region . (2) per (1)''Wastes discharged shall not contain phenols, mercaptans, or other substances in concentratioc

which would impart taste , color, odors, foaming or other objectionable characteristics to re-ceLving waters . . .", "or any substance in concentrations toxic to human, animal, plant, or fist

life ."

PPS = PARTS PER BILLION= LESS TRAII( ND = !T )NE DE'rECTEq DNA = DOES NOT APPLY TB = TRACE

APPROVED

JI'T 619-V

IIOI m u imi i iumm i im i IO 100 I DID 0 IBNA0147645 9

DEPT./GROUP :

SSFL ANALYTICAL CFiDdISTRY UNI T

HDMSE00624733


r : M . MoggDEPT./GROUP S L'

FROM : SSFL ANALYTICAL CHF.IIISTRY UNI T

REFERENCE : Logbook ' 3 E.

LOG N O

3-2/3 S3

PHONE SLh7

DATE 3//3/ ~

LOG NO.SAMPLE


2 l3'83 Wastewater, Canoga Capper a mg/L

FRern No ( Ac,p 1Roo+r1 Nickel ! 3 . 5VNOCeCF~ .OU JD TANK3LD(x 0 35 QMRp,.,,y s i= N

-.D

. <p.o5MsJL

SP-otP *pke~ p I-1 ! = . 3

3/9/8 3

ample received 3/g 183

lyzed for copper, pIIad nickel1 C ► +P.6~+ i~l .r •

COMMENTS : The L.A . City discharge Limit for copper is 15 mg/1,12 nsg/ l .

Analyses per ?4 . l4ogg 's IL 81 fl-122, 27 Oct . 1981.K.D. - none detected

APPROVED

f ~rT Fs14-V

4(7


SSFL ANALYTICAL CHEMISTRY (JNL r

IIOI m u imi i iumm i im i 00100100 I IBNA0147646 0

HDMSE00624734

Page 1 of 4' page s

CS€MICAL ANALYSIS OF CANOGA WASTE WATERSDATE : 2 / ,14R,'23

.MPLE TYPE : R.4 8 : MONTHL Y TESTS

SUS1iITYED BY : 7? , SC ftMC2e. DATE : 9 M~1R.`B3 LOG BK ' .3 PAGE __

RsFSRErrcES : C/M 5 F/I.E1 A . A . 5 ./LEA . C. Hsu, 5. R. /-/ uRr

ANALYSIS ERFOID ED BY : .~, aQ. GARLAA/b, S. N. MAGLALANE , SSFL ANALYTICAL CHEMISTRY

APPSOVED : AJJr. MANM R , SSFL ANALYTICAL CHEMISTRYNHS-l~I WA

LOG # PH

DOD

(ppm)

COD

(ppm)

SUSPENDED

SOLIDS(mg/1)

A B/OO1 MANHOLE 3-2C'3 &- 9.0 39 53

B PROCESS CLARIFIER 3-204-83

C ssxE YCCFC 3 -2 - 83

D vo MAr~ou 3-~c6-P3 e. c

E VO WEST CLARIFIE R

Qo sovr$ cLARIFIER 3- 2G 7-83 7: D

G VO EAST CLARIFIER

H -1 ltsNHOLE 3-.2C-P3 9 .2 7-S (• 2

I lB-1 CLARIFIER

J ID-1 Be PTT

K ]41TERL1L BLDG ,

L D.`544 SCRUBBER StMP 3-2(- 3

GARAGE CLARIFIER 3-2 /~83

N TAP WATER .3-2/1-9.? Z9 /

C~NTS : Current maximum permissible limits are as follows : pH = 5 .5-11 .0 , DOD and COD havenose specified , and Suspended Solids = 1000 mg/liter .

a,m.

* Environmental Office ( ) as notified of this result on @ p .m .


I IHDMSE00624735

- - .- fp r.O L . J

\E -O J

-J'-. .-.O` J

J\ _O_. ` ~•.

a .a a(Maximum Permissible E

L \.C E

E'.

7

E\ J_OLimits) Lt

-L. r

a. eSI TE: m i.

eO

J

o rnC. ôv

- -

uv `__ov E E u z

.

A 8/001 Manhole p,p$- MD .O . oS

S Process . Clarif a ./3N.T .t D.OS

TR< O, dS

C SSNE MCCFC 0.09 41. /

0 VO Manhole TQ<O . oS

N.D.G o, oS ~-

E VO Vest Clari f

F VO So . Clarif // /./ 75 D. /S

6 VO East Clarif

N.D.H ME-i Manhole <c.oS

I M5-l Clari f

J MB-l Be Pi t

K Mat') Bldg .

rE D/5Z114 Scrubber Surd 3 7C

88M Ga-aie CIar f,D. N.D • MD.

M la ; Water <O.&. <O.OS <O,D5'

iimm u imi i iumm i iumumuu mu

SAMPLESat

rY

~

IDENTIFICATION m p E0 "

0Li

E

..N

-

'

}•. .

U

I. as ..0 .r 0

aZ

0^ L i

M

.r.

E+ ~

.

r~

. . m 0 0

O

.- ~.G

o1Oi U

Ot -i>.U

b Oh

l U G .. . i E U- Ut

a0 0

U Oa CA ) NON

U NF Total$ 0

G

0 U

U~

' 88

LOG NiMBER ppb~" -, .. .r .. .. .w . ~ o

I1!A /V.11 ND. NA. N.D. N.l~. M.D.A ~B33•,?d /DS 2 <r <I 2 1 .cl BI <r / <r cr «

ND. MV. N.R N. D . N.v. N.D.B 3-2c3 / 9/ <i / < / i' <r iss < f I <, <~ / o

C

i N..a. N.D. Nn. M . o.n -206 B7,3 19'f / .c., <,

,90<1 <! </

! ~/ /

g

3-2c7- 83 13 SB s2ao ,~ 2y< <~ / <! / / ~SF

G

TR N. ~. N. D. /y D . N.V. T4' ND.

B 3-29-S3 27 <~ <~ <~ /7 <, 3 <i G~ <I / < i

I

J

K

L

Y

N Z2 N. D. AN..a. N.D. iy.,a N..a. N.A N• D.

N 3-2II-83 S/ <1 <r 32 <1 <r < r 1 6 <i 3 < j

CHE1 .̀ICAL ANALYSIS OF C~NOGA WASTE WATERS

MONr'14Y TES r52 MARCH /983

ANALYSES OF HALOGENATED ORGANIC COMPOUNDS

RESULTS, ppb (micrograms/liter)(maximum permissible limit : essentially none )

S0

Li0

tU

Page 3 o L

ND = ]ONI DET! T' TB = TBACE <= LESS THAN

For a detailed description of the location of each site , please refer to page 1 .

(2, T'EFO ..raO TG E. 7:7: .r: .Mo«) l"iA Pft /J on/ 17 /Nr►R•~B3

IIOI iiiuiiuuimmmi i ii IOVID IO IBNA01476463

I IHDMSE00624737

CHE~f I CAL ANALYSIS OF C.a_NOGA WASTE WATERS

MONTHLY TESTS1 ,MARCH /983

ANALYSES OF NON-HALOGENATED VOLATILE ORGANIC COMPOUNDS

RESULTS, ppb (micrograms /liter )

m

Page ,L0f [.f

SAMPLE m 04,

IDENTIFICATIONmY

rd ~ ~

.• r

c7

O 4C p0

n

# O u o- > cO

Y

Total

ci~+ M

< CiO. ch

M Ej,o c~ rC c~ 7C

LOG NI!dBER ppbF

A 3-.23-a3 $9B 292 Q97 8Np..~ ~

N..D. Na. TleB 33 75 3'9 /(o <I <! < 1

C

' ^ T~D 3- 2 CG-83 988 9e'f 8~ <~ •cr < t

El TR ~1(A

F 3-20 7 -83 /5042 (3W.1 //9 cl . / 2.

G

3 08 - &? 76 39 =SIVY<~

N~cf /5-g

I

J

1 '

L

Y

N 3-2 //- 63 8 6ND< i

ND<,

ND.c t

= KE DfTECrE) TB. = TRACE < = LESS THAN

: For a detailed description of the locatiac of each site , please refer to page 1 .

(z) REpo+4reD Tc E.1 T (M.V,4 Pw~o.vF Q,y ' /7A14s . . .3

II0I m u imi i iumm i im i 1001001 0B NA01476464

I IHDMSE00624738

R . Schmued ~. D/564, FB 66 W . Baisley , R . Knight , 0/59$, SS 1 1

J . BowmaniF rancN . „,


F . B . LARY, 0/596 , S5 11 R E P O R TC . WINZER, D/031, SS 1 2

TO: DEPT. /GROUP


REFERENCE : Lnchnnk 83 F 4c 4 2 /93

K . Johns, D/031 ,SS 1 2

LOG N O

3- 20o- $3

TO

3-202-83

PHONE 5447

DATE 9-nA_ -63

LOG NO .SAMPLE



FLUORIDE ANALYSI S

3- 2 00-83 BELL CANYON O 6 * 0. 5 pp,.1t i me= ~s14 /I'1

3-z0(-$3 PP BYPASS /. D ppw+time Il`~DA N

3-202-83 ICIOv#Jm/N RuuoFF /. 2 ppmtime= 1195 A M

time=

time=


and analyzed ASAP

.3/ 9 / 6 3

DAY= WEDNESDAY EPA distillation method

COMMENTS : The NPDES permit for SSFL allows a maximum of 1 .0 ppwn fluoride tobe discharged from the property .

APPROVED

NG

SSFL %LSTICAL CHENISTFS LI T

IIOI m u imi i iumm i im i DDi 010 I 0I iBNA0147646 5

HDMSE00624739


To: K. Mogg DEPT./GROUp 54_

FROM : SSFL A7IALYTIGIL Oi 4ISTRY UNIT

REFERENCE : Logbook ~83P L./ Z

LOG N O

3-i983

PHONE ~T

DATE

LOG NO .SAMPLE

IDENTIFICATION - RESULTS

3- 9Q - g3 1t.water, Canog e

Site L, Df 5 Scrubber Ctiroaiua . 390 9 L.pH . q y

•Grab Sample taken

3/9/ 3

Sa le Reeeired 3/S/8309 30

AEalyzed for pH, andchroai~

COMMENTS : The limit for Site L 1 . 75 m&11 .

P! . Nogg Rotified by phone

APPROVED ' • \iSSFL A A ; YTIGL Q... ISTRY UNI T

IIOI muim i iiu mmiiu m umimiuu


TO : M . Mogg


REFERENCE : Logbook ' 83 Tw- g 2

L

3N

iga-a3DEPT./GROUP 564

PHONE 5447

DATE 9 183

LOG NO .SAMPLE


:5-198'83 Wastewater , Canoga Copper - 0. 2 1 mg/L

Site C, "Sea World" Nickel - 2) . 0 mg/L

pE- 8 024 hr . Proportional .Sp-rle take r

ample received 31912 3@0930

Analyzed for copper, pE

and nickel

COMMENTS : The L.A. City discharge limit for copper is L5 mg/I, for nickel the Limit i s12 mg/1 .

Analyses per M. Kogg's II/ 81 FE-422, 27 Oct . 1981K.D . - None detecte d

APPROVED

r .)r~ 619-V

M1B NAO147646 7

4?4AL'tTICAL CHEMISTRY UNIT

ID mHDMSE00624741

TO V . Mo¢ ¢

!lROI~


Of/T.~3lDtl~ 56 4

3SFI . AMLYTICAL OtWSTIIT UNIT

1eEpERtp .CE : Logbook ' S3J pg. 4 2

LOQ so .

3J c178 3

P 4ONE 544 7

DATE .3//q1

LOG NO .SAMPI.!

IDENTIFICATION 1eESULTs

3 -A7 83 Wasterater , Canoga t~romium = 0 .2 1 m~ /L

Site B, D/544 Process pH = 7 LJ!/

Clarifier


sample

t

Sample received 3/9/83

@ 0930Analyzed for pH, an d

chromium

COMMENTS : The L .A . city discharge halt for chromium is 10 mg/L

Analyses per V . Mogg ' a IL1 FE-422, 27 Oct . 198 1

A~ROVEO

I ~r rw 619-V

5 SL. ANALT:ICAL. Ot. .ISTU IT

IIOI m u imi i iumm i im i DDi 0 010 0 IBNA0147646 8

H D M S E00624742

R . Schmued D/56, FB 66 W . Baisley , R . Knight, 0 / 596 . SS 1 1

J . Bowma nF iran cM .

CHEMICAL ANALYSIS

F . B . LARY, D/596, SS 11 R E P O RTC . WINZER, 0 /031, SS 1 2

TO DEPT./ GROU P


REFERENCE : 1 .r anrnk 83 P49e 42

K . Johns, 0/031 ,

LOG N O

3-19r- B3TO

3- i 9i-8 3

PHONE 5447

DATE 9-MAR 83

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time=

3-191- 83 CViVCRT ~°I' 0.time a °4 i/'I

3-192-S3 R L So~f i- 4 . 8 f j~w+time= ___

3-I3-3 RI ~ i+ 4 • j F!"time= g _ _I

3-131-83 R I Ncrfk i g PPn~time=

Received in the laband analyzed ASA P

3/9 /s 3

0AY=MUEDNESDA *= EPA distillation metho d



APPROVED / .

'Y L F y .'' IS C_FL A .' L .'TI C c UY . _

IIvI m u imi i iumm i im i Volvo I DIV V IBNAO147646 9

SS 12

HDMSE00624743

R . 5chued L D/554, FE 66 W . Baisley, R . Knight, D 1598, SS 1 1

J . B o wca ni sM . Franc

CHEMICAL ANALYSI SMog a .~M .

F . B . LAR. Y, D/596 , sS REPORTC . 'wIN2ER , 0/031, SS 1 2

TO DEPT./GROUP


REFERENCE : t .nat,nnk '3 Pass q2

K . Johns, 0/031 ,55 1 2

LOG N O

3- / 87 - 83To

3- /w-83

PHONE 5__

DATE 9-MAR-6 3

LOG NO .SAMPLE


WATER SAMPLES FORPPM FLUORIDE , BY ELECTRODE

FLUORIDE ANALYSI S

BELL CANYO N

time =

3-187-$3 PP BYPASS `. 47 ~Pr>-►

time= 7SSAr1

3-/s'-83 PP BYPASS sp,uv~ ' /. .5 ppMtime= /0 °OP"i 3/8

3-/69-83 MOUNTA 1J RUA)LFF /, 6 PPM

time= /000Pr! 3%

3-/9O-3 Hou .h.,TA,N /Pv~voF`F /.time= 8°OA M


and analyzed ASAP

3/g /R 3

DAY= W E DIJESDAY EPA distillation method

_EXC(P7 'H&J A, T[D

COMMENTS . The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVEDSSFL LYT I CA L CHEW I _ : F' UN I T

IIOI m u imi i iumm i im i uui DID IBNA01476470

I IH D M S E00624744

R . Schmued D/564, FB 66 W . Baisley , R . Knight, D/598, SS 1 1

J . Bovr'aniF ranc1.s


F . B . LAPY , D 1 596, 56 „ R E PORTC . WINZER, 0/031, $S 12

K . Johns, 0/031,SS 1 2

LOG N O

3-184- 6 3TO

3 - 186- 8 3

T0= DEPT/GROUP

FRO M SSFL ANALYTICAL CHEMISTRY UNIT

REFERENCE : Lnohnnk 83 PQ9C 4Z

PHONE 5__

DATE 9-MAR-9 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYD N

time=

3-,g-g3 PP East /. 3 ,optime= 7 SoA f'I

3 -/85- 83 PP I,Ves iL I ,~..PPm

time- 7 SHA H

3-1$`'63 PP Nor#A / . 7 pp, ,

t i me= 7 SSA/'!

time=


and analyzed ASAP

3,' 9 / 8 3

DAY= WEDNESDAY EPA distillation method

COMMENTS The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVED

SccL . MLITICAL C CISTF. UNI T

IIOI m u imi i iumm i im i uui ID IBNA01476471

I IHDMSE00624745

R . Schnued D/56!, FB 66 W . Baisley , R . Knight, D/598, SS 1 1

nJ . Br nF n. c ,raM

CHEMICAL ANALYSI SM . M

F . B . LARY , D!596, SS 11 R E P QRTC . WINZER , 0/031, 55 12

TO :


REFERENCE : T .r hnnk 83 Pag e. 4z

K. Johns, D/031 ,SS 1 2

LOG NO

3-180-$ 3A ►a D

3- 181 - 8 3DEPT./GROUP

PHONE 5447

DATE 1 - n AR` - g 3

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time=

3-/go-83 pp BYPASS 0.9 ppr-,time= 3`'S / i

3-/6/-$3 4 ,wr~jN RvNOFF 0.9 ppw,

time 3 iopl`'1

time=

time=


and anaiyzed ASAP

3/9 /83

DAY= TOES DAY .= EPA distillation metho d

O M MENT S : The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to


APPROVED

SEF? A'A LPY :C'. L

iimm u imi i iumm i im i uui DID IBNA01476472

UH D M S EOO624746

R . Schmued 0/564, FB 66 W . Baisiey, R . Knight, 0/598, SS 1 1

J . Bow*nanf irancM .

. CHEMICAL ANALYSISM Moc

F . B . LARY , 0 1 596, ss 11 REPORTC . WINZER, D/031, 55 12

K . Johns, 0/031 ,SS 1 2

LOG NO

3 - 178 - 83

TO DEPT./GROUP


REFERENCE : T .n'hnnk g3 Page. 42

PRONE 5447

DATE 9-_'4_"8 3

LOG NO .SAMPLE


PPM FLUORIDE, BY ELECTRODEWATER SAMPLES FOR

FLUORIDE ANALYSI S

3-I~8'83 BELL CANYON 0 3 PPOA P P= / 'Pt-it i m

.e

tine=

time-

time=

time=


and analyzed ASA P

3/8 / 8 3

DAY= TUESDAY= EPA distillation method

COMMENTS : The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride tobe discharged from the property .

APPROVED

SsFL Afia `':ICML C D' :STR Y

IIOI m u imi i iumm i im i uui ID IBNA01476473

I IHDMSE00624747

R . Schmued .. D/561+, FB 66 W . Baisley, R. Knight, 0 / 598, SS 1 1

J . Bowm.a n

. CHEMICAL ANALYSI S:

F . B . LARY, 0/596, ss „ R E P OR TC . W NZER , 0/031, SS 1 2

TO

FRO M' SSFL ANALYTICAL CHEMISTR Y IY I T

REFERENCE : ' .nabmri g3 P9 42

K . Johns, D/031 ,

LOG NO

SS 1 2

3- !73 -83TO

3 - l75- 8 3

DEPT./ GROUP

PHONE 544 7

DATE 8 -1-1AR-B 3

LOCH NO•SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time=

3-/73-g3 PP 6Y PASS 1. o PP•~time /I 3O /gri

3-179-B3 Mo~NrA1N RWJO,CF / /

time- 1/ 3 /4/1

3-175-83 Pip 1 . 2 op i-

t i me= J215/'M

time=


and analyzed ASAP

3i 8 / 8 3

DAY= T'JESDA`( EPA distillation metho d



APPROVED

t'? .L/424Af4'u .

IIOI m u imi i iumm i im i uu iBNA01476474

HDMSE00624748

LOG NO .

CHEMICAL ANALYSI S

TO; QUALITY ASSURANCE

FROM : _ SSYL ANALYTICAL C®[ISTRY

REFERENCE : LOGHOOH 8J

REPORT

DEPT./eROUP

PAGE 42-

D/556

3-/f~8-83

PHONE 5447

DATE/MAR . 9, /98,3


GAS :

RECD : 3 / 8 / .3

3 -r68 83SAMPLER : fL o a 63 / 9

PRESSURE 17& D N.p. < ( (ppm ) TOTAL HYDROCARBONS AS CH4

ANALYSIS REQUESTED


AS MSPHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE ND = NONE DETECTED < = LESS THAN

ALFA BRAVOAPPGREATER THA DNA D N= =N OES OT LY

COCA DELTA

CFL-3 CFL-4

CT L-5 DELIVERY

TANK FO ,

TRAILER

OTHER: __ -f _

COMMENTS: *riaaisua allowable licit per RAO 615-072 for total hydrocarbons as methan e

is 5 ppm by volume, for .oi~ture is 9 pp. in He or H2 , and 26.3 ppm in N2 or O2 .

APPROVED

r_MANAGER

s,2 JSSFL LYTICA CHEljISTRY UNI T


HDMSE00624749

LOG NO .

CHEMICAL ANALYSI S

To: QUALITY ASSURANCE

FROM : SSFL ANALYTICAL (&ISTRY

REPORT

DEPT./®ROUP

REFERENCE : LUGR0 E 83 PAGE ~J2

D/556

3-17--83

PHONE 5447

DATE M14 .

SAMPLELOO NO . IDENTIFICATION RESULTS

GAS : hr,EL i __

RECD : 3 / 8 / 83

SAMPLER : ~L c3 - r (v7- 83 _____

PRESSURE /qq, ~5/C, t/.2 L ) (ppm) TOTAL HYDROCARBONS AS CH q

ANALYSIS REQUESTED


AS METHANE ONLY

FROM :

SSFL SUPPLY LINETR = TRACE ND = NONE DETE<TEI) < LESS THAN

ALFA BRAVO= GREATER THAN LA = DOES NOT APPLY

COCA DELTA

CTL-3 CTL-4

CTL-5 DELIVERY

TANK NO .

TRA I L .ER

OTHER : $-// -z

COMMENTS: *Maxi aum allowable limit per RN) 615-072 for total hydrocarbons as methan e

is 5 ppm by volu.e, for .piature 1s 9 ppa in He or H2, and 26 .3 ppm in N2 or 02 ,

APPROVED

, .c ._ t . ..MANAGER

~a R

SSFL ANALYTICAL CHHdISTRY UNIT


HDMSE00624750


TO : M . Mogg DEPT./GROUP 56k


REFERENCE* Logbook '83 pg. q2

PHONE 5"T

DATE 3 /a $

LOG NO .SAMPL E


U J

WeBtevater p Canoga

I_ Site Lp D/544 Scrubber LChromiua - 3 / 0 iv5=p PH (D . 3Grab Sample taken

3/$./e3

l ecited

dAnalyze for P$, andchromium

COMMENTS:

APPROVED

The licit for Site L is T5 mg/l .M . Mogg Notified by phone

JrSSFL .4!%A- TICA L CIUDCSTRY NIT

h RBNA0147647 7

HDMSE00624751


TO : M . Mogg


REFERENCE : Logbook ' 25 3 DR . 1q2.,

E

LOGNO •

3-1(5-S 3DEPT./GROUP -)'-)'"

PHONE 54L7

DATE 3 /8

LOG NO .SAMPLE


~- j (o5 Wastewater , Canoga Copper - d . 2, 8 rng/L

Site C, "Sea World " Nickel - (D . 1 :ng/L

piq2L hr . Provortlonal!r-rle toke n

aumle received

(e 09'20alyzed for copper, plnd nickel

COMMENTS : The L .A . City discharge limit for copper is 15 mg/1, for nickel the limit is12 mg/1 .

Analyses per M . Kogg 'e IL 81 FL-L22, 27 Oct . 1981N .D. • gone detected

APPROVED

SSFL ANALYTE AL CHB5IL TRY ;,! T

F ,rr+. 5, 9-V

uu iBNA0147647 8

HDMSE00624752

CHEMICAL ANALYSISREPORT .

TC : M_ Moro

SSTL ANALYTICAL OUXIBTRT UNI T

RE,ERENCE : Logbook '63 Pg .-4Z

PPlON 5447

LOG NO .SAMPLE

IDENTIFICATION 1lESULT!

3-/b4-83 Wastewater , Canoga Chromium = O. / 7 my /z_"Site B, D/544 Process pH = 7.2 /

Cl


sample

Sample receive d

0920Analyzed for pH, an d

chromium

COMMENTS : The L .A . city discharge 21olt for chromium is 10 mg,L

Analyses per M . Mogg's IL 81 FE-422, 27 Oct . 19B1

A PIPROvED

1 .cn, d1Q-V

hBNA0147647 9

LOO NO

3-1 (2 q-83QEPT./oftouP 564

SSFL ANALYTICAL CKEWISTILY UNI T

HDMSE00624753

LOG NO .


TO :

FROM'

DEPT. /GROUP


REFERENCE : InG BY ' S- A .~.:~

qg

■

PHONE 544

DATE Ma)V I/ . 19 3

LOG NO .SAMPLE


iTO from STL - 4, DENSITY . . . . . . . . . . . . ,5' ga,/ aa at 60° F

CELL 29 11204 . . . . . . . . . . . . . . . 9 9, il3 _r 76sd 3 Ego . . . . . . . . . . . . . . . . 6 . 0 - %

Cl. . . . . . . . . . . . . . . . . O1Ob' %

. . . . . . . . . . . . . . . . . 0, 4q %ANALYSIS PER

4Fe* . . . . . . . . . . . . . . . . . 1 • 5 PPM ()A`3/K5)

SPECIFICATION :

Nil-P-265390 1~* . . . . . .• .

. ."' . . . sg/liter

RECEIVED 9 LAB :

3~~ X4,3

COMMENTS : MA = DOES NOT APPLY

APPROVED ,

I . rr v. 618-V

BNA01476480I I

HDMSE00624754

CHEMICAL ANALYSISN4o REPORT

0: 11 . FrancisDo,

.r /ei jp "I

LOG N O

3-163-83

FROM : SSFL ARALYTIO% L CMUSTRYUNIT 10"ONE

REFEAW.Po i - L -83-Paie 40, NB 329, p .112 .

5447

DATEMar . 10, 1983

LOG NO . IDENT ISA

FICLATION RESULTS (OC P.MsiC I Bl

3-163-83 Canoga wastes , As Aroclor 1260 (mg/kg)= 7 3Perchloroethylene Drum

#12 .

Received 8 Mar . 1983 :Results were obtained using a gas chroeatographequipped with an electron capture detector . A sixfoot glass oolum packed with 3% SP-2100 an 100!120mesh Bupelooport was utilised under the followingcaandi t inns :

0V1W TAPE ATMB POOR :Initial value = 200o'C

Initial time = 1 .00 minute

Level 1

Program rate = 8 .00 °'CFinal value - 335 °C

OOM*AEMS

APPROVED

V . rm619--V

WL AMLTl1D11L CSIO 13TH MIT

VBNA0147648 1

HDMSE00624755

cc : R . Schmued D/541, FB12M . Francis D/541, FB12M . V[ogg D/541, FB12


To : PLANT SERVI CES DEPT./GROUP: D/031


REFERENCE : LOG BK ' 93 PAGE 4L NOTEBOOK

LOG NO .

3-/9/-8 3

PHONE 5447

DATE

LOG NO .SAMPLE

IDENTIFICATION © PURGE & TRAP © GC/VS RESULTS (PPB )


A 8 S P pond atproved under the guidelines stated in the curren tSSFL NPDES permit , the following VOLATILE ORGANI CCOMPOUNDS were found :

Rocket dyne .

Acetone (CH3COCH3 ) = TR < /D

Freeboard = 0 ft Bromodichloromethane (BrCHC12) = AID I f

30ACarbon Tetrachloride (CC14) = NQ

Sampled @ HChloroform (CHC13) _

By : L . 6,111",-rMethylene Chloride ( CH2C12 ) = T/q

1,1,1-Trichloroethane (CE3CC13) = NDRECEIVED @ LAB : Trichloroethylene (C1CS :CC12) = /-I

3 Tetrachloroethylene* (C12C:CC12) =

1,2-Dichloroethylene (ClCH :CHCl) = 2Notation about appear-ance of the sample : Dibromochloromethane (C1CHBr2) _ /U11< /

NO RAIN Isopropyl Alcohol ; also (CH3CHOHCH3) = TR /0known as IPA ; 2-propanol

Freon TF (C12FCCF2C1) = Nb

1,1-Dichloroethane (C12CHCH3 ) = jyD ' /

COMMENTS : * Tetrachloroethylene is also known as perchloroethylene . (1) -Monitoring specifi-

cally required according to the Rocketdyne NPDES permit, Order # 76-146, NPDES g CA0001309from the California Regional Water Quality Control Board, Los Angeles Region . (2) per (1)

"Wastes discharged shall not contain phenols, mercaptans, or other substances in concentratiorwhich would impart taste, color, odors, foaming or other objectionable characteristics to re-

ceiving waters . . .", "or any substance in concentrations toxic to human, animal, plant, or fistlife ."

PPB = PARTS PER BILLION= LESS THAN ND = NONE DETECTED j DNA = DOES NOT APPLY TR = TRACE

APPROVED

rJrm 619-V

LLSSSFL iGL C ISTRY UNIT

I IBNA0147648 2

HDMSE00624756

R . Scbmue I. D/564, FB 66 d . Bais'ey, R . Knicht, D/598, 5S 11 K . Jc~-s, D/031,S5 1 2

J . Bowmannci s,M . Fra


F . B . LARY, D/596, SS 1 1 R E P O R TC . WINZER, D/031, SS 12

LOG NO .

3 - /S.S- S3To

3- 1,57-9 3

TO: DEPT./GROUP


REFERENCE : 1,nchnnk 33 J44 4 Z

PHONE 5447

DATE -,?-/'-fA9-9 3



FLUORIDE ANALYSI S

BELL CANYON

time=

3-155-83 CALVEKT rAOM ROD

Itime= // Ph 7- 'WAR

3-/56-93 PP BYPASS D . 9 ppPI

time= 7'4OAM

3-117-93 hovmmN Rv uo Q . -4 f prn

time= 74'A &Y

time=


3 / B / 8 3

DAY= TU ESDAYEPA distillation metho d

COMMENTS; The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride to

be discharged from the properly .

APPROVE D

Form 619-v

SSFL HALYTICAL CHEMISTRY UNI T

BNA0147648 3

HDMSE00624757

R . Schmued 1 D/564, FB 66 W . Baisley, R . Knight, D/598, SS 1 1

J . Bowman

M .ANALYSIS

F . B . LARY, D/596 , SS 11 REPORTC . WINZER, D/031, SS 1 2

TO: DEPT./GROU P

FROM: SSFL ANALYTICAL CHEMISTRY UNI T

REFERENCE : i .nvhnnk 83 Page 92

K . Johns, D/031,SS 1 2

LOG NO .

3-/51-83TO

3-J53 -8 3

PHONE 5447

DATE 8- HA+2- 93

LOG NO .SAMPLE



FLUORIDE ANALYSI S

BELL CANYO N

time=

3-61-93 PP 8YPAs5 0. 3 ppmtime- 2 42 PM

3-152-83 rfDVNr14 /N WomorF p. q PP,.,time= 2'fj PH

3-/.53-83 Bows. N4AD 8L0ac p. 9 p p,,,,

time= 3'°

time=


and analyzed ASA P

3/7/8 3

DAY- MDNOAY EPA distillation method

COMMENTS: The NPDES permit for SSFL allows a maximum of 1 .0 ppm fluoride t o


APPROVE D

Fern 6tc_vSSFL A. LYTICAL

BNA01476484

HDMSE00624758

CHEMICAL ANALYSIS

REPORT

LOGNO-

3-lS"c-sr?

VA

DEPT./GROUP J;' .. I

PHONE 9_Z

19 83-40 DATE

LOG NO .SAMPLE


3_ ~Sv -Y3 NTo s,M tl~e fpo .- D. ~I AA Ft5,1_ 4 ce/(7'1 r~ofNTo)(D ' tAN/( io M

l 01 O,v

(s wµrkg(,'.. ,

1/7 /t 3

Norma Fujiko Manoycr.SS. 47' A mol

SSFL ANAL .ICAL CHWISTRY U L

iimmuim i iiu mmiiu m mu umiu

LOG N O

TO:

FROM :

CHEMICAL ANALYSIS

M-Mo&& REPORTY . Franci s


3-142-83 to

3-149-8 3

OEPT./3,Ip $4 1

REFERENCE *LB-83-page 40, NB 329,p . 1 04-111 .

PHONE 5447

DATEMar . 10, 1983

LOG NO .SAMPLE

IDENTIFICATION RESULTS ( QC REV1SIOIN B3

As Aroclor 1260

Canoga Wastes, (mg/kg )

erchloroethylene Drum

3-142-83 #2 23

3-143-83 #3 4

3-144-83 #4 7

3-145-83 #6 3

3-146-83 #7 2

3-147-83 #8 10

3-148-83 #10 9

3-149-83 #i1 Less than 2

Received 7 Mar . 1983 *Results were obtained using a gas chromatograph

equipped with an electron capture detector . A six

foot glass column packed with 3% SP-2100 on 100/120

mesh Supelcoport was utilized under the following

conditions :

0'P~I T E iIERATURE PROFILE :Initial value = 200°C

Initial time - 1 .00 minute

Level 1

Program rate = 8 .00 °C

Final value = 335 °C

COMMENTS :

A

APPROVED

Farm 619-V

NfBSFL ANALYTICAL C HIN1STIY OKI T

BNAO147648 6

HDMSE00624760

R . Schmued i? D/564, FB 66 W . Baisley , R . Knight, 0/598, SS 1 1

J . Bowma n

M . 9 ' CHEMICAL ANALYSI S

F . B . LARY , D/596 , SS 11 REPORTC . WINZER, D/031, SS 1 2

TO DEPT./GROUP


REFERENCE : T .nchnnk 33 Page 40

K . Johns, D/031,SS 1 2

LOG NO .

3- 1 -1 1-83

PHONE 5447

DATE 8- MAR-8 3



3-141.83 BELL CANYON Q , 9 p Ptime= /' PM

time=

time=

time=

time=


and analyzed ASA P

3/7 / 8 3

DAY= H O ► )DAV EPA dist illation method



APPROVED

Form 619-V

EDBNAO147648 7

SSFL ANALYTI L CHEMISTRY UNIT

loomHDMSE00624761

R . Sch~ued +?, D/564, FB 66 w . Baisley, R . Knigrc, D/ ;93, SS 1 1

J . Bowma n

.s' CHEMICAL ANALYSI SoF . B . LARY , D/596 , SS 11 REPORTC . WINZER, D/031, 5S 12

K . Johns , D/231,SS 1 2

[LOG NOM

3-/I4I-8 3

TO: DEPT./GROU P


REFERENCE : T .nuhnnk 83 Pays -16)

PHONE 5447

DATE7- MA R- 8 3

LOG NO .SAMPLE



BELL CANYON

3"J l-433 time=//Sp/`~ O 1 3 pp

time=

time=

time=

time=


3/7/83n

DAY= M o N .I~ y = EPA distillation metho d



APPROVED

Form 619-V

SSFL A LYTICAL EMISTRY UNI T

BNA0147648 8

H D M S E00624762


-M KINSPECTION REQUIRED

YES I I NO

DATE

APPLICAB E DRAWINGS (ATTACH IF REQUIRED (

DOING DEPT . LEDGER ACCOUNT

IUESTED BY ~ EXT.

ASSIGNED TO :

T 3 til,clnsl5 S6LAB SUPERVISION

GENERAL ORDER G.0 ITEM S MCR INIT . GROU P

FACILITY SHIFT

J-

REO . SUPERVISI Q

LEADM A

SHOP I i LAB

NOW . OR TASK


DOING GROUP (ACTUAL COMPLETION DAT E

ESTIMATE


D

INSTRUCTIONS (BE SPECIFIC) NOTE THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY .

Rey' E w& soy 31 1NUR 4n ajysls Fro ... a CF/vc~

de ~e e- rr;+ 2 N V 1Q for R L l o 0 0 I

• J QOM S Q rr'~' / S c. ,a l 4 ;' i - y5 q =n c In

sg F ►-Are0. of seals .7 8~7~ea ©F Vv>n vi cl „7 5 5 9 'F

Hard t- O (

rB lam k

RECEIVED @ LAB

MAR 7 - 198 3

S FL ANALYTICAL CHEMISTR YB1

3- i39-83

55 1j 9,? 8LIST OF MATERIAL S

FORM R ?4 .L REV E-57

BNA0147648 9

HDMSE00624763

55o

CHEMICAL ANALYSI S

TO: EQUrPMEW LAB

FROM : SSFL-ANALYTICAL CF.-*M1S TY

REFERENCE : LB-':F3 ' R L{ 0

LOG N O

3 -/.39 - b3To

PHONE 5447

DATE /4'47r. r r 76 3

LOG NO .SAMPL E

IDENTIFICATION RESULTS + 0 .3 mg

TRICH for NVR per

RL10001-F

EWR No . 5043 / Z

BLANK • Ong/500 ml

A O • ^4500 ml

vVA 5W r *a c m 5' I5A -

EWR No .

BLANK mg/500 ml

HARDW mg/

EWR No .

BLANK mg/;G

WARE • mg/500 mi

COMMENTS :

APPROVED

Rea'd. - -3

SSFL Analytical C1 emistr y

BNA0147649 0

REPORT

DEPT./GROUP 5 q3-344

H D M S E00624764

CHEMICAL ANALYSIS

REPORT

TO : M . Mogg DEPT./GROUP 56

FROM : SSFL ANALYTICAL CHEYIISTRY UNI T

REFERENCE :Lc3book !53 p g . y

J J

LOGNO-

3-139-s,3

PHONE 5"T

DATE

LOG NO -SAMPLE


3_/-35--J, JWastevster, Canoga

Site L, D/5 U Scrubber /LChromium - lg,05 . . .,., /

PH ' 4. 5Grab "le taken

y1~3

iv dl Re ece eQ~ /000Analysed for pH, andchromium

COMMENTS : The limit for Site L is 75 -mg/M . Mogg Notified by phone

A 'PROVEDSSFL ANALYTICAL CMEr[ISTRY UNI T

iimmuim i iiu mmiiu m m i m imu


LOG NO .

3 - 1 3/ - 83to

~- ! 54 - 1 3

DEPT./GROUP E 2

PHONE -- 5'/ 't 7

DATE , aIIs 83

LOG NO .SAMPLE


- r 3 1 - 9 3 L, Ofl L ; (t ''' ( L ; bH = D. 1 70~# -

3-r3 fl o N = D.21~~ L'6l = O h1 7 y

3 - 13't-t3 .# 0I L ; Oil = 4, l~3y L ; Cl = D,9L~ 2

13 13 // L i OH = 0 . 1/07 Li CL = /.2 317,

3-136-73 >'2 [ OH = C . 12 92 : fl = l .'t6~ }

-e c

31783

"ITANornw Manage?,1;Z1 V A nc, U CAA-. :s t

5 SFL APiALYI 1 CA L CHEY.I STR L u

iimmuim i iiu mmiiu m m muiuuu


LOGNO-

3-121-8 3

DEPT. /GROUP 5T 8/.3q -1 S s/ /

PHONE -5,14 7

DATE 23- HAP, -83

LOG NO .SAMPLE


(,SAS SAMPL E N ITRO6E) TPIFLUORIIE (NF3 )

(mol,- / )

3- 392-83 NF3 C TL - 3 3-7 .3 % NF3

RE ('D

7- MAX-63

SSF1 ANALYTICA L

iimm u imi i iumm i iumm iu ui iuu

vv . CA S5 i iU 5

. gpwrr+~~ ~ b9 R . Ku~ GA T

a FQAA .) J$ F8 K. Jo~~s D/oil 55, 2

Ho6~ CHEMICAL ANALYSIS

14 ,pr .D/sq4 ss fl REPORT

To: C . W, u Z E R DEPT./GROUP 6 3


REFERENCE : L k 83 Pa ge ,4 D

LOG NO .

3- 1 27 -g3AND

3-129-P S

Ssi z

PHONE 5544 .7

DATE 7- MAR- 83

LOG NO.SAMPLE


"TER SAmPLE S

3-)27-83 PP BYPASS D. 9 Pp~7 SSA/1

3-128-83 /1ovNTA/N RvNOPf l ,Ooprh

7- MAR-6 3

HGNDA Y

COMMENTS : Mxi'U" ^'.Lpw"4LE PI voR/OE DISCNAKGABLE

VA1OeR A/POfs PER"lr = /. o !pti

APPROVED

► 3rn" 619-V

-&2d6e(.12 &e*SSFL AXA IGL STRY UNIT

BNA01476494

HDMSE00624768

? 5crirvco W . bAISLCY j afS~S SSIt

-T . Bow"A"a 0/5,, l R . K Pi IGHT5 5 12

H . FKAuc t5 F86 K jot pfc3 !

H . Ho66 CHEMICAL ANALYSIS5q6F . $ . LAR Y REP RTSS l I

TO : C . W I Qz ER DEPT. /GROUP 6 3


REFERENCE :Logbuck 83 Paj e. -q O

LOGNo-

3-//3-83To

3-126-9 3

SSI Z

PHONE 544-7

DAT E 7- M'qR-83

LOG NO -SAMPLE


WATER SAMPLES ByELELTAOO c

4V0XjDE Z )

3-113-R3 dFL G CANYOA' 10wtR Q 5 PPM 0, 5 P~wa

3-114-93 BE'Lt CAA-''WV (/P"EA 0 .'1 PPM 0. .q

3-115-83 ABovE PP 11JOAM 0. 1 ppm

3-1/6-83 ABOVE PP1 5,PAAYffWcAc D . 9 PFAI

3-117-83 PPG // "'An 5Ppr"

3-118-$3 LFAvING ;SA (-Ii 'rY 0.9 ppn-,

3-119-83 R i , I1)-°A M C. 9 pp►>7

3- 1 20-83 BEFolE 0 . 3 PPM u N D A Y6s MRR-- 8 3

FXAF C o3-121-83 PP 1 , 3"cPN 1.5 4p^-l

3-122-83 sMAY RuJb -, PP 0 . 9 pp m

3-123-83 RI 3°°'° 9. Z pp1

3-121-8 $ SE .ow P 0.9 PPm

3-/25-83 Cv4vERr B£roAE R1 0.3 ppr

Co vcRr Bv'PV5 PPL 0 . 9 pp ►.~

pER&1 7- = 1,6) 1-f

APPROVE D

COMMENTS : $ AF EIZ o1$7-,« r,'.., (Z-tA "enwoo)

M~tX~r,vrr ALLof,cwABLE FLUOR/DE DiSCNA 9 6A5L E

T Cloy - v

v~DER NPAES

SSFL ANA 1GL

BNA0147649 5

HDMSE00624769

cc' IEPT. 556 % D• C . Akeson, D,15914, DA 86

CHEMICAL ANALYSI S

TO : N • t . YORE

FROMSSFL ANALYTICAL CK!1ISTRY

REFERENCE : LB' 8a P. q e)

REPORT

DEPT./ GROUP 598598

LOGNO-

3-/05 .83

PHONE 7

DATE / 7

LOG NOSAMPLE


3 -lD5• g3 Lox

ALFA

PURITY ONLY (D % OXYGEN BY VOLU. E

W # UD$

SAMLPI,ER

FL wN,, gc 7

0 ,_. P- ___PSIG

RECEIVED :

3/x/83

COMMENTS :

i

APPRO L-0'~ 14-Z ~a,~VE

Ld,BORATO . M1AI4AGE R SSFL Analytical Chemistry

BNA0147649 6

HDMSE00624770

/7LOG N O

TO :

Fi~OM~

M . Kog$

CHEMICAL ANALYSIS

REPORT

DEPT./GROUP Sst

SS FL ANALYTICAL CHISTRY UNI T

REFERENCE : Logbook pg. L.~ Q

3-103 -S3

PHONE 5~► '7

DATE

LOG NO.SAMPL E

{OENTIF{CATION RESULTS

3 - 83C~

Wa etexater , Canoga

/ b4/Q t / 1 -Ch ium - (ScrubberSite L, D 5 _prom

Sump Px (c' S

Grab Sample taken

3 /q Jt 3

le Received 3I1//SS p


COMMENTS : The limit for Site L 1s 75 mg/l.

M . Mogg NotifieB by phgn e

APPROVE D

r r .' 6'9V

/tU j; ;LarSSFL A!.ALYTIC~L CHEIEI~TRY' u'u'r

iimm u imi i iumm i im i IDDIM DBNA0147649 7

HDMSE00624771


LOG NO .

3-/02-83TO: M . MOM DEPT./GROUP 57h

FROM : SSFL ANALrrIGIL O{DIISTRY UNI T

R£FER£NCEI Logbook ' 83 oor . Q

PHONE Skh7

DATE 83LOG NO .

SAMPL EIDENTIFICATION RESULTS

3'102 3 Wastewater, Canoga Copper - 0. 30 mg/L

Site C, "Sea World" Nickel - -3.5 'ng/L

pf24 hr . Prooortiona lTQ-rl fOLPR

maple received 31/,//0//,30

alyzed for copper, pIInd nickel

COMMENTS: The L.A. City discharge limit for copper is 15 mg/l, for nickel the limit i s12 mg/1 .

Analyses per M . Mogg 's 7~ 81 7!•422, 27 Oct . L98lN.D. + None detected /111

APPROVED G. FL A!iA~ . I .:d.

:, v im= -RYCNI T

BNAO147649 8

HDMSE00624772


p,o SSlL A %ALTTIGL OFimF14TtT UR T

REFERENCE= Logbook ' 33 pg• i.40

Los NO

3 -/o)- 3

OE►T.~3R0{,~' 564.

PtiOeeL 5447

,__

LOG NO .SAMPLI

tOfNT ( !<ICATtON RESULTS

3 /O I CS3 ltasteweter , Canoga Chromi u _ W. I). K 4 . 05 " " V IL...Site B , D/544 process p8 = Q , 3

Clarifier

24 hr . PTOportioaa l

sample

r

ample received

~13d1

Analyzed for pH, ■nd

chromiumi

14

COMMENTS : The L .A . city discharge licit for chromium is 10 mg/L

Analyses per M1 . Yogg ' s 11„81 FE-422, 27 Oct . 1981

APPROVED

/ ~rrn 619-V

SSFL AMLY'ICAL Oi13T1tY t.~(I T

IIOI m u imi i iumm i im i 100 I 0 I 0 IBNA01476499

UHDMSE00624773

LOG N O

CHEMICAL ANALYSIS

REPORT~- (tl -4 3

DEPT./GROUP S~► t - 3 1t(

PHONE f y 7

Lg 11-9t DATE 3 7 3

LOG NO .SAMPLE


-!o 1t -83 N Tv S pk/Ft = o. yo •~, ~ F~

ST-'t k7 N To

cell 2'b Rey t,~ k

(5 A An r Lf •( M ,~~ YM i y . M

C

3~`ff s~3 t

No'T11a Fujikau Af6 nape'SSFL Arsalyttc4 Chemistrb•

SSFL AML 'ICAL C~{DEISTRY UNI T

IIDI m u imi i iumm i im i II I U

CHEMICAL ANALYSIS

REPORT

LOG NO

3- So-8 3to

3- z.-g 3

DEPT./GROUP S 2 2

LAS 3 _ g

PHONE Jai `t i

DATE

LOG NO.SAMPLE


3- B7 -i3 L : off t L ; tl 1 ; OH d. rSD 9M i X di `r

C L

3- s~- 8z L'OH t L, CL L . off = o .o s 6 yLCL

t0 . H 1

b' L, CC = !• -1 06 9M, x

honwG P iAa 4 Manaper

S.S r. d n -, .. •s .•rr ~kr-r • . ~-,

S~FL AMLI'TIGAL CHEIJISTR1' L'NI T

IIDI m u imi i iumm iimni i imu U


To: s°8 WALTE R


REFERENCE :L og,o~{ 83 Page 38

DEPT./ GROUP 5____ HG 4 2

PHONE 5417

~-. DATE

LOG NO•SAMPLE


t D C-v sal iplcs (. H L OR f D E

3-71-83 /o QPT- /7o 29 pp '

3-75-83 /oQPT-/70 2'1 ?P '

3-NAR-83 '

COMMENTS :

APPROVE D

)rrn 619-V

NoTEBooc 0235 a'c 6Z

SSFL ABIALY't ICAL C.~!) STR1 U tT

II0I m u imi i iumm iimni i iuuuiiu

R Sc~ rcvE~ v/ J . &4~SLEr? o/s9e Ss /I

gS . ~owrlau S6

N . FRAJCi5JF666

K . J-ol.ns D/3 l SS/2

M. /-fo6 6

TO

CHEMICAL ANALYSI S

: . WIUZ~R

FROM :

R~QR~'~' S S I {

DDD E! PP T.(GROUP ~03/


REFERENCE : L oy koo k 83 Pc 3B

LOG NO

3-70-9 3To

3-73-83SS/ Z

PHONE ,S9 y 7

DATE 5-/-1A .-8 3

LOG NO .SAMPLE


WATER SAFIPLE S F L L)OR i DE ION!

3-70-83 PP, S P ► LLWA Y ~•9 PP"''~y

3-71-83 PP , SOUTH SIbE '4 .1 pp,-i R'E SAMf'LEI)

FCCt_ LOW n J6

2 pp Q~ }G I ►\J A LO3-72.83 PP, SOUTHEasT .s, DE ~ t 5C H Pc' & E

SAMPLE W+4IC )

3-73-83 PP, No, rHEAsr g . S pp''~ 54OUJEt i

4.4 ~~ ►~ F/PEC D 3-MM 83 -~ y aLECTROY

THCi/ZSAh Y

V PO N STA R.'TZ G

A* I ~tSC &E LTE'D

IMwt~ 1+~ Y ~~ ~~c~3 t~ u~o N

p tS ) r>J FD RM "n' fCOMMENTS :

M AXtMU&- . 14 L(.ICWL~ fLU bR t~£ 7>tSC t -f M3(F

U I3 D 3PD€ ~€ ran tT

APPROVE D

f .~rrr 619-V

iimm u imi i iumm i im i II IBNA0147650 3

S- FLAAM ~TICAL CtiO?STAI' LThI T

HDMSE00624777

R . 5ctTvc~)6 pwr+gnl•j- ,

M, F A(-t5

lyt_ HO&&

W . 8AISLlY} afsgg ssnR . KIuiGHT

5512.K Jo v s 0/03 r

CHEMICAL ANALYSI S

1c• LPr'TO: C . k1 l IJ L E R

FROM :

R~j %~F~TS 5 l

LOG NO

3-7a-8 3Tp

3-`77-53

DEPT./GROUP O31 SS 1 2


REFERENCE : LOg b oo k 83 J7 e. 3 $

PHONE 5.44 7

DATE S-MM k-- 8 3

LOG NO .SAMPLE


WATER SA rLPE.fiS FL UOR ODE ION

' 3>,3-76-83 R i S PI L ~WAY I' ELEcT12.0PE

3-77g3 3 b I TC H SCFoRE /~ ! 1 1 FP'

I

/PEC'v 3 -t-1M-8 3

TM'.'RS DA Y

Fo LLo U,1 t 1~) Cs.r,E

1 H4 off} LT O F

~sctf-,A~.G E .

COMMENTS :

:X rM U rat AL(- o Ut) > c9 L'E FLU OR 1 D~ DI RG t3

V1JD,ER 1J'~' PE h tT .= 1 .0 PPM .

APPROVED N.SGLDLISTRY UN F

IIDI m u imi i iumm i im i II IBNA01476504

HDMSE00624778

R . S CHhvCV W . 8AISLC ' '} a/S9a sst~Y . EowHA .' 51 R . Kr~I GN T

1 . FRAr✓ c IS F866 K. JOhr S D/o3 t 55'i2.

H_ Ho6& CHEMICAL ANALYSI S

fFILLPY R 7 TSsi (TO C . W i u z E R DEPT./GROUP O3 /


REFERENCE : L O9I o k ~3 PQ9 e 38

LOG NO

3- 79-8 3

Ssl 2

PHON E 544 7

DATE 5 -__x'8 3

LOG NO.SAMPLE


WATER .SAMPLE FL UOR 1DE ION, by

E~ccr,wDE3-79 - 83 B~ L-ow PP $, 5 pj n-i

r

/?Ec D 3 - MgR-83

T$vRSPAY

Fpc. Lo c) r NQ'F1 fM'LT'

TIC csc -R.,~ .

COMMENTS :

Nt~~ O `

PZ4

U xIM.U~ ALLo ~b L~ DE5 ~ .0 PPM .

APPROVEDSSFL A?iA'LI^SGL~ IZSTRY ufiI T

IIDI m u imi i iumm i im i II IBNA0147650 5

HDMSE00624779

D/s?5 Ss UQ, Sc•1r+ ~cpD1S61 W .

SAtSL T

J, 6owr1A►J R• j h~GS D/&3 t SS 1 2FRRvc 15 FBt6 .Ml, K

N . !-066 CHEMICAL ANALYSI S

F. L3 . l .P Ry R~W.( b Tss « _ .

FROM' - SSFL AKA LYf I CA L O{DII STRY u r

ReFERENCC :L k _k 83 Pagc. 3$

LOG NO

3-3 ._'3TO

3-€ -8 3S S' 1 2

PHONE _44

DATE S ____ - _3

LOG NO.SAMPLE

IDENTIFICATION REStI LTS

WATER MF1P«S FLXR/OE ION

$y ELEtW-ODE -~

3-E3-83 BELL, (.mp Yov 3thM

2 .0 PP'11 ~. 6 PPMTIMT p+O ► B Y £ A

N6BFFORt

° 'PROPE&TyOFF tSTf ~t,JRT?o

3- 8 g- B 3 A P TF, PM 3.4 pp"i M ~-Ttf OL1

3-85-83 LETF, VPPER Di TW , 6 ppF i

'PMr

3- 86 -S 3 L E T F, GoWER D i TCK D. 8 fpm9 Pr1

RE~I p 3-NAe-B3

TM vat DA YII.OW II)G- LT O~ 'TNT tSCt f R.&'E

COMME NT5 :

K*XIMUM At.IOLJ D UIJPE N is PERM t T =1.0 PPM_

SL AM IG: IS RY t - T.

IIOI m u imi i iumm i im i II I I D I IBNA0147650 6

DEPT/OROuP 0 F

HDMSE00624780

g . 5 L .th D.7 . aowHgNN . FA' SN . MO&&

W . 8AisL e 'f 4Jc ssliDIS69 R . K ►.11bHT 551 2F866 K.

I1IEMICAL ANALYS I S

L~fZYTo : ~ . 1~lIUZE R

FROM :

R~ l5O9~ 55 1

LOG NO .

3- 87 -83Ta

3- 9a -8 3

- DEPT./ GROUP O3/ .S S l 7..

SSFL ANALYTICAL CFiF.MI STRY UNI T

REFERENCE . LogbQO "' $3gage 3 8

t .O PPM FLUOR. c T ~ .APPROVED At /_A

COMMENTS : AFTER Dl S T,W TI Al (FPq /yk TNOD )

f4Ax~ Flu R A U.vw E'D vw~€R NP~FS ERM iT

PHON E 544 7

DATE 5 - H4R- 3

LOG NO .SAMPLE


WATER SAMPLE FLVaRIDE £O-'Y E 1.~tTRODf

3-87-83 8L- '- G9 AvYW 0 .5 pp~ ►-~ O, Spp~q-MAR-83 A M

3-88-83 8ELO1J PP, ~ - AM

3-gy .g3 pp, rU A,4 z .gPp~

r

3-9o_83 R/ / ~M 7.6 pp

/?c +D 4 - t AR-83FRIDAY

IIDI m u imi i iumm i im i II IBNA01476507

I I IHDMSE00624781

P. . Sc~:rrvt~

J- . B Ow HA NFQ,q~,c 1 SM .

H . Hc6C~

w . 6 AIsLE` ' } v/s9>3 ssrrD~569 Q . KJI GMT SS

I 2

CHEMICAL ANALYSIS

~.5 . ~ ..A Y REPORTrD 54 6 .5u

LOG NO

3-91-83Ta

3-99- e 3

C, w uI L E R DEPT./GROUP O3/ S s t 2

FRC?MSSFL ANALYTICAL CHEMISTRY JKIT

REFERENCE : L.' '00k S3 Page 38

PHONE 544 -7

DATE

LOG NO .SAMPLE


WATER 5 MP1,E5 f L v°K/ D E IOIV

3- 9,'83 PP , NORTH 3• R P1'"' '

3 - 92-63 PPS So&TH z . 3 pp"-

3 - 93-83 PP, .vs T 3.3 pp'

3-98-83 rrotiPostrE , 1 "AL 3 . 2 ppri Z• ~/°p'"3-9t,92,`J3 -B 3

3 • q4 - $3 R (, WoKT AT PvHP$ 7. pM

3 - 95_ $3 R 1 cis T q'¢OAM ~. 2 Pa m

3-9-e3 R 1, w Fs T wsAR ae~ 0 . ! pPm •

3-99-83 R { (OHfos / TE' 6, 0 pp,► , S. ppM .EQ c'4t_ 3-91195,96-8 3

/PEA rD 4 -MAk- $3

FR IDAY

~ U ►1~~R. I-Ps PE M iTMAXI iUtit LLou.) J

cs 1 .0 PPM FLL) OQflfAPP ROVED

crtS A!N

rNao)COMMENTS ti AFTER D/S r/LLAT/PAJ (EPA ME

_______T U1•'I ?

IIOI m u imi i iumm i im i II I 0 D IBNA01476508

UHDMSE00624782

R S~~ ►,,,cu W. 8AISLcY} p/S76 ssi t

. 7 . 8ow ►~q► , ~~561 R . K ► wr ss t 11 . FRAe,c' S F5 K. Jo k" S &,"3 t

CHEMICAL ANALYSI Si H o6 v.

~. 8 . L. Ry /REf?RT~: C . WIUZE R

FROM=SSFL AMLYfIUL OiZ7t1STRY UNI T

REFERENCE :ip~ DOK 83 Page 4o

DEPT./®1lOUP ~ 3 ~

LOG NO .3 ../O4 ; -3

A'Jo

3 -/07 -$ 3

SSi 2

PONE 544 7

DATE _ _ - _

LOG NO .SAMPLF

IDEN11FtCATION RESULTS

WATER SAMPLES FL 'CR/DE ZON

rl SY ELEC R.c~C3-/O-€3 BEc CAMYow

°2 P/'9

3-/07-83 LEr 3 PM 55O/7/1/'1

Be TToH

s

eE'l.L C ANVOI ( S

'RED b 4- nAI43TAE LT 5F}MIPL 1

FR 1 PAY {'O t N T $ FORE Ga,r~ a

6rF ---# PRO

TNtsD)C01r1kIEhtT5 : AFTER Ors-'« #1Tio~I (EPA NE cRN+ rrrt AX ratv ~t A Leo wA d L~ u►.~vEP N PT S

ltS ( .0 L ~ L o c I ate .

•►vovE o ~'6SFL AliA I G L OiD[I S TH ~LZR I

IIOI m u imi i iumm i im i II I I D IBNA01476509

I IHDMSE00624783

R . ScHhu[p W . BAISLt:Yj o/S9S SSII

.7 gowr,q ►,l ~15b9 R . KNIGHT SS12

H . FRANC 1 S F866 K. Jo k'^ s DIo3 I

H . H O66 CHEMICAL ANALYSI S

TO

f $ . LPr2y D 5°1 sS~iRT

LC yV I u Z E R DEPT./GROUP O3 /

FROMSSFL ANALYTICAL CHEN.ISTRY U11T

REFERENCE Look 43 Page. 4 D

LOG N O

3-//O-S>3

.SS / 2

PHONE 54'4 7

DATE 5- MA k - 8 3

LOG NO .SAMPLE


WATER SAMPt.E FLtiORIDE IO N

3-//0-$3 PP A'Efi/( cry -IIL 0 . 6 ppM e Y EL ECTROA E1

I -t ,yk e~o c~

r

,q6 `p $-MA, 3

SAT &? PAY

COMMENTS :

k~X1M4UM fLeo )AC3L~ UNDER. PE&ML1

is ~• o PPM ~"LVot~~~+~ .

A :,iu4~Pti._._-A P P R O V E D `1 ~SSFL AhALYTIdL Q ISTRF UMI

,~ .- Esc V

iimm u imi i iumm i im iBNA01476510

UHDMSE00624784

R . 5cNr+ J cp W . 8A~SLEY D/s9a SSJI

j , 8OWP A ►J D>'SA R . Ku l GNT SS 1 2

M FE,q ,~c I S F866 K . Jo1+„ s

p .

0%3 I

. H~bc, CHEMICAL ANALYSI S

TO :

R B . L A Y R~ 5~F6~'ss c (C 1nJ l IJ Z E R. DEPT /GROUP O3 /


REFERENCE :~c9 1C b 3 Pag; 40

LOG NO

3- 1I1- $ 3.4 )+

3-1/2-$ 3•

SS/2.

PHONE 544 7

DATE _ BAR- 83

LOG NO .SAMPLE


WATER SAIIt'LES FL t'og/Dff IoN / b

C .pL3-111-8 3 BEL ow P' .2 . d PPr-~

3 en

3-1/2 . $ 3 S PR/A1 kt ER RUNOFF 0 . 4 pp .i/N7'v PP

i

~4r~ 'p S-1yAR-B3

SA TvRO~

Lt&4T RA ► MM .

COMMENTS : MAX IM V INS f~tLLO JftE LE LUURI bE

tS C44 ARG~S Lc VNaE'ti~ ?ES P ~I J tT 1 .0 P M

APPROVED

r ,••r E'9-' .1

„/&, 4 (SSFL A?ALL1T1 CA L C STP.Y NI T

IIOI m u imi i iumm i im i ID ID DVI I IBNA0147651 I

HDMSE00624785


DEPT/GROUP

PHON E

DATE _L (y' %~+=l u T ~

LOG NO .SAMPLE

IDENTIFiCATIQN RESULTS

S T L ~~ LE>aN ~~.~ •'' ~

T 1

(I )

Lt

T

j 'f~ 4nrt t.

r , l C

Z _ C ~v r ,~ rlc

3 5 3 #3 R+ L I~ & L.:N

(I )

C I iZ.IC t4 )- r L c N T' F

~) 3 7 TIZ c 1, i, 1 N E

I-ZICHLCLC i.T HL N c L I ~" ,=i u !A

>~~tom,=~~~~.ESS IH0 L' T

SSWL ANALYTICAL CHEMISTRY UNIT

E NG INEERING WORK REQUES TI TIT i_r _^r C B

INSPECTION REQUIRED

YES NO

APPLICABLE DRAWINGS (ATTACH IF REQUIRED

DAT E

DOING DEPT . LEDGER ACCOUN T

REQUESTED B Y

LAS SUPERVISION

GENERAL ORDER G .O . ITEM S MCR INIT GROUP NOW . OR TASK DOING GROU P

EXT .

130FACILITY SHIFT

ASSIGNED TO :

SHOP A I LAB

REQ . SUPERVISIO N

LEADMAN

ESTIMATO R

MECHANIC 0

INSTRUCTIONS (BE SPECIFIC) NOTE: THIS FORM WILL BE USED FOR NON-DELIVERABLE ARTICLES ONLY.

TL-

~; o ? 1K Ai .14 .. / y s s e A -i Adz -7e-

f ,Z r G.-'Or

23

3-65-83


LIST OF MATERIP.LS

II II II II II I III IBNA0147651 3

No .R 34624 1EDUESTED COMPLETION DAT E


ESTI MAT EHOURS MATERIALS

REQUIRED REQUI RE D

HDMSE00624787

M . NovR . SCM -D 4/569 F8 66

N . V A ►-' $

3, 8or✓ HA ►J

~.8 . LfRY D/596 £5 11

LOG NO .

CHEMICAL ANALYSIS 3 -6O - g3

REPORT 3-/,2-83

TO : C . &h j2E R


REFERENCE :LO9~ook $3 NG~e 3$

DATE 4-fl-93

LOG NO .SAMPLE


Ir./ TER SAMPLES TR / cN ZO,~oE rN - ENE (TC F

3-60-83 BACK sLD6. 3c3 AID' / PP 6AT

3-6/-83 FRONT BIOG . 353 ND~ /p,AZ

2 4-2 2 63-6 -53 5

A2Ec' o

3/3/8 3

COMMENTS : S pY! 2/ i To 3Pr1 3/2. = 2 •Z3 ikI '

APPROVED Rte./

DEPT./ GROUP O3 SS 1 2 .

PHONE -544 7

SSFL AliALY'T"fCAL CH@EISTRY U2~I i

IIDI m u imi i iumm i im i ID DID D II I

TO: M . Mogg

FROM


DEPT/GROUP

SSFL ANALYTICAL CREIISTRY UNIT

REFERENCE : Logbook ' $ 3 p, . 3?

LOCI Pt0

3-59-~3

PHONE 5hh7

DATE

LOCI NO .SAMPLE


3- 54,-$3 Wastewater, Canoga Copper - Q.23 ,ng/L

Site C, "Sea World" Nickel • Z . (a rig/L

2) hr . Provortiflnsla 7 "-++ l p t o ~r ~ n

31~Z~ S ~

mple rece ived 3/3/ 3H~ 15. 15

alyzed for copper, pEad nicke l

COMMENTS : The L.A . City discharge limit for copper 1s 15 mg/1, for nickel the limit is12 mg/1 .

Ane1yses per M. l[ogg'p IL 81 7L-122 , 27 Oct . 1981X .D. - Hone detecte d

APPROVEDS~FL AMLYTICAL CH l STRY [TI T


I IHDMSE00624789


SSFL AMLYTICAL Ot1~JtISTRY VIrIT

RLrpERENCE: Logbook ' pg. GATE

LOO NO •SAMPLE


3'S6`~3 O / V1 /Wastewater, Canoga Chromium = . '-f 1 5 L,

Site B, D/544 Process pH = 7 , ,

Clarifier


sample

1

Sample received 3/3/S3r~ )11 .S


chromium

COMMENTS : The L .A . city discharge limit for chromium is 10 mg/LAnalyses per M . Mogg ' s IL 81 FE-422 , 27 Oct . 1981

APPROVELI ,

Isrm E19'V

Nf5SFL A?ALYfICAL OD .13TRY W(I T


LOG NO .

3-58-S3DEPT./GROUP 564

PHONE 5447

I IHDMSE00624790

!LOG NO •


TO: M . Mogg


REFERENCE : Logbook ' 53pg . 3'

PHONE 5447

DATE /37 3

LOG NO .SAMPLE


Wastewater, Canoga/

OO r''`5 L(Site L, D/544 Scrubber Chromium - D !S:imp PH CD . `7-

Grab Seaple taken

3~3/s 3

Semple Received 33/8 3@iir .SAnalyzed for pH, and

chromium

COMMENTS : The limit for Site L is 75 mg/l .

APPROVED

Jrrn E`9-V

DEPT./GROUP 564

jFL ANALYTICAL CR ISTFi 'i ~;N :T

ID D

LOG N1. BER :

CI-IEMiCAL ANALYSISREPORT

TO : Quality Assurance DEPT ./GROUP :

FROM : S M AKA LYTICA L CW' STRY LABORATORY

REFERENCE :

a

LOG NO .M

3-56 -93

Logbook - 83 Page -38

SAMPLEID 2TI FI CATI ON

SAMPLER : FLXDS3 74

PRESSURE : a ODOP.si q #IMFURITIES

02 = D .N .A . % 02 ND . / Ppm

N2 = D .N . A . % N R = N ..f ppm

Ar D.N. A . % Ar = D .N .A . pp m

1?- 5-e,-93

PHONE : 5447

I1 .TE : 7 4 4ktH /98. ?

GAS : HYDRO EW PURITY D .N .A . % D .N .A . By Difference

RECEIVED : 3 MAR, X8.3 PARA D .N .A .

ANALYSIS REQUESTED :

Cow7I, m

SPECIAL: For

0, and N2 Only .

FRO[ :

SSFL SUPPLY LINE

ALFA

BRAVO

DELTA

COCA

CTL #3

CTL #4

CTL 05

TANK NO .

DELIVERY

TRAILE R

OTtD✓ R S-K SvapYCoMC~E$•$ S'rAr~a✓

CO = D .N .A . % CO = D .N .A . ppm

CO2 = D.N .A . % C02 = D .N .A . ppm

CR4 = D .N .A . % CH4 = D .N .A . ppm

C2H2 = D.N .A . C2H2 = D.N.A . ppm

H2 = D .N .A . % H2 = D.N .A . ppm

D.N .A .

MOISTURE = D .N .A .

556

RESULTS

(ppm) Total Hydrocarbons as CH4

PPm H2O ( D .N . A . or DEN POINT)

Tr = Trace= Less Than

• Greeter Than

N .D . : None Detected

D .N .A . = Does Not Apply

OOMENTS : Maximum allowable limit per/kA0 615-072 for N2 is 15 ppm ; for 02 + Ar, it

is 5 ppm . /

APPROVED :

LABORATORY &A',10CER

II II II II I I II IBNA0147651 8

SSFL ANA,V~T1CAL C'rIE CISTRY

I IHDMSE00624792

cc : P . Kleinsmith D/768, T040

R . Schmued D/541, FB12M . Francis D/541, FB12M . Mogg D/541, FB1 2




DEPT/GROUP D/03 1

REFERENCE : LOG BK ' 83 PAGE 3cf NOTEBOOK -

LOG NO .

3- 54 -g 3

PHONE 544 7

DATE -J -H14I`- 8 3

I

J

LOG NO .SAMPLE

IDENTIFICATION PURGE & TRAP©

GC/MS RESULTS (PPB )


3_5-4 - F ? AI Inlet to the R2 proved under the guidelines stated in the curren tretention pond at SSFL NPDES permit , the following VOLATILE ORGANI CRocketdyne . COMPOUNDS were found :

Acetone (CH3C0CH3) = TK< /D

Sampled @ M Bromodichloromethane (BrCHC12 ) _ )UD <

3 3Z9_3 Carbon Tetrachloride (CC14) = N,64 /

)By : L . (,I417J Chloroform ( CSC13 ) = IT < 1

Methylene Chloride (CH2C12) _ NDC

RECEIVED @ LAB :

313 /13 1,1,1-Trichloroethane (CH3CC13) _ [ /

Trichloroethylene (C1CS :CC12) _ a.

Notation about appear- Tetrachloroethylene* (Cl2C :CC12 ) _ NO<

ante of the sample :

D <1,2-Dichloroethylene (C1CH :CHC1 ) = /V

Dibromochloromethane (C1CHBr2 )

Isopropyl Alcohol ; also (CH3CHOHCH3 ) = 71Q ~~D


Freon TF (C12FCCF2C1) = NQ[ l

1,1-Dichloroethane (C12CHCH3) = 11494 1

COMMENTS : * Tetrachioroethylene is also known as perchloroethylene . (1) Monitoring specifical-ly required according to the Rocketdyne N ?DES permit, Order # 76-146, NPDES # CA 0001309 from

the California Regional Water Quality Control Board, Los Angeles Region . (2) per ( 1) "Wastes

discharged shall not contain phenols , mercaptans , or other substances in concentrations whichwould impart taste , color , odors , foaming or other objectionable characteristics to receiving,waters . . ." , "or any substance in concentrations toxic to human, animal, plant , or fish life . "



APPROVED

f,Drm 619-V

SSFL A ICA- &EMISTR-i UNIT

II II II II I I IIII IBNA0147651 9

HDMSE 00624793


K . Francis D/541, FB12

H . Mogg D/541, FB12



REFERENCE : LOG BK PAGE

CHEMICALANALYSI S

REPORT

DEPT./GROUP D/03 1

NOTEBOOK

LOG NO .

3-53- ? 3

PHONE 5447

DATE 4 ' ~i'1R~0 3

"SAMPL E

IDENTIFICATION© PURGE & TRAP© GC/MS RESULTS (PPS)

F Water sample from the Using the concentration techniques and methods ap -~7 _-R2 retention pond at

Rocketdyne .

proved under the guidelines stated in the curren t

SSFL NPDES permit, the following VOLATILE ORGANI CCOMPOUNDS were found :

Freeboard f t

Sampled A / M?

P

Acetone (CH3COCH = / 7Bromodichloromethane (BrCHC12) = NO z3

,J

r

By : L . CoCarbon. Tetrachloride (CC14) = /VD T

Chloroform (CHC13) _

RECEIVED ® LAB :Methylene Chloride. (CH2CI2)

1,1,1-+Trichloroethane (CH3CC13 )

Notation about appear- Trichloroethylene (ClCH :CCl2) = 3ante of the sample :

Tetrachloroethylene* (C12C :CC12) = N40 4 f

1,2-Dichloroethylene (C1CH :CHCl) = 3

DDibromochloromethane (ClCHBr2 ) = N

1Isopropyl Alcohol ; also ( CH3CHOHCH3 )


Freon TF ( C12FCCF2C1) = 21,1-Dichloroethane ( C12CHCH3 ) = /V,44 G 1

COMMENTS : * Tetrachloroethylene is also known as perchloroethylene . ( 1) Monitoring specificall

required according to the Rocketdyne NPDES permit , Order # 76-146 , NPDES $ CA0001309 from theCalifornia Regional Water Quality Control Board, Los Angeles Region . (2) per ( 1) "Wastes dis-

charged shall not contain phenols , mercaptans , or other substances in concentrations whichwould impart taste , color, odors, foaming or other objectionable characteristics to receiving

waters . . .", "or any substance in concentrations toxic to human , animal, plant , or fish life . "

PPB - PARTS PER BILLION

= LESS THAN ND = NONE DETECJD DNA = DOES NOT APPLY TR = TRACE

APPROVE D

r arm E19-V

&~~~z7 &EtzSSFL ANALYTICAL C STRY UNIT

IIIII II I II I II IBNA0147652 0

HDMSE00624794


M . Francis D/541, FB12M . Mogg D/541, FB12

TO: ROCKETDYNE PLAINT SERVICES


REFERENCE : LOG BK ' PAGE


DEPT./ GROUP

NOTEBOOK

LOG N O

3-52-8 3

PHONE 5447

DATE 4 _ Mi49 - 3

a

LOG NO .SAMPLE

IDENTIFICATION ❑✓ PURGE & TRAP ✓ GC/MS RESULTS (PPB)

Water sample f rom the Using the concentration techniques and methods ap-

3 -5 2- S 3 PP retention pond at proved under the guidelines stated in the currentRocketdyne . SSFL NPDES permit , the following VOLATILE ORGANI C

COMPOUNDS were found :Freeboard = - ft

/ 7Acetone (CH3OO0CH3)_Sampled @ M

313~~3 Bromodichloromethane (BrCHC12 ) _ /VO < 1

L Carbon Tetrachloride (CC14) = NO < IBy : .L

Chloroform (CHCl3) = NN' /

RECEIVED @ LAB : Methylene Chloride (CH2C12) = Q < I

3 / 3 / 83 1,1,1-Trichloroethane (CH3CC13) = NQ /

Trichloroethylene (C1CH :CC12 )Notation about appear-ance of the sample : Tetrachloroethylene* (C12C : CC12)

1,2-Dichioroethylene (ClCH :CHCl )

Dibromochloromethane (C1CHBr2) = NU

Isopropyl Alcohol ; also ( CH3CHOHCH3) = /ik' /0


Freon TF (C12FCCF2C1) =

1,1-Dichloroethane (C12CHCH3) = NO

MIMENTS : * Tetrachloroethylene is also known as perchloroethylene . (1) Monitoring specifical-



discharged shall not contain phenols, mercaptans , or other substances in concentrations which



IPPB = PARTS PER BILLION

= LESS THAN ND = NONE DETE DNA = DOES NOT APPLY TR = TRACE

APPROVED

r ~rrr, 519-V

D/031

SSFL ANA STICAL C EMISTRY UNIT

IIIII II II II III IBNAO147652 1

HDMSE00624795


CHEi CAS. AN ALYS IS RESULT S

TO : INDUSTRIAL ENGINEERING D/031 SS12

LOG NO

3-51-83

DATE : 11-Mar-83

FROM : SSFL ANALYTICAL CHaIISTRY D/539 5511 PHONE : 544 7

REFERENCE : LOG BK '83 PAGE 36

SAMPLED FROM! : AI inlet to R2 lt 9 :10AM AM /Ml ON : 3-Mar-83

CONSTIT't1ENTRESULTS

I1NCENTRATION3MIT /1

ptl at 25° C 8 .1 pH twit to 9 unit s

Total Dissolved Solids on Drying at 180a C 535 950

Temperature of Water 10 .8 3T .8 ° C

C:iloride 39 150


Settleable Solids 0 .2 otl/l 0.3 ml/1

PCD at 20' C 2 60Grease and Oil < 1 15

Residual Chlorine < 0.04 0. 1

Surfactants as MBAS < 0.01 0. 5

Sulfate 178 300

Total CItromi= 0 .007 0 .01

Fluoride 0 .3 1 . 0

Boron < 0 .2 1.0

T+:-bidity 12 (5 )

Phertols < 0 .001 (4 )

MUr c :tptall s 0 .6 (4 )

Cyanide <0 .001

( ;l F :Iter d with'hi n,an GF'C ptuk - .

(2) Faltered with uhatr,3r. GF'C papt'r and dried at 1030 to 1050 C .

(Ii) Lin, tat ion not rc, t1ired to t d_trin rainfall .

(,) Rates discharged ;hall not conln1n phenol mercaptans, or other substances in

COtlcen t nit Toni which VOL-,!,! irtp . it td~, t color, odors, foaminc or or her ohjecl -

ioc . . I le charnc :erii C s to recc tvin , u .ttet- . . .or any substance in concentration

.o .\ic to human, animal , plant or fit lift' .

(5) >iaste= discharged shall not increase the nn:tural turbidity of the receivinc

caters at the time of discharge .

r iAppro'•'c

FL A'v'1i ]C4L CF! . . 'ISTRY 17

ft

IIIII II II II III IBNA0147652 2

HDMSE00624796

EFFLUENT DISCHARGE REPOR T

(5 i

Four 6rc_ti


LOG NO

3-46-83to

3-50-8 3

TO :- - Industrial Enaineerina IEPT . /G1i0UP 031

J 4 • TL MA TrICaL C RY. XPT . 539 P3MMW 5"7

RMFUUM : _ LB- 83 -p . 36 DATE: 11-Mar-8 9

SA(PL =13 CATION : SRiPI,B FRIES R2 • 9 :25AM ON 3-Mar-8 3

CONSTTItme R1'4ULTS/1

NCE f RATIO N/1

pH at 25' C 7 .8 pH wait to Units

Total Dissolved Solids on Drying at 180 ' C 124 950

ure of plater 10 .3 37.8' C

Chloride 10 150


Settleable Solids < 0 .1 ml/1 0.3 al/1

BCD at 20'C 1 60Grease and Oil 2 15

Residual Chlorine < 0 .04 0 .1

Surfactants as NBAS < 0 .01 0.5

Sulfate 31 300

Total Cnramium 0 .012 0 .01

Fluoride 0 .3 1 . 0

Boras < 0,2 1.0

Turbidity 15 NTU (5 )

Sewage Treatment Plant Influent BCD at 20 C 461 (4 )Sewage Treatment Plant Efflneat BOD at 20 C 3 (4 )

Sewage Treatment Plant Influent Suspended Solids 2886 (L )

Sews-re Treatment Plant E,, fluent Swpended Solids 16 (4 )

Filtered with Whatman GF/C paper .

Filtered with Whatman GF/C paper and dried at 103°to 105° C.

Limitation not required to be wt taring rainfall.

The sverage final ef.'luent concentrations shall not exceed 15% by weight ofthe average sewage treatment pmt influent concentrations of BOD5 20'C andsuJ-,~ende-3 o1idz dur-I ng periods of ar.so serge .

.asses discharged shall not increase the na~~al trbiditf of the receiviagveters at t e ttne of djsc.7Arre .

N,f &43a. &uMAXACER SSFL ARALF T- Z% . LFMISTRI 7

IIIII II III I II IBNA0147652 3

HDMSE00624797