Brownfield Redevelopment Assessment Report for Tamarack City … · 2016-09-02 · TriMatrix . f~...

~ TriMatrix ~~ Labotalorles, Inc.

ANALYTICAL REPORT

IDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 13:00

ERD- Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10:00

Sample #: 307102 Sample ID: SS-4

Matrix: Soil

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chern Citation -- ---- -- -- --- ----- ---- -- - ----- ----- --------- ---------- --- - --- - ---- --- -- --- -- -Percent Solids 97 0.1 % 06/07/02 GEH SW-846 3550B

Page 10

This r~port <hoi! not be reproduced ~X<~pl in (ull, without written ;ttJthorit.Hinnnfliii\ l:u rix Labur,r turin, In<. lndividu"l <.unple rc.<ults rcbtc only to the >~ mpl~ t<'< tt'd .

5560 Corpnrare Excha ng~ Cuurt SE o Grand Rapids, wll -1Y5 12 o (616) 975 -4500 o Fax (6 16) 942-74 6.1

~ TriMatrix f~ Labomlorlcs, Inc.

ANALYTICAL REPORT

.IDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02@ 13:00

ERD-Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10:00

Extracted: Sample #: 307102 Anal yzed: 06/13/02 by DLVV Sample ID: SS-4 Ref. Citation: USEPA- 82608

Dilution Factor: 1 Analytical Batch: 187179

Matrix: Soil QC Batch: 075930 - 113

Analytical Quantitation MDEQ Plus List Volatiles Result Limit

CAS Number USEPA Method 5035/8260 (rng/kg dry) (rng/kg dry)

630 - 20 - 6 1,1 , 1,2 - Tetrachloroethane <0 .10 0.10 71-55-6 1,1,1-Trichloroethane <0 .050 0.050 79 - 34-5 1,1,2,2-Tetrachloroethane <0.10 0.10 79-00-5 1,1,2-Trichloroethane <0.050 0.050 75-34-3 1,1-Dichloroethane <0 . 050 0.050 75-35-4 1,1- Dichloroethylene <0.050 0.050 87-61-6 1,2,3 - Trichlorobenzene <0.25 0.25 96 - 18-4 1,2,3-Trichloropropane <0.10 0.10 120-82-1 1,2,4 -Trichlorobenzene <0.25 0.25 95 - 63-6 1,2,4-Trimethylbenzene <0.10 0.10 96 - 12 - 8 1,2-Dibromo-3- <0.25 0.25

chloropropane 106-93 - 4 1,2 - Dibromoethane <0 . 050 0.050 95 - 50 - 1 1,2 -Dichlorobenzene <0 .10 0.10 107 - 06 - 2 1,2-Dichloroethane <0 . 050 0.050 156 - 59-2 cis-1,2 - Dichloroethene <0.050 0.050 156-60 - 5 trans-1,2-Dichloroethene <0.050 0 . 050 78-87 - 5 1,2-Dichloropropane <0.050 0.050 108 - 67-8 1,3,5 -Trimethylbenzene <0.10 0.10 541-73-1 1,3 -Dichlorobenzene <0.10 0 . 10 10061-01- 5 cis-1,3 - Dichloropropene <0.050 0.050 10061 - 02-6 trans-1,3 - Dichloropropene <0.050 0.050 110 - 57-6 trans - 1,4-Dichloro- <0 .050 0.050

2-butene 106 - 46-7 1,4-Dichlorobenzene <0 . 10 0.10 78 -93-3 Methyl Ethyl Ketone <0.25 0.25 591 - 78-6 2-Hexanone <0.25 0.25 91-57-6 2 - Methylnaphthalene <0.25 0.25 67-64-1 Acetone <0.75 0.75 108 - 10-1 4-Methyl - 2-Pentanone <0. 25 0.25 107 - 13-1 Acrylonitrile <0.25 0.25 71-43-2 Benzene <0.050 0 .0 50 108 - 86-1 Bromobenzene <0.10 0 . 10 74 - 97-5 Bromochloromethane <0 .10 0 .1 0

Page 11

T hi, l(' jlOrt sh.tllnot be «produced <X<cjH in full , without written auduui1.1t ion of"Tr i~l.ltl ix [ ,[llu.uori~,. Inc. lndi,·idu:rl >ample '~'"' " rd,te onlr w the ~.Hnplc tc1tcd.

5560 Corpora tl' Exd1;1nge Cou rt S E • Gr.llld Rapids, ~·II 49512 • (6 16) Y75-4500 • Pax (ll l ll) ')4 2-746]

~ TriMatrix ~~ La borillolies, Inc.

ANALYTICAL REPORT

IDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 13:00

ERD-Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02@ 10:00

Extracted: Sample#: 307102 Analyzed : 06/13/02 by DLW Sample ID: SS-4 Ref. Citation: USEPA-8260B




CAS Number USEPA Method 5035/8260 (mg/kg dry) (mg/kg dry)

75-27-4 Dichlorobromomethane <0. 10 0.10 75 - 25-2 Bromoform <0.10 0.10 74-83 - 9 Bromomethane <0 . 25 0.25 75 - 15-0 Carbon Disulfide <0 . 25 0.25 56-23-5 Carbon Tetrachloride <0.050 0.050 108 - 90-7 Chlorobenzene <0.050 0.050 75-00-3 Chloroethane <0.25 0.25 67 - 66 - 3 Chloroform <0.050 0.050 74 - 87-3 Chloromethane <0.25 0.25 124-48-1 Chlorodibromomethane <0.10 0 . 10 74 - 95-3 Dibromomethane <0 .10 0 .1 0 75 - 71-8 Dichlorodifluoromethane <0.25 0.25 60-29-7 Ethyl Ether <0.25 0. 25 100 - 41 -4 Ethylbenzene <0 .050 0 . 050 67-72-1 Hexachloroethane <0.10 0.10 98 - 82-8 Isopropylbenzene <0 . 10 0.10 13 6777-61-2 Xylene, Meta & Para <0.10 0.10 74 - 88 - 4 Iodomethane <0.10 0.10 1634-04-4 Methyl(tert)butyl Ether <0.25 0.25 75 - 09-2 Methylene Chloride <0.25 0.25 91-20 - 3 Naphthalene <0.25 0 .25 104 -51 - 8 n - Butylbenzene <0 .25 0.25 103 - 65-1 n - Propylbenzene <0 .10 0 .10 95-47-6 o-Xylene <0.050 0.050 99-87 - 6 4 - Isopropyltoluene <0.25 0.25 135 - 98-8 sec - Butylbenzene <0.25 0.25 100 - 42-5 Styrene <0.050 0.050 98-06-6 tert-Butylbenzene <0.25 0.25 127 - 18-4 Tetrachloroethene <0.050 0.050 109-9 9-9 Tetrahydrofuran <1. 0 1.0 108-88 - 3 Toluene <0.050 0.050 79 - 01-6 Trichloroethene <0.050 0.050 75 - 69-4 Trichlorofluoromethane <0.25 0.25 75-01 - 4 Vinyl Chloride <0 .10 0 . 10

Page 12

Thi, r~pnrt ,holl not[,., rcprotltl<·ed e~«pt in full , wirhnut written .uu lturit.uion o(' liil\buix Libm.llulicl, llll . lnJividu;ll ,,unplc '"""" •dol<' onlr ro 1hc ;.nnple 1<'\ ted.

55 60 Corporan· Exchange Cnur t SE • Grand Rapids, M I 495 12 • (61 G) 975-4500 • Fax (6 I G) 942-7463

~ TriMatrix f~ Laboratories, In c.

ANALYTICAL REPORT

IDEQ Submittal #: 36024-1 Project: Tamar ack City Stamp Mi l l Sa mp l e d: 06 / 04/02 @ 13:20

ERD - Superfund, Lansing Samp ler: Spielbe r g Submittal: J une 4 , 2002 Soils Rece ived: 06/06/02 @ 10 : 00

Sample # : 307103 Sa mple ID : SS - 5

Matr ix: Soi l

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chem Citat i on - - - - -- - -- -- -- - -- - -- - - --- - ------ ---- - --- - - -- - - -- - -- -- - - - -- - -- - - -- -- --- --- -- -- -Percent Solid s 93 0. 1 % 06/ 07/ 02 GEH SW - 846 35 50B

Page 13

T his report > l~;r ll nnt 1..: rcprnduted except in fttll, widtntH wriuen audtoriz.uiun of Tri.\ l.urix l.1Lur.nnrin, Inc. lndividuJI sample resulh rdJte onlr to thL· s.unplc rc~ t cd .

5560 Corpora te txchang~ Court SE • Grand Rapid ~. M I 4~ 5 1 2 • (()I ()) 975-i'f500 • Fax (6 1 G) 94 2-7 46 3

~ TriMatrix ~· Laborntories, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 13:20


Extracted: Sample #: 307103 Analyzed: 06/13/02 by DLW Sample ID: SS-5 Ref. Citation: USEPA- 8260B


Matrix: Soil QC Batch: 075930-113



630-20-6 1,1,1,2-Tetrachloroethane <0.10 0.10 71 - 55-6 1,1,1-Trichloroethane <0 .050 0.050 79-34 -5 1,1,2,2-Tetrachloroethane <0. 10 0.10 79-00-5 1, 1,2-Trichloroethane <0 .050 0.050 75-34-3 1,1- Dichloroethane <0. 050 0.050 75-35 - 4 1,1-Dichlo roethylene <0 .050 0.050 87 - 61 - 6 1, 2,3-Trichl orobenzene <0.25 0.25 96 - 18-4 1, 2,3 - Trichloropropane <0.10 0.10 120-82 - 1 1,2,4-Trichlorobenzene <0 .25 0 . 25 95-63 - 6 1,2,4-Trimethylbenzene <0 . 10 0.10 96 - 12-8 1,2 - Dibromo-3- <0.25 0.25

chloropropane 106 - 93-4 1,2 - Dibromoethane <0.050 0.050 95-50 - 1 1,2-Dichlorobenzene <0. 10 0.10 107-06 -2 1,2 - Dichloroethane <0. 050 0.050 156-59 - 2 cis-1,2-Dichloroethene <0.050 0.050 156-60-5 trans-1,2 - Dichloroethene <0.050 0.050 78-87 - 5 1,2 - Dichloropropane <0. 050 0.050 108-67 - 8 1,3,5-Trimethylbenzene <0 . 10 0.10 541-73 - 1 1,3 - Dichlorobenzene <0. 10 0.10 10061 - 01-5 cis-1,3-Dichloropropene <0.050 0.050 10061-02-6 trans-1,3 - Dichloropropene <0.050 0.050 110-57 - 6 trans - 1,4-Dichloro- <0.050 0.050

2 -butene 106-46 - 7 1,4 - Dichlorobenzene <0.10 0.10 78 - 93-3 Methyl Ethyl Ketone <0.25 0 . 25 591-78-6 2-Hexanone <0 .25 0. 25 91-57 - 6 2 - Methylnaphthalene <0.25 0 . 25 67 - 64-1 Acetone <0.75 0 .75 108-10-1 4-Methyl -2- Pentanone <0.25 0.25 107-13 - 1 Acrylonitrile <0 .25 0.25 71-43 - 2 Benzene <0.050 0.050 108 - 86 -1 Bromobenzene <0.10 0.10 74-97 - 5 Bromochloromethane <0 . 10 0 . 10

Page 14

This r<·pun , h,tll llt>l h~ r~pwduc~d cxcqn in full , wirhuur wrillen .unhnri101ion ofTr i;<. l ,mi~ L1bor.uuri~,. IrK. lllclividual '"mplc r~suiiS rda1c unl)' 10 1h~ ,.unplc IC\t~d .

5560 Corporate: Exchange Cuu rt Sr. • Gr~nd RapiJs, 1\·11 495 12 • (C> I G) 'J75-4500 • Fax (6 1 G) 942-7463

~ TriMatrix f~ Lilbotalorlcs, Inc.

ANALYTICAL REPORT

IDEQ Su bmitt a l #: 36024 - 1 Project: Tamarack Ci ty Stamp Mi l l Sampled: 06/04 /02 @ 13 :20

ERD - Supe rfund, La n s i ng Sampler : Spi elberg Submittal: June 4, 2002 Soi ls Received: 06 / 06/02 @ 10 : 00

Extracted : Samp l e # : 307103 An alyzed: 06/13/02 by DLVV Sample ID: SS-5 Ref . Ci tat i on: USEPA- 8260B

Di l ution Factor: 1 Ana l ytic a l Batch : 18717 9

Ma trix: Soi l QC Batch : 075930 - 113

Analytica l Quantitation MDEQ Plus List Volatiles Result Li mit

CAS Number USEPA Method 5035 / 82 6 0 (mg/kg dry ) (mg/kg dry)

75 - 27 - 4 Dich lorobromomet hane <0. 1 0 0 . 10 75-25-2 Bromoform <0.10 0 . 10 74-83-9 Bromomethane <0.25 0 . 25 75 - 15-0 Carbon Disulfide <0 . 25 0.25 56 - 2 3-5 Carbon Tetrachl oride <0 . 050 0.050 108-90 - 7 Ch lorobenzene <0.050 0.050 75 - 00 - 3 Chl oroethane <0 . 25 0 .25 67 - 66- 3 Chlo roform <0 . 050 0.050 74 - 87 - 3 Chloromethane <0.25 0. 25 124 - 48-1 Ch lorodibromomethane <0.10 0 . 10 74 - 95-3 Dibromome tha n e <0 . 10 0 . 10 75 - 71 - 8 Di c h lorodif l uoromethane <0 . 25 0 . 25 60- 2 9-7 Ethyl Ether <0.25 0.25 100 - 41 - 4 Ethyl benzene <0 .050 0.050 67 - 72 - 1 Hexachloroe thane <0 . 1 0 0 .10 98-82- 8 Iso propyl benzene <0.10 0 . 10 136777 - 61 - 2 Xylene, Meta & Para 0 . 12 0 . 1 0 74 - 88 - 4 Iodomethane <0. 10 0 .1 0 1634-04 - 4 Me t hyl(tert)butyl Ether <0 . 25 0 . 25 75 - 09 - 2 Methylene Chloride <0 . 25 0 . 25 91 - 20-3 Naphthale ne <0.25 0 . 25 104 - 5 1- 8 n-Butylbenzene <0 . 25 0 .25 103 - 65-1 n - Propylbenzene <0 . 10 0.10 95 - 47-6 o - Xylene 0.089 0 . 050 99-87-6 4 - Isop ropyltoluen e <0.25 0 . 25 135 - 98-8 sec- Butyl benzene <0. 25 0.25 100 - 42-5 Styrene <0 . 050 0 . 050 98-06-6 tert-Butyl ben zene <0 . 25 0.25 127 - 18 - 4 Tetrachl oroeth ene <0.050 0 . 050 109 -99 - 9 Tetrahydrofura n <1. 0 1 . 0 108 - 88-3 Toluene 0.070 0 . 050 79-01-6 Trichl oroethene <0 . 050 0 . 050 75 - 69 - 4 Trichlorofluoromethane <0.25 0 . 25 75-01 - 4 Vinyl Chloride <0 . 10 0.10

Page 15

I hi< rcpor! >hall nut be rq>roduc:ccl cxcq>t in lidl, without wrin<n audwlit.H ionor'lr i~btrix L!b01.uoric>. Inc. lndil' id u :~l sample rc,u lt ' rd.uc unlr to dw >:tmplc tc,rcd.

5560 Corporate Exchange C out r SE • Grand R;lp id.,, M l !J9512 • (6 16) 975-4 500 • F.rx (6 16) 9!J2-7463

~ TriMatrix ~~ Laborator ies. Inc.

ANALYTICAL REPORT

':IDEQ Submittal #: 36024 -1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 13:30

ERD-Super fund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10:00

Sample # : 307104 Sample ID: SS-6

Matrix : Soil

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chern Citation - -- -- - - -- - -- - -- - - - -- - -- -- ---- --- --- ---- ----- - - -- - - - -- - - -- - -- - - -- --- --- ---- ---Percent Solids 91 0.1 % 06/07/02 GEH SW-846 3550B

Page 16

Thi< •~pon shall not h~ reprucluccd except in fu ll, without wr iu~n .tud1Clri7.uinn nf Trilvbuix Lalmr.ut>rk>. Int. l n dividu :~ l ,.tmplc rl'sull< rcb tc un ly to the ,.un plc tc, tcd.

556 0 Corpo rat <' Excha nge Courr SE • Gra nd Rapi d s, lvll -195 12 • (GIG) ~75-t\ 5 00 • Fax (G I G) 94 2-74GJ

~ TriMatrix f~ l aboratories, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024 - 1 Project: Tamarack City Stamp Mill Sampled: 06/04 / 02 @ 13:30

ERD- Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soi l s Received: 06/06/02@ 10:00

Extracted: Sample#: 3 07104 Analyzed: 06/13/02 by DLVV Sample ID: SS-6 Ref. Citation: USEPA- 82608

Dilution Factor: 1. 03 Analytical Batch: 187179




630 - 20-6 1 ,1,1 ,2-Tetrachloroethane <0.10 0.10 71-55-6 1,1,1- Trichloroethane <0.052 0.052 79 - 34-5 1,1,2,2 - Tetrachloroethane <0 . 10 0.10 79 - 00-5 1,1,2-Trichloroethane <0.052 0.052 75 - 34 - 3 1,1 - Dichloroethane <0.052 0.052 75 - 35-4 1,1 - Dichloroethylene <0.052 0.052 87 - 61-6 1,2,3 - Trichlorobenzene <0.26 0.26 96- 1 8-4 1,2,3- Trichloropropane <0.10 0 . 10 120-82-1 1,2,4- Trichlorobenzene <0.26 0 . 26 95 - 63-6 1,2,4-Trimethylbenzene <0 . 10 0 . 10 96-12-8 1,2-Dibr omo - 3 - <0 .26 0 . 26

chloropropane 106 - 93-4 1,2-Dibromoethane <0 . 052 0 . 052 95 - 50-1 1,2-Dichlorobenzene <0 . 10 0.10 107-06 - 2 1,2 - Dichloroethane <0.052 0 . 052 156 - 59-2 cis - 1,2-Dichloroethene <0.052 0 . 052 156-60 - 5 trans - 1,2-Dichloroethene <0.052 0.052 78 - 87-5 1,2 - Dichloropropane <0.052 0.052 108-67 - 8 1,3,5- Trimethylbenzene <0.10 0.10 541 - 73 -1 1,3-Dichlorobenzene <0.10 0.10 10061-01-5 cis - 1,3 - Dichloropropene <0.052 0.052 10061-02 - 6 trans-1 ,3 - Dichloropropene <0.052 0.052 110 - 57-6 trans-1,4-Dichloro- <0 . 052 0.052

2-butene 106- 46-7 1,4 - Dichlorobenzene <0.10 0 . 10 78-93 - 3 Methyl Ethyl Ketone <0.26 0.26 591 - 78-6 2 - Hexanone <0 .26 0.26 91 -57-6 2 - Methylnaphthalene <0.26 0.26 67 - 64-1 Acetone <0 . 77 0 . 77 108-10 - 1 4 - Methyl - 2-Pentanone <0.26 0.26 107 - 13-1 Acrylonitrile <0.26 0 . 26 71 -43 -2 Benzene <0.052 0.052 108 - 86-1 Bromobenzene <0. 10 0.10 74 - 97 - 5 Bromochloromethane <0.10 0.10

Page 17

Thi< rcpntt shall nut be reprodll<ed exwpl in fu ll, wit hour written .tuthurit.uion of'lri~ t.u o ix L:Ihor.tturie<, lm. lndil'idual ,,11nple rc<ttlt< tcl:uc only ru the " 'mplt· te\lt'd ,

5560 Corpora r.: Exchange Coun S£ • G ranJ Rapids, ~·11 1195 1 2 • (GI G) 975 ·4500 • F.tx (616) 942-746.>

~ TriMatrix f~ Laboralories, Inc.

-------------------------------------------------------ANALYTICAL REPORT



Extracted: Sample #: 307104 Ana lyzed: 06/13/02 by DLW Sample ID: SS-6 Ref. Citation: USEPA-8260B





75 - 27-4 Dichlorobromomethane <0.10 0.10 75 - 25-2 Bromoform <0 .10 0 . 10 74-83 - 9 Bromomethane <0.26 0.26 75 - 15-0 Carbon Disulfide <0 .26 0.26 56-23-5 Carbon Tetrachloride <0.052 0.052 108 - 90-7 Chlorobenzene <0 .052 0.052 75-00-3 Chloroethane <0. 26 0.26 67 -66 -3 Chloroform <0 . 052 0 . 052 74-87-3 Chloromethane <0.26 0 . 26 124-48-1 Chlorodibromomethane <0.10 0 . 10 74 - 95-3 Dibromomethane <0.10 0.10 75-71 - 8 Dichlorodifluoromethane <0 .26 0.26 60-29-7 Ethyl Ether <0.26 0.26 100 - 41-4 Ethylbenzene <0 . 052 0.052 67-72 - 1 Hexachloroethane <0.10 0.10 98 - 82-8 Isopropylbenzene <0.10 0.10 136777 - 61-2 Xylene, Meta & Para <0.10 0.10 74-88-4 I odomethane <0.10 0 . 10 1634 - 04 - 4 Methyl(tert)butyl Ether <0 . 26 0.26 75-09-2 Methylene Chloride <0.26 0.26 91 - 20-3 Naphthalene <0 .2 6 0.26 104 - 51-8 n-Butylbenzene <0.26 0.26 103-65 - 1 n-Propylbenzene <0.10 0.10 95 - 47-6 a - Xylene <0.052 0.052 99- 87- 6 4-Isopropyltoluene <0.26 0.26 135-98 - 8 sec-Butylbenzene <0.26 0.26 100 - 42-5 Styrene <0 .05 2 0.052 98 - 06- 6 tert-Butylbenzene <0.26 0.26 127-18 - 4 Tetrachloroethene <0.052 0.052 109 - 99-9 Tetrahydrofuran <1.0 1.0 108- 88- 3 To luene <0 . 052 0.052 79-01-6 Trichloroethene <0 . 052 0.052 75-69-4 Trichlorofluoromethane <0.26 0 .2 6 75 - 01-4 Vinyl Chloride <0 . 10 0.10

Page 18

T hi' oqwrr sh.lll nut be repnnlut ed """I'' in l'ull. wirhour wriucn authooitarinn ofToio\l .uoix bbor.uurios, lnl. lndividu;ol o.unple '"''"' ' od :uc nnlr ro rhc ;ample 1<'1«1.

5 560 Cor porare Exch;ll>g<' Cour1 SE • Gra nJ Rap ids, M l 495 12 • (616) 97 5-4 500 • Fax (() 16) ')42-7463

~ TriMalrix f~ Laboratories, Inc.

ANALYTICAL REPORT

'IDEQ Submi t t al # : 36024 - 1

Project: Tamarack Ci ty Stamp Mill Sampl ed: 06/04/02 @ 13 : 25

ERD- Superfund, Lansing Sampl er : Spielberg

Submittal: June 4, 2002 Soi l s Received : 06/06/02@ 10:00

Samp l e #: 307105 Sample ID: SS-7

Matrix: Soi l

Analy tical Quant. Analysis Refer e nce

Result Lindt Unit Date Chern Citatio n Parameter ---- ---- ---- ---------- --- ---------- ---- -- --- ----- - ---- - ---- -- - ---- ----------Percen t Solids 88 0. 1 % 06/07/02 GEH SW - 846 3550B

Page 19

-

Thi' r~port sk•llou>t he reproduced nccpt in 1\oll, widooou wrillell .unhnri1.uinn ofToi~l.uoix Llbor.uori~, , Inc. lndil'idu.ol s.unplc rcsuh;, rd.uc nnl)' to doc ' :111oplc lC<IC<L

5560 Co1 poratc Exchange Coun SF. • Grand Rapids, ivll 49512 • (616) 975-4 500 • Fax (616) 94 2-74 63

~ TriMatrix ~~ tnborillmics, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02@ 13 :25


Extracted: Sample #: 307105 Analyzed: 06/13/02 by DLVV Sample ID : SS-7 Ref. Citation: USEPA-8260B

Dilution Factor: 1.04 Analytical Batch: 18717 9




630 - 20-6 1,1,1 , 2 - Tetrachloroethane <0 .10 0.10 71 - 55-6 1,1,1 - Trichloroethane <0.052 0.052 79 -34 - 5 1 ,1, 2,2-Tetrachloroethane <0. 10 0.10 79-00-5 1,1,2- Trichloroethane <0.052 0.052 75 - 34 -3 1,1- Dichloroethane <0.052 0.052 75-35-4 1,1-Dichloroethylene <0 . 052 0.052 87 - 61-6 1,2,3 - Trichlorobenzene <0 .26 0. 26 96 - 18-4 1,2,3-Trichloropropane <0 . 10 0 . 10 120-82 - 1 1,2,4 - Trichlorobenzen e <0 . 26 0 . 26 95 -63-6 1 ,2,4 - Trimethylbenzene <0.10 0.10 96 - 12-8 1 ,2-Dibromo-3- <0.26 0.26

chloropropane 106 - 93-4 1,2-Dibromoethane <0.052 0.052 95-50-1 1,2-Dichlorobenzene <0 .10 0.10 107-06 - 2 1,2 - Dic hloroethane <0.052 0.052 156 - 59 -2 cis-1,2 - Dichloroethene <0.052 0.052 1 56 - 60-5 trans-1,2-Dichloroethene <0 . 052 0.052 78-87-5 1,2-Dichloropropane <0.052 0.052 108 - 67-8 1,3,5-Trimethylbenzene <0.10 0.10 541 - 73 - 1 1,3-Dichlorobenzene <0 .10 0.10 10061-01-5 cis-1,3-Dichloropropene <0.052 0.052 10061-02- 6 trans - 1,3-Dichloropropene <0.052 0.052 110 - 57 - 6 trans - 1,4-Dichloro- <0.052 0.052

2-butene 106-46-7 1,4-Dichlorobenzene <0.10 0.10 78-93 - 3 Methyl Ethyl Ketone <0.26 0 . 26 591 - 78-6 2 - Hexanone <0.26 0.26 91 -57-6 2-Methylnaphthalene <0.26 0 . 26 67-64 - 1 Acetone <0.78 0.78 108- 10-1 4 - Methyl-2 - Pentanone <0 . 26 0.26 107 - 13-1 Acrylonitrile <0.26 0.26 71-43 - 2 Benzene <0.052 0.052 108-86-1 Bromobenzene <0.10 0.10 74 - 97-5 Bromochloromethane <0.10 0 . 10

Page 20

Tfr i, rq~<1 11 shall not be r~prudul'ed n<ept in full, without wri tten .nulrorii.Hion nfTril.l:wix bbu1.uorie,, llll . Individ ual ' " '"Jllt '"'"I'' rcl.ue nnl)' 10 dw u mpl<' te, ted.

5560 Corpor.tr~ Exchan~<· C outr SE • GranJ Rapids, ~vii 4951 2 • (616) 975-4500 • Fax (616) 94 2-7463

~ TriMatrix ~~ l..a boral01ies, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06 /04/02 @ 13:25

ERD- Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10 : 00

Extracted : Sample #: 307105 Analyzed: 06/13/02 by DLW Sample ID: SS-7 Ref. Citation: USEPA - 8260B

Dilution Factor: 1.04 Analytical Batch: 187179

Matrix: Soil QC Batch: 075930- 113


CAS Number USEPA Method 5035/8260 (rng/kg dry) (mg/kg dry)

75 -27-4 Dichlorob romomethane <0. 10 0.10 75 - 25-2 Bromoform <0.10 0.10 74-83-9 Bromomethane <0.26 0.26 75 - 15 - 0 Carbon Disulfide <0 .26 0.26 56 - 23-5 Carbon Tetrachloride <0.052 0.052 108 - 90-7 Chlorobenzene <0.052 0 . 052 75-00 - 3 Chloroethane <0.26 0.26 67 - 66-3 Chloroform <0.052 0.052 74 - 87-3 Chloromethane <0 .26 0 . 26 124-48-1 Chlorodibromomethane <0.10 0.10 74 - 95-3 Dibromomethane <0.10 0.10 75 - 71-8 Dichlorodifluoromethane <0.26 0. 26 60-29-7 Ethyl Ether <0 . 26 0.26 100-41-4 Ethylbenzene <0.052 0.052 67 - 72-1 Hexachloroethane <0.10 0.10 98 -82 -8 Isopropylbenzene <0. 10 0.10 136777-61 - 2 Xylene, Meta & Para <0. 10 0.10 74-88-4 Iodomethane <0.10 0.10 1634-04 - 4 Methyl(tert)butyl Ether <0.26 0 . 26 75 - 09-2 Methylene Chloride <0.26 0.26 91-20-3 Naphthalene <0.26 0.26 104 - 51 - 8 n - Butylbenzene <0.26 0.26 103 - 65-1 n - Propylbenzene <0 .10 0.10 95-47-6 o - Xylene <0.052 0.052 99-87-6 4-Isopropyltoluene <0.26 0.26 135 - 98-8 sec-Butylbenzene <0.26 0.26 100-42-5 Styrene <0 .052 0.052 98-06-6 tert-Butylbenzene <0.26 0. 26 127 - 18-4 Tetrachloroethene <0.052 0.052 109-99 - 9 Tetrahydrofuran <1.0 1 . 0 108 - 88-3 Toluene <0 . 052 0.052 79 - 01 - 6 Trichloroethene <0 . 052 0.052 75-69-4 Trichlorofluoromethane <0.26 0.26 75-01-4 Vinyl Chloride <0 .10 0.10

Page 21

'I hi ' report •hall nut b~ reproduced t•xcqu in fu ll, wiUlOUl wliu~n .uuhnrit.Hion uf'liil\·lauix Labur.umies, Inc lndividu:ll ."unple rc,ult ' rd:uc only to the s.lmpl~ '"' '""·

5560 Corporal~ Exchange Courr SE • GranJ Rapids , 1\ll l ti'J5 12 • (GIG) 'J75 -4500 • Fax (6 1 (i) 942-7463

~ TriMatrix f~ Laboratories. Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Pro j ect : Tamarac k Ci ty Stamp Mill Sampled: 06 /04/02@ 13:10

ERD- Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10 : 00


Matrix: Soi l

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chern Citation ------ ---- ------ --------- --- -- ----- -- -- --- -- --- --- ---- -- - ---- - ----- --- -- ---- -Percent Solids 95 0.1 % 06/07/02 GEH SW- 846 35508

Page 22

Thi, report shall not he repruduceJ exceJH in ful l. widwtn wriucn .uuhoriz.lliunofTri ,\l:trri' I .thllt .trnrir<, Inc. lnJiviJu.tl ~ample re, ttl t, rda te n11l)' tn tht· ,,tm ple IL'' ted.

5560 Cot por:Hl' Exchang<' Cuun SE • Gr:1 nd Rapids. tvll 495 12 • (6 16) 'J75--i500 • Fax (6 16) 942 -7~6 .1

~ TriMatrix f~ 1~1tJUralorics, Inc.

ANALYTICAL REPORT

MDEQ Submittal # : 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02@ 13:10

ERD- Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received : 06/06/02@ 10:00

Extracted: Sample # : 307106 Analyzed: 06/13/02 by DLVV Sample ID: SS-8 Ref. Citation: USEPA- 8260B





630 - 20-6 1,1,1,2 -Tetrachloroeth ane <0.10 0.10 71-55-6 1,1 ,1 - Trichloroethane <0.052 0.052 79 - 34-5 1,1,2,2 - Tetrachloroethane <0.10 0.10 79-00-5 1,1,2-Trichloroethane <0 .052 0.052 75-34-3 1,1-Dichloroethane <0.052 0.052 75- 35-4 1,1-Dichloroethylene <0 . 052 0.052 87 - 61-6 1,2,3-Trichlorobenzene <0.26 0.26 96 - 18-4 1,2,3-Trichloropropane <0.10 0.10 120-82 -1 1,2,4 - Trichlorobenzene <0 . 26 0 . 26 95 - 63 - 6 1,2,4-Trimethylbenzene <0.10 0.10 96 - 12-8 1,2-Dibromo- 3- <0.26 0.26

chloropropane 106 - 93-4 1, 2-Dibromoethane <0.052 0.052 95-50-1 1, 2 -Dichlorobenzene <0 . 10 0.10 107 - 06-2 1,2 - Dichloroethane <0.052 0.052 156 - 59- 2 cis-1, 2-Dichloroethene <0 . 052 0.052 156-60-5 trans - 1,2-Dichloroethene <0 .0 52 0.052 78 - 87-5 1, 2 - Dichloropropane <0.052 0.052 108 - 67 - 8 1 ,3,5 - Trimethylbenzene <0 .10 0.10 541-73-1 1,3-Dichlorobenzene <0.10 0.10 10061- 01-5 cis-1 ,3-Dichloropropen e <0.052 0.052 10061-02 - 6 trans - 1,3-Dichloropropene <0.052 0.052 110 - 57-6 trans-1,4-Dichloro- <0.052 0.052

2-butene 106-46-7 1,4-Dichloroben zene <0 . 10 0.10 78 - 93-3 Methyl Ethyl Ketone <0 .2 6 0.26 591 - 78-6 2 - Hexanone <0 . 26 0.26 91 - 57-6 2-Methylnaphthalene <0.26 0. 26 67-64-1 Acetone <0 .78 0.78 108-10-1 4 - Methyl-2-Pentanone <0.26 0.26 107 - 13-1 Acrylonitrile <0 .2 6 0.26 71-43-2 Benzene <0 . 052 0. 052 108 - 86-1 Bromobenzene <0.10 0.10 74-97 - 5 Bromochloromethane <0.10 0.10

Page 23

T hi\ r~port shall nm be rcproduc~d <'W<'(H in full. without writt<' n :uuhurit.u inn uf' l'rii'vl.urix Labor.uorie>. hll. lndi"idu:ol '·"""'"'"'"It ' rchue onlr to the •. unple te\l e<l.

5560 Corpor3rc Exchan~;.: Coun SE • C. rand Ra pids, ~·1 1 4 ~ 5 1 2 • (61 6) 975-4500 • Fax (61 6) 942-7463

~ TriMatrix f~ La boratolies, Inc.

ANALYTICAL REPORT


ERD-Superfund, Lansing Sampler: Spielbe rg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10 : 00

Extracted : Sample #: 307106 Analyzed: 06/13/02 by DLVV Sample I D: SS - 8 Ref. Citation: USEPA - 8260B

Dilution Factor: 1 . 04 Analytic al Batch : 1 87179

Matrix: Soil QC Batch: 07593 0 - 113



7 5 - 27 - 4 Dichlorobromomethane <0.10 0.10 75 - 25-2 Bromoform <0.10 0 .10 74 - 83 - 9 Bromomethane <0.26 0 . 26 75 - 15 - 0 Carbon Disulfide <0.26 0 . 26 56 - 23- 5 Carbon Tetrachloride <0.052 0 . 052 108-90-7 Chl orobenzene <0 . 052 0 . 052 75 - 00-3 Chloroethane <0 . 26 0 . 26 67 - 66 - 3 Chlorofo r m <0.052 0 . 052 74 -87 - 3 Chloromethane <0.26 0.26 124 - 48 - 1 Chlorodibromomethane <0 . 10 0 . 10 74 - 95 - 3 Dibromomethane <0. 10 0 . 10 75 - 71-8 Dichl orodifluoromethane <0.26 0.26 60 - 29-7 Ethyl Ether <0 . 26 0 . 26 100 - 41 - 4 Ethylbenzene <0.052 0.052 67- 72-1 He xachl oroethane <0.10 0.10 98 - 82 - 8 Isopropylbenz ene <0 . 10 0.10 136777-61 - 2 Xylene, Meta & Para <0.10 0. 10 74 - 88 - 4 Iodomethane <0.10 0.10 1634-04 - 4 Meth yl(tert)butyl Ether <0 . 26 0.26 75 - 09- 2 Methylene Chl oride <0 . 26 0 . 26 91- 20 - 3 Naphthalene <0.26 0. 2 6 104 - 51-8 n - Butylbenzene <0 . 26 0 . 26 103-65- 1 n - Propylben zene <0.10 0 . 10 95 - 47-6 a- Xylene 0.071 0.052 99 - 87-6 4 - Isopropyltoluene <0 . 26 0.26 135 - 98-8 sec - Butylbenzene <0 . 26 0 . 26 100-42 - 5 Styrene <0 . 052 0.052 98 - 06-6 tert-Butylbenzene <0.26 0.26 127 - 18 - 4 Tetrachloroethene <0.052 0 . 052 109-99- 9 Tetrahydrofuran <1. 0 1 . 0 10 8 - 88-3 Toluene 0.052 0.052 79 - 01 - 6 Trichloroethene <0.052 0. 052 75 - 6 9 - 4 Trichl orofluoromethane <0 . 26 0 . 26 75-01 - 4 Vinyl Chloride <0.10 0.10

Page 24

T hi, report slr ~ ll not he rcp11,J ucrJ <XlCfH in full . wid10t11 wt itr<"n .uuhoriz~tiun ur-I i-i /\1.urix I ahnr.u orie<, Inc. lnJ iviJtul >.unplc rclult , rd:ut' olll)' to eire s.tmplc t<>l<'<l.

5560 Corp o rat e Excha nge.: Conti SE • C. r.lll d Ra pid>,lvl l4'J5 12 • (ll l ll) 'J75-4500 • r:ax (6 16) 'J t12-7463

~ TriMatrix f~ Labo ra lories, In c.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-~

Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 13:45 ERD-Superfund, Lansing Sampler: Spielberg

Submittal: June 4, 2002 Soils Received: 06 /06/ 02 @ 10:00

Sample #: 307~07

Sample ID: SS-9

Matrix: Soil

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chem Citation ------ ----- ------- ------- --- --- --- - -- ------- ------ -- -- -- - - - -- - --- ----- --- -- --Percent Solids 92 0.1 % 06/07/02 GEH Svl-846 3550B

Page 25

Thi' r~pnrt shall not lw r~prmhK~d ~\ccpt in lirll. without wrill<'n .unlrnrit.n ion nfTri1\ btrix Labor.noriel, Inc. lndil'idu:~ l ,, ,llnple ICitdt < rchtL· nnly w the ,,tnlple lC\tCd.

S560 Co rpora n· Exchange Court SE • Gr.md Ra pids, t\•11 195 11 • (GIG) ~75 -1 500 • Fax (6 16) 942-74G3

ANALYTICAL REPORT

MDEQ Submitta l #: 36024-1 Projec t: Tamarac k Ci ty Stamp Mill Sampled: 06/04 / 02 @ 13:45

ERD - Superf und , Lans i ng Sa mpler: Spi e l berg Submittal : June 4 , 2002 So i l s Received: 06/06/02 @ 1 0:00

Extracted : Sample #: 307107 Analyzed : 06/1 4/02 by DLVV Samp l e ID : SS- 9 Ref. Ci tat i on: USEPA - 8260B

Dilu tion Factor : 1 . 01 Ana l ytica l Ba t ch: 187270

Mat rix: Soil QC Bat c h : 075930 - 114



630 - 20 - 6 1,1,1,2-Tetrachloroethane <0.10 0.10 71 - 55 - 6 1,1,1-Tri c h loroethane <0. 051 0 . 051 79- 3 4 - 5 1 ,1,2,2 - Tetrachloroethane <0 . 10 0.10 7 9 - 00-5 1 , 1, 2 - Tri c hloroethane <0 .051 0 . 051 75 - 34 - 3 1 ,1 - Dich loroethane <0.051 0 . 0 51 75-35-4 1 , 1-Dic h loroethylene <0 . 051 0.051 87- 61-6 1,2 , 3- Trich lorobenzene <0 . 25 0. 25 96 - 18 - 4 1 , 2,3-Trichlor opropane <0.10 0.10 120 - 82 - 1 1,2 , 4 - Tri chl oroben zene <0.25 0.25 95 - 63 -6 1 ,2, 4 -Trimethyl be nzene <0.10 0 . 10 96 - 12 - 8 1 ,2-Dibromo - 3- <0.25 0.25

c h loropropane 106 - 93 - 4 1,2 - Dibromoethane <0.051 0 . 051 95 - 50 - 1 1 , 2 - Dichloroben zene <0 . 10 0.10 107-06-2 1,2-Dichloroe t hane <0 .051 0.051 156 - 59 - 2 cis - 1 , 2 - Dich l oroethene <0.051 0 . 051 156 -60-5 trans - 1,2-Dichloroethen e <0.051 0 . 051 78 - 87 - 5 1,2 - Dic h l oropropane <0 . 051 0 . 051 108 - 67 - 8 1,3 , 5 - Trimethylben zene <0 .10 0. 1 0 541 - 73-1 1 ,3-Dichl orobenze ne <0 .10 0.10 10061-01 - 5 cis-1,3 - Dich loropropene <0.051 0.051 1 0061-02 - 6 t r a ns - 1 ,3 - Dichl o r opropen e <0 .051 0. 051 110 - 57 - 6 tra ns - 1,4-Dichl oro- <0.051 0.051

2-buten e 106 - 46-7 1 ,4 - Dichlor oben zene <0.10 0.1 0 78 - 93 - 3 Methyl Ethyl Ketone <0.25 0.2 5 591 - 78 - 6 2 - He xanone <0 . 25 0 . 25 91-57 - 6 2-Methyln aphthalene <0.25 0 . 25 67 - 64 - 1 Acetone <0 .7 6 0.76 108 - 10 - 1 4 - Met hyl-2 - Pentanone <0.25 0 . 25 107 - 13 - 1 Acrylonitrile <0.25 0.25 71 - 43-2 Benzene <0.051 0.051 108 - 86- 1 Bromobenzene <0 . 10 0.10 74 - 97 - 5 Bromochloromethane <0.10 0.10

Page 26

TJ.i, rcpnr1 >hall not he reproduced except in fu ll, without "'' iucn .unl10riz.uiun uf Trilll:tt ri' l .thclr.llc ll ic<, Inc. lnJ i\' idual >Jmpl< '""tl' ' rd~ t<' cllll)' to the \J illpk· tt'>ted.

5560 Corpor~ rc Exchange Cou rt S E • C rand Rap id s, ~vi i4'J 5 1 2 • (tl l 6 ) 975-4500 • F.1x (6 1()) 'J42-74tlj

~ TriMatrix ·~ L<1boralories, Inc.

ANALYTICAL REPORT


ERD - Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10:00

Extracted: Sample #: 307107 Analyzed: 06/14/02 by DLVV Sample ID: SS-9 Ref. Citation: USEPA- 8260B


Matrix : Soil QC Batch: 075930-114

Analytical QuantitatioMDEQ Plus List Volatiles Result Limit


75 - 27-4 Dichlorobromomethane <0. 10 0.10 75-25-2 Bromoform <0.10 0.10 74-83 - 9 Bromomethane <0 . 25 0. 25 75- 15 - 0 Carbon Disulfide <0.25 0 . 25 56-23-5 Carbon Tetrachloride <0.051 0.051 108-90 - 7 Chlorobenzene <0. 051 0.051 75-00-3 Chloroethane <0 .25 0.25 67-66 - 3 Chloroform <0.051 0.051 74-87-3 Chloromethane <0 . 25 0.25 124-48 - 1 Chlorodibromomethane <0 .10 0.10 74-95- 3 Dibromomethane <0.10 0.10 75-71-8 Dichlorodifluoromethane <0.25 0.25 60 - 29- 7 Ethyl Ether <0 .25 0.25 100-41-4 Ethylbenzene <0.051 0.051 67 - 72-1 Hexachloroethane <0 .10 0 . 10 98-82 - 8 Isopropylbenzene <0.10 0.10 136777 -61 -2 Xyl ene, Meta & Para <0. 10 0.10 74-88 - 4 Iodomethane <0 .1 0 0. 10 1634-04-4 Methyl(tert)butyl Ether <0.25 0.25 75 - 09 - 2 Methylene Chloride <0 .25 0.25 91-20- 3 Naphthalene <0 .25 0 . 25 104-51 - 8 n - Butylbenzene <0 .25 0.25 103 -6 5-1 n-Propylbenzene <0.10 0.10 95-47-6 a-Xylene <0.051 0 . 051 99-87 - 6 4 - Isopropyltoluene <0.25 0.25 135 - 98-8 sec- Butylbenzene <0.25 0.25 100-42 - 5 Styrene <0 .051 0 . 051 98 - 06-6 tert-Butylbenzene <0.25 0.25 127-18- 4 Tetrachloroethene <0.051 0.051 109-99-9 Tetrahydrofuran <1.0 1.0 108-88-3 Toluene 0.051 0.051 79-01 -6 Trichloroethene <0.051 0 . 051 75 - 69-4 Trichlorofluoromethane <0.25 0.25 75 - 01 - 4 Vinyl Chloride <0 .10 0.10

Page 27

n

Thi; rcporl •h~ ll no 1 he reproduced <'X<<'Ill in full . wi1l.out wr iucn .nuhuriz:uinn of"li-io\l.utix L•bor.uor i ,·~. Inc Individual >J IIlpi<' '"'"" ' rd.uc nuly ru rh,· s.1mpl~ tc,tcd.

5560 Corpor~t c Exchange C ourt S E • Grand Rapid ,, lvi i 4'J5 12 • ((, 16) 9 75-4500 • foa x ((1 16) 94 2-7463

~ TriMatrix ~~ 1 ~1homtor ies, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Proj e c t: Tamara c k City Stamp Mill Sampled : 06/04/02 @ 13:55

ERD-Superfund, Lansing Sampler: Spi elberg Submittal: June 4, 2002 Soils Received: 06/06/02@ 10:00

Sample #: 307108 Sample ID : SS-10

Matrix : Soil

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chern Citation

-- ---- ----- --- ------- ---- --- ----- -- --- ----- - -- -------- -------- ---------- -----Percent Solids 96 0.1 % 06/07/02 GEH SW-846 35508

Pag e 2 8

T h is report shall nur be reproduced except in fu ll, with nut wri ucn .nrd wrizatiun ufT ril. l:tllix Lahor.uorics, lnr. lndiviJuol ,,unplc rc"rl t> rd ate n u lr to the , ,rmplc tl',t<d.

5560 Corporarl' Exchange Court SE • Grand Rapids, ~vi i 495 12 • (il I 6) 975-4500 • Fax (il 1 6) 'J42-71tGJ

~ TriMatrix ~~ Lilbomtories, Inc.

ANALYTICAL REPORT


ERD-Superfund, Lansing Sampler: Spielberg Submittal: June 4 , 2002 Soils Received: 06/06/02 @ 10:00

Extracted: Sample #: 307108 Analyzed: 06/14/02 by DLVV Sample ID : SS-10 Ref . Citation : USEPA-8260B

Di lution Factor: 1 Analytical Batch: 187270

Matrix : Soil QC Bat ch: 075930 - 114



630 - 20 - 6 1,1,1,2 - Tetrachloroethane <0. 10 0 . 10 71 - 55-6 1 ,1,1-Trichloroethane <0 . 050 0.050 79 - 34-5 1,1,2, 2-Tetrachloroethane <0 . 10 0. 10 79 - 00-5 1,1,2 - Trichloroethane <0. 050 0 . 050 75-34 - 3 1, 1-Dichloroethane <0.050 0.050 75 - 35-4 1, 1 - Dichloroethylene <0 .050 0.050 87-61 - 6 1,2,3- Trichlo robenzene <0 .25 0.25 96 - 18 - 4 1,2,3 - Trichloropropane <0 . 10 0 . 10 120 - 82 - 1 1, 2 ,4-Trichl orobenzene <0 . 25 0.25 95 - 63-6 1 ,2,4 - Trimethylbe nzene <0.10 0. 10 96 - 12 - 8 1, 2-Dibromo - 3 - <0 . 25 0.25

chlor opropane 106 - 93 - 4 1,2 - Dibromoethane <0.050 0.050 95-50-1 1 , 2-Dichlorob enzene <0 . 10 0. 10 107 - 06-2 1 ,2 - Dichloroethane <0 .050 0.050 156 - 59 - 2 cis-1,2 - Dichloroethene <0. 050 0.050 1 56 - 60-5 trans - 1,2-Dichloroethene <0 . 050 0 . 050 78-87-5 1,2-Dichloropropane <0.050 0.050 1 08 - 67-8 1,3, 5-Trimethy lbenzene <0.10 0 . 10 541 - 73 - 1 1,3-Dichlorobenzene <0.10 0 .10 10061 - 01-5 cis - 1 ,3 - Dichloropropene <0.050 0 . 050 10061 - 02 - 6 trans-1,3 - Dichloropropene <0.050 0.050 110 - 57 - 6 trans - 1,4-Dichloro- <0.050 0.050

2-butene 106-46-7 1,4-Dich lorobenzene <0.10 0 . 10 78 - 93 - 3 Methyl Et hyl Ketone <0 . 25 0 . 25 591-78 - 6 2 - Hexanone <0.25 0. 25 91 - 57-6 2-Methylnaphthalene <0.25 0 . 25 67-64 - 1 Acetone <0 . 75 0.75 108- 10-1 4 - Methyl - 2 - Pentanone <0.25 0.25 107 - 13-1 Acrylonitrile <0.25 0 .2 5 71 - 43 - 2 Benzene <0 . 050 0.050 108 - 86 - 1 Bromobenzene <0 . 10 0 .10 74 - 97-5 Bromochloromethane <0.10 0.10

Page 29

T hi< repor t sl"tll ouot lo~ reproduced except in lid!, wi d1011t wriucn .nuhuriz.uiuoo of'lii l\ l.nlix Lahor.rturie,, ' " '" ludividu!!l s.unplt· rn tol t> rd .ne oooly to the sample tested.

5560 Corporate Exchange Court SE • Grand Ra pich , ~vii 4951 2 • (6 16) 975-4500 • r:ax (6 16) 942-746.>

~ TriMatrix f~ Laboratories, Inc.

ANALYTICAL REPORT



Extracted: Sample #: 307108 Analyzed: 06/14/02 by DLVV Sample ID: SS-10 Ref. Citation: USEPA-8260B

Dilution Factor: 1 Analytical Batch: 18727 0


Analytical QuantitatioMDEQ Plus List Volatiles Result Limit

CAS Number USEPA Method 5035/8260 (rng/kg dry} (rng/kg dry}

75 - 27-4 Dichlorobromomethane <0.10 0.10 75-25 - 2 Bromoform <0 .10 0 . 10 74-83-9 Bromomethane <0 .25 0.25 75-15-0 Carbon Disulfide <0 . 25 0.25 56-23-5 Carbon Tetrachloride <0.050 0.050 108-90 - 7 Chlorobenzene <0. 050 0.050 75-00 - 3 Chloroethane <0.25 0. 25 67 - 66 -3 Chloroform <0 . 050 0.050 74 - 87-3 Chloromethane <0.25 0.25 124-48-1 Chlorodibromomethane <0.10 0.10 74 - 95-3 Dibromomethane <0.10 0.10 75-71 - 8 Dichlorodif l uoromethane <0.25 0.25 60-29-7 Ethyl Ether <0 .25 0. 25 100-41- 4 Ethylbenzene <0.050 0.050 67-72-1 Hexachloroethane <0 . 10 0.10 98-82 - 8 Isopropylbenzene <0.10 0. 10 136777-61-2 Xylene, Meta & Para <0 .10 0.10 74-88 - 4 Iodomethane <0 .10 0.10 1634-04 - 4 Methyl (tert}butyl Ether <0 . 25 0.25 75 - 09-2 Methylene Chloride <0 .2 5 0. 25 91-20 -3 Naphthalene <0 .25 0. 25 104-51 - 8 n - Butylbenzene <0 .25 0.25 103-65 - 1 n-Propylbenzene <0. 10 0.10 95 - 47-6 a-Xylene <0.050 0.050 99-87 - 6 4-Isopropyltoluene <0.25 0. 25 135 - 98-8 sec-Butylbenzene <0.25 0. 25 100-42 - 5 Styrene <0 .050 0 . 050 98 - 06-6 tert-Butylbenzene <0.25 0.25 127 - 18-4 Te trachloroethene <0 . 050 0.050 109-99- 9 Tetrahydrofuran <1.0 1.0 108-88- 3 Toluene <0.050 0.050 79 - 01-6 Trichloroethene <0.050 0.050 75-69 - 4 Trichlorofluoromethane <0.25 0 . 25 75 - 01-4 Vinyl Chloride <0 . 10 0.10

Page 30

n

' I hi< ' ''POll shall not be r~prodll<t'd e"epo iu full. widllllll woiucn .oudoooiz.oriou of Tri l\ l.noix l ,olun.Hnlit·<, Inc. lndividu.oii:Hnple re,ulo < od.ll'' on!)' oo oloc ,,moplc ononl.

5560 Corpor:uc I~Xl hangc: Coun SE • Grand Rapid:., o'vii 4'J5 12 • (6 16} 975-4500 • Fax (6 16) 942-71'!()1

~ TrlMatrix ft Laboratories, Inc.

ANALYTICAL REPORT

MDEQ Submitta l #: 36024-1 Projec t: Tamarack City Stamp Mill Sampled: 06/04/02 @ 14: 15

ERD-Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02@ 10 : 00


Matrix: Soil


------ -- --- -- --- --- --- --- -- --- -- -- - --- - - -- -- - - -- -- -- -- - --- -- -- --- -- -- -- --- ---Percent Solids 97 0.1 % 06 / 07/02 GEH SW-846 35508

Page 31

T loi, ocpon ''"'"""'he ' ' 'l'ro<luccd cxcq11 in lid!, withom written aouhoriz,Hion ofTriM.mix I ahm Jlorir,, Inc lndil'idual >.unple re""' ' tdJtc on I)' 10 the ~:unplc t<'\lcd.

5560 Corpomt• Exchange Court SE • Gra nd Rapid~. M l IJ9512 • (616) ')75-4500 • f ax (6 16) 942 -746J

~ TriMatrix f~ Laboratolics, Inc.

ANALYTICAL REPORT

MDEQ Submittal # : 36024-1 Project : Tamar ack City Stamp Mill Sampled: 06/04/02 @ 14: 15

ERD- Superfund, Lansing Sample r : Spielberg Submittal : June 4, 2002 Soils Received : 06/06/02 @ 10 : 00

Extracted : Sample #: 307109 Analyzed: 06/14/02 by DLW Sample ID: SS-11 Re f. Citation: USEPA- 8260B

Dilu tion Factor : 1 .03 Analytical Batch: 187270

Mat r ix: Soil QC Batch : 075930 - 114


CAS Number USEPA Method 5035 / 82 6 0 (mg/ kg dry) (mg/ kg dry)

630 - 20-6 1, 1 ,1,2-Tetrachl oroet hane <0 . 10 0 . 10 71 - 55 - 6 1 ,1 ,1 - Tr i c h lor o e than e <0.052 0.052 79-34-5 1, 1 ,2,2-Tetr achloroetha ne <0. 10 0. 1 0 79 - 00 - 5 1, 1 ,2 - Tr ichloroethane <0.052 0.052 75-34 - 3 1 ,1-Dichloroetha ne <0.052 0.052 75 - 35-4 1, 1-Di c hlo r oeth y l e ne <0.052 0. 052 87-61-6 1,2,3- Trichlorobenzen e <0.26 0. 26 96- 1 8 - 4 1 ,2,3-Tric hlorop ropan e <0.10 0.10 120 - 82 - 1 1,2,4-Tr i ch l orobenzene <0 . 26 0.26 95 - 63 - 6 1 , 2 ,4 - Tri methylbenzene <0.10 0.10 96 - 12- 8 1 ,2 - Dibromo-3 - <0 . 26 0 . 26

chl oropropane 106 - 93 -4 1,2-Dibr omoetha ne <0.052 0.052 95 - 50-1 1,2 - Dich lorobenzene <0 . 10 0 . 10 107 - 06-2 1,2 - Dichlo r oetha ne <0 . 052 0 . 052 156 - 59-2 cis -1 ,2-Dichl oroethen e <0.052 0.052 156 - 60-5 trans-1,2 -Di c hloroethene <0.052 0.052 78 - 87-5 1,2 - Dich loropropane <0 . 052 0 . 052 108-67-8 1 ,3,5-Tri methylbe n zen e <0.10 0.10 541 - 73 - 1 1,3-Dich lorobe n zene <0 . 10 0.10 10061 - 0 1 - 5 cis- 1 ,3 - Dichloropropene <0 . 052 0.052 10061-02 - 6 tran s-1,3 - Dichloropropene <0 . 052 0 . 052 110-57-6 trans - 1,4 - Dichl oro - <0.052 0. 052

2 - bu tene 106 - 46 - 7 1 ,4 - Dichlorobenzene <0 . 10 0.10 78-93 - 3 Me t hyl Ethyl Ke t one <0.26 0.26 591 - 78-6 2-Hexanone <0.26 0.26 91-57-6 2-Meth y lnaph thal ene <0 . 26 0.26 67-64 - 1 Acetone <0.77 0.77 108 - 10- 1 4-Meth y l -2-Pentanone <0.26 0.26 107 - 13- 1 Acryl oni tri le <0.26 0 . 26 71-43-2 Benzene <0 . 052 0.052 108 - 86 -1 Bromoben zene <0.10 0.10 74 - 97 - 5 Bromochloromethane <0.10 0 . 10

Page 32

This r~port ~h.rllnut be reproduced rxccpr in ful l, wirhnur written ;ltrthuriur inn ufTril\ l.urix l .rhoraruries, Inc. lndil'iUuJI s.rmple rnult, rda t~ nnlr ro rhe """l'lc te~rcd .

5560 Curpur:Ht' Excha nge Cour t SE • G rand lbpid,, ~-If 4~5 1 .2 • (616) ~7 5 -4500 • F;lx (6 16) ~42-746J

~ TriMatrix f~ Lilboratorics, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/0 2@ 14:15


Extracted: Sample #: 307109 Analyzed : 06/14/02 by DLVV Sample ID: SS-11 Ref . Citation: USEPA- 82608

Dilution Factor: 1 .03 Analytical Batc h : 187270




75 - 27-4 Dichlorobromomethane <0.10 0.10 75 - 25 - 2 Bromoform <0. 10 0.10 74-83 - 9 Bromomethane <0.26 0.26 75 - 15 -0 Carbon Disulfide <0.26 0.26 56-23 - 5 Carbon Tetrachloride <0.052 0.052 108-90 - 7 Chlorobenzene <0 . 052 0.052 75-00 - 3 Chloroethane <0.26 0.26 67 - 66-3 Chl oroform <0.052 0.052 74-87 - 3 Chloromethane <0.26 0 . 26 124 - 48-1 Chlorodibromomethane <0.10 0.10 74 -95- 3 Dibromomethane <0 . 10 0.10 75-71 - 8 Dichlorodifluoromethane <0.26 0.26 60-29 - 7 Ethyl Ether <0.26 0.26 100-41 - 4 Ethy lbenze ne <0.052 0.052 67-72 - 1 Hexachloroethane <0 . 10 0.10 98-82 - 8 Isopropylbenzene <0.10 0.10 136777 - 61 - 2 Xylene, Meta & Para <0.10 0.10 74 - 88 - 4 I odomethane <0.10 0.10 1634-04 - 4 Methyl(tert)but yl Ether <0.26 0 . 26 75 - 09-2 Methylene Chloride <0.26 0 . 26 91-20-3 Naphthalene <0.26 0 .26 104-51 - 8 n - Butylbenzene <0.26 0.26 103-65 - 1 n - Propylbenzene <0. 10 0.10 95-47-6 a - Xylene <0.052 0.052 99-87 - 6 4-Isopropyltoluene <0.26 0.26 135-98- 8 sec- Butylbenzene <0.26 0.26 100-42 - 5 Styrene <0.052 0.052 98 - 06-6 tert - Butylbenzene <0 .26 0.26 127-18 -4 Tetrachloroethene <0.052 0.052 109-99 - 9 Tetrahydrofuran < 1. 0 1 .0 108 - 88-3 Toluene <0.052 0.052 79 - 01 - 6 Trichloroethene <0 .052 0 . 052 75-69-4 Trichloro fluoromethane <0 .26 0.26 75-01-4 Vinyl Chloride <0.10 0 . 10

Page 33

T hi< rcpurc , hall rHll he reproduced except in full. wicluuoc wricceoc .ucchmin ciun of"liil-lacr ix I JhnrJcoric,, Inc. lndi1·iduJI s,unplc f<'Mth > rd.ue unlr co chr s.unple cncrd,

5560 Curpur:lrl' Exchange Cuun SE • Crand Rapid.,, J'vll 495 12 • (616) 975 -4500 • Fax (G IG) 94 2-74o.1

~ TriMatrix f~ Lnhomlories, Inc.

ANALYTICAL REPORT


ERD-Superfund, La ns i ng Sampler: Spielberg Submi ttal : June 4, 2002 Soils Received: 06/06/02 @ 10:00

Sample #: 307110 Sample I D: SS-12

Mat r ix: Soil


--- ---- -- ----- ------ -- --- --- -- -- -- - ------- -- --- --- --- - -------- -------- -------Percent Solids 92 0 . 1 % 06 /07/02 GEH S\'1-846 3550B

Pa ge 34

T hi> rq10n >hallnnt he repr oduced except in full , withom wri ucn Jllthuriz;uion nf"l i-i ~l.mix Lthnr,uori<'<, Inc. Ind ividual s.mtpl<· results relate only to thl" >.tmplc tl">trd.

55<10 Corpora te Exclungc Court SE • Grand Rap i d ~, i'vll 49512 • (GI (i) 975-4500 • Fax (6 16) ')42-7463

~ TriMatrix ~~ L<~bomtorics, Inc.

ANALYTICAL REPORT

MDEQ Submittal # : 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 14:05


Extracted: Sample # : 307110 Analyzed : 06/14/02 by DLVV Sample ID: SS-12 Ref. Citation: USEPA - 8260B


Matrix : Soil QC Batch: 075930- 114



630-20 - 6 1,1,1,2 - Tetrachloroethane <0.11 0.11 71-55 - 6 1,1 ,1-Trichloroethane <0 .055 0.055 79- 34-5 1,1,2,2-Tetrachloroethane <0 .11 0 . 11 79-00 - 5 1,1,2-Trichloroethane <0.055 0.055 75 - 34-3 1,1-Dichloroethane <0 . 055 0.055 75-35 - 4 1,1 - Dichloroethylene <0 .055 0.055 87-61-6 1,2,3-Trichlorobenzene <0 . 27 0.27 96-18 - 4 1 ,2,3-Trichloropropane <0 .11 0.11 120-82-1 1,2,4 -Trichlorobenzene <0 .27 0.27 95-63 - 6 1,2,4-Trimethylbenzene <0 .11 0.11 96-12 - 8 1 ,2-Dibromo-3- <0 .27 0.27

chloropropane 106 - 93-4 1,2-Dibromoethane <0 .055 0.055 95-50 - 1 1,2-Dichlorobenzene <0.11 0. 11 107-06-2 1,2 - Dichloroethane <0.055 0.055 156-59-2 cis - 1,2 - Dichloroethene <0 . 055 0.055 156-60 - 5 trans-1,2-Dichloroethene <0 . 055 0.055 78-87 - 5 1,2 - Di c hloropropane <0.055 0 . 055 108-67-8 1,3,5-Trimethylbenzene <0.11 0.11 541-73 - 1 1,3 - Dichlorobenzene <0. 11 0.11 10061-01-5 cis-1,3-Dichloropropene <0 . 055 0.055 10061- 02 -6 trans -1 ,3 - Dichloropropene <0.055 0 .0 55 110-57 - 6 trans-1,4 - Dichloro - <0.055 0.055

2-butene 106-46 - 7 1,4 - Dichlorobenzene <0.11 0. 11 78- 93-3 Methyl Ethyl Ketone <0.27 0 . 27 591-78 - 6 2-Hexanone <0 . 27 0.27 91-57 - 6 2 - Methylnaphthalene <0.27 0 . 27 67-64-1 Acetone <0 .82 0.82 108-10 - 1 4 - Methyl - 2- Pentanone <0.2 7 0. 27 107 - 13 - 1 Acrylonitrile <0 . 27 0 . 27 71 - 43-2 Benzene <0.055 0.055 108-86 - 1 Bromobenzene <0 .11 0.11

74 - 97 - 5 Bromochloromethane <0 .11 0.11

Page 35

This •~pun sl"'ll nol [,,. rcpn><lu<c·d c\<'epl in full, witlun11 wri tt<ll .wdmtit.llinn ofTii~l:111ix LlhOJJwrin.l nc. lndividu:tl >:nuplc tc>ttll> rel.uc uu ly 10 1hc ,.unple I<'Sil'd.

5560 Curflo r:tlt' l~xchange C:ourr SE • Grand ltapids, t\.11 49512 • (G IG) ~75 -4500 • E1x (G i o) ~-'12-7-'! Cl .~

~ TriMatrix f~ L.,boratorie.s, Inc.

ANALYTICAL REPORT

MDEQ Submittal # : 36024-1 Projec t: Tamarack City Stamp Mill Sampled : 06/04/02 @ 14 : 05

ERD-Superfund, Lansing Sampler : Spielberg Submit t a l: June 4 , 2002 Soils Recei ved : 06/06/02 @ 10 :00

Ext r acted: Sample #: 307110 Analyzed: 06/14/02 by DLVV Sample ID : SS-12 Ref. Cita t i o n: USEPA-8 260B

Dilution Factor : 1.09 Analytica l Batc h: 187270

Matrix: Soil QC Batch : 075930-114



75 - 27-4 Dichlorobromomethane <0 . 11 0.11 75-25 - 2 Br omoform <0.11 0.11 74-83 - 9 Bromomethane <0 . 27 0.27 75-15-0 Carbon Disulfide <0.27 0.27 56 - 23-5 Carbon Tetrachloride <0.055 0.055 108-90 - 7 Chlorobenzene <0 .055 0.055 75 - 00-3 Chloroethane <0 . 27 0.27 67-66-3 Chloroform <0.055 0.055 74-87 - 3 Chloromethane <0.27 0.27 12 4 - 48 - 1 Chlo rodibromomethane <0 . 11 0.11 74 - 95-3 Dibromomethane <0 . 11 0.11 75 - 71 - 8 Dichlorodifluoromethane <0 . 27 0.27 60 - 29 - 7 Ethyl Ether <0.27 0.27 100-41-4 Ethyl benzene <0 . 055 0.055 67 - 7 2 -1 Hexachloroethane <0 . 11 0.11 98 - 82 - 8 Isopropylbenzene <0. 11 0.11 136777 - 61- 2 Xylene, Meta & Para <0 . 11 0.11 74 - 88 - 4 Iodomethane <0 . 11 0.11 1 634-04 - 4 Methyl (tert)butyl Ether <0.27 0.27 75 - 09 - 2 Methyl ene Chl or ide <0.27 0.27 91- 20 - 3 Naphthalene <0.27 0.27 104 - 51-8 n - Butylbenzene <0.27 0.27 103-65- 1 n - Propyl benzene <0. 11 0.11 95-47 -6 a - Xylene <0 . 055 0 . 055 99 - 87-6 4-Isopropyltoluene <0.27 0 . 27 135-98 - 8 sec - Butylbenzene <0.27 0. 2 7 100-42 -5 Styrene <0.055 0 . 055 98 - 06 - 6 tert - Butylbenzene <0 . 27 0. 27 127-18- 4 Tetrachloroethene <0.05 5 0 . 055 109 - 99-9 Tetrahydrofuran <1. 1 1 . 1 108 - 88 -3 Toluene <0 . 055 0 . 055 79-01 - 6 Trichlor oethene <0.055 0 . 055 75- 69 - 4 Trichlorofluoromethane <0.27 0 . 27 7 5 - 01 - 4 Vinyl Chloride <0 .11 0.11

Pa ge 36

T his rcpun >h.tll nuc L~ r~prmhrtcd excqH in Iiiii, wid10u1 wriu r n .unhurizaciun ufTri l\l.u ri~ l .chor.Hmic,, Inc. lnd ivid rr.cl >.unplc """" rcl.ll l' only m the ,,L111ple rc>ecd.

5560 Curpur~ t ~ Exchange Courr SE • Gra nd Rapid, , Ml 4<J5 12 • (lli G) <J75-45UO • Fax (GIG) 942-74 63

~ TriMatrix f~ l.ahoratories, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1

Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 14:10

ERD- Superfund, Lansing Sampler: Spielberg Received: 06/06/02@ 10:00 Submittal: June 4, 2002 Soils


Matrix : Soil

Analytical Quant. Analysis Reference

Parameter Result Limit Unit Date Chern Citation

-- - -- --- -- -- ---- - -- --- ----- -- - --- --- - - - - - - -- ------------- --- --- - -- -- ------- --Percent Solids 90 0.1 % 06/07/02 GEH SW-846 3550B

Page 37

Tit is rcpo ru h .tll nut be reproduced nt't:pt in full. withou t wri tten authorization ofTri:-.btrix Labur.uuries, Inc. lndividua.l sample results relate o nlr 10 the sample tested.

55 60 Corporate E~ch a nge Court SE • Grand Rapids, M l tl9512 • {61(,) 9 75-tiSOO • Fa ~ ((, JG) ')42-746.3

~ TriMatrix f~ labomlorics, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024 - 1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 14 :10


Extracted: Sample #: 307111 Analyzed: 06/14/02 by DLVV Sample I D: SS- 13 Ref. Citation: USEPA-8260B

Dilution Factor: 1 .02 Analytical Batch: 187270



CAS Number USEPA Method 5035/8260 (mg/kg dry) (mg/ kg dry)

630-20-6 1 ,1,1,2-Tetrachloroethane <0.10 0.10 71-55-6 1,1,1 - Trichloroethane <0.051 0 . 051 79-34 - 5 1 ,1,2,2-Tetrachloroethane <0 .10 0.10 79-00-5 1 ,1 ,2 - Trichloroethane <0.051 0 . 051 75 - 34-3 1,1 - Dichloroethane <0 .051 0.051 75-35- 4 1,1- Dichloroethyl ene <0.051 0 . 051 87-61 - 6 1 ,2,3-Trichl orobenzene <0.26 0.26 96 - 18-4 1,2,3-Trichloropropane <0 .10 0.10 120 - 82 - 1 1,2,4 - Tric hlorobenzene <0.26 0.26 95 - 63-6 1,2,4 - Trimethylbenzene <0 .10 0 . 10 96 - 12-8 1,2 -Dibromo-3- <0 . 26 0.26

chloropropane 106-93 - 4 1 ,2 - Dibromoethane <0.051 0.051 95-50-1 1 ,2-Di chlorobenzene <0. 10 0 . 10 107 - 06-2 1 ,2 - Dichloroethane <0 . 051 0 . 051 156-59-2 cis-1,2-Dichloroethene <0 .051 0.051 156-60 -5 tran s - 1,2-Dichloroethene <0.051 0.051 78-87 - 5 1,2-Dichloropropane <0.051 0 . 051 108 - 67-8 1,3,5-Trimethylbenzene <0 .10 0. 10 54 1 - 73 - 1 1,3 - Dichlorobenzene <0. 10 0.10 10061-01-5 c i s-1,3-Di chl oropropene <0 . 051 0.051 10061-02-6 t rans-l , 3-Dichloropropene <0 .051 0.051 110-57-6 trans - 1,4-Dichloro- <0.051 0.051

2 - butene 106-46-7 1,4-Dichl o r obenzene <0 .10 0.10 78-93-3 Methyl Ethyl Ketone <0.26 0.26 591 - 78 - 6 2-Hexanone <0.26 0.26 91 - 57-6 2-Methylnaphthalene <0.26 0.26 67-64- 1 Acetone <0 .77 0.77 108-10-1 4-Methyl-2-Pentanone <0.26 0.26 107-13-1 Acrylonitrile <0.26 0.26 71 - 43-2 Benzene <0 .051 0.051 108-86-1 Bromobenzene <0 .10 0.10 74 - 97 - 5 Bromochloromethane <0. 10 0.10

Page 38

Thi> report shall not h~ reproduced except in li1ll, without wtilten ;Hithoriz.uionoi"'Jii,\l.urix I ah111,uorie,, Inc l ncli1·idu.1l >Jonpl~ r<'ul" rd .ue nulr 111 the ,,unple tt'>ted.

5560 Corporate Exchange Cou rt SF. • Grotnd RaJ.>id,, /vii 4'>5 12 • (6 16) 975-4500 • Fax (6 16) 942-7463

~ TriMatrix f~ Lilboratories, Inc.

ANALYTICAL REPORT



Extracted: Sample #: 307111 Analyzed: 06/14/02 by DLVV Sample ID: SS-13 Ref. Citation: USEPA-82608





75 -27-4 Dichlorobromomethane <0 .10 0.10 75-25-2 Bromoform <0.10 0.10 74 - 83 - 9 Bromomethane <0 . 26 0.26 75- 15 - 0 Carbon Disulfide <0.26 0.26 56-23 - 5 Carbon Tetrachloride <0 . 051 0 . 051 108-90-7 Chlorobenzene <0.051 0. 051 75-00 - 3 Chloroethane <0.26 0 . 26 67-66 - 3 Chloroform <0.051 0.051 74-87-3 Chloromethane <0 . 26 0.26 124-48- 1 Chlorodibromomethane <0.10 0.10 74-95-3 Dibromomethane <0. 10 0.10 75-71 - 8 Dichlorodifluoromethane <0 . 26 0.26 60-29-7 Ethyl Ether <0.26 0.26 100-41 - 4 Ethylbenz ene <0 . 051 0.051 67 - 72-1 Hexachloroethane <0 . 10 0.10 98-82-8 Isopropylbenzene <0.10 0.10 136777 - 61-2 Xylene, Meta & Para <0.10 0.10 74-88-4 Iodomethane <0.10 0.10 1634 -04-4 Methyl(tert}butyl Ether <0.26 0.26 75-09-2 Methylene Chloride <0.26 0.26 91 - 20-3 Naphthalene <0 .26 0 . 26 104-51- 8 n - Butylbenzene <0.26 0.26 103-65-1 n-Propylbenzene <0.10 0.10 95-47-6 a - Xylene <0 . 051 0.051 99-87 - 6 4 - Isopropyltoluene <0.26 0.26 135-98 - 8 sec - Butylbenzene <0.26 0.26 100 - 42-5 Styrene <0 . 051 0.051 98-06- 6 tert-Butylbenzene <0.26 0.26 127 - 18 - 4 Tetrachloroethene <0 . 051 0.051 109-99 - 9 Tetra hydrofuran <1.0 1.0 108-88-3 Toluene <0.051 0.051 79 - 01 -6 Trichloroethene <0.051 0 . 051 75 - 69 - 4 Trichlorofluoromethane <0 .26 0.26 75-01-4 Vinyl Chloride <0. 10 0.10

Page 39

'I hi' "'POll shall not b~ reprmlucn l ~x..-ept in fu ll, wir hullt wrill<'ll .unhorizJrion nf Tri:O,I.ttrix Lrbor.ttorin, Inc lndi1·idual >.lnlple re>trlt > rd.uc unlr 10 drc ,,unpk tcllnl.

5560 Corporatr: ExL hange Coun SE • Grand Rapids, r\•11 49 5 12 • (6 16) Y75-4500 • Fax (6 16} 9-12-746.)

~ TriMatrix ~~ l nhornlo1ies, Inc.

ANALYTICAL REPORT

MDEQ Submi t tal # : 36024-1

Project: Tamarack City Stamp Mi ll Sampled : 06 / 04 / 02 @ 14:25

ERD - Superfund, Lansing Sampler: Spiel berg

Submittal: June 4 , 2002 Soils Received: 06 / 06 / 02 @ 10:00

Sample#: 307112 Sample ID: SS-14

Matrix: Soil


Parameter Result Limit Unit Date Chern Citation

--- --- - ------ - ----- - -- - -- --- ------- --- ----- - -- -- ---- -- ---- - --- - -- -- - ----- ----Percent Solids 95 0. 1 % 06 / 07/02 GEH SW-846 35508

Pag e 40

T hi' rrpon >hall nut bt rq>roduced <XlCpt in full . without writtl'll authoriz.uion ufTri ~bt rix l.tbor.uorie,, Inc. lodividu.tl , ,un pk ll'lldt, oebtc onlr 10 the s•mplc te>tcd.

5560 Corporate Excha nge Courr SE • Grand Rapid>, o\oll 495 12 • (6 1Cl) 975-ti500 • Fax (6 16) 942-746J

·~ TriMatrix ·~ ~boratorics, Inc. ------------------------------

ANALYTICAL REPORT ----------------------



Extracted: Sample# : 307112 Analyzed: 06/14/02 by DLW Sample ID: SS-14 Ref. Citation: USEPA- 8260B





630-20-6 1,1, 1, 2 - Tetrachloroethane <0.10 0.10 71-55 - 6 1,1,1-Trichloroethane <0 . 050 0.050 79-34 - 5 1,1,2,2-Tetrachloroethane <0.10 0.10 79 - 00-5 1, 1,2 -Trichloroethane <0 .050 0.050 75-34-3 1,1 - Dichloroethane <0 .050 0.050 7 5 - 35-4 1,1-Dichloroethylene <0.050 0.050 87-61 - 6 1,2,3-Trichlorobenzene <0.25 0.25 96-18 - 4 1,2,3 - Trichloropropane <0.10 0.10 120-82 - 1 1,2,4- Trichlorobenzene <0.25 0.25 95-63-6 1,2,4-Trimethylbenzene <0.10 0.10 96 - 12 - 8 1,2-Dibromo-3- <0.25 0.25

chloropropane 106 - 93-4 1,2 - Dibromoethane <0.050 0 . 050 95-50 - 1 1, 2 - Dichlorobenzene <0 . 10 0.10 107-06 - 2 1,2 - Dichloroethane <0.050 0.050 156 - 59-2 cis-1,2-Dichloroethene <0.050 0.050 156-60 - 5 trans-1,2 - Dichloroethene <0 .050 0.050 78 - 87 -5 1,2-Dichloropropane <0.050 0.050 108-67- 8 1,3,5 - Trimethylbenzene <0.10 0.10 541-73 - 1 1,3 - Dichlorobenzene <0.10 0.10 10061-01-5 cis-1,3-Dichloropropene <0 . 050 0.050 10061 - 02-6 trans-1,3- Dichloropropene <0.050 0.050 110 - 57 -6 trans - 1,4 - Dichloro- <0.050 0.050

2-butene 106-46 - 7 1,4 - Dichlorobenzene <0.10 0 . 10 78 - 93-3 Me thyl Et hyl Ketone <0 .25 0.25 591 - 78-6 2 - Hexanone <0 . 25 0 . 25 91 - 57 - 6 2-Methylnaphthalene <0.25 0 . 25 6 7 - 64 - 1 Acetone <0.75 0.75 108 - 10-1 4 - Methyl-2 - Pentanone <0.25 0.25 107-13 -1 Acrylonitrile <0 . 25 0.25 71 - 43-2 Benzene <0 .050 0 . 050 108- 86 - 1 Bromobenzene <0.10 0.10 74 - 97 - 5 Bromochloromethane <0.10 0.10

Page 41

Thi' «purl 'hallno1 he reproduced exc~pr in fu ll, without written .nodwri1a1iun uf'lii.\Louix Lahoo31oric,, lnc. lndividu.ol s.o mplc rc><Jts r< l.11e only tu doc ;.moplc '"'led.

5560 C:orp orar<.: Exchange Court SE • Grand Rapids, Ml -19 '5 1.2 • (GIG) 975-4500 • Etx (G I G) ')4 2-74(i1

~ TriMatrix ·~ Laboraloties, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02@ 14:25



Dilution Factor : 1 Analytical Batch: 187270




75-27 - 4 Dichlorobromomethane <0.10 0.10 75-25 - 2 Bromoform <0 . 10 0.10 74-83-9 Bromomethane <0 .25 0.25 75-15 - 0 Carbon Disulfide <0.25 0.25 56-23 - 5 Carbon Tetrachloride <0.050 0.050 108 -90 -7 Chlorobenzene <0.050 0 .050 75-00 - 3 Chloroethane <0.25 0.25 67-66 - 3 Chloroform <0. 050 0 . 050 74-87 - 3 Chloromethane <0 .25 0.25 124 -48 -1 Chlorodibromomethane <0.10 0.10 74-95 - 3 Dibromomethane <0 .10 0.10 75 -71 - 8 Dichlorodifluoromethane <0 . 25 0.25 60 - 29-7 Ethyl Ether <0 . 25 0.25 100 -41 - 4 Ethylbenzene <0.050 0.050 67-72 - 1 Hexachloroethane <0.10 0. 10 98-82- 8 Isopropylbenzene <0. 10 0.10 136777-61-2 Xylene, Meta & Para <0. 10 0.10 74-88 - 4 Iodomethane <0.10 0.10 1634-04-4 Methyl(tert)butyl Ether <0.25 0.25 75-09 - 2 Methylene Chloride <0.25 0. 25 91-20-3 Naphthalene <0 .25 0. 25 104-51- 8 n - Butylbenzene <0 .25 0. 25 103-65 - 1 n-Propylbenzene <0 . 10 0.10 95-47-6 a-Xylene <0 .050 0 . 050 99-87 - 6 4 - Isopropylto luene <0.25 0.25 135-98-8 sec-Butylbenzene <0.25 0.25 100-42 - 5 Styrene <0 .050 0.050 98-06-6 tert-Butylbenzene <0.25 0.25 127-18 - 4 Tetrachloroethene <0.050 0.050 109-99-9 Tetrahydrofuran <1.0 1.0 108 - 88 -3 Toluene <0 .050 0.050 79 - 01 - 6 Trichloroethene <0.050 0 . 050 75 - 69-4 Trichlorofluoromethane <0.25 0.25 75-01-4 Vinyl Chloride <0. 10 0.10

Page 42

Thi~ report <h.tllnm he reproduced cxccpr in full , withuur writt<'n .unhuriL.niun of l'r ii\ l,1arix I Jhor.unoic,, Inc. Individual <.tmplc rc<ult> rd.ut' onlr w rhc >.tmple l t'\l t'd .

5560 C:o rporarc Exchange Cnurr SE • Grand Rapids, o\ •l! lj9SI2 • (GIG) 975-lj SUO • Fax (6 16) 94 2-7463

~ TriMatrix f~ Laboratories. Inc.

ANALYTICAL REPORT

MDEQ Submi t t al# : 36 024-1

Pro j ect : Tamarack Ci ty Stamp Mill Sampl e d : 06/04/02 @ 14 : 40

ERD - Superf und, Lans i ng Sampler : Sp i elberg

Submi t tal: June 4, 2002 Soils Received: 06 /0 6/02 @ 1 0:00

Sampl e # : 307113 Sampl e I D: SS-15

Matrix : Soi l


Parameter Result Lirni t Unit Date Chern Citation

------ --- -- -- -- --- --- ---- ---- -- -- -- ---- -- --- -- - - - - - -- - - ---- - - - ---- -- -- --- --- -Percen t Solids 83 0. 1 % 06/07/02 GEH SW-846 355 08

Page 43

Thi, rqw11 <ldl nor be rcprodu,c<l "'l<l>l in ful l. wirhour w1irr<n aurlonrit:ll imlof'l'li l\lauix L>bur.nurie,, inc lndi\'idu:ll ,,H nple rc"ol r< rcl.l!c only w rhe '-1m pic re'[(·tl.

5560 Corporarl· Exchange Cnun SE • Grand Rapids, M l !'J95 12. • (616) 975-4500 • F.1x (6 16) 942-7463

~ TriMatrix f~ Labomtories, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 14 :40


Extracted: Sample#: 307113 Analyzed: 06/14/02 by DLVV Sample ID: SS-15 Ref. Citation: USEPA- 8260B


Matrix: Soil QC Ba tch: 075930-114



630-20 - 6 1,1,1,2-Tetrachloroethane <0 .12 0.12 71-55 - 6 1, 1,1- Tric hloroethane <0 . 060 0.060 79-34 - 5 1,1,2,2-Tetrachloroethane <0.12 0.12 79 - 00-5 1,1,2-Trichloroethane <0.060 0.060 75-34 - 3 1,1-Dichloroethane <0.060 0.060 75-35-4 1,1- Dichloroethylene <0.060 0.060 87-61 - 6 1,2,3 -Tri chlorobenzene <0.30 0.30 96 - 18-4 1,2 ,3-Trichloropropane <0.12 0.12 120 -82 -1 1,2,4- Trichlorobenzene <0 .30 0.30 95-63 - 6 1,2,4- Trimethyl benzene <0.12 0.12 96-12 - 8 1,2 - Dibromo-3 - <0 . 30 0. 30

chloropropane 106 - 93-4 1,2-Dibromoethane <0 .060 0.060 95-50 - 1 1,2 - Dichlorobenzene <0 . 12 0.12 107-06 - 2 1 , 2-Dichloroethane <0.060 0.060 156-59-2 cis - 1,2-Dichl oroethene <0 . 060 0.060 156-60-5 trans-1,2 - Dichloroethene <0.060 0.060 78- 87-5 1,2 - Dichloropropane <0.060 0. 060 10 8 -67 - 8 1,3,5-Trimethylbenzene <0.12 0.12 541-73 - 1 1,3 - Dichlorobenzene <0.12 0.12 1,0061-01-5 cis-1,3-Dichloropropene <0 . 060 0.060 10061 - 02 - 6 trans-1,3 - Dichloropropene <0.060 0.060 110 - 57-6 trans- 1,4 - Dichloro - <0.060 0.060

2-butene 106-46 -7 1,4 - Dichlorobenzene <0.12 0.12 78 - 93 - 3 Methyl Ethyl Ketone <0.30 0.30 591-78 - 6 2 - Hexanone <0.30 0.30 91-57 - 6 2-Methylnaphthalene <0.30 0.30 67- 64 - 1 Acetone <0.90 0.90 108-10-1 4-Methyl-2 - Pentanone <0.30 0.30 107-13 -1 Acrylonitrile <0 .30 0 . 30 71-43 - 2 Benzene <0 .060 0.060 108-86 - 1 Bromobenzene <0 . 12 0 . 12 74-97 -5 Bromochloromethane <0.12 0 . 12

Page 44

Thi> report >h:tll ttnl lw 1cp1oduc.·J cxccpr in fu ll, witlu1111 wriuen .nnhCJrizJ!ion ofTri!\ l .mi~ I .obur.nurie,, Inc. lndil'idual sample· rr>uh~ rd.11c unlr 111 1hr ''""Pic 1<'\ICd.

5560 Corpora tC' Exchang<: Court Sr. • C r:1ncl Rap ids, ovll 495 12 • (6 16) 975-lt500 • Fax (GIG) 942-7461


ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02@ 14:40

ERD-Superfund , Lansing Sampler: Spielberg Submittal: June 4, 2002 Soi l s Received: 06/06/02 @ 10:00

Extr acted: Sample #: 307113 Analyzed : 06/14/02 by DLW Sample ID: SS-15 Ref. Citation: USEPA-8260B

Dilution Factor : 1.2 Analytical Batch: 187270


Analyt i cal Quantitation MDEQ Plus List Volatiles Result Limit


75 - 27 - 4 Dichlorobromomethane <0.12 0 . 12 75-25-2 Bromoform <0.12 0.12 74 - 83-9 Bromomethane <0 . 30 0.30 75 - 15 - 0 Carbon Disulfide <0 . 30 0.30 56 - 23 - 5 Carbon Tetrachloride <0.060 0.060 1 08 - 90-7 Chl orobenzen e <0 . 060 0 . 060 75 - 00 - 3 Chloroethane <0.30 0.30 67-66 - 3 Chloroform <0.060 0.060 74 - 87-3 Chloromethane <0.30 0. 30 124-48 - 1 Chlorodibromomethane <0 . 12 0 .12 74 - 95-3 Dibromomethane <0 . 12 0.12 75-71 - 8 Dichlorodifluoromethane <0.30 0. 30 60 - 29-7 Ethyl Ether <0.30 0. 30 1 00-41 - 4 Eth y l benzene <0.060 0. 060 67 - 72 - 1 Hexa chloroethane <0 . 12 0 . 12 98-82 - 8 Isopropylbenzene <0.12 0.12 136777-61- 2 Xyl ene, Meta & Para <0. 1 2 0 .1 2 74 - 88 - 4 Iodomethane <0.12 0.12 1634 - 04 - 4 Methy l (tert)butyl Ether <0 . 30 0.30 7 5 - 09 - 2 Methyl ene Chlor ide <0.30 0.30 91 - 20 - 3 Naphthalene <0.30 0 . 30 104-51 - 8 n - Butylbenzene <0.30 0. 30 103 - 65-1 n-Propylbenzene <0 . 1 2 0 . 12 95 - 47 - 6 o-Xylene <0.060 0.060 99 - 87 - 6 4 - Isopropyltoluene <0 . 30 0.30 135 - 98 - 8 sec - Butylbenzene <0 . 30 0.30 100 - 42-5 Styrene <0.060 0 . 060 98-06 - 6 tert-Butylbenzene <0.30 0 . 30 127 - 18 - 4 Tet rachloroethene <0 .060 0 . 060 109- 99-9 Tetrahydrofuran <1 .2 1.2 108-88 - 3 Toluene <0 . 060 0 . 060 79 - 01-6 Trichloroethene <0.060 0.060 75-69-4 Trichlorofluoromethane <0 . 30 0.30 75 - 01-4 Vinyl Chloride <0 . 1 2 0.12

Page 45

This rrpun sh.J II Il<>t hr rcpwduc<J rx.:cpt in Ii lii, withuttt wri tt<'ll .uuhoJ ization ofTri i\ l.ttri' I ,Jiu>r.ttu1i,·, , Inc. lndiviclml s.1mpk· '"'"I" rdilt<' onlr to the '·'"'l' le tc<tcd.

5560 Corpora l ~ Exchang~: Cuurt SE • Grand Rapitb, 1\ •ll 495 12 • (() Ill) 9 75-~ 500 • Fax (6 I G) 942-74 1d

~ TriMatrix ·~ Lilboratories, trrc:.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project : Tamarack City Stamp Mill Sampled: 06/04/02 @ 14:30

ERD-Superfund, Lansing Sampler: Spielberg Submitta l: June 4, 2002 Soils Rece ived: 06/06/02 @ 10:00


Matrix: Soil


--- ------ -- ----- -- ---- -- - - ---- -- --- -- --- --- - --- ---- -- - -- --- --- -- ------ -------Percent Solids 94 0 . 1 % 06/07/02 GEH SW-846 3550B

Page 46

Thi, '"l'"fl ,),,Ji nm be ••·produn·J l'Xcepr in fir ll. widurur wriueu .un llluiz.uion ofTrii\l:tu i~ L.rl>Ur.umir,, Inc. lndil'idu.tl Y.lmple re>lllt> rd.n• onlr '" dr< ,,unplc tc\ln l.

5560 Corporate Exc.:harr gl' Coun SE • Grand Rap ids. 1vll 49') 12 • (6 16) 975-4500 • Fax (6 16) 942-7 463


ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 14 : 30

ERD- Superfund, La nsing Sampler: Spielberg Submittal : June 4, 2002 Soils Received: 06/06/02 @ 10 :00

Extracted : Sample #: 307114 Ana lyzed : 06/14/02 by DLW Sample I D: SS-16 Ref. Citation: USEPA-8260B

Dilution Factor: 1 .04 Analytical Batch: 187270




630 - 20-6 1 , 1,1, 2-Tetrachloroethane <0.10 O.lO 71 - 55-6 1,1,1 - Trichloroethane <0.052 0 . 052 79-34-5 1,1, 2,2-Tetrachloroethane <0 .10 0 . 10 79 - 00 -5 1,1,2-Trichloroethane <0 . 052 0 .052 75-34-3 1,1-Dichloroethane <0 .052 0.052 75-35 - 4 1,1-Dichloroethylene <0.052 0.052 87 - 61-6 1,2,3-Trichlo robenzene <0.26 0.26 96-18-4 1,2,3 - Trichloropropane <0 . 10 0 . 10 120 - 82 - 1 1,2,4-Trichlorobe nzene <0.26 0 .2 6 95-63-6 1, 2 , 4 - Trimethylbenzene <0 .10 0.10 96 - 12-8 1,2 - Dibromo- 3 - <0.26 0.26

chloropropane 106 - 93-4 1,2-Dibromoethane <0 .052 0.052 95 - 5 0 - 1 1,2-Dichlorobenzene <0 . 10 0.10 1 07 - 06-2 1,2-Dichloroethane <0 .052 0.052 156 - 59-2 cis-1 ,2 - Dich loroethene <0 . 052 0.052 156-60 - 5 trans - 1,2-Dichloroethene <0.052 0.052 78 - 87-5 1, 2-Dic hloropropane <0 . 05 2 0.052 108 - 67-8 1,3,5 - Trimethylbenzene <0 .10 0.10 541 -7 3 - 1 1,3-Dichlorobenze ne <0 .10 0.10 10061 - 01-5 cis -1,3-Dichloropropene <0 . 052 0 .052 10 061 - 02-6 trans - 1 ,3-Dichloropropene <0.052 0.052 110 - 57-6 tra ns - 1,4 - Dic hloro- <0.052 0.052

2-butene 106 - 46-7 1,4-Dichlorobenzene <0.10 0 .10 78-93- 3 Methyl Ethyl Ketone <0.26 0 .2 6 591 - 78 - 6 2 - Hexanone <0.26 0.26 91 - 57-6 2-Methylnaphthalene <0 .26 0.26 67-64-1 Acetone <0.78 0.78 108 - 10 -1 4 - Methyl - 2 - Pentanone <0.2 6 0.26 107 - 1 3-1 Acrylonitrile <0.26 0.26 71 - 43-2 Benzene <0.052 0.052 108 - 86-1 Bromobe nzene <0 . 10 0.10 74 -97- 5 Bromochloromethane <0 .10 0.10

Page 4 7

Thi• rrpott '""" llnl he repwduccd cxcq>t in fu ll, wiliJOIII wriuen .lllllroritJiinn urTri" l.urix L.rbot.llurie>, luc ludi"idu:rl ~ .rrnplr rnllh> rd:Hc uulr to dtc ,.r rrrplc· tc, tcd.

5560 Corporal~ Exchange Coun SE • Grand Rapids, lvll -195 12 • (616) Y75-450U • Fax (6 16) 942- 7463


ANALYTICAL REPORT








75-27 - 4 Dichlorobromomethane <0 . 10 0.10 75-25-2 Bromoform <0.10 0.10 74-83-9 Bromomethane <0.26 0. 26 75 - 15 - 0 Carbon Disulfide <0.26 0.26 56-23 - 5 Carbon Tetrachloride <0 .052 0.052 108-90 - 7 Chlorobenzene <0 . 052 0.052 75 - 00-3 Chloroethane <0 . 26 0. 26 67-66 - 3 Chloroform <0. 052 0.052 74-87-3 Chloromethane <0.26 0.26 124-48 - 1 Chlorodibromomethane <0. 10 0.10 74 - 95-3 Dibromomethane <0 . 10 0.10 75-71 - 8 Dichlorodifluoromethane <0.26 0.26 60-29 - 7 Ethyl Ether <0. 26 0.26 100-41-4 Ethylbenzene <0.052 0.052 67-72-1 Hexachloroethane <0 .10 0.10 98-82 - 8 Isopropylbenzene <0 .10 0.10 136777-61-2 Xylene, Meta & Para <0.10 0.10 74-88-4 Iodomethane <0.10 0.10 1634-04-4 Methyl(tert)butyl Ether <0.26 0.26 75-09 - 2 Methylene Chloride <0.26 0.26 91-20-3 Naphthalene <0 . 26 0.26 104-51 - 8 n - Butylbenzene <0.26 0 . 26 103 - 65-1 n-Propylbenzene <0 .10 0.10 95-47 - 6 a-Xylene <0 . 052 0.052 99 - 87 - 6 4-Isopropyltoluene <0.26 0.26 135 - 98-8 sec-Butylbenzene <0.26 0.26 100-42 - 5 Styrene <0 .052 0.052 98-06-6 tert - Butylbenzene <0 .26 0.26 127 - 18-4 Tetrachloroethene <0. 052 0.052 109 - 99-9 Tetrahydrofuran <1.0 1.0 108-88-3 Toluene <0.052 0.052 79 - 01-6 Trichloroethene <0 . 052 0.052 75-69-4 Trichlorofluoromethane <0.26 0.26 75-01-4 Vinyl Chloride <0. 10 0.10

Page 48

T his rcpon shallnrll he rqunJuc,·J cxcrpt in rull, wicl11111l wriuc11 .un lmriution ofTril\ l.u ri\ l .lhllrJw Jics, Inc. l11dividual s.tmpl< r~'ult, rd.Ht nnly to th,· >.tmple tcsttd.

5560 Corpo rate:- Exchange ClHirt SE • Grand Rapids, r\•11 495 12. • (tlltl) 975-!J500 • Fax ((ll tl) <J42-7tl tl3

~ TriMatrix ·~ Laboratories, Inc,

ANALYTICAL REPORT

MDEQ Submit tal #: 36024-1 Pro j ect : Tamarack Ci ty S tamp Mill Sampled: 06/04/02@ 11 : 35

ERD - Superfund, Lansing Sampler: Spielberg Submi ttal: June 4, 2002 Soils Received: 06/06/02 @ 10 : 00

sampl e # : 307115 Sampl e ID: SS - 17

Matrix: Soi l

Analytical Quant . Analysis Reference Parameter Result Limit Unit Date Chern Citation ------ --- -- -- -- ----- ----- -- -- --- -- - -- ------ - ----- --- -- --- -- - - - ----- ---- ---- --Percent Solids 83 0 .1 % 06/07/02 GEH SW - 846 3550B

Page 49

This rqlllrl sh,ollowo he r~produn·d except in fu ll . wiohnuo woiucn auohoriz,uion ofTril\l:urix I ~l uor.llorie<, Inc lnd ividual >.l lllple r.·,uh, rd:ue on I)' w ohc ,,omplc l<>t«l.

5 560 Corporate Exchange Court SE • Grand ltlpitls , M l 495 12 • ((, Ill) '.1 75-4 500 • Fax (616) 94 2-741l3

~ TriMatrix ~~ Labora tolies, Inc.

ANALYTICAL REPORT



Extracted: Sample #: 307115 Analyzed: 06/14/02 by DLW Sample ID: SS-17 Ref. Citation: USEPA-8260B





630-20 - 6 1,1,1, 2 - Tetrachloroethane <0.12 0.12 71 - 55-6 1,1,1-Trichloroethane <0.062 0.062 79-34-5 1,1,2,2 - Tetrachloroethane <0. 1 2 0.12 79- 00-5 1,1,2-Trichloroethane <0.062 0.062 75-34 - 3 1,1-Dichloroethane <0.062 0 . 062 75 - 35 -4 1,1-Dichloroethylene <0.062 0.062 87-61-6 1 , 2 , 3 -Trichlorobenzene <0.3 1 0.31 96 - 18-4 1,2,3-Trichloropropane <0.12 0.12 120 - 82-1 1,2,4 -Trichlorobenzene <0.31 0 0 31 95-63-6 1,2,4 - Trimethylbenzene <0.12 0 . 1 2 96-12 - 8 1,2-Dibromo- 3- <0.31 0.31

chloropropane 106 - 93-4 1,2-Dibromoethane <0.062 0.062 95-50 - 1 1,2-Dichlorobenzene <0.12 0 . 12 107 - 06-2 1,2-Dichloroethane <0.062 0.062 156 -59 - 2 cis-1,2 - Dichloroethene <0 . 062 0.062 156 - 60 - 5 trans - 1,2- Dichloroethene <0 . 062 0.062 78- 87-5 1,2-Dichloropropane <0.062 0.062 108-67-8 1,3,5-Trimethylbenzene <0.12 0.12 541-73 - 1 1,3 -Dichlorobenzene <0.12 0.12 10061-01 - 5 cis - 1,3 - Dichloropropene <0 . 062 0.062 10061-02-6 trans-1,3 - Dichloropropene <0.062 0.062 110-57 - 6 trans - 1,4-Dichloro- <0.062 0.062

2-butene 106-46-7 1 ,4 - Dichlorobenzene <0.12 0.12 78 - 93-3 Methyl Ethyl Ketone <0.31 0.31 591-78 - 6 2 - Hexanone <0.31 0.31 91 - 57 - 6 2-Methylnaphthalene <0 .31 0.31 67-64-1 Acetone <0.92 0.92 108 - 10-1 4-Methyl-2-Pentanone <0 . 31 0.31 107 - 13-1 Acrylonitrile <0.31 0.31 71-43 - 2 Benzene <0 .062 0 . 062 108 - 86 - 1 Bromobenzene <0.12 0.12 74 - 97-5 Bromochloromethane <0.12 0.12

Page 50

T his tL'port •hall m>t he t<produccd cxcL" pt in full, witiHHII wriuen :tntllllrizJriun ufTri!o. l:m i' I :thor.uoric, , Inc. Individual <tllnplc '""'It' rd:ue onlr w rhc , Jmpk t<'<IL'<I.

5560 Curpural e Excltan{:c Court SE • Grand Rapids, /vii 495 1.2 • (616) ~75-4 500 • Fax (61 6) <J42-7/j6:S


ANALYTI CAL REPORT

MDEQ Submittal #: 360 24 - 1 Project: Tamarack City Stamp Mill Sampl ed: 06/04/02 @ 11:35

ERD-Superfund, Lansing Sampl er: Spiel berg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10 : 00

Extracted: Sample #: 307115 Anal yzed: 06/14/02 by DLVV Sample ID: SS -17 Ref . Citation: USEPA-8260B

Di l ution Factor : 1.23 Analyt i ca l Batch: 187270

Matrix : Soil QC Batch: 075930-114

Analytical Quant i tation MDEQ Plus List Volatiles Result Limit

CAS Number USEPA Method 503 5 /8 26 0 (mg/kg dr y ) (mg/ kg dry)

75 - 27-4 Dichlorobr omomethane <0. 1 2 0 . 12 75-25 - 2 Bromofo rm <0.12 0.12 74-83 - 9 Bromomethane <0.31 0.31 75 - 1 5 -0 Carbon Disul f i de <0. 31 0 . 3 1 56-23 - 5 Carbon Tetrachl oride <0.062 0.062 108 - 90-7 Chlorobenzene <0 . 062 0 . 062 75-00-3 Chlor oethane <0.31 0.31 67 - 66 -3 Chl oroform <0.062 0.062 74 -87-3 Chloromethane <0.31 0.31 1 24 - 48 - 1 Chlorodibromometha ne <0.12 0.12 74 -95 -3 Dibromometh a ne <0.12 0.12 75-71-8 Dichl orodifluoromethane <0.31 0 .31 60-29-7 Ethyl Ether <0 . 31 0 . 31 100 - 41-4 Ethy l benzen e <0.062 0 . 062 67 - 72 -1 Hexachloroethane <0.12 0. 1 2 98 - 82-8 Isopropyl benzene <0 . 12 0 . 12 136777 - 61 - 2 Xylene, Meta & Para <0 . 12 0.12 74-88-4 Iodomethane <0.12 0.12 1634 - 04-4 Methy l (tert)bu tyl Ether <0.31 0 . 31 75 - 09 - 2 Methylene Chlori de <0 .31 0.31 91-20-3 Naphthalene <0.31 0 . 31 104 - 51 -8 n-Buty l benzene <0.31 0 . 31 1 03-65-1 n - Propyl ben zene <0.12 0.12 95-47-6 a - Xyl ene <0 . 062 0 . 062 99 - 87-6 4 - Isopropyltoluene <0.31 0.31 135-98-8 sec-Butylbenzene <0.31 0 . 31 1 00 - 42-5 Styrene <0 . 062 0 . 062 98-06-6 tert - Buty l ben zene <0.31 0.31 127- 18 - 4 Tetrachloroethene <0.062 0.062 109 - 99 - 9 Tetrahydrofuran <1 . 2 1 . 2 108 - 88-3 Toluene <0 . 06 2 0.062 79 - 01 - 6 Trich l oroethen e <0 .0 62 0.062 75 -69-4 Trich l orof l uoromethane <0 . 31 0.31 75 - 01-4 Vinyl Chl oride <0 . 12 0 . 12

Page 51

Thi' report , ldlnot he rt'ptOduced exccpr in full. widuun written .ltrtluuiz.uiun ufTrii\ l:u rix l .rhnr.ltolir,, Inc. Individual ,,1111ple rcsttll> rd:ne rHll)' rn tile "'"'pic tl'ltcd .

'5560 Cut por:lt l' Exchange Courr SE • Grand Rapid ., , 1VII 495 12 • (6 1Cl} 975-4500 • Fax (6 1(,) 'J42-7It6 j

~ TriMatrix f~ Laboratories, Inc:.

ANALYTICAL REPORT

MDEQ Submi t tal # : 36024 - 1 Project: Tamarack Ci t y Stamp Mi l l Sampled: 06/04/02 @ 11 :20

ERD - Superf und, Lansing Sampl er : Spielber g Submittal: June 4, 2002 Soi l s Recei ved: 06/06/02 @ 10:00

Sampl e #: 307116 Sample I D: SS-18

Matri x : Soil

Analytical Quant. Analysis Reference Parameter Result Limit Uni t Date Chern Citation

-- --- ------- --- ----- --- -- ---- ------ --- --- -- - ------- --- -- -- -- -- - -- ---- - -- --- - -Percent Solids 92 0 . 1 % 06/ 07/02 GEH SW-846 35508

Page 52

T lti' '''POll shall not be repoudll<«l cX<epo in full . wio ltnut wriucn .uorllllriz.uiun ufTrill l.uri~ J,,hnr.unoic,, Inc. lndil'idoo.ol >ao uple re,uio< ,,.1.11(' only to the sample ll'Stnl.

5560 Curpumt· P.xc:hange C nun SE • Grand Rapids, 1-vll 4Y5 12 • (6 I 6) 975-4500 • Fax (G I(,) Y42-7463


ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Proj ect : Ta marac k City Stamp Mill Sampled: 06/04/02@ 11:20

ERD - Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02 @ 10:00

Extracted: Sample # : 307116 Analyzed: 06/14 /02 by DLVV Sample ID: SS-18 Re f . Citation: USEPA- 8260B

Dilution Fac tor: 1.09 Ana lytical Batch: 187270




630-20-6 1 , 1,1, 2 -Tetrachloroethane <0 .11 0.11 71 - 55-6 1,1,1-Trichloroethane <0.055 0.055 79-34-5 1 ,1,2,2 - Tetrach loroethane <0.11 0 .11 7 9 - 00-5 1 ,1,2 - Trichloroethane <0.055 0.055 75 - 34- 3 1 , 1-Dichloroethane <0 . 055 0.055 75-35-4 1,1-Dichloroe thylene <0 . 055 0.055 87 - 61-6 1,2, 3 - Trichlorobenzene <0 . 27 0.27 96 - 18-4 1,2,3-Trichloropropane <0.11 0 . 11 120 - 82 - 1 1,2,4 - Trichlorobe nzene <0.27 0.27 95-63-6 1,2,4- Trimethylbenzene <0 . 11 0.11 96 - 12 - 8 1, 2 - Dibromo-3- <0 .27 0. 27

chloropropane 106-93 - 4 1,2 - Dibromoethane <0.055 0.055 95 - 50-1 1,2-Dichlorobenzene <0.11 0. 11 107-06-2 1 ,2 -Dichloroethane <0.055 0.055 156 - 59 -2 cis - 1,2 - Dichloroethene <0.055 0.055 156 - 60 - 5 tran s - 1,2-Dichloroethene <0 . 055 0.055 78-87 -5 1,2-Dichloropropane <0.055 0.055 108 - 67-8 1, 3,5-Trimethylbenzene <0. 11 0.11 541 - 73 - 1 1 ,3-Dichl orobenze ne <0.11 0 . 11 10061 - 01 - 5 cis-1,3 - Dichlo ropropene <0.055 0.055 10061 - 02 - 6 trans-1,3-Dichloropropene <0.055 0.055 110 -57- 6 trans - 1 ,4-Dichloro- <0.055 0.055

2 - butene 10 6- 46 - 7 1,4 - Dichlorobenzene <0 . 11 0 . 11 78 -93 - 3 Methyl Ethyl Ketone <0.27 0 .2 7 591-7 8- 6 2 - Hexanone <0 . 27 0 . 27 91 - 57-6 2 - Methylnaphthalene <0.27 0 .27 67- 64-1 Acetone <0.82 0.82 108 - 10 - 1 4 - Methyl-2 - Pentanone <0 . 2 7 0 . 27 107 - 13 - 1 Acry lonitrile <0.27 0 . 27 71 - 43 - 2 Benzene <0 .055 0 . 055 108 - 86-1 Bromobenzene <0 . 1 1 0 . ll 74-97-5 Bromochloromethane <0 .11 0 . 11

Pag e 53

Thi, « pun , l,, ll ,un be rcprodut·n l ~X<~Jil in fu ll, wirhour wriuen :llllhurit.n iuu nfl ri,\btrix Lohur .Huri~'• lil t. lndi"idu;d s.uu ple '"''"'' rchre nnlr ro rhe ;;unple te,rn l.

5560 Corpor;He Exchangt· Cou rt SE • Gr~ nJ Rapids, i\•11 495 1.2 • (G I G) 9 75-4500 • F;lx (616) 942- 746 .1

~ TriMatrix ·~ Labmnl01i es, Inc.

ANALYTICAL REPORT



Extracted: Sample#: 307116 Analyzed: 06/14/02 by DLVV Sample ID: SS-18 Ref. Citation: USEPA - 8260B





75 -27-4 Dichl orobromomethane <0.11 0.11 75 -2 5-2 Bromoform <0 . 11 0.11 74-83-9 Bromomethane <0.27 0.27 75 - 15-0 Carbon Disulfide <0 .2 7 0.27 56 -2 3 - 5 Carbon Tetrachloride <0 . 055 0 . 055 108 - 90-7 Chlorobenzene <0.055 0.055 75 - 00 -3 Chloroethane <0 . 27 0.27 67 - 66 -3 Chloroform <0.055 0.055 74 - 87 - 3 Chloromethane <0.27 0.27 124 - 48-1 Chlorodibromomethane <0.11 0.11 74 -95- 3 Dibromomethane <0.11 0.11 75 - 71-8 Dichlorodifluoromethane <0.27 0.27 60-29-7 Ethyl Ether <0.27 0.27 100 - 41-4 Ethylbenzene <0.055 0 . 055 67 -72 - 1 Hexachloroethane <0.11 0.11 98-82-8 Isopropylbenzene <0.11 0. 11 136777 - 61-2 Xylene, Meta & Para <0.11 0.11 74 - 88-4 Iodomethane <0 .11 0.11 1634 - 04 - 4 Methyl(tert)butyl Ether <0. 27 0 . 27 75 - 09-2 Methylene Chloride <0.27 0 . 27 91 - 20-3 Naphthalene <0 . 27 0.27 104 - 51-8 n-Butylbenzene <0.27 0.27 103 -65 - 1 n - Propylbenzene <0 .11 0 . 11 95-47 - 6 a-Xylene <0.055 0.055 99- 87-6 4 - Isopropyltoluene <0.27 0 . 27 135-98 -8 sec -Butylbenz ene <0.27 0 .27 10 0 - 42-5 Styrene <0 . 055 0.055 98 -06 - 6 tert - Butylbenzene <0.27 0.27 127-18 -4 Tetrachl oroethene <0.055 0 . 055 109 - 99-9 Tetrahydrofuran <1.1 1 . 1 108-88 -3 Toluene <0.055 0.055 79 - 01-6 Trichloroethene <0.055 0.055 75 - 69-4 Trichlorofluoromethane <0.27 0.27 75-01-4 Vinyl Chloride <0.11 0.11

Page 54

' I hi' report <hall nor be reproduced e \l e)ll in lioll. widolllll woiucn authuriz.nion ufTril>l.urix l .lhllr.Hwil·<, Inc. lndividn:ol '"lll)'le "" "'' ' rd~t<' only to rhc s.1mplc tl'llcJ .

5560 Co rporate Exchan g<' Cnurt SE • GrJnd Rapids, /vi i 4~5 1 2 • (6111) 975-4500 • Fax (616) ~42-746.>

~ TriMatrix f~ Labomlories, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024 -1 Project: Tamarack City Stamp Mill Sampled: 06/04/02 @ 11:25

ERD-Superfund, Lansing Sampler : Spielberg Submittal: J une 4, 2002 Soils Received: 06/06/02@ 10:00

Sample #: 307117 Sampl e ID: SS-19

Matrix: Soil

Analytical Quant. Analysis Reference Parameter Result Limit Unit Date Chern Citation --- -- -- --- ---- - - -- -- - - - -- ---- -- ---- -- -- -- --- -- -- ----- - -- - -- - -- -- ------- ---- --Percent Solids 92 0.1 % 06/07/02 GEH SW-846 3550B

Page 55

Thi< r~pou shall no t l>c "'l""ducrd except in full , withnut written authurizJtion ufTri~l.uri' l .thur.twri~'• Inc. Individual ,;tmpk· r<·sult< rchnr onlr tn the s.tmpk· tntcd.

5560 Corporate Exch angt· Court SE • GranJ R;lpids, M l 495 12 • (ll l ll) 975-4500 • Fax (616) 942-74 63


ANALYTICAL REPORT


ERD- Superfund, Lansing Sampler: Spielberg Submittal: June 4, 2002 Soils Received: 06/06/02@ 10:00

Extracted: Sample#: 307117 Analyzed: 06/14/02 by DLVV Sample ID: SS-19 Ref. Citation: USEPA- 8260B





630-20 - 6 1,1,1,2-Tetrachloroethane <0 .10 0.10 71 - 55-6 1,1,1-Trichloroethane <0.050 0.050 79-34-5 1,1,2,2 - Tetrachloroethane <0.10 0.10 79 - 00-5 1,1,2 - Trichloroethane <0.050 0.050 75 - 34-3 1,1-Dichloroethane <0.050 0 . 050 75 - 35 - 4 1,1-Dichloroethylene <0.050 0.050 87-61-6 1,2,3 -Trichlorobenzene <0.25 0.25 96 - 18-4 1,2,3-Trichloropropane <0. 10 0.10 120-82 - 1 1, 2 ,4 - Trichlorobenzene <0.25 0.25 95 - 63-6 1 ,2,4-Trimethylbenzene <0 . 10 0.10 96-12-8 1,2-Dibromo-3 - <0 .25 0.25

chloropropane 106-93-4 1,2-Dibromoethane <0.050 0.050 95 - 50-1 1,2 - Dichlorobenzene <0 .10 0.10 107 - 06-2 1,2-Dichloroethane <0.050 0.050 156-59-2 cis-1,2 - Dichloroethene <0 .050 0.050 156-60 - 5 trans - 1,2 - Dichloroethene <0.050 0.050 78 - 87-5 1,2 - Dichloropropane <0 .050 0.050 108 - 67-8 1,3,5-Trimethylbenzene <0.10 0 . 10 541-73 - 1 1,3 - Dichlorobenzene <0. 10 0.10 10061-01-5 cis-1,3 - Dichloropropene <0.050 0.050 10061-02 - 6 trans-1,3-Dichloropropene <0.050 0.050 110-57-6 trans-1,4-Dichloro- <0 . 050 0.050

2 - butene 106-46 - 7 1,4-Dichlorobenzene <0 . 10 0.10 78 - 93-3 Methyl Ethyl Ketone <0 . 25 0.25 591 - 78-6 2-Hexanone <0 . 25 0.25 91-57-6 2 - Methylnaphthalene <0.25 0.25 67-64-1 Acetone <0.75 0.75 108 - 10-1 4-Methyl-2 - Pentanone <0 . 25 0.25 107 -13 - 1 Acrylonitrile <0.25 0.25 71 - 43 - 2 Benzene <0.050 0.050 108-86-1 Bromobenzene <0.10 0.10 74-97 - 5 Bromochloromethane <0.10 0.10

Page 56

T his repml ' hall nor be t~pJUd ucnl r\«' Jll in full , wi thout written .nu hori ,,uilln llf1ii~ l.ur ix bbor.uuri~' · Inc. lndividuol ,,unple r,·,uhs rclntc 1111l)' tu th,· ,,unpi<· tell<'<!.

5560 Corpo r3!c EXl·bang<: Coun SE • Grand Rapids, t\-11 4 ') 5 12 • (61 6) ')75-4500 • Fax (61 6) 942-746.1

~ TriMatrix f~ L<tboratori es, Inc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarac k City Stamp Mill Sampled: 06/04/02 @ 11: 25



Dilution Factor : 1 Analytical Batc h: 187270

Matrix: Soil QC Batch : 075930- 1 14



75-27 - 4 Dichlorobromomethane <0.10 0.10 75-25 - 2 Bromoform <0.10 0.10 74 - 83-9 Bromomethane <0.25 0.25 75-15-0 Carbon Disulfide <0 . 25 0.25 56 - 23 - 5 Carbon Tetrachloride <0.050 0.050 108-90- 7 Chlorobenzene <0 . 050 0.050 75-00 - 3 Chloroethane <0.25 0 .25 67-66 - 3 Chloroform <0 .050 0 . 050 74-87-3 Chloromethane <0.25 0.25 124-48 - 1 Chlorodibromomethane <0.10 0 . 10 74 - 95-3 Dibromomethane <0.10 0.10 75-71 - 8 Dichlorodifluoromethane <0.25 0 . 25 60-29- 7 Ethyl Ether <0.25 0.25 100 - 41-4 Ethylbenzene <0 . 050 0.050 67-72 - 1 Hexachloroethane <0 . 10 0 .10 98 - 82 - 8 Isopropylbenzene <0.10 0 . 10 136777-61-2 Xylene, Meta & Para <0 . 10 0.10 74-88 - 4 I odomethane <0.10 0.10 1634-04-4 Methyl(tert)butyl Ether <0.25 0.25 75-09-2 Methylene Chloride <0.25 0.25 91-20 - 3 Naphthalene <0 . 25 0.25 1 04-51-8 n - Butylbenzene <0.25 0.25 103-65- 1 n-Propylbenzene <0 .10 0.10 95 - 47-6 o-Xylene <0 . 050 0.050 99-87-6 4 - Isopropyltoluene <0.25 0.25 135-98 - 8 sec - Butyl benzene <0 . 25 0 . 25 100-42 - 5 Styrene <0 .050 0.050 98-06-6 tert-Butylbenzene <0.25 0. 25 12 7-18 - 4 Tetrachloroethene <0.050 0.050 109-99-9 Tetrahydrofuran <1.0 1.0 108 - 88 - 3 Toluene <0.050 0.050 79 - 01-6 Trichloroethene <0.050 0.050 75 - 69-4 Trichlorofluoromethane <0.25 0 . 25 75-01 - 4 Vinyl Chloride <0.10 0.10

Page 57

T hi< · ~poll sh·ll not b~ rcproduL~d t:Xcept in lioll, wiohour wrinrn .uuhorit.uiun urTri.\t .uri' I .obor.ttori"· lnt'. lndividuotl sJmpk• r<:lub rebtt' unlr w " "' s.omplr on ted.

55GO Corporate Ext'hange Court SF. • Gra nd Rapids, 1'vll <195 12 • (6 1()) 975-4500 • Fax (G IG) 942-7463


ANALYTICAL REPORT

MDEQ Submi t tal #: 36024 -1 Proj e ct: Tamarack City Stamp Mi ll Sampl ed: 06 / 04/02 @ 11: 10

ERD-Superfund , Lansing Sampl er: Spiel berg Submittal: June 4 , 2002 Soils Received: 06/06/02 @ 10 : 00

Sa mple # : 307118 Sample I D: SS-20

Ma tri x : Soil

Analyt i cal Quant. Analysis Refer ence Parameter Result Limit Unit Date Chern Citation

-- ---- --- --- -- ------ ---- - ----- ----- --------- -- -- ---- -- - - - - -- -- ----- -- ---- -- --Percent Solids 93 0. 1 % 06/07/02 GEH SW-846 3SSOB

Page 58

Thi< r~port , h.tll not I>~ r~prmlttt~d except in full. without writt<·n :unhori~.u iun ofTrii\ I:Hrix l .t hur.ttmi~'• Inc. lndi"idu.tl <.unpl<' r~<uh< rd.nt· onlr 10 rhe ,,unple resred.

5560 Corpor:ll e Exchange Coun SE • Gra nd Ra pid:., ,\If 495 12 • (() I()) 975-4500 • Fax (GIG) 942-7463


ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tamarack City Stamp Mi l l Sampl ed: 06 / 04/02 @ 11:10

ERD - Superfund, Lan s i ng Sampler: Spielberg Submittal: June 4, 2002 Soils Received : 06/06 / 02@ 10:00

Extracted : Sample #: 307118 Analyzed: 06/14/02 by DLVV Sample ID: SS-20 Ref. Citation: USEPA- 8260B

Dilution Factor: 1 .03 Analytical Batch: 1 87270




630-20 - 6 1,1,1,2-Tetrachloroethane <0.10 0.10 71 - 55 - 6 1,1, 1- Trichloroethane <0.052 0 . 052 79 - 34 - 5 1,1,2,2 - Tetrachloroethane <0.10 0.10 7 9-00 - 5 1,1,2-Trichloroethane <0.052 0 . 052 75-34 - 3 1,1- Dichloroethane <0.052 0.052 75 - 35-4 1,1- Dichloroethylene <0 .05 2 0 . 052 87-61-6 1,2,3 - Trichl orobenzene <0.26 0 . 26 96 - 18 - 4 1,2,3-Trichloropropane <0 . 10 0.10 120-82 - 1 1,2,4-Trichlorobenzene <0 . 26 0.26 95 - 63-6 1,2,4 - Trimethyl benzene <0.10 0.10 96 - 12-8 1, 2 - Dibromo-3- <0.26 0 . 26

chloropropane 106-93 - 4 1,2-Dibromoethane <0.052 0.052 95 - 50 - 1 1,2 - Di chlorobenzene <0 .1 0 0.10 107-06 - 2 1,2 - Dichloroethane <0.052 0.052 156-59 - 2 cis-1,2 - Dichloroethene <0.052 0 . 052 1 56 - 60 - 5 trans - 1,2-Dichl oroethene <0 . 052 0.052 78 - 87 - 5 1 , 2-Dichloropropane <0.052 0.052 108-67- 8 1,3,5-Trimethylbenzene <0.10 0.10 541-73-1 1,3 - Dichlorobenzene <0. 1 0 0 . 10 10061 - 01 - 5 cis-1,3-Dichloropropene <0.052 0.052 10061 - 02 - 6 trans-1,3 - Dichloropropene <0.052 0 . 052 110-57 - 6 trans - 1,4- Dichloro- <0 . 052 0.052

2-butene 106 - 46-7 1,4 - Dichlorobenzene <0. 1 0 0.10 78-93 - 3 Methyl Ethyl Ke tone <0. 26 0 . 26 591 - 78- 6 2-Hexanone <0.26 0.26 91-57 - 6 2-Methylnaphthalene <0.26 0 . 26 67 - 64 - 1 Acetone <0 . 77 0.77 108-10 - 1 4-Methyl-2 - Pentanone <0.26 0.26 107-13- 1 Acrylonitrile <0 .2 6 0.26 71 - 43 -2 Be n zene <0.052 0.052 108-86 -1 Bromobenzene <0.10 0.10 74 - 97 - 5 Bromochloromethane <0.10 0 . 10

Page 59

T hi1 r~port dt.tll 1101 he •cprnducd <'X<l'pt i11 fu ll, wid10t11 wri ltcn .uulturit.u ion of lii.\ l.mix Lthor.uoric>, Inc. lndi1·idual s.tmplc results rdatc on ly 10 the '"m plc t <·>~< d.

5 5<l0 Cur porJ tl' ExchJ ngl' C ourt SF. • G ran J Rap ids , ,\I I 495 12 • (G I G) 975- 450 0 • f. ;Jx (ol6) 'Jit2-71tG3

~ TriMatrix ~~ Li!homlories, Inc.

ANALYTICAL REPORT



Extracted : Sample #: 307118 Analyzed: 06/14/02 by DLW Sample ID: SS-20 Ref. Citation: USEPA- 8260B

Di lution Factor: 1.03 Analyti cal Batch: 187 270

Matrix: Soil QC Batch: 075930-1 14

Analytical Quantitation MDEQ Plus List Volatiles Result Lirni t


75-27 - 4 Dichlorobromomethane <0 .10 0.10 75-25-2 Bromoform <0.10 0.10 74-83 - 9 Bromomethane <0 .2 6 0.26 75- 15-0 Carbon Disulfide <0 .26 0.26 56-23 - 5 Carbon Tetrachloride <0 . 052 0.052 108-90-7 Chlorobenzene <0. 052 0.052 75-00 - 3 Chloroethane <0.26 0. 26 67 - 66 - 3 Chloroform <0.052 0.052 74-87-3 Chloromethane <0.26 0. 26 124-48- 1 Chlorodibromomethane <0.10 0.10 74 - 95-3 Dibromomethane <0.10 0.10 75 - 71-8 Dichlorodifluoromethane <0.26 0.26 60-29 - 7 Ethyl Ether <0.26 0 . 26 100-41 -4 Ethylbenzene <0.052 0.052 67-72 - 1 Hexachloroethane <0 .10 0.10 98-82 - 8 Isopropylbenzene <0 .10 0.10 136777 - 61 -2 Xylene, Meta & Para <0.10 0.10 74-88-4 Iodomethane <0.10 0.10 1634-04 - 4 Methyl(tert)butyl Ether <0.26 0.26 75 - 09-2 Methylene Chloride <0.26 0.26 91-20-3 Naphthalene <0.26 0.26 104-51- 8 n - Butylbenzene <0.26 0.26 103-65- 1 n - Propylbenzene <0 . 10 0.10 95-47-6 o-Xylene <0 . 052 0.052 99- 87 - 6 4 - Isopropyltoluene <0.26 0.26 135-98- 8 sec - Butylbenzene <0.26 0.26 100 - 42 - 5 Styrene <0 . 052 0.052 98-06 - 6 tert-Butylbenzene <0.26 0.26 127-18-4 Tetrachloroethene <0 . 052 0.052 109-99 - 9 Tetrahydrofuran <1.0 1.0 108-88 - 3 Toluene <0.052 0.052 79 - 01-6 Trichloroethene <0.052 0 . 052 75-69-4 Trichlorofluoromethane <0.26 0.26 75-01- 4 Vinyl Chloride <0.10 0.10

Page 60

Thi' rcpuoo ,h,rllnot he reproduced cxcq11 in full. witlrunc wril!cn .urchnriutinn nfTri.\l.urix bbor.uori<'>. lnL lmli\·iduoJ ,,rmplc IC>tth> rd.uc onlr to eire '"'"l'lc cc<el·d .

5560 C orpora te Exclrangl' C ourt S l~ • Gra nd Rapids, Ml 495 12 • (G IG) ~75-4500 • Fax (6 16) 942-74Gj

~ TriMatrix ~~LilhOtillOi iCs, lnc.

ANALYTICAL REPORT

MDEQ Submittal #: 36024-1 Project: Tama rack City Stamp Mi ll Sampled: 06/04/02 @ 10:45

ERD -Superfund, Lansing Sampler: Spiel berg Submittal: June 4, 200 2 Soils Rece i ved : 06/06/02 @ 10 : 00


Matrix: Soil

Analytical Quant. Analysis Refe rence Parameter Result Limit Unit Date Chern Citation

Percent Solids 93 0.1 % 06/07/02 GEH SW-846 3 5508

Page 61

T hi< report ,ll.lllnnt h,· rq nnduced except in full , withour writt<' ll .nrtlrurit;uioll ufTr i ~ l;u r ix Labor.Horin, Inc l11d i"idual '""'l'lc IL'<trl r- rcLH~ unlr to th~ ' arnple ' ~' ' "' 1.

5560 Corporal <: Exchanbc C uu rr S E • Gr.rnd ltt picl s, a\•11 4') 5 12 • (GI G) 975-4500 • f-:tx (6 16) 9til-746j

~ TriMatrix ~~ L.1homlorles, Inc. -----------------------------------------------------------------------

ANALYTICAL REPORT


ERD-Superfund , Lansing Sampler: Spie l ber g Submittal: June 4 , 2002 Soils Received : 06/06/02 @ 1 0:00

Extracted: Sample It: 307119 Ana lyzed: 06/13/02 by LEI·/ Sampl e ID : SS-21 Ref. citation: USEPA - 82608

Dilut ion Factor : 1 Analytical Batch: 187112

Mat rix: Soil QC Batch: 076008-113


CAS Number * USEPA Method 5035/8260 (rng / kg dry) (mg/kg dry)

630 - 20-6 1,1,1,2 - Tetrachloroethane <0.10 0.10 71-55-6 1 ,1,1 -Trichloroethane <0.050 0 . 050 79-34-5 1,1 ,2 ,2 -Tetrachloroethane <0 .10 0. 10 79 - 00-5 1,1,2 - Trichloroethane <0. 050 0.050 75 - 34-3 1,1-Dichloroethane <0.050 0 . 050 75-35-4 1,1-Dichloroethylene <0.050 0 . 050 87 - 61 - 6 1,2,3 -Tr ichlorobenzene <0.25 0.25 96-18-4 1,2,3-Trichloropropane <0. 10 0. 10 120-82-1 1, 2 ,4 - Trichlorobenzene <0.25 0.25 95 - 63 - 6 1,2,4-Trimethylbenzene <0 .10 0 . 10 96 - 12 - 8 1, 2 - Dibromo- 3 - <0.25 0 . 25

chloropropane 106-93 - 4 1,2-Dibromoethane <0 . 050 0.050 95-50-1 1,2 - Dichlorobenzene <0.10 0.10 107-06 - 2 1,2-Di chloroethane <0.050 0 . 050 156 - 59-2 cis-1,2 - Dichloroethene <0 .0 50 0. 050 156-60-5 trans-1,2-Dichloroethene <0 . 050 0 . 050 78-87-5 1 , 2-Dichloropropane <0 . 050 0 . 050 108 -67-8 1,3,5-Trimethylbenzene <0.10 0. 10

54 1 -73-1 1,3-Dichloroben zene <0.10 0 . 10 10061 - 01 - 5 cis-1,3-Dichloropropene <0 . 050 0 .050 10061-02-6 trans- 1 ,3 - Dichloropropene <0.050 0.050 110-57-6 trans - 1 ,4-Dichloro- <0 .0 50 0 . 050

2-butene 106 - 46 -7 1,4-Dichlorobenzene <0.10 0. 10 78-93-3 Methyl Ethyl Ketone <0.25 0 . 25 591-78- 6 2 - Hexanone <0 .2 5 0.25 91-57-6 2 - Methylnaphtha l ene <0.25 0.25 67 - 6 4 - 1 Acetone <0 . 75 0.75 108 - 10-1 4 - Methyl - 2 - Pentanone <0.25 0.25 107 - 13-1 Acrylonitri l e <0 .2 5 0.25 71-43-2 Benzene <0.050 0.050 108-86- 1 Bromobenzene <0 .10 0.10 74 - 97 - 5 Bromochloromethane <0 .10 0 . 10

* See a t tached Statement of Data Qual i fications.

Page 62

I hi1 r~port ; hall nut be r<prmluncd except in full. without wriucn aurhoriz:uion ofTr i,\larrix L.rbur.uurit ,, Inc. Individual >.tmplc rc<rdt> relate nnlr ru rhc <omplc rcsrctl.

55 (;0 C o rporat e Exch:111ge C nnn SE • Cr:tnJ Rapid.,, r\ 11 4 ~ 5 1 2 • (rl l 6) 975-4500 • F:1x ((, 16) ')42-7 tl6.i

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