e-Hardcopy 2.0 SDMS DOCID#1142263 Automated ReportProject: PGA-N Phoenix-Goodyear Airport North, 102...

06/22/11

Technical Report for

Matrix New World Engineering, Inc.

PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

11-100E-06

Accutest Job Number: C16602

Sampling Date: 06/17/11

Report to:

Matrix New World Engineering, Inc.

[email protected]

ATTN: Jody Mack

Total number of pages in report:

Certifications: CA (08258CA) AZ (AZ0762) DoD/ISO/IEC 17025:2005 (L2242)

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

Test results relate only to samples analyzed.

Northern California • 2105 Lundy Ave. • San Jose, CA 95131 • tel: 408-588-0200 • fax: 408-588-0201 • http://www.accutest.com

Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Conference

and/or state specific certification programs as applicable.

Client Service contact: Beth Proffitt 408-588-0200

Laurie Glantz-MurphyLaboratory Director

Northern California

06/22/11

e-Hardcopy 2.0Automated Report

19

Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.

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SDMS DOCID#1142263

1111 Ill ACCUTEBT

L/\BO~/\TO~IES

•• • ACCUTEST.

Table of Contents-1-

Sections:

Section 1: Sample Summary ................................................................................................... 3Section 2: Sample Results ........................................................................................................ 4

2.1: C16602-1: EA08-EFF-06172011 ................................................................................. 52.2: C16602-2: TB001-06172011 ........................................................................................ 7

Section 3: Misc. Forms ............................................................................................................ 93.1: Chain of Custody ........................................................................................................... 10

Section 4: GC/MS Volatiles - QC Data Summaries .............................................................. 124.1: Method Blank Summary ................................................................................................ 134.2: Blank Spike Summary ................................................................................................... 154.3: Blank Spike/Blank Spike Duplicate Summary .............................................................. 164.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 18

12

34

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Accutest LabLink@17136 08:28 22-Jun-2011

Sample Summary

Matrix New World Engineering, Inc.Job No: C16602

PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZProject No: 11-100E-06

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

C16602-1 06/17/11 18:00 TV 06/18/11 AQ Ground Water EA08-EFF-06172011

C16602-2 06/17/11 00:00 TV 06/18/11 AQ Trip Blank Water TB001-06172011

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Sample Results

Report of Analysis

Northern California

Section 2

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21111 II ACCUTES--r:

LABORATORIES

•• • ACCUTEST. L.A . QftAYDftt • •


Report of Analysis Page 1 of 2

Client Sample ID: EA08-EFF-06172011 Lab Sample ID: C16602-1 Date Sampled: 06/17/11 Matrix: AQ - Ground Water Date Received: 06/18/11 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 R2907.D 1 06/18/11 BD n/a n/a VR104Run #2

Purge VolumeRun #1 10.0 mlRun #2

VOA 8260 List

CAS No. Compound Result RL MDL Units Q

67-64-1 Acetone ND 20 10 ug/l71-43-2 Benzene ND 1.0 0.30 ug/l108-86-1 Bromobenzene ND 1.0 0.30 ug/l74-97-5 Bromochloromethane ND 1.0 0.50 ug/l75-27-4 Bromodichloromethane ND 1.0 0.30 ug/l75-25-2 Bromoform ND 1.0 0.50 ug/l104-51-8 n-Butylbenzene a ND 5.0 0.50 ug/l135-98-8 sec-Butylbenzene a ND 5.0 0.50 ug/l98-06-6 tert-Butylbenzene ND 5.0 0.50 ug/l108-90-7 Chlorobenzene ND 1.0 0.30 ug/l75-00-3 Chloroethane ND 1.0 0.30 ug/l67-66-3 Chloroform ND 1.0 0.30 ug/l95-49-8 o-Chlorotoluene ND 5.0 0.50 ug/l106-43-4 p-Chlorotoluene ND 5.0 0.50 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-34-3 1,1-Dichloroethane ND 1.0 0.30 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l563-58-6 1,1-Dichloropropene ND 1.0 0.30 ug/l106-93-4 1,2-Dibromoethane ND 1.0 0.20 ug/l107-06-2 1,2-Dichloroethane ND 1.0 0.30 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.30 ug/l142-28-9 1,3-Dichloropropane ND 1.0 0.30 ug/l594-20-7 2,2-Dichloropropane ND 1.0 0.30 ug/l124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l75-71-8 Dichlorodifluoromethane a ND 1.0 0.30 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.30 ug/l10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.50 ug/l541-73-1 m-Dichlorobenzene ND 1.0 0.30 ug/l95-50-1 o-Dichlorobenzene ND 1.0 0.30 ug/l106-46-7 p-Dichlorobenzene ND 1.0 0.30 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.30 ug/l10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.20 ug/l

ND = Not detected MDL - Method Detection Limit J = Indicates an estimated valueRL = Reporting Limit B = Indicates analyte found in associated method blankE = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

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Client Sample ID: EA08-EFF-06172011 Lab Sample ID: C16602-1 Date Sampled: 06/17/11 Matrix: AQ - Ground Water Date Received: 06/18/11 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

VOA 8260 List


100-41-4 Ethylbenzene ND 1.0 0.30 ug/l591-78-6 2-Hexanone ND 20 10 ug/l99-87-6 p-Isopropyltoluene ND 5.0 0.50 ug/l108-10-1 4-Methyl-2-pentanone ND 20 5.0 ug/l74-83-9 Methyl bromide ND 5.0 1.5 ug/l74-87-3 Methyl chloride ND 1.0 0.30 ug/l75-09-2 Methylene chloride ND 20 5.0 ug/l78-93-3 Methyl ethyl ketone ND 20 5.0 ug/l1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.50 ug/l103-65-1 n-Propylbenzene ND 5.0 0.50 ug/l100-42-5 Styrene ND 1.0 0.20 ug/l71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l87-61-6 1,2,3-Trichlorobenzene ND 5.0 0.50 ug/l96-18-4 1,2,3-Trichloropropane ND 5.0 0.50 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.50 ug/l95-63-6 1,2,4-Trimethylbenzene ND 5.0 0.50 ug/l108-67-8 1,3,5-Trimethylbenzene ND 5.0 0.50 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.20 ug/l108-88-3 Toluene ND 1.0 0.50 ug/l79-01-6 Trichloroethylene ND 1.0 0.30 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.30 ug/l75-01-4 Vinyl chloride ND 1.0 0.30 ug/l108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l

m,p-Xylene ND 1.0 0.50 ug/l95-47-6 o-Xylene ND 1.0 0.20 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 100% 60-130%2037-26-5 Toluene-D8 99% 60-130%460-00-4 4-Bromofluorobenzene 96% 60-130%

(a) CCV outside of control limits (biased high); not detected in sample.


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Client Sample ID: TB001-06172011 Lab Sample ID: C16602-2 Date Sampled: 06/17/11 Matrix: AQ - Trip Blank Water Date Received: 06/18/11 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 R2906.D 1 06/18/11 BD n/a n/a VR104Run #2

Purge VolumeRun #1 10.0 mlRun #2

VOA 8260 List


67-64-1 Acetone ND 20 10 ug/l71-43-2 Benzene ND 1.0 0.30 ug/l108-86-1 Bromobenzene ND 1.0 0.30 ug/l74-97-5 Bromochloromethane ND 1.0 0.50 ug/l75-27-4 Bromodichloromethane ND 1.0 0.30 ug/l75-25-2 Bromoform ND 1.0 0.50 ug/l104-51-8 n-Butylbenzene a ND 5.0 0.50 ug/l135-98-8 sec-Butylbenzene a ND 5.0 0.50 ug/l98-06-6 tert-Butylbenzene ND 5.0 0.50 ug/l108-90-7 Chlorobenzene ND 1.0 0.30 ug/l75-00-3 Chloroethane ND 1.0 0.30 ug/l67-66-3 Chloroform ND 1.0 0.30 ug/l95-49-8 o-Chlorotoluene ND 5.0 0.50 ug/l106-43-4 p-Chlorotoluene ND 5.0 0.50 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-34-3 1,1-Dichloroethane ND 1.0 0.30 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l563-58-6 1,1-Dichloropropene ND 1.0 0.30 ug/l106-93-4 1,2-Dibromoethane ND 1.0 0.20 ug/l107-06-2 1,2-Dichloroethane ND 1.0 0.30 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.30 ug/l142-28-9 1,3-Dichloropropane ND 1.0 0.30 ug/l594-20-7 2,2-Dichloropropane ND 1.0 0.30 ug/l124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l75-71-8 Dichlorodifluoromethane a ND 1.0 0.30 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.30 ug/l10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.50 ug/l541-73-1 m-Dichlorobenzene ND 1.0 0.30 ug/l95-50-1 o-Dichlorobenzene ND 1.0 0.30 ug/l106-46-7 p-Dichlorobenzene ND 1.0 0.30 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.30 ug/l10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.20 ug/l


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22.2




Client Sample ID: TB001-06172011 Lab Sample ID: C16602-2 Date Sampled: 06/17/11 Matrix: AQ - Trip Blank Water Date Received: 06/18/11 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

VOA 8260 List


100-41-4 Ethylbenzene ND 1.0 0.30 ug/l591-78-6 2-Hexanone ND 20 10 ug/l99-87-6 p-Isopropyltoluene ND 5.0 0.50 ug/l108-10-1 4-Methyl-2-pentanone ND 20 5.0 ug/l74-83-9 Methyl bromide ND 5.0 1.5 ug/l74-87-3 Methyl chloride ND 1.0 0.30 ug/l75-09-2 Methylene chloride ND 20 5.0 ug/l78-93-3 Methyl ethyl ketone ND 20 5.0 ug/l1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.50 ug/l103-65-1 n-Propylbenzene ND 5.0 0.50 ug/l100-42-5 Styrene ND 1.0 0.20 ug/l71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l87-61-6 1,2,3-Trichlorobenzene ND 5.0 0.50 ug/l96-18-4 1,2,3-Trichloropropane ND 5.0 0.50 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.50 ug/l95-63-6 1,2,4-Trimethylbenzene ND 5.0 0.50 ug/l108-67-8 1,3,5-Trimethylbenzene ND 5.0 0.50 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.20 ug/l108-88-3 Toluene ND 1.0 0.50 ug/l79-01-6 Trichloroethylene ND 1.0 0.30 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.30 ug/l75-01-4 Vinyl chloride ND 1.0 0.30 ug/l108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l


CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits




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22.2



Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Chain of Custody

Northern California

Section 3

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3

1111 II ACCUTES--r:

LABORATORIES


C16602: Chain of CustodyPage 1 of 2

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C16602

33.1

• CHAIN OF CUSTODY

• ACCUTES"T; 2105lundy Ava, SonJoso, CA 95131

,,.~ ..... ,~~ - , . .... "'""c ...... .

(~OB) 5811·0200 FAX: (408) 588-0201 11 [Accut"*\ NC J<>b '' C C1 LABORATOR IE S '' 1VI\iFPt-l.f3i;4-D --- ~ r Hepon" g tntonna~o ..

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[:==J 5 O•y(WMI\Ioad dep1ndenl) Camm.erlc:LI"I!U• • Rttu•IS. OC, and chromltogr&ms

~ 30~y{12lo%mJtkup) fUL.Tt . teve14data pcetapo

(:==J 2 C•y (1$0% mrukup) ID EOFiorCiectratlcer 0 EOO Form•~·-·· ~ 1 D"y (1M"m1Jftup) ~ - -

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[=:J S.1me Dar(300% merkup) f>t ovkle EOF L.cgcod~:

Emergency TfA data available VIA Lablink " ' IVSI bo dnoumenle< belo\Y enoh Ume • OO' '"eoslon, Including cour ier de l ive~ • . ,':;1 · i ,-s~%·!,'<,~:5,

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........ RKoMno ChKkl 'N


C16602: Chain of CustodyPage 2 of 2

11 of 19

C16602

33.1

Accutest Laboratories Northern California Sample Receiving Check List Job# : c . .!.!lfo~b~oCI<1/:__ ___ _ Initial: El<

Review Chain o1 Cus1cdv

P1\l:~.(l]~s.~ 1.~Yuli:t~OIY.(I'fl:f-1f;$}.aflnlp!e:&.? ... ~ ....

v(~ pH requ-;;ed?

Chain of Custody Is to be co-mpl~te and leg1blft..

@!~Q .. .. ........ cllont.SamphldD .. ·-----·--·-OU\et.CurntnenWis.s.uos......___t---

•• Was Cllr:l"'t Informed 1hat hold time is 1.5 min?

u Wn.~ or1hr.-Pho5phate ftl!ered with in15 min?

~ samp~e \"'ilhin ho!d lime?

Arc samp!c In danger of exceeding Mld-ttme,

Yes I No

Yas (No

~xisling Client? @1 No Exfsting PmjeGl?

If No: Is R:epoctlo inft-J t:::olnplele and legib!e, Tncluding;

o deliverable o Name o At1dress o phone 11 ~1nnil

Is RHI!o inio comple1e ond ~eg!ble, ~ncludlng;

o PO# o CrecJil card a Coni act r ~addrass n phona o c-milH

Is Contac.t omdlor Prajed ManagtH ide111ified, including;

c phone oe-mEtil

Ye•l(!!? Continue Yt~~ J No

Conlinue Yos 1 No

lf91 Na

Yo• I~ @I No

o Project nama I numb~r

...S~ecia1 requireme~1t.s? iS} No

~fHnra~e IDs J date & time of col\eciJon provided'? f!!jJl No

Pis Matrix llsl131d ~r1d Mrrecl? ~I No

VAnalyses lis led, we do, or cllenl has aulhorizcd a subc:Jnlrect? ~I No

M"Chain is s.tgned and dal~d by bolh ctren1 and sample cuslDdicm? {!31 No

.rfAT requested "'ailable? (!!}J No Appwvoo by _,Pc:I'Ylc:.L ____ _

Re\llew Coolers:

lliWere all Coo,erg temprmtiUrAs lllf!asur(!d t:~t :s:a'''C? @I No

.. If cooler is outsidP.: the !;6•c; note down the affected bollles ~n lhat cooJer on thalefl J!/'Are s<trupl!ii:~ 1JI1 tea? el No

Note that ANC does NOT accept 9Vid'entiary samples. (We do uot lock refrigerators)

.,(Shipment Received Method Ff>dft (!:g\tlrdat) 9"Cusl00y Sears: Presoent Yes J @ If Yes; Unbro~en:

Reviow of Samp!o Bottlas: If you ans.wer no. explain to the side

~haln ma1chcs boUle labels? el No ~ample boUle In lad?

ds there enough s8mple vollltnfl In proper boutc for requested analyses?

~roper Preservatives? e No

Vosl No

~/No ~/No

5h~d; pH nn pre-served samptesexcepl16&1, 625, a270 and~ make notes on left

~M;~QKpaca-VOAs? Greater than 6mm In diameter t.. ~..,., "&... ~ List sample 10 and affc~1cd container ......__-{!E)

1--------+------+----------···-~

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Non-Compliance issues and discrepancies on the COC are forwarded to Project Management

\\Accunca.accutestcom\depls\qa\saps\sop_completclist_2010\current_active_sop_ocL2010\sc001t1_0_form1_samplecontrol_samplercceivingchecklist_2009-01-01.doc



GC/MS Volatiles

QC Data Summaries

Includes the following where applicable:

• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries

Northern California

Section 4

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1111 II ACCUTES--r:

LABORATORIES


Method Blank Summary Page 1 of 2 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR104-MB R2905.D 1 06/18/11 BD n/a n/a VR104

The QC reported here applies to the following samples: Method: SW846 8260B

C16602-1, C16602-2


67-64-1 Acetone ND 20 10 ug/l71-43-2 Benzene ND 1.0 0.30 ug/l108-86-1 Bromobenzene ND 1.0 0.30 ug/l74-97-5 Bromochloromethane ND 1.0 0.50 ug/l75-27-4 Bromodichloromethane ND 1.0 0.30 ug/l75-25-2 Bromoform ND 1.0 0.50 ug/l104-51-8 n-Butylbenzene a ND 5.0 0.50 ug/l135-98-8 sec-Butylbenzene a ND 5.0 0.50 ug/l98-06-6 tert-Butylbenzene ND 5.0 0.50 ug/l108-90-7 Chlorobenzene ND 1.0 0.30 ug/l75-00-3 Chloroethane ND 1.0 0.30 ug/l67-66-3 Chloroform ND 1.0 0.30 ug/l95-49-8 o-Chlorotoluene ND 5.0 0.50 ug/l106-43-4 p-Chlorotoluene ND 5.0 0.50 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-34-3 1,1-Dichloroethane ND 1.0 0.30 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l563-58-6 1,1-Dichloropropene ND 1.0 0.30 ug/l106-93-4 1,2-Dibromoethane ND 1.0 0.20 ug/l107-06-2 1,2-Dichloroethane ND 1.0 0.30 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.30 ug/l142-28-9 1,3-Dichloropropane ND 1.0 0.30 ug/l594-20-7 2,2-Dichloropropane ND 1.0 0.30 ug/l124-48-1 Dibromochloromethane ND 1.0 0.20 ug/l75-71-8 Dichlorodifluoromethane ND 1.0 0.30 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.30 ug/l10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.50 ug/l541-73-1 m-Dichlorobenzene ND 1.0 0.30 ug/l95-50-1 o-Dichlorobenzene ND 1.0 0.30 ug/l106-46-7 p-Dichlorobenzene ND 1.0 0.30 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.30 ug/l10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.20 ug/l100-41-4 Ethylbenzene ND 1.0 0.30 ug/l591-78-6 2-Hexanone ND 20 10 ug/l99-87-6 p-Isopropyltoluene ND 5.0 0.50 ug/l108-10-1 4-Methyl-2-pentanone ND 20 5.0 ug/l

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44.1.1


Method Blank Summary Page 2 of 2 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR104-MB R2905.D 1 06/18/11 BD n/a n/a VR104


C16602-1, C16602-2


74-83-9 Methyl bromide ND 5.0 1.5 ug/l74-87-3 Methyl chloride ND 1.0 0.30 ug/l75-09-2 Methylene chloride ND 20 5.0 ug/l78-93-3 Methyl ethyl ketone ND 20 5.0 ug/l1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.50 ug/l103-65-1 n-Propylbenzene ND 5.0 0.50 ug/l100-42-5 Styrene ND 1.0 0.20 ug/l71-55-6 1,1,1-Trichloroethane ND 1.0 0.20 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l79-00-5 1,1,2-Trichloroethane ND 1.0 0.20 ug/l87-61-6 1,2,3-Trichlorobenzene ND 5.0 0.50 ug/l96-18-4 1,2,3-Trichloropropane ND 5.0 0.50 ug/l120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.50 ug/l95-63-6 1,2,4-Trimethylbenzene ND 5.0 0.50 ug/l108-67-8 1,3,5-Trimethylbenzene ND 5.0 0.50 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.20 ug/l108-88-3 Toluene ND 1.0 0.50 ug/l79-01-6 Trichloroethylene ND 1.0 0.30 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.30 ug/l75-01-4 Vinyl chloride ND 1.0 0.30 ug/l108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l


CAS No. Surrogate Recoveries Limits



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44.1.1


Blank Spike Summary Page 1 of 1 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR104-BS1 R2904.D 1 06/18/11 BD n/a n/a VR104


C16602-1, C16602-2

Spike BSP BSPCAS No. Compound ug/l ug/l % Limits

CAS No. Surrogate Recoveries BSP Limits


15 of 19

C16602

44.2.1


Blank Spike/Blank Spike Duplicate Summary Page 1 of 2 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR104-BS R2901.D 1 06/18/11 BD n/a n/a VR104VR104-BSD R2903.D 1 06/18/11 BD n/a n/a VR104


C16602-1, C16602-2

Spike BSP BSP BSD BSD LimitsCAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD

67-64-1 Acetone 80 83.1 104 74.2 93 11 60-130/3071-43-2 Benzene 20 22.2 111 20.5 103 8 60-130/30108-86-1 Bromobenzene 20 21.6 108 20.1 101 7 60-130/3074-97-5 Bromochloromethane 20 22.1 111 20.0 100 10 60-130/3075-27-4 Bromodichloromethane 20 23.0 115 20.8 104 10 60-130/3075-25-2 Bromoform 20 22.3 112 20.2 101 10 60-130/30104-51-8 n-Butylbenzene 20 23.4 117 a 21.3 107 a 9 a 60-130/30135-98-8 sec-Butylbenzene 20 23.2 116 a 21.4 107 a 8 a 60-130/3098-06-6 tert-Butylbenzene 20 21.7 109 20.3 102 7 60-130/30108-90-7 Chlorobenzene 20 21.7 109 19.9 100 9 60-130/3075-00-3 Chloroethane 20 22.1 111 19.9 100 10 60-130/3067-66-3 Chloroform 20 22.4 112 20.1 101 11 60-130/3095-49-8 o-Chlorotoluene 20 21.4 107 20.9 105 2 60-130/30106-43-4 p-Chlorotoluene 20 23.0 115 20.1 101 13 60-130/3056-23-5 Carbon tetrachloride 20 23.0 115 20.8 104 10 60-130/3075-34-3 1,1-Dichloroethane 20 22.1 111 20.2 101 9 60-130/3075-35-4 1,1-Dichloroethylene 20 22.2 111 20.7 104 7 60-130/30563-58-6 1,1-Dichloropropene 20 22.4 112 20.6 103 8 60-130/30106-93-4 1,2-Dibromoethane 20 22.3 112 20.2 101 10 60-130/30107-06-2 1,2-Dichloroethane 20 22.5 113 20.3 102 10 60-130/3078-87-5 1,2-Dichloropropane 20 22.2 111 20.2 101 9 60-130/30142-28-9 1,3-Dichloropropane 20 21.9 110 20.0 100 9 60-130/30594-20-7 2,2-Dichloropropane 20 22.6 113 20.2 101 11 60-130/30124-48-1 Dibromochloromethane 20 22.8 114 20.6 103 10 60-130/3075-71-8 Dichlorodifluoromethane 20 24.7 124 21.8 109 12 60-130/30156-59-2 cis-1,2-Dichloroethylene 20 21.9 110 19.8 99 10 60-130/3010061-01-5 cis-1,3-Dichloropropene 20 23.2 116 21.0 105 10 60-130/30541-73-1 m-Dichlorobenzene 20 21.7 109 19.9 100 9 60-130/3095-50-1 o-Dichlorobenzene 20 21.8 109 20.0 100 9 60-130/30106-46-7 p-Dichlorobenzene 20 21.7 109 19.9 100 9 60-130/30156-60-5 trans-1,2-Dichloroethylene 20 22.2 111 20.4 102 8 60-130/3010061-02-6 trans-1,3-Dichloropropene 20 22.9 115 20.8 104 10 60-130/30100-41-4 Ethylbenzene 20 22.9 115 21.0 105 9 60-130/30591-78-6 2-Hexanone 80 93.8 117 86.2 108 8 60-130/3099-87-6 p-Isopropyltoluene 20 23.0 115 21.2 106 8 60-130/30108-10-1 4-Methyl-2-pentanone 80 96.7 121 87.8 110 10 60-130/30

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C16602

44.3.1


Blank Spike/Blank Spike Duplicate Summary Page 2 of 2 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR104-BS R2901.D 1 06/18/11 BD n/a n/a VR104VR104-BSD R2903.D 1 06/18/11 BD n/a n/a VR104


C16602-1, C16602-2

Spike BSP BSP BSD BSD LimitsCAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD

74-83-9 Methyl bromide 20 22.5 113 20.0 100 12 60-130/3074-87-3 Methyl chloride 20 20.0 100 18.4 92 8 60-130/3075-09-2 Methylene chloride 20 19.9 100 18.1 91 9 60-130/3078-93-3 Methyl ethyl ketone 80 90.0 113 81.1 101 10 60-130/301634-04-4 Methyl Tert Butyl Ether 20 22.0 110 19.8 99 11 60-130/30103-65-1 n-Propylbenzene 20 23.3 117 21.5 108 8 60-130/30100-42-5 Styrene 20 23.0 115 21.1 106 9 60-130/3071-55-6 1,1,1-Trichloroethane 20 22.8 114 20.6 103 10 60-130/3079-34-5 1,1,2,2-Tetrachloroethane 20 22.4 112 20.6 103 8 60-130/3079-00-5 1,1,2-Trichloroethane 20 22.0 110 20.1 101 9 60-130/3087-61-6 1,2,3-Trichlorobenzene 20 21.4 107 19.6 98 9 60-130/3096-18-4 1,2,3-Trichloropropane 20 21.0 105 18.8 94 11 60-130/30120-82-1 1,2,4-Trichlorobenzene 20 21.5 108 19.6 98 9 60-130/3095-63-6 1,2,4-Trimethylbenzene 20 22.8 114 21.0 105 8 60-130/30108-67-8 1,3,5-Trimethylbenzene 20 22.5 113 20.8 104 8 60-130/30127-18-4 Tetrachloroethylene 20 17.8 89 16.8 84 6 60-130/30108-88-3 Toluene 20 21.6 108 20.0 100 8 60-130/3079-01-6 Trichloroethylene 20 21.8 109 20.0 100 9 60-130/3075-69-4 Trichlorofluoromethane 20 23.8 119 20.6 103 14 60-130/3075-01-4 Vinyl chloride 20 23.0 115 20.3 102 12 60-130/30108-05-4 Vinyl Acetate 20 23.1 116 20.8 104 10 60-130/30

m,p-Xylene 40 44.5 111 41.1 103 8 60-130/3095-47-6 o-Xylene 20 21.9 110 20.1 101 9 60-130/30

CAS No. Surrogate Recoveries BSP BSD Limits

1868-53-7 Dibromofluoromethane 104% 100% 60-130%2037-26-5 Toluene-D8 99% 99% 60-130%460-00-4 4-Bromofluorobenzene 101% 100% 60-130%

(a) CCV outside of control limits; results may be biased high.

17 of 19

C16602

44.3.1


Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchC16602-1MS R2917.D 1 06/18/11 BD n/a n/a VR104C16602-1MSD R2918.D 1 06/18/11 BD n/a n/a VR104C16602-1 R2907.D 1 06/18/11 BD n/a n/a VR104


C16602-1, C16602-2

C16602-1 Spike MS MS MSD MSD LimitsCAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD

67-64-1 Acetone ND 80 74.1 93 75.6 95 2 60-130/2571-43-2 Benzene ND 20 22.1 111 21.4 107 3 60-130/25108-86-1 Bromobenzene ND 20 21.4 107 20.8 104 3 60-130/2574-97-5 Bromochloromethane ND 20 21.4 107 20.9 105 2 60-130/2575-27-4 Bromodichloromethane ND 20 22.0 110 21.2 106 4 60-130/2575-25-2 Bromoform ND 20 18.7 94 18.4 92 2 60-130/25104-51-8 n-Butylbenzene ND 20 22.6 113 a 21.8 109 a 4 a 60-130/25135-98-8 sec-Butylbenzene ND 20 22.8 114 a 22.1 111 a 3 a 60-130/2598-06-6 tert-Butylbenzene ND 20 20.8 104 20.0 100 4 60-130/25108-90-7 Chlorobenzene ND 20 21.6 108 21.1 106 2 60-130/2575-00-3 Chloroethane ND 20 21.7 109 21.3 107 2 60-130/2567-66-3 Chloroform ND 20 21.9 110 21.4 107 2 60-130/2595-49-8 o-Chlorotoluene ND 20 21.1 106 20.3 102 4 60-130/25106-43-4 p-Chlorotoluene ND 20 22.7 114 20.6 103 10 60-130/2556-23-5 Carbon tetrachloride ND 20 22.7 114 21.9 110 4 60-130/2575-34-3 1,1-Dichloroethane ND 20 21.5 108 21.2 106 1 60-130/2575-35-4 1,1-Dichloroethylene ND 20 21.6 108 21.4 107 1 60-130/25563-58-6 1,1-Dichloropropene ND 20 22.2 111 21.4 107 4 60-130/25106-93-4 1,2-Dibromoethane ND 20 21.5 108 21.2 106 1 60-130/25107-06-2 1,2-Dichloroethane ND 20 22.1 111 21.4 107 3 60-130/2578-87-5 1,2-Dichloropropane ND 20 21.5 108 21.1 106 2 60-130/25142-28-9 1,3-Dichloropropane ND 20 21.2 106 20.9 105 1 60-130/25594-20-7 2,2-Dichloropropane ND 20 19.6 98 19.1 96 3 60-130/25124-48-1 Dibromochloromethane ND 20 20.6 103 20.1 101 2 60-130/2575-71-8 Dichlorodifluoromethane ND 20 22.4 112 a 21.8 109 a 3 a 60-130/25156-59-2 cis-1,2-Dichloroethylene ND 20 21.6 108 21.3 107 1 60-130/2510061-01-5 cis-1,3-Dichloropropene ND 20 21.5 108 20.8 104 3 60-130/25541-73-1 m-Dichlorobenzene ND 20 21.6 108 20.8 104 4 60-130/2595-50-1 o-Dichlorobenzene ND 20 21.4 107 20.8 104 3 60-130/25106-46-7 p-Dichlorobenzene ND 20 21.3 107 20.6 103 3 60-130/25156-60-5 trans-1,2-Dichloroethylene ND 20 21.0 105 20.7 104 1 60-130/2510061-02-6 trans-1,3-Dichloropropene ND 20 20.1 101 19.9 100 1 60-130/25100-41-4 Ethylbenzene ND 20 22.6 113 22.1 111 2 60-130/25591-78-6 2-Hexanone ND 80 88.1 110 88.2 110 0 60-130/2599-87-6 p-Isopropyltoluene ND 20 21.8 109 21.1 106 3 60-130/25108-10-1 4-Methyl-2-pentanone ND 80 90.5 113 89.8 112 1 60-130/25

18 of 19

C16602

44.4.1


Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number: C16602Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchC16602-1MS R2917.D 1 06/18/11 BD n/a n/a VR104C16602-1MSD R2918.D 1 06/18/11 BD n/a n/a VR104C16602-1 R2907.D 1 06/18/11 BD n/a n/a VR104


C16602-1, C16602-2

C16602-1 Spike MS MS MSD MSD LimitsCAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD

74-83-9 Methyl bromide ND 20 21.7 109 21.5 108 1 60-130/2574-87-3 Methyl chloride ND 20 20.1 101 21.4 107 6 60-130/2575-09-2 Methylene chloride ND 20 19.1 96 18.9 95 1 60-130/2578-93-3 Methyl ethyl ketone ND 80 80.2 100 81.6 102 2 60-130/251634-04-4 Methyl Tert Butyl Ether ND 20 20.2 101 20.4 102 1 60-130/25103-65-1 n-Propylbenzene ND 20 22.9 115 22.1 111 4 60-130/25100-42-5 Styrene ND 20 8.9 45* b 8.9 45* b 0 60-130/2571-55-6 1,1,1-Trichloroethane ND 20 22.2 111 21.9 110 1 60-130/2579-34-5 1,1,2,2-Tetrachloroethane ND 20 21.4 107 21.1 106 1 60-130/2579-00-5 1,1,2-Trichloroethane ND 20 21.3 107 21.0 105 1 60-130/2587-61-6 1,2,3-Trichlorobenzene ND 20 20.7 104 20.0 100 3 60-130/2596-18-4 1,2,3-Trichloropropane ND 20 18.4 92 18.2 91 1 60-130/25120-82-1 1,2,4-Trichlorobenzene ND 20 20.7 104 20.1 101 3 60-130/2595-63-6 1,2,4-Trimethylbenzene ND 20 15.1 76 15.1 76 0 60-130/25108-67-8 1,3,5-Trimethylbenzene ND 20 20.4 102 19.9 100 2 60-130/25127-18-4 Tetrachloroethylene ND 20 17.6 88 17.1 86 3 60-130/25108-88-3 Toluene ND 20 21.4 107 20.9 105 2 60-130/2579-01-6 Trichloroethylene ND 20 22.0 110 21.3 107 3 60-130/2575-69-4 Trichlorofluoromethane ND 20 22.8 114 22.4 112 2 60-130/2575-01-4 Vinyl chloride ND 20 22.2 111 21.8 109 2 60-130/25108-05-4 Vinyl Acetate ND 20 16.9 85 16.9 85 0 60-130/25

m,p-Xylene ND 40 42.4 106 41.6 104 2 60-130/2595-47-6 o-Xylene ND 20 21.0 105 20.6 103 2 60-130/25

CAS No. Surrogate Recoveries MS MSD C16602-1 Limits

1868-53-7 Dibromofluoromethane 102% 102% 100% 60-130%2037-26-5 Toluene-D8 98% 100% 99% 60-130%460-00-4 4-Bromofluorobenzene 101% 100% 96% 60-130%

(a) CCV outside of control limits; results may be biased high.(b) Outside control limits due to matrix interference.

19 of 19

C16602

44.4.1


Date post:	27-Mar-2021
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