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J. of Supercritical Fluids 79 ( 2013 ) iii – xiv
doi:10.1016/S0896-8446(13)00211-8
Contents
Contents lists available at ScienceDirect
The Journal of Supercritical Fluids
journal homepage: www.elsevier .com/locate/supf lu
Special issue—10th International Symposium on Supercritical Fluids (Keith W. Hutchenson, Guest Editor, The Journal of Supercritical Fluids)
Jerry W. King, Ram B. Gupta, Keith W. Hutchenson, Mark A. McHugh, Feral Temelli
University of Arkansas, Fayetteville, AK, USA
Auburn University, Auburn, AL, USA
DuPont CR&D, Wilmington, DE, USA
Virginia Commonwealth University, Richmond, VA, USA
University of Alberta, Edmonton, Alberta, Canada
The Journal of Supercritical Fluids, 79 (2013) 1
Preface
Phase behavior measurement for poly(isobornyl acrylate) � cosolvent systems in supercritical solvents at high pressure
Dong-Sun Yang, Sang-Ha Cho, Soon-Do Yoon, Hyeon-Ho Jeong, Hun-Soo Byun
Department of Chemical and Biomolecular Engineering, Chonnam National University, Yeosu, Jeonnam 550-749, South Korea
The Journal of Supercritical Fluids, 79 (2013) 11
Experimental determination and activity coeffi cient based models for mixture solubilities of nitrophenol isomers in supercritical carbon dioxide
Sivamohan N. Reddy, Giridhar Madras
Department of Chemical Engineering, Indian Institute of Science, Bangalore 560012, India
The Journal of Supercritical Fluids, 79 (2013) 2
Thermodynamics, Phase Equilibria, Solubility
iv Contents
SCFs-Ionic Liquids Coupled Media
Separation Processes
High pressure phase equilibria of ethyl esters in supercritical ethane and propane
C.E. Schwarz, C. Schlechter, J.H. Knoetze
Department of Process Engineering, University of Stellenbosch, Private Bag X1, Matieland, South Africa
High-pressure phase equilibrium data for the L-lactic acid � (propane � ethanol) and the L-lactic acid � (carbon dioxide � ethanol) systems
Isabel C.N. Debiena, Aline A. Rigob, Marcio A. Mazuttic, J. Vladimir Oliveirad, M. Angela A. Meirelesa
aDEA/FEA (School of Food Engineering)/UNICAMP, Campinas, 13083-862 SP, Brazil bDepartment of Food Engineering, URI – Erechim Campus, Erechim, RS 99700-000, Brazil cDepartment of Chemical Engineering, UFSM, Santa Maria, RS 97105-900, Brazil dDepartment of Chemical and Food Engineering, UFSC, Florianópolis, SC 88040-900, Brazil
The Journal of Supercritical Fluids, 79 (2013) 27
Partition coeffi cients of furan derivative compounds in 1-n-butyl-3-methylimidazolium chloride ([bmim][Cl])–supercritical CO2 biphasic systems and their correlation and prediction with the LSER-� model
Yuya Hiragaa, Atsushi Hayasakaa, Yoshiyuki Satob, Masaru Watanabeb, Richard L. Smith Jr.a,b
aGraduate School of Environmental Studies, Tohoku University, Aramaki Aza Aoba 6-6-11, Aoba-ku, Sendai 980-8579, Japan
bResearch Center of Supercritical Fluid Technology, Tohoku University, Aramaki Aza Aoba 6-6-11, Aoba-ku, Sendai 980-8579, Japan
The Journal of Supercritical Fluids, 79 (2013) 32
Adsorption of 2-phenylethyl alcohol on silica aerogel from saturated solution in supercritical CO2
Xiaohui Hua, Shengxuan Zhenga, Linjing Zhua, Ako Rajour Tanyia, Hongqiao Lanb, Yanzhen Honga, Yuzhong Sua, Hongtao Wanga, Jun Lia
aDepartment of Chemical and Biochemical Engineering, College of Chemistry and Chemical Engineering, National Engineering Laboratory for Green Chemical Productions of Alcohols, Ethers and Esters, Xiamen University, Xiamen 361005, PR China
bTechnology Center of China Tobacco Fujian Industry Corporation, Xiamen 361022, PR China
The Journal of Supercritical Fluids, 79 (2013) 41
The Journal of Supercritical Fluids, 79 (2013) 19
Contents v
Biomass and Energy-Related Conversions
Semi-preparative supercritical chromatography scale plant for polyunsaturated fatty acids purifi cation
Fernando Montañés, Owen J. Catchpole, Stephen Tallon, Kevin Mitchell, Kirill Lagutin
Integrated Bioactive Technologies, Industrial Research Limited, 69 Gracefi eld Road, 5040 Lower Hutt, New Zealand
Liquid and supercritical CO2 extraction of fat from rendered materials
Jose Luis Orellana, Tyler D. Smith, Christopher L. Kitchens
Clemson University, Department of Chemical and Biomolecular Engineering, 206 S. Palmetto Boulevard, Clemson, SC 29634, USA
The Journal of Supercritical Fluids, 79 (2013) 55
Fatty acids recovery from vegetable oil wet sludge by supercritical alcoholysis
G. Soto, A. Velez, P. Hegel, G. Mabe, S. Pereda
PLAPIQUI, Universidad Nacional del Sur - CONICET, CC 717, 8000 Bahía Blanca, Argentina
The Journal of Supercritical Fluids, 79 (2013) 62
Microwave-mediated non-catalytic transesterifi cation of algal biomass under supercritical ethanol conditions
Prafulla D. Patila, Harvind Reddya, Tapaswy Muppanenia, Sundaravadivelnathan Ponnusamya, Peter Cookeb, Tanner Schuabc, Shuguang Denga
aChemical Engineering Department, New Mexico State University, Las Cruces, NM 88003, USA
bElectron Microscopy Laboratory, New Mexico State University, Las Cruces, NM 88003, USA
cChemical Analysis and Instrumentation Laboratory, New Mexico State University, Las Cruces, NM 88003, USA
The Journal of Supercritical Fluids, 79 (2013) 67
The Journal of Supercritical Fluids, 79 (2013) 46
vi Contents
Production of feruloylated arabino-oligosaccharides (FA-AOs) from beet fi ber by hydrothermal treatment
Nobuaki Satoa, Yohei Takanoa, Masahiro Mizunoa, Kouichi Nozakia, Shingo Umemuraa, Tsunetomo Matsuzawaa, Yoshihiko Amanoa, Satoshi Makishimaa,b
aDepartment of Chemistry and Material Engineering, Faculty of Engineering, Shinshu University, 4-17-1 Wakasato, Nagano 380-8553, Japan
bB Food Science Co. Ltd., Chiyoda-ku 101-0054, Tokyo, Japan
The Journal of Supercritical Fluids, 79 (2013) 84
Natural Products, Nutraceuticals, and Food-Related Materials
Hydrothermal conversion of glucose in multiscale batch processes. Analysis of the gas, liquid and solid residues
Qian Michelle Yu-Wu, Elsa Weiss-Hortala, Radu Barna
Université de Toulouse, Mines Albi, CNRS UMR 5302, Centre RAPSODEE, Campus Jarlard, F-81013 Albi Cedex 09, France
The Journal of Supercritical Fluids, 79 (2013) 76
Infl uence of impurities on biodiesel production from Jatropha curcas L. by supercritical methyl acetate process
Noorzalila Muhammad Nizaa, Kok Tat Tanb, Keat Teong Leec, Zainal Ahmadc
aFaculty of Chemical Engineering, UiTM Pulau Pinang, 13500 Permatang Pauh, Pulau Pinang, Malaysia
bDepartment of Petrochemical Engineering, Faculty of Engineering and Green Technology, Universiti Tunku Abdul Rahman, Jalan Universiti, Bandar Barat, 31900 Kampar, Perak, Malaysia
cSchool of Chemical Engineering, Universiti Sains Malaysia, Engineering Campus, Seri Ampangan, 14300 Nibong Tebal, Pulau Pinang, Malaysia
The Journal of Supercritical Fluids, 79 (2013) 73
High pressure carbon dioxide pasteurization of fresh-cut carrot
Sara Spilimbergoa, Drazenka Komesb, Aleksandra Vojvodicb, Branka Levajb, Giovanna Ferrentinoa
aUniversity of Trento, Department of Industrial Engineering, via Mesiano 77, Trento, Italy
bFaculty of Food Technology and Biotechnology, University of Zagreb, Pierottijeva 6, Zagreb, Croatia
The Journal of Supercritical Fluids, 79 (2013) 92
Contents vii
Supercritical rosemary extracts, their antioxidant activity and effect on hepatic tumor progression
Gonzalo Vicentea, Susana Molinab, Margarita González-Vallinasb, Mónica R. García-Riscoa, Tiziana Fornaria, Guillermo Regleroa,b, Ana Ramírez de Molinab
aInstituto de Investigación en Ciencias de la Alimentación (CIAL), CEI UAM�CSIC, C/Nicolás Cabrera 9, Universidad Autónoma de Madrid, 28049 Madrid, Spain
bIMDEA-Food Institute, CEI UAM�CSIC, C/Faraday 7, 28049 Madrid, Spain
The Journal of Supercritical Fluids, 79 (2013) 101
Extraction and solubility evaluation of functional seed oil in supercritical carbon dioxide
Karin Tomitaa, Siti Machmudahb, Armando T. Quitaina, Mitsuru Sasakia, Ryuichi Fukuzatoc, Motonobu Gotob
aGraduate School of Science and Technology, Kumamoto University, Kumamoto 860-8555, Japan
bDepartment of Chemical Engineering, Nagoya University, Nagoya 464-8603, Japan
cSCF Techno-Link, Inc., Ashiya 659-0033, Japan
The Journal of Supercritical Fluids, 79 (2013) 109
Phase equilibrium engineering of jojoba oil extraction with mixed-CO2 � propane solvent
Pablo Hegel, Guillermo Mabe, Esteban A. Brignole, Selva Pereda
Planta Piloto de Ingeniería Química, PLAPIQUI Universidad Nacional del Sur, CONICET Camino La Carrindanga Km 7, CC 717, 8000 Bahía Blanca, Argentina
The Journal of Supercritical Fluids, 79 (2013) 114
Extraction of rotundifuran and casticin from chaste tree fruits by near critical liquid carbon dioxide
Altin Melea, Harro Lentzb, Ardita Melea, Elisabeth Feizlmayrc, Sokol Abazia, Rudolf Bauerc
aUniversity of Tirana, Faculty of Natural Sciences, Department of Chemistry, Bulevardi “Zogu i parë”, Nr. 2, Tirana, Albania
bGro�beeren Stra�e 72, D-10963 Berlin, Germany
cInstitute of Pharmaceutical Science, Karl Franzens University Graz, Universitätsplatz 4, 8010 Graz, Austria
The Journal of Supercritical Fluids, 79 (2013) 123
viii Contents
Fundamental mechanisms of cell nucleation in polypropylene foaming with supercritical carbon dioxide—Effects of extensional stresses and crystals
Anson Wonga, Yanting Guob,a, Chul B. Parka
aDepartment of Mechanical and Industrial Engineering, University of Toronto, Ontario, Canada
bNational Engineering Research Center of Novel Equipment for Polymer Processing, South China University of Technology, Guangdong, China
The Journal of Supercritical Fluids, 79 (2013) 142
Polymers, Materials Applications, and Processes
Enzymatic synthesis of poly(�-caprolactone) in supercritical carbon dioxide medium by means of a variable-volume view reactor
Sibele R. Comim Rossoa, Emanuel Bianchinb, Débora de Oliveiraa, J. Vladimir Oliveiraa, Sandra R.S. Ferreiraa
aEQA-CTC/UFSC, Chemical and Food Engineering Department, Federal University of Santa Catarina, C.P. 476, CEP 88040-900, Florianópolis, SC, Brazil
bDepartment of Food Engineering, URI – Campus de Erechim, Av. Sete de Setembro, 1621, Erechim, RS 99700-000, Brazil
The Journal of Supercritical Fluids, 79 (2013) 133
Kinetic enzymatic resolution in scCO2 – Design of continuous reactor based on batch experiments
E. Székely, M. Utczás, B. Simándi
Department of Chemical and Environmental Process Engineering, Budapest University of Technology and Eco-nomics, H-1111 Budapest, Budafoki út 6-8, Hungary
The Journal of Supercritical Fluids, 79 (2013) 127
Reactions in Critical Fluids
Use of supercritical fl uid technology for the production of tailor-made aerogel particles for delivery systems
C.A. García-González, I. Smirnova
Institute of Thermal Separation Processes, Hamburg University of Technology, Eißendorferstraße 38, D-21073 Hamburg, Germany
The Journal of Supercritical Fluids, 79 (2013) 152
Contents ix
Lysozyme encapsulation within PLGA and CaCO3 microparticles using supercritical CO2 medium
M.-K. Trana,b, L.N. Hassania,b, B. Calvignaca,b, T. Beuvierc, F. Hindréa,b, F. Bourya,b
aLUNAM Université, Angers, France
bINSERM U1066, Micro et Nanomedécines Biomimétiques, IBS, 4 rue Larrey, F-49933 Angers Cedex 9, France
cUniversité du Maine, CNRS UMR 6087-Laboratoire de Physique de l’Etat Condensé, 72085 Le Mans Cedex 9, France
The Journal of Supercritical Fluids, 79 (2013) 159
Fractionation of an oligomeric pyrene pitch via supercritical extraction
David F. Esguerraa, Wesley P. Hoffmanb, Mark C. Thiesa
aDepartment of Chemical and Biomolecular Engineering, Center for Advanced Engineering Fibers and Films, Clemson University, Clemson, SC 29634-0909, USA
bAir Force Research Laboratory, AFRL/RQRC, 10 E. Saturn Blvd., Edwards, CA 93524-7680, USA
The Journal of Supercritical Fluids, 79 (2013) 170
Unleashing the potential of supercritical fl uids for polymer processing in tissue engineering and regenerative medicine
Ana Rita C. Duartea,b, Vitor E. Santoa,b, Anabela Alvesa,b, Simone S. Silvaa,b, Joana Moreira-Silvaa,b, Tiago H. Silvaa,b, Alexandra P. Marquesa,b, Rui A. Sousaa,b, Manuela E. Gomesa,b, João F. Manoa,b, Rui L. Reisa,b
a3B’s Research Group – Biomaterials, Biodegradables and Biomimetics, University of Minho, Headquarters of the European Institute of Excellence on Tissue Engineering and Regenerative Medicine, AvePark, 4806-909 Taipas, Guimarães, Portugal
bICVS/3B’s – PT Government Associate Laboratory, Braga, Guimarães, Portugal
The Journal of Supercritical Fluids, 79 (2013) 177
Comparison of the physical stability and physicochemical properties of amorphous indomethacin prepared by co-milling and supercritical anti-solvent co-precipitation
Ron Tau Yee Lima,b, Wai Kiong Nga, Effendi Widjajaa, Reginald B.H. Tana,b
aInstitute of Chemical and Engineering Sciences (ICES), Agency for Science Technology and Research (A*STAR), 1, Pesek Road, Jurong Island, Singapore 627833, Singapore
bNational University of Singapore, Department of Chemical & Biomolecular Engineering, 4 Engineering Drive 4, Blk E5 #02-09, Singapore 117576, Singapore
The Journal of Supercritical Fluids, 79 (2013) 186
x Contents
Encapsulation of nanoparticles using CO2-expanded liquids
M. Vinjamur, M. Javed, M. Mukhopadhyay
Department of Chemical Engineering, IIT Bombay, Powai, Mumbai 400 076, India
The Journal of Supercritical Fluids, 79 (2013) 216
Preparation of multi-membrane alginate aerogels used for drug delivery
Anja Veronovski, Zeljko Knez, Zoran Novak
University of Maribor, Faculty of Chemistry and Chemical Engineering, Smetanova 17, SI-2000 Maribor, Slovenia
The Journal of Supercritical Fluids, 79 (2013) 209
Pharmaceutical Applications
Superabsorbent alginate aerogels
Rajendar R. Mallepallya,c, Ian Bernarda, Michael A. Marina, Kevin R. Wardb,d, Mark A. McHugha,c
aDepartment of Chemical and Life Science Engineering, Virginia Commonwealth University, Richmond, VA 23284, USA bDepartment of Emergency Medicine, University of Michigan, Ann Arbor, MI 48109, USA cMaterial Science Division, VCU Reanimation Engineering Science Center, Virginia Commonwealth University Medical Center, Richmond, VA 23298-0614, USA
dMichigan Center for Integrative Research in Critical Care, University of Michigan, Ann Arbor, MI 48109, USA
The Journal of Supercritical Fluids, 79 (2013) 202
Modeling of precipitation of ultra-fi ne particles by pressure reduction over CO2-expanded liquids
K. Arjun Kumar, Rajarshi Chattaraj, Umesh Dhumal, Mamata Mukhopadhyay, Madhu Vinjamur, Sameer V. Dalvi
aChemical Engineering, IIT Gandhinagar, Ahmedabad 382 424, India
bChemical Engineering, IIT Bombay, Powai, Mumbai 400 076, India
The Journal of Supercritical Fluids, 79 (2013) 227
Contents xi
Hydrothermal Processing
Reverse micelle synthesis of silver nanoparticles in gas expanded liquids
Ashley E. Hart, David B. Akers, Samuel Gorosh, Christopher L. Kitchens
Clemson University, Department of Chemical and Biomolecular Engineering, 206 South Palmetto Boulevard, Clemson, SC 29631, United States
The Journal of Supercritical Fluids, 79 (2013) 236
Strontium ruthenium oxide deposition in supercritical carbon dioxide using a closed reactor system
Kyubong Jung, Takeshi Momose, Yukihiro Shimogaki
Department of Materials Engineering, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-8656, Japan
The Journal of Supercritical Fluids, 79 (2013) 244
Hydrothermal processing and in situ surface modifi cation of metal oxide nanomaterials
K. Namratha, K. Byrappa
Center for Materials Science, University of Mysore, P.B. No. 21, NCHS Bldg., Manasagangothri, Mysore 570006, India
The Journal of Supercritical Fluids, 79 (2013) 251
SCF Particle / Film Technology
A theoretical study of factors affecting corrosion in supercritical water reaction vessels
Simon James Halstead
Department of Chemical Engineering, Xi Da Zhi Street, Harbin, Heilong Jiang, China 150001
The Journal of Supercritical Fluids, 79 (2013) 261
xii Contents
Supercritical water oxidation—Current status of full-scale commercial activity for waste destruction
Philip A. Marrone
Science Applications International Corporation (SAIC), Newton, MA 02459, USA
The Journal of Supercritical Fluids, 79 (2013) 283
Reprint of: Application of subcritical water liquefaction as pretreatment for supercritical water gasifi cation system in domestic waste water treatment plant
Osamu Sawai, Teppei Nunoura, Kazuo Yamamoto
Environmental Science Center, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033, Japan
The Journal of Supercritical Fluids, 79 (2013) 274
Controlled morphology and size of ZnO nanocrystals using the continuous hot compressed water technique
Zhiqiang Mao, Sining Li, Yuanpeng Leng, Yaping Zhao
School of Chemistry and Chemical Engineering, Shanghai Jiaotong University, 800 Dong Chuan Road, Minhang District, Shanghai 200240, China
The Journal of Supercritical Fluids, 79 (2013) 268
The applicability of subcritical fl uids to the conservation of actively corroding iron artifacts of cultural signifi cance
Liisa M.E. Näsänena, Néstor G. González-Pereyraa, Stéphanie A. Crettéa, Philippe DeViviésb
aClemson University Restoration Institute, Warren Lasch Conservation Center, 1250 Supply Street, Bldg 255, North Charleston, SC 29405, USA
bA-CORROS Expertises, 23 Chemin des Moines, 13200 Arles, France
The Journal of Supercritical Fluids, 79 (2013) 289
Archeological Applications
Contents xiii
Industrial Applications
Conservation of waterlogged archaeological corks using supercritical CO2 and treatment monitoring using structured-light 3D scanning
Stéphanie A. Cretté, Liisa M. Näsänen, Néstor G. González-Pereyra, Benjamin Rennison
Clemson University Restoration Institute, Warren Lasch Conservation Center, 1250 Supply Street, North Charleston, SC 29405, USA
The Journal of Supercritical Fluids, 79 (2013) 299
Application of supercritical carbon dioxide–co-solvent mixtures for removal of organic material from archeological artifacts for radiocarbon datingMarvin W. Rowea, Jenny Phomakayb, Jackson O. Layc, Oscar Guevarad, Keerthi Srinivasb, W. Kirk Hollise, Karen L. Steelmanf, Thomas Guildersong, Thomas W. Stafford Jr.h, Sarah L. Chapmani, Jerry W. Kingb
aTexas A&M University, Doha, QATAR/Conservation Laboratory - Museum of New Mexico, Santa Fe, NM 87505, USA bDepartment of Chemical Engineering, University of Arkansas, Fayetteville, AR 72701, USA cDepartment of Chemistry, University of Arkansas, Fayetteville, AR 72701, USA dDepartment of Biological and Agricultural Engineering, Fayetteville, AR 72701, USA eLos Alamos National Laboratory, Los Alamos, NM 87544, USA fDepartment of Chemistry, University of Central Arkansas, Conway, AR 72035, USA gCenter for AMS, Lawrence Livermore National Laboratory L-397, 7000 East Avenue, Livermore, CA 94551, USA hStafford Research Laboratories, Inc., 200 Acadia Avenue, Lafayette, CO 80026, USA iDepartment of Anthropology, University of Arkansas, Fayetteville, AR 72701, USA
The Journal of Supercritical Fluids, 79 (2013) 314
Metal extraction of a spiked solid with supercritical carbon dioxide
Ming-Tsai Lianga, Ru-Chien Lianga, Chih-Hsiung Lina, Ping-Jui Hsua, Li-Yu Wua, Hong-Fa Chena, Yuh-Wern Wua, Wen-Chen Leeb
aDepartment of Chemical Engineering, I-Shou University, Kaohsiung City 84001, Taiwan, ROC
bInstitute of Nuclear Energy Research, Atomic Energy Council, Taoyuan County 32546, Taiwan, ROC
The Journal of Supercritical Fluids, 79 (2013) 324
Demonstration of NIR inline monitoring for hops extraction and micronization of benzoic acid in supercritical CO2
D. Böhma, T. Graua, N. Igl-Schmidc, S. Johnsena, E. Kaczowkaa, A. Klotza,b, J. Schulmeyrc, M. Türkb, G. Wieganda, A. Wuzikc, B. Zehnderd
aKarlsruhe Institute of Technology (KIT), Institute of Catalytical Research and Technology (IKFT), P.O.B. 3640, D-76021 Karlsruhe, Germany
bKarlsruhe Institute of Technology (KIT), Institute for Technical Thermodynamics and Refrigeration (ITTK), Kaiserstrasse 12, D-76133 Karlsruhe, Germany
cNATECO2 GmbH & Co. KG, Auenstrasse 18-20, 85283 Wolnzach, Germany
dSITEC-Sieber Engineering AG, Maur b. Zürich, Switzerland
The Journal of Supercritical Fluids, 79 (2013) 330
xiv Contents
New considerations in the economic evaluation of supercritical processes: Separation of bioactive compounds from multicomponent mixtures
María P. Fernández-Ronco, Antonio de Lucas, Juan F. Rodríguez, M.T. García, Ignacio Gracia
Departamento de Ingeniería Química, Facultad de C.C. Químicas, Universidad de Castilla-La Man-cha, Avda. Camilo José Cela 12, 13071 Ciudad Real, Spain
The Journal of Supercritical Fluids, 79 (2013) 345
Infl uence of pretreatment on supercritical CO2 extraction from Nannochloropsis oculata
Christelle Crampona, Adil Mouahida, Sid-Ali Amine Toudjia, Olivier Lépineb, Elisabeth Badensa
aAix-Marseille Université, M2P2 UMR CNRS 7340, Europole de l’Arbois, BP80, Pavillon Laennec, Hall C, Aix en Provence Cedex 04, FR 13545,
bAlpha Biotech, Le Frostidié, Asserac, FR 44410, France
The Journal of Supercritical Fluids, 79 (2013) 337
Process Design and Economics