0001
AUXIER & ASSOCIATES, INC.
West Lake NCC
ST AND ARD LEVEL IV REPORT OF ANALYSIS
WORK ORDER #18-03111-OR
May 11, 2018
EBERLINE ANALYTICAL/OAK RIDGE LABO RA TORY
OAK RIDGE, TN
0002
TABLE OF CONTENTS
SECTION DESCRIPTION PAGE
I Chain of Custody 0004
II Sample Acknowledgement 0009
III Case Narrative 0012
IV Analytical Results Summary 0016
V Analytical Standards 0019
VI Quality Control Sample Results Summary 0037
VII Laboratory Technician's Notes 0044
VIII Analytical Data (Isotopic Uranium) 0060
IX Analytical Data (Isotopic Thorium) 0100
X Analytical Data (Gamma Spectroscopy) 0140
Last Page 0303
0003
Ea STANDARD OPERATING PROCEDURE INE
Sample Receiving
LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
Eberline Services Work Order # ___ ...... l_a_-~0~3~1~1 _1 ____ _ The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial Initials Date Initials Checklist Items
.s~,J.J-/t ~~ Sample Log-In
lJ//1/;[3 t{tJh Data Compilation
</✓1,t✓/0 ✓-~,;-,,_7 First Technical Data Review
MP-001, Rev. 19 Effective: 2111/18
Page 14 of 15
J-11
1\<(\\,£ 2~ Second Technical Data Review
~I \
Data Entry/Electronic Deliverable G & L) I I )j Case Narrative 5 e, ,e,
,:;]~ I~ 9;1tl /fj '-!(pl /2 Electronic Deliverable Proof
sl,o/,·t. Of&X Samples Analyzed within Holding Time Yes? 1 Y I No?I I
I , r / V iJ)- QA/QC~e~iew 5 110 I 'r I/ - ff:_.~ .• -- Client in Possession of Data
Electronic or Hard Con"
Invoiced by Laboratory
Technical/Clerical Corrections, Signatures Needed, Problems, Etc Date/Initials
Date package approved by: _{;-;, 1 ( Co
Laboratory Manager Date
Copy No. ___ _ Radiochemistry Services
0004
SECTION I
CHAIN OF CUSTODY
0005
Chain of ust y Record ~ ~
NO 001 ~ ~ - --------- 0.il( Ridge, TN 37830 EBERLINE
S!!:RV!Cl!:5
- ·-. Project Name: WUr ~ JJtc.- Project Number: E. PA t-u{,'w..,.~ ~I;.}- jfj:/il I I I I I I I I Send Report To: p~ ~&rw Sampler (Pnnt Name):.'1:_ UJl\~..,_ PagLL01_l_
/liti!lt / I , /R~'f M,AR/2 3 2018 Address: GtM:Z: Sampler (Print Name):
Shipment Method: F d ~ 1- I 1/ I / 1 , /~ I ~ - . 1 I I /1~ r ' 1 1 Airbil! Number -=1-:r,e 'OU,i KM ~1 i / I I / I / / Pocchase Phone: laboratory Receiving: , ~ ~ / I / I , I Order ii·
Fax: /~ I I I I I I Sample ! Sample I Sample Number o! / J / I Comments, Speaal Lab Sample ID
l Field Sample 10 ,/ t!J I,;;;, I 1 / / Instructions, etc. I Date I T,me Matrn, Containers (to be romple!ed by lab)
Ae-_j~h- H 1-\ c :}id 1.i 13to &;1 1 ~ '£, ~ I
I
.
l Relinquished by: (Signature) Received by: (Signature) Date: Time: Sample Custodian Remarks (Completed By laboratory):
iJ~~ /Ft;r f'-qti.,:,. .ria/,s 111:o QA/QC level Turnaround Sample Receipt
'l)Feliflquished by: (Signature) ~~by;;;f~ Date: Time: Total# Containers Received?
' Level I 0 Routine O COC Seals Present? _y~·/f il{;tJ Level l! D 24 Hour • GOC Seals intact?
Relinquished by: (Signature) L,/ ,,l'leceiv~tur. Date: Time: Level 111 0 1 Week 0 Received Containers Intact? Other 0 Other -- Temperature?
0006
EBERLINE SEnv,c:ES
Oak Ridge Laboratory
Internal Chain of Custody
Comments
REPORT ON DRY WEIGHT BASIS.
Location (circle one
Received by ~ ~oughj~p Prep Separations
,,,-. ...----'""'.,\
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Separations
Relinquished by Sample Storage Rough Prep Separations
Received by Sample Storage Rough Prep ~
Relinquished by Sample Storage Rough Prep Prep ~
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by s[~e~~) Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room /(30
Count Room o)1S
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
I
18-03111 4/12/2018
UUISO - Level 4 Soil/Solid
HP 210 / 270 Storage Detector Activity i Location
63 :
Ll.3
Initials Date
\["", ')(./ Jl {I
(,<_? ·~11c:l18 o'1,SD )Cb :s/ao h 9 \ lQ.oo
Printed: 3/23/2018 4.51 PM
0007
( . .r.;-J\ EBER ~.1,,Nv, _EE···, @ -.. >i......... \ (_, _,_,
· Oak Ridge Laboratory
Internal Chain of Custody
Comments
REPORT ON DRY WEIGHT BASIS.
-l..Pcation (circle one)
Received by )
Rough Prep Prep Separations
Relinquished by Sample Storage
,.;,,:='~ b~p Prep Separations
Received by Sample Storage Rough Prep ~ Separations
Relinquished by Sample Storage Rough Prep Q/_ Separations
Received by Sample Storage Rough Prep Prep
Relinquished by Sample Storage Rough Prep Prep
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix !
Sample ! Fraction
04
' '
i
'
18-03111 4/12/2018
ThlSO - Level 4 Soil/Solid
HP 210 / 270 '
Storage Detector Activity Location
63 Ll.3
Initials
Count Room f /?.Jb ~~ s tf\ Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
L(I t° 1-✓~o ,,g o7'1~
-,h . ;--. ·>f .,0 //
Printed: 3/2312018 4:51 PM
0008
. EB ER~.~<~-~
· Oak Ridge Laboratory
Internal Chain of Custody
Comments
REPORT ON DRY WEIGHT BASIS.
21 day ingrowth - Report Ac228, Bi214, K40, Pa231, Pb210/212/214, Ra226 from Bi214, Ra228 from Ac228,Tl208 &
Th234.
Location (circle one)
~ ,/ ·,
Received by ~~p Prep Separations
(;···---, Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by /--~~
e,am~l~~orag_~ Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Received by Sample Storage Rough Prep Prep Separations
Relinquished by Sample Storage Rough Prep Prep Separations
Work Order#
Lab Deadline
Analysis
Sample Matrix
Sample Fraction
04
Count Room // 50
Count Room al ~-s ~o/ eun~~~~"
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
Count Room
18-03111 4/12/2018
Gamma - Level 4 Soil/Solid
1 HP 210 / 270 Storage
Location : Detector Activity :
63 Ll.3
Initials Date
v(1 ) (rj j).J, ( y
h~,., St.1 3, )7,l Y
{r ~ /z;~/28 o[3ec5J 1;p 4/21As dtlcf&
Printed: 3123/2018 4:51 PM
0009
SECTION II
SAMPLE ACKNOWLEDGEMENT
0010
Client Name Contract/PO Project Type Date Received Required Turnaround Days .. . ln.u:..i
Auxier & Associates, Inc. WESTLAKE NCC Environmental 03/23/2018 28 18-03111 Project Name Client WO Sample Disp Lab Deadline Internal Deadline I .• •
WESTLAKE NCC WESTLAKE NCC SOIL H 04/12/2018 04/19/2018 04/20/2018 "' 0 0 E
Internal ID Client ID Sample Date Matrix Storage E CJ) CJ) i'='.
"' .c ::J c:J f- ::J
01 LCS 03/23/18 so Ll.3 X X X 3
02 BLANK 03/23/18 so Ll.3 X X X 3
03 DUP 03/23/18 so Ll.3 X X X J
04 AC-SED-11 03/21/18 13:20 so Ll.3 X X X J'
• 0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Totals Per Analysis (non QA samples) 1 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Invoice Accounts Payable Report Data Cecilla Greene
( Auxier & Associates. Inc. Auxier & Associates, Inc
Oak Ridge Laboratory 9821 Cogdill Drive #1 9821 Cogdrl! Road, Suite 1 . EBERLINE 601 Scarboro Rd. Knoxville. TN 37932 Knoxville, TN 37932
~ SERVICES Oak Ridge, TN 37830 Voice 865-675-3669 Voice 865-675-3669
Sample Log In Report Voice: (865) 481-0683 Fax 865-675-3677 Fax 865-675-3677
Fax: (865) 483-4621 Contact Paul Rosasco P E
Voice 303-940-3426
Fax
Printed 3/2312018 4 51 PM
0011
STANDARD OPERATING PROCEDURE MP-001, Rev. 19 Effective: 2111/18
Page 13 of 15 Sample Receiving
SAMPLE RECEIPT CHECKLIST MP-001-2
WORKORDER#_1 __ 8~--Q~3_1_1_1_ SAMPLE MATRIX/MATRICES:
WERE SAMPLES:
Received in good condition?
If aqueous, properly preserved
WERE CHAIN OF CUSTODY SEALS:
Present on outside of package?
Unbroken on outside of package?
Present on samples?
Unbroken on samples?
Was chain of custody present upon sample receipt?
(CIRCLE ONE OR BOTH)
AQUEOUS c:::::§-AQUEOUS ~ (CIRCLE EITHER YES, NO, ORN/A)
N
y N
Ct> N
~ N
0? N
~ N
(-) N
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: ___________________________ _
SIGNA~~ DATE: J~23;-l,Y
Copy No. ___ _ Radiochemistry Services
0012
SECTION III
CASE NARRATIVE
0013
EBERLINE
~ EBS-OR-43705
May 11, 2018
Cecilia Greene
SERVICES
Auxier & Associates, Inc. 9821 Cogdill Road #1 Knoxville, TN 37932
SAMPLE RECEIPT
CASE NARRATIVE Work Order# 18-03111-OR
EBERLINE ANALYTICAL C0RF'0f(ATI0~1
601 SCARBOFW R01\ll
OAK RIDGE. TENNESSEE rn:so PHONE (865) L,81--0685
FAX (865) 483-L,621
This work order contains one soil sample received 03/23/2018. Sample was analyzed for Isotopic
Uranium, Thorium-230 and Gamma Spectroscopy.
CLIENT ID
AC-SED-11
ANALYTICAL METHODS
LAB ID
18-03 111-04
Isotopic Uranium was analyzed using EPA Method 908.0 Modified. Thorium-230 was analyzed using
EPA Method 907.0 Modified. Gamma Spectroscopy was performed using EPA Method 901.1 Modified.
ANALYTICAL RES UL TS
Combined Standard Uncertainty is reported at I-sigma value.
Minimum Detectable Activity (MDA) values for data represented in this report are sample-specific.
MDA measurements are determined based on factors and conditions including instrument settings, aliquot
size and matrix type.
SPECIAL CIRCUMSTANCES
Results are reported on a "dry weight" basis.
ISOTOPIC URANITJM
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as
appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238. Chemical
recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Page 1 of 3
0014
ANALYTICAL RESULTS CONTINUED
ISOTOPIC URANIUM CONTINUED
Sample demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for
all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234 and Uranium-235 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Uranium-238 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Uranium-234 and Uranium-238 laboratory control sample
demonstrated an acceptable percent recovery.
THORIUM-230
Sample was prepared by removing a representative aliquot followed by mixed acid digestions as
appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Thorium-230. Chemical recovery was determined by the use
of a Thorium-229 tracer. Activity of the Thorium-229 tracer was determined by alpha spectroscopy using
an energy specific region of interest.
Sample demonstrated acceptable results for all Thorium-230 analyses. Chemical recovery was acceptable
for all samples. The Thorium-230 method blank demonstrated acceptable results. Results for the
Thorium-230 duplicate demonstrated an acceptable relative percent difference and normalized difference.
Results for the Thorium-230 laboratory control sample demonstrated an acceptable percent recovery.
GAMMA SPECTROSCOPY
Sample was dried, homogenized and placed into an appropriate gamma spectroscopy geometry container.
Sample was then sealed for 21 days to allow for ingrowth of Radon-222 and progeny. Sample was
counted on High Purity Gennanium (HPGe) gamma ray detectors. Energy lines from Lead-214 and
Bismuth-214 were analyzed for determinations of Radium-226 activity.
Sample demonstrated acceptable results for all gamma-emitting radionuclides as reported. The method
blank demonstrated acceptable results for all radionuclides as reported. Results for the Actinium-228,
Bismuth-214 and Potassium-40 replicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Cobalt-60 and Cesium-137 laboratory control sample demonstrated
an acceptable percent recovery.
Page 2 of 3
0015
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
signee to be accurate as verified by the following signature.
~;#?..(_,,.(_
M.R. McDougaff--Laboratory Manager
Date: 5/1I/2018 \
Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://cberlineanalytical.com/ to provide us with feedback on our services.
Page 3 of 3
0016
SECTION IV
ANALYTICAL RESULTS SUMMARY
0017
Printed: 5/11/2018 9:48 AM Page 1 of 2
Report To: Work Order Details:
Eberline Analytical Cecilia Greene SOG.· 18-03111 "~•·
Auxier & Associates, Inc. Project_ WEST LAKE NCC
Final Report of Analysis r---,- '"""~ ~,,,,,,,, __________ ._ ------ ·--·· ,,,,,,,,_,,__,,
9821 Cogdill Road, Sui!~__:1 Analysis Category: ENVIRONMENTAL
Knoxville, TN 37932 Sample Matrix: so Lab i Sample Client Sample Receipt Analysis Batch Report
ID Type ID Date Date Date ID Analyte Method I Result cu CSU MDA CV
Units
18-03111-01 LCS I KNOWN 03/23/18 00:00 3/23/2018 I 4/17/2018 l 18~03111 Cobalt-60 EPA 901.1 Modified I 1.35E+02 5.27E+00 pCi/g --,-- _,,_,_, ___
18-03111-01 ' LCS i KNOWN 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Cesium-137 EPA 901.1 Modified 8.44E+01 3.38E+00 pCi/g
··-----·-~·- ~~•"~"""" •••••••••~~~ -•·~···--···
18-03111-01 LCS '
SPIKE 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Cobalt-60 EPA 901.1 Modified ; 1.32E+02 8.11E+00 1.06E+01 9.45E-01 8.10E-01 pCi/g
------- -· --18-03111-01 LCS SPIKE 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Cesium-137 EPA 901.1 Modified ' 8.31E+01 7.72E+00 8.82E+00 1.27E+00 6.30E-01 pCi/g
,, __ ____ , ----·--:
i I
•m•~••'-•"•"••~•--•,,,,,_,,,_,,,_m">••-• ,_,, ,,,,,_,, ...
18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 . 18-03111 Actinium-228 EPA 901.1 Modified : 9.58E-03 2.20E-02 2.20E-02 9.02E-02 3.86E-02 pCi/g
18-03111-02 MBL I
BLANK 03/23/18 00:00 3/23/2018 4/17/2018 ' 18-03111 Bismuth-214 EPA 901.1 Modified I
2.99E-02 4.01E-02 4.01E-02 6.90E-02 3.17E-02 pCi/g I
18-03111-02 MBL BLANK 03/23/18 00:00 : 3/23/2018 4/17/2018 18-03111 Potassium-40 EPA 901.1 Modified . 1.62E-01 1.S0E-01 1.S0E-01 3.39E-01 1.45E-01 pCi/g
-·~-~--<-••-,,·--- ·····•···-" 18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 I 18~03111 Protactinium-231 EPA901.1 Modified -4.91E-01 5.96E-01 5.97E-01 7.86E-01 3.60E-01 pCi/g
18-03111-02 MBL i BLANK 03/23/18 00:00 3/23/2018 4/17/2018 : 18-03111 I Lead-210 EPA 901.1 Modified 3.72E-01 3.67E-01 3.67E-01 5.55E-01 2.62E-01 pCi/g
18-03111-02 MBL I BLANK 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Lead-212 EPA 901.1 Modified 4.19E-02 2.44E-02 2.45E-02 4.68E-02 2.19E-02 pCi/g
-----•-·-· ... ,,,,,,,,,_,,, ____ ~--
18-03111-02 : MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Lead-214 EPA 901.1 Modified 2.52E-02 3.78E-02 3.78E-02 6.34E-02 2.94E-02 , pCi/g
·----- ·-18-03111-02 • MBL BLANK 03/23/18 00:00 3/23/2018 41rn2018 - 18-03111 1 Radium-226 EPA 901.1 Modified 2.99E-02 4.01E-02 4.01E-02 6.90E-02 3.17E-02 : pCi/g
18-03111-02 MBL ' BLANK 03/23/18 00:00 3/23/2018 4/17/2018 ; 18~03111 I Radium-228 EPA 901.1 Modified 9.58E-03 2.20E-02 2.20E-02 9.02E-02 3.86E-02 pCi/g
18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 4/17/2018 18-03111 Thorium-234 EPA 901.1 Modified 1.08E+00 3.97E-01 4.01E-01 6.57E-01 3.15E-01 pCi/g
18-03111-02 MBL BLANK 03/23/18 00:00 : 3/23/2018 4/17/2018 , 18-03111 I Thallium-208 EPA 901.1 Modified I
-5.60E-03 5.22E-02 5.22E-02 1 7.99E-02 3.58E-02 pCi/g
' I
18-03111-03 i DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 I Actinium-228 EPA 901.1 Modified 8.74E-01 2.34E-01 ' 2.38E-01 3.52E-01 1.63E-01 i pCi/g
18-03111-03 I ' AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 Bismuth-214 EPA 901.1 Modified 1.06E+00 1.93E-01 2.00E-01 2.46E-01 1.17E-01 I pCi/g
DUP I I
18-03111-03 ; DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 ; Potassium-40 EPA 901.1 Modified 1.60E+01 2.13E+00 ' 2.28E+00 1.15E+00 5.25E-01 '
pCi/g __________ ,.
18-03111-03 i DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 i Protactinium-231 EPA 901.1 Modified 1.37E+00 : 1.41E+00 1.41E+00 3.33E+00 2.70E+00 pCi/g
18-03111-03 • DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 i 18-03111 ; Lead-210 EPA 901.1 Modified 2.10E+00 1.33E+00 1.33E+00 2.15E+00 ' 1.04E+00 pCi/g
18-03111-03 DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 I Lead-212 EPA 901.1 Modified 1.44E+00 2.66E-01 ' 2.76E-01 2.35E-01 1.15E-01 pCi/g
1a-03111-03 l DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 ; 18-03111 I Lead-214 EPA901.1 Modified 1.13E+00 1.98E-01 2.06E-01 2.42E-01 1.16E-01 pCi/g
18-03111-03 i DUP ' AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 I 18-03111 , Radium-226 EPA901.1 Modified 1.06E+00 1.93E-01 2.00E-01 2.46E-01 1.17E-01 pCi/g
18-03111-03 DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 Radium-228 EPA 901.1 Modified 8.74E-01 2.34E-01 2.38E-01 3.52E-01 ; 1.63E-01 pCi/g -18-03111-03 DUP I AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 1 18-03111 Thorium-234 EPA 901.1 Modified 1.72E+00 1.49E+00 1.49E+00 1 2.05E+00 1.00E+00 ' pCi/g
18-03111-03 I DUP AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 ! Thallium-208 EPA 901.1 Modified 7.74E-01 1.68E-01 1.73E-01 1.34E-01 1.82E-01 pCi/g
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Slank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original; CV=Critical Value
( . EBERLINE _@ ANALYTiCAL
EBERLINE CAL CORPORATION
601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/483-4621
0018
Printed: 5/11/2018 9:48 AM Page 2 of2
Report To: Work Order Details:
Eberline Analytical Cecilia Greene SDG.· 18-03111 ···········--·---•·-···-"--~•-, ······- .. "········-·--·--···-- ····--~ .. ••'-•• -·-· ~-- I····· • ••• ,.,,,~,_,,. ·•-❖--••·
Auxier & Associates, Inc. Project: WEST LAKE NCC Final Report of Analysis ~· -----
9821 Cog_qil! Road, Suite 1 Analysis Category: ENVIRONMENTAL - . ---- - -------Knoxville, TN 37932 Sample Matrix: so
Lab Sample Client Sample Receipt Analysis ! Batch Analyte Method Result CSU
I Report
ID Type ID Date Date Date ID ! cu MDA CV
Units
_18-03111-04 : DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 : 18-03111 Actinium-228 EPA 901.1 Modified : 1.09E+00 2.60E-01 2.66E-01 3.95E-01 1.84E-01 pCi/g "------
18-03111-04 DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 i 18-03111 Bismuth-214 EPA901.1 Modified 1.11E+00 1.95E-01 2.03E-01 2.12E-01 1.01E-01 pCi/g -•••w••• •••-•-'•••~"' "'-•-•~•••"'-•-•m• -
18-03111-04 DO AC-SED-11 03/21/1813:20 3/23/2018 4/17/2018 1 18-03111 , Potassium-40 EPA 901.1 Modified 1.68E+01 2.27E+00 2.42E+00 1.36E+00 6.32E-01 pCi/g
18-03111-04 DO AC-SED-11 03/21/1813:20 I 3/23/2018 4/17/2018 18-03111 Protactinium-231 EPA 901.1 Modified 4.02E-01 1.98E+00 1.98E+00 2.65E+00 1.26E+00 pCi/g
18~03111~04 I DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 ; 18-03111 Lead-210 EPA 901.1 Modified 2.01E+00 1.66E+00 1.66E+00 2.74E+00 1.34E+00 pCi/g I 18-03111-04 DO AC-SED-11 03/21/1813:20 3/23/2018 4/17/2018 18-03111 i Lead-212 EPA 901.1 Modified i 1.31E+00 2.57E-01 2.65E-01 2.45E-01 1.19E-01 : pCi/g
18-03111-04 : DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 18-03111 Lead-214 EPA 901.1 Modified 1.10E+00 1.94E-01 2.02E-01 2.16E-01 : 1.04E-01 : pCi/g
18-03111-04 DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 j 18-03111 ! Radium-226 EPA 901.1 Modified I 1.11E+00 1.95E-01 2.03E-01 2.12E-01 1.01E-01 pCi/g ----~- .,_.,.,_,,
18-03111-04 DO AC-SED-11 03/21/18 13:20 I 3/23/2018 4/17/2018 : 18-03111 I Radium-228 EPA 901.1 Modified 1.09E+00 2.60E-01 2.66E-01 3.95E-01 : 1.84E-01 : pCi/g
18-03111-04 I DO AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 : 18-03111 Thorium-234 EPA901.1 Modified 1.01E+00 1.14E+00 1.14E+00 1.91E+00 9.27E-01 I
pCi/g
18-03111-04 i DO : AC-SED-11 03/21/18 13:20 3/23/2018 4/17/2018 i 18-03111 Thallium-208 EPA 901.1 Modified •
9.65E-01 1.89E-01 1.95E-01 1.34E-01 1.71E-01 : pCi/g
: ' I : I
18-03111-01 LCS KNOWN 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 Thorium-230 EPA 907 .0 Modified :
5.39E+00 1.45E-01 : pCi/g
18-03111-01 LCS : SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 j 18-03111 : Thorium-230 EPA 907.0 Modified I 6.57E+00 1.01E+00 : 1.30E+00 8.10E-02 7.95E-02 pCi/g
18-03111-02 MBL : BLANK 03/23/18 00:00 3/23/2018 3/30/2018 ! 18-03111 Thorium-230 EPA 907.0 Modified 4.58E-02 i 8.80E-02 8.82E-02 1.63E-01 1.44E-01 pCi/g
18-03111-03 DUP i AC-SED-11 03/21/18 13:20 3/23/2018 3/30/2018 l 18-03111 Thorium-230 EPA 907.0 Modified 1.17E+00 3.38E-01 3.68E-01 8.46E-02 8.67E-02 : pCi/g
18-03111-04 I DO : AC-SED-11 03/21/18 13:20 3/23/2018 313012018 I 18-03111 ; Thorium-230 EPA 907.0 Modified 1.34E+00 4.14E-01 4.47E-01 1.06E-01 1.09E-01 : pCi/g
I : I : I
18-03111-01 i LCS KNOWN 03/23/18 00:00 3/23/2018 313012018 ; 18-03111 I Uranium-234 EPA 908.0 Modified i 7.27E+00 2.62E-01 : pCi/g
18-03111-01 LCS SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 I 18-03111 Uranium-234 EPA 908.0 Modified 6.71E+00 9.02E-01 1.02E+00 7.09E-02 1.22E-02 pCi/g
18-03111-02 I MBL BLANK 03/23/18 00:00 : 3/23/2018 313012018 I 18-03111 , Uranium-234 EPA 908.0 Modified 1.66E-02 4.01E-02 4.01E-02 8.04E-02 1.94E-02 pCi/g
18-03111-03 ; DUP AC-SED-11 03/21/18 13:20 3/23/2018 3/30/2018 18-03111 i Uranium-234 EPA 908.0 Modified 6.S0E-01 1.95E-01 2.00E-01 1.12E-01 4.20E-02 i pCi/g
18-03111-04 DO AC-SED-11 03/21/18 13:20 3/23/2018 3/30/2018 i 18-03111 Uranium-234 EPA 908.0 Modified 9.93E-01 : 2.42E-01 2.52E-01 9.59E-02 ' 2.86E-02 I pCi/g
i
18-03111-01 LCS SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 I 18-03111 1 Uranium-235 EPA 908.0 Modified 4.97E-01 1.78E-01 1.81E-01 9.21E-02 1.34E-02 [ pCi/g
18-03111-02 MBL BLANK 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 ! Uranium-235 EPA 908.0 Modified -5.02E-03 , 3.04E-02 3.04E-02 9.57E-02 1.66E-02 1 pCi/g
18-03111-03 DUP i
AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 i Uranium-235 EPA 908.0 Modified 1.54E-01 1.06E-01 1.06E-01 1.15E--01 2.44E-02 pCi/g I I
18-03111-04 I DO AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 I Uranium-235 EPA 908.0 Modified i 8.12E-02 7.21E-02 7.23E-02 7.76E-02 7.43E-03 : pCi/g
! ·-·~""""
18-03111-01 LCS KNOWN 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 I Uranium-238 EPA 908.0 Modified 7.05E+00 2.54E-01 I pCi/g
18-03111-01 LCS I SPIKE 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified 7.12E+00 9.46E-01 1.07E+00 7.43E-02 1.40E-02 pCi/g
18-03111-02 : MBL BLANK 03/23/18 00:00 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified -2.25E-04 2.39E-02 2.39E-02 7.10E-02 1.34E-02 pCi/g
18-03111-03 I DUP AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified : 7.25E-01 2.05E-01 2.12E-01 1.07E-01 3.76E-02 pCi/g
18-03111-04 DO AC-SED-11 03/21/1813:20 3/23/2018 3/30/2018 18-03111 Uranium-238 EPA 908.0 Modified 7.88E-01 2.10E-01 2.17E-01 7.52E-02 1.42E-02 pCi/g
CU=Counting Uncertainty;CSU=Combined Standard Uncertainty (1-sigma);MDA=Minimal Detected Activity;LCS=Laboratory Control Sample; MBL=Blank; DUP=Duplicate; TRG=Normal Sample; DO=Duplicate Original; CV=Critical Value
( . EBERLINE ~ ANALYTICAL
EBERLINE ALYTICAL ot\J 601 SCARBORO ROAD OAK RIDGE, TN 37830 865/481-0683 FAX 865/ 483-4621
0019
SECTIONV
ANALYTICAL STANDARD
0020
QA/QC REVIEWED CERTIFICATE OF CALIBRATION LL-8
· Date (? q(lnitials Ji£. ALPHA STANDARD SOLUTION
Radionuclide: U-238NAT
Half Life:
Customer:
P.O.No,:
TMA EBERLINE
OR2778
Catalog No.:
(4.468 ± 0.005) x lOA9 years
7338 Reference Date: January 11995 12:00 PST.
Source No.: 479-50 Contained Radioactivity: (Total U) 8.016 µ,Ci
Contained Radioactivity: (fotal U) 297 k:Bq
Description of Solution a. Mass of solution:
b. Chemical form:
65. 2896 g in a 50 ml flame sealed ampoule
Uranyl Nitrate in H20
c. Carrier content: None
d. Density: Approximately 1.3202
Radioimpurities
Radioactive Daughters
Refer to attached technical data sheet
Refer to attached technical data sheet
Radionuclide Concentration
(Total U) 0.1228 Method of Calibration
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level:
NIST Traceability
±3,0%
±0,0%
±2.0%
±3,6%
•
g/mI @20°c.
µCi/g.
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to "~tablish and maintain implicit traceability for a number of nuclides,
based on the blind as6lly (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
ISOTOPE PRODUCTS LABORATORIES
3017 N. SAN FERNANDO BLVD.
BURBANK, CALIFORNIA 91504
8}8•843•7000 FAX 818•843•6168
lE(Z,lv~
YCONTROL
~ t74::€Mk$ 19:z'f Date Signed
:', ·.,·,·•.···;,,,,,
) j ,,
0021
~ """"__i,;; BJ;;;~!':!,"' I QUALITY CONTROL PROGRAM
MP-009
Rev.a; 11/01/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP 009
CURRENT DATE 7/12/20170:00 SOLUTION REFERENCE # .... IP_L_4 ___ 7 __ 9---5-0-··· -------. SOLUTION#"""'·--.. -, .·"""',u.,...;..,...8...,'··'--· -. ---i
Half Life, Years I · .>,4;468E+09!
Radionuclide ' <?&{~U/ Certified Activity . 8t016Ef0O µCi
Certified Concentration · · . µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Half Life, Days I 1.632E+12!
Reference Date!. · :·•.:1/1119950:0o!
• . 9T6400 Weight, Grams ·· · >32;5020. Weight, Grams
65.1380 Weight, Grams 8.0160 µCl
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used l1MHN. O·· ·.·· .. , .... ' .. 3
Dilute to a volume of! . . 1000;00 ··. j milliliters
Certified Total Activity ofj Which Eauals . 1.780E+07jdpm at the date listed above
• • • . . • • . This activity concentration Is based on the original · And after dilution the act1v1ty of this solution 1s! 1;77955E+04!dpm/m•eference date listed above, All activities are corrected
to the date and time of analysis by the laboratory data processing software.
Expiration Date:! June 28, 2018
Date: 7/12/2017 0:00 -------Date: 7 / 23f( '.) ---,--r--1-----
0022
Rev.a; 11101103 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Date 7/12/2017 0:00 Solution Reference# IPL479~50 Solution # U-8a< .
Princi al Radionuclide :z34,•2~:2380:
Half Life, Years 1· 4:46$E+MI
Half Life, Days ! . · 1.632E+12I
Radionuclide of Interest, 234; 2~-: 2.~tJ. Reference Date!> •-.j)1i19950:00)
Parent Solution Cone .. 1.7796E+04 · dpmlml
Chemical Com osition of Standard Solution Uranly:Nitrat!:! in 11VF1:!N0i ·· ··
Dilution Instructions: Dilution Solvent Used !_-1MHNo-· :· . . 3 .
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
)t0000 ml 7.1182E+04 dpm
- 1000;00 ml Final Activity Concentration: I 7.1182E+01!dpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software. ------------------------, Isotopic Distribution as:
U-238 Atom % = 48.239 U-235 Atom % = 2.25 U-234 Atom%= 49.501 All values +/- 3.6%
U-238 = 71.182 dpm/rnl X 0.48249 = 34.345 dprn/ml U-235 = 71.182 dpmlrnl X 0.0225 = 1.602 dpm/ml U-238 = 71.182 dpm/ml X 0.49501 = 35.236 dpmlml
Isotopic ratios from manufacturer's data sheet
Verified&Appr~
Expiration Date:I June 28, 2018
0023
RECORD COf-YY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
Description
(
Product Description & Measurement Certificate
Principal radionuclide: Daughter Nuclide:
uranium 232 (U-232) Th-228
Product code: UDP10050 Batch Number: 92/232/67
Measurement Reference date: 01 March 2000
Accuracy
Radionuclidic Purity
Isotopic Purity
Chemical Composition
Physical Data
Remarks
Approved Signatory
Radioactive concentration U-232 which is equivalent to
6.739E+03 becquerels per gram of solution I.821E-01 microcuries per gram of solution
Volume of solution Total activity of U-232
which is equivalent to
5.035 millilitres 3.6IE+04 becquerels 9.76E-01 microcuries
Method of measurement (see reverse of this certificate) Random uncertainty is:± 0.7% Systematic uncertainty:± 0.5% Overall uncertainty in the radioactive concentration quoted above: ± 1.7% Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages of the activity of the principle radionuclide at the reference date.
Th-228 and daughter activity removed 2 Feb 2000 U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00
""he isotopic composition, exprP,ssed as atom per cent at the reference date .
,\Jot measured
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Recommended halflifo of uranium 232: 6.980E+Ol years Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0% Bra..'lching ratio for alpha emission: I 00% Calculated specific activity of uranium 232: 8.167E+05 Bq per microgram U-232.
For safety information and notes to ensure correct usage by all persons handling this radior-tctive Tracer solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and approved to ISO 9001.
Project Ref. AE:l315
Roger Wiltshire
Prepared and characteri~ed in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
Trkcert.wps I 0/03/00 AEA Techn1ilogy is the trading name of AEA Technology pie
0024
,:EBERS~~~
Rev.B; 11/01 /03
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICA TfON
MP009
CURRENT DATE 10/7/2017 0:00 ...-----------. --------1 SOLUTION REFERENCE# AEA/Amersham 92/232/67 SOLUTION # U-10
Princi al Radionuclide 232u
Radionuclide 232U
Half Life, Years
I· 7.200E+o1 I
Certified Activity 9. 760E-01 µCi Certified Concentration µCi per gram .__ ___ __,
Half Life, Days
I 2.630E+04j
Reference Date! ..... ___ 3/_1_/2_0_00_0:_0__.0 I
Ampoule /Solution Gross~Weight, Grams Empty Ampoule Weight, Grams
Solution Net Weight, Grams
Total Activity in Ampoule 0.9760 µCi
Chemical Com osition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Dilute to a volume ofl 1000.00 !milliliters
Certified Total Activity ofl 0.976DlµCi Which Eauals 2.167E+06!dpm at the date listed above
And after dilution the activity of this solution isl 2.167E+03ldp'm/ml This activity concentration is based on tile original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date: i October 4, 2018
Date: 10/7/2017 0:00
Date:
0025
QUALITY CONTROL PROGRAM MP-009
Rev.8; 11/01/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY · RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Date 10/7/20170:00
Solution Reference # AEA/Amersham 92/232/67 Solution # U-1 Oa
Principal Radionuclide Half Life, Years 3 .u I 7 .200E+01 I
Half Life, Days I 2.630E+04I
Radionuclide of Interest 23 U Reference Date.__l ___ 3_/1_/2_0_0_0_0_:o_o.,JI
Parent Solution Cone. 2.167E+03 dpm/ml
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
10.0000 ml 2.1670E+04 dpm
1000.00 ml Final Activity Concentration: I 2.1670E+01 jdpm/ml
This activity concentration is based on the original reference date listed· above. All activities are · corrected to the date and time of analysis by the laboratory data processing software. ·
Expiration Date:I October 4, 2018
10/7/2017 0:00
Date:
0026
Radionuclide:
Half Life:
CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION
Th-232 Customer:
P.O.No.:
TMA EBERLINE
VH1632
1h-8
Catalog No.:
. (1.405 ± 0.006) x lOA 10 years
7232 Reference Date: November 11993 12:00 PST.
Source No.: 435-104-2 Contained Radioactivity: (Th-232) 0.0933 µCi.
Contained Radioactivity: (Th-232) 3.45 k.Bq.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
11.9712 g (in a 10 ml flame sealed ampoule)
Th(N03)4 in water
None added
d. Density: Approx. 1.21 g/ml@20°C.
Radioimpurities None detected (other than daughters).
Radioactive Daughters Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212, Po-212, Tl-208
Radionuclide Concentration
(Th-232) 0.00779
Method of Calibration Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level:
NIST Traceability
±3.0%
±0,0%
±2,0%
±3.6%
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
I. Nuclear data were taken from "'!'.able of Radioactive Isotopes", edited by Virginia S. Shirley, i 986.
µCi/g,
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4. 15).
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 ~ 7000
QUALITY CONTROL
Date Signed
0027
~Ea EJ¾~!:i!!i I
QUALITY CONTROL PROGRAM MP-009
Rev.8; 1110/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATE 8/16/2017 0:00 SOLUTION REFERENCE #""'IP""'L_A.,...,3,_,,5....,:::1,.....04,..,.. .. :.-2-, -,,------. SOLUTION # · .. . . .. Th-8
Half Life, Years Half Life, Days ! 1AOSE+10I ! 5.132E+12l
Radionuclide · h · Certified Activity . · 9.330E-'-02 µCi
Reference Date I ..... · . _ _;.1.1..;../.1_1_19..,..9_3_0_: o__,o I Certified Concentration.__ ___ _.µCi per gram
Ampoule /Solution Gross · 18,8415 Weight, Grams Empty Ampoule --=·-··.:6.9296 Weight, Grams
Solution Net 11.9119 Weight, Grams Total Activity in Ampoule 0.0933 µCi
Chemical Composition of Standard Solution
DIiution Instructions: Dilution Solvent Used j1% NitricAcid
Dilute to a volume ofl. 1000,00 ·. I milliliters
Certified Total Activity ofl 0.0933jµCi Which Eauals 2.071 E+OSjdpm at the date listed above
I
And after dilution the activity of this solution isl 2.071E+02jdpm/ml This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:! August 11, 2018
R/1R/?017 O·Of)
0028
Rev.8; 1/10/03 Title: Radioactive Reference Standards· Solutions & Records
EBERLINE SERVICES· OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Solution Reference# IPL 435:;:.10~2-
Princi al Radionuclide ·· 226&232Th
Radionuclide of Interest ·• ·. 228 & 232Th ·
Half Life, Years ! 1.405E+1DI
Parent Solution Cone. 2.07E+02 ·· dpm/ml
Chemical Composition of Standard Solution
Date 8/16/2017 O;OO Solution # ·. . Jh-,8b
Half Life, Days ! 5.132E+12I
Reference Date! · 1111/199$ o:ooj
Dilution Instructions: Dilution Solvent Used
SECONDARY VOLUMETRIC DILUTION
) 1 % Nitric Acid
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
• soo:0000 ml 1.0355E+05 dpm
1000.00 ml Final Activity Concentration:! 1.0355E+02!dpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date: I August 11, 2018
Date: 8/16/2017 0:00 ----,----Date: ~ h0/i:1 -----·7 ~)...._, __
I
0029
RTIFICATE OF CALIBRATIOti.it , LPHA STANDARD SOLUTIO~ \)c', ~:;\\tli
Radionuclide
Half Life:
Th-230 Customer:
P.O.No.:
..1{'~i1t~ ~~ TMA EBE!lLM~ 1,i,t
Catalog No.:
(7 .54 ± 0.03) X 10"4 years
7230 TT4944 \\I~'
Reference Date: November 1 1991 12:00 PST.
Source No.: Contained Radioactivity: 1.036 µCi.
Description of Solution a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:
Radioimpurities
Radioactive Daughters
Radionuclide Concentration
Method of Calibration
5,0042 Th(NO3)4 in 0.lN HNO3
None added 1.0016
See attached technical data sheet
See attached technical data sheet
0.207
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
Uncertainty of Measurement a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
NIST Traceability
±2.0% ±0.5% ±0.2% ±2,7%
grams.
gram/ml @ 20°c.
µCi/gram.
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Notes 1. Nuclear data were taken from "Table of Isotopes", Seventh Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay(and later NIST certification) of Standard Reference Materials. (As in NRC Regulatory Guide 4.15)
ISOTOPE PRODUCTS LABORATORIES 1800 No. Keystone Street., Burbank, California 91504 818 843 - 7000
0030
Rev.14; 10/10/2012
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION MP009
CURRENT DATE 2/10/2018 0:00 SOLUTION REFERENCE #.-IP_L_3_8_8_-1_1_6 ____ _, SOLUTION #1----T-h--1---
Princi al Radionuclide 230Th
Half Life, Years
I 7.540E+04I
Radionuclide l30Thorium
Certified Activity 1.036E+OO µCi Certified Concentration .__ ___ _,µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
Chemical Composition of Standard Solution
Half Life, Days
I 2.754E+07I
Reference Date._! __ 1_1/_1_/1_9_91_0:_o_.ol
9.2660 Weight, Grams 4.6218 Weight, Grams 4.6442 Weight, Grams 1.0360 µCi
Dilution Instructions: Dilution Solvent Used !0.1N HN03
Dilute to a volume of! 1000. 00 I milliliters
Certified Total Activity ofl 1.0360/µCi Which Eauals 2.300E+06ldpm at the date listed above
This activity concentration is based on the original
And after dilution the activity of this solution isl 2.300E+03ldpmhmence date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date: I January 10, 2019
,,,,-· ··--~.~----
Date: 2/10/2018 0:00 --------Date: '3 cg;·
--~,;i.i::.<:.µ....;;.;::;::___
0031
.. ~1;)
)G.,--, ,E B EJ P. LJHN E '~)· '·! ,,,,.,,_'j'.
Rev,14; 10/10/2012
QUALITY CONTROL PROGRAM MP-009
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE STANDARD SOLUTIONS SECONDARY DILUTION RECERTIFICATION
MP-009 Date! 2/10/2018 O:OOI
Solution Reference# IPL 388-116 I Solution #I Th-1 b I
Principal Radionuclide Half Life, Years
I 7.540E+04I
Half Life, Days
,ouTh I I 2.754E+07I
Radionuclide of Interest ,ouThorium Reference Date!~ __ 1_1_/1_/1_9_9_1 _0_:o~ol
Parent Solution Cone. 2.30E+03 dpmlml
Chemical Composition of Standard Solution
Dilution Instructions: Dilution Solvent Used j0.1N HNO3
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: 10.0000 ml
Total Activity: 2.2999E+04 dpm
final Volume: 1000.00 ml
NOTES:
Final Activity Concentration: I 2.2999E+01 \dpmlml
This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by th,e
laboratory data processing software.
Expiration Date:l January 10, 2019 I
Date: 2/10/2018 0:00
Date:
-----,----
s:?, I 31/ ~ I
0032
-~ Isotope Products Laboratories
An Eckert & Ziegler Company
24937 Avenue Tibbitts Valencia, California 91355
Tel 661•309·1010 Fax 661•257•8303
CERTIFICATE OF CALIBRATION ALPHA STANDARD SOLUTION
Radionuclide: Half-life: Catalog No.:
Th-229 7340 ± 160 years 7229
Customer: P.O.No.: Reference Date:
EBERLINE SERVICES 00009633 15-Jan-02 12:00 PST
Source No.: 867-54 Contained Radioactivity: (Th-229 only)
1.013 µCi 37.48
Physical Description: A. Mass of solution: B. Chemical form:
5.0147 gin 5 ml flame-sealed ampoule Th(NO3) 4 in 0.1 M HNO3
C. Carrier content: 10µg Th/ml D. Density: 1.0016 g/mL@ 20°c.
Radioimpurities:
None detected (daughters in equilibrium)
Radionuclide Concentration: 0.2020 µCi/g, 7.474 kBq/g
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in µCi/g was determined using gamma ray spectrometry. · Peak energy used for integration: 193.5 keV Branching ratio used: 0.0441 gammas per decay
Uncertainty of Measurement: A. Type A (random) uncertainty: B. Type B (systematic) uncertainty: C. Uncertainty in aliquot weighing: D. Total uncertainty at the 99% confidence level:
Notes: - See reverse side for leak test(s) performed on this source.
± 0.7 % ± 3.0 % ± 0.0 % ± 3.1 %
kBq
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRG Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261. - This solution has a working life of 5 years.
Quality'control Date Signed IPL Ref. No.: 867-54
------------------ ISO 9001 CERTIFIED ------------------
Medical Imaging Laboratory Industrial Gauging Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1800 North Keystone Street Burbank,California 91504
0033
;: I;. BEIR!,,.~!';'o!/i I QUALITY CONTROL PROGRAM
MP-009
Rev.a; 1/10/03 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY RADIOACTIVE REFERENCE SOLUTIONS PRIMARY DILUnON RECERTIFICATION
MP 009
CURRENT DATE SOLUTION REFERENCE # .... IP __ L .... ':8 .... 67-~-54.....,•.--,,.------. SOLUTION #1-•· ....,.......,......,,.., ____ _
Half Life, Years 1 · . i340E+03l
Radionuclide ~h . Certified Activity · 1;013E+00 µCi
Certified Concentration.._ ___ _. µCi per gram
Ampoule /Solution Gross Empty Ampoule
Solution Net Total Activity in Ampoule
, .. , .. .,.
Chemical Com osition.of Standard Solution
8.7752 ;3..79~1 5.0161 1.0130
Half Life, Days l 2.681E+06l
Reference Date._! __ 1_/_15_/2_0_0 __ 2_0-'--:0 ...... oj
Weight, Grams Weight, Grams Weight, Grams µCi
Dilution Instructions: Dilution Solvent Used
Dilute to a volume of! • 1000.00C !milliliters
Certified Total Activity ofl 1.0130jµCi Which EQuals 2.249E+06jdpm at the date listed above
This activity concentration is based on the original And after dilution the activity of this solution isl 2.249E+03jdpm/ml reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data processing software.
Expiration Date: I August 11, 2018 I
n::itA· R/1Rf?n11 n·nn
Date: -.....a~~[(.o+-{t 1-+--
0034
, e; .. a~RL..JN __ E; I auAuTY coMP~T00RoL PROGRAM
~ S~"VIC~'S ""'
Rev.7; 9/29/99 Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES-OAK RIDGE LABORATORY RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009 Solution Reference # IPLB67:-54 •·
Princi al Radionuclide · · 229r11 ·
Radionuclide of Interest · 229th ·
Half Life, Years ! i.340E+03!
Parent Solution Cone. ·· 2.25E+03 .. dpm/ml
Chemical Com osition of Standard Solution TH(N03kin 0.1M HNOi . .· · .
Date 8/16/2017 0:00 Solution # Th-.18a ..
Half Life, Dar I 2.a
Reference Date! ._ __ 11_1 s_/_20_0_2_0_:o_o .... l
Dilution Instructions: Dilution Solvent Used
Vol. Parent Solution: Total Activity: Final Volume:
NOTES:
SECONDARY VOLUMETRIC DILUTION
< 10:0000 ml 2.2490E+04 dpm
10b0:oo ml Final Activity Concentration:! 2.2490E+01 !dpm/ml
This activity concentration is based on the original reference date listed above. All activities are corrected to the date and time of analysis by the laboratory data processing software.
Expiration Date:1 August 11, 2018
::::: ====~=,1=6=:::;:;-7_=7:o_:_o_o __ _
0035
-4!r t:ckert & Ziegier Analytics
CERTIFICATE OF CALIBRATION Standard Reference Source
SRS Number: 104852
Source Description: Sand in 16 Ounce PP Omega Jar Filled to Capacity
Product Code: 8401-EG-SAN
Customer: Eberline Analytical Corporation
P.O. Number: OR-1610009, Item 4
1380 Seaboard Industrial lllvd. Atlanta, Georgfa 303 lB Tel 404•352•8677
Fax 404•352•2837
www.ezag.com
This standard radionuclide source was prepared from an aliquot measured gravimetrically from a master
radionuclide solution calibrated with a germanium gamma-ray spectrometer system. Additional radionuclides were
added gravimetrically from solutions calibrated by gamma-ray spectrometry, ionization chamber, or liquid
scintillation counting. Calibration and purity were checked using germanium gamma-ray spectrometry. At the time
of calibration no interfering gamma-ray emitting impurities were detected. The gamma-ray emission rates for the
most intense gamma-ray lines are given. Eckert & Ziegler Analytics (EZA) maintains traceability to the National
Institute of Standards and Technology (NIST) through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 2, July 2007, and compliance with ANSI N42.22-l995, "Traceability of Radioactive
Sources to NIST."
Reference Date: 0l-October-2016
MGSMixture
12:00PMEST
Gamma-Ray Uncertainty Calibration Isotope Energy, keV Half-Life, d Activity, Bq Flux, s-i uA, % u8, % u, %* Method**
~~ .. a'~~~-~111.t~~I Cd-109 88.0 4.614E+02 7.668E+04 2.837E+03 0.5 2.0 4.1 HPGe
~~~~~.,,,-z,~=.-,•"\:;jl,~:E~~"r,W-~- . ... - . -~~1'-~~F~~= ~~~~&~~,~~~ -, .. ' - '. ,_.,. ·~@-~~~ =:-;--;.:;::.,::;l,~~~
Ce--139 165.9 l.376E+02 2.655E+03 Z.124E+03 0.4 1.7 3.6 HPGe -1il~D'.~- _;~.-,: .i,· ~,,-.,,, :,.·~: ·-3
Sn-113 391.7 l.151E+02 4.528E+03 2.942E+03 0.4 1.9 3.9 HPGe • ~ .r.=..~. -~~ ~~··.iv,'.'_•;• ; :,: ~~ ~--· $ • J."'' ;:~--~
Y-88 898.0 l.066E+02 7.415E+03 6.948E+03 0.7 1.7 ~~:1~ • ,,. ' . . ~-~ .•-:· -:; ... - -~~
Co-60 1173.2 l .925E+03 3.562E+03 3.557E+03 ~~~~as~~ ---Mixed Gamma (MGS) master solution is EZA's eight isotope mixture which is calibrated quarterly and consists of
Cd-109, Co-67, Ce-139, Hg-203, Sn-113, Cs-137, Y-88, and Co-60, llrlJncertainty: U -Relative expanded uncertainty,
k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncertainty of NIST
Measurement Results." """Calibration Methods: 4n LS - 4n Liquid Scintillation Counting, HPGe - High Purity
Germanium Gamma-Ray Spectrometer, IC - Ionization Chamber.
(Certificate cont.inued on reve!'$e $ide)
EZA Certificate Program Rev. 0, 07-DEC-201 S Page 1 of 2
Corporate Office laboratory
24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
0036
-~ Eckert & Ziegler Analytics
1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404•352•8677
Fax 404•352•2837
www.analyticsinc.com
CERTIFICATE OF CALIBRATION Standard Radionuclide Source GAS- ('+D~
98503 Sand in 16 Ounce PP Taral Jar Filled to Capacity
Customer: Eberline Analytical Corporation P.O. No.: OR-1405030, Item 6 Product Code: 8401-EG-SAN
Reference Date: 01-0ct-2014 12:00 PM EST Grams of Master Source: 0.017608
Thls standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Additional radionuclides were added gravimetrically from solutions calibrated by
gamma-ray spectrometry, ionization chamber, or liquid scintillation counting. Calibration and purity were
checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma
ray emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines
are given. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and
Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15,
Revision 2, July 2007, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST."
EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this
source was produced in accordance with the HPS accreditation requirements. Customers may report any
concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean,
VA 22101.
Master Uncertainty* , %
Gamma-Ray Half-Life, Source* This Source Type Calibration
Nuclide Energy (ke V) Days yps/gram yps UA UB u Method*
Arn-241 69.5 l.580E+05 2.030E+03 0.1 1.8 3.6 -4nLS
Cd-109 88.0 4.614E+02 l.663E+05 2.929E+03 0.5 2.0 4.1 HPGe
Co-57 122.1 2.717E+02 8.913E+04 l.669E+03 0.4 1.7 3.6 HPGe
Ce-139 165.9 l.376E+02 l.241E+05 2.185E+03 0.4 1.7 3.5 HPGe
Hg-203 279.2 4.659E+0l 2.675E+05 4.710E+03 0.3 1.7 3.5 HPGe
Sn-113 391.7 l.151E+02 1.796E+06 3.163E+03 0.4 1.9 3.9 HPGe
Cs-137 661.7 l.099E+04 1.ll 1E+05 1.956E+03 0.7 1.9 4.0 HPGe
Y-88 898.0 l.066E+02 4.223E+06 7.435E+03 0.7 1.7 3.7 HPGe
Co-60 1173.2 l.925E+03 2.091E+05 3.683E+03 0.7 1.8 3.9 HPGe
Co-60 1332.5 l.925E+03 2.094E+05 3.687E+03 0.7 1.8 3.9 HPGe
Y-88 1836.1 l.066E+02 4.471E+05 7.872E+03 0.7 l.7 3.7 HPGe
* Master Source refers to Analytics' 8-isotope mixture which is calibrated quarterly.
Calibration Methods: 4n IB- 4 pi Liquid Scintillation Counting, HPGe. High Purity Germanium Gamma-Ray Spectrometer, IC -
Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k"' 2. See NIST Technical Note 1297, "Guidelines for
Evaluating and Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
MGS Certificate Rev 7, 11 September 2014 Page 1 of 2
Corporate Office Laboratory
24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Slvd. Atlanta, Georgia, 30318
0037
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
0038
Eberline Analytical
Analysis Control Chart
WO
18-03111
Analyte
U-234
U-238
Analyte
Analyte
U-234
U-238
U-235
Version
Nonnalized Difference
Analysis
UUISO
LCS I Measured
92.20%
101.10%
MS Actual %Rec
CSU Measured
15.22%
15.08%
Expected MS Result
Duplicate Results
Nonnalized RPD Original
Difference Result
2.09 41.80 9.93E-01
0.41 8.38 7.88E-01
1.11 61.78 8.12E-02
Run Activity Units Aliquot Units
1 pCi g
Laboratory Control Sample
LCS Expected
100.00%
100.00%
Expected MS Uncerl
Original CSU
2.52E-01
2.17E-01
7.23E-02
Uncert. Expected
Known
3.60% 7.27E+00
3.60% 7.0SE+00
Matrix Spike
Actual MS Result
Duplicate Result
6.S0E-01
7.25E-01
1.54E-01
Actual MS CSU
Duplicate CSU
2.00E-01
2.12E-01
1.06E-01
Known Error
2.62E-01
2.54E-01
Sample Result
LCS Relative
Bias
0.92
1.01
Result
6.71E+00
7.12E+00
Sample CSU
LCS¾R
OK
OK
OK
I
CSU
1.02E+00
1.07E+00
Sample Aliquot
Printed: 4/2/2018 8:31 AM Page 1 of 2
Client Name
Auxier & Associates, Inc.
Standard ID
U-Sa
U-8a
Standard ID
Standard ACT(dpm)
3.20E+01
3.10E+01
Standard ACT(dpm)
Standard Error
3.60E+00
3.60E+00
Standard Error%
Standard Added (g)
5.0SE-01
5.0SE-01
Standard Added (g)
QC Summary
I MS¾R I MSND I RepRPD I Rep ND
INV OK
OK OK
NA OK
0039
Eberline Analytical Analysis Control Chart
WO
18-03111
130.00
120.00
110.00
100.00
90.00
80.00
Analysis Run
UUISO 1
LCS % Recovery
L _________ _
Activity Units Ali_g_uot Units
pCi g
40.00
35.00
30.00
25.00
20.00
15.00
10.00
l
Printed: 4/2/2018 8:31 AM Page 2 of 2
Client Name
Auxier & Associates, Inc.
Replicate Sample RPD
l
70.00 ------------------~-----------------~ !
U-234 U-238 5.00
- LowerError 73.38 82.42
- Upper Error 111.03 119.79 o.oo +------,,.=,;-------,----u~ U-234 U-238 I U-235
• %R 92.20 101.10
- -LCL 75 75 - Lower Error
- UpperError
47.55 9.57
I 85.26
36.05 7.19 38.30
--Mean 100 100
- -UCL 125 125 • RPD
--CL
41.80 8.38
I 61.78
35 35 35
Normalized Difference
3.50 No Matrix Spike
3.00
2.50
2.00
1.50
1.00
0.50
0 00 LCS ND MS ND
-U-234 0.00 2.09 0.00
=U-238 0.00 0.41 0.00
= 0.00 0.00 0.00
- UCL 3 3 3
Version
0040
Eberline Analytical
Analysis Control Chart
WO
18-03111
Analyte
TH-228
TH-230
TH-232
Analyte
Analyte
TH-228
TH-230
TH-232
Version
Analysis
ThlSO
LCS CSU Measured Measured
122.00% 18.20%
121.89% I 19.77%
122.44% I 17.88%
Normalized MS Actual Expected
Difference %Rec MS Result
Duplicate Results
Normalized RPD
Original
Difference Result
1.11 27.71 7.91E-01
0.59 13.93 1.34E+00
1.22 30.19 1.12E+00
Run Activit Units Ali uot Units I
1 I pCi I
g I
Laboratory Control Sample
LCS Uncert. Known
Known Result
Expected Expected Error
100.00% 3.60% 5.11E+00 1.84E-01 6.24E+00
100.00% 2.70% 5.39E+00 1.45E-01 6.57E+00
100.00% 3.60% 5.11E+00 1.84E-01 6.26E+00
Matrix Spike
Expected Actual Actual Sample Sample
MS Uncert MS Result MS CSU Result CSU
I Original Duplicate Duplicate LCS Relative
LCS%R I CSU Result CSU Bias
3.04E-01 1.05E+00 3.32E-01 1.22 OK
4.47E-01 1.17E+00 3.68E-01 1.22 OK
3.79E-01 8.29E-01 2.81E-01 1.22 OK
Printed: 3/30/2018 1 :59 PM Page 1 of 2
Client Name
Auxier & Associates, Inc.
CSU Standard Standard Standard Standard
ID ACT(dpm) Error Added (g)
1.14E+00 Th-Sb 1.04E+02 3.60E+00 1.10E-01
1.30E+00 Th-1b 2.35E+01 2.70E+00 5.0SE-01
1.12E+00 Th-Sb 1.04E+02 3.60E+00 1.10E-01
Sample Standard Standard
I Standard
I Standard
Aliquot ID ACT(dpm) Error¾ Added(g)
QC Summary
I MS%R I MSND I RepRPD I Rep ND
INV OK
OK OK
INV OK
0041
Eberline Analytical Analysis Control Chart
WO
18-03111 Analysis Run
ThlSO 1
LCS % Recovery 130,00
120.00
110.00
100,00
r------r------1-90.00
80.00
-----= ----- -~ I H-228 I H-230 TH-232
- Lower Error' 100.21 99.41 100.96
- Upper Error 143.80 144.36 143.91
• %R 122.00 121.89 122.44
- -LCL 75 75 75
--Mean 100 100 100
- -UCL 125 125 I 125
Normalized Difference
3.50 ~-------------------------------
3.00 l-------------------------------2.50 l-------------------------------
2.00 l ______________________________ _ 1.50 +-------------------------------
1.00 +-------------
0.50
0.00 LCS ND MSND
-TH-2281 0.00 1.11 0.00
=TH-2301 0.00 0.59 0.00
- UCL I 3 3 3
Version
Activity Units Aliguot Units
pCi g
40.00
35.00
30.00
25.00
20.00
15.00
10.00
Printed: 3/30/2018 1 :59 PM Page 2 of 2
Client Name
Auxier & Associates, Inc.
Replicate Sample RPD
! -------------7 !
5.00
o.ooL~---r-~c=~~~= - Lower Error
TH-228 TH-230 TH-232
32.51 16.19 35.29
- UpperError 22.91 11.67 25.08
• RPD 27.71 13.93 30.19
--CL 35 35 35
No Matrix Spike
0042
Eberline Analytical Analysis Control Chart
18-03111
Analyte
CO-60
CS-137
Analyte
Analyte
AC-228
81-214
K-40
Version
Normalized Difference
Analysis
Gamma
LCS Measured
97.25%
98.43%
MS Actual %Rec
CSU Measured
8.02%
10.62%
Expected MS Result
Duplicate Results
Normalized RPD Original
Difference Result
1.20 22.27 1.09E+00
0.35 4.66 1.11E+00
0.51 5.25 1.68E+01
Run Activity_ Units Alig_uot Units
1 pCi g
Laboratory Control Sample
LCS Expected
100.00%
100.00%
Expected MS Uncert
Original CSU
2.66E-01
2.03E-01
2.42E+00
Uncert. Known
Expected
3.89% 1.35E+02
4.01% 8.44E+01
Matrix Spike
Actual MS Result
Duplicate Result
8.74E-01
1.06E+00
1.60E+01
Actual MS CSU
Duplicate CSU
2.38E-01
2.00E-01
2.28E+00
Known Error
5.27E+00
3.38E+00
Sample Result
LCS Relative Bias
0.97
0.98
Result
1.32E+02
8.31E+01
Sample CSU
LCS%R
OK
OK
I
CSU
1.06E+01
8.82E+00
Sample Aliquot
Printed: 4/17/2018 8:28 AM Page 1 of 2
Client Name
Auxier & Associates, Inc.
I Standard
ID
GAS-1402
GAS-1402
Standard ID
Standard ACT(dpm)
1.35E+02
8.44E+01
Standard ACT(dpm)
Standard Error
5.27E+00
3.38E+00
Standard Error¾
Standard Added (g)
7.36E+02
7.36E+02
Standard Added(g)
QC Summary
I MS%R I MSND I RepRPD I RepND
<CS-137 AC-228> OK
<CO-60 81-214> OK OK
K-40> OK OK
0043
Eberline Analytical Analysis Control Chart
WO • 18-03111
130,00
120.00
110.00
100.00
90.00
80.00
Analysis Run
Gamma 1
LCS % Recovery
1 1 I I
70·00
: CO-60 CS-137
- LowerError 85.33 83.81
- Upper Error 109.16 113.05
• %R 97.25 98.43
- -LCL 75 75
--Mean 100 100
- -UCL 125 125
Normalized Difference
3.50
3.00
2.50
2.00
1.50
1.00
0.50
000 LCSND MSND
-
-CO-60 0.00 1.20 0.00
=cs-137 0.00 0.35 0.00
= 0.00 I 0.00 0.00
- UCL 3 I 3 3
Version
Activity_ Units Ali_guot Units
pCi g
40.00
35.00
30.00
25.00
20.00
15.00
10.00
5.00
T • l
Printed: 4/17/2018 8:28 AM Page 2 of 2
Client Name
Auxier & Associates, Inc.
Replicate Sample RPD
• • 0.00 -+--------------~------------~
AC-228 B1-214 K-40
- Lower Error 25.13 5.09 i 5.63
- UpperError
• RPO 19.41 4.22
I 4.87
22.27 4.66 5.25
--CL 35 35 i 35
No Matrix Spike
0044
SECTION VII
LABO RA TORY TECHNICIAN'S NOTES & RUN LOGS
0045
ISOUNOTES
0046
Printed: 3/28/2018 8:16 AM
,:EBER~~~c~ Work Order Analysis Notes
# Date Dept User
1 03/28/18 08: 15 PREP JHARVEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak RidC1e, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Page 1 of 1
Internal Work Order 18-03111 ------~--------,-- _____ ,,
Analysis Code UUISO Run Number 1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS'-ADDED HF AND DRIED SAMPLES DOWN-ADDED
MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS
0047
Printed: 3/29/2018 3:18 PM Page 1 of 1
( Oak Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. 1 .....•• - -· -EBERLINE .... ® SERVICES Oak Ridge, TN 37830 Analysis Code UUISO
Work Order Analysis Notes Voice: 865.481.0683 , .... www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 03/28/18 08:15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND DRIED SAMPLES DOWN- ADDED
MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS
2 03/29/18 15: 18 CHEM JDEMELAS Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH4I, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in ~10 ml of concentrated HCI; Transferred le
new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.
-
0048
Printed: 3/30/2018 4:52 AM Page 1 of 1
~ Oak Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. --EBER~~~c~ Oak Ridge, TN 37830 Analysis Code UUISO Voice: 865,481.0683
Work Order Analysis Notes www.eberlineservices.com 1 Run Number
# Date Dept User Notes
1 03/28/18 08: 15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND DRIED SAMPLES DOWN- ADDED
MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS
2 03/29/18 15:18 CHEM JDEMELAS Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to ~35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H2O. Set samples aside for later precipitation and filtering.
m,•,-•-•
3 03/30/18 04:51 CHEM TSMITH Followed steps 12.1.7 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Uranium)
0049
Eberline Analytical Oak Ridge Laboratory
Q EBERLINE "M> .... ····························· .. SERVICES
Reagents Used in an Analysis
Printed: 3/30/2018 4:58 AM Page 1 of 1
Internal Work Order
18-03111 Analysis Code Run
UUISO 1 ··-·-- -----··-··-·-•-·-··--------· --+-------------,--·-·------··--1-----··-··
Reagent ID
Reagent Name
·············•·····•-··----+-------------------+
019621P Hydrofluoric Acid
Reagent Concentration
Analyst ID
Date Recorded
Reagent Grade JHARVEY 3/28/2018
019673P Nitric Acid Reagent Grade JHARVEY 3/28/2018 ----
019529P Perchloric Acid Reagent Grade JHARVEY 3/28/2018 ··•--············
019351P Sulfuric Acid Reagent Grade JHARVEY 3/28/2018 ····--··········---······-·------·---t-------------------+-····-··-----·····-~
017230P Anion Exchange Resin Reagent Grade JDEMELAS 3/29/2018 --•··-·-···--·--·~····'
019826S HCI - HF 6.5N - 0.04N JDEMELAS 3/29/2018 ----r---- -----
019775D02 Hydrochloric Acid 0.SN JDEMELAS 3/29/2018
019827S Hydrochloric Acid 6.5N JDEMELAS 3/29/2018
019842S Hydrochloric Acid SN JDEMELAS 3/29/2018 --+-----·········---------------------------------+--····•·
019831P Hydrochloric Acid Reagent Grade JDEMELAS 3/29/2018 . ---~-------,~-----·-· ---+----···-·-····----···········-·············----··· ......
019861S HCI - NH4I SN - 0.lM JDEMELAS 3/29/2018 --•••--t--••'"•••~,_,,., __ '<"<¥.,_~••~--"~-•~w•-~•-•-•••->•--------+•
019803S Carbon substrate Solution TSMITH 3/30/2018
019525P Hydrofluoric Acid Reagent Grade TSMITH 3/30/2018
019640S Neodymium Carrier 1 mg/ml TSMITH 3/30/2018 -·····-··+····-·
019599P Reagent Alcohol Reagent Grade TSMITH 3/30/2018
019433P Titanous Chloride Reagent Grade TSMITH 3/30/2018
0050
5
7 I
----+--------------+------+------1-------1----
---1~----------1--------t------+---+---
----~,1..-----.-----+-------1----->-----+------+---
0051
ISO TH NOTES
0052
Printed: 3/28/2018 8:15 AM
,: E BER6tt':'c!';; Work Order Analysis Notes
# Date Dept User
1 03/28/18 08: 15 PREP JHARVEY
Oak Ridge Laboratory
601 Scarboro Rd. Oak Ridae, TN 37830 Voice: 865.481.0683 www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
Notes
Page 1 of 1
18-03111 ThlSO
1
ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND ORI Eb SAMPLES DOWN- ADDED
MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPAR.ATIONS
0053
Printed: 3/29/2018 3:19 PM Page 1 of 1
~ Oak Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. -~'"•·-· ""'"'"" EBERLINE
-~ . . - ... SERV1C:ES Oal< Ridge, TN 37830 Analysis Code ThlSO Voice: 865.481.0683 Work Order Analysis Notes ·--~ --···--··
www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 03/28/18 08: 15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS-ADDED HF AND DRIED SAMPLES DOWN-ADDED
MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS
2 03/29/18 15: 19 CHEM JDEMELAS Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and
transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in -1 O ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water brinaina volume to -1 Sml. Set samples aside for later orecipitation and filterina.
0054
Printed: 3/30/2018 4:54 AM Page 1 of 1
~ Oal< Ridge Laboratory Internal Work Order 18-03111 601 Scarboro Rd. . ..•
EBER~~~c~ Oak Ridge, TN 37830 Analysis Code ThlSO Work Order Analysis Notes Voice: 865,481.0683 M•~---•---••••--• ------··-·-~- ··~- -·~·"-""-
www.eberlineservices.com Run Number 1
# Date Dept User Notes
1 03/28/18 08: 15 PREP JHARVEY ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HF AND DRIED SAMPLES DOWN- ADDED
MIXED ACIDS AND TOOK SAMPLES TO DRYNESS- SUBMITTED SAMPLES TO SEPARATIONS
2 03/29/18 15: 19 CHEM JDEMELAS Added concentrated HNO3 to sample beakers and heated to dryness; Added 20 ml 8N HNO3 to samples and
transferred to new, labeled C-Tubes, adding 8N HNO3 to bring volume to ~35 ml; Preconditioned resin
columns with 50 ml 8N HNO3; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HNO3; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HNO3;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in ~10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water, bringing volume to ~15ml. Set sameles aside for later erecieitation and filtering.
3 03/30/18 04:54 CHEM TSMITH Followed steps 12.2.5 to 12.4.5 in AP-005. ( Precipitated and filtered samples for Thorium)
0055
Eberline Analytical Oak Ridge Laboratory
Printed: 3/30/2018 4:59 AM Page 1 of 1
-----------N·-----·-·-------~-
Q EBERLINE ® ·······························. SERv1c::Es
Reagents Used in an Analysis
Reagent ID
019621P
019673P
019529P
019351P
Reagent Name
Hydrofluoric Acid
Nitric Acid
Perchloric Acid
Sulfuric Acid
Internal Work Order
18-03111 Analysis Code
·-············---·-···---- ----------
ThISO ----•-•" w -··-··--··-- ,_
Reagent Analyst Concentration ID
Reagent Grade )HARVEY
Reagent Grade JHARVEY
Reagent Grade JHARVEY
Reagent Grade JHARVEY
Run
1 Date
Recorded
3/28/2018
3/28/2018
3/28/2018
3/28/2018 -,-~~-·-··-~···--···-----+--------·--------<------------>---------+---
0l 7230P Anion Exchange Resin Reagent Grade JDEMELAS ·········-·-l---------------+-----------+--
019831P Hydrochloric Acid Reagent Grade
Nitric Acid SN 019841S
019859S
019860S
019673P
·•····+···-····-·•·•···············-···············--------+------····-········-
019803S ···--···-·-----
019578S
Hydrochloric Acid
Nitric Acid
Nitric Acid
Carbon substrate
Cerrium Carrier
SN
SN
Reagent Grade
Solution
0.lmg/ml
JDEMELAS
JDEMELAS
JDEMELAS
JDEMELAS
JDEMELAS
TSMITH
TSMITH ----------+-------------t--------
019525P Hydrofluoric Acid Reagent Grade TSMITH ········-·····················•·····~····-·····-······-·········---·---------+-----
o 19599P Reagent Alcohol Reagent Grade TSMITH
3/29/2018
3/29/2018
3/29/2018
3/29/2018
3/29/2018
3/29/2018
3/30/2018
3/30/2018
3/30/2018
3/30/2018 ··················-·------------~---------~--------'··································'
0056
u \ < . l_k_(SU_~_· --t--:~~~\--1----"--""·~,::___- ----
l \ l~ ' ~I\,~-...:.. Yi,J.i!. JC12~-----:c.i • l...(.!c) Zh 6--e>;1u}1 'KCi.. & /(P, ·.
&. r-r.o I ·Z-1,rs~ ,-;, · ·p -_ · · ".::;; A-Lev...,. ·~ t"'-1 \3 ;)..k. ... ~ . ...::. y_1,,., l~ W --_,_,
-=--____________,,_--+-----=-U-"-".u.'-'--;;; .:...::..1--., __ -1-------'l:.....J-_ l '-:l_ ~~ . .:- \q) -_-_, v-l ?J J... · t, tSb....: ~~ •---
!LP
~~'.:..__~~e'....!'...2...---------J---'O~-'?~________,____,,"-'--'--'--'-----_,____, -~oe;-
--------"'---'~'---b-"---------------'--""------i------------"~~---+---0""'---=5-o_&l_i--=---'-L__._L..J"'-~- _,____~-----""---------------1---'-----'-----
o00 + i~k-~~~~L_L_c__J.......~~
-'--'-_,,_,'--------+---~~-----------l- Df§oii_ .z.h_5-01J1k.4----L-'-,.,k-----,__-----+-'(__.::._Y._ L-----------
,1 '(©-/ \-i>
(..1J.. t> o· 5 > -z. h ~1ti't_t1 W. ~ o•:;-fCf 7...bi so ft-11~1 JS~
0057
GAMMA NOTES
0058
/ GG\
0059
f.'------ ------+-------1--------1----+-----I-----
t::,.----------1---------1
~-- ------~----1--------1-----1---~--
--------.:i-'i; ,§r----
,:it --------.::-f~---t-------+-------i---+------+---------1-----
:z:
l--+--------+-------1---------+------1---------t...-
'ffij
--i----------1-----------+------+-----it---------!--------
--------
--------1-------t------+----i-----------------l------------+-
--------t------------+-------------I----
0060
SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
0061
Eberline Analytical Oak Ridge Laboratory
Analysis Sheet
Work Order ... oac I UUISO I
1 Date Received 3/23/2018
Lab Deadline 4/12/2018
Client Auxier & Associates, Inc.
Project WESTLAKE NCC
Report Level 4
Activity Units pCi
Aliquot Units g
Matrix so
Method EPA 908.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer U-232
Radiometric Sol# U-10a
Tracer Act (dpm/g) 18.21
Carrier
Carrier Cone (mg/ml)
18-03111 UUISO Run 1
Printed: 3/30/2018 4:58 AM Page 1 of 3
! ' !
Internal i Sample i Client I Login I Sample Sample
Fraction Desc [ ID , CPM I Date Aliquot
01 i LCS i LCS I I 03/23/18 00:00 1.0000E+00
02 r MBL r BLANK ---- : 03/23/18 00:00 1.0000E+00
I I --
03 DUP I AC-SED-11 -- _ 63 03/21/1813:20 1.0018E+00
04 DO I AC-SED-11 63 03/21 /18 13:20 1.0080E+00
I
I
I
I I I
i I I
i
I
i
: I I
t------+1
- i I
' I !
I • , I I !
l---~,--~-1 l
i I !
i I ---·-,· -
I
I
i i
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0062
Eberline Analytical Oak Ridge Laboratory Analysis Sheet
Tracer Internal I Sample 1
Fraction I Desc \ Aliquot (g)
01 LCS I i
0.6057
02 MBL I 0.6068
I
03 DUP 0.6077
04 DO 0.6068
I
I
Tracer Total ACT(dpm)
11.0 I
11.0
11.1
11.0
I
I
I Radiometric Tracer {pCi)
l
I
i
I
I
18-03111 UUISO Run 1
Radiometric i Grav Carrier Grav Filter
%Rec I Added (ml) I
Tare (g)
o.ooi I
o.oo[
o.oo[
0.00
'
I I Grav Filter I I Final (g) I
!
i I
I !
I
I
!
I
i ! i I
i I
I
• SAF1 is used for-Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
! I
Grav Filter Grav Net(g) %Rec
I
I
I
Printed: 3/30/2018 4:58 AM Page 2 of 3
Mean SAF SAF %Rec 1· 2·
-
I I
I ii
I I I
I
I I
0063
Eberline Analytical 18-03111 Oak Ridge Laboratory
UUISO Analysis Sheet
Run 1
Internal Sample Rough Prep
I Rough Prep Prep Prep Sep to
Fraction Desc Date By Date By Date/Time i
01 LCS I 03128118 01:s1 I JHARVEY
02 MBL I I 03/28/18 01:57 I JHARVEY
03 DUP I I 03/28/18 07:57 I JHARVEY
04 DO I 03/27/18 06:45 I KSALLINGS I 03/28/18 07:57 I JHARVEY
-
:
I I
i
I I -
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. ~ Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Sep to By
Printed: 3/30/2018 4:58 AM Page 3 of 3
Sep t1 Date/Time
I !
__ I
Sep t1 By
0064
Eberline Analytical Oak Ridge Laboratory
( Lab I Nuclide Fraction
01 U-234
§ 0:::
i 0 0 -r!! U)
~ QI i:: "(
~, 0
"""'"
0 en -::::> ::::>
CJ C
u, Cl) -ca CJ 0 u, u, <(
ca ... • 5!:? >< ::::, <(
02 U-234
03 U-234
04 U-234
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Client
I Activity
Results Error Estimate I MDA Identification Units
I I
LCS pCi/g 6.71E+00 9.02E-01 I 7.09E-02
BLANK pCi/g 1.GGE-02 4.01E-02 8.04E-02
AC-SED-11 pCi/g 6.S0E-01 1.95E-01 1.12E-01
AC-SED-11 pCi/g 9.93E-01 2.42E-01 9.59E-02
I
LCS LCS Known %R
7.27E+00 92.20
Printed: 4/2/2018 8:31 AM Page 1 of 3
LCS RPO
I MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
INV OK
OK
0065
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide
Fraction
01 U-234
§ a::
.g 0 0
-!!! ~ iii C:
c:i:
~I
~
0 en -::, ::,
. CJ C:
tn Cl) ..... . ! CJ 0 tn tn
<3'.: ca ~ Cl)
'>< ::::s
<3'.:
02 U-234
03 U-234
04 U-234
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Sample Sample Radiometric Grav
I Mean
Date Aliquot % Rec %Rec % Rec
03/23/18 00:00 1.00E+00 140.90 0.00 0.00
03/23/18 00:00 1.00E+00 126.70 0.00 0.00
03/21/18 13:20 1.00E+00 116.92 0.00 0.00
03/21/18 13:20 1.01E+00 112.61 0.00 0.00
SAF I
SeptO Date/Time
Printed: 4/2/2018 8:31 AM Page 2 of 3
Sept1 Date/Time
I
0066
Eberline Analytical Oak Ridge Laboratory
<( Lab I Nuclide Fraction
01 U-234
§ a::
~ 0 0
-~ ~ ci.i r:: q:
1: Cl)
:::: 0
""'"
0 tn -::::, ::::,
CJ C:
u, Q) --~ CJ 0 u, u,
<C o6 I,.
Q)
>< ::::s
<C
02 U-234
03 U-234
04 U-234
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Counting
I Halflife Detect Carrier
Count Counts
DatefTime (days) Time
03/30/18 13:04 A_Spec Alpha_003 170.02 5.66 E+02
03/30/18 13:04 A_Spec Alpha_004 170 1.47 E+00
03/30/18 13: 04 A_Spec Alpha_010 170.02 5.28 E+01
03/30/18 13:04 A_Spec Alpha_011 170.02 8.28 E+01
Bkg CPM
5.00 E-03
9.00 E-03
1.90 E-02
1.30 E-02
I
Printed: 4/2/2018 8:31 AM Page 3 of 3
Eff
15.9
18.5
18.4
19.5
0067
Eberline Analytical Oak Ridge Laboratory
,: Lab Nuclide Fraction
01 U-238
C: ~ ll:
.g 0 0
-!!? ~ .; C: "(
~I
~
0 en -::, ::,
0 s:: u, Q) -.!2 0 0 u, u, <(
~ ... Q)
>< ::, <(
02 U-238
03 U-238
04 U-238
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Client Activity Results Error Estimate MDA I
Identification Units I I
LCS pCi/g 7.12E+00 9.46E-01 7.43E-02i
BLANK pCi/g -2.25E-04 2.39E-02 7.10E-02
AC-SED-11 pCi/g 7.25E-01 2.0SE-01 1.07E-01
AC-SED-11 pCi/g 7.SSE-01 2.10E-01 7.52E-02
LCS LCS
I Known %R
7.05E+00 101.10
Printed: 4/2/2018 8:31 AM Page 1 of 3
LCS RPD
I MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
OK OK
OK
0068
Eberline Analytical Oak Ridge Laboratory
( . - Lab Nuclide
Fraction
01 U-238
§ It:
.g 0 u
-!!! ~ iii C: <:(
II
~
0 u, -:::, :::,
(.) C
en Cl) -.! (.)
0 en en <(
~ I.. Cl)
">< :::s <(
02 U-238
03 U-238
04 U-238
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Sample Sample Radiometric
I Grav Mean
Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 140.90 0.00 0.00
03/23/18 00:00 1.00E+00 126.70 0.00 0.00
03/21/18 13:20 1.00E+00 116.92 0.00 0.00
03/21118 13:20 1.01E+00 112.61 0.00 0.00
SAF I
SeptO Date/Time
Printed: 4/2/2018 8:31 AM Page 2 of 3
I Sept1
Date/Time
0069
Eberline Analytical Oak Ridge Laboratory
~ Lab
Nuclide Fraction
01 U-238
C: ::s 0::
i 0 0 ,!!! !g_ ca C: ct
~I
~
0 Cl) -::> ::>
(.) C
(/) Cl) -ns (.)
0 (/) (/) <(
~ a.. -~ >< ::s <(
02 U-238
03 U-238
04 U-238
i Sample Oesc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Counting
I Halflife
Detect Carrier Count I
Counts Date/Time (days) Time I
03/30/18 13:04 A_Spec Alpha_003 170.02 6.04 E+02
03/30/18 13:04 A_Spec Alpha_004 170 -2.00 E-02
03/30/18 13:04 A_Spec Alpha_010 170.02 5.91 E+01
03/30/18 13:04 A_Spec Alpha_011 170.02 6.60 E+01
8kg CPM
6.00 E-03
6.00 E-03
1.70 E-02
6.00 E-03
Printed: 4/2/2018 8:31 AM Page 3 of 3
Eff
15.9
18.5
18.4
19.5
0070
Eberline Analytical Oak Ridge Laboratory
~ '\3
C: ::, a:
~ 0 (.)
.r!,!
~ iii C: q;
:: .!l;! u
"'"""
0 en -:::, :::,
0 s:: u, Cl) .... ca 0 0 u, u, <(
~ .... Cl)
'>< :::, <(
Lab Nuclide
Fraction
01 U-235
02 U-235
03 U-235
04 U-235
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Client
I Activity
Error Estimatel I
Results MDA I Identification Units
LCS pCi/g 4.97E-01 1.78E-01 9.21E-02
BLANK pCi/g -5.02E-03 3.04E-02 9.57E-02
AC-SED-11 pCi/g 1.54E-01 1.0GE-01 1.15E-01
AC-SED-11 pCi/g 8.12E-02 7.21E-02 7.76E-02
LCS I LCS
I Known %R
Printed: 4/2/2018 8:31 AM Page 1 of 3
LCS
I RPD MDA Blank
Flag Flag Flag Flag
OK
OK OK
NA OK
OK
0071
Eberline Analytical Oak Ridge Laboratory
( Lab !
Fraction I Nuclide
01 U-235
§ a:
i 8 -!!? ~ <ii I: q:
C: -~ 0
~
0 u, -=> =>
0 C:
r/) Q) -.! 0 0 r/) r/) <{
06 a.. Q)
">< :::s <{
02 U-235
03 U-235
04 U-235
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Sample Sample Radiometric Grav Mean
Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 140.90 0.00 0.00
03/23/18 00:00 1.00E+00 126.70 0.00 0.00
03/21/18 13:20 1.00E+00 116.92 0.00 0.00
03/21/18 13:20 1.01E+00 112.61 0.00 0.00
I Sep to SAF I Date/Time
Printed: 4/2/2018 8:31 AM Page 2 of 3
I Sept1
Date/Time
0072
Eberline Analytical Oak Ridge Laboratory
( Lab Nuclide Fraction
01 U-235
C: ::i a::
,§ 8 -!!! ~ ;; C: q:
1) 0
""'""
0 en -::::, ::::,
(.) C:
th .s cu (.) 0 th th <(
o6 I.,
Cl)
>< :::s <(
02 U-235
03 U-235
04 U-235
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-UUISO-1
Counting Halflife Detect Carrier
Count Counts
Date/Time (days) Time
03/30/18 13:04 A_Spec Alpha_003 170.02 3.40 E+01
03/30/18 13:04 A_Spec Alpha_004 170 -3.60 E-01
03/30/18 13:04 A_Spec Alpha_010 170.02 1.01 E+01
03/30/18 13:04 A_Spec Alpha_011 170.02 5.49 E+00
8kg CPM
6.00 E-03
8.00 E-03
1.10 E-02
3.00 E-03
Printed: 4/2/2018 8:31 AM Page 3 of 3
Eff
15.9
18.5
18.4
19.5
0073
~ /
4
Count Room Report Client: Auxier Associates, Inc.
Internal Fraction
01
02
03
04
Sample Desc
LCS
MBL
DUP
DO
Client ID
LCS
BLANK
AC-SED-11
AC-SED-11
18-03111-UUISO-1 (pCi/g) in SO Tracer ID: U-1 0a
Printed: 3/30/2018 4:58 AM Page 1 of 1
Sample Date
03/23/18 00:00
Sample Aliquot
Tracer Aliquot (g)
Tracer ACT{dpm)
Radiometric Tracer (pC1J
Radiometric I %Rec I
I
1.0000 o.6057 11.0298 I o.oo
SAF 1·
03/23/18 00:00 1.0000 0.6068 i 11.0498 I 0.00
03/21/1813:20 1.0018 0.6077 I - 11.0662 I 0.00 I
0312111813:20 1.0080 o.6068 I 11.0498 I o.oo
I
SAF 2•
---· .. ~ t ____ I I I I i
!
j_ -~----~-----~--~ __ _j_
- i ' •
I I i ! i
f--------------
---~-·----- --- :
i
--------------·----+------+----------<
0074
Eberline Analytical Oak Ridge Laboratory
LCS & Matrix Spikes
Isotope Sol#
U-234 U-8a
U-238 U-8a
fraction Isotope
01 U-232
02 U-232
03 U-232
04 U-232
Version 2.0 08/99
Activity dpmlg
32.0001
Solution Date
3/28/2018
31.0ooj 3/28/2018
Tracers
Sol# Activity dpm/g
U-10a 18.210
U-10a i 18.210
U-10a i 18.210 I
U-10a 18.210
Approx Addff:ion
0.550
0.550
I Solution Date
3/28/2018
3/28/2018
3/28/2018
3/28/2018
I
Spike and Tracer Worksheet
Analysis Code
UUISO LCS
Volume Used (g)
0.5046
0.5046
Volume Used(g)
0.6057
0.6068
0.6077
0.6068
I I
MS Volume Used (g)
Approx Addition
0.6600
0.6600
0.6600
0.6600
Date
3/28/2018 7:55
LCSD T MSD Volume I
Volume Used(g) Used(g)
Technician
JHARVEY
T LCS MS -
I Known Error Added
I Error
pCi Estimate pCi Estimate
7.27 0.262 o.ooi 0.000 I
7.05 0.254 o.ooi 0.000
Balance Printer Tapes
Tracer
Page 1 of 1 Printed: 3/28/2018 7:57 AM
Technician Initials Witness Initials
-------CCSD MSD
Known I Added I Error \ Error I pCi Estimate pCi I
Estimate
o.oo/ 0.000 0.00; 0.000 I ------
o.ool 0.000 I
0.001 0.000
LCS
Matrix Spike
0075
Lab
Eberline Analytical Oak Ridge Laboratory
Auxier & Associates, Inc.
Fraction Client ID
01 LCS 02 BLANK 03 AC-SED-11 04 AC-SED-11
Comments
Analysis Code
UUISO
Sample Muffle Data Ratio
Type Post/Pre
LCS MBL DUP DO
Techn;ciaoc ~ ~ Gl.J\~;:=:;i
Aliquot Worksheet
Rpt Units Lab Deadline
grams 4/12/2018
Dilution Data Aliquot Data
No of Dils Dil Factor Ratio Aliquot Net Equiv
1.0000E+00 1.0000E+00
1.0000E+00 1.0000E+00
1.0018E+00 1.0018E+0O
1.0080E+00 1.0080E+00
Date: ~(@_;~
Technician
JHARVEY
MS Aliquot Data
Printed: 3/28/2018 7:51 AM Page 1 of 1
H-3 Solids Only Water Actcteu H:nnst--
Aliquot Net Equiv (ml) Aliq
i
0076
Eberline Services - Oak Ridge Prep Logbook Version 2.0 8/1999
Eberline Auxier & Associates, Inc. Fraction Client ID
04 AC-SED-11
Comments
Special Codes
Technician: ¼"27 ,.s·:::::5:
Lab Deadline
4/12/2018
Tare (g) Pan Wt
28.2500
Rough Sample Preparation Log Book
Date Received in Prep Date Sealed
3/26/2018 3/27/2018
Gross (g) Net (g) WetWt. Dry Wt. Wet Wt. I Dry Wt.
1839.8000 1287.5600 , _ 1811.5501- 1259.3100
------
----·- ---------!-----------·----.
---·-· -
----
---------~-------------~----
-----
----
Date Returned
3/28/2018
Percent Liquid r·-· Solid
3o.4s%I 69.52% ___ , !
·----·----•--~-
i
- .. -----~-i--·····---_I•··· I
I
I I I
Printed: 3/27/2018 6:45 AM Page 1 of 1
Technician
KSALLINGS
Gamma Special Dry Wt. LEPS Wt. Info
0.00001 0.0000
.--------
i
-------- ---·- ------·-
I ----
I
'
I
H: Hot, 0: Qrnanic Hazard, e..=_ PCB Haza.-g,~R: Rush,_I:__ Other (see comments)
Date:Analysis: Rough Prep Logbook Analysis: UUISO Page No. 10439
0077
-11Apex-Alpha'" Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803111A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
01 Shelf 2 U iso
Alpha_003
3 System Bkgd 211450
<not performed>
l.000E+000 3/30/2018 3/30/2018
170.0
+/- 0.000E+000 gram 6:48:14 AM 1:04:28 PM
minutes 170.0 minutes
0.0121
Counting Efficiency:
U232 UU-l0A 0.606 mL 0.2241 +/-0.1591 +/-1.4090 +/-
0.0028 on 2/16/2018 0.0804
3:44:29 PM
Chem. Recovery Factor:
Control Certificate Name: NatU U-8A Chem. Recov. of Control: U-238 0.889436 +/- 0.065927
Peak Match Tolerance: 0.150 MeV
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.268 4.720 4. 371 4.139
PEAK AREA REPORT
Net Pk Area
416.98 566.15
33.98 603.98
Pk Area Error%
9.61 8.24
34.21 7.98
Ambient Backgnd
1.02 0.85 1.02 1.02
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
6.8 4.8 3.0
46.1
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.991 0.988 0.999 0.986
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/gram
4.94E+000 +!- 5.25E-001 6.71E+000 +!- 9.02E-001 4.97E-001 +!- l.78E-001 7.12E+000 +/- 9.46E-001
I¼ 1/i(rs
MDA (pCi/gram
7.46E-002 +!-7.09E-002 +!-9.21E-002 +!-7.43E-002 +/-
7.93E-003 7.53E-003 9.78E-003 7.89E-003
0078
60
55
50
45
40
35 V> -I-' C: :::s 8 30
25
20
15
10
5
0 r Ill I I rn IIIIIA Alll!IWl!IIOONVIW\ Ii · , ,1 Ah, ;, du ' · \ MIMI/II I 3500
1 111' \
4000 4500
ROI Type: 1
0000209976.CNF
I ,I I A 1 [PHI II 11111\IYI jl 1 1
5000 Energy(kev)
IM A I IA
5500
Live Time :10201.000 sec Rea 1 Ti me : 10201. 000 sec Start: 1:3496.G(kev) Stop : 1024:6544.G(kev) Acq. start :Fri Mar 30 13:04:28 2018
1 1 Al ! A 1 I I A I I
6000
ROI Type: 3
A I I I
6500
0079
Channel Data Report 3/30/2018 3:59:09 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10201 Elapsed Real Time: 10201
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 10201 10201 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 1 0 0 0 0 0 1 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 1
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 1 0 0 0
65: 0 0 1 0 0 0 0 0
73: 1 0 1 0 0 0 1 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 1 1 0 0 1
97: 2 1 1 0 0 0 0 0
105: 0 1 0 0 0 0 0 0
113: 0 0 0 0 1 0 0 2
121: 0 0 0 2 0 1 0 0
129: 0 1 1 0 1 0 2 0
137: 0 0 1 0 0 0 2 0
145: 0 2 0 1 0 0 1 0
153: 2 1 1 0 1 1 1 0
161: 4 1 2 0 1 0 1 2
169: 1 2 1 1 4 2 2 1
177: 5 2 1 6 3 3 4 2
185: 2 4 5 3 6 5 4 3
193: 6 1 3 3 3 4 7 6
201: 2 6 8 12 7 11 12 7
209: 1 4 10 9 13 13 13 11
217: 16 14 9 19 14 19 16 17
225: 16 16 21 14 17 18 23 15
233: 14 18 9 17 11 9 5 7
241: 0 2 0 2 0 0 0 0
249: 0 0 0 1 0 0 0 0
257: 0 0 1 1 0 0 0 0
265: 1 0 0 0 1 0 0 0
273: 1 1 2 0 1 0 0 1
281: 1 1 1 1 2 1 0 1
289: 1 0 0 0 2 1 0 3
297: 0 0 1 1 2 2 0 0
305: 1 0 1 0 1 1 1 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 1 0 0 1 1
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 1 0 0
345: 1 0 0 0 1 2 1 0
353: 1 0 1 0 2 1 0 0
361: 1 2 1 0 0 1 5 1
0080
Channel Data Report 3/30/2018 3:59:09 PM Page 2
369: 1 1 2 1 1 1 2 3
Sample Title: 01
Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 3 4 3 4 1 2 1 3
385: 3 7 5 3 5 11 6 3
393: 10 5 6 4 13 6 4 10
401: 6 9 14 6 8 14 10 8
409: 15 9 9 14 11 13 19 10
417: 24 8 13 17 15 21 17 22
425: 18 21 17 14 12 13 12 7
433: 5 1 3 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 1 0 0 0
489: 0 0 0 0 0 0 0 0
497: 1 0 0 0 0 0 0 0
505: 0 0 0 1 0 0 0 0
513: 1 0 1 0 1 1 1 0
521: 0 0 0 0 0 0 1 2
529: 1 0 0 0 0 0 0 2
537: 0 0 0 1 2 0 1 1
545: 0 0 2 1 0 1 2 1
553: 2 1 0 1 2 4 2 1
561: 0 1 3 5 1 0 2 1
569: 2 4 2 6 7 3 3 4
577: 5 3 3 6 4 5 6 9
585: 5 4 5 5 6 13 7 10
593: 15 16 10 9 6 12 8 9
601: 9 12 9 15 12 15 14 16
609: 5 18 12 7 14 6 5 8
617: 1 4 0 1 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 1 0 1 0 0 0 0
649: 0 0 0 0 0 1 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 1 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 1 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 1 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 1 0 0 0 0 0 0 0
793: 0 0 0 1 0 0 0 0
0081
Channel Data Report 3/30/2018 3:59:09 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 1
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 1 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0082
_,A Al h TM ~/-\pex- p a Sample Description: Spectrum File: Batch Identification:
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803111A-UU Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
02 Shelf 2 U iso
Alpha_004
4 System Bkgd 211451
<not performed>
l.000E+000 3/30/2018 3/30/2018
+/- 0.000E+000 gram 6:48:14 AM 1:04:29 PM
170.0 minutes 170.0 minutes
U232 UU-l0A 0.607 mL 0.2347 +/- 0.0125
Counting Efficiency: 0.1853 +/- 0.0032 on 2/16/2018 1.2670 +/- 0.0708
3:44:30 PM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.270 4.680 4.487 4.161
0.150 MeV
PEAK AREA REPORT
Net Pk Area
437.49 1. 47
-0.36 -0.02
Pk Area Error%
9.38 240.74 604.15 10624.
Ambient Backgnd
0.51 1. 53 1. 36 1. 02
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
27.9 2.9 2.9 2.9
T = Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Con£.
0.992 0.954 0.930 0. 996
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/gram
4.95E+000 +/- 5.15E-001 1. 66E-002 +/- 4.0lE-002
-5.02E-003 +/- 3.04E-002 -2.25E-004 +/- 2.39E-002
A~ 1(:2((¼
MDA (pCi/gram
5.94E-002 +/-8.04E-002 +!-9.57E-002 +!-7.l0E-002 +/-
6.18E-003 8.37E-003 9.96E-003 7.38E-003
0083
60
55
50
45
40
35 Vl -I-' C: :::s 8 30
25
20
15
10
5 ~
0000209977.CNF
~ = ~ ' ::,
Live Time :10200.000 sec Real Time :10200.000 sec Start: 1:3488.l(kev) Stop : 1024:6492.S(kev) Acq. Start :Fri Mar 30 13:04:29 2018
0 F 1 1 1 11 'J: I I I i I !1
3500
1 1 i !I\ 'I l. . c ; 1 ! ! ! ! I U [ti ii 1 11
4000 4500 5000 Energy(kev)
I I I ! I I ! 1 I I I I I I I I 5500 6000 6500
ROI Type: 1 ROI Type: 3
0084
Channel Data Report 3/30/2018 3:59:17 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channell------l-------l-------1-------1-------1-------I-------I-------I 1: 10200 10200 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 1 0 0
129: 0 0 1 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 1 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 1 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 1 0 0 0
345: 0 0 0 0 0 1 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0085
Channel Data Report 3/30/2018 3:59:17 PM Page 2
369: 0 0 0 1 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 0 0 0 0 0 0 1 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 0 0 0 0 0
401: 0 0 0 0 0 0 0 1
409: 0 0 0 0 0 0 0 0
417: 0 0 0 0 0 0 0 0
425: 0 0 0 0 0 1 0 0
433: 0 0 0 0 0 0 0 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 0 0 0 0
457: 0 0 0 0 0 1 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 1 0 0 0
481: 0 0 0 0 0 0 0 0
489: 0 1 0 0 0 0 0 0
497: 0 0 0 0 0 0 0 0
505: 1 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 0 0 0 0 0 0 0 0
529: 1 0 0 0 0 0 0 1
537: 0 0 0 0 0 0 1 1
545: 1 0 1 0 0 0 0 3
553: 1 1 2 1 1 2 2 0 561: 1 0 0 1 2 1 2 1
569: 3 0 0 2 3 2 3 2 577: 4 0 1 1 1 2 1 2
585: 2 5 3 3 4 5 7 5 593: 6 6 5 9 7 7 12 7
601: 13 7 7 9 10 13 9 13 609: 13 12 10 8 7 11 13 15 617: 16 12 12 10 15 18 9 16 625: 15 7 7 5 1 0 1 0 633: 0 0 0 0 0 0 0 0 641: 0 0 0 0 0 0 0 0 649: 0 0 0 0 0 0 0 0 657: 0 0 0 0 0 1 0 0 665: 0 0 0 0 0 0 0 0 673: 0 0 0 0 0 0 0 0 681: 0 0 0 0 0 0 0 0 689: 0 0 0 0 0 0 0 0 697: 0 0 0 0 0 0 0 0 705: 0 0 0 0 0 0 0 0 713: 0 0 0 0 0 0 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 1 0 0 0 0 0 753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 0 769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 0 0 0 0 0 793: 0 0 0 0 0 0 0 0
0086
Channel Data Report 3/30/2018 3:59:17 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0087
~-~~pex-Alpha,. Sample Description: Spectrum File: Batch Identification:
AC-SED-11 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099 1803111A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
03 Shelf 2 U iso
Alpha_0l0
10 System Bkgd 211452
<not performed>
l.002E+000 +!- 0.000E+000 3/21/2018 6:48:14 3/30/2018 1:04:26
170.0 minutes 170.0 minutes
U232 UU-l0A 0.608 rnL 0.2152 +/- 0.0119
AM PM
gram
Counting Efficiency: Chern. Recovery Factor:
0.1841 +/- 0.0032 on 2/16/2018 1.1692 +/- 0.0675
3:44:30 PM
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.281 4.722 4.379 4.147
0.150 MeV
PEAK AREA REPORT
Net Pk Area
401.79 52.77 10.13 59.11
Pk Area Error%
9.81 27.93 67.91 26.21
Ambient Backgnd
2.21 3.23 1. 87 2.89
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
8.6 4.9 2.9 4.9
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0.997 0.989 1.000 0.990
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761.50* 4385.50* 4184.40*
Activity (pCi/grarn
4.95E+000 +!- 5.34E-001 6.50E-001 +/- l.95E-001 l.54E-001 +!- 1. 06E-001 7.25E-001 +!- 2.05E-001
Ni, lf/JftS
MDA (pCi/grarn
9.85E-002 +/-l.12E-001 +!-l.15E-001 +!-1. 07E- 001 +/-
l.06E-002 l.21E-002 l.24E-002 1.16E-002
0088
60
55
50
45
40
35 V> -I-' C: :::l
8 30
25
20
15
10
5
0000209978.CNF
Live Time 10201.000 sec Rea 1 Ti me 10202. 000 sec Start: 1 3509.l(keV) stop : 1024 6494.S(kev) Acq. Start Fri Mar 30 13:04:26 2018
\1
0 II I !Mlfl ! Im I! Mq ,'\!!,rf.';i,i\'li!i llH'S,1,', ,\[ HH1 i'itfllpfi'!!l\il~A IMl\!11![! ! l~!IW!li:' 11 It!! I I I !I I [! I I ! I I '
4000
ROI Type: 1
4500 5000 Energy(kev)
5500 6000 6500
ROI Type: 3
0089
Channel Data Report 3/30/2018 3:59:24 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10201 Elapsed Real Time: 10202
Channell------l-------1-------1-------1-------I-------I-------I-------I 1: 10202 10201 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 1 0
49: 0 0 0 0 0 0 0 1
57: 0 1 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 1 1 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 1 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 1 0 0 0 0 0
113: 0 1 0 0 0 1 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 1 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 1 0 0 1 0 0 0 0
161: 1 0 0 0 0 0 0 0
169: 0 1 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 0 0 0 0 0 1 0 0
193: 1 0 1 0 0 2 1 1
201: 0 0 2 0 3 0 0 1
209: 2 1 0 1 1 3 1 1
217: 1 0 2 4 1 0 1 2
225: 0 3 4 2 0 1 3 1
233: 1 1 1 2 0 4 1 0
241: 0 0 2 0 1 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 1 0
281: 0 0 1 0 0 0 0 0 289: 0 1 0 0 0 2 0 0
297: 1 0 2 0 1 0 0 0
305: 0 1 0 0 0 0 0 0
313: 0 0 1 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 1 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 1 361: 0 0 0 0 0 1 0 1
0090
Channel Data Report 3/30/2018 3:59:24 PM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 1 1 1 0 1 0 0 0
385: 0 0 0 0 0 0 0 0
393: 0 0 0 1 0 0 0 0
401: 0 2 1 0 2 4 1 2
409: 0 1 3 2 0 2 0 4
417: 0 1 0 4 1 2 0 3
425: 2 0 1 2 0 0 0 2
433: 0 2 1 2 1 0 1 0
441: 0 0 0 0 0 0 0 0
449: 0 0 0 0 1 0 0 0
457: 1 0 0 0 0 0 0 0
465: 0 0 0 0 0 0 0 0
473: 0 0 0 0 0 0 0 1
481: 0 0 1 0 0 0 0 0
489: 0 0 1 1 0 0 0 0
497: 0 1 0 0 0 0 0 2
505: 0 0 1 0 0 0 0 0
513: 0 1 0 0 0 0 0 0
521: 0 0 0 0 0 1 0 0
529: 0 0 0 0 0 0 0 0
537: 2 1 0 1 0 0 0 1
545: 0 0 0 0 1 0 0 0
553: 1 0 3 3 0 0 1 0
561: 0 0 1 2 1 2 1 0
569: 0 1 1 1 2 1 4 0
577: 0 5 1 2 3 1 1 2
585: 4 5 3 3 3 4 4 5
593: 5 2 7 4 4 6 7 4
601: 13 5 5 9 4 11 10 11
609: 11 13 13 8 13 6 21 16
617: 11 9 13 16 15 10 12 9
625: 9 11 8 3 2 0 1 2
633: 1 1 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 1 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 1 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0091
Channel Data Report 3/30/2018 3:59:24 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 1 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 0 0 0 1 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0092
~-~~Apex-Alpha™ Sample Description: Spectrum File: Batch Identification:
AC-SED-11 \\OR-ALPHAl\Canberra\Apex.Alpha\Root\Data\00002099
1803111A-UU
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
04 Shelf 2 U iso
Alpha_0ll
11 System Bkgd 211453
<not performed>
l.008E+000 3/21/2018 3/30/2018
+/- 0.000E+000 gram 6:48:14 AM 1:04:27 PM
170.0 minutes 170.0 minutes
U232 UU-l0A 0.607 mL 0.2196 +/- 0.0120
Counting Efficiency: 0.1950 +/- 0.0034 on 2/16/2018 1.1261 +/- 0.0646
3:44:30 PM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
U-232 T U-234 U-235 U-238
Energy (MeV)
5.279 4.729 4.422 4.153
0.150 MeV
PEAK AREA REPORT
Net Pk Area
409.28 82.79
5 .49 65.98
Pk Area Error%
9.73 21.87 88.08 24.35
Ambient Backgnd
2.72 2.21 0.51 1. 02
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
8.8 7.4 2.6 3.5
T Tracer Peak used for Effective Efficiency
Nuclide
U-232 U-234 U-235 U-238
Id Conf.
0. 996 0.993 0.990 0.993
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5302.50* 4761. 50* 4385.50* 4184.40*
Activity (pCi/gram
4.91E+000 +/- 5.26E-001 9.93E-001 +!- 2.42E-001 8.12E-002 +/- 7.21E-002 7.88E-001 +!- 2.l0E-001
~IK
MDA (pCi/gram
l.03E-001 +/-9.59E-002 +/-7.76E-002 +/-7.52E-002 +/-
l.l0E-002 l.03E-002 8.33E-003 8.07E-003
0093
V) ....,
60
55
50
45
40
35
C: ::::s 8 30
25
20
15
10
5
0000209979.CNF
Live Time :10201.000 sec Real Ti me : 10201. 000 sec Start: 1:3638.?(kev) Stop : 1024: 6325. 9(keV) Acq. Start :Fri Mar 30 13:04:27 2018
0 II I I A! ! n A 11!,\ ,\!U ii,j/i!/,/!jli l!Ji ,I //1 f \; I Ill ,r,n,u,,,1 ll 11 " M! 111 ! ~ A NIWl)lrn1,, ,I, I! A 'A IA I A I Ai I
4000
ROI Type: 1
4500 5000 Energy(kev)
5500 6000
ROI Type: 3
0094
Channel Data Report 3/30/2018 3:59:31 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10201 Elapsed Real Time: 10201
Channell------l-------l-------l-------1-------1-------1-------I-------I 1: 10201 10201 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 1
73: 0 0 0 0 0 1 0 0
81: 0 0 0 0 0 0 0 0
89: 0 1 0 0 0 0 0 0
97: 0 0 0 0 0 1 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 1 0 0 0
129: 0 0 0 0 0 0 1 0
137: 0 0 0 0 1 0 1 0
145: 0 0 0 0 0 0 1 0
153: 0 0 1 0 1 0 0 0
161: 0 1 0 0 0 0 0 0
169: 1 1 1 0 0 0 0 1
177: 2 0 1 1 1 0 0 0
185: 2 0 1 0 0 0 1 0
193: 0 3 1 4 1 0 2 0
201: 2 2 0 1 2 3 1 2
209: 2 4 2 2 2 4 4 0
217: 2 0 1 1 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 1 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 1 0 1
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 1 0 0
313: 0 0 0 0 0 0 1 0
321: 0 0 1 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 1 1 0 0 0 0 0 0
0095
Channel Data Report 3/30/2018 3:59:31 PM Page 2
369: 0 0 0 0 0 0 1 1
Sample Title: 04
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 0 1 0 1 1 1 0 0
385: 1 1 0 0 1 1 1 0
393: 1 0 1 1 0 0 1 3
401: 0 0 2 0 0 2 2 0
409: 0 3 3 4 0 1 3 3
417: 3 0 1 1 1 1 3 3
425: 2 1 1 1 3 2 1 2
433: 4 2 1 1 3 1 3 0
441: 1 1 0 0 0 0 0 0
449: 0 0 0 0 0 0 1 0
457: 0 0 0 0 0 0 0 0
465: 0 1 0 1 0 0 0 1
473: 0 0 0 0 0 0 0 0
481: 0 0 0 0 0 0 0 0
489: 1 1 0 0 0 0 0 0
497: 1 0 0 0 0 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 0 0 0 0 0 0 0
521: 1 0 0 0 0 0 0 0
529: 0 0 0 1 0 0 0 0
537: 0 0 0 0 0 0 1 0
545: 0 2 0 0 1 0 0 0
553: 0 2 0 0 0 1 0 0
561: 2 0 0 1 2 0 1 1
569: 1 1 1 0 0 1 0 0
577: 2 0 1 2 2 1 0 0
585: 0 0 0 2 2 1 3 2
593: 0 3 2 1 1 3 4 3
601: 5 0 3 5 1 5 9 10
609: 9 3 2 2 2 3 5 8
617: 3 8 11 4 10 7 5 8
625: 6 8 11 13 13 13 12 13 633: 11 10 12 4 10 16 13 8
641: 7 14 16 12 10 7 6 3
649: 1 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 1 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0 697: 1 0 0 0 0 0 0 0 705: 0 0 0 0 0 0 1 0 713: 0 0 0 0 0 1 0 0 721: 0 0 0 0 0 0 0 0 729: 0 0 0 0 0 0 0 0 737: 0 0 0 0 0 0 0 0 745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0 761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0 777: 0 0 0 0 0 0 0 0 785: 0 0 0 1 0 0 0 0 793: 0 0 0 0 0 0 0 0
0096
Channel Data Report 3/30/2018 3:59:31 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------l-------l-------l-------1-------1-------1-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 1 0 0 0 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 1 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0097
r-age I OT L
~Apex-AlphaT] 0-A .C,tlAI/AlARY REPORT
Review Of QA Results - Pulser Check
Date : 3/30/2018 Time : 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG
Alpha 001 2lf ALL Not Done
Alpha 002 2lf ALL Not Done
Alpha 003 2lf ALL Passed
Alpha 004 2lf ALL Passed
Alpha 005 21f ALL Not Done
Alpha 006 21f ALL Not Done
Alpha 007 21f ALL Not Done
Alpha 008 2lf ALL Not Done
Alpha 009 2lf ALL Not Done
Alpha 010 2lf ALL Passed
Alpha 011 2lf ALL Passed
Alpha 012 21f ALL Passed
Alpha 013 21f ALL Not Done
Alpha 014 2lf ALL Passed
Alpha 015 2lf ALL Not Done
Alpha 016 2lf ALL Not Done
Alpha 033 Alpha Analystl00DC ALL Passed
Alpha 034 Alpha Analvstl00DC ALL Passed
Alpha 035 Alpha Analystl 00DC ALL Passed
Alpha 036 Alpha Analystl 00DC ALL Passed
Alpha 037 Alpha Analystl 00DC ALL Not Done
Alpha 038 Alpha AnalystlO0DC ALL Passed
Alpha 039 Alpha Analystl00DC ALL Not Done
Alpha 040 Alpha Analystl00DC ALL Passed
Alpha 041 Alpha AnalystlO0DC ALL Passed
Alpha 042 Alpha Analystl00DC ALL Passed
Alpha 043 Alpha Analystl00DC ALL Passed
Alpha 044 Alpha Analystl00DC ALL Passed
Alpha 045 Alpha Analystl00DC ALL Passed
Alpha 046 Alpha Analystl00DC ALL Passed
Alpha 047 Alpha Analvstl00DC ALL Not Done
Alpha 048 Alpha Analystl00DC ALL Not Done
Alpha 049 Alpha Analystl00DC ALL Passed
Alpha 050 Alpha Analystl 00DC ALL Passed
Alpha 051 Alpha Analystl00DC ALL Passed
Alpha 052 Alpha Analvstl 00DC ALL Passed
Alpha 053 Alpha Analyst 1 00DC ALL Passed
Alpha 054 Alpha Analystl00DC ALL Passed
Alpha 055 Alpha Analystl00DC ALL Passed
Alpha 056 Alpha Analystl 00DC ALL Passed
Alpha 057 Alpha Arialystl00DC ALL Passed
Alpha 058 Alpha Analystl00DC ALL Passed
3/30/2018 5:55:22 AM
DATE
3/30/2018 5:03:13 AM 3/30/2018 5:03:14 AM
3/30/2018 5:03:15 AM 3/30/2018 5:03:16 AM 3/30/2018 5:03:17 AM
3/30/2018 5:03:18 AM
3/30/2018 5:03:19 AM 3/30/2018 5:03:21 AM 3/30/2018 5:03:22 AM 3/30/2018 5:03:24 AM
3/30/2018 5:03:26 AM
3/30/2018 5:03:28 AM 3/30/2018 5:03:30 AM 3/30/2018 5:03:32 AM 3/30/2018 5:03:34 AM 3/30/2018 5:03:37 AM 3/30/2018 5:03:39 AM 3/30/2018 5:03:42 AM
3/30/2018 5:03:44 AM 3/30/2018 5:03:47 AM 3/30/2018 5:03:49 AM 3/30/2018 5:03:52 AM 3/30/2018 5:03:54 AM 3/30/2018 5:03:57 AM 3/30/2018 5:03:59 AM 3/30/2018 5:04:02 AM
3/30/2018 5:04:05 AM 3/30/2018 5:04:08 AM
0098
Page 2 of 2 Kev1ew ot UA Kesults - t-'u1ser 1.,;necK 3/30/2018 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 059 Alpha Analvstl00DC ALL Not Done
Alpha 060 Alpha Analyst 1 00DC ALL Not Done
APPROVED BY:
APPROVAL DATE:,~ /3()// 7)
0099
Library Listing Report 6/12/12 12:17:04 PM Page 1
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Uranium
Nuclide Library Description: U-232,-234,-235,-238
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV (%) Uncert. (Abs.+-)
U-232 2.174E+009 5302.500* 0,000 99.8000 0.0000
U-234 7.731E+012 4761.500* 0.000 99.8000 0.0000
U-235 2.221E+016 4385.500* 0.000 80.9000 0.0000
U-238 1.410E+017 4184.400* 0.000 100.2300 0.0000
* = key line
TOTALS: 4 Nuclides 4 Energy Lines
0100
SECTION IX
ANALYTICAL DAT A (ISOTOPIC THORIUM)
0101
Eberline Analytical Oak Ridge Laboratory
Analysis Sheet
Work Order
Analysis Code
Run
18-03111 rhlso~·=7
1
Internal i Sample
Fraction Desc
01 LCS
02 MBL I
18-03111 ThlSO Run 1
Client ID
LCS
BLANK I 1
Login CPM
Printed: 3130/2018 4:59 AM Page 1 of 3
Sample Date
03/23/18 00:00
03/23/18 00:00
Sample Aliquot
1.0000E+00
1.0000E+00
Date Received 3/23/2018 03 DUP [ AC-SED-11 63 03/21/1813:20 9.9780E-01
Lab Deadline 4/12/2018 04 DO I AC-SED-11 63 03/21/18 13:20 1.0036E+00
l ! Client Auxier & Associates, Inc.
Project WESTLAKE NCC
Report Level 4
Activity Units pCi
Aliquot Units g
Matrix so
Method EPA 907.0 Modified
Instrument Type Alpha Spectroscopy
Radiometric Tracer Th-229
Radiometric Sol# Th-18a
Tracer Act (dpm/g) 22.46 I
Carrier
Carrier Cone (mg/ml)
i
i
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0102
Eberline Analytical
Oak Ridge Laboratory Analysis Sheet
I
Internal [ Sample Tracer
Fraction i Desc Aliquot(g) I
I 01 LCS 0.4656 I I
02 I
MBL 0.2324 I
03 DUP 0.2329
04 DO 0.2336
I
~
--
----
-----
Tracer Total Radiometric
ACT(dpm) Tracer (pCi)
10.5
5.2
5.2
5.2
18-03111 ThlSO Run 1
I Radiometric/ Grav-Carrier I Grav Filter
[ % Rec [ Added (ml) Tare (g)
I
0.001
o.oo[ I
!
I
I 0.00
0.00
I
I
Grav Filter Final (g)
I I I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
I i
i
Grav Filter Grav Net (g) %Rec
I i
i I
I
I i
I ! i
I
I
I I I
I
I I !
!
I ! I
I
I
Printed: 313012018 4:59 AM Page 2 of 3
I I Mean SAF SAF %Rec 1· 2·
I
-
0103
Eberline Analytical
Oak Ridge Laboratory
Analysis Sheet
Internal I Sample Fraction Desc
01 LCS
02 MBL
03 DUP
04 DO
I Rough Prep
Date i
03/27 /18 06:45
I
Rough Prep Prep I
By Date I I
03/28/18 07:55
03/28/18 07:55
03/28/18 07:55
KSALLINGS 03/28/18 07:55
I
!
I
i
18-03111 ThlSO Run 1
Prep By
JHARVEY
JHARVEY
JHARVEY
JHARVEY
I Sep to
Date/Time I
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
! Sep to
I By
I I !
---
I
I
l I
I
I I I
!
i ~--· ! I I I
Printed: 3/30/2018 4:59 AM Page 3 of 3
Sep t1 Sep t1 Date/Time By
I
0104
Eberline Analytical Oak Ridge Laboratory
~ Lab I Nuclide
Fraction
01 TH-228
&
~ 0 0 -!!! ~ iii i::: q:
~I
"""""
0 en -.c I-
(J C:
u, Cl) -ca (J 0 u, u, <(
ca ... Cl)
·;;: :::::s <(
02 TH-228
03 TH-228
04 TH-228
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Client
I Activity
Results Error Estimate MDA I
Identification Units I
LCS pCi/g 6.24E+00 9.71E-01 8.S0E-02
BLANK pCi/g -7.30E-02 5.48E-02 1.99E-01
AC-SED-11 pCi/g 1.0SE+00 3.17E-01 1.19E-01
AC-SED-11 pCi/g 7.91E-01 2.95E-01 1.34E-01
'
LCS LCS
Known %R
5.11E+00 122.00
Printed: 3/30/2018 1 :59 PM Page 1 of 3
LCS I RPD MDA Blank
Flag I Flag Flag Flag
OK OK
OK OK
INV OK
OK
0105
Eberline Analytical Oak Ridge Laboratory
( Lab Fraction
Nuclide
01 TH-228
C: ::, 0::
.g 0 (.)
,!!! ~ cii C: <t
~I
""""
0 en -.c I-
(.) C:
u, Cl) -ca (.) 0 u, u,
<C otS ...
Cl) ·;;: :::, <C
02 TH-228
03 TH-228
04 TH-228
I Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Sample Sample
I Radiometric Grav Mean I
Date Aliquot %Rec %Rec %Rec I 03/23/18 00:00 1.00E+00 100.47 0.00 0.00
03/23/18 00:00 1.00E+00 71.21 0.00 0.00
03/21/18 13:20 9.98E-01 92.52 0.00 0.00
03/21/18 13:20 1.00E+00 83.60 0.00 0.00
SAF I
SeptO
Printed: 3/30/2018 1 :59 PM Page 2 of 3
Sept1
Date/Time I Date/Time
0106
Eberline Analytical Oak Ridge Laboratory
<( Lab Nuclide
Fraction
01 TH-228
C: ::s 0::
{l 0 u .!!,!
~ cu C: ct
C: ,!!! u
~
0 Cl) -.c I-
CJ C
(/) Q) -ns CJ 0 (/) (/) <(
~ a.. Q)
>< :::s <(
02 TH-228
03 TH-228
04 TH-228
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Counting Halflife
I Count
Detect Carrier Counts DatefTime (days) Time
03/30/18 08:11 A_Spec Alpha_044 170 4.35 E+02
03/30/18 08:11 A_Spec Alpha_045 170 -3.40 E+00
03/30/18 08:11 A_Spec Alpha_046 170 6.43 E+01
03/30/18 10:29 A_Spec Alpha_049 170 3.88 E+01
Bkg I I
CPM I
0.00 E+00 I
2.00 E-02
1.00 E-02
7.00 E-03
Printed: 3/30/2018 1 :59 PM Page 3 of 3
Eff
18.4
17.4
17.8
15.6
0107
Eberline Analytical Oak Ridge Laboratory
<\ Lab I Nuclide Fraction I
01 TH-230
§ n:
.g 0 u .!!! ~ iii c::: q:
c:: ~
T"""
0 en -.J:: I-
(.) C: -u, Q) -ca (.) 0 u, u, <(
c6 ... Q)
>< ::::, <(
02 TH-230
03 TH-230
04 TH-230
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
I
Client Activity Results Error Estimate MDA I Identification Units
LCS pCi/g 6.57E+00 1.01E+00 8.10E-02
BLANK pCi/g 4.58E-02 8.S0E-02 1.63E-01
AC-SED-11 pCi/g 1.17E+00 3.38E-01 8.46E-02
AC-SED-11 pCi/g 1.34E+00 4.14E-01 1.0GE-01
I I LCS LCS
Known %R I
5.39E+00 121.89
Printed: 3/30/2018 1 :59 PM Page 1 of 3
I LCS RPD MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
OK OK
OK
0108
Eberline Analytical
Oak Ridge Laboratory
( Lab
Nuclide Fraction
01 TH-230
C: :, a::
~ 0 (.)
.!(!
~ ;; C: <t
~I
~
0 u, -.c I-
0 r:: -u, .s ca 0 0 u, u, <(
~ ... Cl) ·;: ::s <(
02 TH-230
03 TH-230
04 TH-230
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Sample Sample
I Radiometric Grav Mean
I Date Aliquot %Rec %Rec %Rec
03/23/18 00:00 1.00E+00 100.47 0.00 0.00
03/23/18 00:00 1.00E+00 71.21 0.00 0.00
03/21/18 13:20 9.98E-01 92.52 0.00 0.00
03/21/18 13:20 1.00E+00 83.60 0.00 0.00
SAF SeptO
Printed: 3/30/2018 1 :59 PM Page 2 of 3
I Sep t1
Date/Time I Date/Time
0109
Eberline Analytical Oak Ridge Laboratory
<( Lab Nuclide
Fraction
01 TH-230
&
.g 0 (.)
-!!! ~ cii c:: q:
~I
~
0 en -..c I-
(.) C:
ti)
.s ca (.)
0 ti) ti) <(
~ ,_ Q)
'>< :::::s <(
02 TH-230
03 TH-230
04 TH-230
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Counting Halflife Carrier I
Count Counts
Date/Time (days) Detect Time
03/30/18 08:11 A_Spec Alpha_044 170 4.57 E+02
03/30/18 08:11 A_Spec Alpha_045 170 2.13 E+00
03/30/18 08:11 A_Spec Alpha_046 170 7.25 E+01
03/30/18 10:29 A_Spec Alpha_049 170 6.65 E+01
! 8kg
I CPM
4.00 E-03
1.10 E-02
3.00 E-03
3.00 E-03
Printed: 3/30/2018 1 :59 PM Page 3 of 3
Eff
18.4
17.4
17.8
15.6
0110
Eberline Analytical Oak Ridge Laboratory
;: Lab Nuclide
Fraction
01 TH-232
§ a::
.g 0 0 ,!!! ~ cii C: "(
II
""'"
0 Cl) -.c I-
. (.) C -th Q) -cu (.) 0 th th <(
~ lo. Q)
'>< ~ <(
02 TH-232
03 TH-232
04 TH-232
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Client Activity Results Error Estimate MDA I Identification Units
LCS pCi/g 6.26E+00 9.74E-01 5.98E-02
BLANK pCi/g -1.S0E-02 4.78E-02 1.58E-01,
AC-SED-11 pCi/g 8.29E-01 2.72E-01 1.14E-01
AC-SED-11 pCi/g 1.12E+00 3.66E-01 9.65E-02
LC$
I LC$
Known %R
5.11E+00 122.44
Printed: 3/30/2018 1 :59 PM Page 1 of 3
LC$
I RPD
I MDA Blank
Flag Flag Flag Flag
OK OK
OK OK
INV OK
OK
0111
Eberline Analytical Oak Ridge Laboratory
~ Lab I Nuclide
Fraction
01 TH-232
c:: :, a:
i 0 0 -!!! ~ iij c:: "(
~I
~
0 u, -.c I-
(.) C:
ti) Cl) -.! (.)
0 ti) ti) <(
oa a.. -~ >< ::::::s <(
02 TH-232
03 TH-232
04 TH-232
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Sample Sample Radiometric Grav Mean I Date Aliquot %Rec %Rec %Rec
I
03/23/18 00:00 1.00E+00 100.47 0.00 0.00
03/23/18 00:00 1.00E+00 71.21 0.00 0.00
03/21 /18 13:20 9.98E-01 92.52 0.00 0.00
03/21 /18 13:20 1.00E+00 83.60 0.00 0.00
SAF I I
SeptO
Printed: 3/30/2018 1 :59 PM Page 2 of 3
Sept1
DatefTime DatefTime
0112
Eberline Analytical Oak Ridge Laboratory
( Lab I Nuclide Fraction
01 TH-232
~
.g 0 0 .!/? ~ cii C: q;
~I
~
0 en -.c I-
(.) C:
u, a, -ns (.)
0 u, u, <(
ca 11,,, a, ·;: ::, <(
02 TH-232
03 TH-232
04 TH-232
Sample Desc
LCS
MBL
DUP
DO
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-ThlSO-1
Counting Halflife Detect Carrier Count I Counts DatefTime (days) Time
03/30/18 08:11 A_Spec Alpha_044 170 4.37 E+02
03/30/18 08:11 A_Spec Alpha_045 170 -7.00 E-01
03/30/18 08:11 A_Spec Alpha_046 170 5.15 E+01
03/30/18 10:29 A_Spec Alpha_049 170 5.57 E+01
Bkg CPM
1.00 E-03
1.00 E-02
9.00 E-03
2.00 E-03
I
I
Printed: 3/30/2018 1 :59 PM Page 3 of 3
Eff
18.4
17.4
17.8
15.6
0113
Count Room Report Client: Auxier Associates, Inc.
Internal Fraction
01
I Sample I I Desc j
LCS
Client ID
LCS
18-03111-ThlSO-1 (pCi/g) in SO Tracer ID: Th-18a
Sample Date
Sample Aliquot
Tracer Aliquot (g)
Tracer ACT(dpm)
03/23/18 00:00 1.0000 I 0.4656 10.4574
Radiometric Tracer (pCi)
Printed: 3/30/2018 4:59 AM Page 1 of 1
ii Radiometric ¾Rec
0.00
SAF ! 1*
SAF 2*
\D f 02 MBL BLANK 03/23/18 00:00 1.0000 0.2324 5.2197 0.00
\),.. I
- i
~ 03 DUP AC-SED-11 03/21/18 13:20 ' 0.9978 0.2329 5.2309 0.00 I I _._
i I __J
, 04 DO AC-SED-11 03/21/1813:20 1.0036 0.2336 5.2467 I 0.00 /
,~ . . , 1 l : ~- l i I
. I I I I
,-.-------,.-----+--·
1--------+-----.l--
l I - l 7
I
i I !
i
-----l----+---il--1--1 I ----+----
I ! i
I
•
i
I
------+--------+[----! ' • ~·~~ -~ ~ -------+--------+-- i I -----,----- ---
·-- - -----f--------------1- ---------~---~---!--- +-- I -·
r·· ---+----+-----+-----+---- ··--·--- -------4--~- +-----t--- i ~·~ -~----
0114
Eberline Analytical Oak Ridge Laboratory
Spike and Tracer Worksheet
Analysis Code
ThlSO
LCS & Matrix Spikes LCS MS
1 ·s 1 # Activity I Solution I Approx Volume Volume
sotope O dpmlg Date I Addition Used (g) Used (g)
Th-228 Th-8b 103.560 3/28/2018[ 0.100 0.1096
Th-230 Th-1b I 23.520 3/28/20181 0.500 0.5084
Th-232 1:'7-8b I 103.560 3/28/20181 0.100 0.1096
Tracers
i I Activity Solution [ Volume
I Approx
fraction Isotope !
Sol# I dpmlg Date 1
Used(g) Addition
01 Th-229 Th-18a 22.460 3/28/2018 0.4656 0.2200
02 Th-229 Th-18a 22.460 3/28/2018 0.2324 0.2200
03 Th-229 Th-18a 22.460 3/28/2018 0.2329 0.2200
04 Th-229 Th-18a 22.460 3/28/2018 0.2336 0.2200
I
I I I
I
Version 2.0 08/99
Date
3/28/2018 7:51
LCSD Volume Used(g)
MSD Volume Used(g)
Technician
JHARVEY
LCS MS Known
pCi
5.11
5.39
5.11
Tracer
\
Error _ Estimate
0.184
0.145
0.184
Added Error pCi Estimate
o.ooi I 0.00!
o.ooi I
0.000
0.000
0.000
Balance Printer Tapes
Page 1 of 1
Printed: 3/28/2018 7:55 AM
Technician Initials
LCSD Known
pCi
0.00
0.00
0.00
Error Estimate
0.000
0.000
0.000
LCS
Matrix Spike
Witness Initials
MSD Added
pCi
0.00
0.00
0.00
Error Estimate
0.000
0.000
0.000
0115
Lab
Eberline Analytical Oak Ridge Laboratory
Auxier & Associates, Inc.
Fraction Client ID
01 LCS
02 BLANK
03 AC-SED-11
04 AC-SED-11
Comments
Technician:
Aliquot Worksheet
Analysis Code Rpt Units Lab Deadline
ThlSO grams 4/12/2018
Sample Muffle Data Dilution Data Aliquot Data
Ratio Type Post/Pre No of Dils Dil Factor Ratio Aliquot Net Equiv
LCS 1.0000E+OO 1.0000E+OO
MBL 1.0000E+OO 1.0000E+OO
DUP 9.9780E-01 9.9780E-01
DO 1.0036E+OO 1.0036E+OO
~f),/0 '7t.-: Date: 3_1@_1--15!,
Technician
JHARVEY
MS Aliquot Data
Printed: 3/28/2018 7:50 AM Page 1 of 1
H-3 Solids Only WaterAaaea R3 UISt
Aliquot Net Equiv (ml) Aliq
I
I
I
0116
Eberline Services - Oak Ridge Prep Logbook Version 2.0 8/1999
Eberline Auxier & Associates, Inc. Fraction Client ID
04 AC-SED-11
Comments
Special Codes
' ~~ / ..
Technician: ' ) ~
Lab Deadline
4/12/2018
Tare (g) Pan Wt
28.2500
Rough Sample Preparation Log Book
Date Received in Prep Date Sealed
3/26/2018 3/27/2018
Gross (g) Net (g) ------
Wet Wt. ! Dry Wt. Wet Wt. Dry Wt.
1839.80001 1287.5600 1811.5500 1259.3100
--·
·--·-·--·--·--- ---·--I
---------·-- ·-·--
----·--
-~---·
-·-···-
..
Date Returned
3/28/2018
Percent Liquid
T Solid
30.48% • 69.52% ··--·- ----+--·-··-··--···· I
I --------
-·-
I ·- --·-·:=1- --·-· ·-·-i ...
,----·
I - ----
i I ·------------
I I
------·--------------~--
I
I
I ---------I I
I
H: Hot, O: Organic Hazard, P: PCB Hazard, R: Rush, T: Other (see comments)
Printed: 3/27/2018 6:45 AM Page 1 of 1
Technician
KSALLINGS
Gamma Special Dry Wt. I LEPS Wt. Info
0.00001 0.0000
1'
l I ·---
. I
I
Date:Analysis: Rough Prep Logbook Analysis: Th ISO Page No, 10439
0117
c&fA Al h TM ~ J-\ p ex- p a Sample Description: Spectrum File: Batch Identification:
SPIKE \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803111A-TH Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
01 Shelf 2 Th iso
Alpha_044 04026481B 84168 System Bkgd 211467
<not performed>
1. 000E+000 3/30/2018 3/30/2018
170.0
+/- 0.000E+000 gram 6:44:48 AM 8:11:12 AM
minutes 170.0 minutes
Th229 S TH-18A
0. 0117
Counting Efficiency:
0.466 mL 0.1849 +/-0.1840 +/-1.0047 +/-
0.0032 on 2/16/2018 0.0660
9:34:19 AM
Chem. Recovery Factor:
Control Certificate Name: NatTh Th-8 Chem. Recov. of Control: TH-232 1.224356 +/- 0.103873
Peak Match Tolerance: 0.175 MeV
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.883 5.365 4.851 4.616 3.960
PEAK AREA REPORT
Net Pk Area
2.32 435.00 328.66 457.32 436.83
Pk Area Error%
149.12 9.41
10.82 9.17 9.38
Ambient Backgnd
0.68 0.00 0.34 0.68 0.17
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 16.8
4.4 5.1
38.9
T Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.994 0.994 0.998 0.984 0.993
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/gram
3.41E-002 +!- 5.l0E-002 6.24E+000 +!- 9.71E-001 4.73E+000 +!- 5.87E-001 6.57E+000 +!- l.0lE+000 6.26E+000 +!- 9.74E-001
~ 3/30/18
MDA (pCi/gram
8.29E-002 +/-8.60E-002 +/-6.88E-002 +/-8.l0E-002 +!-5.98E-002 +/-
l.03E-002 1. 07E-002 8.54E-003 l.00E-002 7.42E-003
0118
60
55
50
45
40
35 V) .µ C: :::::s
8 30
25
20
15
10
5
g
' er I-
0000209956.CNF
Live Time :10200.000 sec Real Time :10200.300 sec Start: 1:3463.6(kev) Stop : 1024:6522. 9(kev) Acq. Start :Fri Mar 30 08:11:12 2018
0 I j! 11 1 Ml 1111! Mllll/illMI 1 1 , I ' 1 M !MRm rn 1 111i n 11Mv 11 1n1 1 .• 3500 I ,1,1 I I I 1:i11 fU;',P!ii'IJMMl!llll I I I ' ' f II M IW II Ill JI I :: 1 1 ~ , ' I I l!AAN\NU\IVIUIMII\I\ I I' 4000 4500 5000
Energy(kev) 5500 6000 6500
ROI Type: 1 ROI Type: 3
0119
Channel Data Report 3/30/2018 1:46:48 PM Page 1
******************************************************* ***** s p E C T R A L DAT A R E P O R T ***** *******************************************************
Sample Title: 01
Elapsed Live time: 10200 Elapsed Real Time: 10200
Channe 1 I - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I 1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 1 0 0 0
17: 0 1 0 0 0 0 0 0
25: 0 2 0 0 0 1 0 0
33: 0 0 0 0 0 0 0 0
41: 0 1 0 1 0 0 0 0
49: 0 0 0 0 1 1 0 0
57: 2 0 1 0 0 0 1 0
65: 0 0 0 0 0 0 1 0
73: 1 0 0 3 0 0 0 0
81: 0 1 0 1 0 1 1 0
89: 0 0 0 2 1 1 1 0
97: 1 0 1 0 2 2 0 5
105: 3 1 2 1 1 2 1 0
113: 2 3 2 2 1 1 2 1
121: 4 2 2 4 2 1 5 4
129: 7 1 4 7 5 6 5 5
137: 4 5 8 5 5 10 7 6
145: 9 3 6 8 7 9 7 4
153: 12 14 7 16 9 8 11 14
161: 17 14 9 11 15 14 13 11
169: 14 13 14 11 17 21 15 12
177: 10 11 11 10 15 15 4 5
185: 3 3 2 1 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 1 0 0 1 0 0 0 0
233: 0 0 0 0 0 0 1 0
241: 0 1 0 1 0 0 2 0
249: 0 1 0 0 0 0 0 1
257: 2 0 0 0 0 1 0 1
265: 0 0 0 0 0 0 0 0
273: 0 1 0 0 0 0 2 0
281: 0 0 0 0 0 0 0 0
289: 1 0 0 0 0 0 0 1
297: 0 1 0 1 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 2 0 0 0 0 0 2 0
321: 0 1 0 0 1 2 1 0
329: 1 2 3 3 0 0 1 1
337: 1 1 1 1 0 2 0 1
345: 0 4 1 1 2 1 3 4
353: 2 2 2 1 5 5 0 2
361: 2 3 6 5 6 10 6 8
0120
Channel Data Report 3/30/2018 1:46:48 PM Page 2
369: 3 3 11 7 4 6 9 16
Sample Title: 01
Channell------l-------l-------1-------1-------1-------I-------I-------I 377: 3 6 9 8 8 8 8 10
385: 7 17 13 7 9 10 7 9
393: 9 10 9 9 10 9 7 21
401: 10 16 11 9 9 8 7 4
409: 4 4 2 1 0 2 0 0
417: 3 2 0 3 3 2 4 1
425: 2 2 3 2 3 4 1 3
433: 0 3 2 3 6 4 3 8
441: 4 10 4 6 5 4 6 5
449: 6 4 4 7 3 9 3 3
457: 11 4 5 7 6 5 5 7
465: 8 2 4 4 8 3 1 1
473: 2 3 6 4 4 2 3 3
481: 2 6 4 2 6 1 1 3
489: 2 3 2 1 5 2 3 2
497: 0 2 0 0 4 0 2 2
505: 0 2 3 2 1 1 1 2
513: 2 0 1 1 0 1 1 2
521: 1 0 1 0 0 0 0 1
529: 0 0 0 1 0 0 0 0
537: 1 0 0 1 0 1 0 1
545: 1 0 0 0 1 1 0 0
553: 1 0 1 0 0 0 0 0
561: 1 0 0 1 0 2 2 2
569: 1 0 3 0 2 0 1 2
577: 0 0 0 0 3 1 2 1
585: 1 1 1 1 4 1 1 8
593: 0 2 5 4 4 4 5 4
601: 3 3 5 8 4 6 5 6
609: 3 5 10 5 6 5 9 10
617: 6 6 10 11 5 7 9 7
625: 4 7 12 7 16 6 4 6
633: 13 10 10 10 6 14 12 14
641: 15 17 8 12 15 14 12 11
649: 10 14 10 16 12 10 6 4
657: 3 1 2 1 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 1 0 0 0 0 0
689: 0 0 0 0 0 0 2 0
697: 0 0 0 1 0 1 0 0
705: 0 0 0 0 0 0 1 1
713: 1 0 1 0 1 1 1 1
721: 0 0 0 3 1 2 2 0
729: 1 2 3 2 0 4 0 2
737: 1 2 2 0 1 1 2 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 1 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0121
Channel Data Report 3/30/2018 1:46:48 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 01
Channell------l-------l-------1-------1-------1-------I-------I-------I 809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 1 0
825: 0 0 0 0 0 0 0 0
833: 1 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 1 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 1 0 0 0
889: 0 0 1 0 0 0 1 0
897: 0 0 0 0 1 0 1 1
905: 0 0 0 0 0 0 1 0
913: 1 1 1 0 0 1 1 1
921: 0 0 1 1 0 1 3 1
929: 1 2 1 1 0 3 1 3
937: 0 2 0 2 0 0 0 1
945: 0 0 1 0 0 0 0 0
953: 0 1 1 0 0 1 1 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0122
c&,,A Al h TM ~-~~Mpex- p a Sample Description: Spectrum File: Batch Identification:
BLANK \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803111A-TH
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
02 Shelf 2 Th iso
Alpha_045 04026482A 91131 System Bkgd 211468
<not performed>
l.000E+000 +!- 0.000E+000 3/30/2018 6:44:48 3/30/2018 8:11:15
170.0 minutes 170.1 minutes
Th229 S TH-18A 0.232 mL 0.1236 +/- 0.0125
AM AM
gram
Counting Efficiency: Chem. Recovery Factor:
0.1735 +/- 0.0031 on 2/16/2018
0.7121 +/- 0.0734 9:34:18 AM
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5. 912 5.298 4.897 4.647 4.062
0.175 MeV
PEAK AREA REPORT
Net Pk Area
0.79 -3.40
109.62 2.13
-0.70
Pk Area Error%
455.84 72.42 18. 96
191.21 317.90
Ambient Backgnd
2.21 3.40 2.38 1.87 1. 70
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 0.0 6.6 3.0 3.0
T = Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.980 0.947 0.997 0.997 0.978
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/gram
1. 74E-002 +!- 7.93E-002 -7.30E-002 +/- 5.48E-002
2.36E+000 +/- 4.70E-001 4.58E-002 +/- 8.80E-002
-l.50E-002 +/- 4.78E-002
~ 3/~o!,s
MDA (pCi/gram
1. 76E-001 +!-l.99E-001 +/-l.77E-001 +/-l.63E-001 +/-l.58E-001 +!-
3.50E-002 3.96E-002 3.52E-002 3.24E-002 3.14E-002
0123
Vl .µ
60
55
50
45
40
35
C: :::s 8 30
25
20
15
10
5
0000209922.CNF
Live Time :10200.000 sec Real Time :10203.600 sec Start: 1: 3510. S(keV) stop : 1024:6578.4(kev) Acq. start :Fri Mar 30 08:11:15 2018
0 I 1 1 i 1'!'1 ' r11111 ,,, I' I h I I l ,. __ ),: u ,G:id lli \ . ~
& I 1! I, !;,ii, 1,1, !11/11 \ 'lil'.i V'lj,1, 11:i, 1! 1 ! 1 ! 1 I I /. I ,'.I,\ I ! I (W\ ! I !t I '
4000
ROI Type: 1
4500 5000 Energy(kev)
5500 6000 6500
ROI Type: 3
0124
Channel Data Report 3/30/2018 1:27:29 PM Page 1
*******************************************************
***** s p E C T R A L D A T A RE P O R T *****
*******************************************************
Sample Title: 02
Elapsed Live time: 10200 Elapsed Real Time: 10204
Channell------l-------l-------l-------l-------1-------1-------1-------I
1: 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 0 0 0
129: 0 0 0 0 0 0 0 0
137: 0 0 0 0 0 0 0 0
145: 0 0 0 0 0 0 0 0
153: 0 0 0 0 0 0 0 0
161: 0 0 0 0 0 0 0 0
169: 0 0 0 0 0 0 0 0
177: 0 0 0 0 0 0 0 0
185: 1 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 1 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 1 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 0 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 1 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0125
Channel Data Report 3/30/2018 1:27:29 PM Page 2
369: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------1-------1-------1-------I-------I 377: 0 0 0 0 0 0 0 0
385: 0 0 1 0 0 0 0 1
393: 0 0 0 0 0 0 0 1
401: 0 0 0 0 0 0 0 0
409: 0 0 0 0 0 2 0 0
417: 1 0 0 0 0 0 0 0
425: 0 0 0 0 1 1 1 0
433: 0 1 0 1 2 1 0 0
441: 3 2 4 1 3 4 5 0
449: 2 2 2 2 2 7 5 2
457: 1 1 0 0 2 2 4 1
465: 2 2 1 1 2 0 1 2
473: 0 2 1 0 0 0 0 1
481: 2 1 1 1 2 2 2 2
489: 2 1 0 1 1 1 0 1
497: 0 0 0 0 1 0 0 0
505: 0 0 0 0 0 0 0 0
513: 0 1 1 0 2 0 0 0
521: 1 1 2 0 0 0 0 0
529: 0 0 0 0 1 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 0 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 0 0 0 0 0
625: 0 0 0 0 0 0 0 0
633: 0 0 0 0 0 0 0 0
641: 0 0 0 0 0 0 0 0
649: 0 0 0 0 0 0 0 0
657: 0 0 0 0 0 0 0 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 1 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 1 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 1 0 0
745: 0 0 0 0 0 0 0 0
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0126
Channel Data Report 3/30/2018 1:27:29 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 02
Channell------l-------l-------l-------1-------1-------1-------I-------I
809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 1 0 0 0 0 0
833: 0 0 0 1 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 1 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 1 1 1 2 0
937: 1 0 2 2 1 0 0 0
945: 0 0 0 0 0 0 1 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 1 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0127
c!!tA Al h TM ~J-\pex- p a Sample Description: Spectrum File: Batch Identification:
AC-SED-11 DUP \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803111A-TH
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
03 Shelf 2 Th iso
Alpha_046 04026482B 58762 System Bkgd 211469
<not performed>
9.978E-001 3/21/2018 3/30/2018
170.0
+/- 0.000E+000 gram 6:44:48 AM 8:11:18 AM
minutes 170.1 minutes
Th229 S TH-18A 0.233 mL 0.1649 +/- 0.0146
Counting Efficiency: 0.1783 +/- 0.0031 on 2/16/2018
0.9252 +/- 0.0836 9:34:16 AM
Chem. Recovery Factor:
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.866 5.384 4.889 4.647 3. 971
0.175 MeV
PEAK AREA REPORT
Net Pk Area
0.47 64.30
146.64 72.49 51.47
Pk Area Error%
626.93 24.82 16.27 23.12 27.79
Ambient Backgnd
1. 53 1. 70 1.36 0.51 1. 53
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 8.2
19.1 4.6 4.4
T = Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Con£.
0.999 0.999 0.998 0.997 0.997
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/gram
7.77E-003 +!- 4.87E-002 l.05E+000 +!- 3.17E-001 2.37E+000 +!- 4.12E-001 l.17E+000 +/- 3.38E-001 8.29E-001 +!- 2.72E-001
-A~ 3/30/,s
MDA (pCi/gram
1.1 7E- 001 +!-l.19E-001 +!-l.llE-001 +!-8.46E-002 +/-l.14E-001 +!-
2.04E-002 2.07E-002 l.93E-002 l.47E-002 l.99E-002
0128
0000209923.CNF
Live Time :10200.000 sec
60+ Real Time :10203.600 sec Start: 1:3490.6(kev) Stop : 1024:6554.S(kev) Acq. Start :Fri Mar 30 08:11:18 2018
L 55
50
45
40
35 V) .µ C: :::s 8 30
25
20
15
10
5
Q ~ I I I ! I H I I I I I I
3500 4000 4500 5000 5500 6000 6500 Energy(kev)
ROI Type: 1 ROI Type: 3
0129
Channel Data Report 3/30/2018 1:27:36 PM Page 1
******************************************************* ***** s p E CTR AL DAT A RE P O R T ***** *******************************************************
Sample Title: 03
Elapsed Live time: 10200 Elapsed Real Time: 10204
Channell------l-------l-------l-------1-------1-------1-------I-------I
1: 0 0 0 0 1 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 1
25: 0 0 0 0 0 0 0 0
33: 0 0 0 0 0 0 0 0
41: 0 0 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 1 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 1 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 1 0 0 0 1 0 0 0
129: 0 0 0 0 0 0 0 0
137: 1 0 0 1 1 0 0 0
145: 1 0 1 0 1 1 0 1
153: 0 3 0 3 0 2 2 1
161: 1 1 1 1 2 3 1 1
169: 2 5 1 5 1 5 1 0
177: 1 0 0 0 0 0 0 0
185: 0 0 0 0 0 0 0 0
193: 0 0 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 1 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 0 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 1 0 0 0 0 0 0 0
289: 0 0 0 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 0 0 0
313: 0 0 0 0 0 0 1 0
321: 0 0 0 0 0 0 0 0
329: 0 0 0 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 1 0 0 1 0 0
361: 1 1 0 1 0 1 0 0
0130
Channel Data Report 3/30/2018 1:27:36 PM Page 2
369: 1 2 2 0 2 1 0 1
Sample Title: 03
Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 2 0 1 2 2 1 1 0
385: 2 0 1 0 0 1 2 6
393: 2 3 2 4 10 3 2 5
401: 1 2 1 0 0 0 0 1
409: 0 0 0 0 0 1 0 0
417: 0 0 1 0 0 0 1 0
425: 0 0 0 0 1 0 1 1
433: 0 1 2 1 1 2 2 1
441: 2 2 4 2 3 4 0 4
449: 2 4 4 4 5 5 5 1
457: 2 2 0 3 3 2 0 2
465: 1 0 2 2 1 4 1 1
473: 1 3 2 1 0 1 0 0
481: 1 0 4 1 2 2 1 2
489: 0 1 1 1 0 1 0 1
497: 2 2 3 0 0 0 1 1
505: 3 0 0 1 0 2 2 0
513: 1 3 0 2 1 1 0 1
521: 0 1 0 0 1 1 0 0
529: 0 0 0 0 0 0 0 0
537: 0 0 0 0 0 0 0 0
545: 0 0 0 0 0 0 0 0
553: 1 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 1 0 2 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 1 0 0 0 1
601: 1 0 0 0 0 0 0 0
609: 0 0 1 0 1 1 0 1
617: 0 0 1 0 0 1 2 0
625: 0 0 0 0 0 0 3 2
633: 2 0 3 2 5 4 2 2
641: 1 5 3 5 6 2 1 0
649: 3 1 0 0 0 0 0 0
657: 0 0 0 1 0 0 0 1
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 1 0 0 0 0
697: 0 0 0 1 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 1 0 1 0 0 0
721: 0 0 1 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 1 0 0 0 0 0 0 0
745: 0 0 0 0 0 0 0 0
753: 0 1 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 0 0 0
793: 0 0 0 0 0 0 0 0
0131
Channel Data Report 3/30/2018 1:27:36 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 03
Channell------l-------l-------l-------l-------1-------1-------1-------I
809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 1 0 0 0 0 0 0
841: 0 0 0 0 0 0 0 0
849: 0 0 0 0 0 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 1 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 0
905: 0 0 0 0 0 0 0 0
913: 0 0 0 0 0 0 0 0
921: 0 1 0 0 0 0 0 0
929: 0 1 0 1 1 0 0 0
937: 0 0 0 1 0 0 0 0
945: 0 0 0 0 0 0 0 0
953: 0 0 0 0 0 0 0 0
961: 0 0 0 0 0 0 0 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0132
c!t;'A Al h TM ~-~A!!'l""\pex - p a Sample Description: Spectrum File: Batch Identification:
AC-SED-11 \\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00002099
1803111A-TH
Sample Identification: Sample Geometry: Procedure Description:
Detector Name: Chamber Serial Number: Detector Serial Number: Env. Background: Reagent Blank:
Sample Size: Sample Date/Time: Acquisition Date/Time: Acquisition Live Time: Acquisition Real Time:
Tracer Certificate: Tracer Quantity: Effective Efficiency:
04 Shelf 2 Th iso
Alpha_049 10006121A 49 System Bkgd 211470
<not performed>
l.004E+000 3/21/2018 3/30/2018
170.0
+/- 0.000E+000 gram 6:44:48 AM
10:29:04 AM minutes
170.0 minutes
Th229 S TH-18A 0.234 mL 0.1308 +/- 0.0128
Counting Efficiency: Chem. Recovery Factor:
0.1565 +/- 0.0028 on 2/16/2018 12:37:01 PM
0.8360 +/- 0.0831
Peak Match Tolerance:
Nuclide
TH-227 TH-228 TH-229 T TH-230 TH-232
Energy (MeV)
5.879 5.390 4.887 4.654 3.970
0.175 MeV
PEAK AREA REPORT
Net Pk Area
3.49 38.81
116. 66 66.49 55.66
Pk Area Error%
113. 53 32.02 18.18 24.14 26.37
Ambient Backgnd
0.51 1.19 0.34 0.51 0.34
Reagent Backgnd
0.00E+000 0.00E+000 0.00E+000 0.00E+000 0.00E+000
FWHM (keV)
3.0 5.9 3.6 4.1 3.7
T = Tracer Peak used for Effective Efficiency
Nuclide
TH-227 TH-228 TH-229 TH-230 TH-232
Id Conf.
0.996 0.999 0.999 0.998 0.996
NUCLIDE ANALYSIS RESULTS
Energy (keV)
5850.00* 5400.00* 4872.00* 4672.00* 3997.00*
Activity (pCi/gram
7.23E-002 +/- 8.32E-002 7.91E-001 +/- 2.95E-001 2.37E+000 +!- 4.53E-001 l.34E+000 +!- 4.14E-001 l.12E+000 +/- 3.66E-001
~ c3/3o(<?S
MDA (pCi/gram
1. 09E-001 +/-l.34E-001 +/-9.70E-002 +!-l.06E-001 +/-9.65E-002 +/-
2.08E-002 2.57E-002 1.86E-002 2.03E-002 1.85E-002
0133
V) ...... C :::J
60
55
50
45
40
35
8 30
25
20
15
10
5
0000209945.CNF
Live Time :10200.000 sec Real Time :10201.000 sec Start: 1:3474.l(kev) stop : 1024:6513.l(kev) Acq. start :Fri Mar 30 10:29:04 2018
i ti. · , ... 1;,;•,,-
0 I. ·, /i
litt I i. _lt1n\/!.\,\1:j ·11 A !, l I , ;\ .. i ; I, "
3500 4000 4500
ROI Type: 1
5000 Energy(kev)
5500 6000
ROI Type: 3
6500
0134
Channel Data Report 3/30/2018 1:27:44 PM Page 1
******************************************************* ***** s p E C T R A L D A T A R E P O R T ***** *******************************************************
Sample Title: 04
Elapsed Live time: 10200 Elapsed Real Time: 10201
Channell------l-------l-------1-------1-------1-------I-------I-------I
1: 0 0 0 0 0 0 0 0
9 : 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 0 0 0 1 0
33: 0 0 0 0 0 0 0 0
41: 0 1 0 0 0 0 0 0
49: 0 0 0 0 0 0 0 0
57: 0 0 0 0 0 0 0 0
65: 0 0 0 0 0 0 0 0
73: 0 0 0 0 0 0 0 0
81: 0 0 0 0 0 0 0 0
89: 0 0 0 0 0 0 0 0
97: 0 0 0 0 0 0 0 0
105: 0 0 0 0 0 0 0 0
113: 0 0 0 0 0 0 0 0
121: 0 0 0 0 0 1 0 0
129: 0 0 0 0 0 0 0 0
137: 0 2 1 0 0 0 0 0
145: 0 0 1 0 1 0 1 1
153: 2 0 2 0 1 0 2 1
161: 0 2 2 0 2 3 1 0
169: 1 0 1 2 1 1 2 4
177: 1 5 1 0 2 0 1 3
185: 1 1 0 1 1 0 0 0
193: 0 1 0 0 0 0 0 0
201: 0 0 0 0 0 0 0 0
209: 0 0 0 0 0 0 0 0
217: 0 0 0 0 0 0 0 0
225: 0 0 0 0 0 0 0 0
233: 0 0 0 0 0 0 0 0
241: 0 0 0 0 0 0 0 0
249: 0 0 0 0 0 0 0 0
257: 0 0 0 0 0 1 0 0
265: 0 0 0 0 0 0 0 0
273: 0 0 0 0 0 0 0 0
281: 0 0 0 0 0 0 0 0
289: 0 0 1 0 0 0 0 0
297: 0 0 0 0 0 0 0 0
305: 0 0 0 0 0 1 0 0
313: 0 0 0 0 1 0 0 0
321: 1 0 0 0 0 0 0 0
329: 0 0 1 0 0 0 0 0
337: 0 0 0 0 0 0 0 0
345: 0 0 0 0 0 0 0 0
353: 0 0 0 0 0 0 0 0
361: 0 0 0 0 0 0 0 0
0135
Channel Data Report
369: 0 0 1
Sample Title: 04
3/30/2018
0
1:27:44 PM
1 0 0
Page 2
0
Channell------l-------l-------l-------l-------1-------1-------1-------I 377: 0 0 1 0 2 1 1 0
385: 2 1 1 0 3 2 0 0
393: 0 1 1 4 0 0 1 1
401: 3 1 1 5 3 0 7 3
409: 5 4 2 4 1 1 1 0
41 7: 0 0 0 0 0 0 0 0
425: 1 0 0 0 0 3 1 0
433: 0 0 0 0 0 1 1 0
441: 0 0 0 0 1 1 2 1
449: 1 0 4 1 2 1 1 3
457: 1 6 1 0 1 6 2 4
465: 3 6 2 1 3 2 0 1
473: 0 3 1 3 1 1 1 0
481: 2 2 1 1 1 2 0 0
489: 2 1 2 1 0 0 0 1
497: 2 0 1 1 0 1 1 0
505: 0 0 0 1 0 2 2 0
513: 1 0 0 0 1 0 0 3
521: 0 0 2 1 0 0 2 0
529: 0 0 0 0 1 0 2 1
53 7: 0 0 1 0 0 0 0 0
545: 0 0 1 0 0 1 0 0
553: 0 0 0 0 0 0 0 0
561: 0 0 0 0 0 0 0 0
569: 0 0 0 0 0 0 0 0
577: 0 0 0 0 0 0 0 0
585: 0 0 0 0 0 0 0 0
593: 0 0 0 0 1 0 0 0
601: 0 0 0 0 0 0 0 0
609: 0 0 0 0 0 0 0 0
617: 0 0 0 1 0 1 0 1
625: 0 1 1 0 1 0 0 0
633: 1 0 1 0 1 0 0 1
641: 1 0 0 0 1 3 1 0
649: 0 3 0 2 2 4 2 1
657: 3 0 2 1 1 1 1 0
665: 0 0 0 0 0 0 0 0
673: 0 0 0 0 0 0 0 0
681: 0 0 0 0 0 0 0 0
689: 0 0 0 0 0 0 0 0
697: 0 0 0 0 0 0 0 0
705: 0 0 0 0 0 0 0 0
713: 0 0 0 0 0 0 0 0
721: 0 0 0 0 0 0 0 0
729: 0 0 0 0 0 0 0 0
737: 0 0 0 0 0 0 1 0
745: 0 0 0 0 0 0 0 1
753: 0 0 0 0 0 0 0 0
761: 0 0 0 0 0 0 0 0
769: 0 0 0 0 0 0 0 0
777: 0 0 0 0 0 0 0 0
785: 0 0 0 0 0 1 0 0
7 93: 0 0 0 0 0 0 0 0
0136
Channel Data Report 3/30/2018 1:27:44 PM Page 3
801: 0 0 0 0 0 0 0 0
Sample Title: 04
Channell------1-------1-------1-------I-------I-------I-------I-------I
809: 0 0 0 0 0 0 0 0
817: 0 0 0 0 0 0 0 0
825: 0 0 0 0 0 0 0 0
833: 0 0 0 0 0 0 0 0
841: 0 0 0 0 0 0 1 0
849: 0 0 0 0 1 0 0 0
857: 0 0 0 0 0 0 0 0
865: 0 0 0 0 0 0 0 0
873: 0 0 0 0 0 0 0 0
881: 0 0 0 0 0 0 0 0
889: 0 0 0 0 0 0 0 0
897: 0 0 0 0 0 0 0 1
905: 0 0 0 0 0 0 0 1
913: 0 0 0 0 0 0 0 0
921: 0 0 0 0 0 0 0 0
929: 0 0 0 0 0 0 0 0
937: 0 0 0 1 0 0 0 0
945: 0 1 0 0 0 0 1 0
953: 0 0 0 0 1 0 0 0
961: 2 0 0 0 0 0 1 0
969: 0 0 0 0 0 0 0 0
977: 0 0 0 0 0 0 0 0
985: 0 0 0 0 0 0 0 0
993: 0 0 0 0 0 0 0 0
1001: 0 0 0 0 0 0 0 0
1009: 0 0 0 0 0 0 0 0
1017: 0 0 0 0 0 0 0 0
0137
t""age I OT "
f ~Apex-AlphaT]
Date : 3/30/2018
Q_A Sl)A/TAAARY REPORT Review Of QA Results - Pulser Check
Time : 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG
Alpha 001 2lf ALL Not Done
Alpha 002 21f ALL Not Done
Alpha 003 21f ALL Passed
Alpha 004 21f ALL Passed
Alpha 005 21f ALL Not Done
Alpha 006 21f ALL Not Done
Alpha 007 21f ALL Not Done
Alpha 008 21f ALL Not Done
Alpha 009 21f ALL Not Done
Alpha 010 21f ALL Passed
Alpha 011 21f ALL Passed
Alpha 012 2lf ALL Passed
Alpha 013 21f ALL Not Done
Alpha 014 21f ALL Passed
Alpha 015 21f ALL Not Done
Alpha 016 21f ALL Not Done
Alpha 033 Alpha Analvstl00DC ALL Passed
Alpha 034 Alpha AnalvstlO0DC ALL Passed
Alpha 035 Alpha Analystl00DC ALL Passed
Alpha 036 Alpha Analystl 00DC ALL Passed
Alpha 037 Alpha Analystl 00DC ALL Not Done
Alpha 038 Alpha Analystl00DC ALL Passed
Alpha 039 Alpha Analyst l 00DC ALL Not Done
Alpha 040 Alpha Analystl00DC ALL Passed
Alpha 041 Alpha Analystl00DC ALL Passed
Alpha 042 Alpha Analvstl00DC ALL Passed
Alpha 043 Alpha Analystl 00DC ALL Passed
Alpha 044 Alpha Analystl00DC ALL Passed
Alpha 045 Alpha Analyst l 00DC ALL Passed
Alpha 046 Alpha Analvstl00DC ALL Passed
Alpha 047 Alpha Analvstl 00DC ALL Not Done
Alpha 048 Alpha Analystl00DC ALL Not Done
Alpha 049 Alpha Analystl00DC ALL Passed
Alpha 050 Alpha AnalystlO0DC ALL Passed
Alpha 051 Alpha AnalystlO0DC ALL Passed
Alpha 052 Alpha Analystl 00DC ALL Passed
Alpha 053 Alpha Analystl 00DC ALL Passed
Alpha 054 Alpha Analystl00DC ALL Passed
Alpha 055 Alpha Analystl00DC ALL Passed
Alpha 056 Alpha Analystl 00DC ALL Passed
Alpha 057 Alpha Analvstl 00DC ALL Passed
Alpha 058 Alpha Analvstl00DC ALL Passed
3/30/2018 5:55:22 AM
DATE
3/30/2018 5:03:13 AM 3/30/2018 5:03:14 AM
3/30/2018 5:03:15 AM 3/30/2018 5:03:16 AM 3/30/2018 5:03:17 AM
3/30/2018 5:03:18 AM
3/30/2018 5:03:19 AM 3/30/2018 5:03:21 AM 3/30/2018 5:03:22 AM 3/30/2018 5:03:24 AM
3/30/2018 5:03:26 AM
3/30/2018 5:03:28 AM 3/30/2018 5:03:30 AM 3/30/2018 5:03:32 AM 3/30/2018 5:03:34 AM 3/30/2018 5:03:37 AM 3/30/2018 5:03:39 AM 3/30/2018 5:03:42 AM
3/30/2018 5:03:44 AM 3/30/2018 5:03:47 AM 3/30/2018 5:03:49 AM 3/30/2018 5:03:52 AM 3/30/2018 5:03:54 AM 3/30/2018 5:03:57 AM 3/30/2018 5:03:59 AM 3/30/2018 5:04:02 AM 3/30/2018 5:04:05 AM 3/30/2018 5:04:08 AM
0138
Page 2 of 2 Kev,ew ot UA Kesults - t-'ulser L;necK 3/30/2018 5:55:22 AM
CHAMBER DEVICE PARAMETER FLAG DATE
Alpha 059 Alpha AnalystlO0DC ALL Not Done
Alpha 060 Alpha AnalvstlO0DC ALL Not Done
APPROVED BY:
APPROVAL DATE:'')/;;()/[ s
0139
Library Listing Report 6/12/12 12:16:29 PM Page 1
*************************************************************************
***** L I B R A R Y L I S T I N G R E P O R T *****
*************************************************************************
Nuclide Library Title: Thorium
Nuclide Library Description: Th-227,-228,-229,-230,-232
Nuclide Half-Life Energy Energy Yield Yield
Name (Seconds) (keV ) Uncert. (keV (%) Uncert. (Abs.+-)
TH-227 6.873E+008 5850.000* 0.000 97.5000 0.0000
TH-228 6.034E+007 5400.000* 0.000 99.9400 0.0000
TH-229 2.487E+Oll 4872.000* 0.000 99.5200 0.0000
TH-230 2.379E+Ol2 4672.000* 0.000 99.8200 0.0000
TH-232 4.434E+017 3997.000* 0.000 100.0000 0.0000
* = key line
TOTALS: 5 Nuclides 5 Energy Lines
0140
SECTIONX
ANALYTICAL DATA (GAMMA SPECTROSCOPY)
0141
Eberline Services Oak Ridge Laboratory Analysis Sheet
Work Order
Analysis Code
Run
Date Received
Lab Deadline
Client
3/23/2018
4/12/2018
Auxier & Associates, Inc.
Internal Sample Fraction Desc
01 LCS
02 MBL
03 DUP
18-03111 Gamma
Run 1
Client ID
LCS
BLANK
AC-SED-11 -----------
AC-SED-11 --~~- D0-r _ _ _ _ _ __ _
Login CPM
Sample Date
Printed: 3/27/2018 7:42 AM Page 1 of 3
Sample Aliquot
03/23/18 00:00 1.0000E+00
1.0000E+00
63 ! 03/21/1813:20 4.7630E+02 ----~-- -- - r~ ---
63 1
03/21/18 13:20 I 4.7630E+02 ------------- -- -+-- ~-- ----·------
1
Repo:':~::: WEST~KE NCC~ I I T ~---- -7 ~ 7- 7 - .
Activity Units I pCi I I I- ~----.~~ . ---------'·· -~::::~:~-~ ... ---~-Aliquot Units I g I I I ~--- I ____ ·"-i __
I
I Matrix I SO 11 ~~-~~~-L-- _______ ~---~--~-~-~ -
1
--~ ~~~~~, Method EPA 901.1 Modified I
I Instrument Type I Gamma Spectroscopy I [ . ·- ---=~~: - +-- [ -~----·~ ~~ ------'------+--------------i ____ .. ________ I ~----
- 1--+ ~·-------~ ~ ~---1 _,, ___ ,,,, _____ _
Radiometric Tracer
Radiometric Sol#
Tracer Act (dpm/g)
Carrier
Carrier Cone (mg/ml)
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0142
Eberline Services Oak Ridge Laboratory Analysis Sheet
18-03111 Gamma
Run 1
Printed: 3/27/2018 7:42 AM Page 2 of 3
Internal Fraction
Sample Desc
Tracer Aliquot (g)
Tracer Total ACT(dpm)
Radiometric Tracer (pCi)
Radiometric Grav Carrier ' % Rec I Added (ml)
I
I '1 0.00 Les I
I -- - -------r-- I
Grav Filter Tare (g)
Grav Filter Final (g)
Grav Filter Net (g)
Grav %Rec
Mean %Rec
I SAF SAF
l 1* 2*
01 _ -- - -- -- I 0.00! _ ! -- _ -~ ·········-·--- -- I
_02 I MBL I~ 7 ______ .. --- +- ·~~ I-- I
•-OJlouP-i- ..... -----. -- --1 ----·~--~-:~~I -·i------ I -~- ~-- I I 04 I DO L-~-~- i _____ , -- ~
00 ~~ - - - -- +·~- -- -- i
-[
µ
_I !
I
I I I r- l
I I
•
I
i I
7 -· L I ---
I I
I I
I
I_ I I
j I
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. A Indicates estimated SAF value.
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0143
Eberline Services Oak Ridge Laboratory Analysis Sheet
18-03111 Gamma
Run 1
Printed: 3/27/2018 7:42 AM Page 3 of 3
Internal Fraction
Sample Desc
Rough Prep Date
Rough Prep By
~; I ~-:-:- !,------------------------,-----
-·-·-- - ---·--··-------- --,------ . ··--------·---
03 _ DUP
Prep Date
Prep By
04 i DO i---0-3-/2-7/1_8_06-:4-5-+--K ____ S_A_L--LI-NG-S --------
Sep to Date/Time
Sep to By
Sep t1 Date/Time
Sep t1 By
--- ---,
-----
1'
------
-~- - - +-------- i -----r----~- -r-- --- t--~ ----------+------- - --~ - i
- --------1---~~---+--------,--~~------1 l------+-------1 ~~__,_____---t-~~+---------- ____ J______ I
- I I 1---------+-------+---------------+-----------+--------~---+-------+- I - ,
t-~-- ==== _:
I- I
- ~ I ,
I r---j- . I ~--- I
I
:
• SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only. "Indicates estimated SAF value.
•• Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
0144
Lab Fraction
01 01 02 02 02 02 02 02 02 02 02 02 02 03 03 03 03 03 03 03 03 03 03 03 04 04 04 04 04 04 04 04 04 04 04
Eberline Analytical Oak Ridge Laboratory
Nuclide I Sample
I Desc
CO-60 LCS
CS-137 LCS
AC-228 MBL
Bl-214 MBL
K-40 MBL
PA-231 MBL
PB-210 MBL
PB-212 MBL
PB-214 MBL
RA-226 MBL
RA-228 MBL
TH-234 MBL
TL-208 MBL
AC-228 DUP
Bl-214 DUP
K-40 DUP
PA-231 DUP
PB-210 DUP
PB-212 DUP
PB-214 DUP
RA-226 DUP
RA-228 DUP
TH-234 DUP
TL-208 DUP
AC-228 DO
Bl-214 DO
K-40 DO
PA-231 DO
PB-210 DO
PB-212 DO
PB-214 DO
RA-226 DO
RA-228 DO
TH-234 DO
TL-208 DO
Client
Identification
LCS
LCS
BLANK
BLANK
BLANK
BLANK
BLANK
BLANK
BLANK
BLANK
BLANK
BLANK
BLANK
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
AC-SED-11
Preliminary Data Report & Analytical Calculations
Work Order: 18-03111-Gamma-1 Activity
I Error LSC LCS LCS
Units Results
Estimate MDA Known %R Flag
pCi/g 1.32E+02 8.11E+00 9.45E-01 1.35E+02 97.25 OK
pCi/g 8.31E+01 7.72E+00 1.27E+00 8.44E+01 98.43 i OK
pCi/g 9.58E-03 2.20E-02 9.02E-02
pCi/g 2.99E-02 4.01E-02 6.90E-02
pCi/g 1.62E-01 1.S0E-01 3.39E-01
pCi/g -4.91E-01 5.96E-01 7.86E-01
pCi/g 3.72E-01 3.67E-01 5.55E-01
pCi/g 4.19E-02 2.44E-02 4.68E-02
pCi/g 2.52E-02 3.78E-02 6.34E-02
pCi/g 2.99E-02 4.01E-02 6.90E-02
pCi/g 9.58E-03 2.20E-02 9.02E-02
pCi/g 1.08E+00 3.97E-01 6.57E-01
pCi/g -5.60E-03 5.22E-02 7.99E-02
pCi/g 8.74E-01 2.34E-01 3.52E-01
pCi/g 1.06E+00 1.93E-01 2.46E-01
pCi/g 1.60E+01 2.13E+00 1.15E+00
pCi/g 1.37E+00 1.41E+00 3.33E+00
pCi/g 2.10E+00 1.33E+00 2.15E+00
pCi/g 1.44E+00 2.66E-01 2.35E-01
pCi/g 1.13E+00 1.98E-01 2.42E-01
pCi/g 1.06E+00 1.93E-01 2.46E-01
pCi/g 8.74E-01 2.34E-01 3.52E-01
pCi/g 1.72E+00 1.49E+00 2.05E+00
pCi/g 7.74E-01 1.68E-01 1.34E-01
pCi/g 1.09E+00 2.60E-01 3.95E-01
pCi/g 1.11E+00 1.95E-01 2.12E-01
pCi/g 1.68E+01 2.27E+00 1.36E+00
pCi/g 4.02E-01 1.98E+00 2.65E+00
pCi/g 2.01E+00 1.66E+00 2.74E+00
pCi/g 1.31E+00 2.57E-01 2.45E-01
pCi/g 1.10E+00 1.94E-01 2.16E-01
pCi/g 1.11E+00 1.95E-01 2.12E-01
pCi/g 1.09E+00 2.60E-01 3.95E-01
pCi/g 1.01E+00 1.14E+00 1.91E+00
pCi/g 9.65E-01 1.89E-01 1.34E-01
RPO
I Sample
Flag Date
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
03/23/18 00:00
OK 03/21/18 13:20
OK 03/21/18 13:20
OK 03/21/1813:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/1813:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
03/21/18 13:20
Printed: 4/17/2018 8:28 AM Page 1 of 1
Sample
I Counting
Identified Aliquot Date/Time
1.00E+00 04/17/18 05:42 YES
1.00E+00 04/17/18 05:42 YES
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
1.00E+00 04/17/18 06:13 NO
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17 /18 05:42 YES
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 05:42 NO
4.76E+02 04/17/18 05:42 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 NO
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17 /18 06:44 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 YES
4.76E+02 04/17/18 06:44 YES
0145
Count Room Report Client: Auxier Associates, lnco
Internal Fraction
Sample Desc
Client JD
18-03111-Gamma-1 (pCi/g) in SO Tracer ID:
Sample Sample Tracer
Date Aliquot Aliquot (g) Tracer
ACT(dpm)
Printed: 3/27/2018 7:42 AM Page 1 of 1
1ht Radiometric Radiometric SAF SAF
Tracer (pCi) % Rec 1* 2*
~ I LCS l LCS 03/23/1800:00 1.0000 i ~---------------·····--·•·-------·--··-------- 0.00 1
f7- I MBL , BLANK 03/23/18 00:00 . 1.0000 '
03/23/18 00:00 1.0000 j i
I
I
~, : ---- -ill~ 1--------'----'---------·--· . ----------+-- _ ___J____ - ·----, --~-T--------+.------1
t I · ' • I
1
__ ------ :=--=~=~ 1 ---- ------~! I
f
-- -1 ___ J _________ - I --+--~-
- I !---t-----------1.-------t -- I I
___ ___j_ ··-----
r--------,-7 , I -
I i ' t--_l --~I __ I
0146
Lab
Eberline Analytical Oak Ridge Laboratory
Auxier & Associates, Inc.
Fraction Client ID
01 LCS 02 BLANK 03 AC-SED-11 04 AC-SED-11
Analysis Code
Gamma
Sample Muffle Data Ratio
Type Post/Pre LCS MBL
------·-DUP DO
Aliquot Worksheet
Rpt Units Lab Deadline
grams 4/12/2018
Dilution Data Aliquot Data
No of Dils I Oil Factor7. Ratio Aliquot Net Equiv
I 1.0000E+00 1.0000E+00
i 1.0000E+00 1.0000E+00 i
I 4.7630E+02 4.7630E+02
I 4.7630E+02 4.7630E+02 -·--- .. ------·--··----+· ·- -··--·-------· --··-·--------·-,.·--
____ ! ___
--1-- -- --·-·--·--·-·--
! ---·- ---·-··- :-------·-··----t--- -----··--·~----
i I
! -----·--- ·--~--- ---------·-----
I --····---------- ------------- - I --- -- ----·--· . ---- -----·------ -
'
i
- -·- - --------- -----!- ---
! -·--·--- ------
I I -----!
Comments
')/ 4
Technician: ~/s..r<-f., )?-::::z Date: _3__; JI I / f
Printed: 3/27/2018 7:42 AM Page 1 of 1
Technician
KSALLINGS
MS Aliquot Data H-3 Solids Only
Aliquot Net Equiv wat~~~tea -
1
- H~~t-!
I I . -- -- ------~----
-----
. ----- _______ ,. ...
I - -----------· ---
----~-------- -----
-----··~---
----·--
-·------
0147
I
Eberline Services - Oak Ridge Prep Logbook Version 2.0 8/1999
Rough Sample Preparation Log Book
Date Received in Prep Date Sealed
3/26/2018 3/27/2018
Date Returned
3/28/2018
Printed: 3/27/2018 6:45 AM Page 1 of 1
Technician
KSALLINGS
Eberline I Auxier & Associates, lnc-j__ Tare (g) Gross (g) 1-- Net (_g) -I·-·- --~e_r~ent Pan Wt Wet Wt. Dry Wt. Wet Wt. Dry Wt. Liquid I Fraction Client ID
Gamma Solid Dry Wt. LEPS Wt.
Special Info
04 AC-SED-11 28.25001 1839.80001 1287.56001 1s11.5500I 1259_31001 30.48%I --·--·t---- . -- .... -- _ .. ~-~:52%1 0.0000 0.00001 I
I --------·· • I I
J - '·-- --- ··t· --· -· -- I
' !
..l
l~j - -~----1-~+---------------+------t-- · t~=-•·-·1-··- -T~~ -- I I I I I I 11-·········-:=[~ ~ ~-~1·~~~1 -----1---1
Comments
Special Codes H: Hot, 0: Organic Hazard, P: PCB Hazard, R: Rush, T: Other (see comments}
Technician: -~_,....,,'7 )t,.;,{ Date:Analysis: Rough Prep Logbook Analysis: Gamma Page No. 10439
0148
4/17/2018 6:13:23AM
pex-G mma Analysis Report for 1803111-01
GAS-1402
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator
Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803111-01
: GAS-1402
: SOIL
: 7.360E+02 grams
: Countroom
: 10/1/2014 9:14:17AM
: 4/17/2018 5:42:50AM
: GAS-1602 pCi
: Administrator
: GE1
: GAS-1602
: 1800.0 seconds
: 1821.9 seconds
: 1.20 %
: 2.50
: 1 - 4096
: 17 - 4096
: 1.000 keV
: 2/17/2018
: 2/17/2018
: 64638
PEAK-TO-TOTAL CALIBRATION REPORT
Peak-to-Total Efficiency Calibration Equation
Page 1 of 25
l/ /(l/18
0149
4/17/2018 6:13:23AM
Analysis Report for 1803111-01
GAS-1402
PEAK LOCATE REPORT
Peak No.
1 2 3 4 5 6 7 8 9
10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak Search Sensitivity
Energy (keV)
31.75 49.82 55.64 59.34 65.26 84.76 87.94 93.62
121.93 136.49 165.23 187.80 238.60 352.74 518.37 639.07 661.79 666.87
1073.55 1115.79 1121.26 1173.53 1178.72 1332.83 1338.00 1452.45 1835.51 2004.08 2011.16 2273.36 2445.44 2505.69 2614.03
? = Adjacent peak noted
Errors quoted at 2.000sigma
: 4/17/2018 6:13:15AM
: 1 : 4096 : 2.50
Centroid Channel
32.26 50.31 56.12 59.82 65.73 85.22 88.40 94.07
122.35 136.89 165.62 188.16 238.92 352. 96 518.45 639.06 661.76 666.84
1073.24 1115.44 1120.91 1173.15 1178.33 1332.36 1337.52 1451. 91 1834.78 2003.29 2010.37 2272.48 2444.52 2504.75 2613.07
Centroid Uncertainty
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Page 2 of 25
Peak Significance
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0;00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0150
4/17/2018 6:13:23AM Page 3 of 25
Analysis Report for 1803111-01
GAS-1402
PEAK ANALYSIS REPORT ,.
Peak Analysis Performed on : 4/17/2018 6: 13:15AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM
No. (keV) start end Centroid Area Uncertainty Counts (keV)
1 31.75 31 - 35 32.26 l.51E+03 225.53 9.73E+03 1. 74
M 2 49.82 45 - 63 50.31 6.00E+03 363.22 l.84E+04 1. 77
m 3 55.64 45 - 63 56.12 6.84E+03 382.93 l.85E+04 1. 78
m 4 59.34 45 - 63 59.82 8.68E+04 686.49 l.87E+04 1. 79
5 65.26 65 - 68 65.73 l.28E+03 248.85 l.38E+04 2.56
M 6 84.76 83 - 91 85.22 6.66E+02 204.69 l.06E+04 2.15
m 7 87.94 83 - 91 88.40 2.11E+04 368.89 l.10E+04 1. 60
8 93.62 93 - 97 94.07 6.09E+02 203.08 8.37E+03 1. 64
9 121.93 119 - 126 122.35 2.83E+03 293.69 l.25E+04 1. 88
10 136.49 134 - 140 136.89 3.62E+02 238.83 l.01E+04 1. 86
11 165.23 164 - 168 165.62 l.93E+02 173.82 6.55E+03 1. 63
12 187.80 186 - 191 188.16 l.79E+02 209.68 8.67E+03 3.83
13 238.60 237 - 241 238.92 2.70E+02 173.72 6.43E+03 1. 50
14 352.74 350 - 356 352. 96 l.70E+02 188.04 6.28E+03 1. 87
15 518.37 515 - 521 518.45 l.53E+02 150.58 4.01E+03 3.75
16 639.07 637 - 642 639.06 l.18E+02 114.71 2.55E+03 2.36
M 17 661.79 655 - 672 661.76 2.98E+04 364.88 2.60E+03 1. 94
m 18 666.87 655 - 672 666.84 l.46E+03 334. 72 4.12E+03 3.36
19 1073.55 1070 - 1076 1073.24 l.43E+02 124.02 2.69E+03 4.21
20 1115.79 1112 - 1119 1115.44 l.08E+02 131.85 2.80E+03 3.04
21 1121.26 1119 - 1123 1120.91 7.llE+0l 84.89 l.54E+03 2.09
M 22 1173.53 1167 - 1183 1173.15 2.38E+04 322.27 l.41E+03 2.21
m 23 1178.72 1167 - 1183 1178.33 l.14E+03 222.49 l.68E+03 3.07
M 24 1332.83 1326 - 1343 1332.36 2.17E+04 298.36 3.43E+02 2.32
m 25 1338.00 132 6 - 1343 1337.52 l.08E+03 212.92 2.50E+02 2.98
26 1452.45 144 9 - 1455 1451.91 2.60E+0l 26.14 l.06E+02 3.00
27 1835.51 1831 - 1840 1834.78 2.28E+0l 28.21 l.02E+02 1. 98
M 28 2004.08 2000 - 2013 2003.29 2.58E+0l 16.85 4.18E+0l 3.42
m 29 2011.16 2000 - 2013 2010.37 2.06E+0l 19.18 3.94E+0l 3.43
30 2273.36 2269 - 2277 2272.48 l.77E+0l 21.99 6.47E+0l 2.52
31 2445.44 2441 - 2448 2444.52 7.85E+00 7.48 4.30E+00 3.44
32 2505.69 2499 - 2512 2504.75 3.36E+02 41.55 4.42E+0l 2.85
33 2614.03 2609 - 2 61 7 2613.07 2.05E+0l 11. 85 9.00E+00 1. 44
0151
Analysis Report for 1803111-01
GAS-1402
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 6:13:23AM
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/17/2018 6:13:15AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI ROI Net Peak Net Area Continuum
No. (keV) start end Area Uncertainty Counts
1 31.75 31 - 35 1.51E+03 225.53 9.73E+03
M 2 49.82 45 - 63 6.00E+03 363.22 1.84E+04
m 3 55.64 45 - 63 6.84E+03 382.93 1.85E+04
m 4 59.34 45 - 63 8.68E+04 686.49 1.87E+04
5 65.26 65 - 68 1.28E+03 248.85 1.38E+04
M 6 84.76 83 - 91 6.66E+02 204.69 1.06E+04
m 7 87.94 83 - 91 2.11E+04 368.89 1.10E+04
8 93.62 93 - 97 6.09E+02 203.08 8.37E+03
9 121.93 119 - 126 2.83E+03 293.69 1.25E+04
10 136.49 134 - 140 3.62E+02 238.83 1.01E+04
11 165.23 164 - 168 1.93E+02 17 3. 82 6.55E+03
12 187.80 186 - 191 1.79E+02 209.68 8.67E+03
13 238.60 237 - 241 2.70E+02 173.72 6.43E+03
14 352.74 350 - 356 1.70E+02 188.04 6.28E+03
15 518.37 515 - 521 1.53E+02 150.58 4.01E+03
16 639.07 637 - 642 1.18E+02 114.71 2.55E+03
M 17 661.79 655 - 672 2.98E+04 364.88 2.60E+03
m 18 666.87 655 - 672 1.46E+03 334. 72 4.12E+03
19 1073.55 1070 - 1076 1.43E+02 124.02 2.69E+03
20 1115.79 1112 - 1119 1.08E+02 131.85 2.80E+03
21 1121.26 1119 - 1123 7. llE+0l 84.89 1.54E+03
M 22 1173.53 1167 - 1183 2.38E+04 322.27 1.41E+03
m 23 1178.72 1167 - 1183 1.14E+03 222.49 1.68E+03
M 24 1332.83 1326 - 1343 2.17E+04 298.36 3.43E+02
m 25 1338.00 1326 - 1343 1.08E+03 212.92 2.50E+02
26 1452.45 144 9 - 1455 2.60E+0l 26.14 1.06E+02
27 1835.51 1831 - 1840 2.28E+0l 28.21 1.02E+02
M 28 2004.08 2000 - 2013 2.58E+0l 16.85 4.18E+0l
m 29 2011.16 2000 - 2013 2.06E+0l 19.18 3.94E+0l
30 2273.36 22 69 - 2277 1.77E+0l 21.99 6.47E+0l
31 2445.44 2 441 - 2448 7.85E+00 7.48 4.30E+00
Page 4 of25
Critical Level
1.74E+02 2.23E+02 2.23E+02 2.25E+02 2.51E+02 1.69E+02 l.72E+02 1.62E+02 2.25E+02 1.94E+02 1.41E+02 1. 71E+02 1.40E+02 1.53E+02 1.22E+02 9.26E+0l 8.38E+0l 1.06E+02 1.00E+02 1.07E+02 6.84E+0l 6.17E+0l 6.74E+0l 3.05E+0l 2.60E+0l 1.98E+0l 2.18E+0l 1.06E+0l 1.03E+0l 1.67E+0l 4.08E+00
0152
4/17/2018 6:13:23AM Page 5 of 25
Analysis Report for 1803111-01
M
m m
M m
M
m
GAS-1402
Peak Energy ROI
No. (keV) start
32 2505.69 24 99 -33 2614.03 2 609 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Net Peak Net Area Continuum
end Area Uncertainty Counts
2512 3.36E+02 41. 55 4.42E+0l
2617 2.05E+0l 11.85 9.00E+00
PEAK WITH N/0 REPORT
Peak Analysis Performed on : 4/17/2018 6:13:15AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Tentative NID Library
Peak Match Tolerance
Peak Energy
No. (keV)
1 31.75 2 49.82
3 55.64 4 59.34 5 65.26 6 84.76 7 87.94
8 93.62 9 121.93
10 136.49
11 165.23 12 187.80 13 238.60 14 352.74 15 518.37 16 639.07 17 661.79 18 666.87
: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB
: 1.000 keV
ROI ROI Peak Net Peak
start end Centroid Area
31 - 35 32.26 l.51E+03 45 - 63 50.31 6.00E+03
45 - 63 56.12 6.84E+03 45 - 63 59.82 8.68E+04 65 - 68 65.73 l.28E+03 83 - 91 85.22 6.66E+02 83 - 91 88.40 2. 11E+04
93 - 97 94.07 6.09E+02
119 - 126 122.35 2.83E+03
134 - 140 136.89 3.62E+02
164 - 168 165.62 l.93E+02
186 - 191 188.16 l.79E+02
237 - 241 238.92 2.70E+02
350 - 356 352. 96 l.70E+02
515 - 521 518.45 l.53E+02
637 - 642 639.06 l.18E+02
655 - 672 661.76 2.98E+04
655 - 672 666.84 l.46E+03
Net Area Continuum Uncertainty Counts
225.53 9.73E+03 363.22 l.84E+04
382.93 l.85E+04 686.49 l.87E+04 248.85 l.38E+04 204.69 l.06E+04 368.89 l.10E+04
203.08 8.37E+03 293.69 l.25E+04
238.83 l.01E+04
173.82 6.55E+03 209.68 8.67E+03 173.72 6.43E+03 188.04 6.28E+03 150.58 4.01E+03 114.71 2.55E+03 364.88 2.60E+03 334.72 4.12E+03
Critical Level
l.61E+0l 6.29E+00
Tentative Nuclide
TE-132 TH-227
AM-241
TH-231 CD-109 SN-126 LU-176 GA-67 CO-57 EU-152 SE-75 CO-57 SE-75 CE-139
PB-212 PB-214
CS-137 SB-126
0153
4/17/2018 6:13:23AM
Analysis Report for 1803111-01
M m M m
M m
M m m
M m
GAS-1402
Peak Energy ROI
No. (keV) start
19 1073.55 1070 -20 1115.79 1112 -21 1121.26 1119 -
22 1173.53 1167 -23 1178. 72 1167 -24 1332.83 132 6 -25 1338.00 1326 -26 1452.45 14 4 9 -27 1835.51 1831 -28 2004.08 2000 -29 2011.16 2000 -30 2273.36 22 69 -31 2445.44 2441 -32 2505.69 24 99 -33 2614.03 2 60 9 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area
end Centroid Area Uncertainty
1076 1073.24 1.43E+02 124.02 1119 1115.44 1.08E+02 131.85 1123 1120.91 7.llE+0l 84.89
1183 1173.15 2.38E+04 322.27
1183 1178.33 1.14E+03 222.49
1343 1332.36 2.17E+04 298.36 1343 1337.52 l.08E+03 212.92
1455 1451.91 2.60E+0l 26.14 1840 1834.78 2.28E+0l 28.21 2013 2003.29 2.58E+0l 16.85 2013 2010.37 2.06E+0l 19.18 2277 2272.48 l.77E+0l 21.99 2448 2444.52 7.85E+00 7.48 2512 2504.75 3.36E+02 41.55 2617 2613.07 2.05E+0l 11. 85
PEAK EFFICIENCY REPORT
Peak Analysis Performed on : 4/17/2018 6:13:15AM
Peak Energy Net Peak Net Area Peak
No. (keV) Area Uncertainty Efficiency
1 31.75 l.51E+03 225.53 l.00E-02
2 49.82 6.00E+03 363.22 2.14E-02
3 55.64 6.84E+03 382.93 2.38E-02
4 59.34 8.68E+04 686.49 2.49E-02
5 65.26 l.28E+03 248.85 2.63E-02
6 84.76 6.66E+02 204.69 2.84E-02
7 87.94 2 .11E+04 368.89 2.85E-02
8 93.62 6.09E+02 203.08 2.85E-02
9 121.93 2.83E+03 293.69 2.73E-02
10 136.49 3.62E+02 238.83 2.63E-02
11 165.23 l.93E+02 173.82 2.43E-02
12 187.80 l.79E+02 209.68 2. 27E-02
13 238.60 2.70E+02 173.72 l.97E-02
Page 6 of25
Continuum Tentative Counts Nuclide
2.69E+03 2.80E+03 ZN-65 1.54E+03 TA-182
SC-46 BI-214
1.41E+03 CO-60 l.68E+03 3.43E+02 CO-60 2.50E+02 l.06E+02 l.02E+02 Y-88 4.18E+0l 3.94E+0l 6.47E+0l 4.30E+00 4.42E+0l 9.00E+00 TL-208
Efficiency Uncertainty
l.85E-03 l.85E-03 l.85E-03 l.85E-03 l.96E-03 2.35E-03 2.41E-03 2.38E-03 2.21E-03 2.45E-03 2.94E-03 2.88E-03 2.70E-03
0154
4/17/2018 6:13:23AM Page 7 of25
Analysis Report for 1803111-01
M m
M m M m
M m
M m m
M m
GAS-1402
Peak Energy Net Peak Net Area Peak Efficiency
No. (keV) Area Uncertainty Efficiency Uncertainty
14 352.74 1.70E+02 188.04 1.51E-02 2.30E-03
15 518.37 1.53E+02 150.58 1.13E-02 1.56E-03
16 639.07 l.18E+02 114. 71 9.59E-03 9.84E-04
17 661.79 2.98E+04 364.88 9.33E-03 8. 77E-04
18 666.87 1.46E+03 334. 72 9.27E-03 8.85E-04
19 1073.55 1.43E+02 124.02 6.34E-03 7.73E-04
20 1115.79 1.08E+02 131.85 6.15E-03 6.65E-04
21 1121.26 7.llE+0l 84.89 6.12E-03 6.51E-04
22 1173.53 2.38E+04 322.27 5.91E-03 5.18E-04
23 1178.72 1.14E+03 222.49 5.89E-03 5,17E-04
24 1332.83 2.17E+04 298.36 5.35E-03 4.71E-04
25 1338.00 1.08E+03 212.92 5.33E-03 4. 71E-04
26 1452.45 2.60E+0l 26.14 5.0lE-03 4.72E-04
27 1835.51 2.28E+0l 28.21 4.23E-03 4. 77E-04
28 2004.08 2.58E+0l 16.85 3.99E-03 4. 77E-04
29 2011.16 2.06E+0l 19.18 3.98E-03 4.77E-04
30 2273.36 1.77E+0l 21.99 3.69E-03 4. 77E-04
31 2445.44 7.85E+00 7.48 3.54E-03 4. 77E-04
32 2505.69 3.36E+02 41. 55 3.50E-03 4. 77E-04·
33 2614.03 2.05E+0l 11. 85 3.42E-03 4. 77E-04
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000 sigma
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on
Env. Background File
Peak Energy
No. (keV)
1 31.75 2 49.82 3 55.64 4 59.34 5 65.26 6 84.76 7 87.94 8 93.62 9 121.93
10 136.49
: 4/17/2018 6:13:15AM
: \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000063824.CNF
Original Orig. Area Ambient Backgr. Subtracted Subtracted
Area Uncertainty Background Uncert. Area Uncert.
l.51E+03 225.53 l.51E+03 2.26E+02
6.00E+03 363.22 6.00E+03 3.63E+02
6.84E+03 382.93 6.84E+03 3.83E+02
8.68E+04 686.49 8.68E+04 6.86E+02
1.28E+03 248.85 1.28E+03 2. 4 9E+02
6.66E+02 204.69 5.20E+00 1.31E+00 6.60E+02 2.05E+02
2. 11E+04 368.89 1.93E+00 1.15E+00 2.11E+04 3.69E+02
6.09E+02 203.08 6.09E+02 2.03E+02
2.83E+03 293.69 2.83E+03 2.94E+02
3.62E+02 238.83 3.62E+02 2.39E+02
0155
4/17/2018 6:13:23AM Page 8 of25
Analysis Report for 1803111-01
GAS-1402
Peak Energy Original Orig. Area Ambient Backgr. Subtracted
No. (keV) Area Uncertainty Background Uncert. Area
11 165.23 1.93E+02 173.82 1.93E+02
12 187.80 1.79E+02 209.68 1.79E+02
13 238.60 2.70E+02 173.72 1.05E+0l 3.06E+00 2.59E+02
14 352.74 1.70E+02 188.04 3.23E+00 2.56E+00 1.67E+02
15 518.37 1.53E+02 150.58 1.53E+02
16 639.07 1.18E+02 114. 71 1.18E+02
M 17 661.79 2.98E+04 364.88 2.98E+04
m 18 666.87 1.46E+03 334. 72 1.46E+03
19 1073.55 1.43E+02 124.02 1.43E+02
20 1115.79 1.08E+02 131.85 1.08E+02
21 1121.26 7.llE+0l 84.89 7.llE+0l
M 22 1173.53 2.38E+04 322.27 2.38E+04
m 23 1178.72 1.14E+03 222.49 1.14E+03
M 24 1332.83 2.17E+04 298.36 2.17E+04
m 25 1338.00 1.08E+03 212.92 1.08E+03
26 1452.45 2.60E+0l 26.14 2.60E+0l
27 1835.51 2.28E+0l 28.21 2.28E+0l
M 28 2004.08 2.58E+0l 16.85 2.58E+0l
m 29 2011.16 2.06E+0l 19.18 2.06E+0l
30 2273.36 1.77E+0l 21.99 1.77E+0l
31 2445.44 7.85E+00 7.48 7.85E+00
32 2505.69 3.36E+02 41. 55 3.36E+02
33 2614.03 2.05E+0l 11. 85 2.50E+00 8.43E-01 1.80E+0l
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
AREA CORRECTION REPORT REFERENCEPEAKIBKG.SUBTRACT
Peak Analysis Performed on
Ref. Peak Energy
Peak Ratio
: 4/17/2018 6:13:15AM
: 0.00 Reference Date
: 0.00 Uncertainty : 0.00
Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CN F
Corrected Area is: Original * Peak Ratio - Background
Peak Energy Original Orig. Area Ambient Backgr.
No. (keV) Area Uncertainty Background Uncert.
1 31.75 1.51E+03 225.53
M 2 49.82 6.00E+03 363.22
m 3 55.64 6.84E+03 382.93
m 4 59.34 8.68E+04 686.49
5 65.26 1.28E+03 248.85
Corrected Area
1.51E+03 6.00E+03 6.84E+03 8.68E+04 1.28E+03
Subtracted Uncert.
1.74E+02 2.10E+02 1.74E+02 1.88E+02 1.51E+02 1.15E+02 3.65E+02 3.35E+02 l.24E+02 1.32E+02 8.49E+0l 3.22E+02 2.22E+02 2.98E+02 2.13E+02 2.61E+0l 2.82E+0l 1.69E+0l 1.92E+0l 2.20E+0l 7.48E+00 4.15E+0l 1.19E+0l
Corrected Uncert.
2.26E+02 3.63E+02 3.83E+02 6.86E+02 2.49E+02
0156
4/17/2018 6:13:23AM Page 9 of25
Analysis Report for 1803111-01
GAS-1402
Peak Energy Original Orig. Area Ambient Backgr. Corrected Corrected
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
M 6 84.76 6.66E+02 204.69 5.20E+00 1.31E+00 6.60E+02 2.05E+02
m 7 87.94 2.11E+04 368.89 1.93E+00 1.15E+00 2.11E+04 3.69E+02
8 93.62 6.09E+02 203.08 6.09E+02 2.03E+02
9 121. 93 2.83E+03 293.69 2.83E+03 2.94E+02
10 136.49 3.62E+02 238.83 3.62E+02 2.39E+02
11 165.23 l.93E+02 173.82 1.93E+02 1.74E+02
12 187.80 1.79E+02 209.68 l.79E+02 2.10E+02
13 238.60 2.70E+02 173.72 1.05E+0l 3.06E+00 2.59E+02 1.74E+02
14 352.74 1.70E+02 188.04 3.23E+00 2.56E+00 l.67E+02 1.88E+02
15 518.37 1.53E+02 150.58 1.53E+02 l.51E+02
16 639.07 1.18E+02 114.71 1.18E+02 1.15E+02
M 17 661.79 2.98E+04 364.88 2.98E+04 3.65E+02
m 18 666.87 1.46E+03 334. 72 l.46E+03 3.35E+02
19 1073.55 1.43E+02 124.02 1.43E+02 1.24E+02
20 1115.79 l.08E+02 131.85 1.08E+02 1.32E+02
21 1121.26 7. llE+0l 84.89 7.llE+0l 8.49E+01
M 22 1173.53 2.38E+04 322.27 2.38E+04 3.22E+02
m 23 1178.72 l.14E+03 222.49 l.14E+03 2.22E+02
M 24 1332.83 2.17E+04 298.36 2.17E+04 2.98E+02
m 25 1338.00 l.08E+03 212. 92 l.08E+03 2.13E+02
26 1452.45 2.60E+0l 26.14 2.60E+0l 2.61E+0l
27 1835.51 2.28E+0l 28. 21 2.28E+0l 2.82E+0l
M 28 2004.08 2.58E+0l 16.85 2.58E+0l 1.69E+0l
m 29 2011.16 2.06E+0l 19.18 2.06E+0l 1.92E+01
30 2273.36 1.77E+0l 21. 99 1.77E+0l 2.20E+01
31 2445.44 7.85E+00 7.48 7.85E+00 7.48E+00
32 2505.69 3.36E+02 41.55 3.36E+02 4.15E+01
33 2614.03 2.05E+0l 11. 85 2.50E+00 8.43E-0l 1.80E+0l 1.19E+0l
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \ \0 R-GAM MA 1 \Apex Root\Cou ntroom\Library\ TMA2. NLB
IDENTIFIED NUCLIDES
Nuclide Name Id Confidence Energy (keV) Yield(¾) Activity Activity
(pCilgrams) Uncertainty
CO-57 0.890 122.06 * 85.51 6.78E+0l 8.92E+00
136.48 * 10.60 7.26E+01 4.83E+0l
CO-60 0.980 1173.22 * 100.00 1.31E+02 1.17E+0l
0157
Analysis Report for 1803111-01
GAS-1402
Nuclide Name Id Confidence
CO-60 0.980 ZN-65 0.859 CD-109 0. 961 SN-126 0.978 CS-137 0.997 CE-139 0.605 PB-212 0.894
PB-214 0.365
AM-241 0.994
* == Energy line found in the spectrum.
- == Manually added nuclide.
? == Manually edited nuclide.
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold == 0.30
Errors quoted at 2.000sigma
4/17/2018 6:13:23AM
Energy (keV) Yield(%) Activity
(pCi/grams)
1332.49 * 100.00 1.32E+02
1115.52 * 50.75 2.76E+0l
88.03 * 3. 72 2.80E+03
87.57 * 37.00 4.08E+0l
661.65 * 85.12 8.31E+0l
165.85 * 80.35 1.37E+02
238.63 * 44.60 6.02E-01
300.09 3.41 295.21 19.19 351.92 * 37.19 6.06E-01
59.54 * 35.90 1.99E+02
UNIDENTIFIED PEAKS
M
m
M
m
m m
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
1 31.75 2 49.82
3 55.64 5 65.26 6 84.76 8 93.62
12 187.80 15 518.37 16 639.07 18 666.87 19 1073.55 21 1121.26
23 1178.72 25 1338.00 26 1452.45
: 4/17/2018 6:13:15AM
: 1 : 4096
Peak Size (CPS)
8.36269E-01 3.33603E+00
3.80080E+00 7.12556E-01 3.66911E-01 3.38259E-0l 9.93056E-02 8.49036E-02 6. 57231E-02 8.11195E-01 7.92306E-02 3.95080E-02
6.35087E-01 5.98856E-01 1.44374E-02
Peak CPS(%) Uncertainty
7.49 3.02
2.80 9.70
15.50 16.68 58.65 49.27 48.48 11. 4 6 43.48 59.68
9.73 9.88
50.30
Peak Type
Tol.
Tol. D-Esc
Sum
Tol.
Tol.
Sum
Page 10 of25
Activity
Uncertainty
1.18E+0l 3.39E+0l 2.43E+02 3.53E+00 7.88E+00 l.24E+02 4. llE-01
6.90E-01 l.49E+0l
Tolerance Nuclide
TE-132 TH-227
TH-231
SB-126
SC-46 TA-182 BI-214
0158
Analysis Report for 1803111-01
M m
GAS-1402
Peak No. Energy (keV)
27 1835.51 28 2004.08 29 2011.16 30 2273.36 31 2445.44 32 2505.69 33 2614.03
M = First peak in a multiplet region
m = other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
Peak Size (CPS)
1.26426E-02 l.43245E-02 1.14191E-02 9. 81111E-03 4. 36111E-03 1.86598E-01 l.00000E-02
4/17/2018 6:13:23AM
Peak CPS(%) Peak
Uncertainty Type
61.99 Sum 32.68 46.66 62. 2 6 47.66
6.18 Sum 33.01 Tol.
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(¾) Activity
Page 11 of25
Tolerance
Nuclide
TL-208
Activity
Name Confidence (keV) (pCilgrams) Uncertainty
CO-57 0.89 122.06 * 85.51 6.78E+0l 8.92E+00
136.48 * 10.60 7.26E+0l 4.83E+0l
CO-60 0.98 1173.22 * 100.00 l.31E+02 1.17E+0l
1332.49 * 100.00 1.32E+02 1.18E+0l
ZN-65 0.85 1115.52 * 50.75 2.76E+0l 3.39E+0l
CD-109 0. 96 88.03 * 3. 72 2.80E+03 2.43E+02
SN-126 0.97 87.57 * 37.00 4.08E+0l 3.53E+00
CS-137 0.99 661.65 * 85.12 8.31E+0l 7.88E+00
CE-139 0.60 165.85 * 80.35 1.37E+02 1. 2 4E+02
PB-212 0.89 238.63 * 44.60 6.02E-01 4.llE-01
300.09 3.41
PB-214 0.36 295.21 19.19 351.92 * 37.19 6.06E-01 6.90E-01
AM-241 0.99 59.54 * 35.90 1.99E+02 1.49E+0l
0159
Analysis Report for 1803111-01
GAS-1402
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
4/17/2018 6:13:23AM
INTERFERENCE CORRECTED REPORT
Nuclide Name
CO-57 CO-60 ZN-65
? CD-109 ? SN-126
CS-137 CE-139 PB-212 PB-214 AM-241
Nuclide Id
Confidence
0.890 0.980 0.859 0. 961 0.978 0.997 0.605 0.894 0.365 0.994
? X
= =
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
Wt mean Activity
(pCilgrams)
6.79E+0l 1.32E+02 2.76E+0l 2.80E+03 4.08E+0l 8.31E+0l 1.37E+02 6.02E-0l 6.06E-0l 1.99E+02
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Wt mean Activity
Uncertainty
8.77E+00 8.28E+00 3.39E+0l 2.43E+02 3.53E+00 7.88E+00 1.24E+02 4. llE-01 6.90E-01 1.49E+0l
Page 12 of25
Comments
0160
Analysis Report for 1803111-01
M
m
M
m
m m
M
m
GAS-1402
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
1 31.75
2 49.82
3 55.64
5 65.26
6 84.76
8 93.62
12 187.80
15 518.37
16 639.07
18 666.87
19 1073.55
21 1121.26
23 1178.72
25 1338.00
26 1452.45
27 1835.51
28 2004.08
29 2011.16
30 2273.36
31 2445.44
32 2505.69
33 2614.03
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 6:13:23AM
UNIDENTIFIED PEAKS
: 4/17/2018 6:13:15AM
: 1 : 4096
Peak Size (CPS)
8.36269E-01
3.33603E+00
3.80080E+00
7.12556E-01
3.66911E-01
3.38259E-01
9.93056E-02
8.49036E-02
6.57231E-02
8. 11195E-01
7.92306E-02
3.95080E-02
6.35087E-01
5.98856E-01
1.44374E-02
1.26426E-02
1.43245E-02
l.14191E-02
9. 81111E-03
4. 36111E-03
1.86598E-01
1.00000E-02
Peak CPS(%) Peak
Uncertainty Type
7.49 3.02 Tol.
2.80 9.70
15.50 Tol.
16.68 D-Esc
58.65 49.27 Sum
48.48
11. 46 Tol.
43.48
59.68 Tol.
9.73 9.88 Sum
50.30 61.99 Sum
32.68 46.66
62.26 47.66
6.18 Sum
33.01 Tol.
Page 13 of25
Tolerance Nuclide
TE-132
TH-227
TH-231
SB-126
SC-46 TA-182
BI-214
TL-208
0161
4/17/2018 6:13:23AM Page 14 of25
Analysis Report for 1803111-01
GAS-1402
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)
+ BE-7 477.59 10.42 -6.60E+05 8.02E+07 8.02E+07
+ NA-22 1274.54 99.94 -4.74E-03 6.79E-01 6.79E-01
+ NA-24 1368.53 99.99 -5.46E-02 7.35E-02 1.78E-01
2754.09 99.86 2.45E-02 7.35E-02
+ AL-26 1808.65 99.76 -1.20E-03 1.73E-01 1.73E-01
+ K-40 1460.81 10.67 1.26E+00 l.90E+00 1.90E+00
+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26
+ TI-44 67,88 94.40 1.68E-01 3.07E-01 3.62E-01
78.34 96.00 1.33E-02 3.07E-01
+ SC-46 889.25 98.98 -l.81E+03 2.42E+04 2.49E+04
1120.51 99.90 -1.44E+04 2.42E+04
+ @ V-48 983.52 99.98 1.00E+26 1.00E+26 1.00E+26
@ 1312 .10 97.50 1.00E+26 1.00E+26
+ CR-51 320.08 9.83 5.43E+13 3.96E+14 3.96E+14
+ MN-54 834.83 99.97 2.17E+00 8.79E+00 8.79E+00
+ CO-56 846.75 99. 96 5.34E+04 1.12E+05 1.77E+05
1037.75 14.03 6.00E+05 1.38E+06
1238.25 67.00 2.30E+04 1.51E+05
1771.40 15.51 -3.26E+04 4 .11E+05
2587.48 16.90 -3.00E+04 1.12E+05
+ CO-57 122.06 * 85.51 6.78E+0l 1.08E+0l 1.08E+0l
136.48 * 10.60 7.26E+0l 7.82E+0l
+ CO-58 810.76 99.40 -1.28E+05 1.48E+05 1.48E+05
+ FE-59 1099.22 56.50 -1.22E+08 3.16E+08 5.58E+08
1291.56 43.20 1.43E+07 3.16E+08
+ CO-60 1173.22 * 100.00 1.31E+02 9.45E-01 1.63E+00
1332.49 * 100.00 1.32E+02 9.45E-01
+ ZN-65 1115. 52 * 50.75 2.76E+0l 5.56E+0l 5.56E+0l
+ @ GA-67 93.31 35.70 1.00E+26 1.00E+26 1.00E+26
@ 208.95 2.24 1.00E+26 1.00E+26
@ 300.22 16.00 1.00E+26 1.00E+26
+ SE-75 121. 11 16.70 2.25E+04 6.92E+02 3.06E+03
136.00 59.50 1.24E+03 6.92E+02
264.65 59.80 -5.67E+0l 9.74E+02
27 9. 53 25.20 1.33E+03 2.33E+03
400.65 11. 40 2.19E+03 6.07E+03
+ RB-82 776.52 13.00 -8.34E+14 5.97E+15 5.97E+l5
+ RB-83 520.41 46.00 -1.15E+03 2.83E+04 2.83E+04
529.64 30.30 -2.39E+04 4.17E+04
552.65 16.40 9.53E+03 7.58E+04
+ KR-85 513.99 0.43 7.43E+0l 1.16E+02 1.16E+02
+ SR-85 513.99 99.27 2.63E+05 4.10E+05 4.10E+05
0162
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Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)
+ Y-88 898.02 93.40 1.78E+03 8.47E+02 2.76E+03
1836.01 99.38 6.12E+02 8.47E+02
+ MO-93 263.06 56.72 8.80E-02 2.24E-01 7.23E-01
684.67 99.68 -8.70E-02 4.96E-01
1477.11 99.08 -2.71E-03 2.24E-01
+ NB-93M 16.57 9.43 -1.83E+09 1.11E+09 1.11E+09
+ NB-94 702.63 100.00 -9.89E-02 4.02E-01 4.02E-01
871.10 100.00 -1.05E-01 5.30E-01
+ NB-95 765.79 99.81 -3.33E+10 5.57E+10 5.57E+10
+ @ NB-95M 235.69 25.00 1.00E+26 1.00E+26 1.00E+26
+ ZR-95 724.18 43.70 -5.26E+05 9.47E+05 1.13E+06
756.72 55.30 -3.08E+05 9.47E+05
+ @ MO-99 181.06 6.20 1.00E+26 1.00E+26 1.00E+26
@ 739.58 12.80 1.00E+26 l.00E+26
@ 778.00 4.50 1.00E+26 1.00E+26
+ TC-99M 140.51 89.00 4.46E-03 2.46E-01 2.46E-01
+ RU-103 497.08 89.00 1.48E+08 3.54E+09 3.54E+09
+ RU-106 621. 84 9.80 -2.02E+0l 4.58E+0l 4.58E+0l
+ AG-108M 433.93 89.90 -4.79E-0l 4.48E-01 4.65E-0l
614.37 90.40 -1.06E-01 4.48E-01
722.95 90.50 -2.22E-02 4.58E-01
+ CD-109 88.03 * 3. 72 2.80E+03 7.45E+0l 7.45E+0l
+ AG-ll0M 657.75 93.14 -3.12E+02 2.75E+0l 4.44E+0l
677.61 10.53 -2.65E+0l 1.36E+02
706.67 16.46 -1.06E+0l 8.93E+0l
763.93 21.98 1. 96E+0l 7.22E+0l
884.67 21. 98 -1.77E+0l 9.00E+0l
1384.27 23.94 -5.88E+00 2.75E+0l
+ CD-113M 263.70 0.02 2.73E+02 1.69E+03 1.69E+03
+ SN-113 255.12 1. 93 -8.10E+03 1.43E+03 3.41E+04
391.69 64.90 3.25E+02 1.43E+03
+ TE-123M 159.00 84.10 2.37E+02 4.86E+02 4.86E+02
+ SB-124 602.71 97.87 -5.79E+05 1.04E+06 1.16E+06
645.85 7.26 -2.26E+06 1.63E+07
722. 7 8 11.10 -5.24E+05 1.08E+07
1691.02 49.00 -2.19E+05 1.04E+06
+ I-125 35.49 6.49 2.92E+07 2.37E+07 2.37E+07
+ SB-125 176.33 6.89 -4.12E+00 3.38E+00 8.l0E+00
427.89 29.33 1.29E-01 3.38E+00
463.38 10.35 5.46E+00 1.07E+0l
600.56 17.80 -1.68E+00 5.25E+00
635.90 11. 32 -1.94E+00 8.51E+00
+ SB-126 414.70 83.30 -2.42E-0l 3.96E-01 4.74E-01
666.33 99.60 -2.0lE+0l 9.07E-01
695.00 99.60 -1.07E-01 3.96E-01
720.50 53.80 1.22E-01 7.60E-01
+ SN-126 87.57 * 37.00 4.08E+0l 1.08E+00 1.08E+00
+ @ SB-127 473.00 25.00 l.00E+26 1.00E+26 1.00E+26
0163
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Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi!grams) (pCi!grams) (pCi!grams)
@ SB-127 685.00 35.70 l.00E+26 l.00E+26 l.00E+26
@ 783.80 14.70 l.00E+26 l.00E+26
+ I-129 29.78 57.00 -2.14E+00 l.70E+00 l.70E+00
33.60 13.20 l.83E+00 4. 96E+00
39.58 7.52 -2.46E+0l 6.06E+00
+ @ I-131 284.30 6.05 l.00E+26 l.00E+26 l.00E+26
@ 364.48 81.20 l.00E+26 l.00E+26
@ 636.97 7.26 l.00E+26 l.00E+26
@ 722.89 1. 80 l.00E+26 l.00E+26
+ @ TE-132 49.72 13.10 l.00E+26 l.00E+26 l.00E+26
@ 228.16 88.00 l.00E+26 l.00E+26
+ BA-133 81.00 33.00 -4.40E-01 7.58E-01 l.07E+00
302.84 17.80 -l.50E+00 2.33E+00
356.01 60.00 7.74E-03 7.58E-01
+ @ I-133 529.87 86.30 l.00E+26 l.00E+26 l.00E+26
+ @ XE-133 81.00 38.00 l.00E+26 l.00E+26 l.00E+26
+ CS-134 563.23 8.38 3.52E+00 l.31E+00 l.51E+0l
569.32 15.43 l.60E+00 8.24E+00
604.70 97.60 -l.25E-01 l.31E+00
795.84 85.40 5.64E-01 l.79E+00
801.93 8.73 -8.20E+00 l.76E+0l
+ CS-135 268.24 16.00 6.87E-01 2.04E+00 2.04E+00
+ @ I-135 1131.51 22.50 l.00E+26 l.00E+26 l.00E+26
@ 1260.41 28.60 l.00E+26 l.00E+26
@ 1678.03 9.54 l.00E+26 l.00E+26
+ @ CS-136 153.22 7.46 l.00E+26 l.00E+26 l.00E+26
@ 163.89 4.61 l.00E+26 l.00E+26
@ 176.55 13.56 l.00E+26 l.00E+26
@ 273.65 12.66 l.00E+26 l.00E+26
@ 340.57 48.50 l.00E+26 l.00E+26
@ 818.50 99.70 l.00E+26 l.00E+26
@ 1048.07 79.60 l.00E+26 l.00E+26
@ 1235.34 19.70 l.00E+26 l.00E+26
+ CS-137 661.65 * 85.12 8.31E+0l l.27E+00 l.27E+00
+ LA-138 788.74 34.00 2.32E-01 2.76E-01 l.32E+00
1435.80 66.00 2.81E-02 2.76E-01
+ CE-139 165.85 * 80.35 l.37E+02 2.02E+02 2.02E+02
+ @ BA-140 162.64 6.70 l.00E+26 l.00E+26 l.00E+26
@ 304.84 4.50 l.00E+26 l.00E+26
@ 423.70 3.20 l.00E+26 l.00E+26
@ 437.55 2.00 l.00E+26 l.00E+26
@ 537.32 25.00 l.00E+26 l.00E+26
+ @ LA-140 328.77 20.50 l.00E+26 l.00E+26 l.00E+26
@ 487.03 45.50 l.00E+26 l.00E+26
@ 815.85 23.50 l.00E+26 l.00E+26
@ 1596.49 95.49 l.00E+26 l.00E+26
+ CE-141 145.44 48.40 2.66E+ll 4.47E+ll 4.47E+ll
+ @ CE-143 57.36 11.80 l.00E+26 l.00E+26 l.00E+26
0164
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Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)
@ CE-143 293.26 42.00 1.00E+26 1.00E+26 1.00E+26
@ 664.55 5.20 1.00E+26 1.00E+26
+ CE-144 133.54 10.80 -8.05E-01 4.78E+0l 4.78E+0l
+ PM-144 476.78 42.00 1.60E+00 4.74E+00 1.23E+0l
618.01 98.60 -3.15E-01 4.76E+00
696. 4 9 99.49 4.24E-01 4:74E+00
+ PM-145 36.85 21. 70 1.99E+00 1.41E+00 2.57E+00
37.36 39.70 6.18E-01 1.41E+00
42.30 15.10 -3.07E+00 3.68E+00
72.40 2.31 -6.58E+00 1.42E+0l
+ PM-146 453.90 39.94 8.19E-01 1.73E+00 1.73E+00
735.90 14.01 1.90E+00 4.77E+00
747.13 13. 10 2.80E+00 5.17E+00
+ @ ND-147 91.11 28.90 1.00E+26 1.00E+26 l.00E+26
@ 531.02 13.10 1.00E+26 1.00E+26
+ @ PM-149 285.90 3.10 1.00E+26 l.00E+26 1.00E+26
+ EU-152 121.78 20.50 1.23E+0l 1.55E+00 l.68E+00
244.69 5.40 3.76E+00 6.21E+00
344.27 19.13 -1.18E+00 2.16E+00
778.89 9.10 9.48E-01 5.93E+00
964.01 10.40 1.15E+00 7.03E+00
1085.78 7.22 -6.52E-01 9.71E+00
1112.02 9.60 3.26E-01 7.25E+00
1407.95 14. 94 1.88E-01 1.55E+00
+ GD-153 97.43 31.30 6.84E-01 2.70E+0l 2.70E+0l
103.18 22.20 5.77E+00 3.86E+0l
+ EU-154 123.07 40.50 6.57E+00 9.35E-01 9.35E-01
723.30 19.70 -l.32E-01 2.73E+00
873.19 11.50 -1.12E+00 6.15E+00
996. 32 10.30 -2.76E-01 7.40E+00
1004.76 17.90 -4.28E-01 4.28E+00
1274.45 35.50 -6.86E-03 9.84E-01
+ EU-155 86.50 30.90 7.66E+0l 1.65E+00 2.91E+00
105.30 20.70 7.67E-02 1.65E+00
+ @ EU-156 811.77 10.40 l.00E+26 1.00E+26 l.00E+26
@ 1153.47 7.20 l.00E+26 1.00E+26
@ 1230.71 8.90 1.00E+26 1.00E+26
+ HO-166M 184.41 72. 60 -1.02E-01 3.45E-01 3.45E-01
280.45 29.60 4.66E-01 1. llE+00
410.94 11.10 7.50E-01 3.60E+00
711.69 54.10 -1.97E-01 7.62E-01
+ TM-171 66. 72 0.14 2.77E+03 9.01E+02 9.01E+02
+ HF-1 72 67.35 5.31 1.07E+0l 7.32E+00 2.31E+0l
125.82 11. 30 -1.42E+00 7.32E+00
+ @ LU-1 72 181.53 20.60 1.00E+26 1.00E+26 l.00E+26
@ 900.72 29.81 1.00E+26 l.00E+26
@ 1093.66 62.50 1.00E+26 l.00E+26
+ LU-173 100.72 5.24 7.97E+00 9.26E+00 2.39E+0l
272 .11 21.20 1.94E+00 9.26E+00
0165
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Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)
+ HF-175 343.40 84.00 -8.18E+04 l.50E+05 l.50E+05
+ LU-176 88.34 13. 30 l.09E+02 3.03E-01 4.08E+00
201.83 86.00 -2.04E-02 3.03E-01
306.78 94.00 -l.35E-01 3.55E-01
+ HF-181 133.02 41.70 -9.45E+07 7.76E+08 8.03E+08
345.85 17.20 9.27E+08 3.18E+09
482.03 82.80 l.19E+08 7.76E+08
+ TA-182 67.75 41.20 9.39E+02 2.02E+03 2.02E+03
1121.30 34.90 -l.74E+03 3.91E+03
1189.05 16.23 -7.74E+02 6.44E+03
1221. 41 26.98 -9.39E+02 3.09E+03
1231.02 11. 44 -l.37E+03 6.85E+03
+ IR-192 308.46 29.68 l.73E+05 l.72E+05 2.09E+05
468.07 48.10 5.68E+03 l.72E+05
+ HG-203 279.19 77.30 -l.68E+07 9.67E+07 9.67E+07
+ TL-204 374.74 94. 11 8.04E-02 7.42E-01 7.42E-01
899.15 99.16 9.53E-02 l.l0E+00
911. 7 4 91.10 5.73E-01 l.24E+00
+ BI-207 569.67 97. 72 4.53E-03 4.23E-01 4.23E-01
1063.62 74.90 -4.12E-01 8.13E-01
+ TL-208 583.14 30.22 l.07E+00 4.40E-01 l.31E+00
860.37 4.48 l.53E+00 l.17E+0l
2614.66 35.85 4.05E-01 4.40E-01
+ BI-210M 262.00 45.00 6.37E-02 7.27E-0l 7.27E-0l
300.00 23.00 6.83E-01 l.45E+00
+ PB-210 46.50 4.25 -9.55E+0l l.46E+0l l.46E+0l
+ PB-211 404.84 2.90 -7.04E+00 l.33E+0l l.33E+0l
831.96 2.90 l.15E+0l l.72E+0l
+ BI-212 727.17 11. 80 4.65E-01 3.54E+00 3.54E+00
1620.62 2.75 -l.36E+00 6.12E+00
+ PB-212 238.63 * 44.60 6.02E-01 6.58E-01 6.58E-01
300.09 3.41 4.61E+00 9.80E+00
+ BI-214 609.31 46.30 l.03E-02 8.58E-01 8.58E-01
1120.29 15.10 -2.15E+00 3.62E+00
1764.49 15.80 5.83E-01 l.23E+00
2204.22 4.98 -1.0lE+00 3.78E+00
+ PB-214 295.21 19.19 5.19E-01 l.12E+00 l.74E+00
351.92 * 37.19 6.06E-01 l.12E+00
+ RN-219 401.80 6.50 -l.97E+00 5.94E+00 5.94E+00
+ RA-223 323.87 3.88 -4.12E+00 8.76E+00 8.76E+00
+ RA-224 240.98 3.95 -l.29E+00 7.14E+00 7.14E+00
+ @ RA-225 40.00 31.00 l.00E+26 l.00E+26 l.00E+26
+ RA-226 186.21 3.28 l.33E+00 7.80E+00 7.80E+00
+ TH-227 50.10 8.40 3.43E+0l 2.46E+00 7.96E+00
236.00 11. 50 -8.66E-02 2.46E+00
256.20 6.30 -3.44E-01 5.14E+00
+ AC-228 338.32 11. 40 -l.37E+00 2.14E+00 2.99E+00
911. 07 27.70 l.16E+00 2.14E+00
0166
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Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)
AC-228 969 .11 16.60 -2.31E-01 2.14E+00 3.55E+00
+ TH-230 48.43 16.90 1.41E+0l 3.76E+00 3.76E+00
62.85 4.60 -6.15E+02 1.25E+0l
67.67 0.37 4.13E+0l 8.89E+0l
+ PA-231 283.67 1.60 1.87E+00 1.43E+0l 2.05E+0l
302.67 2.30 -9.16E+00 1.43E+0l
+ TH-231 25.64 14.70 -2.57E+02 4.92E+00 2.02E+0l
84.21 6.40 -2.50E+02 4.92E+00
+ PA-233 311.98 38.60 8.14E+13 2.36E+l4 2.36E+14
+ PA-234 131.20 20.40 -8.62E-02 1.06E+00 1.06E+00
733.99 8.80 -2.41E-01 4.87E+00
946.00 12.00 -7.02E-01 5.26E+00
+ PA-234M 1001.03 0.92 -5.20E-01 6.28E+0l 6.28E+0l
+ TH-234 63.29 3.80 -5.92E+02 1.0lE+0l 1.0lE+0l
+ U-235 143.76 10.50 2.64E-01 2.12E+00 2.12E+00
163.35 4.70 -1.42E+00 4.90E+00
205.31 4.70 -2.91E+00 5.55E+00
+ NP-237 86.50 12.60 1.15E+02 4.36E+00 4.36E+00
+ @ NP-239 106.10 22.70 l.00E+26 l.00E+26 1.00E+26
@ 228.18 10.70 l.00E+26 l.00E+26
@ 277.60 14.10 l.00E+26 1.00E+26
+ AM-241 59.54 * 35.90 l.99E+02 3.18E+00 3.18E+00
+ AM-243 74.67 66.00 2.77E-01 4.33E-01 4.33E-0l
+ CM-243 209.75 3.29 -3.05E+00 2.55E+00 8.89E+00
228.14 10.60 2. llE+00 2.94E+00
277. 60 14.00 -3.99E-01 2.55E+00
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
0167
4/17/2018 6:13:23AM Page 20 of25
Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCilgrams)
BE-7 477.59 10.42 8.02E+07 8.02E+07 -6.60E+05 3.97E+07
NA-22 1274.54 99.94 6.79E-0l 6.79E-01 -4.74E-03 3.27E-01
NA-24 1368.53 99.99 1.78E-01 7.35E-02 -5.46E-02 8.40E-02
2754.09 99.86 7.35E-02 2.45E-02 2.85E-02
AL-26 1808.65 99.76 1.73E-01 1.73E-01 -1.20E-03 8.02E-02
K-40 1460.81 10.67 1.90E+00 1.90E+00 1.26E+00 8.96E-01
@ AR-41 1293.64 99.16 l.00E+26 l.00E+26 l.00E+26 1.00E+20
TI-44 67.88 94.40 3.62E-01 3.07E-01 1.68E-01 l.80E-01
78.34 96. 00 3.07E-01 1.33E-02 1.52E-01
SC-46 889.25 98.98 2.49E+04 2.42E+04 -1.81E+03 l.23E+04
1120.51 99.90 2.42E+04 -1.44E+04 1.19E+04
@ V-48 983.52 99.98 l.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 1312.10 97.50 1.00E+26 l.00E+26 1.00E+20
CR-51 320.08 9.83 3.96E+14 3.96E+14 5.43E+13 1.96E+14
MN-54 834.83 99.97 8.79E+00 8.79E+00 2.17E+00 4.33E+00
CO-56 846.75 99. 96 1.77E+05 1.12E+05 5.34E+04 8.74E+04
1037.75 14.03 1.38E+06 6.00E+05 6.81E+05
1238.25 67.00 1.51E+05 2.30E+04 7.29E+04
1771.40 15.51 4 .11E+05 -3.26E+04 1.92E+05
2587.48 16.90 l.12E+05 -3.00E+04 3.95E+04
+ CO-57 122.06 * 85.51 1.08E+0l 1.08E+0l 6.78E+0l 5.39E+00
136.48 * 10.60 7.82E+0l 7.26E+0l 3.88E+0l
CO-58 810.76 99.40 1.48E+05 1.48E+05 -1.28E+05 7.29E+04
FE-59 1099.22 56.50 5.58E+08 3.16E+08 -1.22E+08 2.75E+08
1291.56 43.20 3.16E+08 1.43E+07 l.52E+08
+ CO-60 1173.22 * 100.00 1.63E+00 9.45E-01 1.31E+02 8.l0E-01
1332.49 * 100.00 9.45E-01 1.32E+02 4.64E-01
+ ZN-65 1115.52 * 50.75 5.56E+0l 5.56E+0l 2.76E+0l 2.75E+0l
@ GA-67 93.31 35.70 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 208.95 2.24 1.00E+26 1.00E+26 1.00E+20
@ 300.22 16.00 1.00E+26 1.00E+26 l.00E+20
SE-75 121.11 16.70 3.06E+03 6.92E+02 2.25E+04 l.52E+03
136.00 59.50 6.92E+02 1.24E+03 3.43E+02
264.65 59.80 9.74E+02 -5.67E+0l 4.82E+02
279.53 25.20 2.33E+03 1.33E+03 1.15E+03
400.65 11. 40 6.07E+03 2.19E+03 3.01E+03
RB-82 776.52 13.00 5.97E+15 5.97E+15 -8.34E+14 2.94E+15
RB-83 520.41 46.00 2.83E+04 2.83E+04 -1.15E+03 1.40E+04
529.64 30.30 4.17E+04 -2.39E+04 2.06E+04
552.65 16.40 7.58E+04 9.53E+03 3.74E+04
KR-85 513.99 0.43 1.16E+02 1.16E+02 7.43E+01 5.72E+0l
SR-85 513.99 99.27 4.10E+05 4.10E+05 2.63E+05 2.02E+05
Y-88 898.02 93.40 2.76E+03 8.47E+02 1.78E+03 1.36E+03
1836.01 99.38 8.47E+02 6.12E+02 3.94E+02
MO-93 263.06 56.72 7.23E-01 2.24E-01 8.80E-02 3.58E-01
684.67 99.68 4.96E-0l -8.70E-02 2.44E-01
1477.11 99.08 2.24E-01 -2.71E-03 1.05E-01
NB-93M 16.57 9.43 1.11E+09 1.11E+09 -1.83E+09 5.47E+08
NB-94 702.63 100.00 4.02E-01 4.02E-01 -9.89E-02 1.98E-01
871.10 100.00 5.30E-01 -1.05E-01 2.61E-01
NB-95 765.79 99.81 5.57E+10 5.57E+10 -3.33E+10 2.74E+10
0168
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Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCi/grams)
@ NB-95M 235.69 25.00 1.00E+26 1.00E+26 1.00E+26 l.00E+20
ZR-95 724.18 43.70 1.13E+06 9.47E+05 -5.26E+05 5.54E+05
756. 72 55.30 9.47E+05 -3.08E+05 4.66E+05
@ MO-99 181.06 6.20 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 739.58 12.80 1.00E+26 1.00E+26 1.00E+20
@ 778.00 4.50 1.00E+26 1.00E+26 l.00E+20
TC-99M 140.51 89.00 2.46E-01 2.46E-01 4.46E-03 1.22E-01
RU-103 497.08 89.00 3.54E+09 3.54E+09 1.48E+08 l.75E+09
RU-106 621.84 9.80 4.58E+0l 4.58E+0l -2.02E+0l 2.26E+0l
AG-108M 433.93 89.90 4.65E-01 4.48E-01 -4.79E-01 2.30E-01
614.37 90.40 4.48E-01 -l.06E-01 2.21E-01
722.95 90.50 4.58E-01 -2.22E-02 2.25E-01
+ CD-109 88.03 * 3. 72 7.45E+0l 7.45E+0l 2.80E+03 3.71E+0l
AG-ll0M 657.75 93.14 4.44E+0l 2.75E+0l -3.12E+02 2.21E+0l
677.61 10.53 l.36E+02 -2.65E+0l 6.70E+0l
706.67 16.46 8.93E+0l -1.06E+0l 4.40E+0l
763.93 21.98 7.22E+01 1. 96E+01 3.56E+0l
884.67 21.98 9.00E+0l -1.77E+0l 4.44E+0l
1384.27 23.94 2.75E+0l -5.88E+00 1.30E+0l
CD-113M 263.70 0.02 l.69E+03 1.69E+03 2.73E+02 8.39E+02
SN-113 255.12 1. 93 3.41E+04 l.43E+03 -8.10E+03 l.69E+04
391.69 64.90 l.43E+03 3.25E+02 7.07E+02
TE-123M 159.00 84.10 4.86E+02 4.86E+02 2.37E+02 2.41E+02
SB-124 602.71 97.87 l.16E+06 l.04E+06 -5.79E+05 5.71E+05
645.85 7.26 1.63E+07 -2.26E+06 8.02E+06
722.78 11.10 l.08E+07 -5.24E+05 5.32E+06
1691.02 49.00 1.04E+06 -2.19E+05 4.82E+05
I-125 35.49 6.49 2.37E+07 2.37E+07 2.92E+07 1.17E+07
SB-125 176.33 6.89 8.l0E+00 3.38E+00 -4.12E+00 4.0lE+00
427.89 29.33 3.38E+00 1.29E-01 1.67E+00
463.38 10.35 1.07E+0l 5,46E+00 5.30E+00
600.56 17.80 5.25E+00 -1.68E+00 2.59E+00
635.90 11. 32 8.51E+00 -1.94E+00 4.19E+00
SB-126 414.70 83.30 4.74E-01 3.96E-01 -2.42E-01 2.34E-01
666.33 99.60 9.07E-01 -2.0lE+0l 4.51E-0l
695.00 99.60 3.96E-01 -l.07E-01 1.95E-01
720.50 53.80 7.60E-01 l.22E-01 3.74E-01
+ SN-126 87.57 * 37.00 1.08E+00 1.08E+00 4.08E+0l 5.40E-01
@ SB-127 473.00 25.00 l.00E+26 1.00E+26 l.00E+26 1.00E+20
@ 685.00 35.70 1.00E+26 l.00E+26 l.00E+20
@ 783.80 14.70 1.00E+26 l.00E+26 1.00E+20
I-129 29.78 57.00 1.70E+00 1.70E+00 -2.14E+00 8.47E-01
33.60 13.20 4.96E+00 1.83E+00 2.46E+00
39.58 7.52 6.06E+00 -2.46E+0l 3.00E+00
@ I-131 284.30 6.05 1.00E+26 l.00E+26 1.00E+26 l.00E+20
@ 364.48 81.20 l.00E+26 1.00E+26 l.00E+20
@ 636.97 7.26 1.00E+26 1.00E+26 l.00E+20
@ 722.89 1. 80 l.00E+26 1.00E+26 1.00E+20
@ TE-132 49. 72 13.10 l.00E+26 1.00E+26 l.00E+26 1.00E+20
@ 228.16 88.00 1.00E+26 l.00E+26 l.00E+20
BA-133 81.00 33.00 1.07E+00 7.58E-01 -4.40E-01 5.33E-01
302.84 17.80 2.33E+00 -1.50E+00 1.15E+00
356.01 60.00 7.58E-01 7.74E-03 3.75E-01
0169
4/17/2018 6:13:23AM Page 22 of25
Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams) (pCi/grams)
@ I-133 529.87 86.30 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ XE-133 81.00 38.00 1.00E+26 1.00E+26 1.00E+26 1.00E+20
CS-134 563.23 8.38 1.51E+0l 1.31E+00 3.52E+00 7.44E+00
569.32 15.43 8.24E+00 1.60E+00 4.06E+00
604.70 97.60 1.31E+00 -1.25E-01 6.45E-01
795.84 85.40 1.79E+00 5.64E-01 8.80E-01
801.93 8.73 1.76E+0l -8.20E+00 8.66E+00
CS-135 268.24 16.00 2.04E+00 2.04E+00 6.87E-01 1. 0lE+00
@ I-135 1131.51 22.50 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 1260.41 28.60 1.00E+26 1.00E+26 1.00E+20
@ 1678.03 9.54 1.00E+26 1.00E+26 1.00E+20
@ CS-136 153.22 7.46 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 163.89 4.61 1.00E+26 1.00E+26 1.00E+20
@ 176.55 13.56 1.00E+26 1.00E+26 1.00E+20
@ 27 3. 65 12.66 l.00E+26 1.00E+26 1.00E+20
@ 340.57 48.50 1.00E+26 1.00E+26 1.00E+20
@ 818.50 99.70 1.00E+26 1.00E+26 1.00E+20
@ 1048.07 79.60 1.00E+26 1.00E+26 1.00E+20
@ 1235.34 19.70 1.00E+26 1.00E+26 1.00E+20
+ CS-137 661.65 * 85.12 1.27E+00 1.27E+00 8.31E+0l 6.30E-01
LA-138 788.74 34.00 1.32E+00 2.76E-0l 2.32E-01 6.50E-01
1435.80 66.00 2.76E-01 2.81E-02 1.30E-01
+ CE-139 165.85 * 80.35 2.02E+02 2.02E+02 1.37E+02 9.99E+01
@ BA-140 162.64 6.70 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 304.84 4.50 1.00E+26 1.00E+26 1.00E+20
@ 423.70 3.20 1.00E+26 1.00E+26 l.00E+20
@ 437.55 2.00 1.00E+26 1.00E+26 l.00E+20
@ 537.32 25.00 l.00E+26 1.00E+26 1.00E+20
@ LA-140 328.77 20.50 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 487.03 45.50 1.00E+26 1.00E+26 1.00E+20
@ 815.85 23.50 1.00E+26 1.00E+26 1.00E+20
@ 1596.49 95.49 1.00E+26 1.00E+26 1.00E+20
CE-141 145.44 48.40 4.47E+ll 4.47E+ll 2. 66E+ll 2. 21E+ll
@ CE-143 57.36 11. 80 1.00E+26 l.00E+26 l.00E+26 1.00E+20
@ 293.26 42.00 1.00E+26 1.00E+26 1.00E+20
@ 664.55 5.20 1.00E+26 1.00E+26 1.00E+20
CE-144 133.54 10.80 4.78E+0l 4.78E+0l -8.05E-01 2.37E+0l
PM-144 476.78 42.00 1.23E+0l 4.74E+00 1.60E+00 6.07E+00
618.01 98.60 4.76E+00 -3.15E-01 2.34E+00
696. 4 9 99.49 4.74E+00 4.24E-01 2.33E+00
PM-145 36.85 21.70 2.57E+00 1.41E+00 1.99E+00 1.27E+00
37.36 39.70 1.41E+00 6.18E-01 6.99E-01
42.30 15.10 3.68E+00 -3.07E+00 1.83E+00
72.40 2.31 l.42E+0l -6.58E+00 7.03E+00
PM-146 453.90 39.94 1.73E+00 1.73E+00 8.19E-01 8.55E-01
735.90 14.01 4.77E+00 1.90E+00 2.35E+00
747.13 13.10 5.17E+00 2.80E+00 2.55E+00
@ ND-147 91.11 28.90 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 531.02 13.10 1.00E+26 1.00E+26 1.00E+20
@ PM-149 285.90 3.10 1.00E+26 1.00E+26 1.00E+26 1.00E+20
EU-152 121.78 20.50 1.68E+00 1.55E+00 1.23E+0l 8.33E-01
244.69 5.40 6.21E+00 3.76E+00 3.07E+00
344.27 19.13 2.16E+00 -1.18E+00 1.07E+00
0170
4/17/2018 6:13:23AM Page 23 of 25
Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCilgrams) (pCi/grams) (pCilgrams)
EU-152 778.89 9.10 5.93E+00 l.55E+00 9.48E-01 2.92E+00
964.01 10.40 7.03E+00 l.15E+00 3.47E+00
1085.78 7.22 9. 71E+00 -6.52E-01 4.78E+00
1112.02 9.60 7.25E+00 3.26E-01 3.57E+00
1407.95 14.94 l.55E+00 l.88E-01 7.31E-01
GD-153 97.43 31.30 2.70E+0l 2.70E+0l 6.84E-01 l.34E+0l
103.18 22.20 3.86E+0l 5.77E+00 l.91E+0l
EU-154 123.07 40.50 9.35E-01 9.35E-01 6.57E+00 4.64E-01
723.30 19.70 2.73E+00 -1.32E-01 1.34E+00
873.19 11. 50 6.15E+00 -1.12E+00 3.03E+00
996. 32 10.30 7.40E+00 -2.76E-01 3.65E+00
1004.76 17.90 4.28E+00 -4.28E-01 2. llE+00
1274.45 35.50 9.84E-01 -6.86E-03 4.73E-01
EU-155 86.50 30.90 2.91E+00 1.65E+00 7.66E+0l 1.45E+00
105.30 20.70 1.65E+00 7.67E-02 8.20E-01
@ EU-156 811. 77 10.40 1.00E+26 1.00E+26 l.00E+26 l.00E+20
@ 1153.47 7.20 l.00E+26 1.00E+26 l.00E+20
@ 1230.71 8.90 1.00E+26 l.00E+26 l.00E+20
HO-166M 184.41 72.60 3.45E-01 3.45E-01 -1.02E-01 l.71E-01
280.45 29.60 1.llE+00 4.66E-01 5.52E-01
410.94 11.10 3.60E+00 7.50E-01 1.78E+00
711.69 54.10 7.62E-01 -1.97E-0l 3.75E-01
TM-171 66. 72 0.14 9.01E+02 9.01E+02 2.77E+03 4.48E+02
HF-172 67.35 5.31 2.31E+0l 7.32E+00 1.07E+0l 1.15E+0l
125.82 11. 30 7.32E+00 -1.42E+00 3.63E+00
@ LU-172 181.53 20.60 l.00E+26 l.00E+26 1.00E+26 l.00E+20
@ 900. 72 29.81 1.00E+26 l.00E+26 l.00E+20
@ 1093.66 62.50 l.00E+26 l.00E+26 l.00E+20
LU-173 100. 72 5.24 2.39E+0l 9.26E+00 7.97E+00 l.18E+0l
272.11 21. 20 9.26E+00 1.94E+00 4.59E+00
HF-17 5 343.40 84.00 l.50E+05 l.50E+05 -8. 18E+04 7.44E+04
LU-176 88.34 13.30 4.08E+00 3.03E-01 l.09E+02 2.03E+00
201.83 86.00 3.03E-01 -2.04E-02 1.50E-01
306.78 94.00 3.55E-01 -1.35E-01 1.76E-01
HF-181 133.02 41.70 8.03E+08 7.76E+08 -9.45E+07 3.98E+08
345.85 17.20 3.18E+09 9.27E+08 l.57E+09
482.03 82.80 7.76E+08 1.19E+08 3.84E+08
TA-182 67.75 41. 20 2.02E+03 2.02E+03 9.39E+02 1.00E+03
1121.30 34.90 3.91E+03 -1.74E+03 l.92E+03
1189.05 16.23 6.44E+03 -7.74E+02 3.15E+03
1221.41 26.98 3.09E+03 -9.39E+02 1.50E+03
1231.02 11. 44 6.85E+03 -1.37E+03 3.32E+03
IR-192 308.46 29.68 2.09E+05 1. 72E+05 1.73E+05 l.04E+05
468.07 48.10 1.72E+05 5.68E+03 8.54E+04
HG-203 279.19 77. 30 9.67E+07 9.67E+07 -1.68E+07 4.79E+07
TL-204 374.74 94.11 7.42E-01 7.42E-01 8.04E-02 3.67E-01
899.15 99.16 1.l0E+00 9.53E-02 5.42E-01
911. 74 91.10 1.24E+00 5.73E-01 6.13E-01
BI-207 569.67 97. 72 4.23E-01 4.23E-01 4.53E-03 2.09E-01
1063.62 74.90 8.13E-01 -4.12E-01 4.00E-01
TL-208 583.14 30.22 1.31E+00 4.40E-01 1.07E+00 6.47E-01
860.37 4.48 1.17E+0l 1.53E+00 5.76E+00
2614.66 35.85 4.40E-01 4.05E-01 1.97E-01
0171
4/17/2018 6:13:23AM Page 24 of 25
Analysis Report for 1803111-01
GAS-1402
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi!grams) (pCi!grams) (pCi!grams) (pCi!grams)
BI-210M 262.00 45.00 7.27E-01 7.27E-01 6.37E-02 3.60E-01
300.00 23.00 1.45E+00 6.83E-01 7.20E-01
PB-210 46.50 4.25 1.46E+0l 1.46E+0l -9.55E+0l 7.28E+00
PB-211 404.84 2.90 1.33E+0l 1.33E+0l -7.04E+00 6.58E+00
831.96 2.90 1.72E+0l 1.15E+0l 8.48E+00
BI-212 727.17 11. 80 3.54E+00 3.54E+00 4.65E-01 1.74E+00
1620.62 2.75 6.12E+00 -1.36E+00 2.84E+00
+ PB-212 238.63 * 44.60 6.58E-01 6.58E-01 6.02E-01 3.26E-01
300.09 3.41 9.80E+00 4.61E+00 4.85E+00
BI-214 609.31 46.30 8.58E-01 8.58E-01 1.03E-02 4.23E-01
1120.29 15.10 3.62E+00 -2.15E+00 1.78E+00
1764.49 15.80 1.23E+00 5.83E-01 5.75E-01
2204.22 4.98 3.78E+00 -1.0lE+00 1.74E+00
+ PB-214 295.21 19.19 1.74E+00 l.12E+00 5.19E-01 8.61E-01
351.92 * 37.19 1.12E+00 6.06E-01 5.57E-01
RN-219 401.80 6.50 5.94E+00 5.94E+00 -1.97E+00 2.94E+00
RA-223 323.87 3.88 8.76E+00 8.76E+00 -4.12E+00 4.33E+00
RA-224 240.98 3.95 7.14E+00 7.14E+00 -1.29E+00 3.53E+00
@ RA-225 40.00 31.00 1.00E+26 1.00E+26 1.00E+26 1.00E+20
RA-226 186.21 3.28 7.80E+00 7.80E+00 1.33E+00 3.86E+00
TH-227 50.10 8.40 7. 96E+00 2.46E+00 3.43E+0l 3. 96E+00
236.00 11. 50 2.46E+00 -8.66E-02 l.22E+00
256.20 6.30 5.14E+00 -3.44E-01 2.55E+00
AC-228 338.32 11. 40 2.99E+00 2.14E+00 -1.37E+00 1.48E+00
911.07 27. 70 2.14E+00 1.16E+00 1.06E+00
969.11 16.60 3.55E+00 -2.31E-01 1.75E+00
TH-230 48.43 16.90 3.76E+00 3.76E+00 1.41E+0l 1.87E+00
62.85 4.60 1.25E+01 -6.15E+02 6.23E+00
67.67 0.37 8.89E+0l 4.13E+01 4.42E+0l
PA-231 283.67 1. 60 2.05E+0l 1.43E+0l 1.87E+00 1.0lE+0l
302.67 2.30 1.43E+0l -9.16E+00 7.07E+00
TH-231 25.64 14.70 2.02E+0l 4.92E+00 -2.57E+02 1.0lE+0l
84.21 6.40 4.92E+00 -2.50E+02 2.44E+00
PA-233 311.98 38.60 2.36E+14 2.36E+l4 8.14E+13 1.17E+14
PA-234 131.20 20.40 1.06E+00 1.06E+00 -8.62E-02 5.27E-01
733.99 8.80 4.87E+00 -2.41E-01 2.40E+00
946.00 12.00 5.26E+00 -7.02E-01 2.60E+00
PA-234M 1001.03 0.92 6.28E+0l 6.28E+0l -5.20E-01 3.09E+0l
TH-234 63.29 3.80 1.0lE+0l 1.0lE+0l -5.92E+02 5.04E+00
U-235 143.76 10.50 2.12E+00 2.12E+00 2.64E-01 1.05E+00
163.35 4.70 4.90E+00 -1.42E+00 2.43E+00
205.31 4.70 5.55E+00 -2.91E+00 2.75E+00
NP-237 86.50 12.60 4.36E+00 4.36E+00 1.15E+02 2.17E+00
@ NP-239 106.10 22.70 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 228.18 10.70 1.00E+26 1.00E+26 1.00E+20
@ 277.60 14.10 1.00E+26 1.00E+26 1.00E+20
+ AM-241 59.54 * 35.90 3.18E+00 3.18E+00 1.99E+02 1.59E+00
AM-243 7 4. 67 66.00 4.33E-01 4.33E-01 2.77E-01 2.15E-01
CM-243 209.75 3.29 8.89E+00 2.55E+00 -3.05E+00 4.40E+00
228.14 10.60 2.94E+00 2.llE+00 1.45E+00
277.60 14.00 2.55E+00 -3.99E-01 1.26E+00
0172
Analysis Report for 1803111-01
+
>
GAS-1402
= Nuclide identified during the nuclide identification
= Energy line found in the spectrum
= MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
No Action Level results available for reporting purposes.
4/17/2018 6:13:23AM
DATA REVIEW COMMENTS REPORT
Creation Date Comment
No Data Review Comments Entered.
Page 25 of 25
User
0173
Channel Data Report 4/17/2018 6:13:44 AM Page 1
*******************************************************
***** S P E C T R A L D A T A R E P O R T *****
*******************************************************
Sample Title: GAS-1402
Elapsed Live time: 1800 Elapsed Real Time: 1822
Channell------1-------1-------1-------1-------1-------I-------I-------I
1: 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 2 129 1676 1991 7385 33446 23528 5276
25: 11482 7571 2613 1968 1291 1043 1246 1972
33: 1548 835 7 68 1005 1177 961 987 1085
41: 1176 1384 1580 1758 1900 2036 2433 3004
49: 4025 4876 4913 4545 4518 4624 4840 5387
57: 5671 692 6 22551 55117 15932 2034 1735 2043
65: 2513 2621 1713 1344 1390 1436 1302 1291
73: 1311 1357 1437 1333 1443 1351 1413 1360
81: 1340 1354 1393 1431 1567 1510 2830 11531
89: 9385 1618 8 63 964 1105 1238 960 801
97: 688 775 755 738 760 756 803 770
105: 732 753 747 7 68 764 701 740 733
113: 795 786 773 800 774 777 774 855
121: 905 2207 1910 856 786 786 784 733
129: 827 748 742 704 732 724 700 854
137: 956 803 699 67 6 757 718 696 784
145: 693 710 714 708 685 667 691 68 6
153: 692 693 710 645 68 4 694 687 723
161: 654 675 627 676 707 754 663 666
169: 647 653 662 650 669 640 634 654
177: 649 611 623 673 658 671 721 679
185: 685 721 781 756 755 778 723 750
193: 725 736 727 721 727 708 747 688
201: 677 720 736 701 718 672 697 674
209: 666 7 68 717 747 750 786 759 772
217: 794 740 7 61 794 736 763 771 727
225: 711 742 718 7 60 723 708 694 64 6
233: 652 668 685 681 678 717 7 92 666
241: 632 607 625 682 593 650 661 597
249: 610 654 606 577 569 597 573 578
257: 555 587 579 588 587 592 571 568
265: 532 572 567 546 550 552 544 547
273: 548 517 562 526 519 525 547 550
281: 504 524 566 4 97 472 541 519 485
289: 491 510 479 505 506 465 531 500
297: 513 527 501 489 482 494 484 457
305: 451 470 478 502 508 504 516 488
313: 484 454 511 473 477 469 471 491
321: 484 466 469 472 435 4 69 442 503
329: 457 441 447 478 440 444 486 443
337: 443 485 451 411 430 395 453 439
345: 448 423 469 482 472 470 4 67 515
353: 519 441 439 458 406 444 4 61 444
361: 415 446 443 445 470 453 429 435
0174
Channel Data Report 4/17/2018 6:13:44 AM Page 2
369: 416 416 438 436 445 444 425 416
Sample Title: GAS-1402
Channell------l-------l-------l-------l-------l-------1-------1-------1
377: 435 418 420 435 435 454 433 451
385: 420 419 472 456 429 458 441 500
393: 426 430 437 412 423 471 4 67 447
401: 454 429 433 396 421 453 443 438
409: 443 456 477 443 431 455 432 440
417: 430 409 431 456 441 448 429 459
425: 464 405 427 445 471 483 417 458
433: 427 449 427 447 448 480 475 433
441: 440 466 465 437 4 68 431 450 489
449: 4 62 479 423 485 476 477 477 493
457: 511 403 497 481 484 480 516 4 97
465: 489 478 504 455 465 493 461 4 64
473: 445 493 422 451 432 407 420 375
481: 403 402 354 359 364 355 339 403
489: 363 356 340 353 360 322 330 335
497: 336 365 326 334 312 322 300 340
505: 317 344 344 319 307 327 388 366
513: 287 2 95 287 290 331 337 299 319
521: 293 272 285 263 287 311 290 298
529: 295 271 275 266 2 68 315 278 266
537: 306 276 290 254 292 256 271 280
545: 283 288 304 252 259 257 237 274
553: 266 272 250 219 253 239 249 264
561: 239 244 242 261 266 27 6 247 260
569: 273 245 248 232 255 222 251 226
577: 236 235 256 274 233 252 272 276
585: 245 252 227 225 257 244 222 220
593: 216 256 250 246 240 242 255 216
601: 230 205 218 256 239 238 227 248
609: 259 232 231 248 226 243 229 244
617: 242 245 241 232 210 239 237 221
625: 219 241 235 222 221 226 231 234
633: 224 216 230 197 204 245 258 238
641: 229 219 223 229 206 233 217 209
649: 243 235 222 230 252 218 240 231
657: 259 326 409 1696 9430 14484 4 678 637
665: 406 505 586 565 319 206 205 203
67 3: 206 201 207 204 209 191 183 214
681: 204 218 200 182 223 214 174 176
689: 196 200 192 176 173 207 199 200
697: 201 189 202 200 202 197 205 202
705: 178 192 205 211 203 199 186 218
713: 197 212 197 192 225 195 174 224
721: 17 6 187 186 204 174 193 212 187
72 9: 221 216 193 220 222 231 199 198
737: 197 207 200 206 17 6 167 222 206
745: 210 216 235 186 194 212 199 190
753: 211 201 201 201 216 177 213 199
761: 240 192 193 195 189 202 221 190
7 69: 193 206 214 194 210 213 185 226
777: 190 215 204 203 225 203 215 205
785: 182 201 183 197 207 216 208 215
793: 228 180 202 220 214 231 226 193
0175
Channel Data Report 4/17/2018 6:13:44 AM Page 3
801: 211 208 232 204 226 231 228 192
Sample Title: GAS-1402
Channell------l-------l-------l-------1-------1-------1-------I-------I
809: 203 218 218 196 236 193 237 225
817: 222 249 233 252 235 258 235 234
825: 225 224 220 198 237 211 213 217
833: 257 259 225 214 219 225 233 233
841: 233 222 247 247 255 220 260 223
849: 225 266 204 263 2 69 245 233 246
857: 239 241 228 246 255 212 269 252
865: 221 242 226 241 250 266 243 245
873: 231 223 254 263 252 260 243 266
881: 223 251 243 264 265 246 272 251
889: 269 246 272 255 246 270 250 269
8 97: 257 293 2 60 286 270 227 262 270
905: 227 271 243 283 283 2 97 301 279
913: 265 275 270 279 263 273 2 61 305
921: 273 283 283 266 308 281 257 290
929: 284 287 310 289 263 319 340 303
937: 294 282 308 300 311 273 307 274
945: 293 351 275 296 326 334 304 296
953: 347 299 332 315 323 290 269 311
961: 296 304 271 256 288 256 251 255
969: 256 254 248 257 246 241 229 244
977: 198 226 217 194 245 229 232 235
985: 251 223 246 223 239 218 249 243
993: 238 228 231 229 226 226 243 227
1001: 218 250 231 220 250 217 228 219
1009: 245 232 233 233 216 245 215 212
1017: 233 232 224 227 234 219 197 211
1025: 213 194 200 207 209 184 197 208
1033: 185 201 211 230 218 212 17 6 216
1041: 187 211 201 184 205 195 223 203
1049: 201 199 204 203 203 192 203 208
1057: 191 195 226 196 210 200 213 208
1065: 203 172 215 215 198 183 214 216
1073: 238 221 233 185 203 203 184 216
1081: 214 203 218 201 206 210 194 221
1089: 205 205 202 215 199 233 190 211
1097: 191 225 184 195 223 226 235 195
1105: 179 231 208 196 187 207 191 188
1113: 187 199 222 203 199 164 148 182
1121: 196 172 141 163 170 148 146 119
1129: 137 142 147 132 123 127 118 138
1137: 136 111 112 123 129 116 121 122
1145: 140 112 127 105 120 134 93 107
1153: 133 127 110 135 95 129 112 109
1161: 111 130 97 133 124 96 123 133
1169: 17 6 242 822 4614 10329 7021 1405 294
1177: 300 411 436 250 114 99 82 103
1185: 92 91 102 88 69 82 83 101
1193: 84 85 78 61 70 69 70 62
1201: 73 67 69 69 67 56 52 72
1209: 53 78 60 48 56 55 67 55
1217: 65 57 43 64 50 47 54 57
1225: 58 52 53 55 45 45 35 47
0176
Channel Data Report 4/17/2018 6:13:44 AM Page 4
1233: 45 50 41 50 43 35 38 42
Sample Title: GAS-1402
Channell------l-------l-------l-------l-------1-------1-------1-------I
1241: 41 29 39 45 37 35 31 32
1249: 30 46 41 28 32 41 39 31
1257: 36 31 23 37 32 35 20 29
1265: 26 22 40 32 32 31 32 29
1273: 27 44 28 30 30 23 40 34
1281: 28 27 25 24 26 37 29 27
1289: 33 34 22 27 26 33 25 25
1297: 30 24 32 30 26 27 27 27
1305: 25 43 31 30 31 19 29 33
1313: 26 22 27 27 44 24 34 28
1321: 30 26 37 27 32 40 45 108
1329: 139 535 3104 8454 7384 2062 276 197
1337: 308 343 189 56 23 15 14 12
1345: 7 20 17 23 15 18 13 19
1353: 17 12 17 17 15 14 18 12
1361: 8 11 13 15 14 15 6 12
1369: 16 10 13 17 12 11 10 15
1377: 15 15 12 6 15 16 14 12
1385: 9 16 6 24 10 11 12 15
1393: 10 15 14 18 6 14 23 16
1401: 14 11 12 17 15 20 9 11
1409: 9 16 13 15 13 7 18 11
1417: 15 14 19 14 9 12 6 15
1425: 15 8 14 12 10 10 14 9
1433: 13 11 7 14 15 14 8 13
1441: 10 13 6 8 8 15 11 5
1449: 9 8 14 16 15 10 7 9
1457: 13 14 14 17 19 12 12 14
1465: 8 11 10 10 13 8 17 10
1473: 14 15 10 10 13 8 8 11
1481: 10 10 16 11 10 8 13 11
148 9: 7 5 9 3 5 7 6 11
1497: 12 10 11 11 11 8 7 8
1505: 7 11 13 10 15 13 11 13
1513: 5 10 15 2 8 11 11 13
1521: 11 12 15 10 5 5 11 10
1529: 11 12 8 4 10 8 2 11
1537: 7 11 8 10 8 10 7 10
1545: 10 4 5 15 13 12 11 6
1553: 15 12 8 12 14 7 17 5
1561: 5 9 13 10 8 10 17 8
1569: 7 4 10 13 9 6 5 15
1577: 11 6 10 5 9 8 8 9
1585: 8 11 14 10 15 15 9 12
1593: 12 7 6 9 17 8 6 5
1601: 6 11 8 4 13 8 11 7
1609: 11 11 12 8 14 12 9 10
1617: 8 8 8 2 13 10 9 10
1625: 9 9 11 5 8 12 17 9
1633: 7 8 6 11 10 10 5 5
1641: 7 7 3 3 13 9 6 10
1649: 9 6 6 6 9 7 5 9
1657: 8 10 7 7 10 11 4 2
0177
Channel Data Report 4/17/2018 6:13:44 AM Page 5
1665: 7 8 8 4 7 5 6 13
Sample Title: GAS-1402
Channel[------[-------[-------[-------[-------[-------[-------[-------[
1673: 10 9 8 6 9 9 7 5
1681: 12 14 10 12 7 11 6 8
1689: 9 10 9 9 6 10 9 2
1697: 7 6 9 10 7 4 9 10
1705: 12 7 5 7 8 11 5 7
1713: 5 10 5 9 6 5 7 10
1721: 8 4 10 13 7 7 2 10
1729: 12 6 10 10 7 7 3 6
1737: 5 6 8 13 7 5 6 8
1745: 7 14 9 4 10 8 10 6
1753: 9 5 8 8 9 8 5 6
1761: 10 12 12 14 7 8 6 7
1769: 9 9 6 14 8 10 12 11
1777: 8 7 7 9 10 10 6 8
1785: 5 9 8 7 6 8 10 5
1793: 8 5 7 6 5 7 10 7
1801: 7 4 11 11 9 11 8 6
1809: 9 5 4 7 4 9 5 9
1817: 11 7 7 5 8 8 6 7
1825: 10 12 9 6 8 4 4 7
1833: 8 8 11 14 5 7 6 4
1841: 8 4 9 5 7 3 8 8
1849: 7 8 0 8 7 3 5 4
1857: 4 5 4 8 5 2 8 8
1865: 10 7 6 6 7 7 5 11
1873: 7 6 9 8 5 5 8 7
1881: 4 7 4 3 6 3 3 4
1889: 4 5 6 9 6 9 4 6
1897: 3 5 6 4 7 8 9 6
1905: 7 3 7 6 4 10 12 4
1913: 7 8 7 7 6 4 7 9
1921: 6 3 8 5 7 4 3 7
1929: 12 4 7 8 6 4 2 11
1937: 6 4 3 7 3 4 3 8
1945: 4 4 8 9 7 7 10 4
1953: 6 5 13 5 8 5 7 7
1961: 8 4 5 5 9 7 8 8
1969: 5 5 2 6 6 7 3 8
1977: 9 6 9 3 6 10 4 3
1985: 8 9 6 8 7 5 5 5
1993: 3 8 10 4 6 8 4 4
2001: 7 7 5 14 7 4 3 6
2009: 4 11 7 7 2 2 5 8
2017: 7 8 5 12 7 10 3 9
2025: 8 7 9 5 5 6 6 9
2033: 6 4 7 8 3 4 9 6
2041: 4 7 9 0 6 2 3 9
2049: 2 11 4 4 6 6 8 5
2057: 7 5 4 7 3 3 5 6
2065: 7 6 4 5 5 8 5 3
2073: 3 4 5 5 8 7 8 6
2081: 5 2 2 4 3 5 8 4
2089: 5 7 3 6 6 5 3 4
0178
Channel Data Report 4/17/2018 6:13:44 AM Page 6
2097: 4 6 5 3 6 8 9 6
Sample Title: GAS-1402
Channell------l-------1-------1-------1-------l-------l-------1-------I
2105: 7 2 5 7 3 5 9 6
2113: 10 4 8 4 3 4 6 5
2121: 5 5 3 5 5 5 2 4
2129: 10 2 7 5 5 5 8 4
2137: 5 4 3 10 9 7 4 5
2145: 4 8 9 4 3 1 7 6
2153: 1 4 4 8 1 8 6 2
2161: 3 7 2 2 6 6 3 4
2169: 10 6 3 6 8 4 6 9
2177: 3 4 7 3 2 4 6 3
2185: 6 2 6 7 6 4 3 7
2193: 2 14 7 5 8 4 3 6
2201: 6 4 3 3 10 6 6 7
2209: 6 5 9 5 2 6 9 6
2217: 3 4 4 8 1 4 4 5
2225: 7 5 6 1 2 3 8 6
2233: 6 7 11 4 8 9 5 6
2241: 6 7 2 5 6 4 5 3
2249: 6 2 2 6 3 5 12 5
2257: 6 7 9 8 3 3 5 6
2265: 5 5 6 3 3 4 8 11
2273: 8 6 3 6 1 7 5 8
2281: 7 2 7 4 7 4 5 7
2289: 7 5 4 7 8 4 3 5
2297: 2 3 8 2 3 2 1 2
2305: 6 8 0 5 2 4 1 4
2313: 1 2 7 4 2 5 3 6
2321: 7 4 0 5 3 2 6 0
2329: 2 2 1 2 3 3 3 2
2337: 4 3 7 5 3 2 2 2
2345: 2 2 0 2 3 2 3 6
2353: 0 3 4 1 1 2 3 5
2361: 2 1 3 4 6 1 3 1
2369: 2 4 2 1 2 6 2 0
2377: 2 2 1 4 1 5 3 0
2385: 3 0 3 2 1 2 1 0
2393: 0 1 1 4 0 0 2 2
2401: 0 1 0 3 0 0 2 0
2409: 2 2 1 0 0 1 2 1
2417: 2 0 2 0 1 2 2 2
2425: 0 0 3 0 0 0 1 1
2433: 0 0 1 1 1 0 0 0
2441: 0 0 2 3 2 2 1 0
2449: 1 2 0 2 3 1 2 2
2457: 0 2 1 0 2 0 1 1
2465: 0 1 0 0 1 1 2 0
2473: 0 0 1 1 0 1 0 0
24 81: 2 1 0 0 0 0 1 0
2489: 3 0 1 0 2 1 1 0
2497: 3 2 0 1 6 10 48 85
2505: 109 58 21 6 2 5 4 3
2513: 1 0 1 0 0 1 0 1
2521: 0 0 1 0 0 0 1 0
0179
Channel Data Report 4/17/2018 6:13:44 AM Page 7
2529: 0 1 0 1 0 0 0 0
Sample Title: GAS-1402
Channell------l-------l-------l-------1-------1-------1-------I-------I
2537: 0 0 0 0 1 0 0 0
2545: 0 0 0 0 0 1 1 0
2553: 1 0 0 0 1 1 0 0
2561: 0 1 0 0 1 0 0 0
2569: 1 0 0 0 0 0 0 1
2577: 0 0 1 0 0 1 0 0
2585: 0 0 0 0 0 2 0 1
2593: 0 0 1 0 0 0 0 0
2601: 0 0 1 0 0 0 0 1
2609: 0 0 2 4 12 4 2 1
2617: 0 1 0 0 0 0 0 0
2625: 0 0 0 0 0 0 0 0
2633: 0 0 0 1 0 0 1 0
2641: 0 1 1 0 0 0 0 0
2649: 0 0 0 0 1 1 0 0
2657: 0 0 0 0 0 0 0 0
2665: 0 1 0 0 0 0 0 0
2673: 1 0 0 0 0 0 0 0
2681: 0 0 0 1 0 0 0 1
2689: 0 0 0 0 0 0 0 0
2697: 1 0 0 0 1 0 0 0
2705: 0 0 0 0 0 1 0 0
2713: 0 0 0 0 1 0 0 0
2721: 0 0 2 0 0 0 0 0
2729: 0 0 0 1 0 0 0 0
2737: 0 2 0 0 0 0 0 0
2745: 0 0 0 0 1 0 1 1
2753: 0 0 1 0 0 0 0 0
2761: 0 0 0 0 0 0 0 0
2769: 0 0 0 0 0 0 0 0
2777: 0 0 0 0 0 0 0 0
2785: 0 0 0 0 0 0 0 0
2793: 1 0 0 0 0 0 0 0
2801: 0 0 0 0 1 0 0 0
2809: 0 1 0 0 0 0 0 0
2817: 0 0 0 0 0 0 0 0
2825: 0 0 0 0 0 0 1 0
2833: 0 1 0 0 0 0 0 0
2841: 1 0 0 0 0 0 0 0
2849: 0 1 0 1 0 0 0 0
2857: 0 0 0 0 0 0 0 0
2865: 0 0 0 0 0 0 0 0
2873: 0 0 0 0 0 0 0 1
2881: 0 0 0 0 0 0 0 0
2889: 0 0 0 0 0 0 0 0
2897: 0 0 0 1 0 0 1 0
2905: 0 0 0 0 0 0 0 0
2913: 0 0 0 0 0 0 0 0
2921: 2 0 2 1 0 0 0 1
2929: 0 0 0 0 0 0 0 0
2937: 0 0 0 0 0 0 0 1
2945: 1 0 0 0 0 1 0 0
2953: 0 0 1 0 0 1 0 0
0180
Channel Data Report 4/17/2018 6:13:44 AM Page 8
2961: 0 0 1 0 0 0 0 0
Sample Title: GAS-1402
Channell------l-------l-------1-------1-------1-------I-------I-------I
2969: 2 0 0 0 0 0 0 0
2977: 0 0 0 0 0 0 0 0
2985: 0 0 0 0 0 0 0 0
2993: 0 0 2 0 0 0 0 1
3001: 0 0 1 0 0 0 0 1
3009: 0 1 0 0 0 0 0 0
3017: 0 0 0 0 0 0 0 1
3025: 0 0 0 0 0 0 0 0
3033: 0 0 0 0 0 0 0 0
3041: 0 0 0 1 1 0 0 0
3049: 1 0 0 0 2 1 0 1
3057: 0 0 0 0 0 0 0 0
3065: 0 0 0 1 0 0 0 0
3073: 0 0 0 0 0 0 1 0
3081: 0 0 0 0 0 0 2 0
3089: 0 0 0 0 0 0 0 0
3097: 0 0 0 1 1 0 1 0
3105: 0 1 0 0 0 0 0 0
3113: 0 1 0 0 0 0 0 0
3121: 0 0 0 0 0 2 0 0
3129: 1 0 0 0 0 0 1 0
3137: 0 0 0 0 0 0 0 1
3145: 0 0 0 0 0 0 0 0
3153: 1 1 1 0 0 0 0 0
3161: 0 0 0 0 0 0 0 0
3169: 0 0 0 0 0 0 0 0
3177: 1 0 0 0 0 0 0 1
3185: 0 0 0 0 0 0 0 0
3193: 0 0 0 0 0 2 0 0
3201: 1 0 0 0 0 0 0 0
3209: 0 0 0 0 0 0 0 0
3217: 0 0 0 0 0 0 1 0
3225: 0 0 0 0 0 0 1 0
3233: 0 1 0 0 0 0 0 0
3241: 0 0 0 0 0 0 0 0
3249: 0 0 0 0 0 0 0 0
3257: 0 0 0 0 1 0 0 0
3265: 0 0 0 1 0 0 0 0
3273: 0 0 0 0 0 0 0 0
3281: 0 0 0 0 1 0 0 0
3289: 0 0 0 0 0 0 0 0
3297: 0 0 1 0 0 0 0 0
3305: 0 0 0 0 0 0 0 0
3313: 0 0 0 0 0 0 0 0
3321: 0 0 0 0 0 0 0 0
3329: 0 0 0 0 0 0 0 0
3337: 0 0 0 0 0 0 0 1
3345: 0 0 0 0 0 0 0 0
3353: 0 1 0 0 0 0 0 0
3361: 0 0 0 0 0 0 0 0
3369: 1 0 0 0 0 0 0 0
3377: 0 0 0 0 0 0 0 0
3385: 0 0 0 0 1 0 0 1
0181
Channel Data Report 4/17/2018 6:13:44 AM Page 9
3393: 0 0 0 0 0 0 0 0
Sample Title: GAS-1402
Channell------l-------l-------1-------1-------1-------I-------I-------I
3401: 0 0 0 0 1 0 0 0
3409: 0 0 0 0 0 0 0 0
3417: 0 0 0 0 0 0 0 0
3425: 0 0 0 0 0 0 0 0
3433: 0 0 0 0 0 0 0 0
3441: 0 0 0 0 0 0 0 0
3449: 0 0 0 0 0 0 0 0
3457: 0 0 0 0 0 0 0 0
3465: 0 0 0 0 0 0 0 0
3473: 0 0 0 0 0 0 0 0
3481: 0 1 0 0 0 0 0 0
3489: 0 1 1 1 0 0 0 0
3497: 0 0 0 0 0 0 0 0
3505: 0 0 0 1 0 0 0 0
3513: 0 0 0 0 0 0 0 0
3521: 0 0 0 0 0 1 0 0
3529: 0 0 0 0 0 0 0 0
3537: 0 0 0 0 1 0 0 0
3545: 0 0 1 0 0 0 0 0
3553: 0 0 0 0 0 0 0 1
3561: 0 0 0 0 0 0 0 0
3569: 0 0 0 0 0 0 1 0
3577: 1 0 0 0 1 0 0 0
3585: 0 1 0 0 0 0 0 0
3593: 0 0 0 1 0 0 0 0
3601: 0 0 0 0 0 0 0 0
3609: 0 0 0 0 0 0 0 0
3617: 0 0 0 0 0 0 0 0
3625: 0 0 0 0 0 0 0 0
3633: 0 0 0 0 0 0 0 0
3641: 0 0 0 0 0 0 0 0
3649: 0 1 0 0 0 0 0 0
3657: 0 0 0 0 1 0 0 0
3665: 0 0 0 0 0 0 0 0
3673: 0 0 0 0 0 0 0 1
3681: 0 0 0 0 0 0 0 0
3689: 0 0 0 0 0 0 0 0
3697: 0 0 0 1 0 0 0 0
3705: 0 0 0 1 0 1 0 0
3713: 2 0 0 0 0 0 0 0
3721: 0 0 0 1 0 1 0 0
37 2 9: 0 0 0 0 0 0 0 0
3737: 1 0 0 0 0 0 0 0
3745: 0 1 0 0 0 0 0 0
3753: 1 ' 0 0 0 0 0 0 0
3761: 0 0 0 0 0 0 0 1
37 69: 0 0 0 0 0 0 0 0
3777: 0 0 0 0 0 0 0 0
3785: 0 0 1 0 0 0 0 0
3793: 0 0 0 0 0 0 1 0
3801: 0 0 0 0 0 0 1 0
3809: 0 1 0 0 0 0 0 0
3817: 0 0 0 0 0 0 0 0
0182
Channel Data Report 4/17/2018 6:13:44 AM Page 10
3825: 0 0 1 1 0 0 0 0
Sample Title: GAS-1402
Channell------l-------1-------l-------1-------1-------l-------1-------I
3833: 0 0 0 0 0 0 0 1
3841: 0 0 0 0 0 0 0 0
3849: 0 0 0 1 0 0 0 0
3857: 0 1 0 0 0 0 0 0
3865: 0 0 1 0 0 0 0 0
3873: 0 0 0 0 0 0 0 0
3881: 0 0 0 0 0 0 0 0
3889: 0 0 0 0 0 0 0 0
3897: 0 0 0 1 0 1 0 0
3905: 0 0 0 0 0 0 0 0
3913: 1 0 0 0 0 0 0 0
3921: 0 0 0 1 1 1 0 0
3929: 0 0 0 0 1 0 0 0
3937: 0 0 0 0 0 0 0 0
3945: 0 0 0 0 0 0 0 0
3953: 1 0 0 0 0 0 0 0
3961: 0 0 0 0 0 0 0 0
3969: 0 0 0 0 0 0 0 0
3977: 0 0 0 0 0 0 1 0
3985: 0 0 0 1 0 0 0 0
3993: 0 0 1 0 0 0 1 0
4001: 0 0 0 0 0 0 0 0
4009: 0 0 0 0 0 0 0 0
4017: 0 0 0 0 0 0 0 0
4025: 0 0 0 0 0 0 0 0
4033: 0 0 0 0 0 0 0 0
4041: 0 0 0 0 0 0 0 0
4049: 0 0 0 0 0 0 0 0
4057: 0 0 0 0 1 0 0 0
4065: 0 0 0 0 0 1 0 0
4073: 0 0 0 0 0 1 0 0
4081: 0 0 0 0 0 0 0 0
4089: 0 0 0 0 0 0 0 0
0183
105
104
~ 103 ro u V)
en 0 ,
I V)
-1-' C ::::s 0 u
102
101
_. .._,_
' ;,;
!§
,..__
~ 0 u
cr, ~ ~ _. _. ~ ' ' w "' u ~
,..__ _. ' V,
u ~ 0 u ~
0 u
0000064638.CNF Live Time :1800.000 sec Real Time :1821.900 sec Start: 1: 0.S(kev) Stop : 4096:4096.9(kev) Acq. Start :Tue Apr 17 05:42:50 2018
10°~.l.!...l...J__..l....__.l~...L..lLl_L~~.li__J~r~iL4.~L1-~µ_JL_~~Ul__J_L+__J_L_L_-i-J
500 1000 1500 2000 channel
2500 3000
~ L:.:!..2t::J
3500 4000
~ ROI Type: 1 ROI Type: 2
0184
4/17/2018 7:13:55AM
pex-Gamma Analysis Report for 1803111-02
BLANK
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator
Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803111-02
: BLANK
: SOIL
: 7 .834E+02 grams
: Countroom
: 4/16/2018 9:14:44AM
: 4/17/2018 6:13:43AM
: GAS-1602 pCi
: Administrator
: GE1 : GAS-1602
: 3600.0 seconds
: 3600.4 seconds
: 0.01 %
: 2.50
: 1 - 4096
: 19 - 4096
: 1.000 keV
: 2/17/2018
: 2/17/2018
: 64640
PEAK-TO-TOTAL CALIBRATION REPORT
Peak-to-Total Efficiency Calibration Equation
Page 1 of23
l{P lj/;?/18
0185
4/17/2018 7:13:55AM
Analysis Report for 1803111-02
BLANK
PEAK LOCATE REPORT
Peak No.
1 2 3 4 5 6 7 8 9
10 11 12 13 14 15 16 17 18 19 20
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak Search Sensitivity
Energy (keV)
59.52 11 7. 32 130.85 142.42 313.97 388.35 452.29 515.40 677.85 681.23 692.28 820.91 860.62 907.03 918.40 940.14
1091.54 1112.88 1224.87 1813.64
? = Adjacent peak noted
Errors quoted at 2.000sigma
: 4/17/2018 7:13:47AM
: 1 : 4096
: 2.50
Centroid Channel
60.00 117.74 131.27 142.82 314.23 388.54 452.43 515.49 677.81 681.19 692.23 820.76 860.45 906.82 918.18 939.91
1091.21 1112.54 1224.45 1812.93
Centroid Uncertainty
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Page 2 of23
Peak Significance
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0186
M
m M m
4/17/2018 7:13:55AM
Analysis Report for 1803111-02
BLANK
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/17/2018 7:13:47AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI
No. (keV) start
1 59.52 59 -2 11 7. 32 115-3 130.85 12 9 -4 142.42 139 -5 313.97 312 -6 388.35 386 -7 452.29 44 9 -8 515.40 507 -9 677.85 663 -
10 681.23 663 -11 692.28 688 -12 820.91 817 -13 860.62 858 -14 907.03 902 -15 918.40 915 -16 940.14 933 -17 1091.54 1087 -18 1112.88 1109 -19 1224.87 1221 -20 1813.64 1811 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI Peak
end Centroid
68 60.00 121 117.74 133 131.27 147 142.82 316 314.23 392 388.54 455 452.43 522 515.49 686 677.81 686 681.19 695 692.23 823 820.76 863 860.45 912 906.82 922 918.18 945 939.91
1094 1091.21 1114 1112.54 1228 1224.45 1815 1812.93
Net Peak Net Area Area Uncertainty
1.80E+0l 14.93 2.57E+0l 30.77 2.50E+0l 23.80 4.80E+0l 39.59 1.30E+0l 16.95 1.35E+0l 15.17 1. 96E+0l 16.32 1.26E+0l 22.63 1.07E+0l 11. 96 8.84E+00 12.29 1.30E+0l 13 .11 1.33E+0l 11. 36 7.78E+00 6.71 1.07E+0l 14.46 9.63E+00 10.58 1.98E+0l 13. 73 8.15E+00 7.48 6.77E+00 8.43 6.83E+00 7.21 6.13E+00 6.67
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/17/2018 7:13:47AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Page 3 of23
Continuum FWHM Counts (keV)
6.13E+0l 1. 48 1.53E+02 2.71 1.02E+02 2.09 2.12E+02 5.01 5.20E+0l 2.58 3.31E+0l 3.55 3.28E+0l 3.52 4.72E+0l 2. 67 2.00E+0l 2.09 1.91E+0l 2.09 2.00E+0l 2.62 1.35E+0l 2.03 2.44E+00 1. 20 2.26E+0l 3.01 1.28E+0l 3.75 1.25E+0l 6.77 3.70E+00 3.71 8.45E+00 1. 82 4.33E+00 2.91 3.75E+00 2.80
0187
M
4/17/2018 7:13:55AM Page 4 of23
Analysis Report for 1803111-02
M
m M m
BLANK
Peak Energy ROI
No. (keV) start
1 59.52 59 -2 11 7. 32 115 -3 130.85 12 9 -4 142.42 139 -5 313.97 312 -6 388.35 386 -7 452.29 44 9 -8 515.40 507 -9 677.85 663 -
10 681.23 663 -11 692.28 688 -12 820.91 81 7 -13 860.62 858 -14 907.03 902 -
15 918.40 915 -16 940.14 933 -17 1091.54 1087 -
18 1112.88 1109 -19 1224.87 1221 -20 1813.64 1811 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Net Peak Net Area Continuum
end Area Uncertainty Counts
68 1.80E+0l 14.93 6.13E+01
121 2.57E+0l 30.77 1.53E+02
133 2.50E+0l 23.80 1.02E+02
147 4.80E+0l 39.59 2.12E+02
316 1.30E+0l 16.95 5.20E+01
392 1.35E+0l 15.17 3.31E+01
455 1.96E+0l 16.32 3.28E+01
522 1.26E+0l 22.63 4. 72E+0l
686 1.07E+0l 11. 96 2.00E+0l
686 8.84E+00 12.29 l.91E+01
695 1.30E+0l 13 .11 2.00E+0l
823 1.33E+0l 11. 36 1.35E+0l
863 7.78E+00 6.71 2.44E+00
912 1.07E+0l 14.46 2.26E+0l
922 9.63E+00 10.58 1.28E+0l
945 1.98E+0l 13.73 1.25E+0l
1094 8.15E+00 7.48 3.70E+00
1114 6.77E+00 8.43 8.45E+00
1228 6.83E+00 7.21 4.33E+00
1815 6.13E+00 6.67 3.75E+00
PEAK WITH NID REPORT
Peak Analysis Performed on : 4/17/2018 7:13:47AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Tentative NID Library
Peak Match Tolerance
Peak Energy
No. (keV)
1 59.52 2 11 7. 32 3 130.85
: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB
: 1.000 keV
ROI ROI Peak Net Peak
start end Centroid Area
59 - 68 60.00 1.80E+0l
115 - 121 117.74 2.57E+0l
12 9 - 133 131.27 2.50E+0l
Net Area Continuum Uncertainty Counts
14.93 6.13E+0l 30.77 1.53E+02 23.80 1.02E+02
Critical Level
1.29E+0l 2.39E+0l 1.78E+0l 3.05E+0l 1.26E+01 1.09E+01 1.13E+01 l.13E+01 7.36E+00 7.18E+00 9.0lE+00 7.17E+00 3.06E+00 1.06E+0l 7.05E+00 8.60E+00 3.98E+00 5.45E+00 4.08E+00 3.68E+00
Tentative Nuclide
AM-241
PA-234
0188
4/17/2018 7:13:55AM
Analysis Report for 1803111-02
m M m
M
m M m
BLANK
Peak Energy ROI
No. (keV) start
4 142.42 13 9 -5 313.97 312 -6 388.35 386 -7 452.29 44 9 -8 515.40 507 -9 677.85 663 -
10 681.23 663 -11 692.28 688 -12 820.91 81 7 -13 860.62 858 -14 907.03 902 -15 918.40 915 -16 940.14 933 -17 1091.54 1087 -18 1112.88 1109 -19 1224.87 1221 -20 1813.64 1811 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area
end Centroid Area Uncertainty
147 142.82 4.80E+0l 39.59
316 314.23 1.30E+0l 16.95
392 388.54 1.35E+0l 15.17
455 452.43 1. 96E+0l 16.32
522 515.49 1.26E+0l 22.63
686 677.81 1.07E+0l 11. 96
686 681.19 8.84E+00 12.29
695 692.23 1.30E+0l 13 .11
823 820.76 1.33E+0l 11. 36
863 860.45 7.78E+00 6.71
912 906.82 1.07E+0l 14.46
922 918.18 9.63E+00 10.58
945 939.91 1.98E+0l 13.73
1094 1091.21 8.15E+00 7.48
1114 1112.54 6.77E+00 8.43
1228 1224.45 6.83E+00 7.21
1815 1812.93 6.13E+00 6.67
PEAK EFFICIENCY REPORT
Peak Analysis Performed on : 4/17/2018 7:13:47AM
Peak Energy Net Peak Net Area Peak
No. (keV) Area Uncertainty Efficiency
1 59.52 1.80E+0l 14.93 2.50E-02
2 117.32 2.57E+0l 30.77 2.76E-02
3 130.85 2.50E+0l 23.80 2.67E-02
4 142.42 4.80E+0l 39.59 2.59E-02
5 313.97 1.30E+0l 16.95 1.64E-02
6 388.35 1.35E+0l 15 .17 1.41E-02
7 452.29 1.96E+0l 16.32 1.26E-02
8 515.40 1.26E+01 22.63 l.14E-02
9 677.85 1.07E+01 11. 96 9.15E-03
10 681.23 8.84E+00 12.29 9.12E-03
11 692.28 1.30E+0l 13 .11 9.00E-03
12 820.91 1.33E+01 11. 36 7.85E-03
13 860.62 7.78E+00 6. 71 7.56E-03
Page 5 of23
Continuum Tentative Counts Nuclide
2.12E+02 5.20E+0l 3.31E+0l 3.28E+0l 4.72E+0l 2.00E+0l AG-ll0M 1.91E+0l 2.00E+0l 1.35E+0l 2.44E+00 TL-208 2.26E+0l 1.28E+0l 1.25E+0l 3.70E+00 8.45E+00 EU-152 4.33E+00 3.75E+00
Efficiency Uncertainty
1.85E-03 2.24E-03 2.36E-03 2.56E-03 2.44E-03 2.17E-03 1.87E-03 1.57E-03 9.0lE-04 9.05E-04 9.22E-04 1.llE-03 1.17E-03
0189
4/17/2018 7:13:55AM Page 6 of23
Analysis Report for 1803111-02
M
m M m
BLANK
Peak Energy
Na. (keV)
14 907.03 15 918.40 16 940.14 17 1091.54 18 1112.88 19 1224.87 20 1813.64
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000 sigma
Net Peak Area
l.07E+0l 9.63E+00 l.98E+01 8.15E+00 6.77E+00 6.83E+00 6. 13E+00
Net Area Uncertainty
14.46 10.58 13.73
7.48 8.43 7.21 6.67
Peak Efficiency
7.25E-03 7.18E-03 7.04E-03 6.25E-03 6.16E-03 5.71E-03 4.27E-03
Efficiency Uncertainty
l.20E-03 l.17E-03 1. llE-03 7.27E-04 6.73E-04 5.03E-04 4.77E-04
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on : 4/17/2018 7:13:47AM
Env. Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CNF
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
1 59.52 1.80E+0l 14.93 1.80E+0l 1.49E+0l
2 117. 32 2.57E+0l 30.77 2.57E+0l 3.08E+0l
3 130.85 2.50E+0l 23.80 2.50E+0l 2.38E+0l
4 142.42 4.80E+0l 39.59 4.80E+0l 3.96E+0l
5 313.97 1.30E+0l 16.95 1.30E+0l 1.69E+0l
6 388.35 1.35E+0l 15.17 1.35E+0l 1.52E+0l
7 452.29 1.96E+0l 16.32 1.96E+0l 1.63E+0l
8 515.40 1.26E+0l 22.63 1.26E+0l 2.26E+0l
9 677.85 1.07E+0l 11. 96 1.07E+0l 1.20E+0l
10 681. 23 8.84E+00 12.29 8.84E+00 1.23E+0l
11 692.28 1.30E+0l 13 .11 1.30E+0l 1.31E+0l
12 820.91 1.33E+0l 11. 36 1.33E+0l l.14E+0l
13 860.62 7.78E+00 6.71 7.78E+00 6.71E+00
14 907.03 1.07E+0l 14.46 1.07E+0l l.45E+0l
15 918.40 9.63E+00 10.58 9.63E+00 1.06E+0l
16 940.14 1.98E+0l 13. 73 1.98E+0l 1.37E+0l
17 1091.54 8.15E+00 7.48 8.15E+00 7.48E+00
18 1112.88 6.77E+00 8.43 6.77E+00 8.43E+00
19 1224.87 6.83E+00 7.21 6.83E+00 7.21E+00
20 1813.64 6.13E+00 6.67 6.13E+00 6.67E+00
0190
4/17/2018 7:13:55AM Page 7 of 23
Analysis Report for 1803111-02
BLANK
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
AREA CORRECTION REPORT
REFERENCE PEAK I 8KG. SUBTRACT
Peak Analysis Performed on
Ref. Peak Energy
Peak Ratio
Background File
: 4/17/2018 7:13:47AM
: 0.00 Reference Date
: 0.00 Uncertainty : 0.00
: \\0 R-GAMMA 1 \ApexRoot\Countroom\Data\0000063824.CN F
Corrected Area is: Original * Peak Ratio - Background
Peak Energy Original Orig. Area Ambient Backgr.
No. (keV) Area Uncertainty Background Uncert.
M 1 59.52 l.80E+0l 14.93
2 117. 32 2.57E+0l 30.77
3 130. 85 2.50E+0l 23.80
4 142.42 4.80E+01 39.59
5 313.97 1.30E+0l 16.95
6 388.35 1.35E+0l 15.17
7 452.29 1. 96E+0l 16.32
m 8 515.40 1.26E+0l 22.63
M 9 677.85 1.07E+0l 11. 96
m 10 681.23 8.84E+00 12.29
11 692.28 1.30E+0l 13 .11
12 820.91 1.33E+0l 11. 36
13 860.62 7.78E+00 6.71
14 907.03 1.07E+01 14.46
15 918.40 9.63E+00 10.58
16 940.14 l.98E+0l 13.73
17 1091.54 8.15E+00 7.48
18 1112.88 6.77E+00 8.43
19 1224.87 6.83E+00 7.21
20 1813.64 6.13E+00 6.67
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
Corrected Area
1.80E+0l 2.57E+0l 2.50E+0l 4.80E+0l 1.30E+0l 1.35E+0l 1. 96E+0l 1.26E+0l 1.07E+0l 8.84E+00 1.30E+0l 1.33E+0l 7. 78E+00 1.07E+0l 9.63E+00 l.98E+0l 8.15E+00 6.77E+00 6.83E+00 6.13E+00
Corrected Uncert.
l.49E+0l 3.08E+0l 2.38E+0l 3.96E+0l 1.69E+0l 1.52E+0l 1.63E+0l 2.26E+0l 1.20E+0l l.23E+0l 1.31E+0l l.14E+0l 6.71E+00 1.45E+0l 1.06E+0l l.37E+0l 7.48E+00 8.43E+00 7.21E+00 6.67E+00
0191
4/17/2018 7:13:55AM
Analysis Report for 1803111-02
BLANK
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Nuclide Name Id Confidence
PA-234 0.425
AM-241 1.000
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
Energy (keV)
131. 20 * 733.99 946.00
59.54 *
Yield(%)
20.40 8.80
12.00 35.90
UNIDENTIFIED PEAKS
m M m
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
2 117. 32 4 142.42 5 313.97 6 388.35 7 452.29 8 515.40 9 677.85
10 681.23 11 692.28 12 820.91 13 860.62 14 907.03 15 918.40
: 4/17/2018 7:13:47AM
: 1 : 4096
Peak Size (CPS)
7.13508£-03 1.33342£-02 3.60755£-03 3. 73611£-03 5.44753£-03 3. 5071 7E-03 2.96349£-03 2.45691£-03 3.60507£-03 3.68056£-03 2.16049£-03 2. 9671 7E-03 2.67361£-03
Peak CPS(%) Uncertainty
59.90 41.24 65.25 56.41 41.62 89.61 56.04 69.46 50.53 42.86 43.12 67. 67 54.98
Activity
(pCi/grams)
4.40E-02
1.92E-02
Peak Type
Tol.
Tol.
Page 8 of23
Activity
Uncertainty
4.20E-02
1.60E-02
Tolerance Nuclide
AG-ll0M
TL-208
0192
4/17/2018 7:13:55AM Page 9 of23
Analysis Report for 1803111-02
BLANK
Peak No. Energy (ke V)
16 940.14 17 1091.54 18 1112.88 19 1224.87 20 1813.64
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
Peak Size (CPS) Peak CPS(%) Peak Tolerance
Uncertainty Type Nuclide
5.49145E-03 34. 72 2.26389E-03 45.91 1.88131E-03 62.21 Tol. EU-152
1.89815E-03 52.76 1.70139E-03 54.46
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy
Name Confidence (keV)
PA-234 0.42 131.20 733.99 946.00
AM-241 1.00 59.54
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
*
*
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
Yield(%)
20.40 8.80
12.00 35.90
Activity
(pCi!grams)
4.40E-02
1.92E-02
Activity
Uncertainty
4.20E-02
l.60E-02
INTERFERENCE CORRECTED REPORT
0193
Analysis Report for 1803111-02
BLANK
Nuclide Name
PA-234 AM-241
Nuclide Id
Confidence
0.425 1.000
? nuclide is part of an undetermined solution
X = nuclide rejected by the interference analysis
4/17/2018 7: 13:55AM
Wt mean Wt mean
Activity Activity
(pCilgrams) Uncertainty
4.40E-02 4.20E-02 1.92E-02 1.60E-02
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Page 10 of23
Comments
0194
Analysis Report for 1803111-02
m M
m
BLANK
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (ke V)
2 11 7. 32
4 142.42
5 313.97
6 388.35
7 452.29
8 515.40
9 677.85
10 681.23
11 692.28
12 820.91
13 860.62
14 907.03
15 918.40
16 940.14
17 1091.54
18 1112.88
19 1224.87
20 1813.64
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 7:13:55AM
UNIDENTIFIED PEAKS
: 4/17/2018 7:13:47AM
: 1 : 4096
Peak Size (CPS)
7 .13508E-03
1.33342E-02
3.60755E-03
3. 73611E-03
5.44753E-03
3.50717E-03
2. 9634 9E-03
2.45691E-03
3.60507E-03
3.68056E-03
2.16049E-03
2. 96717E-03
2.67361E-03
5.49145E-03
2.26389E-03
1. 88131E-03
1.89815E-03
1. 70139E-03
Peak CPS(%) Uncertainty
59.90
41.24
65.25
56.41
41.62
89.61
56.04
69.46
50.53
42.86
43.12
67.67
54.98
34.72
45.91
62.21
52.76
54.46
NUCLIDE MDA REPORT
Peak Type
Tol.
Tol.
Tol.
Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB
Nuclide Name
Energy
(keV)
Yield(%) Activity
(pCilgrams) Nuclide MDA
(pCilgrams)
Line MDA
(pCi/grams)
Page 11 of23
Tolerance Nuclide
AG-ll0M
TL-208
EU-152
0195
4/17/2018 7:13:55AM Page 12 of23
Analysis Report for 1803111-02
BLANK
+ BE-7 477.59 10.42 8.60E-03 2.21E-01 2.21E-01
+ NA-22 1274.54 99.94 -1.0lE-02 1.87E-02 1.87E-02
+ NA-24 1368.53 99.99 8.32E-03 2.12E-02 3.18E-02
2754.09 99.86 -9.58E-04 2.12E-02
+ AL-26 1808.65 99.76 6.74E-03 3.57E-02 3.57E-02
+ K-40 1460.81 10.67 1.62E-0l 3.39E-01 3.39E-01
+ AR-41 1293.64 99.16 1.52E+0l 8.58E+01 8.58E+0l
+ TI-44 67.88 94.40 1.76E-03 1.79E-02 1.86E-02
78.34 96. 00 8.90E-04 1.79E-02
+ SC-46 889.25 98.98 5.77E-03 2.07E-02 2.66E-02
1120.51 99.90 -1.58E-02 2.07E-02
+ V-48 983.52 99.98 5.13E-03 2.20E-02 2.20E-02
1312.10 97.50 7.55E-03 2. 27E-02
+ CR-51 320.08 9.83 -4.74E-02 2.19E-01 2.19E-01
+ MN-54 834.83 99.97 7.03E-03 2.78E-02 2.78E-02
+ CO-56 846.75 99. 96 8.91E-03 3.39E-02 3.39E-02
1037.75 14.03 1.02E-01 2.32E-01
1238.25 67.00 -1.59E-02 3.59E-02
1771.40 15.51 0.00E+00 3.89E-02
2587.48 16.90 -2.49E-02 1.79E-01
+ CO-57 122.06 85.51 6.82E-03 1.71E-02 1.71E-02
136.48 10.60 7.57E-03 1.33E-01
+ CO-58 810.76 99.40 -1.38E-03 2.61E-02 2.61E-02
+ FE-59 1099.22 56.50 2. 96E-03 4.15E-02 4.15E-02
1291.56 43.20 -8.21E-03 4.93E-02
+ CO-60 1173.22 100.00 9.59E-03 2.53E-02 2.94E-02
1332.49 100.00 0.00E+00 2.53E-02
+ ZN-65 1115.52 50.75 -1.18E-02 5.59E-02 5.59E-02
+ GA-67 93.31 35.70 l.48E-01 8.16E-02 8.16E-02
208.95 2.24 -3.64E-01 9.08E-01
300.22 16.00 -2.17E-02 1.49E-01
+ SE-75 121.11 16.70 3.49E-02 2.36E-02 8.78E-02
136.00 59.50 -7.44E-03 2.36E-02
264.65 59.80 -5.l0E-03 3.51E-02
279.53 25.20 -9.32E-03 7.14E-02
400.65 11. 40 -1.04E-0l 1.73E-01
+ RB-82 776.52 13. 00 6.96E-02 1.96E-01 1.96E-01
+ RB-83 520.41 46.00 -3.15E-02 4.66E-02 4.66E-02
529.64 30.30 1.97E-03 7.31E-02
552.65 16.40 3.89E-02 1.26E-01
+ KR-85 513.99 0.43 8.44E+00 8.75E+00 8.75E+00
+ SR-85 513.99 99. 27 3.73E-02 3.86E-02 3.86E-02
+ Y-88 898.02 93.40 1.53E-03 1.99E-02 1.99E-02
1836.01 99.38 -2.29E-03 2.75E-02
+ MO-93 263.06 56. 72 9.28E-03 1.99E-02 3.77E-02
684.67 99.68 -9.18E-03 1.99E-02
1477 .11 99.08 5.87E-03 2.35E-02
+ NB-93M 16.57 9.43 -1.17E+00 3.51E+00 3.51E+00
+ NB-94 702.63 100.00 -2.21E-02 2.42E-02 2.42E-02
871.10 100.00 -1.53E-03 2.49E-02
+ NB-95 765.79 99.81 -1.86E-04 2.71E-02 2.71E-02
0196
4/17/2018 7:13:55AM Page 13 of23
Analysis Report for 1803111-02
BLANK
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)
+ NB-95M 235.69 25.00 -5.63E-02 8.23E-02 8.23E-02
+ ZR-95 724.18 43.70 -8.83E-03 4.69E-02 4.97E-02
756.72 55.30 -l.80E-02 4.69E-02
+ MO-99 181.06 6.20 -1.32E-01 2.21E-0l 3.26E-01
739.58 12.80 3.77E-02 2. 21E-01
778.00 4.50 -2.49E-01 5.90E-01
+ TC-99M 140.51 89.00 -2.79E-04 1.90E-02 l.90E-02
+ RU-103 497.08 89.00 -9.88E-03 2.34E-02 2.34E-02
+ RU-106 621.84 9.80 5.07E-02 2.64E-01 2.64E-01
+ AG-108M 433.93 89.90 2.13E-03 2.39E-02 2.39E-02
614.37 90.40 -4.16E-03 2.97E-02
722.95 90.50 -2.18E-03 2.45E-02
+ CD-109 88.03 3. 72 -3.42E-01 4.48E-0l 4.48E-01
+ AG-ll0M 657.75 93.14 l.l0E-03 2.28E-02 2.28E-02
677.61 10.53 1.54E-01 2.63E-01
706.67 16.46 -l.62E-02 1.74E-01
763.93 21.98 7.90E-02 l.36E-01
884.67 21.98 -3.25E-02 1.22E-01
1384.27 23.94 9.65E-03 9.28E-02
+ CD-113M 263.70 0.02 -1.21E-01 9.06E+0l 9.06E+0l
+ SN-113 255.12 1.93 2.37E-02 3.04E-02 8.78E-01
391.69 64.90 -6.90E-03 3.04E-02
+ TE-123M 159.00 84.10 9.71E-03 2.l0E-02 2.l0E-02
+ SB-124 602.71 97.87 -1.66E-02 2.86E-02 2.86E-02
645.85 7.26 2.03E-01 3.30E-01
722.78 11. 10 -1. 79E-02 2.02E-01
1691.02 49.00 1.54E-02 6.62E-02
+ I-125 35.49 6.49 8.07E-02 4.96E-01 4.96E-01
+ SB-125 176.33 6.89 2.80E-02 6.82E-02 2.37E-01
427.89 29.33 -2.l0E-02 6.82E-02
463.38 10.35 -l.29E-02 2.18E-01
600.56 17.80 4.52E-02 l.64E-01
635.90 11. 32 3.54E-02 2.07E-01
+ SB-126 414.70 83.30 -l.61E-02 2.15E-02 2.15E-02
666.33 99.60 4.15E-03 2.69E-02
695.00 99.60 -3.57E-03 2.58E-02
720.50 53.80 7.66E-03 4.36E-02
+ SN-126 87.57 37.00 -3.43E-02 4.50E-02 4.50E-02
+ SB-127 473.00 25.00 -5.32E-02 6.54E-02 9.64E-02
685.00 35.70 -3.0lE-02 6.54E-02
783.80 14.70 3.55E-02 2. llE-01
+ I-129 29.78 57.00 2.59E-02 9.33E-02 9.33E-02
33.60 13.20 -6.62E-02 2.81E-01
39.58 7.52 4.63E-02 3.64E-01
+ I-131 284.30 6.05 -6.48E-02 2.75E-02 3.09E-01
364.48 81.20 1.82E-03 2.75E-02
636.97 7.26 1.48E-01 3.64E-01
722.89 1. 80 -1.18E-01 l.33E+00
0197
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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)
+ TE-132 49. 72 13 .10 -2.95E-01 2.16E-02 1.60E-01
228.16 88.00 -1.50E-03 2.16E-02
+ BA-133 81.00 33.00 -1.14E-02 3.18E-02 5.12E-02
302.84 17.80 -6.35E-02 1.02E-01
356.01 60.00 -2.24E-02 3.18E-02
+ I-133 529.87 86.30 1.41E-03 5. 21E-02 5.21E-02
+ XE-133 81.00 38.00 -1. llE-02 5.00E-02 5.00E-02
+ CS-134 563.23 8.38 -2.03E-02 3.13E-02 2.36E-01
569.32 15.43 -8.03E-02 l.15E-01
604.70 97. 60 2.51E-03 3.15E-02
795.84 85.40 3.49E-04 3.13E-02
801.93 8.73 -2.06E-02 3.08E-01
+ CS-135 268.24 16.00 3.94E-02 1.33E-0l l.33E-01
+ I-135 1131.51 22.50 -8.57E-02 8.56E-01 1.00E+00
1260.41 28.60 8.56E-02 8.56E-01
1678.03 9.54 -4.77E-01 2.55E+00
+ CS-136 153.22 7.46 -1.23E-01 2.94E-02 2.06E-01
163.89 4.61 l.14E-01 3.60E-01
176.55 13.56 1.49E-02 1.26E-01
273.65 12.66 -l.l0E-02 l.73E-01
340.57 48.50 -l.68E-02 4.49E-02
818.50 99.70 -4.27E-04 2.94E-02
1048.07 79.60 8.60E-03 4.05E-02
1235.34 19.70 -8.09E-02 l.18E-01
+ CS-137 661.65 85.12 2.41E-03 2. 71E-02 2.71E-02
+ LA-138 788.74 34.00 -6.95E-03 3.77E-02 7.99E-02
1435.80 66.00 l.44E-02 3.77E-02
+ CE-139 165.85 80.35 -3.77E-03 1.83E-02 l.83E-02
+ BA-140 162. 64 6.70 3.81E-02 9.84E-02 2.54E-01
304.84 4.50 -1.56E-01 4.24E-01
423.70 3.20 2.63E-01 7.39E-01
437.55 2.00 -l.43E-02 1.l0E+00
537.32 25.00 -2.98E-02 9.84E-02
+ LA-140 328.77 20.50 -4.05E-02 2.43E-02 9.58E-02
487.03 45.50 -5.08E-04 5.49E-02
815.85 23.50 4.07E-03 l.06E-01
1596.49 95.49 0.00E+00 2.43E-02
+ CE-141 145.44 48.40 -5. 96E-03 3.46E-02 3.46E-02
+ CE-143 57.36 11. 80 1.00E-01 7.48E-02 2.54E-01
293.26 42.00 -2. 96E-02 7.48E-02
664.55 5.20 l.23E-01 8.08E-01
+ CE-144 133.54 10.80 -3.88E-02 1.30E-01 l.30E-01
+ PM-144 476.78 42.00 -1.27E-02 2.64E-02 5.18E-02
618.01 98.60 -6.19E-03 2.66E-02
696.49 99.49 4.52E-03 2.64E-02
+ PM-145 36.85 21.70 -4. 96E-02 7.54E-02 1.37E-01
37.36 39.70 -1.12E-02 7.54E-02
42.30 15.10 -6.91E-02 1.67E-01
72. 40 2.31 -6.58E-02 7.19E-01
0198
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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCilgrams) (pCilgrams) (pCi!grams)
+ PM-146 453.90 39.94 -6.23E-03 5.56E-02 5.56E-02
735.90 14.01 -1.05E-01 1.39E-01
747.13 13.10 -4.99E-02 1.57E-01
+ ND-147 91.11 28.90 1. 72E-01 8.97E-02 8.97E-02
531.02 13.10 -1.40E-02 1.78E-01
+ PM-149 285.90 3.10 -2.09E-02 7.76E-01 7.76E-01
+ EU-152 121.78 20.50 2.83E-02 7.13E-02 7. 13E-02
244.69 5.40 -1.36E-01 3.04E-01
344.27 19 .13 2.29E-02 1.17E-01
778.89 9.10 -1.61E-01 2.42E-01
964.01 10.40 5.76E-02 2.85E-01
1085.78 7.22 -1.06E-02 2.28E-01
1112.02 9.60 4.20E-02 2.94E-01
1407.95 14.94 -2.71E-02 1.35E-01
+ GD-153 97.43 31.30 -2.82E-02 5.03E-02 5.03E-02
103.18 22.20 3.28E-03 6.58E-02
+ EU-154 123.07 40.50 1.83E-03 3.47E-02 3.47E-02
723. 30 19.70 -1.00E-02 1.13E-01
873.19 11. 50 -3.98E-02 2.24E-01
996.32 10.30 -1.26E-03 2.51E-01
1004.76 17.90 -8.15E-02 1.13E-01
1274.45 35.50 -2.84E-02 5.25E-02
+ EU-155 86.50 30.90 1.18E-03 5.55E-02 5.55E-02
105.30 20.70 -l.83E-02 7.02E-02
+ EU-156 811.77 10.40 9.66E-02 2.65E-01 2.65E-01
1153.47 7.20 -5.79E-02 3.67E-01
1230.71 8.90 5.77E-02 3.13E-01
+ HO-166M 184.41 72.60 3.07E-02 3.04E-02 3.04E-02
280.45 29.60 -1.50E-02 5.86E-02
410.94 11.10 l.43E-02 1.83E-01
711.69 54.10 5.66E-03 5.59E-02
+ TM-171 66.72 0.14 -1.64E+0l 1.35E+0l 1.35E+0l
+ HF-1 72 67.35 5.31 3.14E-02 1.29E-01 3.31E-01
125.82 11. 30 -2.58E-03 1.29E-01
+ LU-1 72 181.53 20.60 -1.87E-01 5.07E-02 8.14E-02
900.72 29.81 -1.61E-03 6.82E-02
1093.66 62.50 2.69E-03 5.07E-02
+ LU-173 100. 72 5.24 -2.56E-03 9.83E-02 2.98E-01
272 .11 21. 20 -7.64E-03 9.83E-02
+ HF-175 343.40 84.00 5.25E-03 2.69E-02 2.69E-02
+ LU-176 88.34 13. 30 -3.72E-01 l.88E-02 1.26E-0l
201.83 86.00 -l.22E-02 1.88E-02
306.78 94.00 6.87E-03 2.07E-02
+ HF-181 133.02 41.70 -9.00E-03 2.64E-02 3.61E-02
345.85 17.20 -5. 79E-04 1.33E-01
482.03 82.80 -l.07E-02 2.64E-02
+ TA-182 67.75 41.20 4.05E-03 4.28E-02 4.28E-02
1121. 30 34.90 0.00E+00 7.86E-02
1189.05 16.23 -2.76E-02 1.53E-01
0199
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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)
TA-182 1221.41 26.98 -3.12E-03 4.28E-02 8.18E-02
1231.02 11. 44 7.40E-02 2.35E-01
+ IR-192 308.46 29.68 -4.07E-03 4.56E-02 6.58E-02
468.07 48.10 1.70E-04 4.56E-02
+ HG-203 279.19 77. 30 6.45E-03 2.51E-02 2.51E-02
+ TL-204 374.74 94 .11 -3.52E-03 1.99E-02 1.99E-02
899.15 99.16 3.97E-03 1.99E-02
911.74 91.10 2.92E-03 2.64E-02
+ BI-207 569.67 97. 72 -1.55E-02 1.82E-02 1.82E-02
1063.62 74.90 -1.30E-02 2.41E-02
+ TL-208 583.14 30.22 -5.60E-03 7.99E-02 7.99E-02
860.37 4.48 6.36E-02 4.93E-01
2614.66 35.85 7.03E-02 l.30E-01
+ BI-210M 262.00 45.00 -4.19E-03 4.68E-02 4.68E-02
300.00 23.00 -1.25E-02 8.59E-02
+ PB-210 46.50 4.25 3.72E-01 5.55E-01 5.55E-01
+ PB-211 404.84 2.90 -3.48E-01 6.51E-01 6.51E-01
831. 96 2.90 -1.83E-01 8.0lE-01
+ BI-212 727.17 11. 80 -9.39E-02 1.70E-01 1.70E-01
1620.62 2.75 3.77E-01 1.13E+00
+ PB-212 238.63 44.60 4.19E-02 4.68E-02 4.68E-02
300.09 3.41 -8.40E-02 5.80E-01
+ BI-214 609.31 46.30 2.99E-02 6.90E-02 6.90E-02
1120.29 15.10 -l.04E-01 1.36E-01
1764.49 15.80 6.97E-02 l.83E-01
2204.22 4.98 -1.79E-01 5.51E-01
+ PB-214 295.21 19.19 1.37E-02 6.34E-02 l.12E-01
351.92 37.19 2.52E-02 6.34E-02
+ RN-219 401.80 6.50 -1.46E-02 3.16E-01 3.16E-01
+ RA-223 323.87 3.88 2.78E-01 5.68E-01 5.68E-01
+ RA-224 240.98 3.95 2.llE-01 4.98E-01 4.98E-01
+ RA-225 40.00 31.00 1.15E-02 9.04E-02 9.04E-02
+ RA-226 186.21 3.28 9.60E-01 6.87E-01 6.87E-01
+ TH-227 50.10 8.40 -2.29E-02 1.51E-01 2.17E-01
236.00 11. 50 -1.03E-01 1.51E-01
256.20 6.30 -8.07E-03 3.18E-01
+ AC-228 338.32 11. 40 2.70E-03 9.02E-02 l.85E-01
911.07 27.70 9.58E-03 9.02E-02
969 .11 16.60 -4.73E-02 1.52E-01
+ TH-230 48.43 16.90 -4.60E-02 1.16E-01 1.16E-01
62.85 4.60 3.63E-01 5.26E-01
67.67 0.37 4.49E-01 4.74E+00
+ PA-231 283.67 1. 60 -5.23E-02 7.86E-01 1.08E+00
302.67 2.30 -4.91E-01 7.86E-01
+ TH-231 25.64 14.70 -5.91E+00 2.77E-0l 7.13E-01
84.21 6.40 1.38E-01 2.77E-01
+ PA-233 311.98 38.60 -3.85E-03 5.73E-02 5.73E-02
+ PA-234 131.20 * 20.40 4.40E-02 6.72E-02 6. 72E-02
0200
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Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCilgrams) (pCi/grams) (pCi/grams)
PA-234 733.99 8.80 5.52E-02 6.72E-02 2.55E-01
946.00 12.00 -5.70E-02 1.81E-01
+ PA-234M 1001.03 0.92 3.50E-01 2.93E+00 2.93E+00
+ TH-234 63.29 3.80 1.08E+00 6.57E-01 6.57E-01
+ U-235 143.76 10.50 8.49E-02 1.70E-01 1.70E-01
163.35 4.70 l.06E-01 3.36E-01
205.31 4.70 3.18E-02 3.77E-01
+ NP-237 86.50 12.60 2.89E-03 l.36E-01 l.36E-01
+ NP-239 106.10 22.70 -2.00E-02 8.18E-02 8.18E-02
228.18 10.70 -3.45E-03 l.95E-01
277.60 14.10 1.0lE-01 1.84E-01
+ AM-241 59.54 * 35.90 l.92E-02 7.75E-02 7.75E-02
+ AM-243 74.67 66.00 -7.05E-04 2.59E-02 2.59E-02
+ CM-243 209.75 3.29 -l.13E-01 1.43E-01 5.29E-01
228.14 10.60 -l.03E-02 l.48E-01
277.60 14.00 7.81E-02 1.43E-01
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCilgrams)
BE-7 477.59 10.42 2.21E-01 2. 21E-01 8.60E-03 1.00E-01
NA-22 1274.54 99.94 l.87E-02 l.87E-02 -1.0lE-02 6.98E-03
NA-24 1368.53 99.99 3.18E-02 2.12E-02 8.32E-03 1.35E-02
2754.09 99.86 2.12E-02 -9.58E-04 6.69E-03
AL-26 1808.65 99.76 3.57E-02 3.57E-02 6.74E-03 1.48E-02
K-40 1460.81 10.67 3.39E-01 3.39E-01 1.62E-01 1.45E-01
0201
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Analysis Report for 1803111-02
BLANK
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams) (pCi/grams)
AR-41 1293.64 99.16 8.58E+0l 8.58E+0l 1.52E+0l 3.47E+0l
TI-44 67.88 94.40 1. 8 6E-02 1.79E-02 1.76E-03 8.76E-03
78.34 96. 00 1.79E-02 8.90E-04 8.49E-03
SC-46 889.25 98.98 2.66E-02 2.07E-02 5.77E-03 1.15E-02
1120.51 99.90 2.07E-02 -1.58E-02 8. 21E-03
V-48 983.52 99.98 2.20E-02 2.20E-02 5.13E-03 9.03E-03
1312.10 97.50 2.27E-02 7.55E-03 8.78E-03
CR-51 320.08 9.83 2.19E-01 2.19E-01 -4.74E-02 1. 0lE-01
MN-54 834.83 99.97 2.78E-02 2.78E-02 7.03E-03 1.22E-02
CO-56 846.75 99. 96 3.39E-02 3.39E-02 8.91E-03 1.53E-02
1037.75 14.03 2.32E-01 1.02E-01 1.02E-01
1238.25 67.00 3.59E-02 -l.59E-02 1.45E-02
1771.40 15.51 3.89E-02 0.00E+00 0.00E+00
2587.48 16.90 1.79E-01 -2.49E-02 6.70E-02
CO-57 122.06 85.51 1.71E-02 l.71E-02 6.82E-03 8.0lE-03
136.48 10.60 1.33E-01 7.57E-03 6.20E-02
CO-58 810.76 99.40 2.61E-02 2.61E-02 -1.38E-03 1.14E-02
FE-59 1099.22 56.50 4.15E-02 4.15E-02 2. 96E-03 1.70E-02
1291.56 43.20 4.93E-02 -8.21E-03 1.91E-02
CO-60 1173.22 100.00 2.94E-02 2.53E-02 9.59E-03 1.25E-02
1332.49 100.00 2.53E-02 0.00E+00 l.02E-02
ZN-65 1115.52 50.75 5.59E-02 5.59E-02 -l.18E-02 2.38E-02
GA-67 93.31 35.70 8.16E-02 8.16E-02 1.48E-01 3.93E-02
208.95 2.24 9.08E-01 -3.64E-01 4.21E-01
300.22 16.00 1.49E-01 -2.17E-02 6.90E-02
SE-75 121.11 16.70 8.78E-02 2.36E-02 3.49E-02 4. llE-02
136. 00 59.50 2.36E-02 -7.44E-03 l.l0E-02
264.65 59.80 3.51E-02 -5.l0E-03 l.64E-02
27 9. 53 25.20 7.14E-02 -9.32E-03 3.28E-02
400.65 11. 40 1.73E-01 -1.04E-01 7.83E-02
RB-82 776.52 13.00 1.96E-0l 1.96E-01 6. 96E-02 8.56E-02
RB-83 520.41 46.00 4.66E-02 4.66E-02 -3.15E-02 2.08E-02
529.64 30.30 7.31E-02 1.97E-03 3. 27E-02
552.65 16.40 1.26E-01 3.89E-02 5.55E-02
KR-85 513.99 0.43 8.75E+00 8.75E+00 8.44E+00 4. llE+00
SR-85 513.99 99. 27 3.86E-02 3.86E-02 3.73E-02 1.82E-02
Y-88 898.02 93.40 1.99E-02 1.99E-02 1.53E-03 8.05E-03
1836.01 99.38 2.75E-02 -2.29E-03 l.07E-02
MO-93 263.06 56. 72 3.77E-02 1.99E-02 9.28E-03 1.76E-02
684.67 99.68 1.99E-02 -9.18E-03 8.53E-03
1477.11 99.08 2.35E-02 5.87E-03 9.l0E-03
NB-93M 16.57 9.43 3.51E+00 3.51E+00 -l.17E+00 1.58E+00
NB-94 702.63 100.00 2.42E-02 2.42E-02 -2. 21E-02 1.06E-02
871.10 100.00 2.49E-02 -1.53E-03 1.07E-02
NB-95 765.79 99.81 2.71E-02 2.71E-02 -1.86E-04 l.19E-02
NB-95M 235.69 25.00 8.23E-02 8.23E-02 -5.63E-02 3.80E-02
ZR-95 724.18 43.70 4.97E-02 4.69E-02 -8.83E-03 2.14E-02
756.72 55.30 4.69E-02 -1. 80E-02 2.06E-02
MO-99 181.06 6.20 3.26E-01 2. 21E-01 -l.32E-01 1.52E-01
739.58 12.80 2.21E-01 3.77E-02 9.57E-02
778.00 4.50 5.90E-01 -2.49E-01 2.51E-01
TC-99M 140.51 89.00 1.90E-02 1.90E-02 -2.79E-04 8.92E-03
RU-103 497.08 89.00 2.34E-02 2.34E-02 -9.88E-03 1.05E-02
0202
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Analysis Report for 1803111-02
BLANK
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi!grams) (pCi/grams) (pCi/grams)
RU-106 621.84 9.80 2.64E-01 2.64E-01 5.07E-02 1.19E-01
AG-108M 433.93 89.90 2.39E-02 2.39E-02 2.13E-03 1.08E-02
614.37 90.40 2.97E-02 -4.16E-03 1.34E-02
722. 95 90.50 2.45E-02 -2.18E-03 1.06E-02
CD-109 88.03 3. 72 4.48E-01 4.48E-01 -3.42E-01 2.12E-01
AG-ll0M 657.75 93.14 2.28E-02 2.28E-02 1.l0E-03 9.91E-03
677.61 10.53 2.63E-01 1.54E-01 l.18E-01
706.67 16.46 1.74E-01 -1.62E-02 7.82E-02
763.93 21.98 1.36E-01 7.90E-02 6. llE-02
884.67 21.98 1.22E-01 -3.25E-02 5.33E-02
1384.27 23.94 9.28E-02 9.65E-03 3.59E-02
CD-113M 263.70 0.02 9.06E+0l 9.06E+0l -1.21E-01 4.23E+0l
SN-113 255.12 1. 93 8.78E-01 3.04E-02 2.37E-02 4.03E-01
391.69 64. 90 3.04E-02 -6.90E-03 1.37E-02
TE-123M 159.00 84.10 2.l0E-02 2.l0E-02 9.71E-03 9.89E-03
SB-124 602.71 97.87 2.86E-02 2.86E-02 -1.66E-02 1.30E-02
645.85 7.26 3.30E-01 2.03E-01 l.46E-01
722.78 11.10 2.02E-01 -1.79E-02 8.73E-02
1691.02 49.00 6.62E-02 1.54E-02 2.71E-02
I-125 35.49 6.49 4. 96E-01 4. 96E-01 8.07E-02 2.32E-01
SB-125 176.33 6.89 2.37E-01 6.82E-02 2.80E-02 l.l0E-01
427.89 29.33 6.82E-02 -2.l0E-02 3.07E-02
463.38 10.35 2.18E-01 -1.29E-02 9.89E-02
600.56 17.80 1.64E-01 4.52E-02 7.46E-02
635.90 11.32 2.07E-01 3.54E-02 9.15E-02
SB-126 414.70 83.30 2.15E-02 2.15E-02 -1.61E-02 9.58E-03
666.33 99.60 2.69E-02 4.15E-03 1.21E-02
695.00 99.60 2.58E-02 -3.57E-03 1.14E-02
720 .50 53.80 4.36E-02 7.66E-03 1.90E-02
SN-126 87.57 37.00 4.50E-02 4.50E-02 -3.43E-02 2.13E-02
SB-127 473.00 25.00 9.64E-02 6.54E-02 -5.32E-02 4.32E-02
685.00 35.70 6.54E-02 -3.0lE-02 2.80E-02
783.80 14.70 2. llE-01 3.55E-02 9.28E-02
I-129 29.78 57.00 9.33E-02 9.33E-02 2.59E-02 4.40E-02
33.60 13.20 2.81E-0l -6.62E-02 l.32E-01
39.58 7.52 3.64E-01 4.63E-02 1.71E-01
I-131 284.30 6.05 3.09E-01 2.75E-02 -6.48E-02 1.41E-01
364.48 81.20 2.75E-02 1.82E-03 l.26E-02
636.97 7.26 3.64E-01 1.48E-01 l.62E-01
722.89 1. 80 1.33E+00 -l.18E-01 5.76E-01
TE-132 49. 72 13.10 1.60E-01 2.16E-02 -2.95E-01 7.45E-02
228.16 88.00 2.16E-02 -1.50E-03 9.91E-03
BA-133 81.00 33.00 5.12E-02 3.18E-02 -1.14E-02 2.42E-02
302.84 17.80 1.02E-01 -6.35E-02 4.65E-02
356.01 60.00 3.18E-02 -2.24E-02 1.44E-02
I-133 529.87 86.30 5.21E-02 5.21E-02 1.41E-03 2.33E-02
XE-133 81.00 38.00 5.00E-02 5.00E-02 -1. llE-02 2.36E-02
CS-134 563.23 8.38 2.36E-0l 3.13E-02 -2.03E-02 1.04E-01
569.32 15.43 1.lSE-01 -8.03E-02 4. 96E-02
604.70 97.60 3.15E-02 2.51E-03 1.44E-02
795.84 85.40 3.13E-02 3.49E-04 1.38E-02
801.93 8.73 3.08E-01 -2.06E-02 1.36E-01
CS-135 268.24 16.00 1.33E-01 l.33E-01 3.94E-02 6.19E-02
0203
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Analysis Report for 1803111-02
BLANK
Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCilgrams) (pCilgrams) (pCi!grams)
I-135 1131. 51 22.50 1.00E+00 8.56E-01 -8.57E-02 4.l0E-01
1260.41 28.60 8.56E-01 8.56E-02 3.51E-01
1678.03 9.54 2.55E+00 -4.77E-01 9.86E-01
CS-136 153.22 7.46 2.06E-01 2.94E-02 -1.23E-01 9.58E-02
163.89 4.61 3.60E-01 1.14E-01 1.68E-01
176.55 13.56 1.26E-01 1.49E-02 5.87E-02
273.65 12.66 1.73E-01 -1.l0E-02 8.06E-02
340.57 48.50 4.49E-02 -1.68E-02 2.06E-02
818.50 99.70 2.94E-02 -4.27E-04 1.30E-02
1048.07 79.60 4.05E-02 8.60E-03 1.76E-02
1235.34 19.70 1.18E-01 -8.09E-02 4.68E-02
CS-137 661.65 85.12 2.71E-02 2.71E-02 2.41E-03 1.19E-02
LA-138 788.74 34.00 7.99E-02 3.77E-02 -6.95E-03 3.53E-02
1435.80 66.00 3.77E-02 l.44E-02 1.49E-02
CE-139 165.85 80.35 1.83E-02 l.83E-02 -3.77E-03 8.46E-03
BA-140 162.64 6.70 2.54E-01 9.84E-02 3.81E-02 1.19E-01
304.84 4.50 4.24E-01 -1.56E-01 1.94E-01
423.70 3.20 7.39E-01 2.63E-01 3.37E-01
437.55 2.00 1.l0E+00 -1.43E-02 4.98E-01
537.32 25.00 9.84E-02 -2.98E-02 4.43E-02
LA-140 328.77 20.50 9.58E-02 2.43E-02 -4.05E-02 4.37E-02
487.03 45.50 5.49E-02 -5.08E-04 2.49E-02
815.85 23.50 1.06E-01 4.07E-03 4.55E-02
1596.49 95.49 2.43E-02 0.00E+00 9.09E-03
CE-141 145.44 48.40 3.46E-02 3.46E-02 -5.96E-03 1.62E-02
CE-143 57.36 11. 80 2.54E-01 7.48E-02 l.00E-01 1.20E-01
293.26 42.00 7.48E-02 -2. 96E-02 3.46E-02
664.55 5.20 8.08E-01 l.23E-01 3.62E-01
CE-144 133.54 10.80 1.30E-01 1.30E-01 -3.88E-02 6.04E-02
PM-144 476.78 42.00 5.18E-02 2.64E-02 -1.27E-02 2.33E-02
618.01 98.60 2.66E-02 -6.19E-03 1.20E-02
696.49 99.49 2.64E-02 4.52E-03 1.18E-02
PM-145 36.85 21.70 1.37E-01 7.54E-02 -4. 96E-02 6.39E-02
37.36 39.70 7.54E-02 -l.12E-02 3.54E-02
42.30 15.10 1.67E-01 -6.91E-02 7.85E-02
72.40 2.31 7.19E-01 -6.58E-02 3.39E-01
PM-146 453.90 39.94 5.56E-02 5.56E-02 -6.23E-03 2.52E-02
735.90 14.01 1.39E-01 -1.05E-01 5.87E-02
747.13 13.10 1.57E-01 -4.99E-02 6.67E-02
ND-147 91.11 28.90 8.97E-02 8.97E-02 1. 72E-01 4.32E-02
531.02 13.10 1. 78E-01 -1.40E-02 7.95E-02
PM-149 285.90 3.10 7.76E-01 7.76E-01 -2.09E-02 3.57E-01
EU-152 121.78 20.50 7. 13E-02 7.13E-02 2.83E-02 3.33E-02
244.69 5.40 3.04E-01 -1.36E-01 1.39E-01
344.27 19.13 1.17E-01 2.29E-02 5.42E-02
778.89 9.10 2.42E-01 -1.61E-01 1.04E-0l
964.01 10.40 2.85E-01 5.76E-02 1.24E-0l
1085.78 7.22 2.28E-01 -1.06E-02 8.52E-02
1112.02 9.60 2.94E-01 4.20E-02 1.25E-0l
1407.95 14.94 1.35E-01 -2.71E-02 5.04E-02
GD-153 97.43 31.30 5.03E-02 5.03E-02 -2.82E-02 2.37E-02
103.18 22.20 6.58E-02 3.28E-03 3.09E-02
EU-154 123.07 40.50 3.47E-02 3.47E-02 1.83E-03 1.62E-02
0204
4/17/2018 7:13:55AM Page 21 of23
Analysis Report for 1803111-02
BLANK
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCilgrams) (pCilgrams) (pCi/grams)
EU-154 723.30 19.70 l.13E-01 3.47E-02 -l.00E-02 4.87E-02
873.19 11. 50 2.24E-01 -3.98E-02 9.71E-02
996.32 10.30 2.51E-01 -l.26E-03 1.07E-01
1004.76 17.90 1.13E-01 -8.15E-02 4.57E-02
1274.45 35.50 5.25E-02 -2.84E-02 1. 96E-02
EU-155 86.50 30.90 5.55E-02 5.55E-02 1.18E-03 2.63E-02
105.30 20.70 7.02E-02 -l.83E-02 3.29E-02
EU-156 811.77 10.40 2.65E-01 2.65E-01 9.66E-02 l.16E-01
1153.47 7.20 3.67E-01 -5.79E-02 l.52E-01
1230.71 8.90 3.13E-01 5.77E-02 l.30E-01
HO-166M 184.41 72.60 3.04E-02 3.04E-02 3.07E-02 l.44E-02
280.45 29.60 5.86E-02 -1.50E-02 2.68E-02
410.94 11.10 1.83E-01 1.43E-02 8.29E-02
711.69 54.10 5.59E-02 5.66E-03 2.52E-02
TM-171 66.72 0.14 1.35E+0l 1.35E+0l -1.64E+0l 6.42E+00
HF-1 72 67.35 5.31 3.31E-01 1.29E-01 3.14E-02 l.56E-01
125.82 11. 30 1.29E-01 -2.58E-03 6.02E-02
LU-172 181.53 20.60 8.14E-02 5.07E-02 -1.87E-01 3.77E-02
900. 72 29.81 6.82E-02 -1.61E-03 2.76E-02
1093.66 62.50 5.07E-02 2.69E-03 2.17E-02
LU-173 100.72 5.24 2.98E-01 9.83E-02 -2.56E-03 l.40E-01
272.11 21.20 9.83E-02 -7.64E-03 4.58E-02
HF-175 343.40 84.00 2.69E-02 2.69E-02 5.25E-03 1.24E-02
LU-176 88.34 13. 30 1.26E-01 1.88E-02 -3.72E-01 5.98E-02
201.83 86.00 1.88E-02 -l.22E-02 8.73E-03
306.78 94.00 2.07E-02 6.87E-03 9.54E-03
HF-181 133.02 41.70 3.61E-02 2.64E-02 -9.00E-03 1.68E-02
345.85 17.20 1.33E-01 -5.79E-04 6.13E-02
482.03 82.80 2.64E-02 -1.07E-02 1.19E-02
TA-182 67.75 41.20 4.28E-02 4.28E-02 4.05E-03 2.02E-02
1121.30 34.90 7.86E-02 0.00E+00 3.32E-02
1189.05 16.23 l.53E-01 -2.76E-02 6.25E-02
1221.41 26.98 8.18E-02 -3.12E-03 3.25E-02
1231.02 11. 44 2.35E-01 7.40E-02 9.74E-02
IR-192 308.46 29.68 6.58E-02 4.56E-02 -4.07E-03 3.02E-02
468.07 48.10 4.56E-02 l.70E-04 2.06E-02
HG-203 279.19 77.30 2.51E-02 2.51E-02 6.45E-03 l.16E-02
TL-204 374.74 94 .11 1.99E-02 1.99E-02 -3.52E-03 8.98E-03
899.15 99.16 1.99E-02 3.97E-03 8.15E-03
911.74 91.10 2.64E-02 2.92E-03 1.12E-02
BI-207 569.67 97.72 1.82E-02 1.82E-02 -1.55E-02 7.83E-03
1063.62 74.90 2.41E-02 -1.30E-02 9.33E-03
TL-208 583.14 30.22 7.99E-02 7.99E-02 -5.60E-03 3.58E-02
860.37 4.48 4.93E-01 6.36E-02 2.08E-01
2614.66 35.85 1.30E-01 7.03E-02 5.45E-02
BI-210M 262.00 45.00 4.68E-02 4.68E-02 -4.19E-03 2.18E-02
300.00 23.00 8.59E-02 -1.25E-02 3. 96E-02
PB-210 46.50 4.25 5.55E-01 5.55E-01 3.72E-01 2.62E-01
PB-211 404.84 2.90 6.51E-01 6.51E-01 -3.48E-01 2.93E-01
831. 96 2.90 8.0lE-01 -1.83E-01 3.43E-01
BI-212 727.17 11. 80 1.70E-01 1.70E-01 -9.39E-02 7.24E-02
1620.62 2.75 1.13E+00 3.77E-01 4.64E-01
PB-212 238.63 44.60 4.68E-02 4.68E-02 4.19E-02 2.19E-02
0205
4/17/2018 7:13:55AM Page 22 of 23
Analysis Report for 1803111-02
BLANK
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCilgrams)
PB-212 300.09 3.41 5.80E-01 4.68E-02 -8.40E-02 2.67E-01
BI-214 609.31 46.30 6.90E-02 6.90E-02 2.99E-02 3.17E-02
1120.29 15.10 1.36E-01 -1.04E-01 5.39E-02
1764.49 15.80 1.83E-01 6.97E-02 7.25E-02
2204.22 4.98 5.51E-01 -1.79E-01 2.06E-01
PB-214 295.21 19.19 1.12E-01 6.34E-02 1.37E-02 5.21E-02
351.92 37.19 6.34E-02 2.52E-02 2.94E-02
RN-219 401.80 6.50 3.16E-01 3.16E-01 -1.46E-02 1.44E-0l
RA-223 323.87 3.88 5.68E-01 5.68E-0l 2.78E-01 2.63E-01
RA-224 240.98 3.95 4.98E-01 4.98E-01 2. llE-01 2.32E-01
RA-225 40.00 31.00 9.04E-02 9.04E-02 1.15E-02 4.25E-02
RA-226 186.21 3.28 6.87E-01 6.87E-0l 9.60E-01 3.26E-0l
TI-l-227 50.10 8.40 2.17E-01 l.51E-01 -2.29E-02 1.0lE-01
236.00 11. 50 1.51E-01 -l.03E-01 6.97E-02
256.20 6.30 3.18E-01 -8.07E-03 1.48E-01
AC-228 338.32 11. 40 1.85E-01 9.02E-02 2.70E-03 8.52E-02
911.07 27. 70 9.02E-02 9.58E-03 3.86E-02
969.11 16.60 1.52E-01 -4.73E-02 6.48E-02
TI-l-230 48.43 16.90 1.16E-01 1.16E-0l -4.60E-02 5.42E-02
62.85 4.60 5.26E-01 3.63E-01 2.52E-01
67. 67 0.37 4.74E+00 4.49E-01 2.24E+00
PA-231 283.67 1. 60 1.08E+00 7.86E-01 -5.23E-02 4.94E-01
302. 67 2.30 7.86E-01 -4.91E-01 3.60E-01
TI-l-231 25.64 14.70 7.13E-01 2.77E-01 -5.91E+00 3.40E-01
84.21 6.40 2.77E-01 1.38E-01 1.31E-01
PA-233 311.98 38.60 5.73E-02 5.73E-02 -3.85E-03 2.66E-02
+ PA-234 131.20 * 20.40 6. 72E-02 6. 72E-02 4.40E-02 3.12E-02
733.99 8.80 2.55E-01 5.52E-02 l.l0E-01
946.00 12.00 1.81E-01 -5.70E-02 7.50E-02
PA-234M 1001.03 0.92 2.93E+00 2.93E+00 3.50E-01 1.25E+00
TH-234 63. 2 9 3.80 6.57E-01 6.57E-01 1.08E+00 3.15E-01
U-235 143.76 10.50 l.70E-01 l.70E-01 8.49E-02 8.02E-02
163.35 4.70 3.36E-01 1.06E-01 1.57E-01
205.31 4.70 3.77E-01 3.18E-02 1.76E-01
NP-237 86.50 12.60 1.36E-01 l.36E-01 2.89E-03 6.44E-02
NP-239 106.10 22. 70 8.18E-02 8.18E-02 -2.00E-02 3.83E-02
228.18 10.70 1.95E-01 -3.45E-03 8.97E-02
277.60 14.10 1.84E-01 1.0lE-01 8.54E-02
+ AM-241 59.54 * 35.90 7.75E-02 7.75E-02 1.92E-02 3.73E-02
AM-243 74.67 66.00 2.59E-02 2.59E-02 -7.05E-04 l.22E-02
CM-243 209.75 3.29 5.29E-01 1.43E-01 -1.13E-01 2.46E-01
228.14 10.60 1.48E-01 -1.03E-02 6.80E-02
277.60 14.00 1.43E-01 7. 81E-02 6.61E-02
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
0206
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Analysis Report for 1803111-02
BLANK
No Action Level results available for reporting purposes.
DATA REVIEW COMMENTS REPORT
Creation Date Comment User
No Data Review Comments Entered.
0207
Channel Data Report 4/17/2018 7:14:12 AM Page 1
*******************************************************
***** S P E C T R A L D A T A R E P O R T *****
*******************************************************
Sample Title: BLANK
Elapsed Live time: 3600 Elapsed Real Time: 3600
Channel[------[-------[-------[-------[-------[-------[-------[-------[
1 : 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 27 36 49 247 476 70
25: 23 22 18 17 12 20 20 23
33: 14 13 15 15 17 14 13 21
41: 19 15 14 20 18 21 30 16
49: 13 9 5 17 24 13 15 20
57: 20 18 12 27 13 19 43 73
65: 32 27 19 14 23 16 18 17
73: 14 25 19 22 21 23 21 26
81: 14 20 21 22 24 22 25 19
89: 17 18 24 37 98 50 19 15
97: 20 13 27 14 17 13 16 21
105: 15 10 11 17 18 19 10 15
113: 15 8 15 12 17 20 17 13
121: 8 13 17 19 7 15 15 12
12 9: 12 14 21 20 9 9 9 13
137: 15 13 10 18 18 23 17 23
145: 17 15 13 11 16 16 18 10
153: 13 12 14 10 16 16 22 16
161: 14 10 16 15 14 10 6 9
169: 15 9 12 16 11 18 12 11
177: 14 15 12 8 12 16 13 5
185: 27 46 25 12 10 11 7 14
193: 4 12 10 7 13 16 14 7
201: 13 14 9 11 15 17 13 8
209: 10 15 10 17 9 16 15 13
217: 8 12 5 6 12 11 12 9
225: 8 8 7 8 9 11 10 9
233: 11 12 5 9 13 12 28 10
241: 12 5 10 8 9 7 9 14
249: 13 7 12 7 11 2 5 13
257: 12 7 8 15 7 11 10 7
265: 9 10 11 7 8 11 11 8
273: 7 8 9 10 9 12 6 3
281: 6 4 3 6 5 6 9 6
289: 8 9 6 6 6 7 12 9
297: 5 14 6 10 5 6 2 8
305: 4 4 5 10 9 5 6 5
313: 10 7 13 4 6 8 0 7
321: 11 11 7 7 9 5 4 6
329: 6 5 6 5 6 7 6 6
337: 9 6 8 7 4 6 7 6
345: 6 11 11 4 6 6 12 13
353: 6 5 7 2 7 4 3 6
361: 4 3 7 5 5 7 7 5
0208
Channel Data Report 4/17/2018 7:14:12 AM Page 2
369: 3 8 2 2 5 5 4 8
Sample Title: BLANK
Channell------l-------l-------l-------1-------1-------1-------I-------I
377: 2 4 6 4 2 11 6 5
385: 2 1 5 6 7 6 3 2
393: 4 5 4 6 11 3 6 4
401: 6 6 2 3 6 5 2 3
409: 4 9 7 1 4 3 1 8
417: 2 4 8 0 2 10 5 6
425: 4 6 4 4 3 2 5 3
433: 7 4 3 4 6 3 8 5
441: 1 2 5 5 6 5 4 3
44 9: 4 4 6 7 7 7 1 2
457: 2 4 3 6 6 5 3 7
465: 7 2 2 4 6 5 3 3
473: 4 4 6 0 7 5 1 5
481: 7 5 4 3 2 10 0 4
489: 8 6 5 5 3 3 2 3
497: 3 4 5 3 7 4 3 5
505: 4 2 1 4 8 13 32 13
513: 13 6 7 10 2 5 3 3
521: 3 3 4 3 4 1 3 5
52 9: 1 3 5 3 4 3 5 5
537: 3 7 2 2 6 6 1 3
545: 5 4 3 3 2 4 2 1
553: 2 2 4 4 1 1 5 4
561: 1 3 2 3 2 2 3 2
569: 2 2 1 1 2 7 4 2
577: 4 5 1 2 2 5 6 4
585: 4 2 3 6 2 2 5 2
593: 5 3 2 1 8 3 8 4
601: 4 7 6 4 3 4 6 10
60 9: 9 4 5 5 3 6 3 2
617: 5 4 3 2 8 3 7 1
625: 2 1 3 2 2 2 2 2
633: 2 4 1 3 5 4 1 4
641: 1 2 0 2 5 1 3 7
649: 2 0 0 3 3 1 3 0
657: 2 2 1 3 4 2 2 2
665: 4 7 5 3 2 3 3 3
673: 2 1 2 2 3 7 3 3
681: 6 2 1 2 4 0 3 0
689: 2 2 4 6 5 2 2 0
697: 2 4 7 2 3 2 3 2
705: 3 3 7 4 1 6 7 4
713: 4 6 1 4 1 1 2 4
721: 2 5 1 1 1 0 3 2
729: 2 2 2 4 1 1 3 2
737: 1 1 1 3 4 2 1 1
745: 2 2 3 1 0 2 3 3
753: 4 4 1 5 1 3 0 4
761: 6 2 3 3 2 5 4 1
7 69: 1 3 1 2 1 6 1 2
777: 1 2 3 0 2 2 2 5
785: 1 2 4 4 1 1 4 3
793: 3 3 6 0 2 2 2 0
0209
Channel Data Report 4/17/2018 7:14:12 AM Page 3
801: 4 3 4 3 2 6 1 1
Sample Title: BLANK
Channell------l-------l-------l-------l-------l-------1-------1-------1
809: 3 2 2 3 2 3 2 1
817: 2 1 2 4 7 4 0 1
825: 2 4 3 1 3 0 2 5
833: 1 0 1 3 2 6 2 3
841: 3 4 5 4 3 2 6 4
849: 4 4 3 0 2 2 1 4
857: 1 0 0 6 2 1 0 0
865: 0 3 0 0 4 0 4 1
873: 1 3 3 2 2 4 2 2
881: 4 1 2 2 2 3 1 1
889: 6 0 2 1 1 1 0 2
897: 1 0 2 1 0 1 0 2
905: 5 1 4 1 2 3 3 0
913: 3 0 0 1 3 3 4 3
921: 1 1 2 1 2 2 4 1
929: 2 1 1 1 1 2 0 2
937: 1 5 3 3 3 1 2 3
945: 0 0 0 1 2 5 1 3
953: 3 2 2 2 2 3 3 2
961: 1 1 4 4 2 3 ·1 1
969: 1 2 3 0 2 2 1 1
977: 4 1 0 2 1 1 0 2
985: 0 1 0 1 2 0 2 0
993: 0 0 1 3 2 2 3 4
1001: 1 2 0 0 1 1 1 1
1009: 2 0 2 0 1 0 1 0
1017: 4 2 2 1 1 1 1 0
1025: 2 0 1 2 1 2 1 2
1033: 2 0 3 3 1 2 5 3
1041: 0 0 1 1 0 2 4 2
1049: 2 3 2 3 1 2 1 2
1057: 1 1 2 0 2 1 1 0
1065: 0 0 2 1 1 2 2 2
1073: 2 3 0 3 3 2 1 2
1081: 1 0 0 2 1 0 0 0
1089: 1 2 2 3 2 0 1 2
1097: 1 1 2 0 0 1 0 2
1105: 0 0 1 2 1 1 1 4
1113: 4 0 0 2 0 1 0 3
1121: 0 1 0 5 1 3 0 0
1129: 3 0 2 1 1 0 2 0
1137: 2 1 1 1 0 3 1 0
1145: 1 0 2 2 2 0 2 0
1153: 1 3 1 1 0 2 1 1
1161: 2 0 2 0 1 1 2 1
1169: 0 1 1 0 1 4 2 2
1177: 2 0 1 2 1 2 1 0
1185: 1 1 1 0 2 2 1 0
1193: 3 1 0 1 2 0 1 1
1201: 0 2 2 1 1 1 3 0
1209: 1 1 0 3 0 0 1 0
1217: 3 0 1 0 0 0 2 2
1225: 3 1 1 0 1 2 2 1
0210
Channel Data Report 4/17/2018 7:14:12 AM Page 4
1233: 1 1 1 0 1 0 1 3
Sample Title: BLANK
Channell------l-------l-------l-------l-------1-------1-------1-------I
1241: 0 3 2 1 0 1 1 1
1249: 0 2 2 1 4 1 0 2
1257: 1 1 0 0 1 1 3 0
1265: 1 0 2 1 0 2 0 0
1273: 1 0 2 0 0 2 1 3
1281: 0 3 0 1 1 0 0 0
1289: 1 1 0 1 1 0 0 3
1297: 0 1 2 0 1 0 1 1
1305: 1 2 0 0 1 0 0 1
1313: 0 1 1 0 0 1 1 0
1321: 5 1 0 1 2 0 0 3
1329: 1 0 0 1 1 1 2 0
1337: 0 0 0 0 0 1 0 0
1345: 0 1 1 1 0 1 1 0
1353: 1 1 0 0 1 0 0 1
1361: 0 0 1 0 1 1 2 2
1369: 1 2 1 0 2 1 1 1
1377: 3 1 1 1 1 1 0 0
1385: 1 0 1 0 0 1 1 0
1393: 3 2 1 1 5 3 1 1
1401: 1 2 0 1 0 0 0 1
1409: 0 1 1 0 0 0 0 0
1417: 2 0 0 2 0 1 0 0
1425: 2 2 0 1 0 0 0 1
1433: 2 0 0 1 0 1 0 0
1441: 0 0 0 2 0 0 3 1
1449: 1 0 0 1 0 1 1 1
1457: 2 0 5 0 2 0 3 0
1465: 0 2 0 0 1 0 0 1
1473: 0 2 0 1 0 0 0 1
1481: 0 0 0 0 0 1 0 1
1489: 2 0 1 0 1 0 1 1
14 97: 1 0 0 1 1 0 3 0
1505: 0 0 1 1 1 1 2 3
1513: 1 0 1 2 0 0 0 1
1521: 0 0 1 0 1 0 1 0
1529: 1 0 0 0 2 3 1 1
1537: 0 1 0 0 0 0 0 0
1545: 0 2 0 3 1 1 0 0
1553: 1 1 0 1 1 1 1 1
1561: 0 0 0 0 1 0 2 2
1569: 0 0 1 0 1 0 0 0
1577: 1 0 2 1 0 0 0 0
1585: 2 1 1 1 0 0 0 2
1593: 0 0 1 1 1 0 0 0
1601: 0 1 1 0 0 1 0 1
1609: 2 2 1 1 0 1 1 0
1617: 0 1 1 0 2 1 2 0
1625: 0 0 0 1 0 0 1 0
1633: 2 1 1 0 0 3 0 0
1641: 1 0 0 0 1 0 0 1
1649: 0 0 0 0 2 2 0 0
1657: l 2 1 0 0 0 0 1
0211
Channel Data Report 4/17/2018 7:14:12 AM Page 5
1665: 1 2 0 1 0 0 0 2
Sample Title: BLANK
Channell------l-------l-------l-------l-------l-------1-------1-------1
1673: 1 1 1 0 0 1 0 1
1681: 0 1 0 1 0 1 1 0
1689: 0 2 2 1 1 0 1 2
1697: 2 0 0 3 0 0 0 0
1705: 1 1 0 2 0 0 0 0
1713: 1 0 1 0 0 0 1 1
1721: 0 2 0 0 0 1 0 1
1729: 1 0 0 0 0 0 1 1
1737: 0 0 0 0 1 1 0 2
1745: 0 0 0 0 1 1 2 0
1753: 0 0 1 1 0 2 0 0
1761: 1 0 0 2 2 0 0 0
1769: 0 0 0 0 0 0 0 1
1777: 0 0 0 2 0 1 1 0
1785: 0 1 0 0 0 0 1 0
1793: 0 1 1 1 0 0 0 0
1801: 0 2 0 0 0 1 1 1
1809: 3 2 0 4 1 3 0 0
1817: 0 0 2 0 0 1 0 1
1825: 0 0 1 1 1 0 0 0
1833: 2 1 0 1 0 0 2 0
1841: 2 0 1 1 0 0 0 0
1849: 0 0 0 1 0 1 0 1
1857: 1 0 1 0 1 0 0 1
1865: 2 1 0 1 0 0 1 0
1873: 1 1 0 0 1 2 0 0
1881: 0 1 0 1 1 1 0 0
1889: 1 0 0 0 0 2 1 0
1897: 1 0 0 1 0 0 0 0
1905: 1 2 0 0 0 0 0 1
1913: 0 0 0 2 0 1 1 2
1921: 0 1 0 0 1 1 0 0
192 9: 2 0 0 1 0 0 0 4
1937: 0 0 0 0 0 0 0 0
1945: 0 0 1 0 1 2 0 0
1953: 0 0 0 0 1 0 1 2
1961: 1 0 1 2 0 0 3 0
1969: 2 1 0 0 1 1 0 2
1977: 3 1 1 0 3 1 1 0
1985: 0 0 0 0 0 0 0 1
1993: 0 0 0 1 1 1 1 0
2001: 0 0 0 1 0 0 0 0
2009: 1 1 0 0 0 0 0 0
2017: 0 1 0 0 0 4 0 1
2025: 0 0 0 1 1 0 1 1
2033: 0 1 0 0 0 0 0 1
2041: 1 1 0 0 0 0 0 1
2049: 1 0 0 0 1 0 0 0
2057: 0 1 0 0 0 0 0 1
2065: 0 0 1 0 0 0 0 0
2073: 0 1 1 0 1 1 0 0
2081: 1 0 1 1 1 0 1 0
2089: 0 2 0 0 0 0 1 0
0212
Channel Data Report 4/17/2018 7:14:12 AM Page 6
2097: 0 0 0 0 0 0 0 1
Sample Title: BLANK
Channell------l-------1-------1-------1-------1-------I-------I-------I
2105: 0 0 0 1 0 0 1 1
2113: 0 0 2 0 0 1 2 0
2121: 0 0 1 0 0 1 0 0
212 9: 0 0 0 1 1 0 0 0
2137: 1 0 0 1 0 0 0 0
2145: 0 0 1 0 0 1 0 0
2153: 0 0 1 0 0 1 0 0
2161: 0 0 0 0 0 1 0 0
2169: 1 0 0 0 0 1 2 1
2177: 0 2 0 0 1 0 0 0
2185: 1 0 0 0 0 0 0 1
2193: 0 0 0 0 1 0 0 0
2201: 0 0 1 1 1 0 0 1
2209: 1 0 0 1 1 1 0 0
2217: 0 0 1 0 0 1 0 0
2225: 0 0 1 1 0 0 0 0
2233: 0 0 0 0 0 0 1 0
2241: 0 0 0 0 0 0 0 0
2249: 0 0 0 4 0 1 0 0
2257: 1 1 0 0 0 1 2 1
2265: 1 0 0 0 0 1 1 1
2273: 0 0 0 0 0 2 0 0
2281: 0 0 0 0 0 0 1 0
2289: 1 0 0 0 0 1 0 2
2297: 1 0 0 0 0 0 0 1
2305: 0 0 0 1 0 0 3 0
2313: 1 1 0 0 0 1 0 0
2321: 0 0 0 0 0 2 0 0
2329: 0 0 1 2 0 0 0 0
2337: 0 0 0 0 0 0 1 0
2345: 1 0 0 0 1 1 0 0
2353: 0 0 1 0 1 0 0 0
2361: 2 0 1 0 2 0 0 1
2369: 0 1 0 1 1 0 0 0
2377: 0 0 1 0 0 0 0 0
2385: 0 0 0 0 0 0 0 0
2393: 0 1 0 1 0 0 0 0
2401: 0 0 0 0 1 2 1 1
2409: 1 0 0 0 0 0 0 1
2417: 0 1 0 0 2 1 0 0
2425: 1 1 1 0 1 0 2 2
2433: 0 0 1 0 0 0 0 0
2441: 0 0 0 0 1 0 0 0
2449: 0 1 0 0 0 0 0 0
2457: 0 0 0 1 0 1 0 0
2465: 0 1 0 0 0 0 0 0
2473: 0 0 0 0 1 0 1 0
2481: 0 1 0 1 0 1 0 0
2489: 2 0 0 1 0 0 0 0
2497: 0 0 0 0 0 1 0 0
2505: 0 0 0 0 0 0 0 0
2513: 0 0 0 0 0 1 1 0
2521: 0 1 1 0 0 0 0 0
0213
Channel Data Report 4/17/2018 7:14:12 AM Page 7
2529: 1 1 0 0 0 0 0 0
Sample Title: BLANK
Channell------l-------l-------l-------l-------l-------1-------1-------1
2537: 0 1 0 0 0 0 0 0
2545: 1 0 0 0 0 0 0 0
2553: 2 0 0 1 1 0 0 0
2561: 1 0 1 0 0 1 0 0
2569: 0 0 0 0 0 0 0 0
2577: 1 1 0 0 1 0 1 1
2585: 0 0 0 1 0 0 0 1
2593: 0 1 0 1 0 0 0 0
2601: 0 1 0 2 0 2 0 0
2609: 0 0 0 0 2 5 0 1
2617: 0 1 0 0 1 1 0 1
2625: 0 0 0 0 0 0 0 0
2633: 0 0 0 0 1 0 0 0
2641: 0 0 1 0 0 0 0 2
2649: 0 0 0 0 1 0 1 1
2657: 0 0 0 0 0 0 0 0
2665: 0 0 0 0 0 0 1 0
267 3: 0 1 0 0 0 0 0 0
2681: 0 1 0 0 0 0 2 0
2 68 9: 0 0 0 1 0 0 0 0
2697: 0 0 0 1 0 0 0 0
2705: 0 0 0 0 2 0 0 2
2713: 0 0 0 0 2 0 0 0
2721: 0 1 0 0 0 0 0 0
2729: 0 0 1 0 0 0 0 0
2737: 0 0 0 0 0 0 0 0
2745: 0 0 2 0 0 0 1 0
2753: 0 0 0 0 0 0 0 0
2761: 0 1 0 0 0 0 0 1
2769: 1 0 1 0 1 0 0 0
2777: 0 1 0 0 0 0 0 0
2785: 0 0 0 0 0 0 1 0
2793: 0 0 1 0 0 0 0 1
2801: 0 0 0 0 0 0 1 0
2809: 0 0 0 0 1 1 0 0
2817: 0 1 0 1 1 0 1 1
2825: 0 1 0 0 0 0 0 2
2833: 0 1 0 0 0 0 0 0
2841: 1 0 2 0 0 0 0 2
2849: 0 2 0 0 0 0 0 0
2857: 0 1 1 0 0 0 0 0
2865: 1 0 0 0 1 0 0 0
2873: 0 0 0 0 0 0 0 0
2881: 1 0 0 0 0 1 0 0
2889: 0 0 0 0 0 0 0 0
2897: 0 1 0 0 1 0 0 0
2905: 0 1 0 0 0 0 1 0
2913: 0 0 0 0 0 0 1 0
2921: 1 1 1 1 2 1 0 0
292 9: 0 1 0 0 0 0 0 1
2937: 0 0 0 0 0 1 0 0
2945: 0 0 0 0 0 0 0 1
2953: 0 0 0 3 0 0 0 0
0214
Channel Data Report 4/17/2018 7:14:12 AM Page 8
2961: 0 0 0 1 1 0 0 0
Sample Title: BLANK
Channell------l-------1-------1-------1-------I-------I-------I-------I
2969: 0 0 1 0 0 0 0 1
2977: 0 0 0 0 0 0 0 0
2985: 0 0 0 0 1 0 0 0
2993: 0 0 0 0 1 1 0 0
3001: 0 0 0 0 0 0 0 0
3009: 2 0 0 0 0 0 0 0
3017: 0 0 0 1 0 1 0 0
3025: 0 1 0 0 0 0 0 1
3033: 1 0 0 0 0 1 0 0
3041: 1 0 0 0 0 0 1 0
3049: 0 0 0 0 0 1 0 0
3057: - 0 0 0 0 0 0 0 0
3065: 0 0 0 0 0 0 0 0
3073: 0 1 0 1 0 1 0 0
3081: 0 0 1 0 0 0 0 0
3089: 0 0 0 0 0 0 0 0
3097: 0 0 0 0 0 0 0 0
3105: 0 0 0 0 0 1 0 0
3113: 0 0 0 0 0 0 0 1
3121: 0 0 0 0 0 0 0 0
3129: 0 0 1 0 0 0 0 0
3137: 1 0 0 1 0 1 0 0
3145: 0 0 0 0 0 0 1 0
3153: 0 0 0 0 0 0 0 0
3161: 0 0 0 0 0 0 0 0
3169: 0 1 1 0 0 0 0 0
3177: 0 0 0 1 0 0 0 0
3185: 0 1 0 0 0 0 1 0
3193: 0 0 0 0 0 0 0 0
3201: 0 1 0 0 0 0 0 0
3209: 0 0 0 0 0 0 0 0
3217: 0 0 0 0 0 0 0 0
3225: 0 0 0 2 0 0 0 2
3233: 0 0 1 0 0 2 1 1
3241: 0 0 0 0 1 0 0 1
3249: 0 0 0 0 0 0 0 0
3257: 2 0 0 0 0 0 0 0
3265: 0 0 0 1 0 0 0 0
3273: 0 0 0 0 1 0 1 2
3281: 0 0 0 1 0 0 0 1
3289: 0 0 1 0 0 0 0 0
3297: 0 0 1 0 0 0 0 0
3305: 0 0 1 0 0 0 1 0
3313: 0 0 1 0 0 0 0 0
3321: 0 0 0 0 0 0 0 0
3329: 0 0 0 0 1 0 0 1
3337: 0 0 0 0 0 0 0 0
3345: 0 0 1 0 1 1 0 0
3353: 0 1 0 0 0 0 0 0
3361: 0 0 0 0 0 0 0 0
3369: 0 0 0 1 0 1 0 0
3377: 0 0 0 0 0 0 0 1
3385: 0 0 0 0 0 0 1 1
0215
Channel Data Report 4/17/2018 7:14:12 AM Page 9
3393: 0 0 0 0 0 0 0 0
Sample Title: BLANK
Channell------l-------l-------1-------1-------1-------I-------I-------I
3401: 0 1 0 1 0 0 0 0
3409: 0 0 0 0 0 0 0 0
3417: 0 0 0 0 0 0 0 1
3425: 1 0 0 0 1 0 0 0
3433: 0 0 0 0 0 0 0 1
3441: 0 0 1 1 1 0 0 0
3449: 1 0 0 0 0 0 1 0
3457: 0 0 0 0 0 1 0 0
3465: 0 0 1 0 0 0 0 0
3473: 1 0 1 1 0 0 1 0
3481: 0 0 0 0 0 0 1 0
3489: 0 0 0 0 0 0 0 0
3497: 0 0 0 0 0 0 1 0
3505: 0 0 0 0 1 0 0 0
3513: 1 0 1 0 0 0 0 0
3521: 0 0 1 0 0 0 0 0
3529: 0 0 0 0 0 0 0 0
3537: 1 0 1 0 1 0 0 0
3545: 0 0 0 0 0 0 1 0
3553: 0 0 0 0 1 0 0 0
3561: 0 0 0 1 0 0 0 0
3569: 0 0 0 0 0 1 1 0
3577: 0 0 0 0 0 0 0 0
3585: 0 0 0 0 0 0 0 1
3593: 0 0 0 0 0 0 1 0
3601: 0 0 1 1 0 0 0 1
3609: 0 0 0 0 0 1 0 0
3617: 0 0 0 0 0 0 0 0
3625: 0 0 0 0 0 0 0 0
3633: 0 0 0 0 1 0 0 1
3641: 0 0 0 0 0 0 0 0
3649: 0 0 0 0 0 0 0 0
3657: 0 0 0 0 0 1 0 0
3665: 0 0 0 0 0 0 0 0
367 3: 0 0 0 0 0 0 0 0
3681: 0 0 0 0 0 0 1 0
3689: 0 0 0 0 0 0 0 0
3697: 0 0 0 0 0 1 0 1
3705: 0 1 0 0 0 1 0 0
3713: 0 0 0 1 0 0 0 0
3721: 0 0 0 0 0 0 1 0
372 9: 1 0 0 0 1 0 0 1
3737: 0 0 0 0 0 0 0 0
3745: 1 1 0 0 0 0 0 0
3753: 0 0 0 0 0 0 0 0
3761: 1 0 1 0 1 0 0 0
3769: 0 1 1 0 0 0 0 0
3777: 1 0 0 0 1 0 0 0
3785: 0 1 0 0 0 0 1 0
3793: 0 0 0 0 1 0 1 0
3801: 0 0 0 0 0 0 1 0
3809: 0 0 0 0 0 0 0 1
3817: 0 0 0 0 0 0 0 2
0216
Channel Data Report 4/17/2018 7:14:12 AM Page 10
3825: 1 0 1 0 0 0 0 0
Sample Title: BLANK
Channell------l-------1-------1-------1-------I-------I-------I-------I
3833: 0 0 1 0 1 0 0 0
3841: 0 0 0 0 0 0 1 0
384 9: 1 0 0 0 0 1 1 0
3857: 0 0 0 0 0 0 0 0
3865: 0 0 0 0 0 0 0 0
3873: 0 0 1 0 0 1 0 1
3881: 0 0 0 0 0 0 1 0
3889: 0 0 0 0 0 1 0 0
3897: 0 0 0 0 0 0 0 0
3905: 0 0 0 0 0 0 1 0
3913: 0 1 0 0 0 0 0 0
3921: 0 1 0 0 0 0 0 0
3929: 0 0 0 0 0 1 0 0
3937: 0 0 0 0 0 0 1 0
3945: 0 0 0 0 0 0 0 0
3953: 0 1 1 1 0 0 0 0
3961: 0 0 0 0 0 0 0 0
3969: 0 0 0 0 0 0 0 0
3977: 0 0 0 0 0 0 1 3
3985: 0 0 0 0 0 0 0 0
3993: 0 0 0 0 0 0 0 0
4001: 0 0 1 0 0 0 0 0
4009: 0 1 0 1 0 0 0 1
4017: 0 0 0 0 0 0 0 0
4025: 0 0 0 0 0 0 0 0
4033: 0 0 0 0 0 0 0 0
4041: 0 1 0 0 0 0 0 0
4049: 0 0 0 0 0 0 1 0
4057: 0 0 0 0 0 0 0 0
4065: 0 0 0 0 0 0 0 0
4073: 0 0 0 1 0 0 0 0
4081: 0 0 0 0 0 1 0 0
4089: 0 0 0 0 0 0 0 0
0217
105
104
~ 103 !"CS u V)
O"'I 0 .
I V)
+-J s:::: :::s 0 u
102
101
0000064640. CNF Live Time :3600.000 sec Real Time :3600.400 sec Start: 1: 0.S(kev) stop : 4096:4096.9(kev) Acq. Start :Tue Apr 17 06:13:43 2018
100 l!Pi\111\ a in~ o 11'.' 11 '·~I I PM qn11 111 11111wm11n11111rnumi111rnnurnm1nu11mw11u1rnumn1mq11 lUll HI rnq1rn11111rn1 DI n unn mmn 11111 iun 10 1 1w11 111 t l 1 1n H\ 1
500 1000
~ ROI Type: 1
1500 2000 channel
2500 3000 r-:;:::m ~
ROI Type: 2
3500 4000
0218
4/17/2018 6:43:09AM
pex- amm Analysis Report for 1803111-03
AC-SED-11
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator
Detector Name
Geometry
Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803111-03
: AC-SED-11
: SOIL
: 4.763E+02 grams
: Countroom
: 3/21/2018 9:15:20AM
: 4/17/2018 5:42:57AM
: GAS-1602 pCi
: Administrator
: GE2
: GAS-1602
: 3600.0 seconds
: 3600.8 seconds
: 0.02 %
: 2.50
: 1 - 4096
: 28 - 4096
: 1.000 keV
: 2/17/2018
: 2/17/2018
: 64639
PEAK-TO-TOTAL CALIBRATION REPORT
Peak-to-Total Efficiency Calibration Equation
Pagel of29 ~p 1//!'1/J8
0219
4/17/2018 6:43:09AM
Analysis Report for 1803111-03
AC-SED-11
PEAK LOCATE REPORT
Peak No.
1 2 3 4 5 6 7 8 9
10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak Search Sensitivity
Energy (ke V)
47.14 76.59 93.65 99.87
185.97 239.38 277.51 295.46 302.20 338.95 352.20 408.80 463.05 477.97 511.42 563.56 583.18 609.34 663.21 750.47 766.58 771.59 795.62 860.86 911.33 932.18 950.24 969.18
1003.27 1098.74 1120.52 1237.76 1327.57 1335.60 1352.42 1377.95 1457.14 1460.90 1510.18 1589.70 1597.80 1639.41
: 4/17/2018 6:43:01 AM
: 1 : 4096 : 2.50
Centroid Channel
46.92 76.35 93.40 99.63
185.68 239.06 277.18 295.12 301.86 338.59 351.83 408.40 462.62 477.54 510.97 563.08 582.70 608.84 662.69 749.89 766.00 771.00 795.02 860.22 910.66 931. 50 949.55 968.48
1002.55 1097.96 1119.73 1236.91 1326.66 1334.67 1351.49 1377.01 1456.14 1459.90 1509.15 1588.61 1596.71 1638.29
Centroid Uncertainty
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Page 2 of 29
Peak Significance
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0220
Analysis Report for 1803111-03
Peak No.
43 44 45 46 47 48 49 50 51 52
AC-SED-11
Energy (ke V)
1662.23 1729.66 1739.41 1764. 67 1832.00 1887.19 1894.20 2027.45 2203.96 2614.32
? = Adjacent peak noted
Errors quoted at 2.000sigma
Centroid Channel
1661.09 1728.48 1738.22 1763.46 1830.75 1885.90 1892.90 2026.06 2202.44 2612.47
4/17/2018 6:43:09AM
Centroid Uncertainty
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Page 3 of 29
Peak Significance
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0221
4/17/2018 6:43:09AM Page 4 of 29
Analysis Report for 1803111-03
AC-SED-11
PEAK ANAL YS/S REPORT
Peak Analysis Performed on : 4/17/2018 6:43:01AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM
No. (keV) start end Centroid Area Uncertainty Counts (keV)
1 47.14 4 4 - 49 46.92 1.21E+02 58.34 5.78E+02 1. 43
2 76.59 72 - 81 76.35 6.37E+02 116.04 l.53E+03 3.04
3 93.65 91 - 96 93.40 1.40E+02 70.29 8.21E+02 1. 67
4 99.87 97 - 104 99.63 8.19E+0l 70.54 7.80E+02 2.33
5 185.97 181 - 190 185.68 1.64E+02 79.46 8.05E+02 1. 55
6 239.38 234 - 244 239.06 7.01E+02 83.70 5.58E+02 1. 93
7 277.51 27 4 - 281 277.18 5.27E+0l 46.35 3.13E+02 2.35
M 8 295.46 2 91 - 306 295.12 2.16E+02 40.73 1.78E+02 1. 52
m 9 302.20 2 91 - 306 301.86 2.86E+0l 29.65 1.45E+02 1. 53
10 338.95 335 - 343 338.59 1.09E+02 52.38 3.44E+02 1. 79
11 352.20 348 - 355 351.83 3.47E+02 55.79 2.87E+02 1. 42
12 408.80 406 - 411 408.40 2.60E+0l 28.18 1.38E+02 1. 79
13 463.05 4 60 - 466 4 62. 62 3.59E+0l 29.62 l.34E+02 1. 54
14 477.97 4 7 4 - 480 477.54 3.32E+0l 29.42 1.34E+02 2.08
15 511.42 506 - 516 510.97 1.28E+02 41. 25 1.56E+02 2.38
16 563.56 5 61 - 567 563.08 2.09E+0l 23.54 8.82E+0l 1. 96
17 583.18 57 8 - 587 582.70 1.66E+02 43.91 l.82E+02 1. 57
18 609.34 604 - 613 608.84 2.78E+02 46.89 1.56E+02 1. 4 9
19 663.21 657 - 668 662.69 7.14E+01 37.20 1.35E+02 1. 96
20 750.47 7 4 6 - 755 749.89 2.52E+01 28.35 1.02E+02 3.83
M 21 766.58 7 63 - 774 766.00 2.24E+0l 17.27 4.l0E+0l 1. 79
m 22 771.59 763 - 774 771.00 1.63E+0l 19.03 4.36E+0l 1. 7 9
23 795.62 7 92 - 798 795.02 3.24E+0l 22 .11 6.32E+0l 3.25
24 860.86 858 - 863 860.22 2.05E+0l 17.55 4.l0E+0l 2.28
25 911. 33 907 - 913 910.66 9.16E+0l 27. 74 7.27E+0l 1. 74
26 932.18 927 - 938 931.50 3.28E+01 27. 57 8.04E+0l 3.59
27 950.24 94 8 - 952 949.55 1.23E+0l 13. 67 3.15E+0l 2.20
28 969.18 966 - 971 968. 48 4.36E+01 25.73 9.08E+0l 2.26
29 1003.27 994 - 1009 1002.55 4.35E+01 32.37 8.49E+0l 7.38
30 1098.74 1095 - 1103 1097.96 1.66E+01 21. 24 6.08E+0l 3.16
31 1120.52 1116 - 1125 1119.73 3.29E+01 28.77 9.82E+0l 1. 95
32 1237.76 1233 - 1240 1236.91 2.39E+0l 23.41 7.42E+0l 1. 75
33 1327.57 1324 - 1329 1326.66 7.50E+00 8.66 9.00E+00 1. 40
34 1335.60 1330 - 1340 1334.67 2.87E+0l 17.87 2.66E+0l 3.57
35 1352.42 134 7 - 1355 1351.49 1.30E+0l 14.04 2.20E+0l 4. 87
36 1377.95 1373 - 1382 1377.01 2.50E+0l 20.32 4.41E+0l 1. 28
M 37 1457.14 14 53 - 1463 1456.14 1.23E+0l 18.22 2.95E+0l 3.20
m 38 1460.90 1453 - 1463 1459.90 4.57E+02 45.12 2.34E+0l 2.12
39 1510.18 1505 - 1512 1509.15 1.31E+0l 14.00 2.38E+0l 1. 27
40 1589.70 1584 - 1593 1588.61 1.35E+01 14.73 1.89E+0l 4. 91
0222
Analysis Report for 1803111-03
AC-SED-11
Peak Energy ROI
No. (keV) start
41 1597.80 1594 -42 1639.41 1635 -43 1662.23 1657 -44 1729.66 1724 -45 1739.41 1 735 -46 1764.67 1760 -47 1832.00 1827 -48 1887.19 1881 -49 1894.20 1890 -50 2027.45 2023 -51 2203. 96 2199 -52 2614.32 2607 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI end
1600 1641 1665 1732 1740 1768 1834 1889 1895 2028 2207 2617
4/17/2018 6:43:09AM Page 5 of 29
Peak Net Peak Net Area Continuum FWHM
Centroid Area Uncertainty Counts (keV)
1596.71 6.94E+00 6.95 4. llE+00 1. 59
1638.29 7.50E+00 8.28 7.00E+00 1. 31
1661.09 1.l0E+0l 6.63 0.00E+00 3.22
1728.48 9.50E+00 9.82 9.00E+00 1. 78
1738.22 5.13E+00 7.07 5.75E+00 1. 84
1763.46 3.50E+0l 16.03 1.80E+0l 2.45
1830.75 8.00E+00 5.66 0.00E+00 1.16
1885.90 6. 72E+00 7.50 4.56E+00 2.98
1892.90 1.00E+0l 6.32 0.00E+00 3.65
2026.06 4.50E+00 5.74 3.00E+00 2. 72
2202.44 2.50E+0l 10.00 0.00E+00 4.29
2612.47 5.50E+0l 14.83 0.00E+00 2.25
PEAK ANAL YS/S REPORT
Peak Analysis Performed on : 4/17/2018 6:43:01AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI ROI Net Peak Net Area Continuum Critical
No. (keV) start end Area Uncertainty Counts Level
1 47.14 44 - 49 1.21E+02 58.34 5.78E+02 4.44E+0l
2 76.59 72 - 81 6.37E+02 116.04 1.53E+03 8.59E+0l
3 93.65 91 - 96 1.40E+02 70.29 8.21E+02 5.44E+0l
4 99.87 97 - 104 8.19E+0l 70.54 7.80E+02 5.60E+0l
5 185.97 181 - 190 1.64E+02 79.46 8.05E+02 6.18E+0l
6 239.38 234 - 244 7.01E+02 83.70 5.58E+02 5.33E+0l
7 277.51 274 - 281 5.27E+0l 46.35 3.13E+02 3.62E+0l
M 8 295.46 2 91 - 306 2.16E+02 40.73 1.78E+02 2.19E+0l
m 9 302.20 2 91 - 306 2.86E+0l 29.65 1.45E+02 1.98E+0l
10 338.95 335 - 343 1.09E+02 52.38 3.44E+02 3.95E+0l
11 352.20 348 - 355 3.47E+02 55.79 2.87E+02 3.42E+0l
12 408.80 40 6 - 411 2.60E+0l 28.18 1.38E+02 2.16E+0l
13 463.05 460 - 466 3.59E+0l 29.62 1.34E+02 2.23E+0l
14 477.97 4 7 4 - 480 3.32E+0l 29.42 1.34E+02 2.23E+0l
15 511.42 506 - 516 l.28E+02 41. 25 l.56E+02 2.84E+0l
16 563.56 561 - 567 2.09E+0l 23.54 8.82E+0l 1.78E+0l
0223
Analysis Report for 1803111-03
M
m
M
m
AC-SED-11
Peak Energy ROI
No. (keV) start
17 583.18 578 -
18 609.34 604 -19 663.21 657 -20 750.47 74 6 -21 766.58 763 -22 771.59 7 63 -23 795.62 7 92 -24 860.86 858 -25 911.33 907 -26 932.18 927 -27 950.24 948 -28 969.18 966 -29 1003.27 994 -30 1098.74 1095 -31 1120.52 1116 -32 1237.76 1233 -33 1327.57 1324 -34 1335.60 1330 -35 1352.42 134 7 -36 1377.95 1373 -37 1457.14 1453 -38 1460.90 1453 -39 1510.18 1505 -40 1589.70 1584 -41 1597.80 1594 -42 1639.41 1635 -43 1662.23 1657 -44 1729.66 1724 -45 1739.41 1 735 -46 1764.67 17 60 -47 1832.00 1827 -48 1887.19 1881 -49 1894.20 1890 -50 2027.45 2023 -51 2203.96 2199 -52 2614.32 2607 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet Errors quoted at 2.000sigma
ROI end
587 613 668 755 774 774 798 863 913 938 952 971
1009 1103 1125 1240 1329 1340 1355 1382 1463 1463 1512 1593 1600 1641 1665 1732 1740 17 68 1834 1889 1895 2028 2207 2617
4/17/2018 6:43:09AM Page 6 of 29
Net Peak Net Area Continuum Critical
Area Uncertainty Counts Level
1.66E+02 43. 91 1.82E+02 2.92E+Ol
2.78E+02 46.89 l.56E+02 2.71E+Ol
7.14E+Ol 37.20 l.35E+02 2.72E+Ol
2.52E+Ol 28.35 1.02E+02 2.18E+Ol
2.24E+Ol 17. 27 4.lOE+Ol 1.05E+Ol
1.63E+Ol 19.03 4.36E+Ol 1.09E+Ol
3.24E+Ol 22 .11 6.32E+Ol 1.56E+Ol
2.05E+Ol 17.55 4.lOE+Ol 1.24E+Ol
9.16E+Ol 27. 74 7.27E+Ol 1.65E+Ol
3.28E+Ol 27.57 8.04E+Ol 2.06E+Ol
1.23E+Ol 13.67 3.15E+Ol 9.66E+OO
4.36E+Ol 25.73 9.08E+Ol l.82E+Ol
4.35E+Ol 32.37 8.49E+Ol 2.43E+Ol
1.66E+Ol 21. 24 6.08E+Ol l.61E+Ol
3.29E+Ol 28.77 9.82E+Ol 2.17E+Ol
2.39E+Ol 23.41 7.42E+Ol 1.75E+Ol
7.50E+OO 8.66 9.00E+OO 5.51E+OO
2.87E+Ol 17.87 2.66E+Ol 1.18E+Ol
1.30E+Ol 14.04 2.20E+Ol 9.91E+OO
2.50E+Ol 20.32 4.41E+Ol l.45E+Ol
1.23E+Ol 18.22 2.95E+Ol 8.94E+OO
4.57E+02 45.12 2.34E+Ol 7.95E+OO
1.31E+Ol 14.00 2.38E+Ol 9.85E+OO
1.35E+Ol 14.73 1.89E+Ol 1.05E+Ol
6.94E+OO 6.95 4.llE+OO 3.72E+OO
7.50E+OO 8.28 7.00E+OO 5.lOE+OO
l.lOE+Ol 6.63 O.OOE+OO O.OOE+OO
9.50E+OO 9.82 9.00E+OO 6.29E+OO
5.13E+OO 7.07 5.75E+OO 4.46E+OO
3.50E+Ol 16.03 1.80E+Ol 8.89E+OO
8.00E+OO 5.66 O.OOE+OO O.OOE+OO
6. 72E+OO 7.50 4.56E+OO 4.45E+00
1.00E+Ol 6.32 O.OOE+OO O.OOE+OO
4.50E+OO 5.74 3.00E+OO 3.18E+OO
2.50E+Ol 10.00 O.OOE+OO O.OOE+OO
5.50E+Ol 14.83 O.OOE+OO O.OOE+OO
0224
4/17/2018 6:43:09AM
Analysis Report for 1803111-03
M m
M m
AC-SED-11
PEAK WITH N/0 REPORT
Peak Analysis Performed on : 4/17/2018 6:43:01AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Tentative NID Library
Peak Match Tolerance
Peak Energy
No. (keV)
1 47.14 2 76.59 3 93.65 4 99.87 5 185.97 6 239.38 7 277.51
8 295.46 9 302.20
10 338.95 11 352.20 12 408.80 13 463.05 14 477.97 15 511 .42 16 563.56 17 583.18 18 609.34 19 663.21 20 750.47 21 766.58 22 771.59 23 795.62 24 860.86 25 911. 33
26 932.18 27 950.24 28 969.18 29 1003.27 30 1098.74 31 1120. 52
32 1237.76 33 1327.57 34 1335.60 35 1352.42 36 1377.95
: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB
: 1.000 keV
ROI ROI Peak Net Peak
start end Centroid Area
44 - 49 46.92 1.21E+02 72 - 81 76.35 6.37E+02 91 - 96 93.40 1.40E+02 97 - 104 99.63 8.19E+0l
181 - 190 185.68 1.64E+02 234 - 244 239.06 7.01E+02 27 4 - 281 277.18 5.27E+0l
291 - 306 295.12 2.16E+02 291 - 306 301.86 2.86E+0l
335 - 343 338.59 1.09E+02 348 - 355 351.83 3.47E+02 406 - 411 408.40 2.60E+0l 4 60 - 466 4 62. 62 3.59E+0l 4 7 4 - 480 477.54 3.32E+0l 506 - 516 510.97 1.28E+02 561 - 567 563.08 2.09E+0l 57 8 - 587 582.70 1.66E+02 604 - 613 608.84 2.78E+02 657 - 668 662.69 7.14E+01 746 - 755 749.89 2.52E+0l 7 63 - 774 766.00 2.24E+0l 7 63 - 774 771. 00 1.63E+0l 7 92 - 7 98 795.02 3.24E+0l 858 - 863 860.22 2.05E+0l 907 - 913 910.66 9.16E+0l
927 - 938 931.50 3.28E+0l 948 - 952 949.55 1.23E+0l
966 - 971 968.48 4.36E+0l 994 - 1009 1002.55 4.35E+0l
1095 - 1103 1097. 96 1.66E+0l 1116 - 1125 1119.73 3.29E+0l
1233 - 1240 1236.91 2.39E+0l 1324 - 1329 1326.66 7.50E+00
1330 - 1340 1334. 67 2.87E+0l
134 7 - 1355 1351.49 1.30E+0l
1373 - 1382 1377.01 2.50E+0l
Net Area Uncertainty
58.34 116.04
70.29 70.54 79.46 83.70 46.35
40.73 29.65
52.38 55.79 28.18 29.62 29.42 41.25 23.54 43.91 46.89 37.20 28.35 17.27 19.03 22 .11 17.55 27.74
27.57 13.67 25.73 32.37 21.24 28.77
23.41 8.66
17.87 14.04 20.32
Page 7 of 29
Continuum Tentative Counts Nuclide
5. 78E+02 PB-210 1.53E+03 8.21E+02 GA-67 7.80E+02 LU-173 8.05E+02 RA-226 5.58E+02 PB-212 3.13E+02 CM-243
NP-239 1. 78E+02 PB-214 l.45E+02 PA-231
BA-133 3.44E+02 AC-228 2.87E+02 PB-214 1.38E+02 1.34E+02 SB-125 l.34E+02 BE-7 1.56E+02 8.82E+0l CS-134 1.82E+02 TL-208 1.56E+02 BI-214 1.35E+02 1.02E+02 4.l0E+0l NB-95 4.36E+01 6.32E+0l CS-134 4.l0E+0l TL-208 7.27E+0l AC-228
TL-204 8.04E+0l 3.15E+01 9.08E+0l AC-228 8.49E+0l 6.08E+01 FE-59 9.82E+0l SC-46
BI-214 TA-182
7.42E+0l CO-56 9.00E+00 2.66E+0l 2.20E+0l 4.41E+01
0225
4/17/2018 6:43:09AM
Analysis Report for 1803111-03
M m
M m
AC-SED-11
Peak Energy ROI
No. (keV) start
37 1457.14 1453 -38 1460.90 1453 -39 1510.18 1505 -40 1589.70 1584 -41 1597.80 1594 -42 1639.41 1635 -43 1662.23 1657 -44 1729.66 1724 -45 1739.41 1 735 -46 1764.67 1760 -47 1832.00 1827 -48 1887.19 1881 -49 1894.20 1890 -50 2027.45 2023 -51 2203.96 2199 -52 2614.32 2 607 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area
end Centroid Area Uncertainty
1463 1456.14 1.23E+0l 18.22
1463 1459.90 4.57E+02 45.12
1512 1509.15 1.31E+0l 14.00
1593 1588.61 1.35E+0l 14.73
1600 1596.71 6.94E+00 6.95
1641 1638.29 7.50E+00 8.28
1665 1661.09 1.l0E+0l 6.63
1732 1728.48 9.50E+00 9.82
1740 1738.22 5.13E+00 7.07
1768 1763.46 3.50E+0l 16.03
1834 1830.75 8.00E+00 5.66
1889 1885.90 6.72E+00 7.50
1895 1892.90 1.00E+0l 6.32
2028 2026.06 4.50E+00 5.74
2207 2202.44 2.50E+0l 10.00
2617 2612.47 5.50E+0l 14.83
PEAK EFFICIENCY REPORT
Peak Analysis Performed on : 4/17/2018 6:43:01AM
Peak Energy Net Peak Net Area Peak
No. (keV) Area Uncertainty Efficiency
1 47.14 1.21E+02 58.34 1.62E-02
2 76.59 6.37E+02 116.04 2.33E-02
3 93.65 1.40E+02 70.29 2.40E-02
4 99.87 8.19E+0l 70.54 2.40E-02
5 185.97 1.64E+02 79.46 1.95E-02
6 239.38 7.01E+02 83.70 1.68E-02
7 277.51 5.27E+0l 46.35 1.52E-02
8 295.46 2.16E+02 40.73 1. 4 6E-02
9 302.20 2.86E+0l 29.65 1.43E-02
10 338.95 1.09E+02 52.38 l.32E-02
11 352.20 3.47E+02 55.79 1.28E-02
12 408.80 2.60E+01 28.18 1.14E-02
13 463.05 3.59E+0l 29.62 l.03E-02
14 477.97 3.32E+0l 29.42 1.00E-02
Page 8 of29
Continuum Tentative Counts Nuclide
2.95E+0l 2.34E+0l K-40 2.38E+0l 1.89E+0l 4. llE+00 7.00E+00 0.00E+00 9.00E+00 5.75E+00 1.80E+0l BI-214 0.00E+00 4.56E+00 0.00E+00 3.00E+00 0.00E+00 BI-214 0.00E+00 TL-208
Efficiency Uncertainty
1.53E-03 1.88E-03 2.09E-03 2.07E-03 2.44E-03 2.41E-03 2.39E-03 2.38E-03 2.38E-03 2.36E-03 2.35E-03 2.23E-03 1.91E-03 1.83E-03
0226
4/17/2018 6:43:09AM Page 9 of29
Analysis Report for 1803111-03
AC-SED-11
Peak Energy Net Peak Net Area Peak Efficiency
No. (keV) Area Uncertainty Efficiency Uncertainty
15 511.42 l.28E+02 41. 25 9.SlE-03 l.63E-03
16 563.56 2.09E+Ol 23.54 8. 77E-03 1.33E-03
17 583.18 1.66E+02 43.91 8.53E-03 1.22E-03
18 609.34 2.78E+02 46.89 8.22E-03 1.07E-03
19 663.21 7.14E+Ol 37.20 7.66E-03 7.70E-04
20 750.47 2.52E+Ol 28.35 6.91E-03 9.36E-04
M 21 766.58 2.24E+Ol 17.27 6.79E-03 9.67E-04
m 22 771.59 1.63E+Ol 19.03 6.7SE-03 9. 77E-04
23 795.62 3.24E+Ol 22 .11 6.59E-03 1.02E-03
24 860.86 2.0SE+Ol 17.55 6.17E-03 1.lSE-03
25 911. 33 9.16E+Ol 27.74 S.89E-03 1.18E-03
26 932.18 3.28E+Ol 27.57 S.79E-03 l.12E-03
27 950.24 l.23E+Ol 13.67 S.70E-03 1.07E-03
28 969.18 4.36E+Ol 25.73 S.61E-03 1.0lE-03
29 1003.27 4.3SE+Ol 32.37 S.46E-03 9.14E-04
30 1098.74 1.66E+Ol 21.24 S.09E-03 6.39E-04
31 1120.52 3.29E+Ol 28.77 S.OlE-03 S.76E-04
32 1237.76 2.39E+Ol 23.41 4.66E-03 4.00E-04
33 1327.57 7.SOE+OO 8.66 4.43E-03 3.67E-04
34 1335.60 2.87E+Ol 17.87 4.41E-03 3.65E-04
35 1352.42 1.30E+Ol 14.04 4.38E-03 3.67E-04
36 1377.95 2.SOE+Ol 20.32 4.32E-03 3.70E-04
M 37 1457.14 l.23E+Ol 18.22 4.17E-03 3.80E-04
m 38 1460.90 4.57E+02 45.12 4.16E-03 3.80E-04
39 1510.18 1.31E+Ol 14.00 4.08E-03 3.86E-04
40 1589.70 1.3SE+Ol 14.73 3.9SE-03 3. 96E-04
41 1597.80 6.94E+OO 6.95 3.94E-03 3.97E-04
42 1639.41 7.SOE+OO 8.28 3.89E-03 4.02E-04
43 1662.23 1.lOE+Ol 6.63 3.86E-03 4.04E-04
44 1729.66 9.SOE+OO 9.82 3.78E-03 4.12E-04
45 1739.41 S. 13E+OO 7.07 3.77E-03 4.13E-04
46 1764.67 3.SOE+Ol 16.03 3.74E-03 4.16E-04
47 1832.00 8.00E+OO 5.66 3.67E-03 4.24E-04
48 1887.19 6.72E+OO 7.50 3.63E-03 4.2SE-04
49 1894.20 1.00E+Ol 6.32 3.62E-03 4.2SE-04
so 2027.45 4.SOE+OO 5.74 3.53E-03 4.2SE-04
51 2203. 96 2.SOE+Ol 10.00 3.44E-03 4.2SE-04
52 2614.32 S.SOE+Ol 14.83 3.36E-03 4.2SE-04
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000 sigma
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on : 4/17/2018 6:43:01AM
0227
4/17/2018 6:43:09AM Page 10 of29
Analysis Report for 1803111-03
AC-SED-11
Env. Background File : \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000063825.CNF
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
1 47.14 1.21E+02 58.34 2.91E+0l 5.55E+00 9.19E+0l 5.86E+0l
2 76.59 6.37E+02 116.04 6.37E+02 1.16E+02
3 93.65 1.40E+02 70.29 5.03E+0l 8.08E+00 8.99E+0l 7.07E+0l
4 99.87 8.19E+0l 70.54 8.19E+0l 7.05E+0l
5 185.97 1.64E+02 79.46 4.04E+0l 9.60E+00 1.23E+02 8.00E+0l
6 239.38 7.01E+02 83.70 1.86E+0l 1.03E+0l 6.82E+02 8.43E+0l
7 277.51 5.27E+0l 46.35 5.27E+0l 4.63E+01
M 8 295.46 2.16E+02 40.73 8.49E+00 5.60E+00 2.07E+02 4. llE+0l
m 9 302.20 2.86E+0l 29.65 2.86E+0l 2.97E+0l
10 338.95 1.09E+02 52.38 1.09E+02 5.24E+0l
11 352.20 3.47E+02 55.79 1.76E+0l 5.14E+00 3.29E+02 5.60E+0l
12 408.80 2.60E+0l 28.18 2.60E+0l 2.82E+0l
13 463.05 3.59E+0l 29.62 3.59E+0l 2. 96E+01
14 477.97 3.32E+0l 29.42 3.32E+0l 2.94E+0l
15 511. 42 l.28E+02 41.25 7.91E+0l 5.07E+00 4.87E+0l 4.16E+0l
16 563.56 2.09E+0l 23.54 2.09E+0l 2.35E+0l
17 583.18 1.66E+02 43.91 6.66E+00 3.73E+00 1.59E+02 4.41E+0l
18 609.34 2.78E+02 46.89 l.26E+0l 6.94E+00 2.66E+02 4.74E+0l
19 663.21 7.14E+0l 37.20 7.14E+0l 3.72E+0l
20 750.47 2.52E+0l 28.35 2.52E+0l 2.84E+0l
M 21 766.58 2.24E+0l 17.27 2.24E+0l 1.73E+0l
m 22 771.59 1.63E+0l 19.03 1.63E+0l 1.90E+0l
23 795.62 3.24E+0l 22 .11 3.24E+0l 2.21E+0l
24 860.86 2.05E+0l 17.55 2.05E+0l 1.75E+0l
25 911. 33 9.16E+0l 27.74 2.63E+00 2.68E+00 8.90E+0l 2.79E+0l
26 932.18 3.28E+0l 27.57 3.28E+0l 2.76E+01
27 950.24 1.23E+0l 13.67 1.23E+0l 1.37E+0l
28 969.18 4.36E+0l 25.73 4.36E+0l 2.57E+0l
29 1003.27 4.35E+0l 32.37 4.35E+0l 3.24E+0l
30 1098.74 1.66E+0l 21.24 1.66E+0l 2.12E+0l
31 1120.52 3.29E+0l 28.77 1.l0E+00 2.71E+00 3.18E+0l 2.89E+0l
32 1237.76 2.39E+0l 23.41 2.39E+0l 2.34E+01
33 1327.57 7.50E+00 8.66 7.50E+00 8.66E+00
34 1335. 60 2.87E+0l 17.87 2.87E+0l 1.79E+0l
35 1352.42 1.30E+0l 14.04 1.30E+0l 1.40E+0l
36 1377.95 2.50E+0l 20.32 2.07E+00 2.17E+00 2.29E+0l 2.04E+0l
M 37 1457.14 l.23E+0l 18.22 l.23E+0l l.82E+0l
m 38 1460.90 4.57E+02 45.12 7.43E+00 2.27E+00 4.50E+02 4.52E+01
39 1510.18 1.31E+0l 14.00 1.31E+0l 1.40E+0l
40 1589.70 1.35E+0l 14.73 1.35E+0l 1.47E+0l
41 1597.80 6.94E+00 6.95 6.94E+00 6.95E+00
42 1639.41 7.50E+00 8.28 7.50E+00 8.28E+00
43 1662.23 l.l0E+0l 6.63 1.l0E+0l 6.63E+00
44 1729.66 9.50E+00 9.82 9.50E+00 9.82E+00
45 1739.41 5.13E+00 7.07 5.13E+00 7.07E+00
46 1764.67 3.50E+0l 16.03 2.32E+00 1.91E+00 3.27E+0l 1.61E+0l
47 1832.00 8.00E+00 5.66 8.00E+00 5.66E+00
48 1887.19 6. 72E+00 7.50 6.72E+00 7.50E+00
49 1894.20 1.00E+0l 6.32 1.00E+0l 6.32E+00
0228
4/17/2018 6:43:09AM Page 11 of29
Analysis Report for 1803111-03
AC-SED-11
Peak Energy No. (keV)
50 2027.45 51 2203.96 52 2614.32
Original Area
4.50E+00 2.50E+0l 5.50E+0l
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
Orig. Area Uncertainty
5.74 10.00 14.83
Ambient Background
4.72E+00
Backgr. Uncert.
1.41E+00
AREA CORRECTION REPORT
Subtracted Area
4.50E+00 2.50E+0l 5.03E+0l
REFERENCEPEAKIBKG.SUBTRACT
Peak Analysis Performed on : 4/17/2018 6:43:01AM
Ref. Peak Energy : 0.00 Reference Date
Peak Ratio : 0.00 Uncertainty : 0.00
Background File : \\OR-GAMMA 1\ApexRoot\Countroom\Data\0000063825.CNF
Corrected Area is: Original* Peak Ratio - Background
Peak Energy Original Orig. Area Ambient Backgr. Corrected
No. (keV) Area Uncertainty Background Uncert. Area
1 47.14 l.21E+02 58.34 2.91E+0l 5.55E+00 9.19E+0l
2 76.59 6.37E+02 116.04 6.37E+02
3 93.65 1.40E+02 70.29 5.03E+0l 8.08E+00 8.99E+0l
4 99.87 8.19E+0l 70.54 8.19E+0l
5 185.97 l.64E+02 79.46 4.04E+0l 9.60E+00 l.23E+02
6 239.38 7.01E+02 83.70 1.86E+0l 1.03E+0l 6.82E+02
7 277.51 5.27E+0l 46.35 5.27E+0l
M 8 295.46 2.16E+02 40.73 8.49E+00 5.60E+00 2.07E+02
m 9 302.20 2.86E+0l 29.65 2.86E+0l
10 338.95 1.09E+02 52.38 l.09E+02
11 352.20 3.47E+02 55.79 1.76E+0l 5.14E+00 3.29E+02
12 408.80 2.60E+0l 28.18 2.60E+0l
13 463.05 3.59E+0l 29.62 3.59E+0l
14 477.97 3.32E+0l 29.42 3.32E+0l
15 511.42 1.28E+02 41.25 7.91E+0l 5.07E+00 4.87E+0l
16 563.56 2.09E+0l 23.54 2.09E+0l
17 583.18 l.66E+02 43.91 6.66E+00 3.73E+00 1.59E+02
18 609.34 2.78E+02 46.89 1.26E+0l 6.94E+00 2.66E+02
19 663.21 7.14E+0l 37.20 7.14E+0l
20 750.47 2.52E+0l 28.35 2.52E+0l
M 21 766.58 2.24E+0l 17.27 2.24E+0l
m 22 771.59 1.63E+0l 19.03 1.63E+0l
23 795.62 3.24E+0l 22 .11 3.24E+0l
24 860.86 2.05E+0l 17.55 2.05E+0l
25 911. 33 9.16E+0l 27.74 2.63E+00 2.68E+00 8.90E+0l
Subtracted Uncert.
5.74E+00 1.00E+0l l.49E+0l
Corrected Uncert.
5.86E+0l l.16E+02 7.07E+0l 7.05E+0l 8.00E+0l 8.43E+0l 4.63E+0l 4.llE+0l 2.97E+0l 5.24E+0l 5.60E+0l 2.82E+0l 2.96E+0l 2.94E+0l 4.16E+0l 2.35E+0l 4.41E+0l 4.74E+0l 3.72E+0l 2.84E+0l 1.73E+0l 1.90E+0l 2.21E+0l 1.75E+0l 2.79E+0l
0229
4/17/2018 6:43:09AM Page 12 of29
Analysis Report for 1803111-03
AC-SED-11
Peak Energy Original Orig. Area Ambient Backgr. Corrected Corrected
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
26 932.18 3.28E+01 27. 57 3.28E+01 2.76E+Ol
27 950.24 1.23E+Ol 13.67 l.23E+Ol 1.37E+Ol
28 969.18 4.36E+Ol 25.73 4.36E+Ol 2.57E+Ol
29 1003.27 4.3SE+Ol 32.37 4.35E+Ol 3.24E+Ol
30 1098.74 1.66E+Ol 21. 24 1.66E+Ol 2.12E+Ol
31 1120.52 3.29E+Ol 28.77 l.lOE+OO 2.71E+OO 3.18E+Ol 2.89E+Ol
32 1237.76 2.39E+Ol 23.41 2.39E+Ol 2.34E+Ol
33 1327.57 7.SOE+OO 8.66 7.SOE+OO 8.66E+OO
34 1335.60 2.87E+Ol 17.87 2.87E+Ol 1.79E+Ol
35 1352.42 1.30E+01 14.04 1.30E+Ol 1.40E+Ol
36 1377.95 2.SOE+Ol 20.32 2.07E+OO 2.17E+OO 2.29E+Ol 2.04E+Ol
M 37 1457.14 1.23E+01 18.22 1.23E+Ol 1.82E+Ol
m 38 1460.90 4.57E+02 45.12 7.43E+OO 2. 27E+OO 4.SOE+02 4.52E+Ol
39 1510.18 1.31E+Ol 14.00 1.31E+Ol 1.40E+Ol
40 1589.70 1.3SE+Ol 14.73 1.3SE+Ol 1.47E+Ol
41 1597.80 6.94E+OO 6.95 6.94E+OO 6.9SE+OO
42 1639.41 7.SOE+OO 8.28 7.SOE+OO 8.28E+OO
43 1662.23 1.lOE+Ol 6.63 1.lOE+Ol 6.63E+OO
44 1729.66 9.SOE+OO 9.82 9.SOE+OO 9.82E+OO
45 1739.41 S.13E+OO 7.07 S.13E+OO 7.07E+OO
46 1764.67 3.SOE+Ol 16.03 2.32E+OO 1.91E+00 3.27E+Ol 1.61E+Ol
47 1832.00 8.00E+OO 5.66 8.00E+OO S.66E+OO
48 1887.19 6.72E+OO 7.50 6.72E+OO 7.SOE+OO
49 1894.20 1.00E+Ol 6.32 1.00E+Ol 6.32E+OO
so 2027.45 4.50E+OO 5.74 4.SOE+OO S.74E+00
51 2203. 96 2.SOE+Ol 10.00 2.50E+Ol 1.00E+Ol
52 2614.32 S.50E+Ol 14.83 4. 72E+00 1.41E+OO S.03E+Ol 1.49E+Ol
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Nuclide Name Id Confidence Energy (keV) Yield(%) Activity Activity
(pCi/grams) Uncertainty
BE-7 0.976 477.59 * 10.42 7.08E-01 6.41E-01
K-40 0.999 1460.81 * 10.67 1.60E+Ol 2.17E+OO
FE-59 0.308 1099.22 * 56.50 1.38E-01 1.78E-01
1291.56 43.20
0230
4/17/2018 6:43:09AM
Analysis Report for 1803111-03
AC-SED-11
Nuclide Name Id Confidence Energy (keV) Yield(%) Activity
(pCi/grams)
GA-67 0.377 93.31 * 35.70 5.00E+0l
208.95 2.24 300.22 16.00
NB-95 0.901 765.79 * 99.81 8.86E-02
TL-208 0.988 583.14 * 30.22 9.75E-01
860.37 * 4.48 l.17E+00
2614.66 * 35.85 6.58E-01
PB-210 0.936 46.50 * 4.25 2.l0E+00
PB-212 0.815 238.63 * 44.60 l.44E+00 300.09 3.41
BI-214 0.997 609.31 * 46.30 l.l0E+00
1120.29 * 15.10 6.62E-01
1764.49 * 15.80 8. 72E-01
2204.22 * 4.98 2.30E+00
PB-214 0.989 295.21 * 19.19 l.17E+00
351.92 * 37.19 l.09E+00
RA-226 0.991 186.21 * 3.28 3.03E+00
AC-228 0.982 338.32 * 11. 40 l.15E+00 911. 07 * 27.70 8.60E-01 969 .11 * 16.60 7.38E-01
PA-231 0.314 283.67 1. 60 302.67 * 2.30 l.37E+00
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
UNIDENTIFIED PEAKS
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (keV)
2 76.59 4 99.87 7 277.51
12 408.80 13 463.05 15 511. 42
: 4/17/2018 6:43:01AM
: 1 : 4096
Peak Size (CPS)
1. 76911E-01 2.27560E-02 l.46292E-02
7.22222E-03 9. 98112E-03 l.35394E-02
Peak CPS(%} Peak
Uncertainty Type
9 .11 D-Esc 43.05 Tol. 44.00 Tol.
54.19 41.22 Tol. 42.63
Page 13 of29
Activity
Uncertainty
3.96E+0l
6.95E-02 3.03E-01 l.02E+00 2.12E-01 l.36E+00 2. 72E-01
2.43E-01 6.07E-01 4. 41E-01 9.64E-01 3. 0lE-01 2.73E-01 2.0lE+00 5.87E-01 3.19E-01 4.56E-01
l.44E+00
Tolerance
Nuclide
LU-173 NP-239 CM-243
SB-125
0231
Analysis Report for 1803111-03
m
M
AC-SED-11
Peak No. Energy (keV)
16 563.56 19 663.21 20 750.47 22 771.59 23 795.62 26 932.18 27 950.24 29 1003.27 32 1237.76 33 1327.57 34 1335.60 35 1352.42 36 1377.95 37 1457.14 39 1510.18 40 1589.70 41 1597.80 42 1639.41 43 1662.23 44 1729.66 45 1739.41 47 1832.00 48 1887.19 49 1894.20 50 2027.45
M ::: First peak in a multiplet region
m == Other peak in a multiplet region
F ::: Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 6:43:09AM
Peak Size (CPS) Peak CPS(%) Peak
Uncertainty Type
5.79914E-03 56.37 Tol.
1. 98391E-02 26.04 Sum
6.99561E-03 56.29 4. 52116E-03 58.47 8.99740E-03 34.13 Sum
9.10769E-03 42.04 3. 40278E-03 55.82 S-Esc
1.20946E-02 37.18 6.63479E-03 49.00 Tol.
2.08333E-03 57.74 7. 96627E-03 31.15 3.60532E-03 54.10 6.36076E-03 44.63 3.40748E-03 74.27 3.64444E-03 53.35 3.76208E-03 54.38 1.92901E-03 50.01 Sum
2.08333E-03 55.18 3.05556E-03 30.15 2.63889E-03 51.70 Sum
1. 42361E-03 68.99 2.22222E-03 35.36 1.86728E-03 55.79 Sum
2.77778E-03 31.62 1.25000E-03 63.83
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Nuclide Id Energy Yield(%) Activity
Page 14 of29
Tolerance Nuclide
CS-134
CO-56
Activity
Name Confidence (keV) (pCi/grams) Uncertainty
BE-7 0.97 477.59 * 10.42 7.08E-01 6.41E-01
K-40 0.99 1460.81 * 10.67 1.60E+0l 2.17E+00
FE-59 0.30 1099.22 * 56.50 1.38E-01 1.78E-01
0232
4/17/2018 6:43:09AM Page 15 of29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCi/grams) Uncertainty
FE-59 0.30 1291.56 43.20
GA-67 0.37 93.31 * 35.70 5.00E+0l 3. 96E+0l
208.95 2.24 300.22 16.00
NB-95 0.90 765.79 * 99.81 8.86E-02 6.95E-02
TL-208 0.98 583.14 * 30.22 9.75E-01 3.03E-01
860.37 * 4.48 l.17E+00 1.02E+00
2614.66 * 35.85 6.58E-01 2.12E-01
PB-210 0.93 46.50 * 4.25 2.l0E+00 1.36E+00
PB-212 0.81 238.63 * 44.60 1.44E+00 2.72E-0l
300.09 3.41
BI-214 0.99 609.31 * 46.30 1.l0E+00 2.43E-01
1120.29 * 15.10 6.62E-01 6.07E-01
1764.49 * 15.80 8. 72E-01 4.41E-01
2204.22 * 4.98 2.30E+00 9.64E-01
PB-214 0.98 295.21 * 19.19 l.17E+00 3.0lE-01
351.92 * 37.19 1.09E+00 2.73E-0l
RA-226 0.99 186.21 * 3.28 3.03E+00 2.0lE+00
AC-228 0.98 338.32 * 11. 40 l.15E+00 5.87E-01
911.07 * 27.70 8.60E-01 3.19E-01
969. 11 * 16.60 7.38E-01 4.56E-01
PA-231 0.31 283.67 1. 60 302.67 * 2.30 1.37E+00 1.44E+00
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
INTERFERENCE CORRECTED REPORT
Nuclide Nuclide Wt mean Wt mean Comments
Name Id Activity Activity
Confidence (pCilgrams) Uncertainty
BE-7 0.976 7.08E-01 6.41E-01
K-40 0.999 1.60E+0l 2.17E+00
FE-59 0.308 1.38E-01 1.78E-01
GA-67 0. 377 5.00E+0l 3.96E+0l
0233
Analysis Report for 1803111-03
? = X =
AC-SED-11
Nuclide Name
NB-95 TL-208 PB-210 PB-212 BI-214 PB-214 RA-226 AC-228 PA-231
Nuclide Id
Confidence
0.901 0.988 0.936 0.815 0.997 0.989 0.991 0.982 0.314
nuclide is part of an undetermined solution
nuclide rejected by the interference analysis
4/17/2018 6:43:09AM
Wt mean Wt mean
Activity Activity
(pCilgrams) Uncertainty
8.86E-02 6.95E-02 7.74E-01 1.71E-01 2.l0E+00 1.36E+00 1.44E+00 2. 72E-01 1.06E+00 1.97E-0l 1.13E+00 2.02E-01 3.03E+00 2.0lE+00 8.74E-01 2.39E-01 1.37E+00 1.44E+00
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigrna
Page 16 of29
Comments
0234
Analysis Report for 1803111-03
m
M
AC-SED-11
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (ke VJ
2 76.59
4 99.87
7 277.51
12 408.80
13 463.05
15 511.42
16 563.56
19 663.21
20 750.47
22 771.59
23 795.62
26 932.18
27 950.24
29 1003.27
32 1237.76
33 1327.57
34 1335.60
35 1352.42
36 1377. 95
37 1457.14
39 1510.18
40 1589.70
41 1597.80
42 1639.41
43 1662.23
44 1729.66
45 1739.41
47 1832.00
48 1887.19
49 1894.20
50 2027.45
4/17/2018 6:43:09AM
UNIDENTIFIED PEAKS
: 4/17/2018 6:43:01AM
: 1 : 4096
Peak Size (CPS)
1. 76911E-01
2.27560E-02
l.46292E-02
7.22222E-03
9. 98112E-03
1.35394E-02
5.79914E-03
1. 98391E-02
6.99561E-03
4. 52116E-03
8.99740E-03
9.10769E-03
3.40278E-03
1.20946E-02
6.63479E-03
2.08333E-03
7. 96627E-03
3.60532E-03
6.36076E-03
3.40748E-03
3.64444E-03
3.76208E-03
1.92901E-03
2.08333E-03
3.05556E-03
2.63889E-03
l.42361E-03
2.22222E-03
1. 86728E-03
2.77778E-03
1.25000E-03
Peak CPS(%) Peak
Uncertainty Type
9 .11 D-Esc
43.05 Tol.
44.00 Tol.
54.19 41. 22 Tol.
42.63
56.37 Tol.
26.04 Sum
56.29
58.47
34. 13 Sum
42.04 55.82 S-Esc
37.18
49.00 Tol.
57.74 31.15
54.10 44.63 74.27 53.35
54.38 50.01 Sum
55.18
30.15
51.70 Sum
68.99 35.36
55.79 Sum
31.62
63.83
Page 17 of29
Tolerance Nuclide
LU-173 NP-239 CM-243
SB-125
CS-134
CO-56
0235
Analysis Report for 1803111-03
AC-SED-11
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 6:43:09AM
NUCLIDE MDA REPORT
Nuclide Library Used : \ \0 R-GAM MA 1 \ApexRoot\Countroom\Library\ TMA2. N LB
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCilgrams) (pCilgrams) (pCi/grams)
+ BE-7 477.59 * 10.42 7.08E-01 1.0lE+00 1.0lE+00
+ NA-22 1274.54 99.94 -1.57E-02 8.99E-02 8.99E-02
+ NA-24 1368.53 99.99 2.00E-02 4.36E-02 8.15E-02
2754.09 99.86 7.04E-03 4.36E-02
+ AL-26 1808.65 99.76 -4. 27E-03 6.78E-02 6.78E-02
+ K-40 1460.81 * 10.67 1.60E+0l 1.15E+00 1.15E+00
+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 l.00E+26
+ TI-44 67.88 94.40 -4.38E-02 7.21E-02 7.21E-02
78.34 96.00 1.63E-01 9.39E-02
+ SC-46 889.25 98.98 -4.30E-02 1.0lE-01 1.0lE-01
1120. 51 99.90 1.41E-01 l.64E-01
+ V-48 983.52 99.98 9.00E-02 2.76E-01 2.76E-01
1312.10 97.50 4.41E-02 3.02E-01
+ CR-51 320.08 9.83 -7.47E-01 1.07E+00 1.07E+00
+ MN-54 834.83 99.97 1.00E-02 9.59E-02 9.59E-02
+ CO-56 846.75 99. 96 -8.84E-04 1.04E-01 1.04E-01
1037.75 14.03 l.l0E-01 8.75E-01
1238.25 67.00 1. 58E-01 2.47E-01
1771.40 15.51 6.59E-02 5.91E-01
2587.48 16.90 3.62E-02 3.36E-01
+ CO-57 122.06 85.51 4.55E-02 6.50E-02 6.50E-02
136.48 10.60 1.05E-01 5.53E-01
+ CO-58 810.76 99.40 1.04E-02 9.87E-02 9.87E-02
+ FE-59 1099.22 * 56.50 1.38E-01 2.88E-01 2.91E-01
1291.56 43.20 -7.54E-02 2.88E-01
+ CO-60 1173.22 100.00 3.08E-02 9.84E-02 1.07E-01
1332.49 100.00 1.95E-02 9.84E-02
+ ZN-65 1115.52 50.75 5.57E-02 2.14E-01 2.14E-01
+ GA-67 93.31 * 35.70 5.00E+0l 6.38E+0l 6.38E+0l
208.95 2.24 1.77E+02 7. 85E+02
300.22 16.00 2.35E+0l 1.09E+02
+ SE-75 121.11 16.70 5.81E-02 1.07E-01 3.55E-01
Page 18 of29
0236
4/17/2018 6:43:09AM Page 19 of29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCilgrams) (pCilgrams)
SE-75 136.00 59.50 2.04E-02 1.07E-01 1.07E-01
264.65 59.80 -2.40E-03 1.l0E-01
279.53 25.20 9.12E-02 2.65E-01
400.65 11. 40 -4.93E-02 5.73E-01
+ RB-82 776.52 13.00 -4.35E-01 1.22E+00 1.22E+00
+ RB-83 520.41 46.00 5.20E-02 1.69E-01 1.69E-01
529.64 30.30 -1.17E-01 2.19E-01
552.65 16.40 -4. llE-02 4.72E-01
+ KR-85 513.99 0.43 -1.llE+0l 1.58E+0l 1.58E+0l
+ SR-85 513.99 99. 27 -6.41E-02 9.18E-02 9.18E-02
+ Y-88 898.02 93.40 2.36E-02 7.26E-02 1.02E-01
1836.01 99.38 1.03E-02 7.26E-02
+ MO-93 263.06 56.72 8.85E-03 6.44E-02 9.83E-02
684.67 99.68 -1.62E-02 7.07E-02
1477.11 99.08 -9.45E-03 6.44E-02
+ NB-93M 16.57 9.43 0.00E+00 l.28E+00 1.28E+00
+ NB-94 702.63 100.00 -3.69E-03 8.49E-02 8.49E-02
871.10 100.00 1.32E-03 9.0lE-02
+ NB-95 765.79 * 99.81 8.86E-02 1.82E-01 1.82E-01
+ NB-95M 235.69 25.00 -3.76E+02 4.04E+0l 4.04E+0l
+ ZR-95 724.18 43.70 8.37E-02 1.98E-01 2.73E-01
756.72 55.30 -2.62E-02 1.98E-01
+ MO-99 181.06 6.20 -1.20E+0l 5.41E+02 8.06E+02
739.58 12.80 1.88E+02 5.41E+02
778.00 4.50 -l.09E+02 1.53E+03
+ TC-99M 140.51 89.00 1.86E-02 6.00E-02 6.00E-02
+ RU-103 497.08 89.00 8.llE-03 1.0lE-01 1.0lE-01
+ RU-106 621.84 9.80 3.58E-01 8.42E-01 8.42E-01
+ AG-108M 433.93 89.90 -2.42E-03 6.31E-02 6.31E-02
614.37 90.40 -1.17E-02 8.34E-02
722.95 90.50 -5.66E-02 8.78E-02
+ CD-109 88.03 3. 72 3.08E+00 2.02E+00 2.02E+00
+ AG-ll0M 657.75 93.14 -l.12E-02 8.34E-02 8.34E-02
677.61 10.53 2.90E-01 7.97E-01
706.67 16.46 -1.58E-03 5.24E-01
763.93 21.98 1.91E-02 4.40E-01
884.67 21.98 4.48E-02 4.21E-01
1384.27 23.94 6.13E-02 3.51E-01
+ CD-113M 263.70 0.02 2.18E+0l 2.42E+02 2.42E+02
+ SN-113 255.12 1. 93 -9.36E-02 9.68E-02 3.27E+00
391.69 64.90 -3.95E-02 9.68E-02
+ TE-123M 159.00 84.10 -2.95E-02 6.83E-02 6.83E-02
+ SB-124 602.71 97.87 -9.49E-03 8.97E-02 8.97E-02
645.85 7.26 4.18E-0l 1.56E+00
722.78 11.10 -6.29E-01 9.75E-01
1691.02 49.00 4.95E-02 2.08E-01
+ I-125 35.49 6.49 -2.29E-01 1.86E+00 1.86E+00
+ SB-125 176.33 6.89 1.12E-01 1.98E-01 8.38E-01
0237
4/17/2018 6:43:09AM Page 20 of 29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCilgrams) (pCi/grams) (pCilgrams)
SB-125 427.89 29.33 -1.90E-03 1.98E-01 1.98E-01
463.38 10.35 S.24E-01 6.79E-01
600.56 17.80 1.66E-01 3.96E-01
635.90 11. 32 2.84E-01 6.30E-01
+ SB-126 414.70 83.30 1.lSE-02 7.40E-02 7.40E-02
666.33 99.60 -9.37E-02 8.lOE-02
695.00 99.60 4.18E-03 8.06E-02
720.50 53.80 1.34E-02 1.46E-01
+ SN-126 87.57 37.00 -3.56E-01 1.83E-01 1.83E-01
+ SB-127 473.00 25.00 -1.97E+OO 2.48E+Ol 2.67E+Ol
685.00 35.70 -S.68E+00 2.48E+Ol
783.80 14.70 3.0SE+Ol 7.81E+Ol
+ I-129 29.78 57.00 -7. llE-03 2.27E-01 2.27E-01
33.60 13.20 1.63E-01 7.98E-01
39.58 7.52 -3.57E-03 9.83E-01
+ I-131 284.30 6.05 2.62E+OO 6.63E-01 9.14E+OO
364.48 81.20 -4.12E-01 6.63E-01
636.97 7.26 2.7SE+OO 9.80E+OO
722.89 1. 80 -2.89E+Ol 4.48E+Ol
+ TE-132 49. 72 13.10 -1.80E+02 1.8SE+Ol 1.26E+02
228.16 88.00 -9.26E-01 1.8SE+Ol
+ BA-133 81.00 33.00 -1.20E-01 9.70E-02 1.79E-Ol
302.84 17.80 1.25E-01 3.23E-01
356.01 60.00 3.53E-02 9.70E-02
+ I-133 529.87 86.30 -7.12E+07 1.34E+08 1.34E+08
+ XE-133 81.00 38.00 -3.62E+OO S.41E+OO S.41E+OO
+ CS-134 563.23 8.38 3.62E-01 6.92E-02 7.7SE-Ol
569.32 15.43 7.SOE-02 4.08E-01
604.70 97.60 -1.91E-02 6.92E-02
795.84 85.40 7.89E-02 1.lSE-01
801.93 8.73 -6.06E-03 9.59E-01
+ CS-135 268.24 16.00 4.80E-02 3.7SE-01 3.75E-01
+ @ I-135 1131. 51 22. so 1.00E+26 1.00E+26 1.00E+26
@ 1260.41 28.60 1.00E+26 1.00E+26
@ 1678.03 9.54 1.00E+26 1.00E+26
+ CS-136 153.22 7.46 4.94E-01 3.02E-01 3.04E+OO
163.89 4.61 2.14E+OO 4.80E+OO
176.55 13.56 2.30E-01 1. 72E+OO
273.65 12.66 -4.22E-01 1.89E+OO
340.57 48.50 1.28E+OO 7.03E-01
818.50 99.70 -4.12E-02 3.02E-01
1048.07 79.60 -1.72E-01 4.68E-01
1235.34 19.70 1.63E-01 2.6SE+OO
+ CS-137 661.65 85.12 4.18E-02 1.16E-01 1.16E-01
+ LA-138 788.74 34.00 8.54E-02 1.36E-01 2.62E-01
1435.80 66.00 3.22E-02 1.36E-01
+ CE-139 165.85 80.35 -3.71E-02 7.43E-02 7.43E-02
+ BA-140 162.64 6.70 -8. 72E-01 1.09E+OO 3.29E+OO
304.84 4.50 3.3SE-01 S.13E+OO
0238
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Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)
BA-140 423.70 3.20 -l.03E+00 l.09E+00 7.16E+00
437.55 2.00 -3.80E-01 1. 27E+0l
537.32 25.00 4.73E-01 l.09E+00
+ LA-140 328. 77 20.50 8.69E-01 2.99E-01 l.29E+00
487.03 45.50 -7.75E-03 5.91E-01
815.85 23.50 -1.0lE+00 l.16E+00
1596.49 95.49 -l.20E-02 2.99E-0l
+ CE-141 145.44 48.40 -2. 21E-02 l.98E-0l l.98E-0l
+ CE-143 57.36 11. 80 -2.92E+05 l.54E+05 4.61E+05
293.26 42.00 l.62E+05 l.54E+05
664.55 5.20 2.05E+06 l.53E+06
+ CE-144 133.54 10.80 -2.83E-01 5.14E-01 5.14E-01
+ PM-144 476.78 42.00 9.66E-02 8.21E-02 l.71E-0l
618.01 98.60 7.25E-03 8. 21E-02
696. 4 9 99.49 -2.87E-02 8.51E-02
+ PM-145 36.85 21.70 l. l3E-01 2.08E-0l 3.91E-0l
37.36 39.70 5.98E-02 2.08E-0l
42.30 15.10 8.42E-02 4.66E-0l
72. 40 2.31 3.09E-0l 3.15E+00
+ PM-146 453.90 39.94 -8.38E-02 l.52E-0l l.52E-0l
735.90 14.01 -5.15E-02 5.37E-0l
747.13 13.10 -4.77E-03 6.29E-0l
+ ND-147 91.11 28.90 6.93E-01 l.39E+00 l.39E+00
531.02 13 .10 -5.86E-01 2.37E+00
+ PM-149 285.90 3.10 -l.68E+03 8.26E+03 8.26E+03
+ EU-152 121.78 20.50 l.78E-01 2.54E-01 2.54E-01
244.69 5.40 l.22E-01 l.19E+00
344.27 19 .13 -4.21E-02 2.92E-01
778.89 9.10 l.56E-0l 9.07E-01
964.01 10.40 l.58E-0l l.0lE+00
1085.78 7.22 2.67E-03 l.24E+00
1112.02 9.60 l. llE-01 l.00E+00
1407.95 14.94 9.l9E-02 5.84E-0l
+ GD-153 97.43 31.30 -2. 96E-0l l.92E-0l l.92E-0l
103.18 22.20 -2. 72E-0l 2.52E-0l
+ EU-154 123.07 40.50 -6. 72E-02 l.27E-0l l.27E-01
723.30 19.70 -l.84E-01 4.20E-01
873.19 11. 50 5.57E-0l 7.74E-0l
996. 32 10.30 -3.23E-01 8.26E-0l
1004.76 17.90 l.23E-01 5.40E-0l
1274.45 35.50 -4.37E-02 2.50E-0l
+ EU-155 86.50 30.90 3.54E-01 2.30E-0l 2.30E-01
105.30 20.70 l.98E-01 2.57E-0l
+ EU-156 811. 77 10.40 3.31E-0l 2.35E+00 2.35E+00
1153.47 7.20 l.22E+00 4.66E+00
1230.71 8.90 5.79E-01 4.l0E+00
+ HO-166M 184.41 72. 60 8.03E-02 9.85E-02 9.85E-02
280.45 29.60 -l.23E-01 l.79E-0l
410.94 11.10 -l.0lE-01 5.21E-0l
0239
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Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)
HO-166M 711.69 54.10 3.09E-02 9.85E-02 1.48E-01
+ TM-171 66. 72 0.14 -2.29E+0l 5.30E+0l 5.30E+0l
+ HF-172 67.35 5.31 -8.30E-01 4.81E-01 1.33E+00
125.82 11. 30 -3.81E-01 4.81E-01
+ LU-1 72 181.53 20.60 -6.68E-02 2.14E+00 4.49E+00
900.72 29.81 -2.46E+00 4.16E+00
1093.66 62.50 -4.43E-01 2.14E+00
+ LU-173 100.72 5.24 l.04E+00 2.97E-01 1.15E+00
272.11 21.20 5. 27E-02 2.97E-01
+ HF-175 343.40 84.00 5.19E-03 8.76E-02 8.76E-02
+ LU-176 88.34 13.30 8.27E-01 5.49E-02 5.42E-01
201.83 86.00 5.25E-03 6.73E-02
306.78 94.00 1.71E-02 5.49E-02
+ HF-181 133. 02 41.70 -1.06E-01 1.14E-01 1.93E-01
345.85 17.20 3. llE-01 5.30E-01
482.03 82.80 1.42E-02 1.14E-01
+ TA-182 67.75 41.20 -1.18E-01 1.94E-01 1.94E-01
1121.30 34.90 4.l0E-01 4.39E-01
1189.05 16.23 4.02E-02 7.66E-01
1221.41 26.98 -3.66E-02 4.86E-01
1231.02 11. 44 l.56E-01 1.l0E+00
+ IR-192 308.46 29.68 4.63E-02 1.44E-01 2.21E-01
468.07 48.10 -6.36E-03 1.44E-01
+ HG-203 279.19 77.30 3.79E-02 1.l0E-01 1.l0E-01
+ TL-204 374.74 94 .11 -1. 96E-02 5.68E-02 5.68E-02
899.15 99.16 -3.74E-02 7.74E-02
911.74 91.10 2.78E-01 1.65E-01
+ BI-207 569.67 97. 72 l.16E-02 6.30E-02 6.30E-02
1063.62 74.90 -1.44E-02 l.24E-01
+ TL-208 583.14 * 30.22 9.75E-01 l.34E-01 3.80E-01
860.37 * 4.48 1.17E+00 1.56E+00
2614.66 * 35.85 6.58E-01 1.34E-01
+ BI-210M 262.00 45.00 -5.81E-02 1.24E-01 1.24E-01
300.00 23.00 5.41E-02 2.50E-01
+ PB-210 46.50 * 4.25 2.l0E+00 2.15E+00 2.15E+00
+ PB-211 404.84 2.90 3.30E-01 1.86E+00 1.86E+00
831.96 2.90 -1.16E+00 2.78E+00
+ BI-212 727.17 11. 80 2.14E-01 7.73E-01 7.73E-01
1620.62 2.75 1.39E+00 2.85E+00
+ PB-212 238.63 * 44.60 1.44E+00 2.35E-0l 2.35E-01
300.09 3.41 3.65E-01 1.69E+00
+ BI-214 609.31 * 46.30 1.l0E+00 2.46E-0l 2.46E-01
1120.29 * 15.10 6.62E-01 9.68E-01
1764.49 * 15.80 8. 72E-01 5. 72E-01
2204.22 * 4.98 2.30E+00 2.49E-01
+ PB-214 295.21 * 19.19 1.17E+00 2.42E-01 6.61E-01
351.92 * 37.19 1.09E+00 2.42E-01
+ RN-219 401.80 6.50 3.65E-01 8.80E-01 8.80E-0l
0240
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Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%} Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCilgrams)
+ RA-223 323.87 3.88 -4.64E-01 1.38E+00 1.38E+00
+ RA-224 240.98 3.95 4.72E+00 2.70E+00 2.70E+00
+ RA-225 40.00 31.00 -3.54E-01 8.l0E-01 8.l0E-01
+ RA-226 186.21 * 3.28 3.03E+00 3.18E+00 3.18E+00
+ TH-227 50.10 8.40 7.63E-02 6.33E-01 6.33E-01
236.00 11. 50 -l.86E+00 7.66E-01
256.20 6.30 -3.36E-01 8.99E-01
+ AC-228 338.32 * 11. 40 1.15E+00 3.52E-01 8.59E-01
911.07 * 27.70 8.60E-01 3.52E-0l
969 .11 * 16.60 7.38E-01 6.61E-01
+ TH-230 48.43 16.90 4. llE-01 4.07E-01 4.07E-01
62.85 4.60 l.42E+00 1.70E+00
67.67 0.37 -1.16E+0l 1.85E+0l
+ PA-231 283.67 1. 60 1.61E+00 3.33E+00 3.33E+00
302.67 * 2.30 1.37E+00 5.53E+00
+ TH-231 25.64 14.70 0.00E+00 7.27E-02 7. 27E-02
84.21 6.40 -9.35E-01 9.87E-01
+ PA-233 311.98 38.60 3.67E-02 2.81E-01 2.81E-01
+ PA-234 131.20 20.40 9.15E-03 2.62E-01 2.62E-01
733.99 8.80 -2.88E-01 8.54E-01
946.00 12.00 5.54E-03 6.76E-01
+ PA-234M 1001.03 0.92 3.68E+00 1.08E+0l 1.08E+0l
+ TH-234 63.29 3.80 1. 72E+00 2.05E+00 2.05E+00
+ U-235 143.76 10.50 4.80E-02 5.06E-01 5.06E-01
163.35 4.70 4.91E-01 1.13E+00
205.31 4.70 -5.06E-01 1.17E+00
+ NP-237 86.50 12.60 8.60E-01 5.58E-01 5.58E-01
+ NP-239 106.10 22.70 2.97E+02 6.19E+02 6.19E+02
228.18 10.70 -6.81E+0l 1.36E+03
277.60 14.10 4.66E+02 1.17E+03
+ AM-241 59.54 35.90 1.49E-01 2.05E-01 2.05E-01
+ AM-243 74.67 66.00 -4.57E-0l 1. 2 9E-01 1.29E-01
+ CM-243 209.75 3.29 3.99E-01 4.36E-01 1.78E+00
228.14 10.60 -2.53E-02 5.07E-01
277.60 14.00 1.73E-01 4.36E-01
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
0241
4/17/2018 6:43:09AM Page 24 of29
Analysis Report for 1803111-03
AC-SED-11
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCilgrams)
+ BE-7 47'7.59 * 10.42 1.0lE+00 1.0lE+00 7.08E-01 4.75E-01
NA-22 1274.54 99.94 8.99E-02 8.99E-02 -1.57E-02 4.02E-02
NA-24 1368.53 99.99 8.15E-02 4.36E-02 2.00E-02 3.58E-02
2754.09 99.86 4.36E-02 7.04E-03 1.54E-02
AL-26 1808.65 99.76 6. 78E-02 6.78E-02 -4. 27E-03 2.81E-02
+ K-40 1460.81 * 10.67 1.15E+00 1.15E+00 l.60E+0l 5.25E-01
@ AR-41 1293.64 99.16 1.00E+26 1.00E+26 l.00E+26 1.00E+20
TI-44 67.88 94.40 7.21E-02 7.21E-02 -4.38E-02 3.50E-02
78. 34 96. 00 9.39E-02 1.63E-01 4.60E-02
SC-46 889.25 98.98 1.0lE-01 1.0lE-01 -4.30E-02 4.62E-02
1120. 51 99.90 1.64E-01 1.41E-01 7.65E-02
V-48 983.52 99.98 2.76E-01 2.76E-01 9.00E-02 l.26E-01
1312.10 97.50 3.02E-01 4.41E-02 1.35E-01
CR-51 320.08 9.83 1.07E+00 1.07E+00 -7.47E-01 5.05E-01
MN-54 834.83 99.97 9.59E-02 9.59E-02 1.00E-02 4.44E-02
CO-56 846.75 99. 96 1.04E-01 1.04E-01 -8.84E-04 4.77E-02
1037.75 14.03 8.75E-01 1.l0E-01 4.00E-01
1238.25 67.00 2.47E-01 1.58E-0l l.15E-01
1771.40 15.51 5.91E-01 6.59E-02 2.48E-01
2587.48 16.90 3.36E-01 3.62E-02 l.19E-01
CO-57 122.06 85.51 6.50E-02 6.50E-02 4.55E-02 3.14E-02
136.48 10.60 5.53E-01 1.05E-01 2.67E-01
CO-58 810.76 99.40 9.87E-02 9.87E-02 1.04E-02 4.50E-02
+ FE-59 1099.22 * 56.50 2.91E-01 2.88E-01 1.38E-01 l.34E-01
1291.56 43.20 2.88E-01 -7.54E-02 1.28E-01
CO-60 1173.22 100.00 1.07E-01 9.84E-02 3.08E-02 4.90E-02
1332.49 100.00 9.84E-02 l.95E-02 4.43E-02
ZN-65 1115.52 50.75 2.14E-01 2.14E-01 5.57E-02 9.81E-02
+ GA-67 93.31 * 35.70 6.38E+0l 6.38E+0l 5.00E+0l 3.12E+0l
208.95 2.24 7.85E+02 1.77E+02 3.77E+02
300.22 16.00 1.09E+02 2.35E+0l 5.16E+0l
SE-75 121.11 16.70 3.55E-0l 1.07E-01 5.81E-02 1.71E-01
136.00 59.50 1.07E-01 2.04E-02 5.18E-02
264.65 59.80 1.l0E-01 -2.40E-03 5.24E-02
279.53 25.20 2.65E-01 9.12E-02 1.26E-01
400.65 11. 40 5.73E-01 -4.93E-02 2.68E-01
RB-82 776.52 13.00 1.22E+00 1.22E+00 -4.35E-01 5.57E-01
RB-83 520.41 46.00 l.69E-01 1.69E-01 5.20E-02 7.83E-02
529.64 30.30 2.19E-01 -l.17E-0l l.00E-01
552.65 16.40 4. 72E-01 -4. llE-02 2.18E-01
KR-85 513.99 0.43 1.58E+0l 1.58E+0l -1.llE+0l 7.39E+00
SR-85 513.99 99. 27 9.18E-02 9.18E-02 -6.41E-02 4.29E-02
0242
4/17/2018 6:43:09AM Page 25 of 29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCi/grams)
Y-88 898.02 93.40 1.02E-0l 7.26E-02 2.36E-02 4.64E-02
1836.01 99.38 7.26E-02 1.03E-02 2.93E-02
MO-93 263.06 56. 72 9.83E-02 6.44E-02 8.85E-03 4.67E-02
684.67 99.68 7.07E-02 -1.62E-02 3.25E-02
1477.11 99.08 6.44E-02 -9.45E-03 2.70E-02
NB-93M 16.57 9.43 1.28E+00 l.28E+00 0.00E+00 0.00E+00
NB-94 702.63 100.00 8.49E-02 8.49E-02 -3.69E-03 3.95E-02
871.10 100.00 9.0lE-02 l.32E-03 4.16E-02
+ NB-95 765.79 * 99.81 1.82E-01 l.82E-01 8.86E-02 8.57E-02
NB-95M 235.69 25.00 4.04E+0l 4.04E+0l -3.76E+02 1.93E+0l
ZR-95 724.18 43.70 2.73E-01 l.98E-01 8.37E-02 l.27E-01
756.72 55.30 l.98E-01 -2.62E-02 9.14E-02
MO-99 181.06 6.20 8.06E+02 5.41E+02 -1.20E+0l 3.88E+02
739.58 12.80 5. 41E+02 1.88E+02 2.50E+02
778.00 4.50 1.53E+03 -l.09E+02 7.02E+02
TC-99M 140.51 89.00 6.00E-02 6.00E-02 1.86E-02 2.89E-02
RU-103 497.08 89.00 1.0lE-01 1.0lE-01 8.llE-03 4.66E-02
RU-106 621. 8 4 9.80 8.42E-01 8.42E-01 3.58E-01 3.92E-01
AG-108M 433.93 89.90 6.31E-02 6.31E-02 -2.42E-03 2.93E-02
614.37 90.40 8.34E-02 -l.17E-02 3.88E-02
722.95 90.50 8.78E-02 -5.66E-02 4.06E-02
CD-109 88.03 3.72 2.02E+00 2.02E+00 3.08E+00 9.85E-01
AG-ll0M 657.75 93.14 8.34E-02 8.34E-02 -l.12E-02 3.85E-02
677.61 10.53 7.97E-01 2.90E-01 3.70E-01
706.67 16.46 5.24E-01 -l.58E-03 2.43E-01
763.93 21.98 4.40E-01 l.91E-02 2.04E-01
884.67 21.98 4.21E-01 4.48E-02 1.93E-01
1384.27 23.94 3.51E-01 6.13E-02 l.53E-01
CD-113M 263.70 0.02 2.42E+02 2.42E+02 2.18E+0l l.15E+02
SN-113 255.12 1. 93 3.27E+00 9.68E-02 -9.36E-02 1.56E+00
391.69 64.90 9.68E-02 -3.95E-02 4.51E-02
TE-123M 159.00 84.10 6.83E-02 6.83E-02 -2.95E-02 3. 27E-02
SB-124 602.71 97.87 8.97E-02 8.97E-02 -9.49E-03 4.13E-02
645.85 7.26 1.56E+00 4.18E-01 7.30E-01
722.78 11.10 9.75E-01 -6.29E-01 4.51E-01
1691.02 49.00 2.08E-01 4.95E-02 8.85E-02
I-125 35.49 6.49 1.86E+00 1.86E+00 -2.29E-0l 8.86E-01
SB-125 176.33 6.89 8.38E-01 1.98E-01 1.12E-01 4.03E-0l
427.89 29.33 l.98E-01 -1.90E-03 9.20E-02
463.38 10.35 6.79E-01 5.24E-0l 3.19E-01
600.56 17.80 3.96E-01 1.66E-0l l.84E-01
635.90 11. 32 6.30E-01 2.84E-01 2.91E-0l
SB-126 414.70 83.30 7.40E-02 7.40E-02 1.15E-02 3.47E-02
666.33 99.60 8.l0E-02 -9.37E-02 3.77E-02
695.00 99.60 8.06E-02 4.18E-03 3.74E-02
720.50 53.80 l.46E-01 1.34E-02 6.74E-02
SN-126 87.57 37.00 1.83E-01 l.83E-01 -3.56E-01 8.89E-02
SB-127 473.00 25.00 2.67E+0l 2.48E+0l -1.97E+00 1.23E+0l
685.00 35.70 2.48E+0l -5.68E+00 l.14E+0l
783.80 14.70 7.81E+0l 3.05E+0l 3.63E+0l
I-129 29.78 57.00 2.27E-01 2.27E-01 -7. llE-03 l.08E-01
33.60 13.20 7.98E-01 l.63E-01 3.81E-01
39.58 7.52 9.83E-01 -3.57E-03 4.69E-01
0243
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Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi!grams) (pCi!grams) (pCi!grams)
I-131 284.30 6.05 9.14E+00 6.63E-01 2.62E+00 4.33E+00
364.48 81.20 6.63E-01 -4.12E-01 3.l0E-01
636.97 7.26 9.80E+00 2.75E+00 4.52E+00
722.89 1. 80 4.48E+0l -2.89E+0l 2.07E+0l
TE-132 49.72 13. 10 1.26E+02 1.85E+0l -l.80E+02 6.02E+0l
228.16 88.00 1.85E+0l -9.26E-01 8.84E+00
BA-133 81.00 33.00 l.79E-01 9.70E-02 -l.20E-01 8.69E-02
302.84 17.80 3.23E-01 l.25E-01 l.53E-01
356.01 60.00 9.70E-02 3.53E-02 4.57E-02
I-133 529.87 86.30 1.34E+08 1.34E+08 -7.12E+07 6.12E+07
XE-133 81.00 38.00 5.41E+00 5.41E+00 -3.62E+00 2.62E+00
CS-134 563.23 8.38 7.75E-01 6.92E-02 3.62E-01 3.58E-01
569.32 15.43 4.08E-01 7.50E-02 l.88E-01
604.70 97.60 6.92E-02 -1.91E-02 3.19E-02
795.84 85.40 l.15E-01 7.89E-02 5.35E-02
801.93 8.73 9.59E-01 -6.06E-03 4.41E-01
CS-135 268.24 16.00 3.75E-01 3.75E-01 4.80E-02 l.79E-01
@ I-135 1131.51 22.50 1.00E+26 1.00E+26 l.00E+26 l.00E+20
@ 1260.41 28.60 1.00E+26 l.00E+26 1.00E+20
@ 1678.03 9.54 1.00E+26 1.00E+26 1.00E+20
CS-136 153.22 7.46 3.04E+00 3.02E-01 4.94E-01 1.47E+00
163.89 4.61 4.80E+00 2.14E+00 2.31E+00
176.55 13.56 1.72E+00 2.30E-01 8.29E-01
27 3. 65 12.66 1.89E+00 -4.22E-01 9.02E-01
340.57 48.50 7.03E-01 1.28E+00 3.38E-01
818.50 99.70 3.02E-01 -4.12E-02 1.37E-01
1048.07 79.60 4.68E-01 -1. 72E-01 2.13E-01
1235.34 19.70 2.65E+00 1.63E-01 1.23E+00
CS-137 661.65 85.12 l.16E-01 1.16E-01 4.18E-02 5.45E-02
LA-138 788.74 34.00 2.62E-01 l.36E-01 8.54E-02 l.22E-01
1435.80 66.00 1.36E-01 3.22E-02 6.05E-02
CE-139 165.85 80.35 7.43E-02 7.43E-02 -3. 71E-02 3.57E-02
BA-140 162.64 6.70 3.29E+00 1.09E+00 -8. 72E-01 1.58E+00
304.84 4.50 5.13E+00 3.35E-01 2.42E+00
423.70 3.20 7.16E+00 -1.03E+00 3.32E+00
437.55 2.00 1.27E+0l -3.80E-01 5.92E+00
537.32 25.00 1.09E+00 4.73E-01 5.07E-01
LA-140 328.77 20.50 1.29E+00 2.99E-01 8.69E-01 6.llE-01
487.03 45.50 5.91E-01 -7.75E-03 2.75E-01
815.85 23.50 1.16E+00 -1.0lE+00 5.19E-01
1596.49 95.49 2.99E-01 -1.20E-02 1.25E-01
CE-141 145.44 48.40 1.98E-01 1.98E-01 -2.21E-02 9.56E-02
CE-143 57.36 11. 80 4.61E+05 l.54E+05 -2.92E+05 2.24E+05
293.26 42.00 1.54E+05 1.62E+05 7.45E+04
664.55 5.20 l.53E+06 2.05E+06 7.26E+05
CE-144 133.54 10.80 5.14E-01 5.14E-01 -2.83E-01 2.47E-01
PM-144 476.78 42.00 l.71E-01 8.21E-02 9.66E-02 8.0lE-02
618.01 98.60 8.21E-02 7.25E-03 3.82E-02
696.49 99.49 8. 51E-02 -2.87E-02 3.95E-02
PM-145 36.85 21.70 3.91E-01 2.08E-01 l.13E-01 1.86E-01
37.36 39.70 2.08E-01 5.98E-02 9.90E-02
42.30 15.10 4.66E-01 8.42E-02 2.23E-01
72. 40 2.31 3.15E+00 3.09E-01 1.53E+00
0244
4/17/2018 6:43:09AM Page 27 of 29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCi/grams)
PM-146 453.90 39.94 l.52E-01 1.52E-01 -8.38E-02 7.08E-02
735.90 14.01 5.37E-01 -5.15E-02 2.47E-01
747.13 13.10 6.29E-01 -4.77E-03 2.91E-01
ND-147 91.11 28.90 1.39E+00 1.39E+00 6.93E-01 6.77E-01
531.02 13.10 2.37E+00 -5.86E-01 1.09E+00
PM-149 285.90 3.10 8.26E+03 8.26E+03 -1.68E+03 3.92E+03
EU-152 121.78 20.50 2.54E-01 2.54E-01 1.78E-0l 1.22E-01
244.69 5.40 1.19E+00 1.22E-0l 5.70E-01
34 4. 27 19.13 2.92E-01 -4. 21E-02 1.37E-01
778.89 9.10 9.07E-01 1.56E-01 4.18E-01
964.01 10.40 1.0lE+00 1.58E-01 4.66E-01
1085.78 7.22 1.24E+00 2.67E-03 5.62E-01
1112.02 9.60 1.00E+00 1. llE-01 4.56E-01
1407.95 14.94 5.84E-01 9.19E-02 2.59E-01
GD-153 97.43 31.30 1.92E-01 1.92E-01 -2. 96E-01 9.32E-02
103.18 22.20 2.52E-01 -2.72E-01 1.21E-01
EU-154 123.07 40.50 1.27E-01 1.27E-0l -6.72E-02 6. llE-02
723.30 19.70 4.20E-01 -1.84E-01 1.95E-01
873.19 11. 50 7.74E-01 5.57E-01 3.57E-01
996. 32 10.30 8.26E-01 -3.23E-01 3.75E-01
1004.76 17.90 5.40E-01 1.23E-01 2.48E-01
1274.45 35.50 2.50E-01 -4.37E-02 1.12E-01
EU-155 86.50 30.90 2.30E-01 2.30E-01 3.54E-01 1.12E-01
105.30 20.70 2.57E-01 1.98E-01 1.24E-01
EU-156 811.77 10.40 2.35E+00 2.35E+00 3.31E-01 1.07E+00
1153.47 7.20 4.66E+00 1.22E+00 2.13E+00
1230.71 8.90 4.l0E+00 5.79E-01 1.88E+00
HO-166M 184.41 72. 60 9.85E-02 9.85E-02 8.03E-02 4.78E-02
280.45 29.60 1.79E-01 -1.23E-0l 8.49E-02
410.94 11.10 5.21E-01 -1. 0lE-01 2.44E-01
711.69 54.10 1.48E-01 3.09E-02 6.83E-02
TM-171 66. 72 0.14 5.30E+0l 5.30E+0l -2.29E+0l 2.58E+0l
HF-1 72 67.35 5.31 1.33E+00 4.81E-0l -8.30E-01 6.47E-01
125.82 11.30 4.81E-01 -3.81E-01 2.32E-01
LU-1 72 181.53 20.60 4.49E+00 2.14E+00 -6.68E-02 2.16E+00
900. 72 29.81 4.16E+00 -2.46E+00 1.89E+00
1093.66 62.50 2.14E+00 -4.43E-01 9.63E-01
LU-173 100.72 5.24 1.15E+00 2.97E-01 1.04E+00 5.55E-01
272.11 21. 20 2.97E-01 5.27E-02 l.42E-01
HF-175 343.40 84.00 8. 76E-02 8.76E-02 5.19E-03 4.12E-02
LU-176 88.34 13.30 5.42E-01 5.49E-02 8.27E-01 2.65E-01
201.83 86.00 6.73E-02 5.25E-03 3.23E-02
306.78 94.00 5.49E-02 1.71E-02 2.58E-02
HF-181 133.02 41.70 1.93E-01 l.14E-01 -1.06E-01 9.30E-02
345.85 17.20 5.30E-01 3.llE-01 2.50E-01
482.03 82.80 1.14E-01 1.42E-02 5.29E-02
TA-182 67.75 41.20 1.94E-01 1.94E-01 -1.18E-0l 9.44E-02
1121.30 34.90 4.39E-01 4.l0E-01 2.05E-01
1189.05 16.23 7.66E-01 4.02E-02 3.51E-01
1221.41 26.98 4.86E-01 -3.66E-02 2.23E-01
1231.02 11. 44 1.l0E+00 1.56E-01 5.04E-01
IR-192 308.46 29.68 2.21E-01 1.44E-01 4.63E-02 1.04E-01
468.07 48.10 1.44E-01 -6.36E-03 6.65E-02
0245
4/17/2018 6:43:09AM Page 28 of29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi!grams) (pCi!grams) (pCi/grams) (pCi/grams)
HG-203 279.19 77.30 1.l0E-01 1.l0E-01 3.79E-02 5.24E-02
TL-204 374.74 94.11 5.68E-02 5.68E-02 -1.96E-02 2.65E-02
899.15 99.16 7.74E-02 -3.74E-02 3.50E-02
911.74 91.10 1.65E-01 2.78E-01 7.84E-02
BI-207 569.67 97. 72 6.30E-02 6.30E-02 1.16E-02 2.90E-02
1063.62 74.90 1.24E-01 -1.44E-02 5.64E-02
+ TL-208 583.14 * 30.22 3.80E-01 l.34E-01 9.75E-01 1.82E-01
860.37 * 4.48 1.56E+00 1.17E+00 7.05E-01
2614.66 * 35.85 1.34E-01 6.58E-01 4.92E-02
BI-210M 262.00 45.00 l.24E-01 1.24E-01 -5.81E-02 5.92E-02
300.00 23.00 2.50E-01 5.41E-02 1.19E-01
+ PB-210 46.50 * 4.25 2.15E+00 2.15E+00 2.l0E+00 1.04E+00
PB-211 404.84 2.90 1.86E+00 1.86E+00 3.30E-01 8.68E-01
831.96 2.90 2.78E+00 -1.16E+00 l.28E-t-00
BI-212 727.17 11. 80 7.73E-01 7.73E-01 2.14E-01 3.61E-01
1620.62 2.75 2.85E+00 1.39E+00 1.23E+00
+ PB-212 238.63 * 44.60 2.35E-01 2.35E-01 1.44E+00 1.15E-01
300.09 3.41 1.69E+00 3.65E-01 8.0lE-01
+ BI-214 609.31 * 46.30 2.46E-01 2.46E-01 1.l0E+00 l.17E-01
1120.29 * 15.10 9.68E-01 6.62E-01 4.56E-01
1764.49 * 15.80 5.72E-01 8. 72E-01 2.50E-01
2204.22 * 4.98 2.49E-01 2.30E+00 0.00E+00
+ PB-214 295.21 * 19.19 6.61E-01 2.42E-01 1.17E+00 3.23E-01
351.92 * 37.19 2.42E-01 1.09E+00 1.16E-01
RN-219 401.80 6.50 8.80E-01 8.80E-01 3.65E-01 4.12E-01
RA-223 323.87 3.88 1.38E+00 l.38E+00 -4.64E-01 6.51E-01
RA-224 240.98 3.95 2.70E+00 2.70E+00 4. 72E+00 l.32E+00
RA-225 40.00 31.00 8.l0E-01 8.l0E-01 -3.54E-01 3.86E-01
+ RA-226 186.21 * 3.28 3.18E+00 3.18E+00 3.03E+00 1.56E+00
TH-227 50.10 8.40 6.33E-01 6.33E-01 7.63E-02 3.02E-01
236.00 11. 50 7.66E-01 -1.86E+00 3. 72E-01
256.20 6 •' 30 8.99E-01 -3.36E-01 4.29E-01
+ AC-228 338.32 * 11. 40 8.59E-01 3.52E-01 1.15E+00 4.15E-01
911.07 * 27.70 3.52E-01 8.60E-01 1.63E-01
969 .11 * 16.60 6.61E-01 7.38E-01 3.07E-01
TH-230 48.43 16.90 4.07E-01 4.07E-01 4.llE-01 1.96E-01
62.85 4.60 1.70E+00 1.42E+00 8.30E-01
67. 67 0.37 1.85E+0l -1.16E+0l 9.0lE+00
+ PA-231 283.67 1. 60 3.33E+00 3.33E+00 1.61E+00 1.58E+00
302. 67 * 2.30 5.53E+00 1.37E+00 2.70E+00
TH-231 25.64 14.70 7.27E-02 7. 27E-02 0.00E+00 0.00E+00
84.21 6.40 9.87E-01 -9.35E-01 4.79E-01
PA-233 311.98 38.60 2.81E-01 2.81E-01 3.67E-02 1.33E-01
PA-234 131.20 20.40 2.62E-01 2.62E-01 9.15E-03 1.27E-01
733.99 8.80 8.54E-01 -2.88E-01 3.93E-01
946.00 12.00 6.76E-01 5.54E-03 3.07E-01
PA-234M 1001.03 0.92 1.08E+0l 1.08E+0l 3.68E+00 5.00E+00
TH-234 63.29 3.80 2.05E+00 2.05E+00 1.72E+00 1.00E+00
U-235 143.76 10.50 5.06E-01 5.06E-01 4.80E-02 2.44E-01
163.35 4.70 1.13E+00 4.91E-01 5.42E-01
205.31 4.70 1.17E+00 -5.06E-01 5.60E-01
NP-237 86.50 12.60 5.58E-01 5.58E-01 8.60E-01 2. 72E-01
NP-239 106.10 22.70 6.19E+02 6.19E+02 2.97E+02 2.99E+02
0246
4/17/2018 6:43:09AM Page 29 of29
Analysis Report for 1803111-03
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCi/grams) (pCilgrams) (pCi/grams)
NP-239 228.18 10.70 1.36E+03 6.19E+02 -6.81E+0l 6.50E+02
277.60 14.10 1.17E+03 4.66E+02 5.60E+02
AM-241 59.54 35.90 2.05E-01 2.05E-01 1.49E-01 9.97E-02
AM-243 74.67 66.00 1.29E-01 1.29E-01 -4.57E-01 6.30E-02
CM-243 209.75 3.29 1.78E+00 4.36E-01 3.99E-01 8.53E-01
228.14 10.60 5.07E-0l -2.53E-02 2.42E-01
277.60 14.00 4.36E-0l l.73E-0l 2.08E-01
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
No Action Level results available for reporting purposes.
DATA REVIEW COMMENTS REPORT
Creation Date Comment User
No Data Review Comments Entered.
0247
Channel Data Report 4/17/2018 6: 43: 33 AM Page 1
*******************************************************
***** S P E C T R A L D A T A R E P O R T *****
*******************************************************
Sample Title: AC-SED-11
Elapsed Live time: 3600 Elapsed Real Time: 3601
Channell------1-------l-------l-------1-------1-------1-------1-------I
1: 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 22 28 42 46 50
33: 51 45 44 43 44 54 40 48
41: 49 54 58 51 51 78 125 63
49: 42 45 59 51 66 79 63 57
57: 61 90 81 84 85 73 132 117
65: 84 78 85 82 78 78 97 84
7 3: 96 129 241 136 341 175 76 68
81: 58 75 61 109 81 70 124 114
89: 71 148 65 107 159 104 73 43
97: 48 65 83 77 44 66 53 36
105: 66 65 53 43 53 46 58 45
113: 61 55 41 49 51 34 43 47
121: 40 60 50 54 37 62 54 50
129: 73 48 56 43 36 51 52 61
137: 42 55 58 52 42 36 45 64
145: 49 41 44 59 40 47 49 51
153: 55 44 42 45 48 31 39 33
161: 33 41 54 36 46 38 39 41
169: 42 41 43 39 45 40 36 57
177: 44 46 41 44 42 44 51 49
185: 74 126 67 36 39 38 38 44
193: 44 41 36 41 44 39 37 44
201: 45 49 35 27 40 40 34 35
209: 58 36 31 33 35 38 36 37
217: 34 45 36 30 33 37 28 39
225: 23 28 25 27 26 40 35 28
233: 23 31 29 43 39 250 296 62
241: 90 92 24 24 24 28 22 26
249: 20 27 34 19 17 27 19 29
257: 34 31 44 26 21 33 23 29
265: 23 24 30 29 26 39 32 27
273: 22 28 26 29 37 32 21 22
281: 14 18 24 18 32 19 23 26
289: 27 22 20 26 22 40 159 61
2 97: 25 18 19 19 25 34 17 17
305: 18 11 16 26 15 17 19 20
313: 21 19 20 11 22 21 20 18
321: 15 16 26 18 13 15 24 34
329: 19 23 18 21 23 25 24 21
337: 20 80 65 20 22 15 14 17
345: 21 19 25 13 15 23 109 246
353: 53 18 13 21 18 19 14 32
361: 23 11 13 22 14 11 17 24
0248
Channel Data Report 4/17/2018 6:43:33 AM Page 2
369: 12 11 18 15 15 11 6 20
Sample Title: AC-SED-11
Channell------l-------l-------1-------1-------1-------I-------I-------I
377: 15 14 16 20 20 14 10 23
385: 22 9 14 19 9 14 14 18
393: 9 14 15 10 12 13 10 15
401: 16 14 16 9 14 9 19 23
409: 14 16 14 9 17 24 12 17
417: 16 12 8 18 6 5 14 12
425: 19 10 13 9 12 11 14 10
433: 15 13 13 10 11 14 18 14
441: 12 8 11 11 13 18 16 15
449: 17 21 14 11 12 14 13 16
457: 16 12 10 8 9 32 22 9
465: 11 12 8 9 9 10 7 9
473: 10 8 11 10 26 22 16 7
481: 13 9 15 15 8 16 9 12
489: 17 7 14 11 15 8 17 8
497: 5 7 10 10 5 10 15 6
505: 11 6 10 7 20 50 45 23
513: 19 14 7 5 7 12 7 5
521: 15 16 10 12 4 12 9 11
529: 4 9 5 10 15 10 11 17
537: 9 9 8 5 5 12 10 10
545: 11 11 9 14 11 13 6 9
553: 9 12 8 10 10 16 8 1
561: 7 8 14 11 9 8 8 8
569: 9 12 8 5 10 12 7 9
577: 10 5 10 12 14 53 107 33
585: 5 7 11 10 8 7 8 10
593: 6 12 9 12 5 10 12 14
601: 12 5 8 6 15 13 9 64
609: 164 53 13 8 11 6 7 7
617: 9 10 6 11 13 8 9 8
625: 5 7 8 13 7 4 3 3
633: 7 7 7 5 8 12 3 9
641: 6 6 10 9 6 14 13 11
649: 10 8 8 7 13 3 9 8
657: 6 8 4 11 24 30 9 8
665: 15 14 6 4 5 7 10 4
67 3: 9 6 10 8 11 5 6 9
681: 5 6 7 4 6 9 6 9
689: 5 7 10 8 6 4 12 9
697: 7 10 8 12 9 10 9 7
705: 7 9 10 5 7 7 6 7
713: 9 12 5 2 7 10 5 6
721: 7 8 7 10 8 9 16 9
729: 10 6 9 8 7 9 1 4
737: 8 6 5 7 5 14 5 6
745: 5 3 6 10 11 10 9 6
753: 6 8 7 5 9 10 5 8
7 61: 10 4 4 9 9 16 10 17
769: 19 5 13 10 8 4 5 7
777: 5 8 4 11 8 8 4 6
785: 13 9 7 6 7 7 7 5
793: 9 13 15 11 8 3 4 4
0249
Channel Data Report 4/17/2018 6:43:33 AM Page 3
801: 11 5 8 10 9 8 5 6
Sample Title: AC-SED-11
Channell------1-------1-------1-------1-------I-------I-------I-------I
809: 5 8 7 4 2 1 4 2
817: 3 9 6 6 4 9 9 6
825: 10 8 3 3 6 5 9 2
833: 6 10 12 8 5 9 7 9
841: 6 7 9 3 5 3 9 7
849: 3 4 6 2 7 4 9 6
857: 8 4 9 13 10 3 2 2
865: 7 6 8 6 5 8 6 9
873: 6 5 9 3 2 1 7 4
881: 6 5 3 7 7 9 5 4
889: 7 3 6 2 6 8 5 6
897: 2 5 6 3 4 4 8 10
905: 7 7 6 8 9 35 55 13
913: 2 6 3 5 7 4 2 5
921: 7 8 5 8 4 2 3 4
92 9: 6 8 12 10 9 5 4 3
937: 6 3 5 2 4 4 5 3
945: 10 6 1 4 8 9 5 2
953: 5 4 5 7 5 1 3 1
961: 4 6 7 13 14 10 16 25
969: 25 10 3 7 7 3 8 3
977: 6 2 4 5 6 6 5 4
985: 3 6 6 2 7 3 6 2
993: 5 3 4 5 4 4 8 9
1001: 8 10 4 3 8 6 4 5
1009: 1 2 2 5 2 6 5 5
1017: 4 3 3 3 12 3 7 7
1025: 8 6 2 5 6 3 8 5
1033: 5 5 7 5 7 6 6 3
1041: 6 4 6 3 5 5 4 6
1049: 8 4 8 8 5 2 5 7
1057: 8 5 2 3 7 8 5 8
1065: 3 2 7 7 5 3 4 6
1073: 3 4 1 3 2 4 3 5
1081: 8 4 4 4 4 6 8 2
1089: 4 2 2 4 4 4 1 10
1097: 3 10 6 7 2 5 3 5
1105: 3 4 3 4 6 3 6 10
1113: 6 1 8 3 5 7 19 23
1121: 8 3 5 4 5 4 6 2
1129: 6 4 4 5 5 4 4 4
1137: 6 4 6 5 5 3 4 7
1145: 8 4 7 3 5 5 2 4
1153: 5 5 5 10 5 3 2 7
1161: 5 5 10 7 4 6 5 5
1169: 3 2 6 9 6 6 9 3
1177: 5 5 6 3 6 4 4 4
1185: 6 8 4 3 10 4 5 6
1193: 7 10 3 5 6 9 2 5
1201: 6 9 5 4 4 3 6 4
1209: 6 4 5 10 7 9 3 5
1217: 8 6 4 8 7 4 4 10
1225: 6 7 6 11 3 4 4 6
0250
Channel Data Report 4/17/2018 6:43:33 AM Page 4
1233: 5 3 8 10 20 12 2 1
Sample Title: AC-SED-11
Channell------l-------1-------1-------1-------I-------I-------I-------I
1241: 7 1 1 9 7 8 5 3
1249: 3 7 2 3 2 5 4 2
1257: 10 6 3 10 2 3 3 3
1265: 4 2 2 3 3 4 3 4
1273: 4 2 3 5 3 5 4 8
1281: 6 3 7 2 6 5 2 1
1289: 2 2 3 3 7 2 5 3
1297: 2 5 4 1 1 5 1 4
1305: 6 2 1 4 4 6 3 0
1313: 5 3 6 2 1 0 5 3
1321: 1 2 0 0 0 5 3 3
1329: 1 2 3 4 8 4 6 4
1337: 3 4 3 1 1 1 4 5
1345: 1 1 2 1 4 1 6 2
1353: 5 3 0 2 1 4 1 3
1361: 3 1 1 1 1 4 2 2
1369: 3 2 4 4 1 3 6 7
1377: 16 3 4 5 1 1 3 2
1385: 1 3 2 1 4 2 3 1
1393: 1 2 2 0 1 1 6 3
1401: 4 5 3 4 0 2 6 3
1409: 2 3 1 1 0 2 3 2
1417: 0 4 1 3 2 1 2 1
1425: 2 1 2 4 2 2 3 4
1433: 3 4 3 3 0 4 2 2
1441: 3 0 0 2 1 1 0 2
1449: 3 1 5 3 2 3 2 8
1457: 6 44 127 201 102 11 0 3
1465: 3 0 1 2 3 3 0 2
1473: 1 2 2 2 0 1 1 0
1481: 4 1 1 1 3 3 2 2
1489: 0 1 1 5 1 3 4 0
1497: 0 2 1 0 2 1 2 1
1505: 1 1 1 8 4 3 4 3
1513: 1 0 1 2 1 0 3 1
1521: 1 1 1 0 0 1 1 0
152 9: 0 2 2 1 4 1 3 1
1537: 2 1 5 2 1 2 2 0
1545: 1 3 2 1 1 0 0 3
1553: 1 1 1 0 2 0 1 2
1561: 1 1 0 2 0 0 0 1
1569: 0 1 2 0 1 2 1 3
1577: 0 1 3 2 3 1 3 2
1585: 1 3 6 3 3 1 3 1
1593: 0 0 1 2 4 1 1 0
1601: 1 0 1 1 0 0 2 2
1609: 0 0 1 0 2 1 0 1
1617: 1 2 3 3 2 1 1 1
1625: 0 3 0 2 2 2 2 1
1633: 0 0 1 0 2 2 5 1
1641: 0 1 2 0 2 0 1 0
164 9: 0 2 2 0 0 2 0 0
1657: 0 1 1 2 2 3 1 1
0251
Channel Data Report 4/17/2018 6:43:33 AM Page 5
1665: 0 0 0 2 0 2 0 0
Sample Title: AC-SED-11
Channell------l-------1-------1-------1-------I-------I-------I-------I
1673: 0 0 0 0 1 1 2 1
1681: 0 1 2 1 1 2 2 1
1689: 2 0 1 4 1 0 1 1
1697: 2 0 2 1 1 1 0 1
1705: 0 1 2 0 2 0 1 0
1713: 0 1 1 2 0 0 3 1
1721: 0 0 1 0 1 1 1 4
1729: 5 0 1 1 0 2 0 1
1737: 2 2 3 0 0 1 1 0
1745: 2 1 0 0 0 2 0 0
1753: 0 0 1 3 3 2 2 0
1761: 3 6 11 15 7 1 1 0
1769: 2 2 1 1 0 1 1 1
1777: 1 0 0 1 1 0 0 0
1785: 0 2 1 2 3 0 3 1
1793: 0 0 1 0 0 0 1 4
1801: 1 1 1 2 1 1 1 0
1809: 0 0 2 1 1 0 1 1
1817: 0 0 1 0 1 0 1 1
1825: 1 0 0 0 1 4 0 2
1833: 1 0 0 1 1 1 0 0
1841: 0 0 0 0 0 1 4 1
1849: 1 2 2 0 0 0 0 1
1857: 1 2 0 1 0 0 0 0
1865: 1 0 0 0 1 1 0 0
1873: 0 1 2 0 0 1 1 0
1881: 1 0 0 1 2 1 3 1
1889: 0 0 3 0 2 5 0 0
1897: 1 0 0 1 1 1 2 1
1905: 1 1 3 1 1 1 2 1
1913: 0 1 1 1 0 2 0 2
1921: 2 1 0 0 0 0 0 2
1929: 1 2 3 0 0 1 1 0
1937: 0 0 1 0 2 0 0 0
1945: 0 0 1 0 0 0 0 3
1953: 1 0 0 3 0 0 1 0
1961: 2 3 0 0 1 1 1 2
1969: 0 1 1 0 1 0 1 1
1977: 0 1 1 1 1 0 0 0
1985: 0 0 1 2 0 1 1 0
1993: 0 1 0 0 1 0 0 0
2001: 2 0 0 0 1 1 0 0
2009: 0 2 1 0 0 0 1 2
2017: 0 0 1 0 1 1 0 0
2025: 2 2 2 0 0 0 1 1
2033: 1 0 1 0 1 1 0 1
2041: 0 2 0 2 1 0 0 3
2049: 0 0 1 0 1 1 0 0
2057: 0 0 3 1 1 0 0 1
2065: 1 0 1 1 0 0 0 0
2073: 0 1 0 2 0 0 0 0
2081: 1 0 1 2 0 0 0 2
2089: 1 2 0 1 0 0 0 3
0252
Channel Data Report 4/17/2018 6:43:33 AM Page 6
2097: 1 1 2 3 0 2 3 1
Sample Title: AC-SED-11
Channell------l-------l-------1-------1-------1-------I-------I-------I
2105: 1 1 2 1 1 2 0 2
2113: 0 1 1 4 2 1 0 1
2121: 1 0 0 1 0 2 1 0
212 9: 0 0 1 0 2 0 0 0
2137: 0 2 1 1 1 0 0 1
2145: 0 0 1 1 1 1 1 0
2153: 0 0 1 3 2 1 1 1
2161: 0 0 0 2 2 0 1 1
2169: 2 0 1 0 0 0 1 1
2177: 1 1 1 0 2 0 0 2
2185: 1 0 0 0 0 2 0 0
2193: 0 1 0 0 0 0 0 4
2201: 3 5 7 4 1 1 0 0
2209: 0 1 0 0 1 1 0 0
2217: 2 0 0 1 2 0 2 1
2225: 0 1 1 0 0 0 2 1
2233: 1 0 0 1 1 2 0 0
2241: 0 3 2 2 1 1 1 0
2249: 0 1 2 1 1 1 1 1
2257: 0 0 2 0 1 0 0 1
2265: 0 1 0 0 1 0 0 1
2273: 0 0 1 0 1 0 0 1
2281: 0 2 1 1 3 0 0 0
2289: 1 0 0 0 0 2 2 1
2297: 0 1 0 2 2 0 0 1
2305: 0 1 1 0 0 0 1 2
2313: 2 0 1 1 3 0 1 2
2321: 0 0 0 2 1 1 1 0
2329: 0 1 0 0 1 2 0 1
2337: 1 1 1 0 0 0 1 1
2345: 2 2 0 1 0 1 0 0
2353: 1 1 0 0 0 0 0 0
2361: 0 1 2 3 0 3 1 1
2369: 0 1 1 1 0 1 2 1
2377: 0 1 1 0 0 0 1 0
2385: 0 0 0 1 0 0 1 1
2393: 1 1 2 0 0 0 3 0
2401: 0 0 0 0 0 0 0 0
2409: 0 0 0 1 0 0 0 2
2417: 0 0 1 1 0 0 0 0
2425: 2 0 1 0 0 0 3 3
2433: 0 2 1 0 0 0 1 1
2441: 1 0 2 0 2 0 0 1
2449: 0 1 0 0 0 0 1 0
2457: 0 1 0 0 1 1 1 0
2465: 1 0 1 1 0 0 0 0
2473: 0 0 0 3 0 0 0 1
2481: 1 0 0 0 0 1 0 0
2489: 1 0 0 0 1 1 2 0
2497: 1 1 2 1 0 0 0 0
2505: 0 0 0 0 0 0 0 1
2513: 1 0 2 1 0 1 0 0
2521: 0 0 0 0 0 1 0 0
0253
Channel Data Report 4/17/2018 6:43:33 AM Page 7
2529: 0 1 0 2 0 1 0 0
Sample Title: AC-SED-11
Channell------l-------l-------l-------1-------1-------l-------1-------I
2537: 0 0 1 0 1 0 0 0
2545: 0 0 0 1 0 1 0 2
2553: 0 0 0 1 1 0 0 0
2561: 0 0 0 0 1 1 0 2
2569: 0 0 1 0 1 1 1 1
2577: 0 2 0 0 0 0 0 0
2585: 0 1 0 0 0 1 0 1
2593: 0 1 0 1 0 0 1 0
2601: 1 1 1 0 0 0 0 1
2609: 2 5 6 11 17 6 5 2
2617: 0 0 1 0 2 0 0 1
2625: 0 0 0 1 1 1 0 0
2633: 0 0 0 0 0 0 0 0
2641: 1 1 0 0 0 0 0 1
2649: 0 0 0 0 0 0 1 0
2657: 0 0 0 0 0 0 0 0
2665: 0 0 0 0 0 0 0 0
2673: 3 0 0 0 1 0 1 0
2681: 1 0 0 1 0 2 0 0
2 68 9: 1 0 0 0 0 1 0 0
2697: 1 0 0 0 0 0 0 1
2705: 0 0 0 1 0 1 0 0
2713: 0 0 0 1 1 1 0 1
2721: 0 0 0 0 0 0 0 0
2729: 0 0 1 0 0 0 0 0
2737: 0 0 0 0 0 0 0 1
2745: 0 0 0 0 0 0 0 0
2753: 0 0 1 1 0 0 1 0
2761: 0 0 0 0 0 0 0 0
2769: 0 0 0 0 2 0 0 0
2777: 0 0 0 0 1 0 0 1
2785: 1 1 0 0 0 1 0 0
2793: 0 1 2 1 1 1 0 1
2801: 0 0 0 0 0 0 1 0
2809: 0 0 1 0 0 0 0 0
2817: 0 0 0 0 1 0 1 0
2825: 0 0 0 0 0 0 0 0
2833: 0 0 2 0 0 0 0 0
2841: 0 0 0 0 0 0 0 0
2849: 0 0 0 0 0 1 0 0
2857: 0 0 0 0 0 0 1 1
2865: 0 0 1 1 0 0 0 0
2873: 0 0 0 0 0 0 0 0
2881: 1 1 0 2 0 0 0 1
2889: 0 0 0 0 0 0 0 0
2897: 0 0 0 1 0 0 0 0
2905: 0 0 0 0 0 0 2 0
2913: 0 0 0 0 0 2 0 0
2921: 1 1 0 0 0 0 0 0
2929: 0 0 0 0 1 1 0 0
2937: 0 0 0 0 0 0 0 0
2945: 1 0 1 0 0 0 0 0
2953: 0 0 1 0 1 0 0 1
0254
Channel Data Report 4/17/2018 6:43:33 AM Page 8
2961: 0 0 0 0 0 0 0 1
Sample Title: AC-SED-11
Channell------l-------l-------l-------1-------1-------1-------I-------I
2969: 0 0 0 1 0 0 0 0
2977: 0 0 1 1 1 0 0 0
2985: 0 0 0 0 0 0 0 0
2993: 1 0 0 0 0 0 1 0
3001: 0 0 0 0 0 0 1 1
3009: 0 0 0 0 0 1 0 0
3017: 0 0 0 0 0 0 0 1
3025: 0 0 0 0 0 0 0 2
3033: 0 0 0 0 1 2 0 0
3041: 1 1 0 1 0 0 0 0
3049: 0 0 0 0 0 0 0 0
3057: 0 0 1 0 0 0 0 0
3065: 0 0 0 0 1 0 0 0
3073: 0 0 0 0 1 0 0 0
3081: 0 0 0 0 0 0 0 1
3089: 0 0 0 0 0 0 1 0
3097: 0 0 0 0 0 1 0 0
3105: 1 0 0 0 0 0 1 0
3113: 0 0 0 0 0 2 0 0
3121: 0 0 0 1 0 0 0 0
3129: 1 0 0 0 0 0 1 0
3137: 0 0 0 1 0 0 0 0
3145: 0 0 0 0 0 0 0 1
3153: 0 1 0 1 0 0 1 0
3161: 0 0 0 0 0 0 2 0
3169: 0 0 1 0 0 0 0 0
3177: 0 0 0 0 0 0 0 0
3185: 0 0 0 0 0 1 1 0
3193: 0 0 0 0 0 3 0 0
3201: 0 0 0 0 0 0 0 0
3209: 0 0 1 0 0 0 1 0
3217: 0 0 0 0 0 0 0 2
3225: 0 0 0 0 1 0 0 0
3233: 0 0 0 0 0 0 0 0
3241: 0 0 1 0 0 0 2 0
3249: 0 1 0 1 0 0 0 0
3257: 0 0 0 0 0 0 0 0
32 65: 0 0 0 0 1 0 0 0
3273: 0 0 0 0 1 0 1 0
3281: 0 0 0 0 0 1 0 0
3289: 0 0 1 0 0 0 0 0
3297: 0 0 0 0 0 0 0 0
3305: 0 0 1 0 0 3 0 0
3313: 0 0 1 1 0 0 0 0
3321: 0 0 1 0 0 0 0 0
3329: 0 0 0 0 1 0 0 0
3337: 0 0 0 0 0 0 0 1
3345: 0 0 0 0 0 0 0 1
3353: 0 0 1 0 1 0 0 0
3361: 0 0 0 0 0 1 0 0
3369: 0 0 0 0 1 0 0 0
3377: 0 0 0 0 0 1 0 1
3385: 0 0 0 0 0 0 0 0
0255
Channel Data Report 4/17/2018 6:43:33 AM Page 9
3393: 0 0 0 1 0 1 0 0
Sample Title: AC-SED-11
Channell------l-------1-------1-------1-------I-------I-------I-------I
3401: 0 0 0 0 0 0 1 0
3409: 1 0 0 0 0 0 1 1
3417: 0 0 1 0 0 0 0 0
3425: 0 0 0 0 0 1 0 0
3433: 1 0 0 0 0 0 0 0
3441: 0 0 0 0 0 0 0 0
3449: 0 0 0 0 0 0 0 0
3457: 1 0 0 0 0 0 0 0
3465: 0 0 0 1 0 1 0 0
3473: 0 0 0 0 0 0 0 0
3481: 0 0 0 0 0 0 0 1
3489: 0 0 0 0 1 0 1 1
3497: 0 0 0 0 0 0 1 0
3505: 0 0 0 0 0 0 0 0
3513: 0 0 0 1 0 0 1 1
3521: 0 0 0 0 1 0 0 0
3529: 0 1 0 0 1 0 0 0
3537: 0 0 0 0 0 0 0 0
3545: 0 0 0 0 0 0 0 0
3553: 0 0 0 0 0 0 0 0
3561: 0 0 0 1 0 1 0 0
3569: 0 0 0 0 1 0 1 0
3577: 1 0 0 0 0 0 0 0
3585: 0 0 0 0 0 0 0 0
3593: 0 0 0 0 0 0 0 0
3601: 0 0 0 0 0 0 0 0
3609: 0 0 2 0 0 0 0 0
3617: 0 0 0 1 0 0 1 0
3625: 0 0 0 0 0 1 0 0
3633: 0 0 0 0 1 0 0 0
3641: 1 0 0 0 0 0 1 1
3649: 0 0 0 0 0 1 0 1
3657: 0 0 0 0 0 1 0 0
3665: 0 0 0 0 0 0 0 0
3673: 0 0 0 0 0 0 1 0
3681: 0 1 0 0 1 0 0 0
3689: 0 0 0 1 0 0 0 0
3697: 0 0 0 1 0 0 0 0
3705: 1 0 1 0 1 0 0 0
3713: 0 0 0 0 0 0 1 0
3721: 0 0 0 0 1 1 0 0
372 9: 0 0 0 0 0 0 0 0
3737: 1 0 0 0 0 1 0 0
3745: 0 0 0 0 0 0 0 0
3753: 1 0 0 0 0 0 0 0
3761: 0 0 0 0 0 0 0 0
3769: 0 0 0 0 0 0 0 0
3777: 0 0 0 0 0 0 1 0
3785: 0 0 0 0 0 0 0 0
3793: 0 0 0 0 0 0 0 1
3801: 0 0 0 0 1 0 0 0
3809: 0 0 0 1 0 0 0 1
3817: 0 0 0 0 0 0 0 0
0256
Channel Data Report 4/17/2018 6:43:33 AM Page 10
3825: 0 0 0 0 0 0 0 1
Sample Title: AC-SED-11
Channell------l-------l-------l-------l-------1-------1-------1-------I
3833: 0 0 0 0 0 0 1 0
3841: 0 0 0 1 0 0 0 0
3849: 0 0 0 0 0 0 0 0
3857: 0 0 0 0 0 0 0 0
3865: 0 0 0 0 0 0 0 0
3873: 0 0 0 0 0 0 0 0
3881: 0 1 0 0 0 0 0 0
3889: 1 0 0 0 0 1 0 0
3897: 0 0 0 0 0 0 0 0
3905: 0 0 0 0 0 0 0 0
3913: 0 0 0 0 0 0 1 0
3921: 0 1 0 1 0 0 0 0
3929: 0 0 0 0 1 0 0 0
3937: 0 0 0 0 0 0 0 0
3945: 0 0 0 0 1 0 0 0
3953: 1 0 0 0 0 0 0 1
3961: 0 0 0 0 0 0 0 0
3969: 0 0 0 0 0 0 0 0
3977: 0 0 1 0 0 0 0 0
3985: 0 0 0 1 0 0 0 1
3993: 0 1 0 0 0 0 0 0
4001: 0 0 0 0 0 0 0 0
4009: 0 0 0 0 1 0 0 0
4017: 0 0 0 1 0 1 0 0
4025: 0 0 0 0 1 0 1 0
4033: 0 0 0 0 0 0 0 2
4041: 0 0 1 0 0 0 0 0
4049: 2 0 0 0 0 0 0 0
4057: 0 0 0 0 0 0 1 0
4065: 0 0 0 0 0 0 0 0
4073: 0 0 0 0 0 0 0 0
4081: 0 0 0 0 0 0 0 0
4089: 1 0 0 0 0 0 0 0
0257
lQS
104
aJ 103 ,-
"" ro .--< u ~ ' V) = ~ o,_
.--< O'I ' 0 =
I o,_
~ r ~ .J-' C> I ~ ci:l i
~ 1Q2 fu r ¥~ 11
101
"" .--<
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=
00
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00
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00
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!
0000064639.CNF
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r
00 G>
1
Live Time :3600.000 sec Real Ti me : 3600. 820 sec Start: 1: l.2(kev) Stop : 4096: 4099. 2 (kev) Acq. Start :Tue Apr 17 05 :42: 57 2018
lQ0111u11 ' 1 ' 11 F 111 1' P! 11 '11 ""! 1• II lrnjll,ll'""'""''''l!ll"'j,lllffi111illllll'ftl111Mllllllllillll/llll/llrnllllllllllqrn11n111m1 !//111/W 111,111rn111 I I ii I I I 1111
500 1000 1500 2000 channel
2500 3000 3500 4000
~ ROI Type: 1 ROI Type: 2
0258
4/17/2018 7:44:46AM
Analysis Report for 1803111-04
AC-SED-11
GAMMA SPECTRUM ANALYSIS
Sample Identification
Sample Description
Sample Type
Sample Size
Facility
Sample Taken On
Acquisition Started
Procedure
Operator Detector Name
Geometry Live Time
Real Time
Dead Time
Peak Locate Threshold
Peak Locate Range (in channels)
Peak Area Range (in channels)
Identification Energy Tolerance
Energy Calibration Used Done On
Efficiency Calibration Used Done On
Efficiency Calibration Description
Sample Number
: 1803111-04
: AC-SED-11
: SOIL
: 4.763E+02 grams
: Countroom
: 3/21/2018 9:15:45AM
: 4/17/2018 6:44:34AM
: GAS-1602 pCi
: Administrator
: GE2 : GAS-1602
: 3600.0 seconds
: 3600.8 seconds
: 0.02 %
: 2.50
: 1 - 4096
: 28 - 4096
: 1.000 keV
: 2/17/2018 : 2/17/2018
: 64641
PEAK-TO-TOTAL CALIBRATION REPORT
Peak-to-Total Efficiency Calibration Equation
Page 1 of29
v{P l//l 7/Jf3
0259
4/17/2018 7 :44 :46AM
Analysis Report for 1803111-04
AC-SED-11
PEAK LOCATE REPORT
Peak No.
1 2 3 4 5 6 7 8 9
10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak Search Sensitivity
Energy (keV)
47.12 63.71 76.81 87.06 92.98
186.24 239.51 269.77 295.30 300.11 328.20 339.04 352.16 384.90 427.01 462.09 477.47 480.28 511.37 583.48 609.42 661.89 665.38 727.24 767.85 794.18 860.05 883.58 911.18 925.35 965. 2 9 969. 0 9
1078.18 1082.18 1120.57 1238.93 1262.15 1334. 92 1460.72 1560.68 1582.32 1587.31
: 4/17/2018 7:44:38AM
: 1 : 4096 : 2.50
Centroid Channel
46.90 63.48 76.58 86.82 92.74
185.95 239.19 269.45 294.97 299.76 327.85 338.68 351.79 384.51 426.60 461.67 477.04 479.84 510.92 582.99 608.92 661.36 664.85 726.68 767.27 793.58 859.41 882.93 910.51 924.67 964.60 968.39
1077.42 1081.42 1119.78 1238.07 1261.28 1334.00 1459. 72 1559.61 1581.24 1586.22
Centroid Uncertainty
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Page 2 of29
Peak Significance
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0260
Analysis Report for 1803111-04
AC-SED-11
Peak No. Energy (keV)
43 1590.31 44 1593.00 45 1764.32 46 1848.86 47 1873.12 48 1939.70 49 2086.60 50 2146.73 51 2614.03
? = Adjacent peak noted
Errors quoted at 2.000sigma
Centroid Channel
1589.23 1591.91 1763.11 1847.60 1871.84 1938.38 2085.17 2145.25 2612.18
4/17/2018 7:44:46AM
Centroid Uncertainty
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Page 3 of 29
Peak Significance
0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
0261
4/17/2018 7:44:46AM Page 4 of29
Analysis Report for 1803111-04
AC-SED-11
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/17/2018 7:44:38AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI ROI Peak Net Peak Net Area Continuum FWHM
No. (keV) start end Centroid Area Uncertainty Counts (keV)
1 47.12 43 - 50 46.90 1.17E+02 73.24 8.16E+02 1. 21
2 63.71 61 - 65 63.48 7.41E+0l 59.28 7.12E+02 1. 51
3 76.81 72 - 82 76.58 7.49E+02 125.00 1.66E+03 3.49
4 87.06 83 - 89 86.82 1.33E+02 81.26 1.11E+03 1. 69
5 92.98 90 - 96 92.74 2.12E+02 79.17 9.46E+02 1. 68
6 186.24 183 - 189 185.95 1.41E+02 59.66 5.43E+02 1.17
7 239.51 234 - 243 239.19 6.69E+02 85.20 6.54E+02 1. 76
8 269.77 266 - 273 269.45 5.70E+0l 50.83 3.94E+02 1. 89
M 9 295.30 2 91 - 303 294.97 2.54E+02 44.30 1.99E+02 1. 73
m 10 300.11 2 91 - 303 299.76 3.17E+0l 37.03 2. 72E+02 1. 85
11 328.20 326 - 331 327.85 3.79E+0l 34.66 2.14E+02 1. 81
12 339.04 334 - 343 338.68 1.14E+02 54.03 3.43E+02 1. 59
13 352.16 348 - 354 351.79 3.05E+02 50.69 2.45E+02 1. 46
14 384.90 382 - 388 384.51 2.72E+0l 32.50 1.74E+02 3.87
15 427.01 424 - 430 426.60 2.32E+0l 27.58 1.20E+02 2.20
16 462.09 457 - 4 67 461.67 7.30E+0l 42.15 1.98E+02 1.85
M 17 477.47 4 72 - 483 477.04 3.89E+0l 23.63 8.66E+0l 1. 72
m 18 480.28 472 - 483 479.84 1.62E+0l 24.05 7.50E+0l 1. 72
19 511.37 506 - 517 510.92 1.42E+02 49.36 2.31E+02 2.73
20 583.48 57 8 - 587 582.99 1.71E+02 42.43 1.58E+02 1. 50
21 609.42 605 - 611 608.92 2.79E+02 43.47 1.42E+02 1. 50
M 22 661.89 657 - 667 661.36 2.92E+0l 21.21 5.56E+0l 2.07
m 23 665.38 657 - 667 664.85 2.16E+0l 20.64 5.03E+0l 2.07
24 727.24 7 24 - 730 72 6. 68 3.41E+0l 24.70 8.38E+0l 3.03
25 767.85 7 64 - 770 767.27 2.81E+01 26.30 1.06E+02 1. 21
26 794.18 7 91 - 798 793.58 2.60E+0l 26.23 1.00E+02 3.56
27 860.05 85 6 - 863 859.41 l.84E+0l 23.58 8.12E+0l 1. 94
28 883.58 87 9 - 886 882.93 1.68E+0l 21.73 6.65E+0l 3.40
29 911.18 90 6 - 915 910.51 1. 11E+02 31.10 7.32E+0l 2.06
30 925.35 919 - 930 924.67 2.97E+0l 28.14 8.45E+0l 7.97
M 31 965. 2 9 962 - 974 964. 60 1.46E+0l 17.18 5.76E+0l 2.32
m 32 969.09 962 - 974 968.39 6.48E+0l 26.86 7.19E+0l 2.32
M 33 1078.18 107 6 - 1089 1077.42 1.15E+0l 6.93 1.02E+0l 1. 96
m 34 1082.18 107 6 - 1089 1081.42 1.54E+0l 17.52 4.09E+0l 2.40
35 1120.57 1115 - 1124 1119.78 5.27E+0l 29.58 9.47E+0l 1. 88
36 1238.93 1232 - 1244 1238.07 4.85E+0l 30.15 8.31E+0l 3.08
37 1262.15 1259 - 1263 1261.28 1.06E+0l 9. 96 1.28E+0l 1. 77
38 1334.92 1328 - 1343 1334.00 3.70E+0l 21.63 3.20E+0l 5.00
39 1460.72 1453 - 1464 1459.72 4.82E+02 48.58 5.46E+0l 2.75
40 1560.68 1555 - 1563 1559.61 8.50E+00 9.62 9.00E+00 2.78
0262
M m m
Analysis Report for 1803111-04
AC-SED-11
Peak Energy ROI
No. (keV) start
41 1582.32 157 9 -42 1587.31 1584 -43 1590.31 1584 -44 1593.00 1584 -45 1764.32 1758 -46 1848.86 184 4 -47 1873.12 1868 -48 1939.70 1934 -49 2086.60 2083 -so 2146.73 2142 -51 2614.03 2 607 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Peak
end Centroid
1584 1581.24 1595 1586.22 1595 1589.23 1595 1591.91 1768 1763.11 1852 1847.60 1875 1871.84 1941 1938.38 2087 2085.17 2147 2145.25 2 616 2612.18
4/17/2018 7:44:46AM Page 5 of29
Net Peak Net Area Continuum FWHM Area Uncertainty Counts (keV)
9.00E+OO 7.87 4.00E+OO 1. so 1.31E+Ol 7.37 4.lSE+OO 2.48
1.lOE+Ol 11. so 3.39E+OO 2.48
1.40E+Ol 10.21 1.91E+OO 2.48
4.56E+Ol 17.51 1.68E+Ol 2.29
1.32E+Ol 8. 96 3.53E+OO 3.46
9.18E+OO 7.75 3.64E+OO 3.10
8.00E+OO 5.66 O.OOE+OO 1. 98
6.00E+OO 4.90 O.OOE+OO 2.74
4.42E+OO 5.74 3.17E+OO 2.57
7.60E+Ol 17.44 O.OOE+OO 3.20
PEAK ANALYSIS REPORT
Peak Analysis Performed on : 4/17/2018 7:44:38AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Peak Energy ROI ROI Net Peak Net Area Continuum Critical
No. (keV) start end Area Uncertainty Counts Level
1 47.12 43 - so 1.17E+02 73.24 8.16E+02 S.7SE+Ol
2 63.71 61 - 65 7.41E+Ol 59.28 7.12E+02 4.66E+Ol
3 76.81 72 - 82 7.49E+02 125.00 1.66E+03 9.24E+Ol
4 87.06 83 - 89 1.33E+02 81.26 1.11E+03 6.40E+Ol
s 92.98 90 - 96 2.12E+02 79.17 9.46E+02 6.0SE+Ol
6 186.24 183 - 189 1.41E+02 59.66 S.43E+02 4.SOE+Ol
7 239.51 234 - 243 6.69E+02 85.20 6.54E+02 S.56E+Ol
8 269.77 266 - 273 S.70E+Ol 50.83 3.94E+02 3.99E+Ol
M 9 295.30 291 - 303 2.54E+02 44.30 1.99E+02 2.32E+Ol
m 10 300.11 291 - 303 3.17E+Ol 37.03 2. 72E+02 2.71E+Ol
11 328.20 326 - 331 3.79E+Ol 34.66 2. 14E+02 2.66E+Ol
12 339.04 334 - 343 1. 14E+02 54.03 3.43E+02 4.08E+Ol
13 352.16 34 8 - 354 3.0SE+02 50.69 2.4SE+02 3.02E+Ol
14 384.90 382 - 388 2. 72E+Ol 32.50 1.74E+02 2.53E+Ol
15 427.01 424 - 430 2.32E+Ol 27.58 1.20E+02 2.12E+Ol
16 462.09 457 - 467 7. 30E+Ol 42.15 1. 98E+02 3.17E+Ol
M 17 477.47 4 7 2 - 483 3.89E+Ol 23.63 8.66E+Ol 1.53E+Ol
0263
Analysis Report for 1803111-04
m
M m
M
m M
m
M
m m
AC-SED-11
Peak Energy ROI
No. (keV) start
18 480.28 472 -
19 511.37 506 -
20 583.48 57 8 -
21 609.42 605 -
22 661.89 657 -
23 665.38 657 -
24 727.24 724 -
25 767.85 7 64 -
26 794.18 7 91 -
27 860.05 856 -
28 883.58 87 9 -
29 911.18 906 -
30 925.35 919 -
31 965. 29 962 -
32 969.09 962 -
33 1078.18 107 6 -
34 1082.18 107 6 -
35 1120.57 1115 -
36 1238.93 1232 -
37 1262.15 1259 -
38 1334.92 1328 -
39 1460.72 1453 -
40 1560.68 1555 -
41 1582.32 157 9 -
42 1587.31 1584 -
43 1590.31 1584 -
44 1593.00 1584 -
45 1764.32 1758 -
46 1848.86 1844 -
47 1873.12 18 68 -
48 1939.70 1934 -
49 2086.60 2083 -
50 2146.73 2142 -
51 2614.03 2 607 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 7:44:46AM Page 6 of 29
ROI Net Peak Net Area Continuum Critical
end Area Uncertainty Counts Level
483 1.62E+0l 24.05 7.50E+0l 1.42E+0l
517 1.42E+02 49.36 2.31E+02 1.93E+0l
587 1.71E+02 42.43 1.58E+02 2.75E+0l
611 2.79E+02 43.47 1.42E+02 2.29E+0l
667 2.92E+0l 21. 21 5.56E+0l 1.23E+0l
667 2.16E+0l 20.64 5.03E+0l 1.17E+0l
730 3.41E+0l 24.70 8.38E+0l 1.79E+0l
770 2.81E+0l 26.30 1.06E+02 1.98E+0l
798 2.60E+0l 26.23 1.00E+02 1.99E+0l
863 1.84E+0l 23.58 8.12E+0l 1.81E+0l
886 1.68E+0l 21.73 6.65E+0l 1.65E+0l
915 1. 11E+02 31.10 7.32E+0l 1.88E+0l
930 2.97E+0l 28.14 8.45E+0l 2. 13E+0l
974 l.46E+0l 17.18 5.76E+0l 1.25E+0l
97 4 6.48E+0l 26.86 7.19E+0l 1.39E+0l
1089 1.15E+0l 6.93 1.02E+0l 5.26E+00
1089 1.54E+0l 17.52 4.09E+0l 1.05E+0l
1124 5.27E+0l 29.58 9.47E+0l 2.12E+0l
1244 4.85E+0l 30.15 8.31E+0l 2.20E+0l
1263 1.06E+0l 9. 96 1.28E+0l 6.19E+00
1343 3.70E+0l 21.63 3.20E+0l 1.47E+0l
1464 4.82E+02 48.58 5.46E+0l 1.71E+0l
1563 8.50E+00 9.62 9.00E+00 6.29E+00
1584 9.00E+00 7.87 4.00E+00 4.19E+00
1595 1.31E+0l 7.37 4.15E+00 3.35E+00
1595 1.l0E+0l 11. 50 3.39E+00 3.03E+00
1595 1.40E+0l 10.21 1.91E+00 2.27E+00
1768 4.56E+0l 17.51 1.68E+0l 9.16E+00
1852 1.32E+0l 8. 96 3.53E+00 4.30E+00
1875 9.18E+00 7.75 3.64E+00 3.97E+00
1941 8.00E+00 5.66 0.00E+00 0.00E+00
2087 6.00E+00 4.90 0.00E+00 0.00E+00
2147 4.42E+00 5.74 3.17E+00 3.22E+00
2616 7.60E+0l 17.44 0.00E+00 0.00E+00
0264
4/17/2018 7:44:46AM
Analysis Report for 1803111-04
M m
M
m
M m
M m
AC-SED-11
PEAK WITH N/0 REPORT
Peak Analysis Performed on : 4/17/2018 7:44:38AM
Peak Analysis From Channel : 1
Peak Analysis To Channel : 4096
Tentative NID Library
Peak Match Tolerance
Peak Energy
No. (keV)
1 47.12 2 63.71
3 76.81 4 87.06
5 92.98 6 186.24 7 239.51 8 269.77 9 295.30
10 300.11
11 328.20 12 339.04 13 352.16 14 384.90 15 427.01 16 462.09 17 477.47
18 480.28 19 511.37 20 583.48 21 609.42 22 661.89 23 665.38
24 727.24 25 767.85 26 794.18 27 860.05 28 883.58 29 911.18
30 925.35 31 965. 2 9 32 969.09
: \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
: 1.000 keV
ROI ROI Peak Net Peak
start end Centroid Area
43 - 50 46.90 1.17E+02 61 - 65 63.48 7.41E+0l
72 - 82 76.58 7.49E+02 83 - 89 86.82 1.33E+02
90 - 96 92.74 2.12E+02
183 - 189 185.95 1.41E+02
234 - 243 239.19 6.69E+02 266 - 273 269.45 5.70E+0l
291 - 303 294.97 2.54E+02
2 91 - 303 299.76 3.17E+0l
326 - 331 327.85 3.79E+0l
334 - 343 338.68 1.14E+02 348 - 354 351.79 3.05E+02 382 - 388 384.51 2.72E+0l 424 - 430 426.60 2.32E+0l
457 - 4 67 461.67 7.30E+0l 4 72 - 483 477.04 3.89E+0l
4 72 - 483 479.84 l.62E+0l
50 6 - 517 510.92 1.42E+02
578 - 587 582.99 1.71E+02
605 - 611 608.92 2.79E+02
657 - 667 661.36 2.92E+0l
657 - 667 664.85 2.16E+0l
724 - 730 726.68 3.41E+0l
7 64 - 770 767.27 2.81E+0l
791 - 798 793.58 2.60E+0l
856 - 863 859.41 1.84E+0l
87 9 - 886 882.93 1.68E+0l
906 - 915 910.51 1. 11E+02
919 - 930 924.67 2.97E+0l
962 - 974 964. 60 1.46E+0l
962 - 974 968.39 6.48E+0l
Net Area Uncertainty
73.24 59.28
125.00 81.26
79.17 59.66 85.20 50.83 44.30 37.03
34.66 54.03 50.69 32.50 27.58 42.15 23.63
24.05 49.36 42.43 43.47 21. 21 20.64
24.70 26.30 26.23 23.58 21. 73 31.10
28.14 17.18 26.86
Page 7 of29
Continuum Tentative Counts Nuclide
8.16E+02 PB-210 7.12E+02 TH-234
TH-230 1.66E+03 1. 11E+03 SN-126
NP-237 EU-155 CD-109
9.46E+02 GA-67 5.43E+02 RA-226 6.54E+02 PB-212 3.94E+02 l.99E+02 PB-214 2. 72E+02 PB-212
BI-210M GA-67
2.14E+02 LA-140 3.43E+02 AC-228 2.45E+02 PB-214 1.74E+02 1.20E+02 SB-125 1.98E+02 8.66E+0l BE-7
PM-144 7.50E+0l 2.31E+02 1.58E+02 TL-208 1.42E+02 BI-214 5.56E+0l CS-137 5.03E+0l CE-143
SB-126 8.38E+0l BI-212 1.06E+02 1.00E+02 ..... '
8.12E+0l TL-208 6.65E+0l 7.32E+0l AC-228
TL-204 8.45E+0l 5.76E+0l 7.19E+0l AC-228
0265
4/17/2018 7:44:46AM
Analysis Report for 1803111-04
M m
M m m
M
AC-SED-11
Peak Energy ROI
No. (keV) start
33 1078.18 107 6 -34 1082.18 1076 -35 1120.57 1115 -
36 1238.93 1232 -37 1262.15 1259 -38 1334.92 1328 -39 1460.72 1453 -40 1560.68 1555 -41 1582.32 157 9 -42 1587.31 1584 -43 1590.31 1584 -44 1593.00 1584 -45 1764.32 1758 -46 1848.86 184 4 -47 1873.12 18 68 -48 1939.70 1934 -49 2086.60 2083 -50 2146.73 2142 -51 2614.03 2607 -
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
ROI Peak Net Peak Net Area
end Centroid Area Uncertainty
1089 1077,42 1.15E+0l 6.93
1089 1081.42 1.54E+0l 17.52
1124 1119.78 5.27E+0l 29.58
1244 1238.07 4.85E+0l 30.15
1263 1261.28 1.06E+0l 9. 96
1343 1334.00 3.70E+0l 21.63
14 64 1459.72 4.82E+02 48.58
1563 1559.61 8.50E+00 9.62
1584 1581.24 9.00E+00 7.87
1595 1586.22 1.31E+0l 7.37
1595 1589.23 1.l0E+0l 11. 50
1595 1591.91 1.40E+0l 10.21
1768 1763.11 4.56E+0l 17.51
1852 1847.60 1.32E+0l 8. 96
1875 1871.84 9.18E+00 7.75
1941 1938.38 8.00E+00 5.66
2087 2085.17 6.00E+00 4.90
2147 2145.25 4.42E+00 5.74
2616 2612.18 7.60E+0l 17.44
PEAK EFFICIENCY REPORT
Peak Analysis Performed on : 4/17/2018 7:44:38AM
Peak Energy Net Peak Net Area Peak
No. (keV) Area Uncertainty Efficiency
1 47.12 l.17E+02 73.24 1.62E-02
2 63. 71 7.41E+0l 59.28 2.15E-02
3 76.81 7.49E+02 125.00 2.33E-02
4 87.06 1.33E+02 81.26 2.39E-02
5 92.98 2.12E+02 79 .17 2.40E-02
6 186.24 1.41E+02 59.66 1.95E-02
7 239.51 6.69E+02 85.20 1.68E-02
8 269.77 5.70E+0l 50.83 1.55E-02
9 295.30 2.54E+02 44.30 l,46E-02
Page 8 of29
Continuum Tentative Counts Nuclide
1.02E+0l 4.09E+0l 9.47E+0l SC-46
BI-214 TA-182
8.31E+0l CO-56 l.28E+0l 3.20E+0l 5.46E+0l K-40 9.00E+00 4.00E+00 4.15E+00 3.39E+00 1.91E+00 1.68E+0l BI-214 3.53E+00 3.64E+00 0.00E+00 0.00E+00 3.17E+00 0.00E+00 TL-208
Efficiency Uncertainty
1.53E-03 1.62E-03 1.89E-03 2.l0E-03 2.l0E-03 2.44E-03 2.41E-03 2.40E-03 2.38E-03
0266
4/17/2018 7:44:46AM Page 9 of29
Analysis Report for 1803111-04
AC-SED-11
Peak Energy Net Peak Net Area Peak Efficiency
No. (keV) Area Uncertainty Efficiency Uncertainty
m 10 300. 11 3.17E+01 37.03 1.44E-02 2.38E-03
11 328.20 3.79E+0l 34.66 l.35E-02 2.36E-03
12 339.04 l.14E+02 54.03 1.32E-02 2.36E-03
13 352.16 3.05E+02 50.69 1.28E-02 2.35E-03
14 384.90 2. 72E+0l 32.50 1.19E-02 2.33E-03
15 427.01 2.32E+0l 27.58 1.l0E-02 2.12E-03
16 462.09 7.30E+0l 42.15 1.03E-02 1.92E-03
M 17 477.47 3.89E+0l 23.63 1.0lE-02 1.83E-03
m 18 480.28 1.62E+0l 24.05 l.00E-02 1.81E-03
19 511. 37 1.42E+02 49.36 9.51E-03 1.63E-03
20 583.48 1.71E+02 42.43 8.53E-03 1. 22E-03
21 609.42 2.79E+02 43.47 8.22E-03 1.07E-03
M 22 661.89 2.92E+0l 21. 21 7.68E-03 7.67E-04
m 23 665.38 2.16E+0l 20.64 7.64E-03 7.74E-04
24 727.24 3.41E+0l 24.70 7.l0E-03 8.92E-04
25 767.85 2.81E+0l 26.30 6.78E-03 9.70E-04
26 794.18 2.60E+0l 26.23 6.60E-03 l.02E-03
27 860.05 1.84E+0l 23.58 6.18E-03 l.15E-03
28 883.58 1.68E+0l 21.73 6.04E-03 1.19E-03
29 911.18 1.11E+02 31.10 5.89E-03 l.18E-03
30 925.35 2.97E+0l 28.14 5.82E-03 1.14E-03
M 31 965. 2 9 1.46E+0l 17.18 5.63E-03 l.02E-03
m 32 969.09 6.48E+0l 26.86 5.61E-03 1.0lE-03
M 33 1078.18 l.15E+0l 6.93 5.16E-03 6.98E-04
m 34 1082.18 1.54E+0l 17.52 5.14E-03 6.87E-04
35 1120.57 5.27E+0l 29.58 5.0lE-03 5.76E-04
36 1238.93 4.85E+0l 30.15 4.65E-03 4.00E-04
37 1262.15 l.06E+0l 9. 96 4.59E-03 3.91E-04
38 1334. 92 3.70E+0l 21.63 4.42E-03 3.65E-04
39 1460.72 4.82E+02 48.58 4.16E-03 3.80E-04
40 1560.68 8.50E+00 9.62 4.00E-03 3.92E-04
41 1582.32 9.00E+00 7.87 3.97E-03 3.95E-04
M 42 1587.31 1.31E+0l 7.37 3.96E-03 3.95E-04
m 43 1590.31 l.l0E+0l 11. 50 3.95E-03 3.96E-04
m 44 1593.00 1.40E+0l 10. 21 3.95E-03 3. 96E-04
45 1764.32 4.56E+0l 17.51 3.74E-03 4.16E-04
46 1848.86 1.32E+0l 8. 96 3.66E-03 4.25E-04
47 1873.12 9.18E+00 7.75 3.64E-03 4.25E-04
48 1939.70 8.00E+00 5.66 3.59E-03 4.25E-04
49 2086.60 6.00E+00 4.90 3.49E-03 4.25E-04
50 2146.73 4.42E+00 5.74 3.46E-03 4.25E-04
51 2614.03 7.60E+0l 17.44 3.36E-03 4.25E-04
M = First peak in a multiplet region
m = other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000 sigma
0267
4/17/2018 7:44:46AM Page 10 of29
Analysis Report for 1803111-04
AC-SED-11
BACKGROUND SUBTRACT REPORT
Peak Analysis Performed on : 4/17/2018 7:44:38AM
Env. Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063825.CN F
Peak Energy Original Orig. Area Ambient Backgr. Subtracted Subtracted
No. (keV) Area Uncertainty Background Uncert. Area Uncert.
1 47.12 l.17E+02 73.24 2.91E+0l 5.55E+00 8.79E+0l 7.34E+0l
2 63.71 7.41E+0l 59.28 2.20E+0l 9.99E+00 5.20E+0l 6.0lE+0l
3 76.81 7.49E+02 125.00 7.49E+02 l.25E+02
4 87.06 l.33E+02 81. 26 l.33E+02 8.13E+0l
5 92.98 2.12E+02 79.17 5.03E+0l 8.08E+00 l.62E+02 7. 96E+0l
6 186.24 l.41E+02 59.66 4.04E+0l 9.60E+00 l.00E+02 6.04E+0l
7 239.51 6.69E+02 85.20 l.86E+0l l.03E+0l 6.50E+02 8.58E+0l
8 269.77 5.70E+0l 50.83 5.70E+0l 5.08E+01
M 9 295.30 2.54E+02 44.30 8.49E+00 5.60E+00 2.46E+02 4.47E+01
m 10 300.11 3.17E+0l 37.03 3.17E+0l 3.70E+0l
11 328.20 3.79E+0l 34.66 3.79E+0l 3.47E+0l
12 339.04 l.14E+02 54.03 l.14E+02 5.40E+0l
13 352.16 3.05E+02 50.69 l.76E+0l 5.14E+00 2.88E+02 5.l0E+0l
14 384.90 2. 72E+0l 32.50 2.72E+0l 3.25E+01
15 427. 01 2.32E+0l 27. 58 2.32E+0l 2.76E+0l
16 462.09 7.30E+0l 42.15 7.30E+0l 4.22E+0l
M 17 477.47 3.89E+0l 23.63 3.89E+0l 2.36E+0l
m 18 480.28 l.62E+0l 24.05 l.62E+0l 2.40E+0l
19 511.37 l.42E+02 49.36 7.91E+0l 5.07E+00 6.33E+0l 4.96E+01
20 583.48 l.71E+02 42.43 6.66E+00 3.73E+00 l.64E+02 4.26E+0l
21 609.42 2.79E+02 43.47 l.26E+0l 6.94E+00 2.67E+02 4.40E+0l
M 22 661.89 2.92E+0l 21. 21 3.98E+00 2.76E+00 2.52E+0l 2.14E+0l
m 23 665.38 2.16E+0l 20.64 2.16E+0l 2.06E+0l
24 727. 24 3.41E+0l 24.70 3.41E+0l 2.47E+0l
25 767.85 2.81E+0l 26.30 2.81E+0l 2.63E+0l
26 794.18 2.60E+0l 26.23 2.60E+0l 2.62E+0l
27 860.05 l.84E+0l 23.58 l.84E+0l 2.36E+0l
28 883.58 l.68E+0l 21. 73 l.68E+0l 2.17E+0l
29 911.18 l.11E+02 31.10 2.63E+00 2.68E+00 l.09E+02 3.12E+0l
30 925.35 2.97E+0l 28.14 2.97E+0l 2.81E+0l
M 31 965. 2 9 l.46E+0l 17.18 l.46E+0l l.72E+0l
m 32 969.09 6.48E+0l 26.86 6.48E+0l 2.69E+0l
M 33 1078.18 l.15E+0l 6.93 l.15E+0l 6.93E+00
m 34 1082.18 l.54E+0l 17.52 l.54E+0l l.75E+0l
35 1120.57 5.27E+0l 29.58 l.l0E+00 2.71E+00 5.16E+0l 2.97E+0l
36 1238.93 4.85E+0l 30.15 4.85E+0l 3.02E+0l
37 1262.15 l.06E+0l 9. 96 l.06E+0l 9. 96E+00
38 1334. 92 3.70E+0l 21.63 3.70E+0l 2.16E+0l
39 1460.72 4.82E+02 48.58 7.43E+00 2.27E+00 4.74E+02 4.86E+0l
40 1560.68 8.50E+00 9.62 8.50E+00 9.62E+00
41 1582.32 9.00E+00 7.87 9.00E+00 7.87E+00
M 42 1587.31 l.31E+0l 7.37 l.31E+0l 7.37E+00
m 43 1590.31 l.l0E+0l 11. 50 l.l0E+0l l.15E+0l
m 44 1593.00 l.40E+0l 10.21 l.40E+0l l.02E+0l
0268
4/17/2018 7:44:46AM Page 11 of29
Analysis Report for 1803111-04
AC-SED-11
Peak Energy No. (keV)
45 1764.32 46 1848.86 47 1873.12 48 1939.70 49 2086.60 so 2146.73 51 2614.03
Original Area
4.56E+Ol 1.32E+01 9.18E+OO 8.00E+OO 6.00E+OO 4.42E+00 7.60E+Ol
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
Orig. Area Uncertainty
17.51 8. 96 7.75 5.66 4.90 5.74
17.44
Ambient Background
2.32E+OO
4.72E+OO
Backgr. Uncert.
1.91E+OO
1.41E+OO
AREA CORRECTION REPORT
Subtracted Area
4.33E+Ol 1.32E+Ol 9.18E+OO 8.00E+OO 6.00E+OO 4.42E+OO 7.13E+Ol
REFERENCE PEAK I 8KG. SUBTRACT
Peak Analysis Performed on : 4/17/2018 7:44:38AM
Ref. Peak Energy : 0.00 Reference Date
Peak Ratio : 0.00 Uncertainty : 0,00
Background File : \\OR-GAMMA 1 \ApexRoot\Countroom\Data\0000063825.CNF
Corrected Area is: Original * Peak Ratio - Background
Peak Energy Original Orig. Area Ambient Backgr. Corrected
No. (keV) Area Uncertainty Background Uncert. Area
1 47.12 1.17E+02 73.24 2.91E+Ol S.SSE+OO 8.79E+Ol
2 63.71 7.41E+Ol 59.28 2.20E+Ol 9.99E+OO S.20E+Ol
3 76.81 7.49E+02 125.00 7.49E+02
4 87.06 1.33E+02 81. 26 1.33E+02
s 92.98 2.12E+02 79.17 S.03E+Ol 8.08E+OO 1.62E+02
6 186.24 1.41E+02 59.66 4.04E+Ol 9.60E+OO 1.00E+02
7 239.51 6.69E+02 85.20 1.86E+Ol 1.03E+Ol 6.SOE+02
8 269.77 S.70E+Ol 50.83 S.70E+Ol
M 9 295.30 2.54E+02 44.30 8.49E+OO S.60E+OO 2.46E+02
m 10 300.11 3.17E+Ol 37.03 3.17E+Ol
11 328.20 3.79E+Ol 34.66 3.79E+Ol
12 339.04 1.14E+02 54.03 l.14E+02
13 352.16 3.0SE+02 50.69 1.76E+Ol S.14E+OO 2.88E+02
14 384.90 2. 72E+Ol 32.50 2.72E+Ol
15 427.01 2.32E+Ol 27.58 2.32E+Ol
16 462.09 7.30E+Ol 42.15 7.30E+Ol
M 17 477.47 3.89E+Ol 23.63 3.89E+Ol
m 18 480.28 1.62E+Ol 24.05 1.62E+Ol
19 511.37 1.42E+02 49.36 7.91E+Ol S.07E+OO 6.33E+Ol
20 583.48 1.71E+02 42.43 6.66E+OO 3.73E+OO 1.64E+02
21 609.42 2.79E+02 43.47 1.26E+Ol 6.94E+OO 2.67E+02
Subtracted Uncert.
1.76E+Ol 8. 96E-1-00 7.7SE+OO S.66E+OO 4.90E+OO S.74E+OO 1.7SE+Ol
Corrected Uncert.
7.34E+Ol 6.0lE+Ol 1.2SE+02 8.13E+Ol 7. 96E+Ol 6.04E+Ol 8.58E+Ol S.08E+Ol 4.47E+Ol 3.70E+Ol 3.47E+Ol S.40E+Ol S.lOE+Ol 3.2SE+Ol 2.76E+Ol 4.22E+Ol 2.36E+Ol 2.40E+Ol 4.96E+Ol 4.26E+Ol 4.40E+Ol
0269
4/17/2018 7:44:46AM Page 12 of29
Analysis Report for 1803111-04
AC-SED-11
Peak Energy Original Orig. Area Ambient Backgr. Corrected
No. (keV) Area Uncertainty Background Uncert. Area
M 22 661.89 2.92E+Ol 21. 21 3.98E+OO 2.76E+OO 2.52E+Ol
m 23 665.38 2.16E+Ol 20.64 2.16E+Ol
24 727.24 3.41E+Ol 24.70 3.41E+Ol
25 767.85 2.81E+Ol 26.30 2.81E+Ol
26 794.18 2.60E+Ol 26.23 2.60E+Ol
27 860.05 l.84E+Ol 23.58 l.84E+Ol
28 883.58 l.68E+Ol 21.73 l.68E+Ol
29 911.18 1. 11E+02 31.10 2.63E+OO 2.68E+OO l.09E+02
30 925.35 2.97E+Ol 28.14 2.97E+Ol
M 31 965. 2 9 l.46E+Ol 17.18 l.46E+Ol
m 32 969.09 6.48E+Ol 26.86 6.48E+Ol
M 33 1078.18 l.15E+Ol 6.93 l.15E+Ol
m 34 1082.18 l.54E+Ol 17.52 l.54E+Ol
35 1120.57 5.27E+Ol 29.58 l.lOE+OO 2.71E+OO 5.16E+Ol
36 1238.93 4.85E+Ol 30.15 4.85E+Ol
37 1262.15 l.06E+Ol 9. 96 l.06E+Ol
38 1334. 92 3.70E+Ol 21.63 3.70E+Ol
39 1460.72 4.82E+02 48.58 7.43E+OO 2.27E+OO 4.74E+02
40 1560.68 8.50E+OO 9.62 8.50E+OO
41 1582.32 9.00E+OO 7.87 9.00E+OO
M 42 1587.31 l.31E+Ol 7.37 l.31E+Ol
m 43 1590.31 l.lOE+Ol 11. 50 l.lOE+Ol
m 44 1593.00 l.40E+Ol 10.21 l.40E+Ol
45 1764.32 4.56E+Ol 17.51 2.32E+OO l.91E+OO 4.33E+Ol
46 1848.86 l.32E+Ol 8. 96 l.32E+Ol
47 1873.12 9.18E+OO 7.75 9.18E+OO
48 1939.70 8.00E+OO 5.66 8.00E+OO
49 2086.60 6.00E+OO 4.90 6.00E+OO
50 2146.73 4.42E+OO 5.74 4.42E+OO
51 2614.03 7.60E+Ol 17.44 4.72E+OO l.41E+OO 7.13E+Ol
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used
Nuclide Name
BE-7
: \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Id Confidence Energy (keV) Yield(%)
0.997 477.59 * 10.42
Activity
(pCi/grams)
8.30E-Ol
Corrected Uncert.
2.14E+Ol 2.06E+Ol 2.47E+Ol 2.63E+Ol 2.62E+Ol 2.36E+Ol 2.17E+Ol 3.12E+Ol 2.81E+Ol 1. 72E+Ol 2.69E+Ol 6.93E+OO l.75E+Ol 2.97E+Ol 3.02E+Ol 9.96E+OO 2.16E+Ol 4.86E+Ol 9.62E+OO 7.87E+OO 7.37E+OO l.15E+Ol l.02E+Ol l.76E+Ol 8.96E+OO 7.75E+OO 5.66E+OO 4.90E+OO 5.74E+00 l.75E+Ol
Activity
Uncertainty
5.26E-01
0270
4/17/2018 7:44:46AM
Analysis Report for 1803111-04
AC-SED-11
Nuclide Name Id Confidence Energy (keV) Yield(%) Activity
(pCilgrams)
K-40 0.999 1460.81 * 10.67 l.68E+0l
GA-67 0.659 93.31 * 35.70 9.08E+0l
208.95 2.24 300.22 * 16.00 6.61E+0l
CD-109 0.860 88.03 * 3.72 2.46E+00
SN-126 0. 960 87.57 * 37.00 2.38E-01
CS-137 0.991 661.65 * 85.12 6.08E-02
EU-155 0.329 86.50 * 30.90 2.88E-01
105.30 20.70
TL-208 0. 960 583.14 * 30.22 l.00E+00
860.37 * 4.48 l.05E+00
2614.66 * 35.85 9.33E-01
PB-210 0.940 46.50 * 4.25 2.0lE+00
BI-212 0.763 727. 17 * 11.80 6.42E-01
1620.62 2.75
PB-212 0.892 238.63 * 44.60 l.37E+00
300.09 * 3.41 l.02E+00
BI-214 0.924 609.31 * 46.30 l.l0E+00
1120.29 * 15.10 l.07E+00
1764.49 * 15.80 l.15E+00
2204.22 4.98
PB-214 0.994 295.21 * 19.19 l.39E+00
351.92 * 37.19 9.54E-0l
RA-226 1.000 186.21 * 3.28 2.47E+00
AC-228 0.982 338.32 * 11. 40 l.20E+00
911. 07 * 27.70 l.05E+00
969. 11 * 16.60 l.l0E+00
TH-234 0. 972 63.29 * 3.80 l.0lE+00
NP-237 0.951 86.50 * 12.60 6.98E-01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
UNIDENTIFIED PEAKS
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (ke V)
: 4/17/2018 7:44:38AM
: 1 : 4096
Peak Size (CPS) Peak CPS(%)
Uncertainty
Peak Type
Page 13 of29
Activity
Uncertainty
2.31E+00 4.54E+0l
7.81E+0l l.52E+00 l.46E-01 5. 21E-02 1. 77E-01
2.97E-01 l.36E+00 2.58E-01 l.69E+00 4.72E-01
2.67E-0l l.20E+00 2.32E-01 6. 31E-01 4.87E-0l
3.39E-0l 2.43E-01 l.52E+00 6.07E-01 3.67E-01 4. 96E-01 l.16E+00 4.30E-01
Tolerance
Nuclide
0271
Analysis Report for 1803111-04
m
m
M M m
M m m
AC-SED-11
Peak No. Energy (keV)
3 76.81 8 269.77
11 328.20 14 384.90 15 427.01 16 462.09 18 480.28 19 511.37 23 665.38
25 767.85 26 794.18 28 883.58 30 925.35 31 965. 2 9 33 1078.18 34 1082.18 36 1238.93 37 1262.15 38 1334.92 40 1560.68 41 1582.32 42 1587.31 43 1590.31 44 1593.00 46 1848.86 47 1873.12 48 1939.70 49 2086.60 50 2146.73
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 7:44:46AM
Peak Size (CPS) Peak CPS(%) Peak
Uncertainty Type
2.08073E-01 8.34 l.58224E-02 44.62
l.05364E-02 45.68 Tol.
7.56944E-03 59.63 6.43072E-03 59.57 Sum
2. 02778E-02 28.87
4. 50231E-03 74.18
l.75959E-02 39.16
6.00885E-03 47.71 Tol.
7.81893E-03 46.71 7.22222E-03 50.44 4.65278E-03 64.85 Sum
8.26389E-03 47.30
4.04624E-03 58.98
3.19991E-03 30.07
4.28806E-03 56.75 l.34583E-02 31.12 2.94935E-03 46.91 1. 027 78E-02 29.23 2.36111E-03 56.57
2.50000E-03 43.74
3.64469E-03 28.07 Sum
3.06760E-03 52.07
3.88818E-03 36.47 D-Esc
3.67593E-03 33.85
2.55051E-03 42.18
2.22222E-03 35.36
l.66667E-03 40.82 l.22685E-03 65.03
NUCLIDE IDENTIFICATION REPORT
Nuclide Library Used : \\OR-GAMMA 1\ApexRoot\Countroom\Library\TMA2.NLB
IDENTIFIED NUCLIDES
Page 14 of 29
Tolerance
Nuclide
LA-140
SB-126 CE-143
0272
4/17/2018 7:44:46AM Page 15 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Id Energy Yield(%) Activity Activity
Name Confidence (keV) (pCi/grams) Uncertainty
BE-7 0.99 477.59 * 10.42 8.30E-01 5.26E-01
K-40 0.99 1460.81 * 10.67 1.68E+0l 2.31E+00
GA-67 0.65 93.31 * 35.70 9.08E+0l 4.54E+0l
208.95 2.24 300.22 * 16.00 6.61E+0l 7. 81E+0l
CD-109 0.86 88.03 * 3.72 2.46E+00 1.52E+00
SN-126 0. 96 87.57 * 37.00 2.38E-01 1.46E-01
CS-137 0.99 661.65 * 85.12 6.08E-02 5.21E-02
EU-155 0.32 86.50 * 30.90 2.88E-01 1.77E-01
105.30 20.70
TL-208 0. 96 583.14 * 30.22 1.00E+00 2.97E-01
860.37 * 4.48 1.05E+00 1.36E+00
2614.66 * 35.85 9.33E-01 2.58E-01
PB-210 0.94 46.50 * 4.25 2.0lE+00 1.69E+00
BI-212 0.76 727.17 * 11. 80 6.42E-01 4. 72E-01
1620.62 2.75
PB-212 0.89 238.63 * 44.60 1.37E+00 2.67E-01
300.09 * 3.41 1.02E+00 1.20E+00
BI-214 0.92 609.31 * 46.30 l.l0E+00 2.32E-01
1120.29 * 15.10 1.07E+00 6.31E-01
1764.49 * 15.80 1.15E+00 4.87E-01
2204.22 4.98
PB-214 0.99 295.21 * 19.19 1.39E+00 3.39E-01
351.92 * 37.19 9.54E-01 2.43E-01
RA-226 1. 00 186.21 * 3.28 2.47E+00 1.52E+00
AC-228 0.98 338.32 * 11. 40 l.20E+00 6.07E-01
911. 07 * 27.70 1.05E+00 3.67E-01
969.11 * 16.60 1.l0E+00 4.96E-01
TH-234 0.97 63.29 * 3.80 1.0lE+00 1.16E+00
NP-237 0.95 86.50 * 12.60 6.98E-01 4.30E-01
* = Energy line found in the spectrum.
- = Manually added nuclide.
? = Manually edited nuclide.
@ = Energy line not used for Weighted Mean Activity
Energy Tolerance : 1.000 keV
Nuclide confidence index threshold = 0.30
Errors quoted at 2.000sigma
INTERFERENCE CORRECTED REPORT
0273
Analysis Report for 1803111-04
AC-SED-11
Nuclide Name
BE-7 K-40 GA-67
? CD-109 ? SN-126
CS-137 ? EU-155
TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RA-226 AC-228 TH-234
? NP-237
Nuclide Id
Confidence
0.997 0.999 0.659 0.860 0. 960 0.991 0.329 0. 960 0.940 0.763 0.892 0.924 0.994 1.000 0.982 0. 972 0.951
? nuclide is part of an undetermined solution
X = nuclide rejected by the interference analysis
4/17/2018 7:44:46AM
Wt mean Wt mean
Activity Activity
(pCi/grams) Uncertainty
8.30E-01 5.26E-01 1.68E+0l 2.31E+00 6.31E+0l 3.94E+0l 2.46E+00 1.52E+00 2.38E-01 1.46E-01 6.08E-02 5.21E-02 2.88E-01 1.77E-01 9.65E-01 1.93E-01 2. 0lE+00 1.69E+00 6.42E-01 4. 72E-01 1.31E+00 2.62E-01 1. llE+00 1.99E-01 1.l0E+00 1.98E-01 2.47E+00 1.52E+00 1.09E+00 2.66E-01 1.0lE+00 1.16E+00 6.98E-01 4.30E-0l
@ = nuclide contains energy lines not used in Weighted Mean Activity
Errors quoted at 2.000sigma
Page 16 of29
Comments
0274
Analysis Report for 1803111-04
m
m
M
M
m
M
m m
AC-SED-11
Peak Locate Performed on
Peak Locate From Channel
Peak Locate To Channel
Peak No. Energy (ke V)
3 76.81
8 269.77
11 328.20
14 384.90
15 427.01
16 462.09
18 480.28
19 511.37
23 665.38
25 767.85
26 794.18
28 883.58
30 925.35
31 965. 2 9
33 1078.18
34 1082.18
36 1238.93
37 1262.15
38 1334.92
40 1560.68
41 1582.32
42 1587.31
43 1590.31
44 1593.00
46 1848.86
47 1873.12
48 1939.70
49 2086.60
so 2146.73
4/17/2018 7:44:46AM
UNIDENTIFIED PEAKS
: 4/17/2018 7:44:38AM
: 1 : 4096
Peak Size (CPS)
2.08073E-01
1.58224E-02
1.05364E-02
7.56944E-03
6. 43072E-03
2.02778E-02
4.50231E-03
1.75959E-02
6.00885E-03
7.81893E-03
7.22222E-03
4.65278E-03
8.26389E-03
4.04624E-03
3 .19991E-03
4.28806E-03
1.34583E-02
2.94935E-03
1. 027 7 8E-02
2. 36111E-03
2.SOOOOE-03
3.64469E-03
3.06760E-03
3.88818E-03
3.67593E-03
2.SSOSlE-03
2.22222E-03
1.66667E-03
1.22685E-03
Peak CPS(%) Peak
Uncertainty Type
8.34 44.62
45.68 Tol.
59.63 59.57 Sum
28.87 74.18
39.16
47.71 Tol.
46.71
50.44
64.85 Sum
47.30
58.98
30.07 56.75
31.12 46.91
29.23 56.57 43.74
28.07 Sum
52.07
36.47 D-Esc
33.85 42.18
35.36
40.82
65.03
Page 17 of29
Tolerance Nuclide
LA-140
SB-126
CE-143
0275
Analysis Report for 1803111-04
AC-SED-11
M = First peak in a multiplet region
m = Other peak in a multiplet region
F = Fitted singlet
Errors quoted at 2.000sigma
4/17/2018 7:44:46AM
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA 1 \ApexRoot\Countroom\Library\TMA2.NLB
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi!grams) (pCi/grams)
+ BE-7 477.59 * 10.42 8.30E-01 1.35E+00 1.35E+00
+ NA-22 1274.54 99.94 1.23E-02 9.64E-02 9.64E-02
+ NA-24 1368.53 99.99 3.74E-02 3.45E-02 8.54E-02
2754.09 99.86 -1. 72E-02 3.45E-02
+ AL-26 1808.65 99.76 -4.57E-02 5.60E-02 5.60E-02
+ K-40 1460.81 * 10.67 1.68E+0l 1.36E+00 1.36E+00
+ @ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26
+ TI-44 67.88 94.40 -1.46E-02 7.14E-02 7.14E-02
78.34 96. 00 9.77E-02 9.80E-02
+ SC-46 889.25 98.98 -1.83E-02 9.87E-02 9.87E-02
1120.51 99.90 2.36E-01 1.84E-01
+ V-48 983.52 99.98 l.29E-01 2.80E-01 2.87E-01
1312.10 97.50 4.76E-02 2.80E-01
+ CR-51 320.08 9.83 -2.07E-01 1.14E+00 l.14E+00
+ MN-54 834.83 99.97 1.54E-02 1.0lE-01 1.0lE-01
+ CO-56 846.75 99. 96 1.64E-03 1.0lE-01 1.0lE-01
1037.75 14.03 -8.16E-02 7.16E-01
1238.25 67.00 1.84E-01 2.59E-01
1771.40 15.51 -2. 96E-02 5.00E-01
2587.48 16.90 -3.62E-02 3.36E-01
+ CO-57 122.06 85.51 1.59E-02 6.68E-02 6.68E-02
136.48 10.60 -6.16E-02 5.68E-01
+ CO-58 810.76 99.40 -2. 96E-02 9.24E-02 9.24E-02
+ FE-59 1099.22 56.50 -5.62E-02 2.31E-01 2.31E-01
1291.56 43.20 5. llE-02 3.30E-01
+ CO-60 1173.22 100.00 -4.98E-02 9.54E-02 9.54E-02
1332.49 100.00 6.57E-02 1.06E-01
+ ZN-65 1115.52 50.75 1.37E-02 2.14E-01 2.14E-01
+ GA-67 93.31 * 35.70 9.08E+0l 7. llE+0l 7. llE+0l
208.95 2.24 3.74E+02 8.08E+02
300.22 * 16.00 6.61E+0l 2.24E+02
+ SE-75 121.11 16.70 -1.23E-01 1.l0E-01 3.68E-01
Page 18 of29
0276
4/17/2018 7:44:46AM Page 19 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCilgrams) (pCi/grams)
SE-75 136.00 59.50 -1.20E-02 1.l0E-01 1.l0E-01
264.65 59.80 1.75E-02 1.l0E-01
279.53 25.20 -2.90E-02 2.53E-01
400.65 11. 40 5.03E-02 6.30E-01
+ RB-82 776.52 13.00 -2.60E-01 1.27E+00 1.27E+00
+ RB-83 520.41 46.00 1.12E-02 1.66E-01 1.66E-01
529.64 30.30 -7.69E-02 2.40E-01
552.65 16.40 3.0lE-01 5.06E-01
+ KR-85 513.99 0.43 -8.18E+00 1.74E+0l 1.74E+0l
+ SR-85 513.99 99.27 -4.75E-02 1.0lE-01 1.0lE-01
+ Y-88 898.02 93.40 -5. llE-02 8.58E-02 1.07E-01
1836.01 99.38 2.32E-02 8.58E-02
+ MO-93 263.06 56. 72 2.16E-02 6.14E-02 1.0lE-01
684.67 99.68 -1.59E-02 7.15E-02
1477.11 99.08 -1.84E-02 6.14E-02
+ NB-93M 16.57 9.43 0.00E+00 1.28E+00 1.28E+00
+ NB-94 702.63 100.00 2.25E-03 7.38E-02 8.93E-02
871.10 100.00 -3.21E-02 7.38E-02
+ NB-95 765.79 99.81 -7.35E-03 1.72E-01 1. 72E-01
+ NB-95M 235.69 25.00 -4.02E+02 4.25E+0l 4.25E+0l
+ ZR-95 724.18 43.70 3.04E-02 l.96E-01 3.04E-01
756.72 55.30 -l.09E-02 1.96E-01
+ MO-99 181.06 6.20 -1.63E+02 5.21E+02 7.93E+02
739.58 12.80 3.l0E+0l 5.21E+02
778.00 4.50 -4.80E+0l 1.58E+03
+ TC-99M 140.51 89.00 -1.39E-02 5.89E-02 5.89E-02
+ RU-103 497.08 89.00 -5.85E-02 9.92E-02 9.92E-02
+ RU-106 621.84 9.80 4.98E-0l 8.65E-01 8.65E-01
+ AG-108M 433.93 89.90 3.52E-02 6.54E-02 6.54E-02
614.37 90.40 -1.22E-01 7.53E-02
722.95 90.50 2.23E-02 9.61E-02
+ CD-109 88.03 * 3. 72 2.46E+00 2.42E+00 2.42E+00
+ AG-ll0M 657.75 93.14 2.62E-03 8.42E-02 8.42E-02
677.61 10.53 2.43E-02 7.84E-01
706.67 16.46 9.70E-02 5.87E-01
763.93 21.98 -2.74E-03 4.33E-01
884.67 21.98 1.13E-01 4.25E-01
1384.27 23.94 9.70E-02 4.12E-01
+ CD-113M 263.70 0.02 5.34E+0l 2.49E+02 2.49E+02
+ SN-113 255.12 1. 93 -4.19E-01 1.07E-01 3.35E+00
391.69 64.90 5.l0E-03 l.07E-01
+ TE-123M 159.00 84.10 2.97E-02 7.39E-02 7.39E-02
+ SB-124 602.71 97.8'7 -1.05E-02 9.33E-02 9.33E-02
645.85 7.26 2.61E-03 1.44E+00
722.78 11.10 2.48E-01 1.07E+00
1691.02 49.00 5.21E-02 2.24E-01
+ I-125 35.49 6.49 2.62E-01 1.93E+00 1.93E+00
+ SB-125 176.33 6.89 1.33E-01 2.05E-01 7.95E-01
0277
4/17/2018 7:44:46AM Pago 20 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA
Name (keV) (pCi!grams) (pCi!grams) (pCilgrams)
SB-125 427.89 29.33 1.25E-01 2.05E-01 2.05E-01
463.38 10.35 3.95E-01 7.05E-01
600.56 17.80 -1.29E-01 3.48E-01
635.90 11. 32 2.41E-01 7.24E-01
+ SB-126 414.70 83.30 -2.23E-02 6.41E-02 6.41E-02
666.33 99.60 -l.31E-02 8.03E-02
695.00 99.60 2.42E-02 9.00E-02
720.50 53.80 2.59E-02 1.58E-01
+ SN-126 87.57 * 37.00 2.38E-01 2.33E-01 2.33E-0l
+ SB-127 473.00 25.00 -2.66E+0l 2.53E+0l 2.85E+0l
685.00 35.70 -5.63E+00 2.53E+0l
783.80 14.70 5.62E+0l 7.74E+0l
+ I-129 29.78 57.00 1.53E-01 2.41E-01 2.41E-01
33.60 13.20 7.87E-02 7.77E-01
39.58 7.52 9.99E-02 9.87E-01
+ I-131 284.30 6.05 1.24E+00 7.99E-01 9.21E+00
364.48 81.20 3.28E-02 7.99E-01
636.97 7.26 3.44E+00 1.14E+0l
722.89 1. 80 1.14E+0l 4.92E+0l
+ TE-132 49.72 13.10 -l.51E+02 2.05E+0l 1.34E+02
228.16 88.00 -3.l0E+00 2.05E+01
+ BA-133 81.00 33.00 -8.25E-01 1.00E-01 1.81E-01
302.84 17.80 5.22E-02 3.44E-01
356.01 60.00 3.59E-02 1.00E-01
+ I-133 529.87 86.30 -4.86E+07 1.51E+08 1.51E+08
+ XE-133 81.00 38.00 -2.50E+0l 5.50E+00 5.50E+00
+ CS-134 563.23 8.38 2.77E-02 7.81E-02 8.l0E-01
569.32 15.43 -3.0lE-02 4.48E-01
604.70 97.60 5.72E-03 7.81E-02
795.84 85.40 7.30E-02 l.22E-01
801.93 8.73 l.03E-01 1.07E+00
+ CS-135 268.24 16.00 6. llE-02 3.99E-01 3.99E-01
+ @ I-135 1131.51 22.50 1.00E+26 1. 00E+2 6 1.00E+26
@ 1260.41 28.60 l.00E+26 1.00E+26
@ 1678.03 9.54 1.00E+26 1.00E+26
+ CS-136 153.22 7.46 1.llE+00 3.26E-01 3.17E+00
163.89 4.61 -2.14E-01 4.73E+00
176.55 13.56 2.74E-01 1.64E+00
273. 65 12.66 3.00E-01 1.95E+00
340.57 48.50 1.06E+00 6.73E-01
818.50 99.70 1.83E-01 3.26E-01
1048.07 79.60 -2.42E-02 4.50E-01
1235.34 19.70 1.13E-01 2.55E+00
+ CS-137 661.65 * 85.12 6.08E-02 1.l0E-01 1.l0E-01
+ LA-138 788.74 34.00 -1.41E-01 1.07E-01 2.27E-01
1435.80 66.00 2.89E-02 l.07E-01
+ CE-139 165.85 80.35 6.51E-03 7.89E-02 7.89E-02
+ BA-140 162. 64 6.70 -3.46E+00 1.14E+00 3.21E+00
304.84 4.50 1.36E+00 5. llE+00
0278
4/17/2018 7:44:46AM Page 21 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(¾) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi!grams)
BA-140 423.70 3.20 -1.llE+00 1.14E+00 7.53E+00
437.55 2.00 -l.92E+00 1.18E+01
537.32 25.00 9.16E-02 1.14E+00
+ LA-140 328.77 20.50 7.77E-01 3.39E-01 1.34E+00
487.03 45.50 6.83E-02 5.74E-01
815.85 23.50 1.08E-01 1.42E+00
1596.49 95.49 2.70E-02 3.39E-01
+ CE-141 145.44 48.40 5.61E-02 2.05E-01 2.05E-01
+ CE-143 57.36 11. 80 -1.08E+05 1.67E+05 4.47E+05
293.26 42.00 2.02E+05 1.67E+05
664.55 5.20 1.32E+06 1.43E+06
+ CE-144 133.54 10.80 -1.36E-01 5.55E-01 5.55E-01
+ PM-144 476.78 42.00 1.14E-01 7.96E-02 1.82E-01
618.01 98.60 -1.55E-02 7. 96E-02
696. 4 9 99.49 l.93E-02 9.31E-02
+ PM-145 36.85 21. 70 1.09E-01 2.l0E-01 3.95E-01
37.36 39.70 5.80E-02 2.l0E-01
42.30 15.10 -5.19E-02 4.47E-01
72. 40 2.31 -1.34E-01 2.96E+00
+ PM-146 453.90 39.94 1.99E-02 1.56E-01 1.56E-01
735.90 14.01 -1.57E-01 5.07E-01
747.13 13.10 2.23E-02 5.88E-01
+ ND-147 91.11 28.90 -l.51E+00 1.37E+00 1.37E+00
531.02 13.10 -1.62E-01 2.57E+00
+ PM-149 285.90 3.10 -2.89E+03 7.99E+03 7.99E+03
+ EU-152 121.78 20.50 6.20E-02 2.61E-01 2.61E-01
244.69 5.40 -1. 96E-01 1.30E+00
344.27 19.13 -5.62E-02 2.68E-01
778.89 9.10 -1.32E-01 9.15E-01
964.01 10.40 -1.17E-01 9.79E-01
1085.78 7.22 2.60E-01 1.39E+00
1112.02 9.60 1.72E-01 1.06E+00
1407.95 14.94 1.62E-01 5.30E-01
+ GD-153 97.43 31.30 2.57E-03 1.86E-01 1.86E-01
103.18 22.20 -2. llE-01 2.49E-01
+ EU-154 123.07 40.50 6.24E-02 1.34E-01 1.34E-01
723.30 19.70 4.75E-02 4.70E-01
873.19 11. 50 -l.24E-01 6.65E-01
996.32 10.30 -8.68E-01 7.28E-01
1004.76 1 7. 90 -4.04E-02 5.l0E-01
1274.45 35.50 3.43E-02 2.68E-01
+ EU-155 86.50 * 30.90 2.88E-01 2.54E-01 2.82E-01
105.30 20.70 -7.34E-02 2.54E-01
+ EU-156 811.77 10.40 -2.85E-01 2.35E+00 2.35E+00
1153.47 7.20 2.34E+00 5.12E+00
1230.71 8.90 1.60E+00 4. llE+00
+ HO-166M 184.41 72. 60 6.24E-02 9.45E-02 9.45E-02
280.45 29.60 -8.49E-02 1.83E-01
410.94 11.10 2.18E-01 5.42E-01
0279
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Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCi/grams) (pCi/grams) (pCi/grams)
HO-166M 711.69 54.10 -9 .16E-03 9.45E-02 1.55E-01
+ TM-171 66. 72 0.14 1.68E+0l 5.25E+0l 5.25E+0l
+ HF-172 67.35 5.31 9.16E-01 4.68E-01 1.31E+00
125.82 11. 30 -5.40E-01 4.68E-01
+ LU-1 72 181.53 20.60 -9.02E-01 2.39E+00 4.39E+00
900. 72 29.81 1.98E+00 5.08E+00
1093.66 62.50 3.77E-02 2.39E+00
+ LU-173 100.72 5.24 9.84E-01 3.12E-01 1.09E+00
272.11 21.20 9.55E-02 3.12E-01
+ HF-175 343.40 84.00 1.85E-02 8.53E-02 8.53E-02
+ LU-176 88.34 13. 30 5.59E-0l 5.99E-02 5.54E-01
201.83 86.00 -3.05E-02 6.47E-02
306.78 94.00 3.98E-02 5.99E-02
+ HF-181 133.02 41.70 -5.llE-02 1.06E-01 2.09E-01
345.85 17.20 1.45E-02 4.60E-01
482.03 82.80 -2.02E-02 1.06E-01
+ TA-182 67.75 41.20 -3.93E-02 1.93E-01 1.93E-0l
1121.30 34.90 5.llE-01 4.92E-01
1189.05 16.23 -2.86E-01 6.72E-01
1221.41 26.98 -1. 72E-01 4.42E-01
1231.02 11. 44 4.30E-01 1.l0E+00
+ IR-192 308.46 29.68 -9.27E-02 1.52E-01 2.25E-01
468.07 48.10 1.04E-02 1.52E-01
+ HG-203 279.19 77.30 -1.21E-02 1.05E-01 1.05E-01
+ TL-204 374.74 94 .11 -1.39E-03 5.95E-02 5.95E-02
899.15 99.16 -2.l0E-02 8.98E-02
911.74 91.10 3.27E-01 1.70E-01
+ BI-207 569.67 97. 72 -4.64E-03 6.91E-02 6.91E-02
1063.62 74.90 -1.03E-02 1.22E-01
+ TL-208 583.14 * 30.22 1.00E+00 1.34E-01 3.59E-01
860.37 * 4.48 1.05E+00 2.21E+00
2614.66 * 35.85 9.33E-01 1.34E-01
+ BI-210M 262.00 45.00 3.55E-02 1.27E-01 1.27E-01
300.00 23.00 2.57E-01 2.74E-01
+ PB-210 46.50 * 4.25 2.0lE+00 2.74E+00 2.74E+00
+ PB-211 404.84 2.90 1.08E+00 2.20E+00 2.20E+00
831.96 2.90 -8.08E-01 3.02E+00
+ BI-212 727.17 * 11.80 6.42E-01 7.25E-01 7.25E-01
1620.62 2.75 1.51E+00 3.21E+00
+ PB-212 238.63 * 44.60 1.37E+00 2.45E-01 2.45E-01
300.09 * 3.41 1.02E+00 3.45E+00
+ BI-214 609.31 * 46.30 1.l0E+00 2.12E-01 2.12E-01
1120.29 * 15.10 1.07E+00 9.48E-01
1764.49 * 15.80 1.15E+00 5.86E-01
2204.22 4.98 1.20E+00 2.12E+00
+ PB-214 295.21 * 19.19 1.39E+00 2.16E-01 6.00E-01
351.92 * 37.19 9.54E-01 2.16E-01
+ RN-219 401.80 6.50 -7.43E-02 9.63E-01 9.63E-01
0280
4/17/2018 7:44:46AM Page 23 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%) Activity Nuclide MDA Line MDA
Name (keV) (pCilgrams) (pCilgrams) (pCilgrams)
+ RA-223 323.87 3.88 6.43E-01 1.43E+00 1.43E+00
+ RA-224 240.98 3.95 6.00E+00 2.80E+00 2.80E+00
+ RA-225 40.00 31.00 -3.61E-0l 7.94E-01 7.94E-01
+ RA-226 186.21 * 3.28 2.47E+00 2.38E+00 2.38E+00
+ TH-227 50.10 8.40 l.45E-01 6.87E-01 6.87E-01
236.00 11. 50 -3.0lE+00 7.63E-01
256.20 6.30 -l.12E-01 8.75E-01
+ AC-228 338.32 * 11. 40 l.20E+00 3.95E-01 8.86E-01
911.07 * 27.70 1.05E+00 3.95E-01
969 .11 * 16.60 1.l0E+00 9.40E-01
+ TH-230 48.43 16.90 4.75E-01 4.21E-01 4.21E-01
62.85 4.60 1.21E+00 1.60E+00
67.67 0.37 1.28E+0l 1.82E+0l
+ PA-231 283.67 1. 60 8. 72E-01 2.65E+00 3.46E+00
302.67 2.30 4.02E-01 2.65E+00
+ TH-231 25.64 14.70 0.00E+00 7.27E-02 7.27E-02
84.21 6.40 -1.99E+00 9.74E-01
+ PA-233 311.98 38.60 9.88E-03 2.76E-01 2.76E-01
+ PA-234 131. 20 20.40 1.llE-01 2.84E-01 2.84E-01
733.99 8.80 2.59E-01 8.08E-01
946.00 12.00 -l.44E-01 7.12E-01
+ PA-234M 1001.03 0.92 7.83E-0l 9.35E+00 9.35E+00
+ TH-234 63.29 * 3.80 1.0lE+00 l.91E+00 1.91E+00
+ U-235 143.76 10.50 -5.22E-01 4.93E-01 4.93E-01
163.35 4.70 -l.60E-01 1.09E+00
205.31 4.70 -2.36E-01 1.20E+00
+ NP-237 86.50 * 12.60 6.98E-01 6.85E-01 6.85E-01
+ NP-239 106.10 22.70 2.18E+02 6.52E+02 6.52E+02
228.18 10.70 -2.29E+02 1.51E+03
277.60 14.10 -l.84E+02 l.09E+03
+ AM-241 59.54 35.90 -2. 96E-03 l.93E-01 1.93E-01
+ AM-243 74.67 66.00 -4.79E-0l l.30E-01 1.30E-01
+ CM-243 209.75 3.29 8.38E-01 3.98E-01 1.81E+00
228.14 10.60 -8.40E-02 5.55E-01
277.60 14.00 -6.74E-02 3.98E-01
+ = Nuclide identified during the nuclide identification
* = Energy line found in the spectrum
> = MDA value not calculated
@ = Half-life too short to be able to perform the decay correction
? = CAUTION: MDA value is inconsistent with Currie MDA at 95% confidence level
0281
4/17/2018 7:44:46AM Page 24 of 29
Analysis Report for 1803111-04
AC-SED-11
NUCLIDE MDA REPORT
Nuclide Library Used : \\OR-GAMMA1\ApexRoot\Countroom\Library\TMA2.NLB
Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCilgrams) (pCi!grams) (pCi/grams)
+ BE-7 477.59 * 10.42 1.35E+00 1.35E+00 8.30E-0l 6.47E-01
NA-22 1274.54 99.94 9.64E-02 9.64E-02 1.23E-02 4.34E-02
NA-24 1368.53 99.99 8.54E-02 3.45E-02 3.74E-02 3.78E-02
2754.09 99.86 3.45E-02 -1.72E-02 1.09E-02
AL-26 1808.65 99.76 5.60E-02 5.60E-02 -4.57E-02 2.22E-02
+ K-40 1460.81 * 10.67 1.36E+00 1.36E+00 1.68E+0l 6.32E-01
@ AR-41 1293.64 99.16 1.00E+26 1.00E+26 1.00E+26 1.00E+20
TI-44 67.88 94.40 7.14E-02 7.14E-02 -1.46E-02 3.47E-02
78.34 96. 00 9.80E-02 9.77E-02 4.80E-02
SC-46 889.25 98.98 9.87E-02 9.87E-02 -1.83E-02 4.49E-02
1120. 51 99.90 1.84E-01 2.36E-01 8.68E-02
V-48 983.52 99.98 2.87E-01 2.80E-01 1.29E-01 1.31E-01
1312.10 97.50 2.80E-01 4.76E-02 1.24E-01
CR-51 320.08 9.83 1.14E+00 1.14E+00 -2.07E-01 5.38E-01
MN-54 834.83 99.97 1.0lE-01 1.0lE-01 1.54E-02 4.68E-02
CO-56 846.75 99. 96 1.0lE-01 1.0lE-01 1.64E-03 4.59E-02
1037.75 14.03 7.16E-01 -8.16E-02 3.21E-01
1238.25 67.00 2.59E-01 1.84E-01 1.21E-01
1771.40 15.51 5.00E-01 -2. 96E-02 2.02E-01
2587.48 16.90 3.36E-01 -3.62E-02 1.19E-01
CO-57 122.06 85.51 6.68E-02 6.68E-02 1.59E-02 3.22E-02
136.48 10.60 5.68E-01 -6.16E-02 2.74E-01
CO-58 810.76 99.40 9.24E-02 9.24E-02 -2. 96E-02 4.19E-02
FE-59 1099.22 56.50 2.31E-01 2.31E-01 -5.62E-02 1.04E-01
1291.56 43.20 3.30E-01 5. llE-02 l.48E-01
CO-60 1173.22 100.00 9.54E-02 9.54E-02 -4.98E-02 4.33E-02
1332.49 100.00 1.06E-01 6.57E-02 4.81E-02
ZN-65 1115.52 50.75 2.14E-01 2.14E-01 l.37E-02 9.81E-02
+ GA-67 93.31 * 35.70 7.llE+0l 7.llE+0l 9.08E+0l 3.48E+0l
208.95 2.24 8.08E+02 3.74E+02 3.88E+02
300.22 * 16.00 2.24E+02 6.61E+0l 1.09E+02
SE-75 121.11 16.70 3.68E-01 1.l0E-01 -l.23E-01 1.78E-01
136.00 59.50 1.l0E-01 -l.20E-02 5.33E-02
264.65 59.80 1.l0E-01 1.75E-02 5.26E-02
279.53 25.20 2.53E-01 -2.90E-02 1. 20E-01
400.65 11.40 6.30E-01 5.03E-02 2. 96E-01
RB-82 776.52 13.00 1.27E+00 1. 27E+00 -2.60E-01 5.84E-01
RB-83 520.41 46.00 1.66E-01 1.66E-01 1.12E-02 7.69E-02
529.64 30.30 2.40E-01 -7.69E-02 1.l0E-01
552.65 16.40 5.06E-01 3.0lE-01 2.35E-01
KR-85 513.99 0.43 1.74E+0l 1.74E+0l -8.18E+00 8.17E+00
SR-85 513.99 99.27 1.0lE-01 1.0lE-01 -4.75E-02 4.74E-02
0282
4/17/2018 7:44:46AM Page 25 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi/grams) (pCilgrams) (pCilgrams) (pCilgrams)
Y-88 898.02 93.40 l.07E-01 8.58E-02 -5. llE-02 4.90E-02
1836.01 99.38 8.58E-02 2.32E-02 3.59E-02
MO-93 263.06 56. 72 l.0lE-01 6.14E-02 2.16E-02 4.80E-02
684.67 99.68 7.15E-02 -l.59E-02 3.29E-02
14Tl.ll 99.08 6.14E-02 -l.84E-02 2.54E-02
NB-93M 16.57 9.43 l.28E+00 l.28E+00 0.00E+00 0.00E+00
NB-94 702.63 100.00 8.93E-02 7.38E-02 2.25E-03 4.17E-02
871.10 100.00 7.38E-02 -3.21E-02 3.34E-02
NB-95 765.79 99.81 1. 72E-01 l.72E-01 -7.35E-03 8.08E-02
NB-95M 235.69 25.00 4.25E+0l 4.25E+0l -4.02E+02 2.04E+0l
ZR-95 724.18 43.70 3.04E-01 l.96E-01 3.04E-02 l.43E-01
756.72 55.30 1. 96E-01 -l.09E-02 9.05E-02
MO-99 181.06 6.20 7.93E+02 5. 21E+02 -l.63E+02 3.81E+02
739.58 12.80 5. 21E+02 3.l0E+0l 2.39E+02
778.00 4.50 l.58E+03 -4.80E+0l 7.26E+02
TC-99M 140.51 89.00 5.89E-02 5.89E-02 -l.39E-02 2.84E-02
RU-103 497.08 89.00 9.92E-02 9.92E-02 -5.85E-02 4.56E-02
RU-106 621.84 9.80 8.65E-01 8.65E-01 4.98E-01 4.04E-01
AG-108M 433.93 89.90 6.54E-02 6.54E-02 3.52E-02 3.05E-02
614.37 90.40 7.53E-02 -l.22E-01 3.48E-02
722.95 90.50 9.61E-02 2.23E-02 4.48E-02
+ CD-109 88.03 * 3.72 2.42E+00 2.42E+00 2.46E+00 l.18E+00
AG-ll0M 657.75 93.14 8.42E-02 8.42E-02 2.62E-03 3.89E-02
677.61 10.53 7.84E-01 2.43E-02 3.63E-01
706.67 16.46 5.87E-01 9.70E-02 2.74E-01
763.93 21.98 4.33E-01 -2.74E-03 2.0lE-01
884.67 21. 98 4.25E-01 l.13E-01 l.95E-01
1384.27 23.94 4.12E-01 9.70E-02 l.84E-01
CD-113M 263.70 0.02 2.49E+02 2.49E+02 5.34E+0l l.18E+02
SN-113 255.12 1. 93 3.35E+00 l.07E-01 -4.19E-01 l.59E+00
391.69 64.90 l.07E-01 5.l0E-03 5.0lE-02
TE-123M 159.00 84.10 7.39E-02 7.39E-02 2.97E-02 3.56E-02
SB-124 602.71 97.87 9.33E-02 9.33E-02 -l.05E-02 4. 31E-02
645.85 7.26 l.44E+00 2.61E-03 6.69E-01
722. 7 8 11.10 l.07E+00 2.48E-01 4.97E-01
1691.02 49.00 2.24E-01 5.21E-02 9.62E-02
I-125 35.49 6.49 l.93E+00 l.93E+00 2.62E-01 9.20E-01
SB-125 176.33 6.89 7.95E-01 2.05E-01 l.33E-01 3.82E-01
427.89 29.33 2.05E-01 l.25E-01 9.56E-02
463.38 10.35 7.05E-01 3.95E-01 3.32E-01
600.56 17.80 3.48E-01 -l.29E-01 l.59E-01
635.90 11. 32 7.24E-01 2.41E-01 3.38E-01
SB-126 414.70 83.30 6.41E-02 6.41E-02 -2.23E-02 2.98E-02
666.33 99.60 8.03E-02 -l.31E-02 3.74E-02
695.00 99.60 9.00E-02 2.42E-02 4.21E-02
720.50 53.80 l.58E-01 2.59E-02 7.32E-02
+ SN-126 87.57 * 37.00 2.33E-01 2.33E-01 2.38E-01 l.14E-01
SB-127 473.00 25.00 2.85E+0l 2.53E+0l -2.66E+0l l.32E+0l
685.00 35.70 2.53E+0l -5.63E+00 l.16E+0l
783.80 14.70 7.74E+0l 5.62E+0l 3.60E+0l
I-129 29.78 57.00 2.41E-01 2.41E-0l l.53E-01 l.15E-01
33.60 13. 20 7.77E-01 7.87E-02 3.70E-01
39.58 7.52 9.87E-01 9.99E-02 4.70E-01
0283
4/17/2018 7:44:46AM Page 26 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi!grams) (pCi!grams) (pCi/grams) (pCi/grams)
I-131 284.30 6.05 9.21E+00 7.99E-01 1.24E+00 4.37E+00
364.48 81.20 7.99E-01 3.28E-02 3. 78E-01
636.97 7.26 1.14E+0l 3.44E+00 5.31E+00
722.89 1. 80 4.92E+0l 1.14E+0l 2.29E+0l
TE-132 4 9. 72 13.10 1.34E+02 2.05E+0l -1. 51E+02 6.39E+0l
228.16 88.00 2.05E+0l -3.l0E+00 9.82E+00
BA-133 81.00 33.00 1.81E-01 1.00E-01 -8.25E-01 8.79E-02
302.84 17.80 3.44E-01 5.22E-02 1.64E-01
356.01 60.00 1.00E-01 3.59E-02 4. 72E-02
I-133 529.87 86.30 1.51E+08 1.51E+08 -4.86E+07 6.97E+07
XE-133 81.00 38.00 5.50E+00 5.50E+00 -2.50E+0l 2.67E+00
CS-134 563.23 8.38 8.l0E-01 7.81E-02 2.77E-02 3.75E-01
569.32 15.43 4.48E-01 -3.0lE-02 2.08E-01
604.70 97.60 7.81E-02 5. 72E-03 3.63E-02
795.84 85.40 l.22E-01 7.30E-02 5.71E-02
801.93 8.73 1.07E+00 1.03E-01 4.97E-01
CS-135 268.24 16.00 3.99E-01 3.99E-01 6. llE-02 1.91E-01
@ I-135 1131.51 22.50 1.00E+26 1.00E+26 1.00E+26 1.00E+20
@ 1260.41 28.60 1.00E+26 1.00E+26 1.00E+20
@ 1678.03 9.54 1.00E+26 1.00E+26 1.00E+20
CS-136 153.22 7.46 3.17E+00 3.26E-01 1. llE+00 1.53E+00
163.89 4.61 4.73E+00 -2.14E-01 2.28E+00
176.55 13.56 1.64E+00 2.74E-01 7.87E-01
273.65 12.66 1.95E+00 3.00E-01 9.27E-01
340.57 48.50 6.73E-01 l.06E+00 3.23E-01
818.50 99.70 3.26E-01 1.83E-01 1.49E-01
1048.07 79.60 4.50E-01 -2.42E-02 2.04E-01
1235.34 19.70 2.55E+00 1.13E-01 1.18E+00
+ CS-137 661.65 * 85.12 1.l0E-01 1.l0E-01 6.08E-02 5.18E-02
LA-138 788.74 34.00 2.27E-01 1.07E-01 -1.41E-01 1.04E-01
1435.80 66.00 1.07E-01 2.89E-02 4.57E-02
CE-139 165.85 80.35 7.89E-02 7.89E-02 6.51E-03 3.80E-02
BA-140 162.64 6.70 3.21E+00 1.14E+00 -3.46E+00 1.54E+00
304.84 4.50 5.llE+00 1.36E+00 2.41E+00
423.70 3.20 7.53E+00 -1. llE+00 3.51E+00
437.55 2.00 1.18E+0l -1.92E+00 5.47E+00
537.32 25.00 1.14E+00 9.16E-02 5.31E-01
LA-140 328.77 20.50 1.34E+00 3.39E-01 7.77E-01 6.36E-01
487.03 45.50 5.74E-01 6.83E-02 2.67E-01
815.85 23.50 1.42E+00 1.08E-01 6.50E-01
1596.49 95.49 3.39E-01 2.70E-02 l.45E-01
CE-141 145.44 48.40 2.05E-01 2.05E-01 5.61E-02 9.90E-02
CE-143 57.36 11. 80 4.47E+05 1.67E+05 -1.08E+05 2.16E+05
293.26 42.00 1.67E+05 2.02E+05 8.10E+04
664.55 5.20 l.43E+06 l.32E+06 6. 72E+05
CE-144 133.54 10.80 5.55E-01 5.55E-01 -1.36E-01 2.68E-01
PM-144 476.78 42.00 1.82E-01 7. 96E-02 1.14E-01 8.56E-02
618.01 98.60 7. 96E-02 -1.55E-02 3.70E-02
696.49 99.49 9.31E-02 l.93E-02 4.35E-02
PM-145 36.85 21.70 3.95E-01 2.l0E-01 1.09E-01 1.88E-01
37.36 39.70 2.l0E-01 5.80E-02 1.00E-01
42.30 15.10 4.47E-01 -5.19E-02 2.14E-01
72. 40 2.31 2.96E+00 -1.34E-01 1.44E+00
0284
4/17/2018 7:44:46AM Page 27 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(¾) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCi!grams) (pCi!grams) (pCi!grams) (pCi/grams)
PM-146 453.90 39.94 1.56E-01 1.56E-01 1.99E-02 7.29E-02
735.90 14.01 5.07E-01 -1.57E-01 2.32E-01
747.13 13.10 5.88E-01 2.23E-02 2.70E-01
ND-147 91.11 28.90 1.37E+00 1.37E+00 -1.51E+00 6.67E-01
531.02 13.10 2.57E+00 -1.62E-01 1.19E+00
PM-149 285.90 3.10 7.99E+03 7.99E+03 -2.89E+03 3.78E+03
EU-152 121.78 20.50 2.61E-01 2.61E-01 6.20E-02 l.26E-01
244.69 5.40 1.30E+00 -1.96E-01 6.24E-01
344.27 19.13 2.68E-01 -5.62E-02 1.26E-01
778.89 9.10 9.15E-01 -1.32E-01 4.23E-01
964.01 10.40 9.79E-01 -1.17E-01 4.53E-01
1085.78 7.22 1.39E+00 2.60E-01 6.36E-01
1112.02 9.60 1.06E+00 1.72E-01 4.87E-01
1407.95 14.94 5.30E-01 1.62E-01 2.31E-01
GD-153 97.43 31.30 1.86E-01 1.86E-01 2.57E-03 9.00E-02
103.18 22.20 2.49E-01 -2.llE-01 1.20E-01
EU-154 123.07 40.50 1.34E-01 1.34E-01 6.24E-02 6.45E-02
723. 30 19.70 4.70E-01 4.75E-02 2.20E-01
873.19 11. 50 6.65E-01 -1.24E-01 3.02E-01
996.32 10.30 7.28E-01 -8.68E-01 3.26E-01
1004.76 17.90 5.l0E-01 -4.04E-02 2.33E-01
1274.45 35.50 2.68E-01 3.43E-02 1.21E-01
+ EU-155 86.50 * 30.90 2.82E-01 2.54E-01 2.88E-01 1.38E-01
105.30 20.70 2.54E-01 -7.34E-02 1.23E-01
EU-156 811.77 10.40 2.35E+00 2.35E+00 -2.85E-01 1.07E+00
1153.47 7.20 5.12E+00 2.34E+00 2.35E+00
1230.71 8.90 4.llE+00 1.60E+00 l.88E+00
HO-166M 184.41 72. 60 9.45E-02 9.45E-02 6.24E-02 4.58E-02
280.45 29.60 1.83E-01 -8.49E-02 8.68E-02
410.94 11.10 5.42E-01 2.18E-01 2.54E-01
711.69 54.10 1.55E-01 -9.16E-03 7.21E-02
TM-171 66. 72 0.14 5.25E+0l 5.25E+0l 1.68E+0l 2.55E+0l
HF-172 67.35 5.31 1.31E+00 4.68E-01 9.16E-01 6.36E-01
125.82 11. 30 4.68E-01 -5.40E-01 2.25E-01
LU-1 72 181.53 20.60 4.39E+00 2.39E+00 -9.02E-01 2. llE+00
900. 72 29.81 5.08E+00 1.98E+00 2.34E+00
1093.66 62.50 2.39E+00 3.77E-02 1.09E+00
LU-173 100.72 5.24 1.09E+00 3.12E-01 9.84E-01 5.25E-01
272.11 21.20 3.12E-01 9.55E-02 1.49E-01
HF-175 343.40 84.00 8.53E-02 8.53E-02 1.85E-02 4.0lE-02
LU-176 88.34 13.30 5.54E-01 5.99E-02 5.59E-01 2.70E-01
201.83 86.00 6.47E-02 -3.05E-02 3.l0E-02
306.78 94.00 5.99E-02 3.98E-02 2.84E-02
HF-181 133.02 41.70 2.09E-01 1.06E-01 -5. llE-02 1.0lE-01
345.85 17.20 4.60E-01 l.45E-02 2.15E-01
482.03 82.80 1.06E-01 -2.02E-02 4. 92E-02
TA-182 67.75 41.20 1.93E-01 1.93E-01 -3.93E-02 9.35E-02
1121.30 34.90 4. 92E-01 5.llE-01 2.32E-01
1189.05 16.23 6. 72E-01 -2.86E-01 3.04E-01
1221.41 26.98 4.42E-01 -1.72E-01 2.0lE-01
1231.02 11. 44 1.l0E+00 4.30E-01 5.04E-01
IR-192 308.46 29.68 2.25E-01 1.52E-01 -9.27E-02 1.06E-01
468.07 48.10 1.52E-01 l.04E-02 7.05E-02
0285
4/17/2018 7:44:46AM Page 28 of29
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%) Line MDA Nuclide MDA Activity Dec. Level
Name (keV) (pCilgrams) (pCilgrams) (pCilgrams) (pCi/grams)
HG-203 279.19 77.30 l.05E-01 l.05E-01 -l.21E-02 4.99E-02
TL-204 374.74 94 .11 5.95E-02 5.95E-02 -l.39E-03 2.79E-02
899.15 99.16 8.98E-02 -2.l0E-02 4.13E-02
911. 7 4 91.10 l.70E-01 3.27E-01 8.08E-02
BI-207 569.67 97.72 6.91E-02 6.91E-02 -4.64E-03 3.20E-02
1063.62 74.90 l.22E-01 -l.03E-02 5.56E-02
+ TL-208 583.14 * 30.22 3.59E-01 l.34E-01 l.00E+00 l.71E-01
860.37 * 4.48 2.21E+00 l.05E+00 l.03E+00
2614.66 * 35.85 l.34E-01 9.33E-01 4.92E-02
BI-210M 262.00 45.00 l.27E-01 l.27E-01 3.55E-02 6.07E-02
300.00 23.00 2.74E-01 2.57E-01 l.31E-01
+ PB-210 46.50 * 4.25 2.74E+00 2.74E+00 2.0lE+00 l.34E+00
PB-211 404.84 2.90 2.20E+00 2.20E+00 l.08E+00 l.03E+00
831. 96 2.90 3.02E+00 -8.08E-01 l.39E+00
+ BI-212 727.17 * 11. 80 7.25E-01 7.25E-01 6.42E-01 3.37E-01
1620.62 2.75 3.21E+00 l.51E+00 l.41E+00
+ PB-212 238.63 * 44.60 2.45E-01 2.45E-01 l.37E+00 l.19E-01
300.09 * 3.41 3.45E+00 l.02E+00 l.68E+00
+ BI-214 609.31 * 46.30 2.12E-01 2.12E-01 l.l0E+00 l.0lE-01
1120.29 * 15.10 9.48E-01 l.07E+00 4.46E-01
1764.49 * 15.80 5.86E-01 l.15E+00 2.57E-01
2204.22 4.98 2.12E+00 l.20E+00 9.34E-01
+ PB-214 295.21 * 19.19 6.00E-01 2.16E-01 l.39E+00 2.92E-01
351.92 * 37.19 2.16E-01 9.54E-01 l.04E-01
RN-219 401.80 6.50 9.63E-01 9.63E-01 -7.43E-02 4.53E-01
RA-223 323.87 3.88 l.43E+00 l.43E+00 6.43E-01 6.73E-01
RA-224 240.98 3.95 2.80E+00 2.80E+00 6.00E+00 l.37E+00
RA-225 40.00 31.00 7.94E-01 7.94E-01 -3.61E-01 3.78E-01
+ RA-226 186.21 * 3.28 2.38E+00 2.38E+00 2.47E+00 l.15E+00
TH-227 50.10 8.40 6.87E-01 6.87E-01 l.45E-01 3.29E-01
236.00 11. 50 7.63E-01 -3.0lE+00 3.70E-01
256.20 6.30 8.75E-01 -l.12E-01 4.16E-01
+ AC-228 338.32 * 11.40 8.86E-0l 3.95E-01 l.20E+00 4.29E-01
911.07 * 27. 70 3.95E-01 l.05E+00 l.84E-01
969 .11 * 16.60 9.40E-01 l.l0E+00 4.47E-01
TH-230 48.43 16.90 4.21E-01 4.21E-01 4.75E-01 2.03E-01
62.85 4.60 l.60E+00 l.21E+00 7.76E-01
67. 67 0.37 l.82E+0l l.28E+0l 8.86E+00
PA-231 283.67 1. 60 3.46E+00 2.65E+00 8. 72E-01 l.64E+00
302.67 2.30 2.65E+00 4.02E-01 l.26E+00
TH-231 25.64 14.70 7. 27E-02 7. 27E-02 0.00E+00 0.00E+00
84.21 6.40 9.74E-01 -l.99E+00 4.73E-01
PA-233 311.98 38.60 2.76E-01 2.76E-01 9.88E-03 1. 30E-01
PA-234 131.20 20.40 2.84E-01 2.84E-01 l. llE-01 l.37E-01
733.99 8.80 8.08E-01 2.59E-01 3.70E-01
946.00 12.00 7.12E-01 -l.44E-01 3.25E-01
PA-234M 1001.03 0.92 9.35E+00 9.35E+00 7.83E-01 4.25E+00
+ TH-234 63.29 * 3.80 l.91E+00 l.91E+00 l.0lE+00 9.27E-01
U-235 143.76 10.50 4.93E-01 4.93E-01 -5.22E-01 2.37E-01
163.35 4.70 l.09E+00 -l.60E-01 5.25E-01
205.31 4.70 l.20E+00 -2.36E-01 5.78E-01
+ NP-237 86.50 * 12.60 6.85E-01 6.85E-01 6.98E-01 3.35E-01
NP-239 106.10 22.70 6.52E+02 6.52E+02 2.18E+02 3.15E+02
0286
Analysis Report for 1803111-04
AC-SED-11
Nuclide Energy Yield(%)
Name (keV)
NP-239 228.18 10.70 277. 60 14.10
AM-241 59.54 35.90
AM-243 74.67 66.00
CM-243 209.75 3.29 228.14 10.60 277.60 14.00
+ = Nuclide identified during the nuclide identification
= Energy line found in the spectrum
> = MDA value not calculated
Line MDA
(pCi/grams)
1.51E+03 1.09E+03 1.93E-01 1.30E-01 1.81E+00 5.55E-01 3.98E-01
@ = Half-life too short to be able to perform the decay correction
No Action Level results available for reporting purposes.
4/17/2018 7:44:46AM
Nuclide MDA Activity
(pCi/grams) (pCi/grams)
6.52E+02 -2.29E+02 -1.84E+02
1.93E-01 -2. 96E-03 1.30E-01 -4.79E-01 3.98E-01 8.38E-01
-8.40E-02 -6.74E-02
DATA REVIEW COMMENTS REPORT
Creation Date Comment User
No Data Review Comments Entered.
Page 29 of 29
Dec. Level
(pCi/grams)
7.25E+02 5.16E+02 9.34E-02 6.34E-02 8.70E-01 2.66E-01 1.89E-01
0287
Channel Data Report 4/17/2018 7:45:09 AM Page 1
*******************************************************
***** S P E C T R A L D A T A R E P O R T *****
*******************************************************
Sample Title: AC-SED-11
Elapsed Live time: 3600 Elapsed Real Time: 3601
Channell------1-------1-------1-------I-------I-------I-------I-------I
1: 0 0 0 0 0 0 0 0
9: 0 0 0 0 0 0 0 0
17: 0 0 0 0 0 0 0 0
25: 0 0 0 15 47 46 39 40
33: 44 54 47 41 45 58 40 45
41: 46 49 53 58 47 75 126 49
49: 71 46 56 55 59 62 60 53
57: 59 62 81 71 79 66 99 120
65: 66 71 85 95 77 65 93 83
73: 83 103 300 127 364 241 66 70
81: 78 62 70 90 91 73 143 152
89: 70 112 85 98 167 112 59 52
97: 54 55 71 64 49 61 39 51
105: 60 66 52 56 60 59 55 59
113: 46 48 52 50 55 57 51 44
121: 57 45 62 57 48 48 43 46
129: 68 76 49 61 47 58 64 48
137: 61 45 63 47 40 39 44 50
145: 51 70 45 54 46 51 53 45
153: 47 56 61 44 50 39 57 38
161: 33 34 44 38 48 44 49 47
169: 44 47 54 35 34 49 45 28
177: 31 47 40 45 44 37 44 47
185: 46 142 61 39 33 42 40 35
193: 45 27 37 35 25 39 40 40
201: 34 35 37 38 45 45 22 43
209: 59 46 32 26 41 25 33 40
217: 38 40 26 43 38 38 33 31
225: 35 29 40 33 42 33 39 36
233: 34 37 39 33 37 242 337 51
241: 78 105 37 23 41 24 31 25
249: 27 28 24 26 29 24 21 35
257: 23 29 27 26 27 31 32 23
265: 23 24 34 28 33 49 39 25
273: 22 29 27 24 26 30 13 24
281: 21 24 28 23 19 18 21 26
289: 23 17 19 24 24 78 157 78
297: 17 25 33 40 28 13 17 30
305: 19 17 18 22 13 18 23 24
313: 10 17 21 16 16 17 20 18
321: 22 25 27 15 15 12 28 39
329: 25 20 21 21 25 19 17 22
337: 35 72 40 28 23 21 9 18
345: 13 11 20 19 13 22 105 214
353: 42 13 18 25 23 16 18 13
361: 16 20 22 12 26 25 24 15
0288
Channel Data Report 4/17/2018 7:45:09 AM Page 2
369: 12 17 15 11 13 20 18 12
Sample Title: AC-SED-11
Channel[------[-------[-------[-------[-------[-------[-------[-------[
377: 15 14 15 19 12 11 20 21
385: 18 22 13 9 17 18 18 15
393: 11 19 15 15 13 15 11 22
401: 19 16 18 20 16 18 9 17
409: 19 20 12 8 17 6 16 11
417: 10 16 13 20 13 17 6 13
425: 13 12 17 17 9 2 14 9
433: 14 18 6 19 11 8 12 8
441: 12 20 15 4 13 8 14 15
449: 15 19 11 14 12 11 20 6
457: 12 16 18 15 10 23 33 16
465: 8 14 7 11 12 10 10 10
473: 8 14 9 10 32 23 12 17
481: 9 12 8 5 6 12 9 16
489: 15 9 20 3 10 16 9 9
4 97: 8 13 6 13 13 14 14 11
505: 11 10 10 15 26 47 58 37
513: 11 16 6 13 9 9 14 9
521: 9 12 14 5 11 10 9 10
529: 7 12 8 16 8 10 13 15
537: 9 10 12 9 16 12 5 6
545: 9 7 14 4 6 13 13 11
553: 11 9 8 8 6 8 11 9
561: 7 8 15 12 12 11 11 14
569: 10 11 9 15 8 10 18 10
577: 10 9 10 9 20 38 97 37
585: 15 8 7 6 7 10 9 5
593: 8 13 9 8 7 7 9 6
601: 8 10 10 15 14 12 17 75
609: 175 53 4 7 11 8 9 6
617: 4 10 11 7 12 15 4 10
625: 9 6 13 6 15 5 7 8
633: 12 12 9 9 11 5 9 8
641: 8 9 6 8 7 8 13 7
649: 5 12 5 10 8 8 8 7
657: 3 10 7 7 21 18 9 10
665: 16 9 4 4 8 12 9 7
673: 9 8 10 6 8 8 4 9
681: 4 10 5 6 5 9 5 7
689: 9 12 12 5 11 12 11 9
697: 11 5 9 9 8 11 17 8
705: 7 9 13 7 8 10 7 11
713: 8 8 6 8 5 8 9 8
721: 11 6 12 3 13 17 20 15
729: 5 3 7 8 3 7 5 6
737: 5 4 13 3 10 3 7 5
745: 5 9 5 4 12 4 6 8
753: 6 3 13 7 8 4 8 7
761: 8 10 4 10 6 13 10 24
769: 11 7 9 7 7 3 8 7
777: 11 6 3 8 6 7 12 8
785: 9 7 5 3 9 5 3 16
793: 5 16 13 7 7 9 7 10
0289
Channel Data Report 4/17/2018 7:45:09 AM Page 3
801: 11 5 8 7 7 7 4 4
Sample Title: AC-SED-11
Channel[------[-------l-------l-------l-------[-------1-------1-------1
809: 3 6 5 7 3 5 5 5
817: 9 5 5 5 6 1 4 4
825: 6 5 9 5 6 6 11 5
833: 9 7 11 8 7 7 10 12
841: 11 4 4 6 5 2 7 6
84 9: 6 1 5 6 11 4 6 3
857: 9 8 8 12 13 2 4 7
865: 7 3 5 6 5 2 5 4
873: 4 6 8 4 6 5 5 6
881: 3 10 10 6 7 3 4 4
889: 5 8 3 7 9 5 3 6
897: 5 7 7 6 9 6 9 5
905: 6 3 7 8 9 47 50 13
913: 3 6 2 4 6 3 3 4
921: 4 12 7 8 6 4 4 4
92 9: 10 6 2 8 10 4 7 3
937: 4 4 11 4 5 3 7 4
945: 7 6 6 4 11 4 3 4
953: 7 2 2 5 4 6 10 4
961: 7 5 10 9 13 4 16 35
969: 31 10 7 7 5 3 6 6
977: 11 5 3 6 6 7 3 3
98 5: 7 6 2 4 7 5 8 6
993: 7 2 5 4 1 5 1 10
1001: 7 5 5 3 6 5 7 6
1009: 6 8 8 4 4 10 4 4
1017: 5 2 0 8 1 2 3 6
1025: 5 7 3 3 2 6 2 5
1033: 7 3 8 5 2 4 0 3
1041: 3 3 4 1 4 6 3 10
1049: 5 3 3 9 6 2 11 6
1057: 4 5 8 5 4 3 8 6
1065: 6 3 5 4 3 7 4 5
1073: 6 4 5 0 9 6 4 4
1081: 10 7 7 2 8 4 7 6
1089: 3 4 5 5 6 6 5 3
1097: 6 4 3 5 3 4 5 3
1105: 6 7 6 6 5 5 8 5
1113: 4 8 2 6 4 11 21 30
1121: 8 9 7 2 7 5 10 4
112 9: 7 6 10 5 4 6 5 4
1137: 2 1 3 9 3 7 4 5
1145: 2 10 6 2 8 9 3 10
1153: 4 7 6 5 3 4 8 4
1161: 3 6 4 6 7 6 6 7
1169: 1 4 4 5 5 7 6 9
1177: 5 1 4 3 1 3 5 7
1185: 0 6 6 5 5 3 5 2
1193: 10 2 7 6 4 9 7 3
1201: 4 6 4 5 3 2 11 6
1209: 3 2 10 5 6 2 8 5
1217: 6 6 3 9 5 2 4 6
1225: 6 9 9 9 3 5 8 0
0290
Channel Data Report 4/17/2018 7:45:09 AM Page 4
1233 :. 5 9 7 8 14 11 10 3
Sample Title: AC-SED-11
Channell------l-------l-------l-------l-------1-------1-------1-------I
1241: 6 7 7 3 2 6 6 7
1249: 3 3 7 5 6 4 6 6
1257: 4 2 0 4 5 8 0 3
1265: 2 4 7 9 5 2 5 5
1273: 2 8 3 3 2 4 3 2
1281: 10 5 5 2 6 3 6 6
1289: 2 5 4 3 6 1 0 5
1297: 1 5 2 5 2 3 0 4
1305: 4 2 4 4 3 2 3 4
1313: 1 4 2 2 2 2 1 4
1321: 4 3 2 3 5 2 1 1
1329: 3 4 5 8 5 3 5 4
1337: 2 3 3 2 2 2 1 1
1345: 1 2 2 5 3 4 3 3
1353: 1 1 1 1 2 5 2 0
1361: 0 3 2 2 4 2 2 5
1369: 3 3 1 2 0 2 2 4
1377: 3 3 4 0 4 4 5 4
1385: 3 3 1 2 3 0 0 2
1393: 1 0 1 3 4 4 4 3
1401: 6 3 2 0 2 5 5 1
1409: 1 2 1 0 2 3 1 1
1417: 0 3 3 1 2 3 3 1
1425: 0 3 2 1 0 1 2 1
1433: 0 3 2 2 3 1 1 0
1441: 0 1 2 3 2 3 1 2
1449: 1 3 3 3 2 3 4 10
1457: 10 35 143 175 115 11 1 0
1465: 4 2 3 1 2 2 4 1
1473: 1 2 3 0 0 2 0 3
1481: 0 2 2 0 2 0 2 2
1489: 1 0 3 0 2 1 2 1
1497: 2 2 1 1 3 0 2 1
1505: 1 3 6 2 3 3 0 5
1513: 3 0 1 2 2 0 0 1
1521: 1 1 3 1 0 2 1 2
1529: 1 0 2 0 3 3 0 0
1537: 2 1 4 1 0 3 1 1
1545: 0 0 0 1 0 0 0 1
1553: 4 0 1 0 1 1 3 3
1561: 2 1 1 0 0 1 1 0
1569: 0 0 2 0 1 2 1 0
1577: 1 0 2 2 2 4 1 0
1585: 0 6 4 2 5 3 4 6
1593: 2 1 0 0 2 1 1 0
1601: 2 0 3 0 0 0 3 1
1609: 1 1 1 1 2 0 2 1
1617: 0 3 3 4 3 3 1 1
1625: 0 2 0 0 3 2 0 0
1633: 3 0 1 2 1 2 1 0
1641: 1 0 2 0 0 2 1 2
1649: 1 2 1 0 0 2 0 1
1657: 2 2 0 3 1 2 1 1
0291
Channel Data Report 4/17/2018 7:45:09 AM Page 5
1665: 2 1 1 0 1 0 1 0
Sample Title: AC-SED-11
Channel[------[-------[-------[-------[-------[-------[-------1-------1
1673: 2 2 2 2 0 1 1 1
1681: 1 0 2 1 0 3 1 1
1689: 4 3 1 2 1 2 0 0
1697: 1 2 1 3 2 0 0 0
1705: 0 0 0 1 1 3 0 1
1713: 1 2 1 0 1 1 1 1
1721: 2 0 0 1 0 0 2 1
1729: 2 2 0 2 2 0 2 1
1737: 3 1 1 0 1 2 0 0
1745: 0 0 2 1 1 2 1 0
1753: 1 2 2 1 0 1 1 2
1761: 3 6 16 17 5 1 1 1
1769: 1 0 1 1 0 0 0 1
1777: 0 1 0 1 4 0 0 0
1785: 0 0 1 1 0 1 1 1
1793: 0 0 2 2 0 1 1 0
1801: 1 0 1 1 1 0 0 0
1809: 1 0 1 3 2 1 0 1
1817: 0 0 0 1 0 0 1 1
1825: 0 1 1 0 1 0 2 1
1833: 0 0 2 1 1 0 2 0
1841: 1 0 1 0 3 0 5 3
1849: 2 1 1 0 0 0 0 0
1857: 2 1 1 1 1 0 1 0
1865: 1 0 1 0 1 1 3 3
1873: 2 1 0 0 1 0 1 1
1881: 2 2 0 2 1 1 2 3
1889: 3 2 1 0 3 0 1 1
1897: 2 1 0 0 2 0 0 1
1905: 1 0 1 3 1 0 1 2
1913: 0 0 1 3 1 0 0 1
1921: 2 0 0 2 1 0 0 0
192 9: 1 0 1 0 0 0 1 0
1937: 1 1 3 2 0 0 0 1
1945: 2 0 1 0 1 1 0 0
1953: 3 1 0 0 1 1 0 2
1961: 2 2 1 0 0 1 0 0
1969: 0 0 0 0 0 1 1 0
1977: 2 0 1 0 1 0 1 0
1985: 0 2 2 1 1 0 0 1
1993: 0 1 2 0 2 0 1 0
2001: 1 1 1 0 2 0 2 1
2009: 1 1 0 0 1 1 2 1
2017: 3 1 1 0 1 1 1 0
2025: 1 1 1 0 1 0 0 0
2033: 3 2 2 1 0 2 0 1
2041: 0 0 1 0 0 0 2 0
204 9: 0 2 0 0 1 1 1 1
2057: 1 0 0 0 0 0 3 1
2065: 2 0 2 0 0 0 0 0
2073: 0 1 0 1 1 0 2 3
2081: 0 0 0 2 1 3 0 0
2089: 1 2 2 0 0 2 0 0
0292
Channel Data Report 4/17/2018 7:45:09 AM Page 6
2097: 0 1 4 3 4 1 2 2
Sample Title: AC-SED-11
Channell------1-------1-------1-------I-------I-------I-------I-------I
2105: 3 0 2 1 1 1 0 0
2113: 1 2 2 1 0 1 1 0
2121: 1 1 1 2 0 1 0 2
2129: 1 1 0 0 2 1 2 0
2137: 2 0 0 0 1 0 0 2
2145: 1 3 0 0 0 1 0 2
2153: 0 1 0 1 1 1 2 1
2161: 0 1 2 0 1 2 0 0
2169: 1 0 1 0 0 1 2 0
2177: 1 0 1 1 3 1 0 1
2185: 0 1 0 1 0 0 1 2
2193: 0 0 1 1 0 1 2 2
2201: 5 1 2 4 0 2 1 1
2209: 0 1 0 1 0 1 0 1
2217: 0 1 0 0 0 0 1 2
2225: 0 0 1 0 0 0 2 0
2233: 0 0 3 1 0 0 1 3
2241: 0 0 1 0 0 1 0 0
2249: 0 0 0 0 0 0 1 0
2257: 0 2 2 1 1 1 0 0
2265: 1 0 0 1 1 0 1 0
2273: 1 0 1 1 1 1 0 2
2281: 0 1 0 0 1 1 0 1
2289: 1 1 0 1 2 0 2 0
2297: 0 1 0 1 0 0 1 1
2305: 1 2 0 0 2 0 1 1
2313: 1 2 1 0 0 0 1 2
2321: 0 0 0 1 1 1 2 1
2329: 1 2 0 0 1 1 1 0
2337: 1 1 1 1 3 0 2 0
2345: 2 1 2 1 1 0 0 2
2353: 1 1 0 2 0 1 0 1
2361: 0 4 1 2 0 2 1 2
2369: 0 1 0 0 2 2 0 1
2377: 1 1 0 2 0 0 1 0
2385: 0 2 1 0 0 1 0 0
2393: 0 1 0 0 0 0 0 0
2401: 2 0 0 0 0 0 1 0
2409: 1 0 0 0 0 1 1 1
2417: 1 1 1 0 1 1 0 2
2425: 0 0 0 0 1 1 0 0
2433: 0 0 0 1 0 1 1 0
2441: 1 0 1 0 1 3 1 0
2449: 1 0 0 0 0 2 0 1
2457: 1 0 1 0 0 0 0 0
2465: 0 0 0 1 1 1 0 0
2473: 2 0 1 0 0 0 0 0
2481: 0 1 1 1 0 0 0 1
2489: 0 0 0 0 0 0 0 0
2497: 0 1 0 0 1 0 0 0
2505: 0 0 0 0 0 0 0 1
2513: 0 0 0 0 1 0 1 0
2521: 0 0 1 0 1 0 1 1
0293
Channel Data Report 4/17/2018 7:45:09 AM Page 7
2529: 0 1 0 0 1 0 1 0
Sample Title: AC-SED-11
Channell------l-------1-------1-------1-------I-------I-------I-------I
2537: 1 0 0 1 0 0 0 1
2545: 3 1 1 0 0 0 0 0
2553: 0 0 0 0 0 0 0 0
2561: 0 1 2 0 0 0 1 0
2569: 1 1 0 0 0 0 1 0
2577: 1 0 0 0 1 1 0 0
2585: 0 0 0 1 0 0 0 1
2593: 0 1 0 0 1 1 1 0
2601: 1 0 1 0 0 0 0 1
2609: 6 6 9 19 18 12 5 0
2617: 0 2 0 1 0 1 0 1
262 5: 0 0 0 1 1 0 0 1
2633: 1 0 0 0 1 1 0 0
2641: 1 0 3 0 0 1 0 2
2649: 0 0 0 0 1 0 0 0
2657: 0 1 0 0 0 0 0 0
2665: 0 0 3 0 0 1 0 0
2 67 3: 0 0 0 2 0 0 0 0
2681: 0 0 0 2 0 1 0 0
2689: 0 0 0 0 1 0 0 0
2697: 0 0 0 0 0 0 0 0
2705: 0 0 1 0 0 0 0 0
2713: 0 0 0 0 0 0 0 0
2721: 0 0 1 0 0 0 0 1
2729: 0 1 0 1 1 0 0 0
2737: 0 2 2 0 0 2 0 0
2745: 0 0 0 0 0 1 0 0
2753: 0 0 0 0 1 1 0 0
27 61: 0 0 0 0 0 0 1 0
2769: 0 0 0 0 0 0 0 1
2777: 2 0 1 0 0 0 1 0
2785: 0 0 0 0 0 0 1 0
2793: 1 1 0 0 0 0 1 0
2801: 1 0 1 0 0 0 0 0
2809: 0 0 0 0 0 0 0 0
2817: 0 0 1 0 2 0 0 0
2825: 0 0 0 1 0 0 0 0
2833: 0 0 1 2 0 0 1 0
2841: 0 0 1 0 0 0 0 0
2849: 0 0 0 0 2 0 0 0
2857: 0 0 1 0 0 0 0 0
2865: 0 0 0 0 0 0 0 0
2873: 1 0 0 0 0 0 0 0
2881: 1 1 1 0 0 0 1 0
2889: 0 0 2 0 0 0 0 0
2897: 0 0 0 0 1 1 1 0
2905: 0 0 0 0 0 0 0 0
2913: 0 0 0 0 0 0 1 0
2921: 1 0 1 0 0 0 1 1
2929: 0 0 0 0 0 0 0 0
2937: 0 0 0 0 0 0 0 0
2945: 0 0 0 0 0 2 1 0
2953: 0 0 1 0 0 0 0 0
0294
Channel Data Report 4/17/2018 7:45:09 AM Page 8
2961: 0 0 0 0 0 0 0 0
Sample Title: AC-SED-11
Channell------l-------1-------1-------1-------I-------I-------I-------I
2969: 2 0 0 0 1 1 0 1
2977: 0 0 0 0 0 0 0 0
2985: 0 1 0 0 0 0 0 0
2993: 0 0 0 0 0 0 1 0
3001: 1 0 0 0 0 0 0 0
3009: 0 0 0 1 0 0 0 0
3017: 0 0 0 0 0 0 0 0
3025: 0 0 0 0 2 0 0 0
3033: 0 0 0 0 0 3 0 0
3041: 0 0 1 0 0 0 0 0
3049: 0 0 0 0 0 1 1 0
3057: 0 0 0 0 0 0 0 0
3065: 0 0 0 0 0 0 0 0
3073: 1 1 0 0 0 0 0 0
3081: 0 0 0 1 0 0 0 0
3089: 0 0 0 1 0 1 0 0
3097: 0 0 0 0 1 0 0 0
3105: 0 0 0 0 0 1 0 0
3113: 0 0 0 0 1 0 0 1
3121: 0 0 0 0 0 0 0 0
3129: 0 0 0 0 0 0 0 0
3137: 0 0 0 0 0 0 0 1
3145: 0 0 0 0 0 0 0 0
3153: 0 0 0 0 0 0 0 0
3161: 0 0 0 0 0 0 0 0
3169: 0 0 0 0 0 0 0 0
3177: 1 1 0 0 0 0 0 0
3185: 2 0 0 1 0 0 0 0
3193: 0 0 1 0 1 0 0 0
3201: 0 0 0 0 0 0 0 1
3209: 1 0 0 0 0 0 1 0
3217: 0 0 0 1 1 0 0 0
3225: 0 0 0 1 1 0 1 0
3233: 0 0 0 1 0 0 0 1
3241: 0 0 0 0 0 0 0 0
3249: 0 0 0 0 0 0 0 0
3257: 0 0 0 1 0 0 0 0
3265: 0 0 1 1 1 0 0 0
3273: 0 0 0 1 0 0 0 0
3281: 0 0 0 2 0 0 0 0
3289: 0 0 0 0 0 0 0 1
3297: 0 0 0 0 0 0 0 1
3305: 0 1 0 2 0 0 0 0
3313: 0 1 0 0 0 0 0 0
3321: 0 0 0 1 0 0 0 0
3329: 0 0 0 0 0 1 0 0
3337: 0 0 1 0 0 0 0 0
3345: 0 0 0 1 0 0 0 1
3353: 0 0 0 0 0 0 0 0
3361: 0 0 0 0 0 0 0 0
3369: 0 0 0 0 1 0 0 0
3377: 0 0 0 0 0 0 0 0
3385: 0 0 1 0 0 0 0 2
0295
Channel Data Report 4/17/2018 7:45:09 AM Page 9
3393: 0 0 1 0 0 0 0 0
Sample Title: AC-SED-11
Channell------l-------l-------l-------1-------1-------1-------I-------I
3401: 0 0 0 0 1 0 0 1
3409: 0 0 0 0 0 1 0 0
3417: 0 0 0 0 0 0 1 0
3425: 0 0 0 0 1 0 0 0
3433: 0 0 0 0 0 1 1 0
3441: 0 0 1 0 0 0 1 0
3449: 0 0 2 0 0 0 0 0
3457: 0 0 0 0 1 0 0 1
3465: 0 0 0 0 1 0 0 0
3473: 1 0 0 0 0 0 0 1
3481: 0 0 0 0 0 0 0 0
3489: 0 0 1 0 0 0 0 0
3497: 1 0 0 0 0 0 0 0
3505: 1 0 0 0 0 0 0 0
3513: 0 0 0 0 0 0 0 0
3521: 0 1 1 0 1 0 0 0
352 9: 0 0 0 1 0 0 0 0
3537: 0 0 0 0 0 0 0 0
3545: 0 0 0 1 0 0 1 0
3553: 0 0 0 0 0 0 0 0
3561: 0 0 0 0 0 0 0 0
3569: 0 0 0 0 1 0 0 0
3577: 1 0 0 0 0 0 0 1
3585: 0 0 0 0 0 0 0 0
3593: 0 0 0 0 1 0 0 0
3601: 0 0 1 0 0 1 0 0
3609: 0 0 0 0 0 1 0 0
3617: 0 1 0 0 0 0 0 1
3625: 0 0 0 1 0 0 1 0
3633: 1 0 0 0 0 0 0 0
3641: 0 0 0 0 0 0 0 0
3649: 0 1 0 0 0 0 0 0
3657: 0 1 0 0 0 0 0 0
3665: 0 0 0 0 0 0 0 0
3673: 0 0 0 0 0 1 0 1
3681: 0 0 0 0 1 1 0 0
368 9: 0 0 0 0 0 1 0 0
3697: 0 0 0 0 0 0 1 0
3705: 0 0 0 0 0 0 0 0
3713: 0 0 0 0 0 0 0 0
3721: 0 0 1 0 0 0 0 0
3729: 0 0 0 0 0 0 0 0
3737: 0 0 0 0 1 0 0 0
3745: 0 0 0 0 1 1 1 0
3753: 0 0 0 0 1 0 0 0
3761: 0 0 0 0 0 0 0 0
3769: 0 0 1 0 0 0 0 0
3777: 1 0 0 1 0 0 0 0
3785: 0 0 0 0 0 0 0 1
3793: 0 0 0 0 0 0 0 0
3801: 0 1 1 0 1 0 0 0
3809: 0 0 1 0 0 0 1 0
3817: 0 0 0 0 0 0 1 1
0296
Channel Data Report 4/17/2018 7:45:09 AM Page 10
3825: 0 0 0 0 0 1 0 0
Sample Title: AC-SED-11
Channell------l-------1-------1-------1-------I-------I-------I-------I
3833: 0 0 0 0 0 0 0 0
3841: 0 0 0 0 0 1 0 0
3849: 0 0 0 0 0 0 0 0
3857: 0 0 0 0 0 0 2 0
3865: 0 0 1 0 0 0 0 0
3873: 0 0 0 0 0 0 0 0
3881: 0 0 0 0 0 0 1 0
3889: 0 1 0 0 0 0 0 0
3897: 0 0 1 0 0 1 0 1
3905: 0 0 1 0 0 0 1 0
3913: 0 0 0 0 0 0 0 0
3921: 0 0 0 0 0 1 0 0
3929: 0 0 0 0 0 0 1 0
3937: 0 0 0 0 0 0 0 0
3945: 1 0 1 0 0 0 1 0
3953: 0 0 0 0 0 0 0 0
3961: 0 0 0 0 0 0 1 1
3969: 1 0 0 0 1 0 1 1
3977: 0 0 0 0 0 0 0 0
3985: 0 0 0 0 1 1 0 0
3993: 0 0 0 0 0 0 0 0
4001: 0 1 0 0 0 1 0 0
4009: 0 0 0 1 0 0 0 0
4017: 0 0 0 0 0 0 1 0
4025: 0 0 0 0 0 1 0 0
4033: 0 0 0 0 0 0 0 0
4041: 0 0 0 0 0 0 0 0
4049: 0 0 0 1 0 0 0 0
4057: 0 1 0 0 1 1 0 1
4065: 0 1 0 0 0 1 0 0
4073: 0 0 0 0 0 0 0 0
4081: 0 0 0 0 0 0 0 1
4089: 0 0 0 0 0 0 0 0
0297
105
104
~ 103 ro u V)
O'l 0
r--1
V) .µ s::: ~ 0 u
102
101
-= '3
';" EB a,
= ';" C, u -= ' o._
z
= _, ' z
V,
.._,_ = ~
~
.._,_
~ ~ ' "' ~ o._
lQO n ""
500
.._,_ _,
' ~ "'
co = ---' f-
co ~ ' Uco « ~
~
1000
~
.._,_ _,
' ~ "'
ROI Type: 1
!
1500
0000064641. CNF
.._,_
~
2000 channel
2500
co = ' ---' f-
Live Time :3600.000 sec Real Time :3600.830 sec Start: 1: 1. 2 (kev) stop : 4096: 4099. 2 (kev) Acq. Start :Tue Apr 17 06:44:34 2018
3000
!Im ROI Type: 2
3500 4000
0298
Last Measurement Q.A. Report 4/17/18 5:24:37 AM Page 1
**************************************************************************
***** G E N I E Q U A L I T Y A S S U R A N C E *****
**************************************************************************
Last Results Report 4/17/18 5:24:37 AM
QA File:
Detector:
\\OR-GAMMAl\ApexRoot\Countroom\QA\D000000000lB.QCK
GEl Geometry: <None> Certificate: <None> Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date: Elapsed Live Time:
QA Background Ch QA Count
1.0000E+000 4/17/18 5:09:22 4/17/18 5:09:24
900.0 seconds Elapsed Real Time:
Parameter Description [Mean+/- Std. Dev.]
900.1 seconds
Value
AM AM
DAILY BKG CT RATE GEl 2.3622E+000
[SD: 2.2718E+000+/- 1.162]
Deviation/Flags <LU: SD: UD: BS>
7.7782E-002 < >
fq) lf/(l/18
Flags Key: LU Lower/Upper Bounds Test SD Sample Driven N-Sigma Test UD = User Driven N-Sigma Test BS Measurement Bias Test
(Ab (In (In (In
Above, Be= Below) Investigate, Ac Action) Investigate, Ac Action) Investigate, Ac Action)
0299
Last Measurement Q.A. Report 4/17/18 5:24:46 AM Page 1
**************************************************************************
***** G E N I E Q U A L I T Y A S S U R A N C E *****
**************************************************************************
Last Results Report 4/17/18 5:24:46 AM
QA File:
Detector:
\\OR-GAMMAl\ApexRoot\Countroom\QA\D0000000002B.QCK
GE2 Geometry: <None> Certificate: <None> Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date: Elapsed Live Time:
QA Background Ch QA Count
l.0000E+000 4/17/18 5:09:28 4/17/18 5:09:31
900.0 seconds Elapsed Real Time:
Parameter Description [Mean+/- Std. Dev.]
900.1 seconds
Value
AM AM
Deviation/Flags < LU : SD: UD: BS>
DAILY BKG CT RATE GE2 l.8489E+000 2.9374E-002
[SD:-l.4680E+035+/-******] < >
Trend Test: The last 9 samples exhibit a bias trend.
KP cr(t,-/tB
Flags Key: LU SD UD BS
Lower/Upper Bounds Test Sample Driven N-Sigma Test User Driven N-Sigma Test Measurement Bias Test
(Ab (In = (In = (In =
Above, Be= Below) Investigate, Ac Action) Investigate, Ac Action) Investigate, Ac Action)
0300
Last Measurement Q.A. Report 4/17/18 5:41:05 AM /l f:::, Page 1 l/ Ii 1/18
**************************************************************************
***** G E N I E Q O A L I T Y A S S O R A N C E *****
**************************************************************************
Last Results Report 4/17/18 5:41:05 AM
QA File:
Detector:
\\OR-GAMMA1\ApexRoot\Countroom\QA\D0000000001GAF-16C.QCK
GEl Geometry: Certificate: Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date:
<None> GAF-16
Elapsed Live Time:
QA Calibration C QA Count
1.0000E+000 10/1/16 12:00:00 4/17/18 5:25:30
900.0 seconds Elapsed Real Time: 919.7 seconds
Value
PM AM
Deviation/Flags Parameter Description [Mean+/- Std. Dev.] < LU : SD: UD: BS>
Peak centroid 59.54 kev 5.9999E+001 Boundary Limits: [ 5.800E+001, 6.l00E+00l] < > Trend Test: The last 9 samples exhibit a bias trend.
Peak centroid 661.65 kev 6.6181E+002 Boundary Limits: [ 6. 600E+002, 6. 630E+002] < > Trend Test: The last 9 samples exhibit a bias trend.
Peak centroid 1332.49 ke 1.3324E+003 Boundary Limits: [ 1.331E+003, 1.334E+003] < >
Peak centroid 1836.01 ke 1.8358E+003 Boundary Limits: [ 1.834E+003, 1.838E+003] < >
Peak FWHM Am-241 1.5083E+000 Boundary Limits: [ 5.000E-001, 3.000E+000] < > Trend Test: The last 9 samples exhibit a bias trend.
Peak FWHM Cs-137 l.8998E+000 Boundary Limits: 5.000E-001, 3.000E+000] < >
Peak FWHM Co-60 2.3028E+000 Boundary Limits: 5.000E-001, 3.000E+000] < >
Peak FWHM Y-88 2.7380E+000 Boundary Limits: 5.000E-001, 3.000E+000] < >
Decay corrected activity 1.5191E+004 Boundary Limits: [ 1.254E-002, 1.881E-002] < > Trend Test: The last 9 samples exhibit a bias trend.
Decay corrected activity 6.4156E+003
0301
Last Measurement Q.A. Report 4/17/18 5:41:05 AM Page 2
Boundary Limits: [ 5.134E-003, 7.700E-003]
Decay corrected activity 1.0396E+004 Boundary Limits: [ 8.130E-003, 1.220E-002]
Parameter Description [Mean+/- Std. Dev.]
Value
Decay corrected activity 1.8411E+004 Boundary Limits: [ l.690E-002, 2.534E-002]
Flags Key: LU Lower/Upper Bounds Test (Ab SD Sample Driven N-Sigma Test (In UD = User Driven N-Sigma Test (In BS Measurement Bias Test (In
< >
< >
Deviation/Flags < LU : SD: UD : BS>
< >
Above, Be= Below) Investigate, Ac Action) Investigate, Ac= Action) Investigate, Ac= Action)
0302
Last Measurement Q.A. Report 4/17/18 5:41:16 AM Page 1
**************************************************************************
***** G E N I E Q U A L I T Y A S S U R A N C E *****
**************************************************************************
Last Results Report 4/17/18 5:41:16 AM
t'P t.r/11/18
QA File:
Detector:
\\OR-GAMMAl\ApexRoot\Countroom\QA\D0000000002GAS-1601C.QC
GE2 Geometry: Certificate: Sample ID: Sample Desc: Sample Quantity: Sample Date: Measurement Date:
<None> GAS-1601
Elapsed Live Time:
QA Calibration C QA Count
1.0000E+000 10/1/16 12:00:00 4/17/18 5:25:38
900.0 seconds Elapsed Real Time: 918.3 seconds
Value
PM AM
Deviation/Flags Parameter Description [Mean+/- Std. Dev.] < LU : SD: UD: BS>
Peak centroid 59.54 kev 6.0000E+00l Boundary Limits: [ 5.800E+001, 6. l00E+00l] < Trend Test: The last 9 samples exhibit a bias trend.
Peak centroid 661.65 kev 6.6128E+002 Boundary Limits: [ 6.600E+002, 6.630E+002] < Trend Test: The last 9 samples exhibit a bias trend.
Peak centroid 1332.49 ke 1.3316E+003 Boundary Limits: [ 1.331E+003, 1.334E+003] < Trend Test: The last 9 samples exhibit a bias trend.
Peak centroid 1836.01 ke 1.8349E+003 Boundary Limits: [ 1.833E+003, 1.838E+003] < Trend Test: The last 9 samples exhibit a bias trend.
Peak FWHM Am-241 1.3606E+000 Boundary Limits: 5.000E-001, 3.000E+000] < Trend Test: The last 9 samples exhibit a bias trend.
Peak FWHM Cs-137 l.9175E+000 Boundary Limits: 5.000E-001, 3.000E+000] < Trend Test: The last 9 samples exhibit a bias trend.
Peak FWHM Co-60 2.3921E+000 Boundary Limits: 5.000E-001, 3.000E+000] < Trend Test: The last 9 samples exhibit a bias trend.
Peak FWHM Y-88 Boundary Limits:
2.4231E+000 5.000E-001, 3.000E+000]
Decay corrected activity 1.4734E+005
<
>
>
>
>
>
>
>
>
0303
Last Measurement Q.A. Report 4/17/18 5:41:16 AM Page 2
Boundary Limits: [ l.190E-001, 1. 785E-001] < > Trend Test: The last 9 samples exhibit a bias trend.
Parameter Oescriptinn [Mean+/- Std. Dev.]
Vri l \JP
Decay corrected activity 6.7614E+004
Deviation/Flags < LU : SD: UD : BS>
Boundary Limits: [ 5.718E-002, 8.577E-002] < > Trend Test: The last 9 samples exhibit a bias trend.
Decay corrected activity 9.5589E+004 Boundary Limits: [ 7.706E-002, l.156E-001]
Decay corrected activity 2.1048E+005 Boundary Limits: [ l.602E-001, 2.403E-001]
Flags Key: LU= Lower/Upper Bounds Test SD= Sample Driven N-Sigma Test UD User Driven N-Sigma Test BS Measurement Bias Test
< >
< >
(Ab= Above, Be= Below) (In= Investigate, Ac Action) (In= Investigate, Ac Action) (In= Investigate, Ac Action)